#------------------------------------------------------------------------------
#$Date: 2016-03-22 12:19:30 +0200 (Tue, 22 Mar 2016) $
#$Revision: 178945 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/74/4117464.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4117464
loop_
_publ_author_name
'Sam C. K. Hau'
'Ping-Shing Cheng'
'Thomas C. W. Mak'
_publ_section_title
;
 Enlargement of Globular Silver Alkynide Cluster via Core Transformation
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              2922
_journal_page_last               2925
_journal_paper_doi               10.1021/ja211438q
_journal_volume                  134
_journal_year                    2012
_chemical_formula_sum            'C128 H197 Ag38 Cl18 O50'
_chemical_formula_weight         7273.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.796(2)
_cell_angle_beta                 116.638(2)
_cell_angle_gamma                116.1750(10)
_cell_formula_units_Z            1
_cell_length_a                   18.3988(14)
_cell_length_b                   18.6925(14)
_cell_length_c                   19.076(2)
_cell_measurement_temperature    173(2)
_cell_volume                     4928.5(8)
_computing_cell_refinement       SAINT(Bruker,2001)
_computing_data_collection       APEX2(Bruker,2003)
_computing_data_reduction        APEX2(Bruker,2003)
_computing_molecular_graphics    DIAMOND
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX II CCD diffractometer'
_diffrn_measurement_method       'φ and ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0435
_diffrn_reflns_av_sigmaI/netI    0.0312
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            88599
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.34
_exptl_absorpt_coefficient_mu    3.983
_exptl_absorpt_correction_T_max  0.5030
_exptl_absorpt_correction_T_min  0.3812
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.451
_exptl_crystal_description       block
_exptl_crystal_F_000             3457
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.823
_refine_diff_density_min         -1.107
_refine_diff_density_rms         0.151
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.108
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1046
_refine_ls_number_reflns         17850
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.108
_refine_ls_R_factor_all          0.0491
_refine_ls_R_factor_gt           0.0338
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0023P)²+45.0354P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0700
_refine_ls_wR_factor_ref         0.0799
_reflns_number_gt                14645
_reflns_number_total             17850
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja211438q_si_002_1.cif
_cod_data_source_block           1
_cod_original_cell_volume        4928.4(8)
_cod_database_code               4117464
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.47583(4) 0.33359(3) 0.52059(3) 0.03071(12) Uani 1 1 d . . .
Ag2 Ag 0.61769(4) 0.46253(3) 0.45412(3) 0.02832(11) Uani 1 1 d . . .
Ag3 Ag 0.71713(4) 0.64355(3) 0.61171(3) 0.03370(13) Uani 1 1 d . . .
Ag4 Ag 0.42604(4) 0.47874(3) 0.31318(3) 0.02993(12) Uani 1 1 d . . .
Ag5 Ag 0.41285(4) 0.24917(3) 0.62579(3) 0.03085(12) Uani 1 1 d . . .
Ag6 Ag 0.37496(4) 0.16069(3) 0.40806(3) 0.03531(13) Uani 1 1 d . . .
Ag7 Ag 0.62387(4) 0.29460(4) 0.60077(4) 0.03437(13) Uani 1 1 d . . .
Ag8 Ag 0.83507(5) 0.47122(4) 0.73589(4) 0.04017(14) Uani 1 1 d . . .
Ag9 Ag 0.72561(4) 0.38439(3) 0.52541(3) 0.03100(12) Uani 1 1 d . . .
Ag10 Ag 0.87024(4) 0.67271(4) 0.77559(4) 0.03608(13) Uani 1 1 d . . .
Ag11 Ag 0.77178(4) 0.81360(4) 0.70937(4) 0.03667(13) Uani 1 1 d . . .
Ag12 Ag 0.87858(4) 0.75144(3) 0.59557(3) 0.03152(12) Uani 1 1 d . . .
Ag13 Ag 0.74902(4) 0.70190(4) 0.39355(3) 0.03540(13) Uani 1 1 d . . .
Ag14 Ag 0.79285(3) 0.57946(3) 0.45513(3) 0.02611(11) Uani 1 1 d . . .
Ag15 Ag 0.51138(4) 0.59882(3) 0.24262(3) 0.03080(12) Uani 1 1 d . . .
Ag16 Ag 0.24828(4) 0.45985(3) 0.18032(3) 0.03069(12) Uani 1 1 d . . .
Ag17 Ag 0.39464(4) 0.35998(3) 0.17759(3) 0.03031(12) Uani 1 1 d . . .
Ag18 Ag 0.36542(4) 0.19315(4) 0.22759(4) 0.04285(15) Uani 1 1 d . . .
Ag19 Ag 0.56755(4) 0.35973(3) 0.29333(3) 0.03154(12) Uani 1 1 d . . .
Cl1 Cl 0.42983(11) 0.35956(9) 0.37690(9) 0.0229(3) Uani 1 1 d . . .
Cl2 Cl 0.64407(10) 0.48520(9) 0.60570(9) 0.0220(3) Uani 1 1 d . . .
Cl3 Cl 0.60911(10) 0.59775(9) 0.44790(9) 0.0223(3) Uani 1 1 d . . .
O1 O 0.8564(3) 0.5733(3) 0.6330(3) 0.0336(11) Uani 1 1 d . . .
O2 O 0.9580(4) 0.5918(3) 0.5843(3) 0.0381(12) Uani 1 1 d . . .
O3 O 0.9937(4) 0.5669(3) 0.7107(3) 0.0401(12) Uani 1 1 d . . .
O4 O 1.0095(4) 0.6964(3) 0.7010(4) 0.0518(15) Uani 1 1 d . . .
Cl4 Cl 0.95623(11) 0.60741(10) 0.65782(10) 0.0266(3) Uani 1 1 d . . .
O5 O 0.7583(3) 0.8127(3) 0.5360(3) 0.0366(12) Uani 1 1 d . . .
O6 O 0.9061(4) 0.9205(4) 0.5626(4) 0.0653(19) Uani 1 1 d . . .
O7 O 0.8209(6) 0.9536(4) 0.6086(5) 0.075(2) Uani 1 1 d . . .
O8 O 0.7649(5) 0.9123(4) 0.4689(4) 0.0592(17) Uani 1 1 d . . .
Cl5 Cl 0.81594(13) 0.90196(11) 0.54649(12) 0.0369(4) Uani 1 1 d . . .
O9 O 0.6241(3) 0.5224(3) 0.2830(3) 0.0321(11) Uani 1 1 d . . .
O10 O 0.5832(5) 0.5319(4) 0.1508(4) 0.0591(17) Uani 1 1 d . . .
O11 O 0.7452(4) 0.5950(3) 0.2576(4) 0.0527(15) Uani 1 1 d . . .
O12 O 0.6451(4) 0.4466(3) 0.1981(4) 0.0451(13) Uani 1 1 d . . .
Cl6 Cl 0.64940(12) 0.52346(10) 0.22081(10) 0.0296(3) Uani 1 1 d . . .
O13 O 0.3595(4) 0.6318(3) 0.2622(3) 0.0365(12) Uani 1 1 d . . .
O14 O 0.4213(5) 0.7202(5) 0.1979(5) 0.081(2) Uani 1 1 d . . .
O15 O 0.2648(6) 0.6037(4) 0.1200(4) 0.078(2) Uani 1 1 d . . .
O16 O 0.3063(5) 0.7218(4) 0.2182(4) 0.0542(15) Uani 1 1 d . . .
Cl7 Cl 0.33648(13) 0.66990(11) 0.19846(11) 0.0348(4) Uani 1 1 d . . .
O17 O 0.6577(4) 1.2101(4) 0.4262(4) 0.0571(16) Uani 1 1 d . . .
O18 O 0.5163(5) 1.1236(3) 0.4222(4) 0.0511(15) Uani 1 1 d . . .
O19 O 0.5408(4) 1.2451(3) 0.3876(3) 0.0426(13) Uani 1 1 d . . .
O20 O 0.5104(5) 1.1272(4) 0.2976(4) 0.0622(17) Uani 1 1 d . . .
Cl8 Cl 0.55704(12) 1.17540(10) 0.38248(11) 0.0322(4) Uani 1 1 d . . .
O21 O 0.2287(4) 1.2649(3) 0.1731(3) 0.0397(12) Uani 1 1 d . . .
O22 O 0.0778(4) 1.2236(4) 0.0622(4) 0.0610(17) Uani 1 1 d . . .
O23 O 0.2038(4) 1.2616(4) 0.0416(3) 0.0611(18) Uani 1 1 d . . .
O24 O 0.1368(5) 1.1355(4) 0.0648(4) 0.0637(18) Uani 1 1 d . . .
Cl9 Cl 0.15956(12) 1.22006(11) 0.08333(11) 0.0354(4) Uani 1 1 d . . .
O25 O 0.5407(8) 0.9685(7) 0.1044(6) 0.111(3) Uiso 1 1 d . . .
C1 C 0.4663(4) 0.2202(4) 0.5483(4) 0.0227(13) Uani 1 1 d . . .
C2 C 0.4527(5) 0.1533(4) 0.5610(4) 0.0248(14) Uani 1 1 d . . .
C3 C 0.4429(5) 0.0741(4) 0.5761(5) 0.0352(17) Uani 1 1 d . . .
C4 C 0.4238(8) 0.0662(6) 0.6460(6) 0.063(3) Uani 1 1 d . . .
H4A H 0.4172 0.0147 0.6557 0.095 Uiso 1 1 calc R . .
H4B H 0.3655 0.0646 0.6299 0.095 Uiso 1 1 calc R . .
H4C H 0.4767 0.1142 0.6963 0.095 Uiso 1 1 calc R . .
C5 C 0.3616(6) -0.0018(4) 0.4957(5) 0.0424(19) Uani 1 1 d . . .
H5A H 0.3551 -0.0532 0.5056 0.064 Uiso 1 1 calc R . .
H5B H 0.3761 0.0041 0.4532 0.064 Uiso 1 1 calc R . .
H5C H 0.3024 -0.0043 0.4774 0.064 Uiso 1 1 calc R . .
C6 C 0.5402(6) 0.0825(5) 0.6042(5) 0.047(2) Uani 1 1 d . . .
H6A H 0.5372 0.0323 0.6148 0.071 Uiso 1 1 calc R . .
H6B H 0.5910 0.1314 0.6543 0.071 Uiso 1 1 calc R . .
H6C H 0.5529 0.0891 0.5607 0.071 Uiso 1 1 calc R . .
C7 C 0.7689(5) 0.3512(4) 0.6347(4) 0.0292(15) Uani 1 1 d . . .
C8 C 0.8354(5) 0.3416(4) 0.6784(4) 0.0240(14) Uani 1 1 d . . .
C9 C 0.9048(5) 0.3175(5) 0.7192(4) 0.0315(16) Uani 1 1 d . . .
C10 C 0.9336(6) 0.3316(7) 0.8101(5) 0.056(2) Uani 1 1 d . . .
H10A H 0.9795 0.3158 0.8372 0.085 Uiso 1 1 calc R . .
H10B H 0.8774 0.2973 0.8115 0.085 Uiso 1 1 calc R . .
H10C H 0.9619 0.3905 0.8388 0.085 Uiso 1 1 calc R . .
C11 C 0.9937(5) 0.3720(5) 0.7160(5) 0.0430(19) Uani 1 1 d . . .
H11A H 1.0398 0.3563 0.7428 0.065 Uiso 1 1 calc R . .
H11B H 1.0221 0.4310 0.7444 0.065 Uiso 1 1 calc R . .
H11C H 0.9749 0.3628 0.6586 0.065 Uiso 1 1 calc R . .
C12 C 0.8548(6) 0.2230(5) 0.6712(5) 0.0430(19) Uani 1 1 d . . .
H12A H 0.8984 0.2045 0.6962 0.064 Uiso 1 1 calc R . .
H12B H 0.8357 0.2149 0.6139 0.064 Uiso 1 1 calc R . .
H12C H 0.7988 0.1905 0.6733 0.064 Uiso 1 1 calc R . .
C13 C 0.7050(4) 0.4375(4) 0.4223(4) 0.0211(13) Uani 1 1 d . . .
C14 C 0.7495(4) 0.4206(4) 0.3997(4) 0.0237(14) Uani 1 1 d . . .
C15 C 0.8084(5) 0.4020(4) 0.3773(4) 0.0284(15) Uani 1 1 d . . .
C16 C 0.7431(6) 0.3213(5) 0.2996(5) 0.0433(19) Uani 1 1 d . . .
H16A H 0.7821 0.3097 0.2859 0.065 Uiso 1 1 calc R . .
H16B H 0.7006 0.3294 0.2534 0.065 Uiso 1 1 calc R . .
H16C H 0.7059 0.2741 0.3108 0.065 Uiso 1 1 calc R . .
C17 C 0.8731(5) 0.3878(5) 0.4531(5) 0.0364(17) Uani 1 1 d . . .
H17A H 0.9130 0.3753 0.4417 0.055 Uiso 1 1 calc R . .
H17B H 0.8335 0.3409 0.4629 0.055 Uiso 1 1 calc R . .
H17C H 0.9132 0.4383 0.5017 0.055 Uiso 1 1 calc R . .
C18 C 0.8694(5) 0.4786(5) 0.3619(5) 0.0408(18) Uani 1 1 d . . .
H18A H 0.9081 0.4673 0.3476 0.061 Uiso 1 1 calc R . .
H18B H 0.9106 0.5280 0.4118 0.061 Uiso 1 1 calc R . .
H18C H 0.8278 0.4884 0.3168 0.061 Uiso 1 1 calc R . .
C19 C 0.8814(5) 0.7138(4) 0.4849(4) 0.0256(14) Uani 1 1 d . . .
C20 C 0.9643(5) 0.7674(4) 0.5148(4) 0.0290(15) Uani 1 1 d . . .
C21 C 1.0666(5) 0.8306(5) 0.5437(5) 0.0373(18) Uani 1 1 d . . .
C22 C 1.0853(6) 0.9190(5) 0.5614(5) 0.046(2) Uani 1 1 d . . .
H22A H 1.1509 0.9595 0.5801 0.069 Uiso 1 1 calc R . .
H22B H 1.0739 0.9311 0.6041 0.069 Uiso 1 1 calc R . .
H22C H 1.0428 0.9228 0.5112 0.069 Uiso 1 1 calc R . .
C23 C 1.1356(6) 0.8244(5) 0.6245(6) 0.055(2) Uani 1 1 d . . .
H23A H 1.2011 0.8650 0.6431 0.082 Uiso 1 1 calc R . .
H23B H 1.1238 0.7680 0.6130 0.082 Uiso 1 1 calc R . .
H23C H 1.1244 0.8362 0.6674 0.082 Uiso 1 1 calc R . .
C24 C 1.0807(7) 0.8075(6) 0.4742(6) 0.075(4) Uani 1 1 d . . .
H24A H 1.1459 0.8469 0.4907 0.112 Uiso 1 1 calc R . .
H24B H 1.0371 0.8103 0.4239 0.112 Uiso 1 1 calc R . .
H24C H 1.0681 0.7508 0.4641 0.112 Uiso 1 1 calc R . .
C25 C 0.8562(4) 0.7587(4) 0.7026(4) 0.0220(13) Uani 1 1 d . . .
C26 C 0.9302(5) 0.8275(5) 0.7502(4) 0.0314(16) Uani 1 1 d . A .
C27 C 1.0239(5) 0.9091(6) 0.8102(5) 0.054(2) Uani 1 1 d . . .
C28 C 1.0284(9) 0.9458(7) 0.8813(8) 0.119(6) Uani 1 1 d . A .
H28A H 1.0897 0.9982 0.9171 0.178 Uiso 1 1 calc R . .
H28B H 1.0207 0.9072 0.9113 0.178 Uiso 1 1 calc R . .
H28C H 0.9778 0.9568 0.8635 0.178 Uiso 1 1 calc R . .
C29 C 1.0190(17) 0.9855(15) 0.7709(15) 0.202(10) Uiso 1 1 d . A .
H29A H 1.0153 0.9747 0.7189 0.303 Uiso 1 1 calc R . .
H29B H 1.0759 1.0400 0.8100 0.303 Uiso 1 1 calc R . .
H29C H 0.9631 0.9853 0.7613 0.303 Uiso 1 1 calc R . .
C30A C 1.0966(12) 0.9185(11) 0.7962(10) 0.062(4) Uiso 0.60 1 d P A 1
H30A H 1.0671 0.8846 0.7395 0.092 Uiso 0.60 1 calc PR A 1
H30B H 1.1341 0.8999 0.8339 0.092 Uiso 0.60 1 calc PR A 1
H30C H 1.1377 0.9772 0.8057 0.092 Uiso 0.60 1 calc PR A 1
C30B C 1.0895(15) 0.8684(13) 0.8716(13) 0.045(5) Uiso 0.40 1 d P A 2
H30D H 1.0999 0.8373 0.8384 0.068 Uiso 0.40 1 calc PR A 2
H30E H 1.0539 0.8312 0.8915 0.068 Uiso 0.40 1 calc PR A 2
H30F H 1.1506 0.9146 0.9185 0.068 Uiso 0.40 1 calc PR A 2
C31 C 0.7186(5) 0.8900(4) 0.7256(4) 0.0299(15) Uani 1 1 d . . .
C32 C 0.7435(5) 0.9538(4) 0.7740(4) 0.0328(16) Uani 1 1 d . . .
C33 C 0.7822(7) 1.0383(5) 0.8305(5) 0.053(2) Uani 1 1 d . . .
C34 C 0.7592(11) 1.0240(9) 0.8997(9) 0.109(5) Uiso 1 1 d . . .
H34A H 0.7837 1.0780 0.9373 0.163 Uiso 1 1 calc R . .
H34B H 0.7892 0.9965 0.9304 0.163 Uiso 1 1 calc R . .
H34C H 0.6907 0.9889 0.8739 0.163 Uiso 1 1 calc R . .
C35 C 0.8852(8) 1.0937(7) 0.8621(11) 0.172(10) Uani 1 1 d . . .
H35A H 0.9109 1.1485 0.8990 0.258 Uiso 1 1 calc R . .
H35B H 0.8926 1.1002 0.8158 0.258 Uiso 1 1 calc R . .
H35C H 0.9193 1.0687 0.8919 0.258 Uiso 1 1 calc R . .
C36 C 0.7249(7) 1.0754(5) 0.7806(6) 0.053(2) Uani 1 1 d . . .
H36A H 0.7487 1.1301 0.8162 0.080 Uiso 1 1 calc R . .
H36B H 0.6579 1.0378 0.7601 0.080 Uiso 1 1 calc R . .
H36C H 0.7321 1.0814 0.7342 0.080 Uiso 1 1 calc R . .
C37 C 0.6371(5) 0.7220(4) 0.3001(4) 0.0273(14) Uani 1 1 d . . .
C38 C 0.6983(5) 0.7668(4) 0.2878(4) 0.0253(14) Uani 1 1 d . . .
C39 C 0.7637(5) 0.8249(4) 0.2652(4) 0.0332(16) Uani 1 1 d . . .
C40 C 0.8675(5) 0.8725(5) 0.3413(5) 0.045(2) Uani 1 1 d . . .
H40A H 0.9103 0.9101 0.3271 0.068 Uiso 1 1 calc R . .
H40B H 0.8846 0.8323 0.3576 0.068 Uiso 1 1 calc R . .
H40C H 0.8726 0.9050 0.3869 0.068 Uiso 1 1 calc R . .
C41 C 0.7309(6) 0.8860(5) 0.2402(5) 0.047(2) Uani 1 1 d . . .
H41A H 0.7711 0.9252 0.2249 0.070 Uiso 1 1 calc R . .
H41B H 0.7358 0.9170 0.2867 0.070 Uiso 1 1 calc R . .
H41C H 0.6651 0.8542 0.1935 0.070 Uiso 1 1 calc R . .
C42 C 0.7536(7) 0.7722(5) 0.1920(5) 0.052(2) Uani 1 1 d . . .
H42A H 0.7957 0.8091 0.1769 0.078 Uiso 1 1 calc R . .
H42B H 0.6881 0.7425 0.1449 0.078 Uiso 1 1 calc R . .
H42C H 0.7704 0.7317 0.2080 0.078 Uiso 1 1 calc R . .
C43 C 0.3763(4) 0.4712(4) 0.1830(4) 0.0239(14) Uani 1 1 d . . .
C44 C 0.3543(5) 0.4707(4) 0.1117(4) 0.0254(14) Uani 1 1 d . . .
C45 C 0.3265(6) 0.4677(5) 0.0256(4) 0.0373(17) Uani 1 1 d . . .
C46 C 0.3877(6) 0.5567(5) 0.0269(5) 0.045(2) Uani 1 1 d . . .
H46A H 0.3696 0.5547 -0.0292 0.067 Uiso 1 1 calc R . .
H46B H 0.4547 0.5756 0.0600 0.067 Uiso 1 1 calc R . .
H46C H 0.3773 0.5956 0.0509 0.067 Uiso 1 1 calc R . .
C47 C 0.2186(6) 0.4365(6) -0.0257(5) 0.050(2) Uani 1 1 d . . .
H47A H 0.1988 0.4341 -0.0822 0.074 Uiso 1 1 calc R . .
H47B H 0.2084 0.4752 -0.0010 0.074 Uiso 1 1 calc R . .
H47C H 0.1813 0.3808 -0.0258 0.074 Uiso 1 1 calc R . .
C48 C 0.3439(6) 0.4055(5) -0.0116(5) 0.0411(19) Uani 1 1 d . . .
H48A H 0.3262 0.4030 -0.0677 0.062 Uiso 1 1 calc R . .
H48B H 0.3056 0.3499 -0.0122 0.062 Uiso 1 1 calc R . .
H48C H 0.4109 0.4246 0.0219 0.062 Uiso 1 1 calc R . .
C49 C 0.4381(5) 0.2719(4) 0.1743(4) 0.0271(14) Uani 1 1 d . . .
C50 C 0.4363(5) 0.2289(4) 0.1220(4) 0.0317(16) Uani 1 1 d . . .
C51 C 0.4374(7) 0.1821(6) 0.0557(5) 0.052(2) Uani 1 1 d . . .
C52 C 0.4849(9) 0.1341(8) 0.0911(6) 0.089(4) Uani 1 1 d . . .
H52A H 0.4858 0.1038 0.0486 0.134 Uiso 1 1 calc R . .
H52B H 0.4493 0.0945 0.1094 0.134 Uiso 1 1 calc R . .
H52C H 0.5498 0.1736 0.1377 0.134 Uiso 1 1 calc R . .
C53 C 0.3335(7) 0.1209(6) -0.0178(5) 0.059(3) Uani 1 1 d . . .
H53A H 0.3327 0.0902 -0.0613 0.089 Uiso 1 1 calc R . .
H53B H 0.3045 0.1525 -0.0390 0.089 Uiso 1 1 calc R . .
H53C H 0.2978 0.0815 0.0007 0.089 Uiso 1 1 calc R . .
C54 C 0.4922(8) 0.2473(8) 0.0268(6) 0.084(4) Uani 1 1 d . . .
H54A H 0.4938 0.2187 -0.0162 0.126 Uiso 1 1 calc R . .
H54B H 0.5568 0.2875 0.0734 0.126 Uiso 1 1 calc R . .
H54C H 0.4603 0.2767 0.0051 0.126 Uiso 1 1 calc R . .
C57B C -0.0822(9) 0.3338(9) 0.0666(8) 0.029(3) Uani 0.50 1 d P . .
C58B C -0.1287(10) 0.2538(10) 0.0876(10) 0.048(4) Uani 0.50 1 d P . .
C55 C 0.1117(5) 0.4177(4) 0.1629(4) 0.0283(15) Uani 1 1 d . . .
C56 C 0.0298(5) 0.3931(5) 0.1202(4) 0.041(2) Uani 1 1 d . . .
C58 C -0.0386(10) 0.4531(9) 0.0074(8) 0.038(4) Uani 0.50 1 d P . .
H58A H -0.0007 0.4495 -0.0130 0.056 Uiso 0.50 1 d PR . .
H58B H -0.0035 0.5091 0.0474 0.056 Uiso 0.50 1 d PR . .
H58C H -0.0981 0.4422 -0.0386 0.056 Uiso 0.50 1 d PR . .
C57 C -0.0605(9) 0.3861(9) 0.0491(8) 0.025(3) Uani 0.50 1 d P . .
C59 C -0.1180(5) 0.3916(5) 0.0807(5) 0.0439(19) Uani 1 1 d . . .
H59A H -0.1741 0.3871 0.0359 0.066 Uiso 1 1 d R . .
H59B H -0.0805 0.4452 0.1252 0.066 Uiso 1 1 d R . .
H59C H -0.1376 0.3461 0.1014 0.066 Uiso 1 1 d R . .
C60 C -0.1104(5) 0.3013(5) -0.0184(5) 0.0430(19) Uani 1 1 d . . .
H60A H -0.0679 0.3028 -0.0353 0.064 Uiso 1 1 d R . .
H60B H -0.1681 0.2918 -0.0658 0.064 Uiso 1 1 d R . .
H60C H -0.1267 0.2560 0.0032 0.064 Uiso 1 1 d R . .
C61 C 0.6765(12) 1.0900(11) 0.1229(12) 0.130(6) Uani 1 1 d . . .
H61A H 0.7388 1.1387 0.1653 0.195 Uiso 1 1 calc R . .
H61B H 0.6370 1.1085 0.0877 0.195 Uiso 1 1 calc R . .
H61C H 0.6837 1.0553 0.0896 0.195 Uiso 1 1 calc R . .
C62 C 0.6285(12) 1.0378(10) 0.1648(9) 0.126(7) Uani 1 1 d . . .
H62A H 0.6687 1.0198 0.2012 0.151 Uiso 1 1 calc R . .
H62B H 0.6210 1.0725 0.1985 0.151 Uiso 1 1 calc R . .
C63 C 0.4883(14) 0.9172(12) 0.1379(12) 0.144(7) Uiso 1 1 d . . .
H63A H 0.5166 0.8855 0.1624 0.173 Uiso 1 1 calc R . .
H63B H 0.4957 0.9546 0.1824 0.173 Uiso 1 1 calc R . .
C64 C 0.3941(17) 0.8623(15) 0.0809(15) 0.203(10) Uiso 1 1 d . . .
H64A H 0.3639 0.8304 0.1072 0.305 Uiso 1 1 calc R . .
H64B H 0.3859 0.8241 0.0372 0.305 Uiso 1 1 calc R . .
H64C H 0.3649 0.8932 0.0575 0.305 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Ag1 Cl3 121.81(17) . 2_666
C1 Ag1 Cl1 128.83(17) . .
Cl3 Ag1 Cl1 92.56(5) 2_666 .
C1 Ag1 Cl2 121.03(17) . .
Cl3 Ag1 Cl2 90.29(5) 2_666 .
Cl1 Ag1 Cl2 92.38(5) . .
C1 Ag1 Ag6 49.85(17) . .
Cl3 Ag1 Ag6 124.36(4) 2_666 .
Cl1 Ag1 Ag6 80.05(4) . .
Cl2 Ag1 Ag6 144.57(4) . .
C1 Ag1 Ag7 49.23(16) . .
Cl3 Ag1 Ag7 142.74(4) 2_666 .
Cl1 Ag1 Ag7 121.40(4) . .
Cl2 Ag1 Ag7 74.69(4) . .
Ag6 Ag1 Ag7 79.95(2) . .
C1 Ag1 Ag5 48.92(17) . .
Cl3 Ag1 Ag5 74.14(4) 2_666 .
Cl1 Ag1 Ag5 148.94(4) . .
Cl2 Ag1 Ag5 115.13(4) . .
Ag6 Ag1 Ag5 84.61(2) . .
Ag7 Ag1 Ag5 81.68(2) . .
C13 Ag2 Cl3 122.44(17) . .
C13 Ag2 Cl1 123.64(17) . .
Cl3 Ag2 Cl1 93.51(5) . .
C13 Ag2 Cl2 123.59(17) . .
Cl3 Ag2 Cl2 91.94(5) . .
Cl1 Ag2 Cl2 93.06(5) . .
C13 Ag2 Ag9 49.84(16) . .
Cl3 Ag2 Ag9 150.50(4) . .
Cl1 Ag2 Ag9 114.33(4) . .
Cl2 Ag2 Ag9 77.66(4) . .
C13 Ag2 Ag19 49.31(16) . .
Cl3 Ag2 Ag19 113.43(4) . .
Cl1 Ag2 Ag19 78.21(4) . .
Cl2 Ag2 Ag19 153.42(4) . .
Ag9 Ag2 Ag19 83.15(2) . .
C13 Ag2 Ag14 48.84(16) . .
Cl3 Ag2 Ag14 76.91(4) . .
Cl1 Ag2 Ag14 151.31(4) . .
Cl2 Ag2 Ag14 113.98(4) . .
Ag9 Ag2 Ag14 82.24(2) . .
Ag19 Ag2 Ag14 80.977(19) . .
C25 Ag3 Cl2 131.35(17) . .
C25 Ag3 Cl3 129.96(17) . .
Cl2 Ag3 Cl3 92.54(5) . .
C25 Ag3 Cl1 111.47(17) . 2_666
Cl2 Ag3 Cl1 87.94(5) . 2_666
Cl3 Ag3 Cl1 89.39(5) . 2_666
C25 Ag3 Ag10 49.67(16) . .
Cl2 Ag3 Ag10 82.09(4) . .
Cl3 Ag3 Ag10 159.88(4) . .
Cl1 Ag3 Ag10 109.67(4) 2_666 .
C25 Ag3 Ag12 49.80(16) . .
Cl2 Ag3 Ag12 129.93(4) . .
Cl3 Ag3 Ag12 85.44(4) . .
Cl1 Ag3 Ag12 141.91(4) 2_666 .
Ag10 Ag3 Ag12 83.30(2) . .
C25 Ag3 Ag11 48.02(16) . .
Cl2 Ag3 Ag11 140.59(4) . .
Cl3 Ag3 Ag11 114.89(4) . .
Cl1 Ag3 Ag11 65.89(3) 2_666 .
Ag10 Ag3 Ag11 80.03(2) . .
Ag12 Ag3 Ag11 82.28(2) . .
C43 Ag4 Cl2 123.84(17) . 2_666
C43 Ag4 Cl1 127.66(17) . .
Cl2 Ag4 Cl1 91.03(5) 2_666 .
C43 Ag4 Cl3 123.95(16) . .
Cl2 Ag4 Cl3 89.11(5) 2_666 .
Cl1 Ag4 Cl3 90.15(5) . .
C43 Ag4 Ag17 49.78(17) . .
Cl2 Ag4 Ag17 148.10(4) 2_666 .
Cl1 Ag4 Ag17 79.51(4) . .
Cl3 Ag4 Ag17 121.00(4) . .
C43 Ag4 Ag15 48.79(16) . .
Cl2 Ag4 Ag15 120.13(4) 2_666 .
Cl1 Ag4 Ag15 145.08(4) . .
Cl3 Ag4 Ag15 76.10(4) . .
Ag17 Ag4 Ag15 80.53(2) . .
C43 Ag4 Ag16 49.31(16) . .
Cl2 Ag4 Ag16 76.35(4) 2_666 .
Cl1 Ag4 Ag16 123.67(4) . .
Cl3 Ag4 Ag16 142.73(4) . .
Ag17 Ag4 Ag16 83.71(2) . .
Ag15 Ag4 Ag16 81.92(2) . .
C37 Ag5 C1 179.4(3) 2_666 .
C37 Ag5 C2 152.5(2) 2_666 .
C1 Ag5 C2 27.9(2) . .
C37 Ag5 Ag15 46.30(18) 2_666 2_666
C1 Ag5 Ag15 133.16(16) . 2_666
C2 Ag5 Ag15 146.48(14) . 2_666
C37 Ag5 Ag1 132.81(17) 2_666 .
C1 Ag5 Ag1 46.74(15) . .
C2 Ag5 Ag1 74.61(14) . .
Ag15 Ag5 Ag1 98.39(2) 2_666 .
C37 Ag5 Ag13 41.19(17) 2_666 2_666
C1 Ag5 Ag13 138.75(16) . 2_666
C2 Ag5 Ag13 148.32(14) . 2_666
Ag15 Ag5 Ag13 64.826(18) 2_666 2_666
Ag1 Ag5 Ag13 101.22(2) . 2_666
C31 Ag6 C1 174.7(2) 2_666 .
C31 Ag6 C2 155.7(2) 2_666 .
C1 Ag6 C2 27.4(2) . .
C31 Ag6 Ag11 46.87(18) 2_666 2_666
C1 Ag6 Ag11 127.84(16) . 2_666
C2 Ag6 Ag11 142.20(14) . 2_666
C31 Ag6 Ag1 128.28(18) 2_666 .
C1 Ag6 Ag1 47.87(15) . .
C2 Ag6 Ag1 75.20(14) . .
Ag11 Ag6 Ag1 88.84(2) 2_666 .
C7 Ag7 C1 171.0(2) . .
C7 Ag7 Ag9 47.01(18) . .
C1 Ag7 Ag9 129.20(16) . .
C7 Ag7 Ag1 134.80(18) . .
C1 Ag7 Ag1 47.88(16) . .
Ag9 Ag7 Ag1 92.92(2) . .
C7 Ag7 Ag8 41.98(19) . .
C1 Ag7 Ag8 146.93(16) . .
Ag9 Ag7 Ag8 66.13(2) . .
Ag1 Ag7 Ag8 110.20(2) . .
C55 Ag8 C7 174.3(2) 2_666 .
C55 Ag8 C8 152.8(2) 2_666 .
C7 Ag8 C8 28.7(2) . .
C55 Ag8 C56 25.1(2) 2_666 2_666
C7 Ag8 C56 158.4(2) . 2_666
C8 Ag8 C56 130.1(2) . 2_666
C55 Ag8 Ag16 41.55(17) 2_666 2_666
C7 Ag8 Ag16 133.19(18) . 2_666
C8 Ag8 Ag16 146.35(14) . 2_666
C56 Ag8 Ag16 65.18(15) 2_666 2_666
C55 Ag8 Ag7 135.40(17) 2_666 .
C7 Ag8 Ag7 39.40(18) . .
C8 Ag8 Ag7 62.54(14) . .
C56 Ag8 Ag7 156.38(17) 2_666 .
Ag16 Ag8 Ag7 93.85(2) 2_666 .
C7 Ag9 C13 170.6(2) . .
C7 Ag9 Ag2 135.02(19) . .
C13 Ag9 Ag2 47.60(16) . .
C7 Ag9 Ag7 46.80(19) . .
C13 Ag9 Ag7 141.09(16) . .
Ag2 Ag9 Ag7 98.08(2) . .
C55 Ag10 C25 172.9(2) 2_666 .
C55 Ag10 Ag3 130.43(18) 2_666 .
C25 Ag10 Ag3 47.78(16) . .
C55 Ag10 Ag16 45.52(17) 2_666 2_666
C25 Ag10 Ag16 138.68(16) . 2_666
Ag3 Ag10 Ag16 98.93(2) . 2_666
C31 Ag11 C25 168.2(2) . .
C31 Ag11 C26 139.9(3) . .
C25 Ag11 C26 28.7(2) . .
C31 Ag11 Ag6 47.32(19) . 2_666
C25 Ag11 Ag6 136.47(16) . 2_666
C26 Ag11 Ag6 143.35(16) . 2_666
C31 Ag11 Ag3 144.84(19) . .
C25 Ag11 Ag3 45.97(16) . .
C26 Ag11 Ag3 74.62(17) . .
Ag6 Ag11 Ag3 103.18(2) 2_666 .
C31 Ag11 Ag18 43.67(19) . 2_666
C25 Ag11 Ag18 144.71(16) . 2_666
C26 Ag11 Ag18 145.51(15) . 2_666
Ag6 Ag11 Ag18 69.31(2) 2_666 2_666
Ag3 Ag11 Ag18 115.47(2) . 2_666
C19 Ag12 C25 167.3(2) . .
C19 Ag12 C20 27.2(2) . .
C25 Ag12 C20 160.5(2) . .
C19 Ag12 C26 163.4(2) . .
C25 Ag12 C26 26.8(2) . .
C20 Ag12 C26 136.2(2) . .
C19 Ag12 Ag3 121.94(17) . .
C25 Ag12 Ag3 47.26(16) . .
C20 Ag12 Ag3 148.20(15) . .
C26 Ag12 Ag3 73.91(15) . .
C19 Ag12 Ag14 41.75(17) . .
C25 Ag12 Ag14 125.52(16) . .
C20 Ag12 Ag14 64.64(15) . .
C26 Ag12 Ag14 147.79(16) . .
Ag3 Ag12 Ag14 83.85(2) . .
C19 Ag12 Ag13 41.21(17) . .
C25 Ag12 Ag13 136.77(16) . .
C20 Ag12 Ag13 62.54(15) . .
C26 Ag12 Ag13 150.09(16) . .
Ag3 Ag12 Ag13 96.01(2) . .
Ag14 Ag12 Ag13 53.583(17) . .
C19 Ag13 C37 165.5(2) . .
C19 Ag13 C38 137.4(2) . .
C37 Ag13 C38 29.1(2) . .
C19 Ag13 Ag14 47.18(17) . .
C37 Ag13 Ag14 146.60(17) . .
C38 Ag13 Ag14 155.31(15) . .
C19 Ag13 Ag12 42.13(17) . .
C37 Ag13 Ag12 138.68(17) . .
C38 Ag13 Ag12 140.62(14) . .
Ag14 Ag13 Ag12 62.359(18) . .
C19 Ag13 Ag5 142.68(17) . 2_666
C37 Ag13 Ag5 38.96(17) . 2_666
C38 Ag13 Ag5 61.69(15) . 2_666
Ag14 Ag13 Ag5 133.24(2) . 2_666
Ag12 Ag13 Ag5 101.29(2) . 2_666
C19 Ag14 C13 177.0(2) . .
C19 Ag14 C14 150.3(2) . .
C13 Ag14 C14 26.7(2) . .
C19 Ag14 Ag13 47.61(18) . .
C13 Ag14 Ag13 134.04(16) . .
C14 Ag14 Ag13 140.72(14) . .
C19 Ag14 Ag2 136.86(18) . .
C13 Ag14 Ag2 46.15(15) . .
C14 Ag14 Ag2 72.86(13) . .
Ag13 Ag14 Ag2 102.09(2) . .
C19 Ag14 Ag12 43.06(17) . .
C13 Ag14 Ag12 139.18(16) . .
C14 Ag14 Ag12 154.68(14) . .
Ag13 Ag14 Ag12 64.057(19) . .
Ag2 Ag14 Ag12 100.19(2) . .
C37 Ag15 C43 177.9(2) . .
C37 Ag15 C44 152.2(2) . .
C43 Ag15 C44 28.2(2) . .
C37 Ag15 Ag5 47.32(18) . 2_666
C43 Ag15 Ag5 130.84(16) . 2_666
C44 Ag15 Ag5 143.64(15) . 2_666
C37 Ag15 Ag4 131.63(17) . .
C43 Ag15 Ag4 47.95(16) . .
C44 Ag15 Ag4 76.17(14) . .
Ag5 Ag15 Ag4 95.12(2) 2_666 .
C55 Ag16 C43 166.3(2) . .
C55 Ag16 Ag4 133.44(18) . .
C43 Ag16 Ag4 47.78(16) . .
C55 Ag16 Ag10 47.55(18) . 2_666
C43 Ag16 Ag10 123.51(17) . 2_666
Ag4 Ag16 Ag10 91.42(2) . 2_666
C55 Ag16 Ag8 43.42(18) . 2_666
C43 Ag16 Ag8 149.00(16) . 2_666
Ag4 Ag16 Ag8 109.00(2) . 2_666
Ag10 Ag16 Ag8 68.701(19) 2_666 2_666
C49 Ag17 C43 168.5(2) . .
C49 Ag17 Ag4 133.26(17) . .
C43 Ag17 Ag4 48.11(16) . .
C49 Ag17 Ag19 46.56(17) . .
C43 Ag17 Ag19 126.71(16) . .
Ag4 Ag17 Ag19 91.64(2) . .
C49 Ag17 Ag18 41.98(18) . .
C43 Ag17 Ag18 147.88(16) . .
Ag4 Ag17 Ag18 105.85(2) . .
Ag19 Ag17 Ag18 61.563(18) . .
C49 Ag18 C31 176.0(3) . 2_666
C49 Ag18 C32 151.0(2) . 2_666
C31 Ag18 C32 27.8(2) 2_666 2_666
C49 Ag18 Ag19 42.44(17) . .
C31 Ag18 Ag19 141.04(18) 2_666 .
C32 Ag18 Ag19 153.54(16) 2_666 .
C49 Ag18 Ag11 137.02(18) . 2_666
C31 Ag18 Ag11 41.29(17) 2_666 2_666
C32 Ag18 Ag11 64.82(17) 2_666 2_666
Ag19 Ag18 Ag11 122.62(3) . 2_666
C49 Ag18 Ag17 41.01(18) . .
C31 Ag18 Ag17 137.19(18) 2_666 .
C32 Ag18 Ag17 151.02(16) 2_666 .
Ag19 Ag18 Ag17 54.966(17) . .
Ag11 Ag18 Ag17 96.03(2) 2_666 .
C49 Ag19 C13 172.5(2) . .
C49 Ag19 C14 148.4(2) . .
C13 Ag19 C14 27.8(2) . .
C49 Ag19 Ag17 46.18(18) . .
C13 Ag19 Ag17 140.37(16) . .
C14 Ag19 Ag17 157.83(14) . .
C49 Ag19 Ag2 136.48(18) . .
C13 Ag19 Ag2 46.17(15) . .
C14 Ag19 Ag2 74.00(15) . .
Ag17 Ag19 Ag2 98.91(2) . .
C49 Ag19 Ag18 43.13(18) . .
C13 Ag19 Ag18 132.34(15) . .
C14 Ag19 Ag18 138.25(14) . .
Ag17 Ag19 Ag18 63.471(19) . .
Ag2 Ag19 Ag18 103.53(2) . .
Ag2 Cl1 Ag4 83.63(4) . .
Ag2 Cl1 Ag1 82.86(5) . .
Ag4 Cl1 Ag1 139.96(6) . .
Ag2 Cl1 Ag3 136.75(6) . 2_666
Ag4 Cl1 Ag3 82.67(4) . 2_666
Ag1 Cl1 Ag3 81.86(4) . 2_666
Ag3 Cl2 Ag4 86.10(5) . 2_666
Ag3 Cl2 Ag2 80.68(4) . .
Ag4 Cl2 Ag2 139.71(6) 2_666 .
Ag3 Cl2 Ag1 140.57(6) . .
Ag4 Cl2 Ag1 85.58(5) 2_666 .
Ag2 Cl2 Ag1 81.16(4) . .
Ag2 Cl3 Ag3 81.61(5) . .
Ag2 Cl3 Ag1 137.86(6) . 2_666
Ag3 Cl3 Ag1 84.94(5) . 2_666
Ag2 Cl3 Ag4 81.79(4) . .
Ag3 Cl3 Ag4 141.05(6) . .
Ag1 Cl3 Ag4 84.20(5) 2_666 .
O4 Cl4 O3 110.8(4) . .
O4 Cl4 O2 109.8(4) . .
O3 Cl4 O2 110.7(3) . .
O4 Cl4 O1 107.7(3) . .
O3 Cl4 O1 109.0(3) . .
O2 Cl4 O1 108.8(3) . .
O7 Cl5 O6 114.5(4) . .
O7 Cl5 O8 107.3(5) . .
O6 Cl5 O8 109.5(4) . .
O7 Cl5 O5 109.1(4) . .
O6 Cl5 O5 109.0(4) . .
O8 Cl5 O5 107.2(3) . .
O12 Cl6 O10 111.9(4) . .
O12 Cl6 O11 110.1(3) . .
O10 Cl6 O11 110.0(4) . .
O12 Cl6 O9 108.4(3) . .
O10 Cl6 O9 108.1(3) . .
O11 Cl6 O9 108.2(3) . .
O15 Cl7 O16 112.4(4) . .
O15 Cl7 O14 108.8(5) . .
O16 Cl7 O14 110.0(4) . .
O15 Cl7 O13 108.2(4) . .
O16 Cl7 O13 109.1(3) . .
O14 Cl7 O13 108.3(4) . .
O20 Cl8 O17 111.2(4) . .
O20 Cl8 O18 110.3(4) . .
O17 Cl8 O18 110.1(4) . .
O20 Cl8 O19 109.7(4) . .
O17 Cl8 O19 108.9(3) . .
O18 Cl8 O19 106.6(3) . .
O22 Cl9 O24 111.7(4) . .
O22 Cl9 O23 111.0(4) . .
O24 Cl9 O23 109.8(4) . .
O22 Cl9 O21 107.8(4) . .
O24 Cl9 O21 108.4(4) . .
O23 Cl9 O21 108.0(3) . .
C62 O25 C63 113.1(14) . .
C2 C1 Ag1 174.5(5) . .
C2 C1 Ag7 102.6(5) . .
Ag1 C1 Ag7 82.9(2) . .
C2 C1 Ag6 95.4(5) . .
Ag1 C1 Ag6 82.3(2) . .
Ag7 C1 Ag6 113.7(3) . .
C2 C1 Ag5 92.9(5) . .
Ag1 C1 Ag5 84.3(2) . .
Ag7 C1 Ag5 118.7(3) . .
Ag6 C1 Ag5 123.4(3) . .
C1 C2 C3 175.6(7) . .
C1 C2 Ag5 59.2(4) . .
C3 C2 Ag5 124.5(5) . .
C1 C2 Ag6 57.2(4) . .
C3 C2 Ag6 122.7(4) . .
Ag5 C2 Ag6 97.2(2) . .
C2 C3 C5 109.6(6) . .
C2 C3 C4 109.4(6) . .
C5 C3 C4 111.2(7) . .
C2 C3 C6 106.6(6) . .
C5 C3 C6 110.4(6) . .
C4 C3 C6 109.6(7) . .
C3 C4 H4A 109.5 . .
C3 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
C3 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
C3 C5 H5A 109.5 . .
C3 C5 H5B 109.5 . .
H5A C5 H5B 109.5 . .
C3 C5 H5C 109.5 . .
H5A C5 H5C 109.5 . .
H5B C5 H5C 109.5 . .
C3 C6 H6A 109.5 . .
C3 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C3 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C8 C7 Ag7 134.5(5) . .
C8 C7 Ag9 134.8(6) . .
Ag7 C7 Ag9 86.2(3) . .
C8 C7 Ag8 91.2(5) . .
Ag7 C7 Ag8 98.6(3) . .
Ag9 C7 Ag8 102.5(3) . .
C7 C8 C9 170.9(7) . .
C7 C8 Ag8 60.1(4) . .
C9 C8 Ag8 128.9(4) . .
C8 C9 C10 109.3(6) . .
C8 C9 C12 106.8(6) . .
C10 C9 C12 110.3(7) . .
C8 C9 C11 109.1(6) . .
C10 C9 C11 110.1(6) . .
C12 C9 C11 111.1(6) . .
C9 C10 H10A 109.5 . .
C9 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C9 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
C9 C11 H11A 109.5 . .
C9 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
C9 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
C9 C12 H12A 109.5 . .
C9 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C9 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C14 C13 Ag2 176.2(5) . .
C14 C13 Ag9 99.4(5) . .
Ag2 C13 Ag9 82.6(2) . .
C14 C13 Ag14 96.8(4) . .
Ag2 C13 Ag14 85.0(2) . .
Ag9 C13 Ag14 119.1(3) . .
C14 C13 Ag19 91.7(4) . .
Ag2 C13 Ag19 84.5(2) . .
Ag9 C13 Ag19 120.0(3) . .
Ag14 C13 Ag19 117.7(3) . .
C13 C14 C15 176.7(7) . .
C13 C14 Ag19 60.5(4) . .
C15 C14 Ag19 122.7(4) . .
C13 C14 Ag14 56.5(4) . .
C15 C14 Ag14 122.6(4) . .
Ag19 C14 Ag14 94.0(2) . .
C14 C15 C18 108.8(6) . .
C14 C15 C16 110.3(6) . .
C18 C15 C16 111.0(6) . .
C14 C15 C17 106.0(5) . .
C18 C15 C17 110.8(6) . .
C16 C15 C17 109.8(6) . .
C15 C16 H16A 109.5 . .
C15 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C15 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C15 C17 H17A 109.5 . .
C15 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C15 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C15 C18 H18A 109.5 . .
C15 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C15 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C20 C19 Ag14 139.2(6) . .
C20 C19 Ag13 132.2(6) . .
Ag14 C19 Ag13 85.2(2) . .
C20 C19 Ag12 95.6(5) . .
Ag14 C19 Ag12 95.2(2) . .
Ag13 C19 Ag12 96.7(3) . .
C19 C20 C21 173.8(7) . .
C19 C20 Ag12 57.2(4) . .
C21 C20 Ag12 129.0(4) . .
C20 C21 C22 109.5(6) . .
C20 C21 C24 107.3(6) . .
C22 C21 C24 111.3(7) . .
C20 C21 C23 109.5(6) . .
C22 C21 C23 109.6(6) . .
C24 C21 C23 109.6(8) . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C21 C23 H23A 109.5 . .
C21 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C21 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
C21 C24 H24A 109.5 . .
C21 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C21 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C26 C25 Ag3 173.8(6) . .
C26 C25 Ag10 103.0(5) . .
Ag3 C25 Ag10 82.5(2) . .
C26 C25 Ag11 88.9(5) . .
Ag3 C25 Ag11 86.0(2) . .
Ag10 C25 Ag11 116.4(3) . .
C26 C25 Ag12 96.5(5) . .
Ag3 C25 Ag12 82.9(2) . .
Ag10 C25 Ag12 119.5(3) . .
Ag11 C25 Ag12 120.7(3) . .
C25 C26 C27 176.6(8) . .
C25 C26 Ag11 62.4(4) . .
C27 C26 Ag11 120.7(6) . .
C25 C26 Ag12 56.7(4) . .
C27 C26 Ag12 122.9(5) . .
Ag11 C26 Ag12 97.1(2) . .
C28 C27 C30A 132.1(10) . .
C28 C27 C26 113.2(7) . .
C30A C27 C26 111.4(9) . .
C28 C27 C29 92.5(12) . .
C30A C27 C29 90.5(11) . .
C26 C27 C29 106.8(10) . .
C28 C27 C30B 88.4(11) . .
C30A C27 C30B 68.1(10) . .
C26 C27 C30B 99.3(9) . .
C29 C27 C30B 151.1(12) . .
C27 C28 H28A 109.5 . .
C27 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C27 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C27 C29 H29A 109.5 . .
C27 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
C27 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
C27 C30A H30A 109.5 . .
C27 C30A H30B 109.5 . .
H30A C30A H30B 109.5 . .
C27 C30A H30C 109.5 . .
H30A C30A H30C 109.5 . .
H30B C30A H30C 109.5 . .
C27 C30B H30D 109.5 . .
C27 C30B H30E 109.5 . .
H30D C30B H30E 109.5 . .
C27 C30B H30F 109.5 . .
H30D C30B H30F 109.5 . .
H30E C30B H30F 109.5 . .
C32 C31 Ag11 140.5(6) . .
C32 C31 Ag6 128.8(6) . 2_666
Ag11 C31 Ag6 85.8(2) . 2_666
C32 C31 Ag18 92.6(5) . 2_666
Ag11 C31 Ag18 95.0(3) . 2_666
Ag6 C31 Ag18 105.9(3) 2_666 2_666
C31 C32 C33 173.0(9) . .
C31 C32 Ag18 59.6(4) . 2_666
C33 C32 Ag18 127.2(6) . 2_666
C35 C33 C32 109.0(8) . .
C35 C33 C36 111.0(10) . .
C32 C33 C36 108.2(6) . .
C35 C33 C34 115.0(11) . .
C32 C33 C34 107.8(9) . .
C36 C33 C34 105.6(9) . .
C33 C34 H34A 109.5 . .
C33 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
C33 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
C33 C35 H35A 109.5 . .
C33 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
C33 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
C33 C36 H36A 109.5 . .
C33 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C33 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C38 C37 Ag15 139.3(6) . .
C38 C37 Ag5 132.1(6) . 2_666
Ag15 C37 Ag5 86.4(2) . 2_666
C38 C37 Ag13 86.0(5) . .
Ag15 C37 Ag13 101.9(3) . .
Ag5 C37 Ag13 99.8(3) 2_666 .
C37 C38 C39 172.1(7) . .
C37 C38 Ag13 64.9(4) . .
C39 C38 Ag13 122.9(5) . .
C38 C39 C42 108.8(6) . .
C38 C39 C41 106.0(6) . .
C42 C39 C41 111.1(7) . .
C38 C39 C40 109.0(6) . .
C42 C39 C40 110.5(7) . .
C41 C39 C40 111.4(6) . .
C39 C40 H40A 109.5 . .
C39 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
C39 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
C39 C41 H41A 109.5 . .
C39 C41 H41B 109.5 . .
H41A C41 H41B 109.5 . .
C39 C41 H41C 109.5 . .
H41A C41 H41C 109.5 . .
H41B C41 H41C 109.5 . .
C39 C42 H42A 109.5 . .
C39 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C39 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
C44 C43 Ag4 176.1(6) . .
C44 C43 Ag15 93.1(5) . .
Ag4 C43 Ag15 83.3(2) . .
C44 C43 Ag16 100.2(5) . .
Ag4 C43 Ag16 82.9(2) . .
Ag15 C43 Ag16 119.0(3) . .
C44 C43 Ag17 98.2(5) . .
Ag4 C43 Ag17 82.1(2) . .
Ag15 C43 Ag17 115.5(3) . .
Ag16 C43 Ag17 120.8(3) . .
C43 C44 C45 178.5(7) . .
C43 C44 Ag15 58.7(4) . .
C45 C44 Ag15 122.6(5) . .
C44 C45 C48 108.7(6) . .
C44 C45 C46 109.6(6) . .
C48 C45 C46 109.7(6) . .
C44 C45 C47 108.0(6) . .
C48 C45 C47 110.3(6) . .
C46 C45 C47 110.5(7) . .
C45 C46 H46A 109.5 . .
C45 C46 H46B 109.5 . .
H46A C46 H46B 109.5 . .
C45 C46 H46C 109.5 . .
H46A C46 H46C 109.5 . .
H46B C46 H46C 109.5 . .
C45 C47 H47A 109.5 . .
C45 C47 H47B 109.5 . .
H47A C47 H47B 109.5 . .
C45 C47 H47C 109.5 . .
H47A C47 H47C 109.5 . .
H47B C47 H47C 109.5 . .
C45 C48 H48A 109.5 . .
C45 C48 H48B 109.5 . .
H48A C48 H48B 109.5 . .
C45 C48 H48C 109.5 . .
H48A C48 H48C 109.5 . .
H48B C48 H48C 109.5 . .
C50 C49 Ag17 135.5(6) . .
C50 C49 Ag19 123.0(5) . .
Ag17 C49 Ag19 87.3(2) . .
C50 C49 Ag18 110.5(5) . .
Ag17 C49 Ag18 97.0(3) . .
Ag19 C49 Ag18 94.4(3) . .
C49 C50 C51 175.3(8) . .
C50 C51 C52 109.1(7) . .
C50 C51 C53 108.3(7) . .
C52 C51 C53 110.8(8) . .
C50 C51 C54 107.8(7) . .
C52 C51 C54 111.7(9) . .
C53 C51 C54 109.1(8) . .
C51 C52 H52A 109.5 . .
C51 C52 H52B 109.5 . .
H52A C52 H52B 109.5 . .
C51 C52 H52C 109.5 . .
H52A C52 H52C 109.5 . .
H52B C52 H52C 109.5 . .
C51 C53 H53A 109.5 . .
C51 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
C51 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C51 C54 H54A 109.5 . .
C51 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C51 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
C57 C57B C60 74.3(12) . .
C57 C57B C58B 172.0(16) . .
C60 C57B C58B 105.0(11) . .
C57 C57B C59 65.6(11) . .
C60 C57B C59 114.8(10) . .
C58B C57B C59 108.2(12) . .
C57 C57B C56 69.7(11) . .
C60 C57B C56 107.0(10) . .
C58B C57B C56 117.7(11) . .
C59 C57B C56 104.6(9) . .
C57 C57B H59C 101.9 . .
C60 C57B H59C 130.7 . .
C58B C57B H59C 72.3 . .
C59 C57B H59C 36.3 . .
C56 C57B H59C 117.8 . .
C57 C57B H60C 113.5 . .
C60 C57B H60C 39.2 . .
C58B C57B H60C 66.4 . .
C59 C57B H60C 133.1 . .
C56 C57B H60C 119.3 . .
H59C C57B H60C 120.0 . .
C56 C55 Ag16 151.2(6) . .
C56 C55 Ag10 110.3(6) . 2_666
Ag16 C55 Ag10 86.9(2) . 2_666
C56 C55 Ag8 102.3(5) . 2_666
Ag16 C55 Ag8 95.0(3) . 2_666
Ag10 C55 Ag8 104.7(3) 2_666 2_666
C55 C56 C57 157.0(10) . .
C55 C56 C57B 162.0(10) . .
C57 C56 C57B 38.8(7) . .
C55 C56 Ag8 52.7(4) . 2_666
C57 C56 Ag8 123.7(7) . 2_666
C57B C56 Ag8 136.9(6) . 2_666
C57 C58 C58 156.0(14) . 2_565
C57 C58 H58A 109.3 . .
C58 C58 H58A 60.5 2_565 .
C57 C58 H58B 109.9 . .
C58 C58 H58B 59.9 2_565 .
H58A C58 H58B 109.5 . .
C57 C58 H58C 109.2 . .
C58 C58 H58C 94.7 2_565 .
H58A C58 H58C 109.4 . .
H58B C58 H58C 109.5 . .
C57B C57 C59 74.7(12) . .
C57B C57 C60 65.2(11) . .
C59 C57 C60 114.8(10) . .
C57B C57 C58 170.0(15) . .
C59 C57 C58 109.5(11) . .
C60 C57 C58 105.0(10) . .
C57B C57 C56 71.5(11) . .
C59 C57 C56 109.8(9) . .
C60 C57 C56 103.6(9) . .
C58 C57 C56 114.2(10) . .
C57 C59 C57B 39.7(7) . .
C57 C59 H59A 109.0 . .
C57B C59 H59A 121.3 . .
C57 C59 H59B 109.8 . .
C57B C59 H59B 126.4 . .
H59A C59 H59B 109.5 . .
C57 C59 H59C 109.6 . .
C57B C59 H59C 70.0 . .
H59A C59 H59C 109.5 . .
H59B C59 H59C 109.5 . .
C57B C60 C57 40.4(7) . .
C57B C60 H60A 125.2 . .
C57 C60 H60A 109.5 . .
C57B C60 H60B 122.7 . .
C57 C60 H60B 109.2 . .
H60A C60 H60B 109.5 . .
C57B C60 H60C 69.3 . .
C57 C60 H60C 109.7 . .
H60A C60 H60C 109.5 . .
H60B C60 H60C 109.5 . .
C62 C61 H61A 109.5 . .
C62 C61 H61B 109.5 . .
H61A C61 H61B 109.5 . .
C62 C61 H61C 109.5 . .
H61A C61 H61C 109.5 . .
H61B C61 H61C 109.5 . .
O25 C62 C61 109.1(14) . .
O25 C62 H62A 109.9 . .
C61 C62 H62A 109.9 . .
O25 C62 H62B 109.9 . .
C61 C62 H62B 109.9 . .
H62A C62 H62B 108.3 . .
C64 C63 O25 113.8(19) . .
C64 C63 H63A 108.8 . .
O25 C63 H63A 108.8 . .
C64 C63 H63B 108.8 . .
O25 C63 H63B 108.8 . .
H63A C63 H63B 107.7 . .
C63 C64 H64A 109.5 . .
C63 C64 H64B 109.5 . .
H64A C64 H64B 109.5 . .
C63 C64 H64C 109.5 . .
H64A C64 H64C 109.5 . .
H64B C64 H64C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C1 2.178(6) .
Ag1 Cl3 2.6332(16) 2_666
Ag1 Cl1 2.6400(16) .
Ag1 Cl2 2.6895(15) .
Ag1 Ag6 2.9109(8) .
Ag1 Ag7 2.9141(8) .
Ag1 Ag5 2.9768(8) .
Ag2 C13 2.158(6) .
Ag2 Cl3 2.6103(15) .
Ag2 Cl1 2.6292(16) .
Ag2 Cl2 2.6704(16) .
Ag2 Ag9 2.8974(7) .
Ag2 Ag19 2.9774(8) .
Ag2 Ag14 2.9809(7) .
Ag3 C25 2.174(6) .
Ag3 Cl2 2.6222(16) .
Ag3 Cl3 2.6326(16) .
Ag3 Cl1 2.7842(16) 2_666
Ag3 Ag10 2.9102(8) .
Ag3 Ag12 2.9368(8) .
Ag3 Ag11 3.0159(8) .
Ag4 C43 2.194(6) .
Ag4 Cl2 2.6258(16) 2_666
Ag4 Cl1 2.6379(16) .
Ag4 Cl3 2.7513(16) .
Ag4 Ag17 2.9189(8) .
Ag4 Ag15 2.9338(7) .
Ag4 Ag16 2.9399(8) .
Ag5 C37 2.147(7) 2_666
Ag5 C1 2.255(6) .
Ag5 C2 2.622(6) .
Ag5 Ag15 2.9142(8) 2_666
Ag5 Ag13 3.3643(8) 2_666
Ag6 C31 2.141(7) 2_666
Ag6 C1 2.245(6) .
Ag6 C2 2.660(6) .
Ag6 Ag11 2.9052(8) 2_666
Ag7 C7 2.122(7) .
Ag7 C1 2.224(6) .
Ag7 Ag9 2.9039(8) .
Ag7 Ag8 3.3046(8) .
Ag8 C55 2.200(7) 2_666
Ag8 C7 2.236(7) .
Ag8 C8 2.578(6) .
Ag8 C56 2.702(7) 2_666
Ag8 Ag16 3.1881(8) 2_666
Ag9 C7 2.129(7) .
Ag9 C13 2.233(6) .
Ag10 C55 2.195(7) 2_666
Ag10 C25 2.238(6) .
Ag10 Ag16 2.9712(8) 2_666
Ag11 C31 2.126(7) .
Ag11 C25 2.247(6) .
Ag11 C26 2.536(7) .
Ag11 Ag6 2.9051(8) 2_666
Ag11 Ag18 3.2095(9) 2_666
Ag12 C19 2.200(6) .
Ag12 C25 2.260(6) .
Ag12 C20 2.605(7) .
Ag12 C26 2.687(7) .
Ag12 Ag14 3.2089(8) .
Ag12 Ag13 3.2573(9) .
Ag13 C19 2.161(7) .
Ag13 C37 2.249(6) .
Ag13 C38 2.477(6) .
Ag13 Ag14 2.9149(8) .
Ag13 Ag5 3.3642(8) 2_666
Ag14 C19 2.146(6) .
Ag14 C13 2.253(6) .
Ag14 C14 2.684(6) .
Ag15 C37 2.111(7) .
Ag15 C43 2.222(6) .
Ag15 C44 2.597(6) .
Ag15 Ag5 2.9143(8) 2_666
Ag16 C55 2.123(7) .
Ag16 C43 2.246(6) .
Ag16 Ag10 2.9712(8) 2_666
Ag16 Ag8 3.1879(8) 2_666
Ag17 C49 2.132(7) .
Ag17 C43 2.250(6) .
Ag17 Ag19 2.9516(8) .
Ag17 Ag18 3.2252(8) .
Ag18 C49 2.173(7) .
Ag18 C31 2.225(7) 2_666
Ag18 C32 2.577(7) 2_666
Ag18 Ag19 3.1698(8) .
Ag18 Ag11 3.2095(9) 2_666
Ag19 C49 2.145(7) .
Ag19 C13 2.268(6) .
Ag19 C14 2.605(6) .
Cl1 Ag3 2.7842(16) 2_666
Cl2 Ag4 2.6259(16) 2_666
Cl3 Ag1 2.6332(16) 2_666
O1 Cl4 1.464(5) .
O2 Cl4 1.427(5) .
O3 Cl4 1.425(5) .
O4 Cl4 1.420(5) .
O5 Cl5 1.464(5) .
O6 Cl5 1.408(6) .
O7 Cl5 1.406(6) .
O8 Cl5 1.440(6) .
O9 Cl6 1.455(5) .
O10 Cl6 1.428(6) .
O11 Cl6 1.428(5) .
O12 Cl6 1.422(5) .
O13 Cl7 1.455(5) .
O14 Cl7 1.430(7) .
O15 Cl7 1.411(6) .
O16 Cl7 1.413(6) .
O17 Cl8 1.419(6) .
O18 Cl8 1.437(5) .
O19 Cl8 1.465(5) .
O20 Cl8 1.413(6) .
O21 Cl9 1.456(5) .
O22 Cl9 1.407(6) .
O23 Cl9 1.423(5) .
O24 Cl9 1.410(6) .
O25 C62 1.359(16) .
O25 C63 1.449(19) .
C1 C2 1.230(9) .
C2 C3 1.480(9) .
C3 C5 1.520(10) .
C3 C4 1.525(11) .
C3 C6 1.549(11) .
C4 H4A 0.9600 .
C4 H4B 0.9600 .
C4 H4C 0.9600 .
C5 H5A 0.9600 .
C5 H5B 0.9600 .
C5 H5C 0.9600 .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
C7 C8 1.237(9) .
C8 C9 1.454(9) .
C9 C10 1.528(10) .
C9 C12 1.531(10) .
C9 C11 1.532(10) .
C10 H10A 0.9600 .
C10 H10B 0.9600 .
C10 H10C 0.9600 .
C11 H11A 0.9600 .
C11 H11B 0.9600 .
C11 H11C 0.9600 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 C14 1.217(9) .
C14 C15 1.484(9) .
C15 C18 1.531(10) .
C15 C16 1.531(10) .
C15 C17 1.542(10) .
C16 H16A 0.9600 .
C16 H16B 0.9600 .
C16 H16C 0.9600 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C18 H18A 0.9600 .
C18 H18B 0.9600 .
C18 H18C 0.9600 .
C19 C20 1.196(9) .
C20 C21 1.497(9) .
C21 C22 1.506(11) .
C21 C24 1.524(11) .
C21 C23 1.550(12) .
C22 H22A 0.9600 .
C22 H22B 0.9600 .
C22 H22C 0.9600 .
C23 H23A 0.9600 .
C23 H23B 0.9600 .
C23 H23C 0.9600 .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
C25 C26 1.218(9) .
C26 C27 1.492(10) .
C27 C28 1.417(14) .
C27 C30A 1.419(17) .
C27 C29 1.69(2) .
C27 C30B 1.76(2) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
C29 H29A 0.9600 .
C29 H29B 0.9600 .
C29 H29C 0.9600 .
C30A H30A 0.9600 .
C30A H30B 0.9600 .
C30A H30C 0.9600 .
C30B H30D 0.9600 .
C30B H30E 0.9600 .
C30B H30F 0.9600 .
C31 C32 1.201(9) .
C31 Ag6 2.141(7) 2_666
C31 Ag18 2.225(7) 2_666
C32 C33 1.482(10) .
C32 Ag18 2.577(7) 2_666
C33 C35 1.472(16) .
C33 C36 1.534(11) .
C33 C34 1.567(16) .
C34 H34A 0.9600 .
C34 H34B 0.9600 .
C34 H34C 0.9600 .
C35 H35A 0.9600 .
C35 H35B 0.9600 .
C35 H35C 0.9600 .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
C37 C38 1.209(9) .
C37 Ag5 2.147(7) 2_666
C38 C39 1.484(9) .
C39 C42 1.527(10) .
C39 C41 1.530(10) .
C39 C40 1.531(10) .
C40 H40A 0.9600 .
C40 H40B 0.9600 .
C40 H40C 0.9600 .
C41 H41A 0.9600 .
C41 H41B 0.9600 .
C41 H41C 0.9600 .
C42 H42A 0.9600 .
C42 H42B 0.9600 .
C42 H42C 0.9600 .
C43 C44 1.230(9) .
C44 C45 1.473(9) .
C45 C48 1.534(11) .
C45 C46 1.535(10) .
C45 C47 1.543(11) .
C46 H46A 0.9600 .
C46 H46B 0.9600 .
C46 H46C 0.9600 .
C47 H47A 0.9600 .
C47 H47B 0.9600 .
C47 H47C 0.9600 .
C48 H48A 0.9600 .
C48 H48B 0.9600 .
C48 H48C 0.9600 .
C49 C50 1.205(10) .
C50 C51 1.490(10) .
C51 C52 1.513(13) .
C51 C53 1.526(12) .
C51 C54 1.526(14) .
C52 H52A 0.9600 .
C52 H52B 0.9600 .
C52 H52C 0.9600 .
C53 H53A 0.9600 .
C53 H53B 0.9600 .
C53 H53C 0.9600 .
C54 H54A 0.9600 .
C54 H54B 0.9600 .
C54 H54C 0.9600 .
C57B C57 1.029(18) .
C57B C60 1.440(15) .
C57B C58B 1.55(2) .
C57B C59 1.555(16) .
C57B C56 1.558(14) .
C57B H59C 1.5226 .
C57B H60C 1.4204 .
C55 C56 1.171(10) .
C55 Ag10 2.195(7) 2_666
C55 Ag8 2.199(7) 2_666
C56 C57 1.541(14) .
C56 Ag8 2.702(7) 2_666
C58 C57 1.541(19) .
C58 C58 1.85(3) 2_565
C58 H58A 0.9600 .
C58 H58B 0.9601 .
C58 H58C 0.9597 .
C57 C59 1.468(15) .
C57 C60 1.526(15) .
C59 H59A 0.9602 .
C59 H59B 0.9599 .
C59 H59C 0.9599 .
C60 H60A 0.9599 .
C60 H60B 0.9599 .
C60 H60C 0.9601 .
C61 C62 1.54(2) .
C61 H61A 0.9600 .
C61 H61B 0.9600 .
C61 H61C 0.9600 .
C62 H62A 0.9700 .
C62 H62B 0.9700 .
C63 C64 1.34(2) .
C63 H63A 0.9700 .
C63 H63B 0.9700 .
C64 H64A 0.9600 .
C64 H64B 0.9600 .
C64 H64C 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Ag1 Ag5 C37 179.6(3) . 2_666
Cl3 Ag1 Ag5 C37 -13.4(2) 2_666 2_666
Cl1 Ag1 Ag5 C37 -81.0(3) . 2_666
Cl2 Ag1 Ag5 C37 69.3(3) . 2_666
Ag6 Ag1 Ag5 C37 -141.4(2) . 2_666
Ag7 Ag1 Ag5 C37 138.0(2) . 2_666
Cl3 Ag1 Ag5 C1 167.1(2) 2_666 .
Cl1 Ag1 Ag5 C1 99.5(2) . .
Cl2 Ag1 Ag5 C1 -110.3(2) . .
Ag6 Ag1 Ag5 C1 39.0(2) . .
Ag7 Ag1 Ag5 C1 -41.6(2) . .
C1 Ag1 Ag5 C2 -2.3(3) . .
Cl3 Ag1 Ag5 C2 164.76(15) 2_666 .
Cl1 Ag1 Ag5 C2 97.20(16) . .
Cl2 Ag1 Ag5 C2 -112.56(15) . .
Ag6 Ag1 Ag5 C2 36.73(15) . .
Ag7 Ag1 Ag5 C2 -43.87(15) . .
C1 Ag1 Ag5 Ag15 144.2(2) . 2_666
Cl3 Ag1 Ag5 Ag15 -48.78(4) 2_666 2_666
Cl1 Ag1 Ag5 Ag15 -116.34(8) . 2_666
Cl2 Ag1 Ag5 Ag15 33.90(4) . 2_666
Ag6 Ag1 Ag5 Ag15 -176.82(2) . 2_666
Ag7 Ag1 Ag5 Ag15 102.59(2) . 2_666
C1 Ag1 Ag5 Ag13 -150.0(2) . 2_666
Cl3 Ag1 Ag5 Ag13 17.07(4) 2_666 2_666
Cl1 Ag1 Ag5 Ag13 -50.49(8) . 2_666
Cl2 Ag1 Ag5 Ag13 99.75(4) . 2_666
Ag6 Ag1 Ag5 Ag13 -110.96(2) . 2_666
Ag7 Ag1 Ag5 Ag13 168.44(2) . 2_666
C1 Ag1 Ag6 C31 175.2(3) . 2_666
Cl3 Ag1 Ag6 C31 70.3(2) 2_666 2_666
Cl1 Ag1 Ag6 C31 -16.0(2) . 2_666
Cl2 Ag1 Ag6 C31 -96.0(2) . 2_666
Ag7 Ag1 Ag6 C31 -140.7(2) . 2_666
Ag5 Ag1 Ag6 C31 136.9(2) . 2_666
Cl3 Ag1 Ag6 C1 -105.0(2) 2_666 .
Cl1 Ag1 Ag6 C1 168.7(2) . .
Cl2 Ag1 Ag6 C1 88.7(2) . .
Ag7 Ag1 Ag6 C1 44.1(2) . .
Ag5 Ag1 Ag6 C1 -38.4(2) . .
C1 Ag1 Ag6 C2 2.4(3) . .
Cl3 Ag1 Ag6 C2 -102.61(15) 2_666 .
Cl1 Ag1 Ag6 C2 171.11(15) . .
Cl2 Ag1 Ag6 C2 91.11(16) . .
Ag7 Ag1 Ag6 C2 46.47(15) . .
Ag5 Ag1 Ag6 C2 -36.00(15) . .
C1 Ag1 Ag6 Ag11 147.7(2) . 2_666
Cl3 Ag1 Ag6 Ag11 42.75(5) 2_666 2_666
Cl1 Ag1 Ag6 Ag11 -43.53(4) . 2_666
Cl2 Ag1 Ag6 Ag11 -123.53(7) . 2_666
Ag7 Ag1 Ag6 Ag11 -168.16(2) . 2_666
Ag5 Ag1 Ag6 Ag11 109.36(2) . 2_666
C1 Ag1 Ag7 C7 168.1(3) . .
Cl3 Ag1 Ag7 C7 -101.0(3) 2_666 .
Cl1 Ag1 Ag7 C7 51.7(3) . .
Cl2 Ag1 Ag7 C7 -31.6(3) . .
Ag6 Ag1 Ag7 C7 123.5(3) . .
Ag5 Ag1 Ag7 C7 -150.6(3) . .
Cl3 Ag1 Ag7 C1 90.9(2) 2_666 .
Cl1 Ag1 Ag7 C1 -116.3(2) . .
Cl2 Ag1 Ag7 C1 160.4(2) . .
Ag6 Ag1 Ag7 C1 -44.6(2) . .
Ag5 Ag1 Ag7 C1 41.3(2) . .
C1 Ag1 Ag7 Ag9 143.8(2) . .
Cl3 Ag1 Ag7 Ag9 -125.27(6) 2_666 .
Cl1 Ag1 Ag7 Ag9 27.47(5) . .
Cl2 Ag1 Ag7 Ag9 -55.83(4) . .
Ag6 Ag1 Ag7 Ag9 99.19(2) . .
Ag5 Ag1 Ag7 Ag9 -174.85(2) . .
C1 Ag1 Ag7 Ag8 -150.6(2) . .
Cl3 Ag1 Ag7 Ag8 -59.67(7) 2_666 .
Cl1 Ag1 Ag7 Ag8 93.08(5) . .
Cl2 Ag1 Ag7 Ag8 9.78(4) . .
Ag6 Ag1 Ag7 Ag8 164.79(2) . .
Ag5 Ag1 Ag7 Ag8 -109.24(2) . .
C7 Ag7 Ag8 C55 -176.5(4) . 2_666
C1 Ag7 Ag8 C55 6.1(4) . 2_666
Ag9 Ag7 Ag8 C55 132.1(3) . 2_666
Ag1 Ag7 Ag8 C55 48.0(3) . 2_666
C1 Ag7 Ag8 C7 -177.4(4) . .
Ag9 Ag7 Ag8 C7 -51.5(3) . .
Ag1 Ag7 Ag8 C7 -135.5(3) . .
C7 Ag7 Ag8 C8 -22.3(3) . .
C1 Ag7 Ag8 C8 160.3(3) . .
Ag9 Ag7 Ag8 C8 -73.75(16) . .
Ag1 Ag7 Ag8 C8 -157.81(16) . .
C7 Ag7 Ag8 C56 -150.8(5) . 2_666
C1 Ag7 Ag8 C56 31.8(5) . 2_666
Ag9 Ag7 Ag8 C56 157.8(4) . 2_666
Ag1 Ag7 Ag8 C56 73.7(4) . 2_666
C7 Ag7 Ag8 Ag16 -177.1(3) . 2_666
C1 Ag7 Ag8 Ag16 5.5(3) . 2_666
Ag9 Ag7 Ag8 Ag16 131.39(2) . 2_666
Ag1 Ag7 Ag8 Ag16 47.33(3) . 2_666
C13 Ag2 Ag9 C7 167.5(3) . .
Cl3 Ag2 Ag9 C7 81.3(3) . .
Cl1 Ag2 Ag9 C7 -78.0(3) . .
Cl2 Ag2 Ag9 C7 9.8(3) . .
Ag19 Ag2 Ag9 C7 -151.7(3) . .
Ag14 Ag2 Ag9 C7 126.5(3) . .
Cl3 Ag2 Ag9 C13 -86.2(2) . .
Cl1 Ag2 Ag9 C13 114.5(2) . .
Cl2 Ag2 Ag9 C13 -157.8(2) . .
Ag19 Ag2 Ag9 C13 40.7(2) . .
Ag14 Ag2 Ag9 C13 -41.0(2) . .
C13 Ag2 Ag9 Ag7 -159.2(2) . .
Cl3 Ag2 Ag9 Ag7 114.61(8) . .
Cl1 Ag2 Ag9 Ag7 -44.74(5) . .
Cl2 Ag2 Ag9 Ag7 43.04(4) . .
Ag19 Ag2 Ag9 Ag7 -118.46(2) . .
Ag14 Ag2 Ag9 Ag7 159.76(2) . .
C1 Ag7 Ag9 C7 -169.1(3) . .
Ag1 Ag7 Ag9 C7 156.5(3) . .
Ag8 Ag7 Ag9 C7 45.7(3) . .
C7 Ag7 Ag9 C13 -172.5(4) . .
C1 Ag7 Ag9 C13 18.4(3) . .
Ag1 Ag7 Ag9 C13 -16.0(3) . .
Ag8 Ag7 Ag9 C13 -126.9(3) . .
C7 Ag7 Ag9 Ag2 -147.9(3) . .
C1 Ag7 Ag9 Ag2 43.1(2) . .
Ag1 Ag7 Ag9 Ag2 8.63(2) . .
Ag8 Ag7 Ag9 Ag2 -102.19(2) . .
C25 Ag3 Ag10 C55 -170.8(3) . 2_666
Cl2 Ag3 Ag10 C55 2.3(2) . 2_666
Cl3 Ag3 Ag10 C55 -73.2(3) . 2_666
Cl1 Ag3 Ag10 C55 87.3(2) 2_666 2_666
Ag12 Ag3 Ag10 C55 -129.6(2) . 2_666
Ag11 Ag3 Ag10 C55 147.1(2) . 2_666
Cl2 Ag3 Ag10 C25 173.1(2) . .
Cl3 Ag3 Ag10 C25 97.6(2) . .
Cl1 Ag3 Ag10 C25 -101.9(2) 2_666 .
Ag12 Ag3 Ag10 C25 41.2(2) . .
Ag11 Ag3 Ag10 C25 -42.1(2) . .
C25 Ag3 Ag10 Ag16 152.1(2) . 2_666
Cl2 Ag3 Ag10 Ag16 -34.73(4) . 2_666
Cl3 Ag3 Ag10 Ag16 -110.29(11) . 2_666
Cl1 Ag3 Ag10 Ag16 50.21(4) 2_666 2_666
Ag12 Ag3 Ag10 Ag16 -166.70(2) . 2_666
Ag11 Ag3 Ag10 Ag16 110.00(2) . 2_666
C25 Ag3 Ag11 C31 172.8(4) . .
Cl2 Ag3 Ag11 C31 -79.5(3) . .
Cl3 Ag3 Ag11 C31 50.4(3) . .
Cl1 Ag3 Ag11 C31 -26.8(3) 2_666 .
Ag10 Ag3 Ag11 C31 -143.7(3) . .
Ag12 Ag3 Ag11 C31 131.7(3) . .
Cl2 Ag3 Ag11 C25 107.7(2) . .
Cl3 Ag3 Ag11 C25 -122.3(2) . .
Cl1 Ag3 Ag11 C25 160.4(2) 2_666 .
Ag10 Ag3 Ag11 C25 43.5(2) . .
Ag12 Ag3 Ag11 C25 -41.0(2) . .
C25 Ag3 Ag11 C26 1.8(3) . .
Cl2 Ag3 Ag11 C26 109.56(17) . .
Cl3 Ag3 Ag11 C26 -120.52(16) . .
Cl1 Ag3 Ag11 C26 162.22(16) 2_666 .
Ag10 Ag3 Ag11 C26 45.29(16) . .
Ag12 Ag3 Ag11 C26 -39.22(16) . .
C25 Ag3 Ag11 Ag6 144.0(2) . 2_666
Cl2 Ag3 Ag11 Ag6 -108.23(6) . 2_666
Cl3 Ag3 Ag11 Ag6 21.68(5) . 2_666
Cl1 Ag3 Ag11 Ag6 -55.57(4) 2_666 2_666
Ag10 Ag3 Ag11 Ag6 -172.51(2) . 2_666
Ag12 Ag3 Ag11 Ag6 102.98(3) . 2_666
C25 Ag3 Ag11 Ag18 -142.9(2) . 2_666
Cl2 Ag3 Ag11 Ag18 -35.11(7) . 2_666
Cl3 Ag3 Ag11 Ag18 94.80(5) . 2_666
Cl1 Ag3 Ag11 Ag18 17.55(4) 2_666 2_666
Ag10 Ag3 Ag11 Ag18 -99.39(3) . 2_666
Ag12 Ag3 Ag11 Ag18 176.10(3) . 2_666
C25 Ag3 Ag12 C19 171.5(3) . .
Cl2 Ag3 Ag12 C19 56.6(2) . .
Cl3 Ag3 Ag12 C19 -32.9(2) . .
Cl1 Ag3 Ag12 C19 -116.0(2) 2_666 .
Ag10 Ag3 Ag12 C19 130.4(2) . .
Ag11 Ag3 Ag12 C19 -148.8(2) . .
Cl2 Ag3 Ag12 C25 -114.9(2) . .
Cl3 Ag3 Ag12 C25 155.6(2) . .
Cl1 Ag3 Ag12 C25 72.5(2) 2_666 .
Ag10 Ag3 Ag12 C25 -41.1(2) . .
Ag11 Ag3 Ag12 C25 39.7(2) . .
C25 Ag3 Ag12 C20 161.1(4) . .
Cl2 Ag3 Ag12 C20 46.2(3) . .
Cl3 Ag3 Ag12 C20 -43.3(3) . .
Cl1 Ag3 Ag12 C20 -126.5(3) 2_666 .
Ag10 Ag3 Ag12 C20 120.0(3) . .
Ag11 Ag3 Ag12 C20 -159.2(3) . .
C25 Ag3 Ag12 C26 -2.9(3) . .
Cl2 Ag3 Ag12 C26 -117.80(17) . .
Cl3 Ag3 Ag12 C26 152.70(17) . .
Cl1 Ag3 Ag12 C26 69.54(17) 2_666 .
Ag10 Ag3 Ag12 C26 -44.00(16) . .
Ag11 Ag3 Ag12 C26 36.80(16) . .
C25 Ag3 Ag12 Ag14 153.5(2) . .
Cl2 Ag3 Ag12 Ag14 38.66(5) . .
Cl3 Ag3 Ag12 Ag14 -50.84(4) . .
Cl1 Ag3 Ag12 Ag14 -134.00(6) 2_666 .
Ag10 Ag3 Ag12 Ag14 112.46(2) . .
Ag11 Ag3 Ag12 Ag14 -166.74(2) . .
C25 Ag3 Ag12 Ag13 -154.2(2) . .
Cl2 Ag3 Ag12 Ag13 90.95(5) . .
Cl3 Ag3 Ag12 Ag13 1.45(4) . .
Cl1 Ag3 Ag12 Ag13 -81.71(6) 2_666 .
Ag10 Ag3 Ag12 Ag13 164.74(2) . .
Ag11 Ag3 Ag12 Ag13 -114.46(2) . .
C25 Ag12 Ag13 C19 -161.2(3) . .
C20 Ag12 Ag13 C19 21.9(3) . .
C26 Ag12 Ag13 C19 158.7(4) . .
Ag3 Ag12 Ag13 C19 -133.4(3) . .
Ag14 Ag12 Ag13 C19 -55.6(3) . .
C19 Ag12 Ag13 C37 -158.1(4) . .
C25 Ag12 Ag13 C37 40.6(3) . .
C20 Ag12 Ag13 C37 -136.2(3) . .
C26 Ag12 Ag13 C37 0.6(4) . .
Ag3 Ag12 Ag13 C37 68.5(3) . .
Ag14 Ag12 Ag13 C37 146.3(3) . .
C19 Ag12 Ag13 C38 -112.5(3) . .
C25 Ag12 Ag13 C38 86.3(3) . .
C20 Ag12 Ag13 C38 -90.6(3) . .
C26 Ag12 Ag13 C38 46.2(4) . .
Ag3 Ag12 Ag13 C38 114.1(2) . .
Ag14 Ag12 Ag13 C38 -168.1(2) . .
C19 Ag12 Ag13 Ag14 55.6(3) . .
C25 Ag12 Ag13 Ag14 -105.6(2) . .
C20 Ag12 Ag13 Ag14 77.50(17) . .
C26 Ag12 Ag13 Ag14 -145.7(3) . .
Ag3 Ag12 Ag13 Ag14 -77.79(2) . .
C19 Ag12 Ag13 Ag5 -171.2(3) . 2_666
C25 Ag12 Ag13 Ag5 27.5(2) . 2_666
C20 Ag12 Ag13 Ag5 -149.34(17) . 2_666
C26 Ag12 Ag13 Ag5 -12.5(3) . 2_666
Ag3 Ag12 Ag13 Ag5 55.38(2) . 2_666
Ag14 Ag12 Ag13 Ag5 133.17(2) . 2_666
C37 Ag13 Ag14 C19 172.8(4) . .
C38 Ag13 Ag14 C19 112.7(4) . .
Ag12 Ag13 Ag14 C19 -49.0(2) . .
Ag5 Ag13 Ag14 C19 -128.1(2) 2_666 .
C19 Ag13 Ag14 C13 -176.6(3) . .
C37 Ag13 Ag14 C13 -3.8(4) . .
C38 Ag13 Ag14 C13 -63.8(4) . .
Ag12 Ag13 Ag14 C13 134.4(2) . .
Ag5 Ag13 Ag14 C13 55.4(2) 2_666 .
C19 Ag13 Ag14 C14 -137.8(3) . .
C37 Ag13 Ag14 C14 35.0(4) . .
C38 Ag13 Ag14 C14 -25.1(4) . .
Ag12 Ag13 Ag14 C14 173.2(2) . .
Ag5 Ag13 Ag14 C14 94.1(2) 2_666 .
C19 Ag13 Ag14 Ag2 144.6(2) . .
C37 Ag13 Ag14 Ag2 -42.7(3) . .
C38 Ag13 Ag14 Ag2 -102.7(4) . .
Ag12 Ag13 Ag14 Ag2 95.56(2) . .
Ag5 Ag13 Ag14 Ag2 16.47(4) 2_666 .
C19 Ag13 Ag14 Ag12 49.0(2) . .
C37 Ag13 Ag14 Ag12 -138.2(3) . .
C38 Ag13 Ag14 Ag12 161.7(4) . .
Ag5 Ag13 Ag14 Ag12 -79.09(3) 2_666 .
C13 Ag2 Ag14 C19 -180.0(3) . .
Cl3 Ag2 Ag14 C19 20.8(3) . .
Cl1 Ag2 Ag14 C19 93.7(3) . .
Cl2 Ag2 Ag14 C19 -65.4(3) . .
Ag9 Ag2 Ag14 C19 -138.2(3) . .
Ag19 Ag2 Ag14 C19 137.6(3) . .
Cl3 Ag2 Ag14 C13 -159.2(2) . .
Cl1 Ag2 Ag14 C13 -86.3(2) . .
Cl2 Ag2 Ag14 C13 114.5(2) . .
Ag9 Ag2 Ag14 C13 41.8(2) . .
Ag19 Ag2 Ag14 C13 -42.4(2) . .
C13 Ag2 Ag14 C14 1.6(3) . .
Cl3 Ag2 Ag14 C14 -157.61(15) . .
Cl1 Ag2 Ag14 C14 -84.71(16) . .
Cl2 Ag2 Ag14 C14 116.13(15) . .
Ag9 Ag2 Ag14 C14 43.39(14) . .
Ag19 Ag2 Ag14 C14 -40.85(14) . .
C13 Ag2 Ag14 Ag13 141.3(2) . .
Cl3 Ag2 Ag14 Ag13 -17.94(4) . .
Cl1 Ag2 Ag14 Ag13 54.97(8) . .
Cl2 Ag2 Ag14 Ag13 -104.20(4) . .
Ag9 Ag2 Ag14 Ag13 -176.94(2) . .
Ag19 Ag2 Ag14 Ag13 98.82(2) . .
C13 Ag2 Ag14 Ag12 -153.3(2) . .
Cl3 Ag2 Ag14 Ag12 47.47(4) . .
Cl1 Ag2 Ag14 Ag12 120.38(8) . .
Cl2 Ag2 Ag14 Ag12 -38.78(4) . .
Ag9 Ag2 Ag14 Ag12 -111.53(2) . .
Ag19 Ag2 Ag14 Ag12 164.23(2) . .
C25 Ag12 Ag14 C19 -179.4(3) . .
C20 Ag12 Ag14 C19 -18.7(3) . .
C26 Ag12 Ag14 C19 -157.1(4) . .
Ag3 Ag12 Ag14 C19 156.9(3) . .
Ag13 Ag12 Ag14 C19 54.7(3) . .
C19 Ag12 Ag14 C13 177.0(4) . .
C25 Ag12 Ag14 C13 -2.4(3) . .
C20 Ag12 Ag14 C13 158.3(3) . .
C26 Ag12 Ag14 C13 19.9(4) . .
Ag3 Ag12 Ag14 C13 -26.1(2) . .
Ag13 Ag12 Ag14 C13 -128.3(2) . .
C19 Ag12 Ag14 C14 135.4(4) . .
C25 Ag12 Ag14 C14 -44.0(4) . .
C20 Ag12 Ag14 C14 116.6(4) . .
C26 Ag12 Ag14 C14 -21.7(4) . .
Ag3 Ag12 Ag14 C14 -67.8(3) . .
Ag13 Ag12 Ag14 C14 -169.9(3) . .
C19 Ag12 Ag14 Ag13 -54.7(3) . .
C25 Ag12 Ag14 Ag13 125.86(19) . .
C20 Ag12 Ag14 Ag13 -73.47(17) . .
C26 Ag12 Ag14 Ag13 148.2(3) . .
Ag3 Ag12 Ag14 Ag13 102.14(2) . .
C19 Ag12 Ag14 Ag2 -153.3(3) . .
C25 Ag12 Ag14 Ag2 27.27(19) . .
C20 Ag12 Ag14 Ag2 -172.06(17) . .
C26 Ag12 Ag14 Ag2 49.6(3) . .
Ag3 Ag12 Ag14 Ag2 3.56(2) . .
Ag13 Ag12 Ag14 Ag2 -98.59(2) . .
C43 Ag4 Ag15 C37 177.3(3) . .
Cl2 Ag4 Ag15 C37 66.9(2) 2_666 .
Cl1 Ag4 Ag15 C37 -83.3(3) . .
Cl3 Ag4 Ag15 C37 -13.7(2) . .
Ag17 Ag4 Ag15 C37 -139.1(2) . .
Ag16 Ag4 Ag15 C37 135.9(2) . .
Cl2 Ag4 Ag15 C43 -110.3(2) 2_666 .
Cl1 Ag4 Ag15 C43 99.5(2) . .
Cl3 Ag4 Ag15 C43 169.0(2) . .
Ag17 Ag4 Ag15 C43 43.6(2) . .
Ag16 Ag4 Ag15 C43 -41.3(2) . .
C43 Ag4 Ag15 C44 -0.7(3) . .
Cl2 Ag4 Ag15 C44 -111.06(16) 2_666 .
Cl1 Ag4 Ag15 C44 98.75(17) . .
Cl3 Ag4 Ag15 C44 168.28(16) . .
Ag17 Ag4 Ag15 C44 42.89(15) . .
Ag16 Ag4 Ag15 C44 -42.04(15) . .
C43 Ag4 Ag15 Ag5 143.4(2) . 2_666
Cl2 Ag4 Ag15 Ag5 33.10(5) 2_666 2_666
Cl1 Ag4 Ag15 Ag5 -117.09(7) . 2_666
Cl3 Ag4 Ag15 Ag5 -47.56(4) . 2_666
Ag17 Ag4 Ag15 Ag5 -172.95(2) . 2_666
Ag16 Ag4 Ag15 Ag5 102.12(2) . 2_666
C43 Ag4 Ag16 C55 161.3(3) . .
Cl2 Ag4 Ag16 C55 -34.0(3) 2_666 .
Cl1 Ag4 Ag16 C55 48.0(3) . .
Cl3 Ag4 Ag16 C55 -103.7(3) . .
Ag17 Ag4 Ag16 C55 121.0(3) . .
Ag15 Ag4 Ag16 C55 -157.8(3) . .
Cl2 Ag4 Ag16 C43 164.7(2) 2_666 .
Cl1 Ag4 Ag16 C43 -113.3(2) . .
Cl3 Ag4 Ag16 C43 95.0(2) . .
Ag17 Ag4 Ag16 C43 -40.4(2) . .
Ag15 Ag4 Ag16 C43 40.9(2) . .
C43 Ag4 Ag16 Ag10 136.3(2) . 2_666
Cl2 Ag4 Ag16 Ag10 -58.95(4) 2_666 2_666
Cl1 Ag4 Ag16 Ag10 23.03(5) . 2_666
Cl3 Ag4 Ag16 Ag10 -128.72(6) . 2_666
Ag17 Ag4 Ag16 Ag10 95.97(2) . 2_666
Ag15 Ag4 Ag16 Ag10 177.25(2) . 2_666
C43 Ag4 Ag16 Ag8 -155.7(2) . 2_666
Cl2 Ag4 Ag16 Ag8 8.98(4) 2_666 2_666
Cl1 Ag4 Ag16 Ag8 90.96(5) . 2_666
Cl3 Ag4 Ag16 Ag8 -60.79(6) . 2_666
Ag17 Ag4 Ag16 Ag8 163.90(2) . 2_666
Ag15 Ag4 Ag16 Ag8 -114.82(2) . 2_666
C43 Ag4 Ag17 C49 164.4(3) . .
Cl2 Ag4 Ag17 C49 -104.3(3) 2_666 .
Cl1 Ag4 Ag17 C49 -29.5(2) . .
Cl3 Ag4 Ag17 C49 54.3(2) . .
Ag15 Ag4 Ag17 C49 121.6(2) . .
Ag16 Ag4 Ag17 C49 -155.5(2) . .
Cl2 Ag4 Ag17 C43 91.2(2) 2_666 .
Cl1 Ag4 Ag17 C43 166.0(2) . .
Cl3 Ag4 Ag17 C43 -110.2(2) . .
Ag15 Ag4 Ag17 C43 -42.8(2) . .
Ag16 Ag4 Ag17 C43 40.0(2) . .
C43 Ag4 Ag17 Ag19 141.0(2) . .
Cl2 Ag4 Ag17 Ag19 -127.73(7) 2_666 .
Cl1 Ag4 Ag17 Ag19 -52.95(4) . .
Cl3 Ag4 Ag17 Ag19 30.85(4) . .
Ag15 Ag4 Ag17 Ag19 98.24(2) . .
Ag16 Ag4 Ag17 Ag19 -178.94(2) . .
C43 Ag4 Ag17 Ag18 -158.1(2) . .
Cl2 Ag4 Ag17 Ag18 -66.88(8) 2_666 .
Cl1 Ag4 Ag17 Ag18 7.90(4) . .
Cl3 Ag4 Ag17 Ag18 91.70(4) . .
Ag15 Ag4 Ag17 Ag18 159.09(2) . .
Ag16 Ag4 Ag17 Ag18 -118.09(2) . .
C43 Ag17 Ag18 C49 -170.0(4) . .
Ag4 Ag17 Ag18 C49 -138.5(3) . .
Ag19 Ag17 Ag18 C49 -55.4(3) . .
C49 Ag17 Ag18 C31 -174.7(4) . 2_666
C43 Ag17 Ag18 C31 15.3(4) . 2_666
Ag4 Ag17 Ag18 C31 46.7(3) . 2_666
Ag19 Ag17 Ag18 C31 129.8(3) . 2_666
C49 Ag17 Ag18 C32 -132.4(4) . 2_666
C43 Ag17 Ag18 C32 57.6(4) . 2_666
Ag4 Ag17 Ag18 C32 89.1(3) . 2_666
Ag19 Ag17 Ag18 C32 172.2(3) . 2_666
C49 Ag17 Ag18 Ag19 55.4(3) . .
C43 Ag17 Ag18 Ag19 -114.6(3) . .
Ag4 Ag17 Ag18 Ag19 -83.11(2) . .
C49 Ag17 Ag18 Ag11 -178.6(3) . 2_666
C43 Ag17 Ag18 Ag11 11.4(3) . 2_666
Ag4 Ag17 Ag18 Ag11 42.90(3) . 2_666
Ag19 Ag17 Ag18 Ag11 126.01(3) . 2_666
C43 Ag17 Ag19 C49 -167.8(3) . .
Ag4 Ag17 Ag19 C49 156.5(2) . .
Ag18 Ag17 Ag19 C49 49.3(2) . .
C49 Ag17 Ag19 C13 -174.6(3) . .
C43 Ag17 Ag19 C13 17.6(3) . .
Ag4 Ag17 Ag19 C13 -18.1(2) . .
Ag18 Ag17 Ag19 C13 -125.3(2) . .
C49 Ag17 Ag19 C14 140.7(5) . .
C43 Ag17 Ag19 C14 -27.1(4) . .
Ag4 Ag17 Ag19 C14 -62.8(4) . .
Ag18 Ag17 Ag19 C14 -170.0(4) . .
C49 Ag17 Ag19 Ag2 -150.1(2) . .
C43 Ag17 Ag19 Ag2 42.2(2) . .
Ag4 Ag17 Ag19 Ag2 6.43(2) . .
Ag18 Ag17 Ag19 Ag2 -100.75(2) . .
C49 Ag17 Ag19 Ag18 -49.3(2) . .
C43 Ag17 Ag19 Ag18 142.9(2) . .
Ag4 Ag17 Ag19 Ag18 107.17(2) . .
C13 Ag2 Ag19 C49 170.0(3) . .
Cl3 Ag2 Ag19 C49 -76.5(3) . .
Cl1 Ag2 Ag19 C49 12.2(3) . .
Cl2 Ag2 Ag19 C49 85.1(3) . .
Ag9 Ag2 Ag19 C49 128.9(3) . .
Ag14 Ag2 Ag19 C49 -147.9(3) . .
Cl3 Ag2 Ag19 C13 113.5(2) . .
Cl1 Ag2 Ag19 C13 -157.8(2) . .
Cl2 Ag2 Ag19 C13 -85.0(2) . .
Ag9 Ag2 Ag19 C13 -41.1(2) . .
Ag14 Ag2 Ag19 C13 42.1(2) . .
C13 Ag2 Ag19 C14 0.0(3) . .
Cl3 Ag2 Ag19 C14 113.48(15) . .
Cl1 Ag2 Ag19 C14 -157.79(14) . .
Cl2 Ag2 Ag19 C14 -84.97(16) . .
Ag9 Ag2 Ag19 C14 -41.12(14) . .
Ag14 Ag2 Ag19 C14 42.07(14) . .
C13 Ag2 Ag19 Ag17 -158.5(2) . .
Cl3 Ag2 Ag19 Ag17 -44.99(4) . .
Cl1 Ag2 Ag19 Ag17 43.74(4) . .
Cl2 Ag2 Ag19 Ag17 116.56(8) . .
Ag9 Ag2 Ag19 Ag17 160.42(2) . .
Ag14 Ag2 Ag19 Ag17 -116.40(2) . .
C13 Ag2 Ag19 Ag18 136.8(2) . .
Cl3 Ag2 Ag19 Ag18 -109.69(4) . .
Cl1 Ag2 Ag19 Ag18 -20.97(4) . .
Cl2 Ag2 Ag19 Ag18 51.86(9) . .
Ag9 Ag2 Ag19 Ag18 95.71(2) . .
Ag14 Ag2 Ag19 Ag18 178.90(2) . .
C31 Ag18 Ag19 C49 -177.1(4) 2_666 .
C32 Ag18 Ag19 C49 135.3(5) 2_666 .
Ag11 Ag18 Ag19 C49 -126.0(3) 2_666 .
Ag17 Ag18 Ag19 C49 -53.2(3) . .
C49 Ag18 Ag19 C13 -171.6(3) . .
C31 Ag18 Ag19 C13 11.3(4) 2_666 .
C32 Ag18 Ag19 C13 -36.3(4) 2_666 .
Ag11 Ag18 Ag19 C13 62.4(2) 2_666 .
Ag17 Ag18 Ag19 C13 135.2(2) . .
C49 Ag18 Ag19 C14 -132.5(3) . .
C31 Ag18 Ag19 C14 50.4(4) 2_666 .
C32 Ag18 Ag19 C14 2.8(4) 2_666 .
Ag11 Ag18 Ag19 C14 101.6(2) 2_666 .
Ag17 Ag18 Ag19 C14 174.3(2) . .
C49 Ag18 Ag19 Ag17 53.2(3) . .
C31 Ag18 Ag19 Ag17 -123.9(3) 2_666 .
C32 Ag18 Ag19 Ag17 -171.5(4) 2_666 .
Ag11 Ag18 Ag19 Ag17 -72.76(3) 2_666 .
C49 Ag18 Ag19 Ag2 146.5(3) . .
C31 Ag18 Ag19 Ag2 -30.6(3) 2_666 .
C32 Ag18 Ag19 Ag2 -78.2(4) 2_666 .
Ag11 Ag18 Ag19 Ag2 20.56(3) 2_666 .
Ag17 Ag18 Ag19 Ag2 93.32(2) . .
C13 Ag2 Cl1 Ag4 -107.8(2) . .
Cl3 Ag2 Cl1 Ag4 25.57(5) . .
Cl2 Ag2 Cl1 Ag4 117.71(5) . .
Ag9 Ag2 Cl1 Ag4 -164.45(3) . .
Ag19 Ag2 Cl1 Ag4 -87.64(3) . .
Ag14 Ag2 Cl1 Ag4 -43.30(9) . .
C13 Ag2 Cl1 Ag1 110.0(2) . .
Cl3 Ag2 Cl1 Ag1 -116.65(5) . .
Cl2 Ag2 Cl1 Ag1 -24.51(5) . .
Ag9 Ag2 Cl1 Ag1 53.33(5) . .
Ag19 Ag2 Cl1 Ag1 130.14(4) . .
Ag14 Ag2 Cl1 Ag1 174.49(6) . .
C13 Ag2 Cl1 Ag3 -179.9(2) . 2_666
Cl3 Ag2 Cl1 Ag3 -46.60(9) . 2_666
Cl2 Ag2 Cl1 Ag3 45.54(9) . 2_666
Ag9 Ag2 Cl1 Ag3 123.38(8) . 2_666
Ag19 Ag2 Cl1 Ag3 -159.81(9) . 2_666
Ag14 Ag2 Cl1 Ag3 -115.47(9) . 2_666
C43 Ag4 Cl1 Ag2 110.9(2) . .
Cl2 Ag4 Cl1 Ag2 -113.23(5) 2_666 .
Cl3 Ag4 Cl1 Ag2 -24.12(5) . .
Ag17 Ag4 Cl1 Ag2 97.43(4) . .
Ag15 Ag4 Cl1 Ag2 41.30(8) . .
Ag16 Ag4 Cl1 Ag2 172.53(3) . .
C43 Ag4 Cl1 Ag1 -178.2(2) . .
Cl2 Ag4 Cl1 Ag1 -42.33(10) 2_666 .
Cl3 Ag4 Cl1 Ag1 46.78(10) . .
Ag17 Ag4 Cl1 Ag1 168.33(10) . .
Ag15 Ag4 Cl1 Ag1 112.20(9) . .
Ag16 Ag4 Cl1 Ag1 -116.57(9) . .
C43 Ag4 Cl1 Ag3 -110.2(2) . 2_666
Cl2 Ag4 Cl1 Ag3 25.65(4) 2_666 2_666
Cl3 Ag4 Cl1 Ag3 114.76(4) . 2_666
Ag17 Ag4 Cl1 Ag3 -123.69(4) . 2_666
Ag15 Ag4 Cl1 Ag3 -179.81(4) . 2_666
Ag16 Ag4 Cl1 Ag3 -48.59(5) . 2_666
C1 Ag1 Cl1 Ag2 -109.8(2) . .
Cl3 Ag1 Cl1 Ag2 114.71(5) 2_666 .
Cl2 Ag1 Cl1 Ag2 24.31(5) . .
Ag6 Ag1 Cl1 Ag2 -120.84(4) . .
Ag7 Ag1 Cl1 Ag2 -49.18(5) . .
Ag5 Ag1 Cl1 Ag2 177.58(5) . .
C1 Ag1 Cl1 Ag4 179.0(2) . .
Cl3 Ag1 Cl1 Ag4 43.54(10) 2_666 .
Cl2 Ag1 Cl1 Ag4 -46.86(10) . .
Ag6 Ag1 Cl1 Ag4 168.00(10) . .
Ag7 Ag1 Cl1 Ag4 -120.34(9) . .
Ag5 Ag1 Cl1 Ag4 106.41(10) . .
C1 Ag1 Cl1 Ag3 110.8(2) . 2_666
Cl3 Ag1 Cl1 Ag3 -24.71(4) 2_666 2_666
Cl2 Ag1 Cl1 Ag3 -115.11(4) . 2_666
Ag6 Ag1 Cl1 Ag3 99.74(3) . 2_666
Ag7 Ag1 Cl1 Ag3 171.40(3) . 2_666
Ag5 Ag1 Cl1 Ag3 38.16(9) . 2_666
C25 Ag3 Cl2 Ag4 91.5(2) . 2_666
Cl3 Ag3 Cl2 Ag4 -114.96(5) . 2_666
Cl1 Ag3 Cl2 Ag4 -25.67(4) 2_666 2_666
Ag10 Ag3 Cl2 Ag4 84.51(4) . 2_666
Ag12 Ag3 Cl2 Ag4 158.86(3) . 2_666
Ag11 Ag3 Cl2 Ag4 20.90(8) . 2_666
C25 Ag3 Cl2 Ag2 -126.7(2) . .
Cl3 Ag3 Cl2 Ag2 26.85(5) . .
Cl1 Ag3 Cl2 Ag2 116.14(4) 2_666 .
Ag10 Ag3 Cl2 Ag2 -133.68(4) . .
Ag12 Ag3 Cl2 Ag2 -59.33(5) . .
Ag11 Ag3 Cl2 Ag2 162.71(4) . .
C25 Ag3 Cl2 Ag1 169.7(2) . .
Cl3 Ag3 Cl2 Ag1 -36.76(10) . .
Cl1 Ag3 Cl2 Ag1 52.54(10) 2_666 .
Ag10 Ag3 Cl2 Ag1 162.72(10) . .
Ag12 Ag3 Cl2 Ag1 -122.94(8) . .
Ag11 Ag3 Cl2 Ag1 99.10(10) . .
C13 Ag2 Cl2 Ag3 104.74(19) . .
Cl3 Ag2 Cl2 Ag3 -27.08(5) . .
Cl1 Ag2 Cl2 Ag3 -120.71(5) . .
Ag9 Ag2 Cl2 Ag3 125.05(4) . .
Ag19 Ag2 Cl2 Ag3 169.80(6) . .
Ag14 Ag2 Cl2 Ag3 49.44(4) . .
C13 Ag2 Cl2 Ag4 177.3(2) . 2_666
Cl3 Ag2 Cl2 Ag4 45.46(10) . 2_666
Cl1 Ag2 Cl2 Ag4 -48.16(10) . 2_666
Ag9 Ag2 Cl2 Ag4 -162.41(9) . 2_666
Ag19 Ag2 Cl2 Ag4 -117.65(9) . 2_666
Ag14 Ag2 Cl2 Ag4 121.99(8) . 2_666
C13 Ag2 Cl2 Ag1 -110.42(19) . .
Cl3 Ag2 Cl2 Ag1 117.76(4) . .
Cl1 Ag2 Cl2 Ag1 24.13(5) . .
Ag9 Ag2 Cl2 Ag1 -90.11(3) . .
Ag19 Ag2 Cl2 Ag1 -45.35(10) . .
Ag14 Ag2 Cl2 Ag1 -165.71(3) . .
C1 Ag1 Cl2 Ag3 178.7(2) . .
Cl3 Ag1 Cl2 Ag3 -53.14(10) 2_666 .
Cl1 Ag1 Cl2 Ag3 39.43(10) . .
Ag6 Ag1 Cl2 Ag3 115.57(9) . .
Ag7 Ag1 Cl2 Ag3 161.39(10) . .
Ag5 Ag1 Cl2 Ag3 -125.71(8) . .
C1 Ag1 Cl2 Ag4 -102.9(2) . 2_666
Cl3 Ag1 Cl2 Ag4 25.24(5) 2_666 2_666
Cl1 Ag1 Cl2 Ag4 117.82(5) . 2_666
Ag6 Ag1 Cl2 Ag4 -166.05(4) . 2_666
Ag7 Ag1 Cl2 Ag4 -120.22(4) . 2_666
Ag5 Ag1 Cl2 Ag4 -47.33(5) . 2_666
C1 Ag1 Cl2 Ag2 115.2(2) . .
Cl3 Ag1 Cl2 Ag2 -116.59(5) 2_666 .
Cl1 Ag1 Cl2 Ag2 -24.02(5) . .
Ag6 Ag1 Cl2 Ag2 52.12(8) . .
Ag7 Ag1 Cl2 Ag2 97.94(3) . .
Ag5 Ag1 Cl2 Ag2 170.84(3) . .
C13 Ag2 Cl3 Ag3 -105.75(19) . .
Cl1 Ag2 Cl3 Ag3 120.08(5) . .
Cl2 Ag2 Cl3 Ag3 26.89(5) . .
Ag9 Ag2 Cl3 Ag3 -41.13(9) . .
Ag19 Ag2 Cl3 Ag3 -161.25(3) . .
Ag14 Ag2 Cl3 Ag3 -87.29(3) . .
C13 Ag2 Cl3 Ag1 -178.5(2) . 2_666
Cl1 Ag2 Cl3 Ag1 47.29(10) . 2_666
Cl2 Ag2 Cl3 Ag1 -45.90(9) . 2_666
Ag9 Ag2 Cl3 Ag1 -113.93(9) . 2_666
Ag19 Ag2 Cl3 Ag1 125.96(8) . 2_666
Ag14 Ag2 Cl3 Ag1 -160.08(9) . 2_666
C13 Ag2 Cl3 Ag4 109.61(19) . .
Cl1 Ag2 Cl3 Ag4 -24.55(5) . .
Cl2 Ag2 Cl3 Ag4 -117.74(4) . .
Ag9 Ag2 Cl3 Ag4 174.23(6) . .
Ag19 Ag2 Cl3 Ag4 54.12(4) . .
Ag14 Ag2 Cl3 Ag4 128.08(4) . .
C25 Ag3 Cl3 Ag2 126.7(2) . .
Cl2 Ag3 Cl3 Ag2 -27.44(5) . .
Cl1 Ag3 Cl3 Ag2 -115.36(4) 2_666 .
Ag10 Ag3 Cl3 Ag2 46.32(13) . .
Ag12 Ag3 Cl3 Ag2 102.42(3) . .
Ag11 Ag3 Cl3 Ag2 -178.27(3) . .
C25 Ag3 Cl3 Ag1 -93.3(2) . 2_666
Cl2 Ag3 Cl3 Ag1 112.51(5) . 2_666
Cl1 Ag3 Cl3 Ag1 24.59(4) 2_666 2_666
Ag10 Ag3 Cl3 Ag1 -173.73(9) . 2_666
Ag12 Ag3 Cl3 Ag1 -117.63(4) . 2_666
Ag11 Ag3 Cl3 Ag1 -38.32(5) . 2_666
C25 Ag3 Cl3 Ag4 -167.6(2) . .
Cl2 Ag3 Cl3 Ag4 38.23(10) . .
Cl1 Ag3 Cl3 Ag4 -49.69(10) 2_666 .
Ag10 Ag3 Cl3 Ag4 111.98(12) . .
Ag12 Ag3 Cl3 Ag4 168.09(9) . .
Ag11 Ag3 Cl3 Ag4 -112.61(9) . .
C43 Ag4 Cl3 Ag2 -113.2(2) . .
Cl2 Ag4 Cl3 Ag2 115.45(5) 2_666 .
Cl1 Ag4 Cl3 Ag2 24.42(5) . .
Ag17 Ag4 Cl3 Ag2 -53.42(5) . .
Ag15 Ag4 Cl3 Ag2 -123.15(4) . .
Ag16 Ag4 Cl3 Ag2 -178.78(4) . .
C43 Ag4 Cl3 Ag3 -178.8(2) . .
Cl2 Ag4 Cl3 Ag3 49.83(10) 2_666 .
Cl1 Ag4 Cl3 Ag3 -41.20(10) . .
Ag17 Ag4 Cl3 Ag3 -119.03(9) . .
Ag15 Ag4 Cl3 Ag3 171.24(10) . .
Ag16 Ag4 Cl3 Ag3 115.61(9) . .
C43 Ag4 Cl3 Ag1 106.7(2) . 2_666
Cl2 Ag4 Cl3 Ag1 -24.70(5) 2_666 2_666
Cl1 Ag4 Cl3 Ag1 -115.73(5) . 2_666
Ag17 Ag4 Cl3 Ag1 166.43(3) . 2_666
Ag15 Ag4 Cl3 Ag1 96.70(4) . 2_666
Ag16 Ag4 Cl3 Ag1 41.07(7) . 2_666
Cl3 Ag1 C1 C2 45(6) 2_666 .
Cl1 Ag1 C1 C2 -80(6) . .
Cl2 Ag1 C1 C2 157(6) . .
Ag6 Ag1 C1 C2 -65(6) . .
Ag7 Ag1 C1 C2 179(100) . .
Ag5 Ag1 C1 C2 60(6) . .
Cl3 Ag1 C1 Ag7 -134.57(11) 2_666 .
Cl1 Ag1 C1 Ag7 100.90(18) . .
Cl2 Ag1 C1 Ag7 -22.2(2) . .
Ag6 Ag1 C1 Ag7 115.2(2) . .
Ag5 Ag1 C1 Ag7 -119.9(2) . .
Cl3 Ag1 C1 Ag6 110.22(15) 2_666 .
Cl1 Ag1 C1 Ag6 -14.3(3) . .
Cl2 Ag1 C1 Ag6 -137.43(10) . .
Ag7 Ag1 C1 Ag6 -115.2(2) . .
Ag5 Ag1 C1 Ag6 124.9(2) . .
Cl3 Ag1 C1 Ag5 -14.7(2) 2_666 .
Cl1 Ag1 C1 Ag5 -139.22(11) . .
Cl2 Ag1 C1 Ag5 97.65(17) . .
Ag6 Ag1 C1 Ag5 -124.9(2) . .
Ag7 Ag1 C1 Ag5 119.9(2) . .
C7 Ag7 C1 C2 68.7(17) . .
Ag9 Ag7 C1 C2 130.5(4) . .
Ag1 Ag7 C1 C2 -179.9(6) . .
Ag8 Ag7 C1 C2 -122.3(4) . .
C7 Ag7 C1 Ag1 -111.3(15) . .
Ag9 Ag7 C1 Ag1 -49.5(3) . .
Ag8 Ag7 C1 Ag1 57.6(3) . .
C7 Ag7 C1 Ag6 -33.0(17) . .
Ag9 Ag7 C1 Ag6 28.8(4) . .
Ag1 Ag7 C1 Ag6 78.3(3) . .
Ag8 Ag7 C1 Ag6 135.94(19) . .
C7 Ag7 C1 Ag5 169.1(14) . .
Ag9 Ag7 C1 Ag5 -129.1(2) . .
Ag1 Ag7 C1 Ag5 -79.5(3) . .
Ag8 Ag7 C1 Ag5 -21.9(5) . .
C31 Ag6 C1 C2 130(3) 2_666 .
Ag11 Ag6 C1 C2 132.5(4) 2_666 .
Ag1 Ag6 C1 C2 175.0(5) . .
C31 Ag6 C1 Ag1 -45(3) 2_666 .
C2 Ag6 C1 Ag1 -175.0(5) . .
Ag11 Ag6 C1 Ag1 -42.5(3) 2_666 .
C31 Ag6 C1 Ag7 -124(3) 2_666 .
C2 Ag6 C1 Ag7 106.3(5) . .
Ag11 Ag6 C1 Ag7 -121.2(2) 2_666 .
Ag1 Ag6 C1 Ag7 -78.7(3) . .
C31 Ag6 C1 Ag5 33(3) 2_666 .
C2 Ag6 C1 Ag5 -97.1(5) . .
Ag11 Ag6 C1 Ag5 35.4(4) 2_666 .
Ag1 Ag6 C1 Ag5 77.9(3) . .
C37 Ag5 C1 C2 149(25) 2_666 .
Ag15 Ag5 C1 C2 132.1(4) 2_666 .
Ag1 Ag5 C1 C2 -175.3(5) . .
Ag13 Ag5 C1 C2 -127.2(4) 2_666 .
C37 Ag5 C1 Ag1 -36(25) 2_666 .
C2 Ag5 C1 Ag1 175.3(5) . .
Ag15 Ag5 C1 Ag1 -52.6(3) 2_666 .
Ag13 Ag5 C1 Ag1 48.1(3) 2_666 .
C37 Ag5 C1 Ag7 43(25) 2_666 .
C2 Ag5 C1 Ag7 -106.0(5) . .
Ag15 Ag5 C1 Ag7 26.1(4) 2_666 .
Ag1 Ag5 C1 Ag7 78.7(3) . .
Ag13 Ag5 C1 Ag7 126.8(2) 2_666 .
C37 Ag5 C1 Ag6 -113(25) 2_666 .
C2 Ag5 C1 Ag6 98.4(5) . .
Ag15 Ag5 C1 Ag6 -129.4(2) 2_666 .
Ag1 Ag5 C1 Ag6 -76.9(3) . .
Ag13 Ag5 C1 Ag6 -28.8(5) 2_666 .
Ag1 C1 C2 C3 154(7) . .
Ag7 C1 C2 C3 -27(9) . .
Ag6 C1 C2 C3 89(9) . .
Ag5 C1 C2 C3 -147(9) . .
Ag1 C1 C2 Ag5 -59(6) . .
Ag7 C1 C2 Ag5 120.2(4) . .
Ag6 C1 C2 Ag5 -124.0(3) . .
Ag1 C1 C2 Ag6 65(6) . .
Ag7 C1 C2 Ag6 -115.8(4) . .
Ag5 C1 C2 Ag6 124.0(3) . .
C37 Ag5 C2 C1 -179.4(5) 2_666 .
Ag15 Ag5 C2 C1 -78.3(5) 2_666 .
Ag1 Ag5 C2 C1 3.6(4) . .
Ag13 Ag5 C2 C1 90.0(5) 2_666 .
C37 Ag5 C2 C3 -2.3(8) 2_666 .
C1 Ag5 C2 C3 177.1(8) . .
Ag15 Ag5 C2 C3 98.8(6) 2_666 .
Ag1 Ag5 C2 C3 -179.4(6) . .
Ag13 Ag5 C2 C3 -92.9(6) 2_666 .
C37 Ag5 C2 Ag6 136.0(4) 2_666 .
C1 Ag5 C2 Ag6 -44.6(4) . .
Ag15 Ag5 C2 Ag6 -122.91(18) 2_666 .
Ag1 Ag5 C2 Ag6 -41.05(13) . .
Ag13 Ag5 C2 Ag6 45.4(4) 2_666 .
C31 Ag6 C2 C1 -170.1(6) 2_666 .
Ag11 Ag6 C2 C1 -71.8(5) 2_666 .
Ag1 Ag6 C2 C1 -3.8(4) . .
C31 Ag6 C2 C3 15.1(9) 2_666 .
C1 Ag6 C2 C3 -174.8(8) . .
Ag11 Ag6 C2 C3 113.4(5) 2_666 .
Ag1 Ag6 C2 C3 -178.6(6) . .
C31 Ag6 C2 Ag5 -124.3(5) 2_666 .
C1 Ag6 C2 Ag5 45.9(4) . .
Ag11 Ag6 C2 Ag5 -26.0(3) 2_666 .
Ag1 Ag6 C2 Ag5 42.04(14) . .
C1 C2 C3 C5 -103(9) . .
Ag5 C2 C3 C5 112.1(6) . .
Ag6 C2 C3 C5 -16.3(8) . .
C1 C2 C3 C4 135(9) . .
Ag5 C2 C3 C4 -10.0(9) . .
Ag6 C2 C3 C4 -138.4(6) . .
C1 C2 C3 C6 17(9) . .
Ag5 C2 C3 C6 -128.4(6) . .
Ag6 C2 C3 C6 103.2(6) . .
C1 Ag7 C7 C8 -88.7(17) . .
Ag9 Ag7 C7 C8 -157.6(9) . .
Ag1 Ag7 C7 C8 168.2(6) . .
Ag8 Ag7 C7 C8 100.3(8) . .
C1 Ag7 C7 Ag9 69.0(16) . .
Ag1 Ag7 C7 Ag9 -34.1(3) . .
Ag8 Ag7 C7 Ag9 -102.0(3) . .
C1 Ag7 C7 Ag8 171.0(14) . .
Ag9 Ag7 C7 Ag8 102.0(3) . .
Ag1 Ag7 C7 Ag8 67.9(3) . .
C13 Ag9 C7 C8 -52.5(19) . .
Ag2 Ag9 C7 C8 -154.3(6) . .
Ag7 Ag9 C7 C8 157.5(9) . .
C13 Ag9 C7 Ag7 150.0(14) . .
Ag2 Ag9 C7 Ag7 48.2(3) . .
C13 Ag9 C7 Ag8 52.0(16) . .
Ag2 Ag9 C7 Ag8 -49.8(4) . .
Ag7 Ag9 C7 Ag8 -98.0(3) . .
C55 Ag8 C7 C8 -110(2) 2_666 .
C56 Ag8 C7 C8 12.4(9) 2_666 .
Ag16 Ag8 C7 C8 -131.5(4) 2_666 .
Ag7 Ag8 C7 C8 -135.5(6) . .
C55 Ag8 C7 Ag7 26(3) 2_666 .
C8 Ag8 C7 Ag7 135.5(6) . .
C56 Ag8 C7 Ag7 147.8(6) 2_666 .
Ag16 Ag8 C7 Ag7 3.9(4) 2_666 .
C55 Ag8 C7 Ag9 114(2) 2_666 .
C8 Ag8 C7 Ag9 -136.6(6) . .
C56 Ag8 C7 Ag9 -124.2(6) 2_666 .
Ag16 Ag8 C7 Ag9 91.9(3) 2_666 .
Ag7 Ag8 C7 Ag9 88.0(3) . .
Ag7 C7 C8 C9 71(5) . .
Ag9 C7 C8 C9 -77(4) . .
Ag8 C7 C8 C9 174(4) . .
Ag7 C7 C8 Ag8 -103.4(7) . .
Ag9 C7 C8 Ag8 109.0(7) . .
C55 Ag8 C8 C7 168.2(5) 2_666 .
C56 Ag8 C8 C7 -174.1(5) 2_666 .
Ag16 Ag8 C8 C7 80.0(5) 2_666 .
Ag7 Ag8 C8 C7 30.1(4) . .
C55 Ag8 C8 C9 -10.6(9) 2_666 .
C7 Ag8 C8 C9 -178.8(9) . .
C56 Ag8 C8 C9 7.1(7) 2_666 .
Ag16 Ag8 C8 C9 -98.8(6) 2_666 .
Ag7 Ag8 C8 C9 -148.7(6) . .
C7 C8 C9 C10 -132(4) . .
Ag8 C8 C9 C10 41.8(8) . .
C7 C8 C9 C12 -12(5) . .
Ag8 C8 C9 C12 161.1(5) . .
C7 C8 C9 C11 108(4) . .
Ag8 C8 C9 C11 -78.7(7) . .
Cl3 Ag2 C13 C14 -94(8) . .
Cl1 Ag2 C13 C14 26(8) . .
Cl2 Ag2 C13 C14 147(8) . .
Ag9 Ag2 C13 C14 121(8) . .
Ag19 Ag2 C13 C14 0(8) . .
Ag14 Ag2 C13 C14 -119(8) . .
Cl3 Ag2 C13 Ag9 144.40(9) . .
Cl1 Ag2 C13 Ag9 -94.93(17) . .
Cl2 Ag2 C13 Ag9 26.3(2) . .
Ag19 Ag2 C13 Ag9 -121.3(2) . .
Ag14 Ag2 C13 Ag9 120.2(2) . .
Cl3 Ag2 C13 Ag14 24.2(2) . .
Cl1 Ag2 C13 Ag14 144.87(9) . .
Cl2 Ag2 C13 Ag14 -93.86(18) . .
Ag9 Ag2 C13 Ag14 -120.2(2) . .
Ag19 Ag2 C13 Ag14 118.5(2) . .
Cl3 Ag2 C13 Ag19 -94.29(17) . .
Cl1 Ag2 C13 Ag19 26.4(2) . .
Cl2 Ag2 C13 Ag19 147.65(9) . .
Ag9 Ag2 C13 Ag19 121.3(2) . .
Ag14 Ag2 C13 Ag19 -118.5(2) . .
C7 Ag9 C13 C14 72.9(16) . .
Ag2 Ag9 C13 C14 -176.7(5) . .
Ag7 Ag9 C13 C14 -142.6(4) . .
C7 Ag9 C13 Ag2 -110.5(15) . .
Ag7 Ag9 C13 Ag2 34.1(3) . .
C7 Ag9 C13 Ag14 -30.4(17) . .
Ag2 Ag9 C13 Ag14 80.1(3) . .
Ag7 Ag9 C13 Ag14 114.1(3) . .
C7 Ag9 C13 Ag19 170.3(13) . .
Ag2 Ag9 C13 Ag19 -79.2(3) . .
Ag7 Ag9 C13 Ag19 -45.2(4) . .
C19 Ag14 C13 C14 -4(5) . .
Ag13 Ag14 C13 C14 118.3(4) . .
Ag2 Ag14 C13 C14 176.6(5) . .
Ag12 Ag14 C13 C14 -140.9(4) . .
C19 Ag14 C13 Ag2 180(100) . .
C14 Ag14 C13 Ag2 -176.6(5) . .
Ag13 Ag14 C13 Ag2 -58.3(3) . .
Ag12 Ag14 C13 Ag2 42.5(3) . .
C19 Ag14 C13 Ag9 101(5) . .
C14 Ag14 C13 Ag9 104.7(5) . .
Ag13 Ag14 C13 Ag9 -136.98(19) . .
Ag2 Ag14 C13 Ag9 -78.6(3) . .
Ag12 Ag14 C13 Ag9 -36.1(4) . .
C19 Ag14 C13 Ag19 -99(5) . .
C14 Ag14 C13 Ag19 -95.5(5) . .
Ag13 Ag14 C13 Ag19 22.8(4) . .
Ag2 Ag14 C13 Ag19 81.1(3) . .
Ag12 Ag14 C13 Ag19 123.7(2) . .
C49 Ag19 C13 C14 65.8(19) . .
Ag17 Ag19 C13 C14 -145.4(3) . .
Ag2 Ag19 C13 C14 180.0(5) . .
Ag18 Ag19 C13 C14 115.8(4) . .
C49 Ag19 C13 Ag2 -114.2(18) . .
C14 Ag19 C13 Ag2 -180.0(5) . .
Ag17 Ag19 C13 Ag2 34.7(3) . .
Ag18 Ag19 C13 Ag2 -64.2(2) . .
C49 Ag19 C13 Ag9 -36.0(19) . .
C14 Ag19 C13 Ag9 -101.9(5) . .
Ag17 Ag19 C13 Ag9 112.8(3) . .
Ag2 Ag19 C13 Ag9 78.1(3) . .
Ag18 Ag19 C13 Ag9 14.0(4) . .
C49 Ag19 C13 Ag14 164.4(16) . .
C14 Ag19 C13 Ag14 98.6(5) . .
Ag17 Ag19 C13 Ag14 -46.8(4) . .
Ag2 Ag19 C13 Ag14 -81.4(3) . .
Ag18 Ag19 C13 Ag14 -145.59(16) . .
Ag2 C13 C14 C15 -168(7) . .
Ag9 C13 C14 C15 -48(12) . .
Ag14 C13 C14 C15 74(11) . .
Ag19 C13 C14 C15 -168(11) . .
Ag2 C13 C14 Ag19 0(8) . .
Ag9 C13 C14 Ag19 120.8(3) . .
Ag14 C13 C14 Ag19 -118.1(3) . .
Ag2 C13 C14 Ag14 118(8) . .
Ag9 C13 C14 Ag14 -121.0(3) . .
Ag19 C13 C14 Ag14 118.1(3) . .
C49 Ag19 C14 C13 -166.9(5) . .
Ag17 Ag19 C14 C13 73.9(6) . .
Ag2 Ag19 C14 C13 0.0(4) . .
Ag18 Ag19 C14 C13 -92.5(4) . .
C49 Ag19 C14 C15 12.4(8) . .
C13 Ag19 C14 C15 179.2(8) . .
Ag17 Ag19 C14 C15 -106.9(5) . .
Ag2 Ag19 C14 C15 179.2(5) . .
Ag18 Ag19 C14 C15 86.7(5) . .
C49 Ag19 C14 Ag14 145.7(4) . .
C13 Ag19 C14 Ag14 -47.5(4) . .
Ag17 Ag19 C14 Ag14 26.5(5) . .
Ag2 Ag19 C14 Ag14 -47.46(13) . .
Ag18 Ag19 C14 Ag14 -140.00(11) . .
C19 Ag14 C14 C13 179.6(5) . .
Ag13 Ag14 C14 C13 -90.8(5) . .
Ag2 Ag14 C14 C13 -2.5(4) . .
Ag12 Ag14 C14 C13 74.8(5) . .
C19 Ag14 C14 C15 3.3(8) . .
C13 Ag14 C14 C15 -176.3(8) . .
Ag13 Ag14 C14 C15 93.0(5) . .
Ag2 Ag14 C14 C15 -178.8(5) . .
Ag12 Ag14 C14 C15 -101.5(5) . .
C19 Ag14 C14 Ag19 -130.1(4) . .
C13 Ag14 C14 Ag19 50.3(4) . .
Ag13 Ag14 C14 Ag19 -40.5(3) . .
Ag2 Ag14 C14 Ag19 47.76(13) . .
Ag12 Ag14 C14 Ag19 125.1(2) . .
C13 C14 C15 C18 -91(11) . .
Ag19 C14 C15 C18 101.3(6) . .
Ag14 C14 C15 C18 -19.3(7) . .
C13 C14 C15 C16 147(11) . .
Ag19 C14 C15 C16 -20.6(8) . .
Ag14 C14 C15 C16 -141.2(5) . .
C13 C14 C15 C17 28(12) . .
Ag19 C14 C15 C17 -139.5(5) . .
Ag14 C14 C15 C17 99.9(6) . .
C13 Ag14 C19 C20 -35(5) . .
C14 Ag14 C19 C20 -37.9(11) . .
Ag13 Ag14 C19 C20 -158.9(9) . .
Ag2 Ag14 C19 C20 145.0(7) . .
Ag12 Ag14 C19 C20 104.8(9) . .
C13 Ag14 C19 Ag13 124(4) . .
C14 Ag14 C19 Ag13 121.0(4) . .
Ag2 Ag14 C19 Ag13 -56.0(3) . .
Ag12 Ag14 C19 Ag13 -96.3(3) . .
C13 Ag14 C19 Ag12 -139(4) . .
C14 Ag14 C19 Ag12 -142.7(3) . .
Ag13 Ag14 C19 Ag12 96.3(3) . .
Ag2 Ag14 C19 Ag12 40.3(4) . .
C37 Ag13 C19 C20 -2.4(15) . .
C38 Ag13 C19 C20 16.2(9) . .
Ag14 Ag13 C19 C20 161.5(8) . .
Ag12 Ag13 C19 C20 -103.8(8) . .
Ag5 Ag13 C19 C20 -89.5(7) 2_666 .
C37 Ag13 C19 Ag14 -164.0(9) . .
C38 Ag13 C19 Ag14 -145.3(2) . .
Ag12 Ag13 C19 Ag14 94.7(3) . .
Ag5 Ag13 C19 Ag14 109.0(2) 2_666 .
C37 Ag13 C19 Ag12 101.4(9) . .
C38 Ag13 C19 Ag12 120.0(3) . .
Ag14 Ag13 C19 Ag12 -94.7(2) . .
Ag5 Ag13 C19 Ag12 14.3(4) 2_666 .
C25 Ag12 C19 C20 -138.4(10) . .
C26 Ag12 C19 C20 -7.0(11) . .
Ag3 Ag12 C19 C20 -168.0(4) . .
Ag14 Ag12 C19 C20 -140.6(6) . .
Ag13 Ag12 C19 C20 133.7(6) . .
C25 Ag12 C19 Ag14 2.2(12) . .
C20 Ag12 C19 Ag14 140.6(6) . .
C26 Ag12 C19 Ag14 133.5(7) . .
Ag3 Ag12 C19 Ag14 -27.4(3) . .
Ag13 Ag12 C19 Ag14 -85.8(3) . .
C25 Ag12 C19 Ag13 87.9(11) . .
C20 Ag12 C19 Ag13 -133.7(6) . .
C26 Ag12 C19 Ag13 -140.7(7) . .
Ag3 Ag12 C19 Ag13 58.4(3) . .
Ag14 Ag12 C19 Ag13 85.8(3) . .
Ag14 C19 C20 C21 74(7) . .
Ag13 C19 C20 C21 -77(7) . .
Ag12 C19 C20 C21 179(100) . .
Ag14 C19 C20 Ag12 -104.6(8) . .
Ag13 C19 C20 Ag12 104.2(7) . .
C25 Ag12 C20 C19 154.0(6) . .
C26 Ag12 C20 C19 177.1(5) . .
Ag3 Ag12 C20 C19 19.6(7) . .
Ag14 Ag12 C20 C19 27.9(4) . .
Ag13 Ag12 C20 C19 -32.5(4) . .
C19 Ag12 C20 C21 -179.9(9) . .
C25 Ag12 C20 C21 -25.9(11) . .
C26 Ag12 C20 C21 -2.8(8) . .
Ag3 Ag12 C20 C21 -160.3(5) . .
Ag14 Ag12 C20 C21 -152.0(7) . .
Ag13 Ag12 C20 C21 147.6(7) . .
C19 C20 C21 C22 118(7) . .
Ag12 C20 C21 C22 -63.1(8) . .
C19 C20 C21 C24 -3(7) . .
Ag12 C20 C21 C24 176.0(6) . .
C19 C20 C21 C23 -122(7) . .
Ag12 C20 C21 C23 57.1(8) . .
Cl2 Ag3 C25 C26 -162(5) . .
Cl3 Ag3 C25 C26 53(5) . .
Cl1 Ag3 C25 C26 -55(5) 2_666 .
Ag10 Ag3 C25 C26 -153(5) . .
Ag12 Ag3 C25 C26 86(5) . .
Ag11 Ag3 C25 C26 -36(5) . .
Cl2 Ag3 C25 Ag10 -9.1(3) . .
Cl3 Ag3 C25 Ag10 -153.59(8) . .
Cl1 Ag3 C25 Ag10 98.08(15) 2_666 .
Ag12 Ag3 C25 Ag10 -121.1(2) . .
Ag11 Ag3 C25 Ag10 117.3(2) . .
Cl2 Ag3 C25 Ag11 -126.35(14) . .
Cl3 Ag3 C25 Ag11 89.1(2) . .
Cl1 Ag3 C25 Ag11 -19.2(2) 2_666 .
Ag10 Ag3 C25 Ag11 -117.3(2) . .
Ag12 Ag3 C25 Ag11 121.6(2) . .
Cl2 Ag3 C25 Ag12 112.07(17) . .
Cl3 Ag3 C25 Ag12 -32.5(3) . .
Cl1 Ag3 C25 Ag12 -140.79(10) 2_666 .
Ag10 Ag3 C25 Ag12 121.1(2) . .
Ag11 Ag3 C25 Ag12 -121.6(2) . .
C55 Ag10 C25 C26 -104.4(19) 2_666 .
Ag3 Ag10 C25 C26 177.1(6) . .
Ag16 Ag10 C25 C26 132.7(4) 2_666 .
C55 Ag10 C25 Ag3 78.5(19) 2_666 .
Ag16 Ag10 C25 Ag3 -44.4(3) 2_666 .
C55 Ag10 C25 Ag11 160.3(18) 2_666 .
Ag3 Ag10 C25 Ag11 81.8(3) . .
Ag16 Ag10 C25 Ag11 37.4(4) 2_666 .
C55 Ag10 C25 Ag12 1(2) 2_666 .
Ag3 Ag10 C25 Ag12 -77.5(3) . .
Ag16 Ag10 C25 Ag12 -121.9(2) 2_666 .
C31 Ag11 C25 C26 17.1(14) . .
Ag6 Ag11 C25 C26 120.2(4) 2_666 .
Ag3 Ag11 C25 C26 176.3(6) . .
Ag18 Ag11 C25 C26 -113.0(4) 2_666 .
C31 Ag11 C25 Ag3 -159.2(11) . .
C26 Ag11 C25 Ag3 -176.3(6) . .
Ag6 Ag11 C25 Ag3 -56.1(3) 2_666 .
Ag18 Ag11 C25 Ag3 70.7(3) 2_666 .
C31 Ag11 C25 Ag10 121.1(12) . .
C26 Ag11 C25 Ag10 104.0(5) . .
Ag6 Ag11 C25 Ag10 -135.78(18) 2_666 .
Ag3 Ag11 C25 Ag10 -79.6(3) . .
Ag18 Ag11 C25 Ag10 -9.0(5) 2_666 .
C31 Ag11 C25 Ag12 -79.9(13) . .
C26 Ag11 C25 Ag12 -97.0(5) . .
Ag6 Ag11 C25 Ag12 23.2(4) 2_666 .
Ag3 Ag11 C25 Ag12 79.4(3) . .
Ag18 Ag11 C25 Ag12 150.05(15) 2_666 .
C19 Ag12 C25 C26 151.5(10) . .
C20 Ag12 C25 C26 37.1(9) . .
Ag3 Ag12 C25 C26 -173.7(6) . .
Ag14 Ag12 C25 C26 153.3(4) . .
Ag13 Ag12 C25 C26 -134.5(4) . .
C19 Ag12 C25 Ag3 -34.8(11) . .
C20 Ag12 C25 Ag3 -149.1(6) . .
C26 Ag12 C25 Ag3 173.7(6) . .
Ag14 Ag12 C25 Ag3 -33.0(2) . .
Ag13 Ag12 C25 Ag3 39.2(3) . .
C19 Ag12 C25 Ag10 42.5(12) . .
C20 Ag12 C25 Ag10 -71.9(7) . .
C26 Ag12 C25 Ag10 -109.0(6) . .
Ag3 Ag12 C25 Ag10 77.3(3) . .
Ag14 Ag12 C25 Ag10 44.3(4) . .
Ag13 Ag12 C25 Ag10 116.5(2) . .
C19 Ag12 C25 Ag11 -115.8(10) . .
C20 Ag12 C25 Ag11 129.8(6) . .
C26 Ag12 C25 Ag11 92.7(6) . .
Ag3 Ag12 C25 Ag11 -81.1(3) . .
Ag14 Ag12 C25 Ag11 -114.1(3) . .
Ag13 Ag12 C25 Ag11 -41.9(4) . .
Ag3 C25 C26 C27 -170(9) . .
Ag10 C25 C26 C27 37(12) . .
Ag11 C25 C26 C27 154(12) . .
Ag12 C25 C26 C27 -85(12) . .
Ag3 C25 C26 Ag11 36(5) . .
Ag10 C25 C26 Ag11 -116.9(3) . .
Ag12 C25 C26 Ag11 120.7(3) . .
Ag3 C25 C26 Ag12 -85(5) . .
Ag10 C25 C26 Ag12 122.4(4) . .
Ag11 C25 C26 Ag12 -120.7(3) . .
C31 Ag11 C26 C25 -174.7(5) . .
Ag6 Ag11 C26 C25 -94.2(5) 2_666 .
Ag3 Ag11 C26 C25 -2.7(4) . .
Ag18 Ag11 C26 C25 110.1(4) 2_666 .
C31 Ag11 C26 C27 7.0(8) . .
C25 Ag11 C26 C27 -178.3(9) . .
Ag6 Ag11 C26 C27 87.5(6) 2_666 .
Ag3 Ag11 C26 C27 179.0(6) . .
Ag18 Ag11 C26 C27 -68.3(7) 2_666 .
C31 Ag11 C26 Ag12 -128.3(3) . .
C25 Ag11 C26 Ag12 46.4(4) . .
Ag6 Ag11 C26 Ag12 -47.9(4) 2_666 .
Ag3 Ag11 C26 Ag12 43.65(15) . .
Ag18 Ag11 C26 Ag12 156.42(11) 2_666 .
C19 Ag12 C26 C25 -158.5(7) . .
C20 Ag12 C26 C25 -163.1(4) . .
Ag3 Ag12 C26 C25 4.8(4) . .
Ag14 Ag12 C26 C25 -43.4(6) . .
Ag13 Ag12 C26 C25 78.3(6) . .
C19 Ag12 C26 C27 17.5(13) . .
C25 Ag12 C26 C27 176.0(10) . .
C20 Ag12 C26 C27 12.9(8) . .
Ag3 Ag12 C26 C27 -179.2(7) . .
Ag14 Ag12 C26 C27 132.6(6) . .
Ag13 Ag12 C26 C27 -105.7(7) . .
C19 Ag12 C26 Ag11 151.4(7) . .
C25 Ag12 C26 Ag11 -50.1(4) . .
C20 Ag12 C26 Ag11 146.8(2) . .
Ag3 Ag12 C26 Ag11 -45.34(16) . .
Ag14 Ag12 C26 Ag11 -93.5(3) . .
Ag13 Ag12 C26 Ag11 28.2(4) . .
C25 C26 C27 C28 -109(12) . .
Ag11 C26 C27 C28 44.9(12) . .
Ag12 C26 C27 C28 168.6(9) . .
C25 C26 C27 C30A 54(12) . .
Ag11 C26 C27 C30A -152.9(9) . .
Ag12 C26 C27 C30A -29.1(12) . .
C25 C26 C27 C29 151(12) . .
Ag11 C26 C27 C29 -55.5(11) . .
Ag12 C26 C27 C29 68.3(11) . .
C25 C26 C27 C30B -16(12) . .
Ag11 C26 C27 C30B 137.1(8) . .
Ag12 C26 C27 C30B -99.1(9) . .
C25 Ag11 C31 C32 -39.8(19) . .
C26 Ag11 C31 C32 -27.2(11) . .
Ag6 Ag11 C31 C32 -154.0(11) 2_666 .
Ag3 Ag11 C31 C32 166.4(7) . .
Ag18 Ag11 C31 C32 100.4(10) 2_666 .
C25 Ag11 C31 Ag6 114.1(12) . 2_666
C26 Ag11 C31 Ag6 126.8(3) . 2_666
Ag3 Ag11 C31 Ag6 -39.6(4) . 2_666
Ag18 Ag11 C31 Ag6 -105.7(3) 2_666 2_666
C25 Ag11 C31 Ag18 -140.2(11) . 2_666
C26 Ag11 C31 Ag18 -127.5(3) . 2_666
Ag6 Ag11 C31 Ag18 105.7(3) 2_666 2_666
Ag3 Ag11 C31 Ag18 66.1(4) . 2_666
Ag11 C31 C32 C33 69(7) . .
Ag6 C31 C32 C33 -77(7) 2_666 .
Ag18 C31 C32 C33 170(6) 2_666 .
Ag11 C31 C32 Ag18 -101.2(9) . 2_666
Ag6 C31 C32 Ag18 112.9(7) 2_666 2_666
C31 C32 C33 C35 -35(7) . .
Ag18 C32 C33 C35 134.3(10) 2_666 .
C31 C32 C33 C36 86(7) . .
Ag18 C32 C33 C36 -104.9(8) 2_666 .
C31 C32 C33 C34 -161(6) . .
Ag18 C32 C33 C34 8.9(10) 2_666 .
C43 Ag15 C37 C38 -134(6) . .
C44 Ag15 C37 C38 -36.1(11) . .
Ag5 Ag15 C37 C38 -163.0(10) 2_666 .
Ag4 Ag15 C37 C38 148.1(7) . .
C43 Ag15 C37 Ag5 29(7) . 2_666
C44 Ag15 C37 Ag5 126.9(4) . 2_666
Ag4 Ag15 C37 Ag5 -48.9(3) . 2_666
C43 Ag15 C37 Ag13 128(7) . .
C44 Ag15 C37 Ag13 -133.8(4) . .
Ag5 Ag15 C37 Ag13 99.3(3) 2_666 .
Ag4 Ag15 C37 Ag13 50.4(3) . .
C19 Ag13 C37 C38 26.4(12) . .
Ag14 Ag13 C37 C38 -132.0(4) . .
Ag12 Ag13 C37 C38 111.3(4) . .
Ag5 Ag13 C37 C38 132.0(6) 2_666 .
C19 Ag13 C37 Ag15 166.0(8) . .
C38 Ag13 C37 Ag15 139.6(6) . .
Ag14 Ag13 C37 Ag15 7.6(5) . .
Ag12 Ag13 C37 Ag15 -109.0(2) . .
Ag5 Ag13 C37 Ag15 -88.3(3) 2_666 .
C19 Ag13 C37 Ag5 -105.6(9) . 2_666
C38 Ag13 C37 Ag5 -132.0(6) . 2_666
Ag14 Ag13 C37 Ag5 96.0(3) . 2_666
Ag12 Ag13 C37 Ag5 -20.7(4) . 2_666
Ag15 C37 C38 C39 83(5) . .
Ag5 C37 C38 C39 -74(5) 2_666 .
Ag13 C37 C38 C39 -174(5) . .
Ag15 C37 C38 Ag13 -103.6(8) . .
Ag5 C37 C38 Ag13 99.6(6) 2_666 .
C19 Ag13 C38 C37 -170.5(5) . .
Ag14 Ag13 C38 C37 101.7(5) . .
Ag12 Ag13 C38 C37 -104.2(5) . .
Ag5 Ag13 C38 C37 -32.0(4) 2_666 .
C19 Ag13 C38 C39 8.5(7) . .
C37 Ag13 C38 C39 179.0(8) . .
Ag14 Ag13 C38 C39 -79.3(6) . .
Ag12 Ag13 C38 C39 74.7(6) . .
Ag5 Ag13 C38 C39 146.9(6) 2_666 .
C37 C38 C39 C42 -96(5) . .
Ag13 C38 C39 C42 91.0(7) . .
C37 C38 C39 C41 24(5) . .
Ag13 C38 C39 C41 -149.5(5) . .
C37 C38 C39 C40 144(5) . .
Ag13 C38 C39 C40 -29.5(8) . .
Cl2 Ag4 C43 C44 124(8) 2_666 .
Cl1 Ag4 C43 C44 -113(8) . .
Cl3 Ag4 C43 C44 9(8) . .
Ag17 Ag4 C43 C44 -95(8) . .
Ag15 Ag4 C43 C44 22(8) . .
Ag16 Ag4 C43 C44 142(8) . .
Cl2 Ag4 C43 Ag15 102.49(16) 2_666 .
Cl1 Ag4 C43 Ag15 -134.50(12) . .
Cl3 Ag4 C43 Ag15 -12.9(3) . .
Ag17 Ag4 C43 Ag15 -117.0(2) . .
Ag16 Ag4 C43 Ag15 120.4(3) . .
Cl2 Ag4 C43 Ag16 -17.9(3) 2_666 .
Cl1 Ag4 C43 Ag16 105.07(17) . .
Cl3 Ag4 C43 Ag16 -133.34(11) . .
Ag17 Ag4 C43 Ag16 122.5(2) . .
Ag15 Ag4 C43 Ag16 -120.4(3) . .
Cl2 Ag4 C43 Ag17 -140.50(10) 2_666 .
Cl1 Ag4 C43 Ag17 -17.5(3) . .
Cl3 Ag4 C43 Ag17 104.11(16) . .
Ag15 Ag4 C43 Ag17 117.0(2) . .
Ag16 Ag4 C43 Ag17 -122.5(2) . .
C37 Ag15 C43 C44 102(7) . .
Ag5 Ag15 C43 C44 129.8(4) 2_666 .
Ag4 Ag15 C43 C44 -178.5(6) . .
C37 Ag15 C43 Ag4 -79(7) . .
C44 Ag15 C43 Ag4 178.5(6) . .
Ag5 Ag15 C43 Ag4 -51.6(3) 2_666 .
C37 Ag15 C43 Ag16 -1(7) . .
C44 Ag15 C43 Ag16 -103.4(6) . .
Ag5 Ag15 C43 Ag16 26.4(4) 2_666 .
Ag4 Ag15 C43 Ag16 78.0(3) . .
C37 Ag15 C43 Ag17 -157(7) . .
C44 Ag15 C43 Ag17 100.6(5) . .
Ag5 Ag15 C43 Ag17 -129.5(2) 2_666 .
Ag4 Ag15 C43 Ag17 -77.9(3) . .
C55 Ag16 C43 C44 81.0(11) . .
Ag4 Ag16 C43 C44 -177.6(6) . .
Ag10 Ag16 C43 C44 126.6(4) 2_666 .
Ag8 Ag16 C43 C44 -128.6(4) 2_666 .
C55 Ag16 C43 Ag4 -101.4(10) . .
Ag10 Ag16 C43 Ag4 -55.9(2) 2_666 .
Ag8 Ag16 C43 Ag4 48.9(4) 2_666 .
C55 Ag16 C43 Ag15 -179.6(8) . .
Ag4 Ag16 C43 Ag15 -78.2(3) . .
Ag10 Ag16 C43 Ag15 -134.1(2) 2_666 .
Ag8 Ag16 C43 Ag15 -29.3(5) 2_666 .
C55 Ag16 C43 Ag17 -25.0(12) . .
Ag4 Ag16 C43 Ag17 76.4(3) . .
Ag10 Ag16 C43 Ag17 20.5(4) 2_666 .
Ag8 Ag16 C43 Ag17 125.3(3) 2_666 .
C49 Ag17 C43 C44 74.0(13) . .
Ag4 Ag17 C43 C44 176.0(5) . .
Ag19 Ag17 C43 C44 124.4(4) . .
Ag18 Ag17 C43 C44 -141.5(4) . .
C49 Ag17 C43 Ag4 -102.1(12) . .
Ag19 Ag17 C43 Ag4 -51.6(2) . .
Ag18 Ag17 C43 Ag4 42.4(4) . .
C49 Ag17 C43 Ag15 -23.5(14) . .
Ag4 Ag17 C43 Ag15 78.6(3) . .
Ag19 Ag17 C43 Ag15 27.0(4) . .
Ag18 Ag17 C43 Ag15 121.0(3) . .
C49 Ag17 C43 Ag16 -178.9(10) . .
Ag4 Ag17 C43 Ag16 -76.8(3) . .
Ag19 Ag17 C43 Ag16 -128.5(2) . .
Ag18 Ag17 C43 Ag16 -34.4(5) . .
Ag4 C43 C44 C45 129(25) . .
Ag15 C43 C44 C45 151(28) . .
Ag16 C43 C44 C45 -89(28) . .
Ag17 C43 C44 C45 35(28) . .
Ag4 C43 C44 Ag15 -22(8) . .
Ag16 C43 C44 Ag15 120.2(4) . .
Ag17 C43 C44 Ag15 -116.3(3) . .
C37 Ag15 C44 C43 -175.6(5) . .
Ag5 Ag15 C44 C43 -78.5(5) 2_666 .
Ag4 Ag15 C44 C43 1.1(4) . .
C37 Ag15 C44 C45 5.2(9) . .
C43 Ag15 C44 C45 -179.2(9) . .
Ag5 Ag15 C44 C45 102.3(6) 2_666 .
Ag4 Ag15 C44 C45 -178.0(6) . .
C43 C44 C45 C48 -45(28) . .
Ag15 C44 C45 C48 105.5(6) . .
C43 C44 C45 C46 -165(28) . .
Ag15 C44 C45 C46 -14.3(8) . .
C43 C44 C45 C47 74(28) . .
Ag15 C44 C45 C47 -134.8(5) . .
C43 Ag17 C49 C50 -78.4(15) . .
Ag4 Ag17 C49 C50 -170.0(7) . .
Ag19 Ag17 C49 C50 -136.8(9) . .
Ag18 Ag17 C49 C50 129.1(9) . .
C43 Ag17 C49 Ag19 58.4(13) . .
Ag4 Ag17 C49 Ag19 -33.2(3) . .
Ag18 Ag17 C49 Ag19 -94.1(3) . .
C43 Ag17 C49 Ag18 152.5(11) . .
Ag4 Ag17 C49 Ag18 61.0(3) . .
Ag19 Ag17 C49 Ag18 94.1(3) . .
C13 Ag19 C49 C50 -62(2) . .
C14 Ag19 C49 C50 -7.7(9) . .
Ag17 Ag19 C49 C50 145.1(8) . .
Ag2 Ag19 C49 C50 -169.2(5) . .
Ag18 Ag19 C49 C50 -118.0(7) . .
C13 Ag19 C49 Ag17 152.8(17) . .
C14 Ag19 C49 Ag17 -152.8(3) . .
Ag2 Ag19 C49 Ag17 45.7(3) . .
Ag18 Ag19 C49 Ag17 96.8(3) . .
C13 Ag19 C49 Ag18 55.9(19) . .
C14 Ag19 C49 Ag18 110.3(4) . .
Ag17 Ag19 C49 Ag18 -96.8(3) . .
Ag2 Ag19 C49 Ag18 -51.2(3) . .
C31 Ag18 C49 C50 -80(4) 2_666 .
C32 Ag18 C49 C50 -12.0(9) 2_666 .
Ag19 Ag18 C49 C50 127.7(6) . .
Ag11 Ag18 C49 C50 -142.4(4) 2_666 .
Ag17 Ag18 C49 C50 -144.5(7) . .
C31 Ag18 C49 Ag17 65(4) 2_666 .
C32 Ag18 C49 Ag17 132.5(4) 2_666 .
Ag19 Ag18 C49 Ag17 -87.8(3) . .
Ag11 Ag18 C49 Ag17 2.1(4) 2_666 .
C31 Ag18 C49 Ag19 153(3) 2_666 .
C32 Ag18 C49 Ag19 -139.8(4) 2_666 .
Ag11 Ag18 C49 Ag19 89.9(3) 2_666 .
Ag17 Ag18 C49 Ag19 87.8(3) . .
Ag17 C49 C50 C51 47(9) . .
Ag19 C49 C50 C51 -78(9) . .
Ag18 C49 C50 C51 172(9) . .
C49 C50 C51 C52 131(9) . .
C49 C50 C51 C53 -109(9) . .
C49 C50 C51 C54 9(9) . .
C43 Ag16 C55 C56 -74.8(18) . .
Ag4 Ag16 C55 C56 -163.4(12) . .
Ag10 Ag16 C55 C56 -128.5(15) 2_666 .
Ag8 Ag16 C55 C56 127.0(15) 2_666 .
C43 Ag16 C55 Ag10 53.7(11) . 2_666
Ag4 Ag16 C55 Ag10 -34.9(3) . 2_666
Ag8 Ag16 C55 Ag10 -104.5(3) 2_666 2_666
C43 Ag16 C55 Ag8 158.2(9) . 2_666
Ag4 Ag16 C55 Ag8 69.6(3) . 2_666
Ag10 Ag16 C55 Ag8 104.5(3) 2_666 2_666
Ag16 C55 C56 C57 -36(3) . .
Ag10 C55 C56 C57 -160(2) 2_666 .
Ag8 C55 C56 C57 89(2) 2_666 .
Ag16 C55 C56 C57B 106(3) . .
Ag10 C55 C56 C57B -18(3) 2_666 .
Ag8 C55 C56 C57B -129(3) 2_666 .
Ag16 C55 C56 Ag8 -125.5(14) . 2_666
Ag10 C55 C56 Ag8 110.9(5) 2_666 2_666
C57 C57B C56 C55 -157(3) . .
C60 C57B C56 C55 -92(3) . .
C58B C57B C56 C55 26(3) . .
C59 C57B C56 C55 146(2) . .
C60 C57B C56 C57 65.6(12) . .
C58B C57B C56 C57 -176.7(19) . .
C59 C57B C56 C57 -56.6(11) . .
C57 C57B C56 Ag8 88.0(14) . 2_666
C60 C57B C56 Ag8 153.6(7) . 2_666
C58B C57B C56 Ag8 -88.6(15) . 2_666
C59 C57B C56 Ag8 31.4(15) . 2_666
C60 C57B C57 C59 127.2(8) . .
C58B C57B C57 C59 41(12) . .
C56 C57B C57 C59 -117.5(7) . .
C58B C57B C57 C60 -86(12) . .
C59 C57B C57 C60 -127.2(8) . .
C56 C57B C57 C60 115.3(8) . .
C60 C57B C57 C58 11(9) . .
C58B C57B C57 C58 -76(17) . .
C59 C57B C57 C58 -116(9) . .
C56 C57B C57 C58 126(9) . .
C60 C57B C57 C56 -115.3(8) . .
C58B C57B C57 C56 158(12) . .
C59 C57B C57 C56 117.5(7) . .
C58 C58 C57 C57B -127(8) 2_565 .
C58 C58 C57 C59 120(4) 2_565 .
C58 C58 C57 C60 -117(4) 2_565 .
C58 C58 C57 C56 -4(4) 2_565 .
C55 C56 C57 C57B 162(2) . .
Ag8 C56 C57 C57B -124.8(11) 2_666 .
C55 C56 C57 C59 -132.3(19) . .
C57B C56 C57 C59 65.4(12) . .
Ag8 C56 C57 C59 -59.4(12) 2_666 .
C55 C56 C57 C60 105(2) . .
C57B C56 C57 C60 -57.6(11) . .
Ag8 C56 C57 C60 177.5(6) 2_666 .
C55 C56 C57 C58 -9(3) . .
C57B C56 C57 C58 -171.2(18) . .
Ag8 C56 C57 C58 64.0(13) 2_666 .
C60 C57 C59 C57B 52.8(11) . .
C58 C57 C59 C57B 170.5(16) . .
C56 C57 C59 C57B -63.4(11) . .
C60 C57B C59 C57 -57.6(12) . .
C58B C57B C59 C57 -174.5(16) . .
C56 C57B C59 C57 59.3(11) . .
C58B C57B C60 C57 171.7(17) . .
C59 C57B C60 C57 53.0(11) . .
C56 C57B C60 C57 -62.5(11) . .
C59 C57 C60 C57B -57.8(12) . .
C58 C57 C60 C57B -178.1(16) . .
C56 C57 C60 C57B 61.9(11) . .
C63 O25 C62 C61 -177.6(13) . .
C62 O25 C63 C64 163.8(18) . .
