#------------------------------------------------------------------------------
#$Date: 2016-03-22 12:50:11 +0200 (Tue, 22 Mar 2016) $
#$Revision: 178965 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/94/4119444.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4119444
loop_
_publ_author_name
'Polly L. Arnold'
'Emmalina Hollis'
'Gary S. Nichol'
'Jason B. Love'
'Jean-Christophe Griveau'
'Roberto Caciuffo'
'Nicola Magnani'
'Laurent Maron'
'Ludovic Castro'
'Ahmed Yahia'
'Samuel O. Odoh'
'Georg Schreckenbach'
_publ_section_title
;
 Oxo-Functionalization and Reduction of the Uranyl Ion through
 Lanthanide-Element Bond Homolysis: Synthetic, Structural, and Bonding
 Analysis of a Series of Singly Reduced Uranyl-Rare Earth 5f1-4fn
 Complexes
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              3841
_journal_page_last               3854
_journal_paper_doi               10.1021/ja308993g
_journal_volume                  135
_journal_year                    2013
_chemical_formula_moiety         'C109 H105 Dy2 N21 O4 U2'
_chemical_formula_sum            'C109 H105 Dy2 N21 O4 U2'
_chemical_formula_weight         2574.20
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 108.32(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.405(3)
_cell_length_b                   27.544(3)
_cell_length_c                   23.131(5)
_cell_measurement_reflns_used    4099
_cell_measurement_temperature    170(2)
_cell_measurement_theta_max      24.3542
_cell_measurement_theta_min      2.9180
_cell_volume                     9922(3)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan  5 2010,16:28:46)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan  5 2010,16:28:46)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan  5 2010,16:28:46)
;
_computing_molecular_graphics    'ORTEP (Farrugia, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      170(2)
_diffrn_detector_area_resol_mean 16.1042
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0713
_diffrn_reflns_av_sigmaI/netI    0.0911
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            63462
_diffrn_reflns_theta_full        24.41
_diffrn_reflns_theta_max         24.41
_diffrn_reflns_theta_min         2.92
_exptl_absorpt_coefficient_mu    4.808
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.80917
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.34.46 (release 25-11-2010 CrysAlis171 .NET)
(compiled Nov 25 2010,17:55:46)
empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.723
_exptl_crystal_description       prism
_exptl_crystal_F_000             5016
_exptl_crystal_size_max          0.1576
_exptl_crystal_size_mid          0.1072
_exptl_crystal_size_min          0.0340
_refine_diff_density_max         1.684
_refine_diff_density_min         -1.869
_refine_diff_density_rms         0.183
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.079
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1314
_refine_ls_number_reflns         16018
_refine_ls_number_restraints     204
_refine_ls_restrained_S_all      1.075
_refine_ls_R_factor_all          0.0725
_refine_ls_R_factor_gt           0.0437
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0221P)²+6.0412P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0753
_refine_ls_wR_factor_ref         0.0915
_reflns_number_gt                11890
_reflns_number_total             16018
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ja308993g_si_007.cif
_cod_data_source_block           p11036b
_cod_database_code               4119444
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.2177(5) 0.0035(3) 0.9374(4) 0.035(2) Uani 1 1 d . . .
H1 H 0.2736 0.0155 0.9419 0.042 Uiso 1 1 calc R . .
C2 C 0.1839(5) -0.0334(3) 0.8939(4) 0.028(2) Uani 1 1 d . . .
C3 C 0.2176(5) -0.0583(3) 0.8546(4) 0.033(2) Uani 1 1 d . . .
H3 H 0.2743 -0.0560 0.8524 0.040 Uiso 1 1 calc R . .
C4 C 0.1520(5) -0.0873(3) 0.8193(4) 0.033(2) Uani 1 1 d . . .
H4 H 0.1556 -0.1092 0.7884 0.039 Uiso 1 1 calc R . .
C5 C 0.0791(5) -0.0786(3) 0.8372(3) 0.0271(19) Uani 1 1 d . . .
C6 C -0.0096(5) -0.1006(3) 0.8136(4) 0.032(2) Uani 1 1 d . . .
C7 C -0.0271(5) -0.1298(3) 0.8650(4) 0.038(2) Uani 1 1 d . . .
H7A H 0.0154 -0.1559 0.8779 0.057 Uiso 1 1 calc R . .
H7B H -0.0848 -0.1439 0.8503 0.057 Uiso 1 1 calc R . .
H7C H -0.0230 -0.1083 0.8995 0.057 Uiso 1 1 calc R . .
C8 C -0.0158(5) -0.1340(3) 0.7599(4) 0.044(2) Uani 1 1 d . . .
H8A H -0.0012 -0.1157 0.7281 0.065 Uiso 1 1 calc R . .
H8B H -0.0744 -0.1466 0.7435 0.065 Uiso 1 1 calc R . .
H8C H 0.0244 -0.1611 0.7734 0.065 Uiso 1 1 calc R . .
C9 C -0.0758(5) -0.0601(3) 0.7936(4) 0.030(2) Uani 1 1 d . . .
C10 C -0.1335(5) -0.0508(3) 0.7371(4) 0.038(2) Uani 1 1 d . . .
H10 H -0.1409 -0.0696 0.7014 0.045 Uiso 1 1 calc R . .
C11 C -0.1787(5) -0.0097(3) 0.7411(4) 0.032(2) Uani 1 1 d U . .
H11 H -0.2221 0.0056 0.7090 0.038 Uiso 1 1 calc R . .
C12 C -0.1481(5) 0.0054(3) 0.8019(4) 0.032(2) Uani 1 1 d . . .
C13 C -0.1688(5) 0.0469(3) 0.8305(4) 0.030(2) Uani 1 1 d . . .
H13 H -0.2110 0.0690 0.8072 0.036 Uiso 1 1 calc R . .
C14 C -0.1426(4) 0.1029(3) 0.9096(4) 0.030(2) Uani 1 1 d . . .
C15 C -0.1673(5) 0.1085(3) 0.9622(4) 0.031(2) Uani 1 1 d U . .
H15 H -0.1753 0.0800 0.9829 0.037 Uiso 1 1 calc R . .
C16 C -0.1805(5) 0.1526(3) 0.9857(4) 0.039(2) Uani 1 1 d . . .
C17 C -0.2072(6) 0.1574(3) 1.0414(4) 0.052(3) Uani 1 1 d . . .
H17A H -0.2637 0.1730 1.0308 0.078 Uiso 1 1 calc R . .
H17B H -0.1651 0.1772 1.0716 0.078 Uiso 1 1 calc R . .
H17C H -0.2104 0.1252 1.0584 0.078 Uiso 1 1 calc R . .
C18 C -0.1718(7) 0.2448(3) 0.9797(5) 0.074(4) Uani 1 1 d . . .
H18A H -0.1617 0.2692 0.9518 0.111 Uiso 1 1 calc R . .
H18B H -0.1285 0.2482 1.0198 0.111 Uiso 1 1 calc R . .
H18C H -0.2291 0.2496 0.9835 0.111 Uiso 1 1 calc R . .
C19 C -0.1660(5) 0.1947(3) 0.9549(4) 0.044(2) Uani 1 1 d . . .
C20 C -0.1411(5) 0.1895(3) 0.9037(4) 0.038(2) Uani 1 1 d . . .
H20 H -0.1325 0.2179 0.8831 0.045 Uiso 1 1 calc R . .
C21 C -0.1278(5) 0.1441(3) 0.8805(4) 0.0246(19) Uani 1 1 d . . .
C22 C -0.1331(5) 0.1682(3) 0.7820(4) 0.040(2) Uani 1 1 d . . .
H22 H -0.1904 0.1782 0.7767 0.048 Uiso 1 1 calc R . .
C23 C -0.0953(6) 0.1807(3) 0.7364(4) 0.041(2) Uani 1 1 d . . .
C24 C -0.1331(7) 0.1979(4) 0.6791(5) 0.073(3) Uani 1 1 d . . .
H24 H -0.1922 0.2050 0.6604 0.088 Uiso 1 1 calc R . .
C25 C -0.0680(7) 0.2030(4) 0.6538(5) 0.075(4) Uani 1 1 d . . .
H25 H -0.0739 0.2144 0.6139 0.090 Uiso 1 1 calc R . .
C26 C 0.0074(7) 0.1887(3) 0.6968(5) 0.049(3) Uani 1 1 d . . .
C27 C 0.0951(7) 0.1889(3) 0.6900(4) 0.053(3) Uani 1 1 d . . .
C28 C 0.1074(8) 0.2361(4) 0.6593(5) 0.098(4) Uani 1 1 d . . .
H28A H 0.0595 0.2406 0.6217 0.146 Uiso 1 1 calc R . .
H28B H 0.1614 0.2347 0.6497 0.146 Uiso 1 1 calc R . .
H28C H 0.1092 0.2635 0.6868 0.146 Uiso 1 1 calc R . .
C29 C 0.1015(6) 0.1464(4) 0.6480(4) 0.067(3) Uani 1 1 d . . .
H29A H 0.0937 0.1156 0.6668 0.100 Uiso 1 1 calc R . .
H29B H 0.1581 0.1468 0.6420 0.100 Uiso 1 1 calc R . .
H29C H 0.0567 0.1498 0.6085 0.100 Uiso 1 1 calc R . .
C30 C 0.1683(6) 0.1834(3) 0.7484(4) 0.042(2) Uani 1 1 d . . .
C31 C 0.2494(7) 0.2048(3) 0.7620(5) 0.061(3) Uani 1 1 d . . .
H31 H 0.2679 0.2270 0.7372 0.074 Uiso 1 1 calc R . .
C32 C 0.2979(7) 0.1874(3) 0.8191(5) 0.064(3) Uani 1 1 d . . .
H32 H 0.3559 0.1955 0.8405 0.076 Uiso 1 1 calc R . .
C33 C 0.2460(6) 0.1564(3) 0.8385(5) 0.043(2) Uani 1 1 d . . .
C34 C 0.2620(5) 0.1363(3) 0.8978(4) 0.038(2) Uani 1 1 d . . .
H34 H 0.3178 0.1400 0.9262 0.045 Uiso 1 1 calc R . .
C35 C 0.2252(4) 0.1071(3) 0.9800(4) 0.0244(19) Uani 1 1 d . . .
C36 C 0.2568(5) 0.1466(3) 1.0182(4) 0.030(2) Uani 1 1 d . . .
H36 H 0.2689 0.1758 1.0006 0.036 Uiso 1 1 calc R . .
C37 C 0.2714(5) 0.1454(3) 1.0812(4) 0.033(2) Uani 1 1 d . . .
C38 C 0.3052(6) 0.1890(3) 1.1194(4) 0.049(3) Uani 1 1 d . . .
H38A H 0.2709 0.1949 1.1466 0.074 Uiso 1 1 calc R . .
H38B H 0.3017 0.2173 1.0930 0.074 Uiso 1 1 calc R . .
H38C H 0.3652 0.1834 1.1437 0.074 Uiso 1 1 calc R . .
C39 C 0.2660(5) 0.0991(3) 1.1738(4) 0.042(2) Uani 1 1 d . . .
H39A H 0.2546 0.0659 1.1843 0.063 Uiso 1 1 calc R . .
H39B H 0.2265 0.1216 1.1842 0.063 Uiso 1 1 calc R . .
H39C H 0.3254 0.1080 1.1965 0.063 Uiso 1 1 calc R . .
C40 C 0.2534(5) 0.1021(3) 1.1071(4) 0.031(2) Uani 1 1 d . . .
C41 C 0.2223(4) 0.0628(3) 1.0688(4) 0.032(2) Uani 1 1 d . . .
H41 H 0.2094 0.0337 1.0863 0.038 Uiso 1 1 calc R . .
C42 C 0.2089(4) 0.0637(3) 1.0063(4) 0.0220(18) Uani 1 1 d U . .
C43 C 0.0645(5) 0.1871(3) 0.9564(5) 0.052(3) Uani 1 1 d . . .
H43 H 0.0471 0.1565 0.9673 0.062 Uiso 1 1 calc R . .
C44 C 0.0776(7) 0.2250(5) 0.9979(5) 0.073(3) Uani 1 1 d . . .
H44 H 0.0699 0.2205 1.0366 0.088 Uiso 1 1 calc R . .
C45 C 0.1021(8) 0.2688(5) 0.9812(8) 0.100(5) Uani 1 1 d . . .
H45 H 0.1117 0.2955 1.0085 0.120 Uiso 1 1 calc R . .
C46 C 0.1127(8) 0.2742(4) 0.9258(7) 0.088(4) Uani 1 1 d . . .
H46 H 0.1299 0.3046 0.9139 0.106 Uiso 1 1 calc R . .
C47 C 0.0983(6) 0.2355(3) 0.8876(5) 0.056(3) Uani 1 1 d . . .
H47 H 0.1051 0.2398 0.8486 0.067 Uiso 1 1 calc R . .
C48 C 0.0671(5) 0.0237(3) 0.7493(4) 0.042(2) Uani 1 1 d . . .
H48 H 0.1097 0.0171 0.7871 0.050 Uiso 1 1 calc R . .
C49 C 0.0601(6) -0.0074(3) 0.7001(4) 0.044(2) Uani 1 1 d . . .
H49 H 0.0979 -0.0342 0.7041 0.053 Uiso 1 1 calc R . .
C50 C -0.0029(6) 0.0018(3) 0.6459(5) 0.046(2) Uani 1 1 d . . .
H50 H -0.0089 -0.0184 0.6116 0.055 Uiso 1 1 calc R . .
C51 C -0.0574(6) 0.0407(3) 0.6418(4) 0.047(3) Uani 1 1 d . . .
H51 H -0.1023 0.0474 0.6051 0.056 Uiso 1 1 calc R . .
C52 C -0.0447(6) 0.0693(3) 0.6922(4) 0.044(2) Uani 1 1 d . . .
H52 H -0.0821 0.0962 0.6890 0.053 Uiso 1 1 calc R . .
C101 C 0.6428(5) 0.9333(3) 0.6655(4) 0.0259(19) Uani 1 1 d . . .
H101 H 0.6716 0.9362 0.7080 0.031 Uiso 1 1 calc R . .
C102 C 0.6503(5) 0.8901(2) 0.6355(4) 0.0253(19) Uani 1 1 d . . .
C103 C 0.6987(5) 0.8482(3) 0.6568(4) 0.032(2) Uani 1 1 d . . .
H103 H 0.7366 0.8428 0.6968 0.039 Uiso 1 1 calc R . .
C104 C 0.6805(5) 0.8161(3) 0.6086(4) 0.036(2) Uani 1 1 d . . .
H104 H 0.7033 0.7843 0.6092 0.044 Uiso 1 1 calc R . .
C105 C 0.6219(5) 0.8394(2) 0.5584(4) 0.029(2) Uani 1 1 d . . .
C106 C 0.5797(5) 0.8204(3) 0.4948(4) 0.031(2) Uani 1 1 d . . .
C107 C 0.6077(5) 0.8509(3) 0.4487(4) 0.042(2) Uani 1 1 d . . .
H10A H 0.5932 0.8850 0.4522 0.063 Uiso 1 1 calc R . .
H10B H 0.5780 0.8393 0.4074 0.063 Uiso 1 1 calc R . .
H10C H 0.6699 0.8478 0.4572 0.063 Uiso 1 1 calc R . .
C108 C 0.6068(5) 0.7677(3) 0.4898(4) 0.054(3) Uani 1 1 d . . .
H10D H 0.6696 0.7659 0.5016 0.081 Uiso 1 1 calc R . .
H10E H 0.5819 0.7565 0.4477 0.081 Uiso 1 1 calc R . .
H10F H 0.5863 0.7471 0.5169 0.081 Uiso 1 1 calc R . .
C109 C 0.4830(5) 0.8231(3) 0.4785(4) 0.030(2) Uani 1 1 d . . .
C110 C 0.4226(5) 0.7861(3) 0.4618(4) 0.035(2) Uani 1 1 d . . .
H110 H 0.4340 0.7528 0.4569 0.043 Uiso 1 1 calc R . .
C111 C 0.3439(5) 0.8063(3) 0.4535(4) 0.036(2) Uani 1 1 d . . .
H111 H 0.2901 0.7900 0.4414 0.043 Uiso 1 1 calc R . .
C112 C 0.3576(5) 0.8554(3) 0.4663(4) 0.027(2) Uani 1 1 d . . .
C113 C 0.2986(5) 0.8940(3) 0.4682(3) 0.029(2) Uani 1 1 d . . .
H113 H 0.2396 0.8867 0.4608 0.035 Uiso 1 1 calc R . .
C114 C 0.2653(4) 0.9716(3) 0.4911(4) 0.026(2) Uani 1 1 d . . .
C115 C 0.2501(4) 1.0154(3) 0.4588(3) 0.0231(18) Uani 1 1 d . . .
H115 H 0.2808 1.0220 0.4310 0.028 Uiso 1 1 calc R . .
C116 C 0.1920(4) 1.0493(2) 0.4658(4) 0.0238(19) Uani 1 1 d . . .
C117 C 0.1770(5) 1.0959(3) 0.4291(4) 0.038(2) Uani 1 1 d . . .
H11A H 0.2174 1.0977 0.4057 0.057 Uiso 1 1 calc R . .
H11B H 0.1858 1.1237 0.4567 0.057 Uiso 1 1 calc R . .
H11C H 0.1180 1.0963 0.4011 0.057 Uiso 1 1 calc R . .
C118 C 0.0799(5) 1.0744(3) 0.5141(4) 0.043(2) Uani 1 1 d . . .
H11D H 0.0564 1.0618 0.5452 0.065 Uiso 1 1 calc R . .
H11E H 0.0334 1.0781 0.4755 0.065 Uiso 1 1 calc R . .
H11F H 0.1067 1.1061 0.5270 0.065 Uiso 1 1 calc R . .
C119 C 0.1460(5) 1.0396(3) 0.5058(4) 0.032(2) Uani 1 1 d . . .
C120 C 0.1629(5) 0.9975(3) 0.5399(4) 0.032(2) Uani 1 1 d . . .
H120 H 0.1329 0.9917 0.5683 0.038 Uiso 1 1 calc R . .
C121 C 0.2227(4) 0.9628(3) 0.5340(4) 0.0237(19) Uani 1 1 d . . .
C122 C 0.1783(5) 0.8988(3) 0.5827(4) 0.033(2) Uani 1 1 d . . .
H122 H 0.1237 0.9023 0.5528 0.040 Uiso 1 1 calc R . .
C123 C 0.1857(5) 0.8675(3) 0.6327(4) 0.030(2) Uani 1 1 d . . .
C124 C 0.1238(6) 0.8376(3) 0.6455(5) 0.045(3) Uani 1 1 d . . .
H124 H 0.0654 0.8339 0.6213 0.054 Uiso 1 1 calc R . .
C125 C 0.1643(6) 0.8147(3) 0.6995(5) 0.049(3) Uani 1 1 d . . .
H125 H 0.1398 0.7916 0.7197 0.059 Uiso 1 1 calc R . .
C126 C 0.2496(6) 0.8322(3) 0.7193(4) 0.039(2) Uani 1 1 d . . .
C127 C 0.3190(6) 0.8143(3) 0.7757(5) 0.053(3) Uani 1 1 d . . .
C128 C 0.2804(6) 0.8008(4) 0.8267(5) 0.077(4) Uani 1 1 d . . .
H12A H 0.2533 0.8295 0.8378 0.115 Uiso 1 1 calc R . .
H12B H 0.3262 0.7892 0.8625 0.115 Uiso 1 1 calc R . .
H12C H 0.2374 0.7752 0.8121 0.115 Uiso 1 1 calc R . .
C129 C 0.3607(7) 0.7683(3) 0.7587(5) 0.079(4) Uani 1 1 d . . .
H12D H 0.3167 0.7433 0.7436 0.119 Uiso 1 1 calc R . .
H12E H 0.4053 0.7562 0.7948 0.119 Uiso 1 1 calc R . .
H12F H 0.3864 0.7764 0.7270 0.119 Uiso 1 1 calc R . .
C130 C 0.3909(5) 0.8512(3) 0.8038(4) 0.036(2) Uani 1 1 d . . .
C131 C 0.4396(7) 0.8549(4) 0.8625(5) 0.077(4) Uani 1 1 d . . .
H131 H 0.4330 0.8362 0.8953 0.093 Uiso 1 1 calc R . .
C132 C 0.5010(6) 0.8902(3) 0.8670(5) 0.059(3) Uani 1 1 d U . .
H132 H 0.5435 0.9009 0.9031 0.070 Uiso 1 1 calc R . .
C133 C 0.4878(6) 0.9071(3) 0.8077(4) 0.039(2) Uani 1 1 d . . .
C134 C 0.5298(5) 0.9446(3) 0.7883(4) 0.037(2) Uani 1 1 d U . .
H134 H 0.5735 0.9622 0.8177 0.044 Uiso 1 1 calc R . .
C135 C 0.5449(5) 1.0020(3) 0.7178(4) 0.0257(19) Uani 1 1 d U . .
C136 C 0.5349(5) 1.0425(3) 0.7516(4) 0.037(2) Uani 1 1 d U . .
H136 H 0.5089 1.0383 0.7826 0.045 Uiso 1 1 calc R . .
C137 C 0.5621(5) 1.0889(3) 0.7411(4) 0.043(2) Uani 1 1 d . . .
C138 C 0.5478(7) 1.1305(3) 0.7800(5) 0.077(4) Uani 1 1 d . . .
H13A H 0.6031 1.1411 0.8082 0.116 Uiso 1 1 calc R . .
H13B H 0.5105 1.1197 0.8033 0.116 Uiso 1 1 calc R . .
H13C H 0.5206 1.1577 0.7537 0.116 Uiso 1 1 calc R . .
C139 C 0.6272(6) 1.1438(3) 0.6815(4) 0.055(3) Uani 1 1 d . . .
H13D H 0.5764 1.1634 0.6611 0.083 Uiso 1 1 calc R . .
H13E H 0.6630 1.1406 0.6549 0.083 Uiso 1 1 calc R . .
H13F H 0.6602 1.1598 0.7195 0.083 Uiso 1 1 calc R . .
C140 C 0.5996(5) 1.0946(3) 0.6954(4) 0.033(2) Uani 1 1 d U . .
C141 C 0.6071(5) 1.0550(3) 0.6608(4) 0.032(2) Uani 1 1 d U . .
H141 H 0.6294 1.0596 0.6279 0.038 Uiso 1 1 calc R . .
C142 C 0.5829(4) 1.0089(3) 0.6726(3) 0.0210(18) Uani 1 1 d . . .
C143 C 0.3365(5) 1.0296(3) 0.6561(4) 0.045(2) Uani 1 1 d . . .
H143 H 0.3538 1.0263 0.6207 0.054 Uiso 1 1 calc R . .
C144 C 0.3198(6) 1.0753(3) 0.6746(5) 0.059(3) Uani 1 1 d . . .
H144 H 0.3251 1.1033 0.6520 0.071 Uiso 1 1 calc R . .
C145 C 0.2954(6) 1.0799(4) 0.7262(5) 0.064(3) Uani 1 1 d . . .
H145 H 0.2852 1.1110 0.7403 0.076 Uiso 1 1 calc R . .
C146 C 0.2860(7) 1.0388(4) 0.7568(5) 0.069(3) Uani 1 1 d . . .
H146 H 0.2674 1.0411 0.7916 0.083 Uiso 1 1 calc R . .
C147 C 0.3037(6) 0.9942(3) 0.7367(4) 0.050(3) Uani 1 1 d . . .
H147 H 0.2979 0.9659 0.7585 0.060 Uiso 1 1 calc R . .
C200 C 0.4845(11) 0.0247(6) 0.9166(7) 0.125(6) Uani 1 1 d . . .
H200 H 0.4528 -0.0038 0.9007 0.150 Uiso 1 1 calc R . .
C201 C 0.4445(9) 0.0646(8) 0.9195(10) 0.186(10) Uani 1 1 d . . .
H201 H 0.3835 0.0645 0.9041 0.223 Uiso 1 1 calc R . .
C202 C 0.4809(11) 0.1038(7) 0.9416(10) 0.192(11) Uani 1 1 d . . .
H202 H 0.4458 0.1309 0.9431 0.230 Uiso 1 1 calc R . .
C203 C 0.5570(16) 0.1089(7) 0.9607(10) 0.187(10) Uani 1 1 d . . .
H203 H 0.5821 0.1392 0.9760 0.224 Uiso 1 1 calc R . .
C204 C 0.6084(11) 0.0675(10) 0.9597(10) 0.180(10) Uani 1 1 d . . .
H204 H 0.6691 0.0705 0.9755 0.216 Uiso 1 1 calc R . .
N110 N 0.4132(12) 0.8271(7) 0.6380(10) 0.040(5) Uani 0.501(14) 1 d PU A 1
C148 C 0.3543(13) 0.7910(6) 0.6162(9) 0.048(5) Uani 0.501(14) 1 d PU A 1
H148 H 0.2953 0.7993 0.6061 0.058 Uiso 0.501(14) 1 calc PR A 1
C149 C 0.3740(13) 0.7438(6) 0.6077(9) 0.047(5) Uani 0.501(14) 1 d PU A 1
H149 H 0.3306 0.7200 0.5928 0.056 Uiso 0.501(14) 1 calc PR A 1
C150 C 0.4591(15) 0.7329(9) 0.6219(12) 0.049(5) Uani 0.501(14) 1 d PU A 1
H150 H 0.4757 0.7011 0.6144 0.059 Uiso 0.501(14) 1 calc PR A 1
C152 C 0.4931(14) 0.8140(8) 0.6505(12) 0.051(5) Uani 0.501(14) 1 d PU A 1
H152 H 0.5363 0.8383 0.6634 0.062 Uiso 0.501(14) 1 calc PR A 1
C151 C 0.5188(14) 0.7658(8) 0.6459(13) 0.063(6) Uani 0.501(14) 1 d PU A 1
H151 H 0.5778 0.7571 0.6598 0.075 Uiso 0.501(14) 1 calc PR A 1
N111 N 0.4505(14) 0.8329(7) 0.6559(11) 0.045(5) Uani 0.499(14) 1 d PU A 2
C153 C 0.4143(17) 0.8055(8) 0.6108(11) 0.057(6) Uani 0.499(14) 1 d PU A 2
H153 H 0.3678 0.8189 0.5792 0.068 Uiso 0.499(14) 1 calc PR A 2
C154 C 0.4377(19) 0.7559(9) 0.6036(11) 0.068(7) Uani 0.499(14) 1 d PU A 2
H154 H 0.4119 0.7378 0.5675 0.082 Uiso 0.499(14) 1 calc PR A 2
C155 C 0.5005(16) 0.7366(8) 0.6530(11) 0.050(5) Uani 0.499(14) 1 d PU A 2
H155 H 0.5138 0.7029 0.6545 0.060 Uiso 0.499(14) 1 calc PR A 2
C156 C 0.5440(12) 0.7674(7) 0.7009(11) 0.053(5) Uani 0.499(14) 1 d PU A 2
H156 H 0.5932 0.7566 0.7325 0.064 Uiso 0.499(14) 1 calc PR A 2
C157 C 0.5140(11) 0.8131(6) 0.7009(12) 0.052(5) Uani 0.499(14) 1 d PU A 2
H157 H 0.5400 0.8326 0.7356 0.063 Uiso 0.499(14) 1 calc PR A 2
N1 N 0.1754(3) 0.0216(2) 0.9712(3) 0.0216(15) Uani 1 1 d . . .
N2 N 0.0975(4) -0.0446(2) 0.8833(3) 0.0242(15) Uani 1 1 d U . .
N3 N -0.0830(4) -0.0258(2) 0.8344(3) 0.0250(16) Uani 1 1 d . . .
N4 N -0.1307(4) 0.0555(2) 0.8885(3) 0.0266(16) Uani 1 1 d . . .
N5 N -0.0925(4) 0.1437(2) 0.8307(3) 0.0274(16) Uani 1 1 d . . .
N6 N -0.0085(5) 0.1746(2) 0.7490(3) 0.0387(18) Uani 1 1 d . . .
N7 N 0.1667(4) 0.1532(2) 0.7949(3) 0.0348(18) Uani 1 1 d . . .
N8 N 0.2055(4) 0.1133(2) 0.9148(3) 0.0274(16) Uani 1 1 d . . .
N9 N 0.0752(4) 0.1918(2) 0.9017(4) 0.044(2) Uani 1 1 d . . .
N10 N 0.0159(4) 0.0624(2) 0.7451(3) 0.0345(18) Uani 1 1 d . . .
N101 N 0.5967(4) 0.9697(2) 0.6360(3) 0.0209(15) Uani 1 1 d . A .
N102 N 0.6032(4) 0.8844(2) 0.5740(3) 0.0250(16) Uani 1 1 d . A .
N103 N 0.4433(4) 0.8659(2) 0.4826(3) 0.0238(15) Uani 1 1 d . A .
N104 N 0.3249(4) 0.9381(2) 0.4796(3) 0.0220(15) Uani 1 1 d . A .
N105 N 0.2429(4) 0.9231(2) 0.5758(3) 0.0317(17) Uani 1 1 d . A .
N106 N 0.2625(4) 0.8637(2) 0.6781(3) 0.0380(19) Uani 1 1 d . A .
N107 N 0.4186(4) 0.8825(2) 0.7688(3) 0.0376(18) Uani 1 1 d U A .
N108 N 0.5109(4) 0.9564(2) 0.7307(3) 0.0292(16) Uani 1 1 d . A .
N109 N 0.3285(4) 0.9896(2) 0.6878(4) 0.0398(19) Uani 1 1 d . A .
N200 N 0.5737(11) 0.0235(7) 0.9367(6) 0.153(6) Uani 1 1 d . . .
O1 O 0.0359(3) 0.06157(16) 0.8851(2) 0.0253(13) Uani 1 1 d . . .
O2 O -0.0113(3) -0.04307(15) 0.9795(2) 0.0211(12) Uani 1 1 d U . .
O3 O 0.4374(3) 0.92819(16) 0.5949(2) 0.0260(13) Uani 1 1 d . A .
O4 O 0.5382(3) 0.97060(15) 0.4744(2) 0.0181(12) Uani 1 1 d . . .
Dy1 Dy 0.05745(2) 0.122792(12) 0.832024(18) 0.02649(11) Uani 1 1 d . . .
Dy2 Dy 0.37908(2) 0.909709(13) 0.665581(19) 0.02941(11) Uani 1 1 d . . .
U1 U 0.012154(18) 0.007951(10) 0.929002(14) 0.02237(9) Uani 1 1 d . . .
U2 U 0.488315(17) 0.945303(9) 0.534189(14) 0.02027(9) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 C1 C2 122.7(7) . .
N1 C1 H1 118.7 . .
C2 C1 H1 118.7 . .
C3 C2 N2 111.6(7) . .
C3 C2 C1 132.4(7) . .
N2 C2 C1 115.7(7) . .
C4 C3 C2 106.1(7) . .
C4 C3 H3 126.9 . .
C2 C3 H3 126.9 . .
C3 C4 C5 107.6(7) . .
C3 C4 H4 126.2 . .
C5 C4 H4 126.2 . .
N2 C5 C4 110.2(7) . .
N2 C5 C6 120.3(7) . .
C4 C5 C6 129.6(7) . .
C5 C6 C8 110.2(7) . .
C5 C6 C9 109.2(6) . .
C8 C6 C9 109.7(7) . .
C5 C6 C7 108.8(7) . .
C8 C6 C7 109.6(6) . .
C9 C6 C7 109.2(6) . .
C6 C7 H7A 109.5 . .
C6 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C6 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
C6 C8 H8A 109.5 . .
C6 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
C6 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
N3 C9 C10 110.2(7) . .
N3 C9 C6 120.4(7) . .
C10 C9 C6 129.4(8) . .
C11 C10 C9 108.2(8) . .
C11 C10 H10 125.9 . .
C9 C10 H10 125.9 . .
C10 C11 C12 106.5(7) . .
C10 C11 H11 126.8 . .
C12 C11 H11 126.8 . .
N3 C12 C11 109.4(7) . .
N3 C12 C13 120.1(8) . .
C11 C12 C13 130.3(8) . .
N4 C13 C12 121.2(7) . .
N4 C13 H13 119.4 . .
C12 C13 H13 119.4 . .
C21 C14 C15 118.3(7) . .
C21 C14 N4 121.4(8) . .
C15 C14 N4 120.2(7) . .
C16 C15 C14 124.2(8) . .
C16 C15 H15 117.9 . .
C14 C15 H15 117.9 . .
C15 C16 C19 116.9(8) . .
C15 C16 C17 123.1(8) . .
C19 C16 C17 120.1(8) . .
C16 C17 H17A 109.5 . .
C16 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C16 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C19 C18 H18A 109.5 . .
C19 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C19 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C20 C19 C16 119.2(8) . .
C20 C19 C18 119.6(8) . .
C16 C19 C18 121.1(8) . .
C19 C20 C21 123.1(8) . .
C19 C20 H20 118.5 . .
C21 C20 H20 118.5 . .
C14 C21 C20 118.3(8) . .
C14 C21 N5 124.0(7) . .
C20 C21 N5 117.6(7) . .
N5 C22 C23 122.9(8) . .
N5 C22 H22 118.5 . .
C23 C22 H22 118.5 . .
C24 C23 N6 112.0(9) . .
C24 C23 C22 129.5(9) . .
N6 C23 C22 118.6(8) . .
C23 C24 C25 105.8(9) . .
C23 C24 H24 127.1 . .
C25 C24 H24 127.1 . .
C24 C25 C26 107.8(9) . .
C24 C25 H25 126.1 . .
C26 C25 H25 126.1 . .
N6 C26 C25 109.9(9) . .
N6 C26 C27 123.4(9) . .
C25 C26 C27 126.7(9) . .
C26 C27 C30 115.4(8) . .
C26 C27 C28 109.0(8) . .
C30 C27 C28 108.7(8) . .
C26 C27 C29 108.6(8) . .
C30 C27 C29 107.1(7) . .
C28 C27 C29 107.9(9) . .
C27 C28 H28A 109.5 . .
C27 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C27 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C27 C29 H29A 109.5 . .
C27 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
C27 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
N7 C30 C31 109.4(9) . .
N7 C30 C27 124.1(8) . .
C31 C30 C27 126.4(8) . .
C32 C31 C30 106.7(8) . .
C32 C31 H31 126.6 . .
C30 C31 H31 126.6 . .
C33 C32 C31 107.1(9) . .
C33 C32 H32 126.4 . .
C31 C32 H32 126.4 . .
N7 C33 C32 109.8(8) . .
N7 C33 C34 121.8(8) . .
C32 C33 C34 127.6(9) . .
N8 C34 C33 123.7(8) . .
N8 C34 H34 118.2 . .
C33 C34 H34 118.2 . .
C36 C35 C42 118.3(7) . .
C36 C35 N8 118.8(7) . .
C42 C35 N8 122.8(7) . .
C35 C36 C37 123.2(7) . .
C35 C36 H36 118.4 . .
C37 C36 H36 118.4 . .
C36 C37 C40 118.1(7) . .
C36 C37 C38 120.5(7) . .
C40 C37 C38 121.4(8) . .
C37 C38 H38A 109.5 . .
C37 C38 H38B 109.5 . .
H38A C38 H38B 109.5 . .
C37 C38 H38C 109.5 . .
H38A C38 H38C 109.5 . .
H38B C38 H38C 109.5 . .
C40 C39 H39A 109.5 . .
C40 C39 H39B 109.5 . .
H39A C39 H39B 109.5 . .
C40 C39 H39C 109.5 . .
H39A C39 H39C 109.5 . .
H39B C39 H39C 109.5 . .
C41 C40 C37 118.4(8) . .
C41 C40 C39 121.3(7) . .
C37 C40 C39 120.3(7) . .
C40 C41 C42 123.6(7) . .
C40 C41 H41 118.2 . .
C42 C41 H41 118.2 . .
C41 C42 C35 118.3(7) . .
C41 C42 N1 119.0(7) . .
C35 C42 N1 122.6(7) . .
N9 C43 C44 123.0(10) . .
N9 C43 H43 118.5 . .
C44 C43 H43 118.5 . .
C45 C44 C43 117.6(12) . .
C45 C44 H44 121.2 . .
C43 C44 H44 121.2 . .
C46 C45 C44 120.2(12) . .
C46 C45 H45 119.9 . .
C44 C45 H45 119.9 . .
C45 C46 C47 118.7(12) . .
C45 C46 H46 120.6 . .
C47 C46 H46 120.6 . .
N9 C47 C46 123.7(11) . .
N9 C47 H47 118.2 . .
C46 C47 H47 118.2 . .
N10 C48 C49 122.5(8) . .
N10 C48 H48 118.8 . .
C49 C48 H48 118.8 . .
C50 C49 C48 118.4(8) . .
C50 C49 H49 120.8 . .
C48 C49 H49 120.8 . .
C49 C50 C51 119.4(9) . .
C49 C50 H50 120.3 . .
C51 C50 H50 120.3 . .
C52 C51 C50 117.8(9) . .
C52 C51 H51 121.1 . .
C50 C51 H51 121.1 . .
N10 C52 C51 124.9(8) . .
N10 C52 H52 117.5 . .
C51 C52 H52 117.5 . .
N101 C101 C102 121.1(7) . .
N101 C101 H101 119.4 . .
C102 C101 H101 119.4 . .
N102 C102 C103 109.7(7) . .
N102 C102 C101 119.6(7) . .
C103 C102 C101 130.7(8) . .
C104 C103 C102 106.8(8) . .
C104 C103 H103 126.6 . .
C102 C103 H103 126.6 . .
C103 C104 C105 107.1(7) . .
C103 C104 H104 126.5 . .
C105 C104 H104 126.5 . .
N102 C105 C104 110.5(7) . .
N102 C105 C106 120.4(7) . .
C104 C105 C106 129.2(7) . .
C105 C106 C109 110.5(6) . .
C105 C106 C108 110.3(7) . .
C109 C106 C108 109.5(6) . .
C105 C106 C107 109.9(6) . .
C109 C106 C107 108.6(7) . .
C108 C106 C107 107.9(7) . .
C106 C107 H10A 109.5 . .
C106 C107 H10B 109.5 . .
H10A C107 H10B 109.5 . .
C106 C107 H10C 109.5 . .
H10A C107 H10C 109.5 . .
H10B C107 H10C 109.5 . .
C106 C108 H10D 109.5 . .
C106 C108 H10E 109.5 . .
H10D C108 H10E 109.5 . .
C106 C108 H10F 109.5 . .
H10D C108 H10F 109.5 . .
H10E C108 H10F 109.5 . .
N103 C109 C110 109.8(7) . .
N103 C109 C106 120.7(6) . .
C110 C109 C106 129.4(7) . .
C111 C110 C109 107.5(7) . .
C111 C110 H110 126.2 . .
C109 C110 H110 126.2 . .
C110 C111 C112 106.5(7) . .
C110 C111 H111 126.7 . .
C112 C111 H111 126.7 . .
N103 C112 C111 110.4(7) . .
N103 C112 C113 118.5(6) . .
C111 C112 C113 131.0(7) . .
N104 C113 C112 120.9(7) . .
N104 C113 H113 119.5 . .
C112 C113 H113 119.5 . .
C115 C114 C121 118.8(7) . .
C115 C114 N104 118.3(7) . .
C121 C114 N104 122.9(7) . .
C116 C115 C114 122.2(7) . .
C116 C115 H115 118.9 . .
C114 C115 H115 118.9 . .
C115 C116 C119 119.2(7) . .
C115 C116 C117 120.3(7) . .
C119 C116 C117 120.5(7) . .
C116 C117 H11A 109.5 . .
C116 C117 H11B 109.5 . .
H11A C117 H11B 109.5 . .
C116 C117 H11C 109.5 . .
H11A C117 H11C 109.5 . .
H11B C117 H11C 109.5 . .
C119 C118 H11D 109.5 . .
C119 C118 H11E 109.5 . .
H11D C118 H11E 109.5 . .
C119 C118 H11F 109.5 . .
H11D C118 H11F 109.5 . .
H11E C118 H11F 109.5 . .
C120 C119 C116 119.1(7) . .
C120 C119 C118 119.1(8) . .
C116 C119 C118 121.8(7) . .
C119 C120 C121 122.5(7) . .
C119 C120 H120 118.8 . .
C121 C120 H120 118.8 . .
C114 C121 C120 118.0(7) . .
C114 C121 N105 123.4(7) . .
C120 C121 N105 118.4(7) . .
N105 C122 C123 123.2(8) . .
N105 C122 H122 118.4 . .
C123 C122 H122 118.4 . .
N106 C123 C124 110.2(7) . .
N106 C123 C122 119.7(7) . .
C124 C123 C122 130.1(8) . .
C125 C124 C123 106.6(8) . .
C125 C124 H124 126.7 . .
C123 C124 H124 126.7 . .
C124 C125 C126 106.6(8) . .
C124 C125 H125 126.7 . .
C126 C125 H125 126.7 . .
N106 C126 C125 110.4(8) . .
N106 C126 C127 124.9(8) . .
C125 C126 C127 124.5(8) . .
C126 C127 C130 114.7(7) . .
C126 C127 C129 108.6(8) . .
C130 C127 C129 107.9(7) . .
C126 C127 C128 110.9(7) . .
C130 C127 C128 106.2(8) . .
C129 C127 C128 108.3(7) . .
C127 C128 H12A 109.5 . .
C127 C128 H12B 109.5 . .
H12A C128 H12B 109.5 . .
C127 C128 H12C 109.5 . .
H12A C128 H12C 109.5 . .
H12B C128 H12C 109.5 . .
C127 C129 H12D 109.5 . .
C127 C129 H12E 109.5 . .
H12D C129 H12E 109.5 . .
C127 C129 H12F 109.5 . .
H12D C129 H12F 109.5 . .
H12E C129 H12F 109.5 . .
C131 C130 N107 110.6(9) . .
C131 C130 C127 127.5(9) . .
N107 C130 C127 121.6(8) . .
C130 C131 C132 108.5(9) . .
C130 C131 H131 125.8 . .
C132 C131 H131 125.8 . .
C131 C132 C133 106.0(10) . .
C131 C132 H132 127.0 . .
C133 C132 H132 127.0 . .
N107 C133 C134 122.9(8) . .
N107 C133 C132 108.4(8) . .
C134 C133 C132 128.6(9) . .
N108 C134 C133 121.9(8) . .
N108 C134 H134 119.1 . .
C133 C134 H134 119.1 . .
C142 C135 C136 118.0(7) . .
C142 C135 N108 124.7(7) . .
C136 C135 N108 117.2(7) . .
C137 C136 C135 122.0(8) . .
C137 C136 H136 119.0 . .
C135 C136 H136 119.0 . .
C140 C137 C136 118.5(8) . .
C140 C137 C138 123.6(8) . .
C136 C137 C138 118.0(8) . .
C137 C138 H13A 109.5 . .
C137 C138 H13B 109.5 . .
H13A C138 H13B 109.5 . .
C137 C138 H13C 109.5 . .
H13A C138 H13C 109.5 . .
H13B C138 H13C 109.5 . .
C140 C139 H13D 109.5 . .
C140 C139 H13E 109.5 . .
H13D C139 H13E 109.5 . .
C140 C139 H13F 109.5 . .
H13D C139 H13F 109.5 . .
H13E C139 H13F 109.5 . .
C141 C140 C137 119.6(7) . .
C141 C140 C139 120.2(8) . .
C137 C140 C139 120.1(7) . .
C140 C141 C142 121.7(8) . .
C140 C141 H141 119.1 . .
C142 C141 H141 119.1 . .
C141 C142 C135 120.0(7) . .
C141 C142 N101 117.8(7) . .
C135 C142 N101 122.2(6) . .
N109 C143 C144 120.7(9) . .
N109 C143 H143 119.7 . .
C144 C143 H143 119.7 . .
C145 C144 C143 119.4(9) . .
C145 C144 H144 120.3 . .
C143 C144 H144 120.3 . .
C146 C145 C144 118.8(9) . .
C146 C145 H145 120.6 . .
C144 C145 H145 120.6 . .
C145 C146 C147 119.6(10) . .
C145 C146 H146 120.2 . .
C147 C146 H146 120.2 . .
N109 C147 C146 121.8(9) . .
N109 C147 H147 119.1 . .
C146 C147 H147 119.1 . .
C201 C200 N200 120.2(15) . .
C201 C200 H200 119.9 . .
N200 C200 H200 119.9 . .
C202 C201 C200 124.3(15) . .
C202 C201 H201 117.8 . .
C200 C201 H201 117.8 . .
C203 C202 C201 123.9(19) . .
C203 C202 H202 118.1 . .
C201 C202 H202 118.1 . .
C202 C203 C204 117.2(19) . .
C202 C203 H203 121.4 . .
C204 C203 H203 121.4 . .
N200 C204 C203 122.5(16) . .
N200 C204 H204 118.7 . .
C203 C204 H204 118.7 . .
C152 N110 C148 115(2) . .
C152 N110 Dy2 119.4(17) . .
C148 N110 Dy2 125.0(14) . .
C149 C148 N110 125.0(18) . .
C149 C148 H148 117.5 . .
N110 C148 H148 117.5 . .
C150 C149 C148 116.4(19) . .
C150 C149 H149 121.8 . .
C148 C149 H149 121.8 . .
C151 C150 C149 121(2) . .
C151 C150 H150 119.4 . .
C149 C150 H150 119.4 . .
N110 C152 C151 123(2) . .
N110 C152 H152 118.3 . .
C151 C152 H152 118.3 . .
C150 C151 C152 119(2) . .
C150 C151 H151 120.7 . .
C152 C151 H151 120.7 . .
C153 N111 C157 116(2) . .
C153 N111 Dy2 118.1(18) . .
C157 N111 Dy2 123.8(16) . .
N111 C153 C154 126(2) . .
N111 C153 H153 117.1 . .
C154 C153 H153 117.1 . .
C155 C154 C153 115(2) . .
C155 C154 H154 122.4 . .
C153 C154 H154 122.4 . .
C154 C155 C156 119(2) . .
C154 C155 H155 120.6 . .
C156 C155 H155 120.6 . .
C157 C156 C155 118(2) . .
C157 C156 H156 121.0 . .
C155 C156 H156 121.0 . .
N111 C157 C156 125(2) . .
N111 C157 H157 117.4 . .
C156 C157 H157 117.4 . .
C1 N1 C42 118.2(6) . .
C1 N1 U1 113.9(5) . .
C42 N1 U1 120.3(4) . .
C5 N2 C2 104.5(6) . .
C5 N2 U1 135.5(5) . .
C2 N2 U1 118.5(5) . .
C9 N3 C12 105.7(7) . .
C9 N3 U1 135.5(5) . .
C12 N3 U1 114.5(5) . .
C13 N4 C14 116.3(6) . .
C13 N4 U1 111.3(5) . .
C14 N4 U1 123.0(4) . .
C22 N5 C21 117.5(7) . .
C22 N5 Dy1 111.2(5) . .
C21 N5 Dy1 128.9(5) . .
C26 N6 C23 104.6(8) . .
C26 N6 Dy1 136.2(6) . .
C23 N6 Dy1 115.2(6) . .
C30 N7 C33 106.9(7) . .
C30 N7 Dy1 134.8(6) . .
C33 N7 Dy1 113.8(6) . .
C34 N8 C35 115.6(7) . .
C34 N8 Dy1 108.9(5) . .
C35 N8 Dy1 129.2(5) . .
C47 N9 C43 116.9(8) . .
C47 N9 Dy1 121.5(7) . .
C43 N9 Dy1 121.6(6) . .
C52 N10 C48 116.9(8) . .
C52 N10 Dy1 125.1(5) . .
C48 N10 Dy1 117.2(6) . .
C101 N101 C142 116.2(6) . .
C101 N101 U2 113.5(5) . .
C142 N101 U2 123.3(4) . .
C105 N102 C102 106.0(6) . .
C105 N102 U2 137.0(5) . .
C102 N102 U2 114.6(4) . .
C109 N103 C112 105.7(6) . .
C109 N103 U2 135.8(5) . .
C112 N103 U2 116.2(4) . .
C113 N104 C114 116.2(6) . .
C113 N104 U2 113.6(5) . .
C114 N104 U2 121.6(4) . .
C122 N105 C121 116.8(7) . .
C122 N105 Dy2 111.3(5) . .
C121 N105 Dy2 128.2(5) . .
C126 N106 C123 106.2(7) . .
C126 N106 Dy2 137.3(6) . .
C123 N106 Dy2 116.6(5) . .
C130 N107 C133 106.5(7) . .
C130 N107 Dy2 139.5(6) . .
C133 N107 Dy2 113.9(5) . .
C134 N108 C135 116.2(7) . .
C134 N108 Dy2 111.2(5) . .
C135 N108 Dy2 128.7(5) . .
C147 N109 C143 119.7(8) . .
C147 N109 Dy2 118.5(6) . .
C143 N109 Dy2 121.2(6) . .
C204 N200 C200 111.8(16) . .
U1 O1 Dy1 177.5(3) . .
U1 O2 U1 107.75(19) . 3_557
U2 O3 Dy2 179.0(3) . .
U2 O4 U2 107.74(18) . 3_676
O1 Dy1 N6 144.2(2) . .
O1 Dy1 N7 138.81(19) . .
N6 Dy1 N7 72.4(2) . .
O1 Dy1 N9 103.7(2) . .
N6 Dy1 N9 89.7(2) . .
N7 Dy1 N9 91.0(2) . .
O1 Dy1 N5 81.55(18) . .
N6 Dy1 N5 69.9(2) . .
N7 Dy1 N5 139.6(2) . .
N9 Dy1 N5 75.2(2) . .
O1 Dy1 N10 83.57(19) . .
N6 Dy1 N10 79.1(2) . .
N7 Dy1 N10 89.4(2) . .
N9 Dy1 N10 168.2(2) . .
N5 Dy1 N10 97.0(2) . .
O1 Dy1 N8 77.65(18) . .
N6 Dy1 N8 138.1(2) . .
N7 Dy1 N8 70.3(2) . .
N9 Dy1 N8 72.7(2) . .
N5 Dy1 N8 135.9(2) . .
N10 Dy1 N8 118.5(2) . .
O3 Dy2 N106 140.0(2) . .
O3 Dy2 N107 140.5(2) . .
N106 Dy2 N107 71.9(2) . .
O3 Dy2 N111 78.5(5) . .
N106 Dy2 N111 88.7(5) . .
N107 Dy2 N111 80.5(6) . .
O3 Dy2 N109 101.7(2) . .
N106 Dy2 N109 96.5(2) . .
N107 Dy2 N109 94.3(2) . .
N111 Dy2 N109 171.1(5) . .
O3 Dy2 N110 80.5(6) . .
N106 Dy2 N110 78.3(5) . .
N107 Dy2 N110 87.6(5) . .
N111 Dy2 N110 15.0(5) . .
N109 Dy2 N110 173.7(5) . .
O3 Dy2 N105 80.56(19) . .
N106 Dy2 N105 69.2(2) . .
N107 Dy2 N105 138.7(2) . .
N111 Dy2 N105 111.7(5) . .
N109 Dy2 N105 77.0(2) . .
N110 Dy2 N105 97.7(5) . .
O3 Dy2 N108 80.60(19) . .
N106 Dy2 N108 139.2(2) . .
N107 Dy2 N108 69.9(2) . .
N111 Dy2 N108 98.4(5) . .
N109 Dy2 N108 72.9(2) . .
N110 Dy2 N108 113.3(5) . .
N105 Dy2 N108 140.1(2) . .
O1 U1 O2 175.2(2) . .
O1 U1 O2 102.91(18) . 3_557
O2 U1 O2 72.25(19) . 3_557
O1 U1 N3 89.9(2) . .
O2 U1 N3 94.09(19) . .
O2 U1 N3 142.04(18) 3_557 .
O1 U1 N2 89.26(19) . .
O2 U1 N2 94.61(19) . .
O2 U1 N2 142.89(18) 3_557 .
N3 U1 N2 71.4(2) . .
O1 U1 N1 74.09(18) . .
O2 U1 N1 104.88(18) . .
O2 U1 N1 84.10(18) 3_557 .
N3 U1 N1 133.9(2) . .
N2 U1 N1 65.50(19) . .
O1 U1 N4 74.22(19) . .
O2 U1 N4 104.79(18) . .
O2 U1 N4 81.68(18) 3_557 .
N3 U1 N4 67.5(2) . .
N2 U1 N4 135.4(2) . .
N1 U1 N4 141.17(18) . .
O1 U1 U1 135.25(15) . 3_557
O2 U1 U1 39.92(14) . 3_557
O2 U1 U1 32.33(11) 3_557 3_557
N3 U1 U1 124.84(14) . 3_557
N2 U1 U1 125.62(14) . 3_557
N1 U1 U1 94.30(14) . 3_557
N4 U1 U1 92.63(15) . 3_557
O3 U2 O4 173.32(18) . .
O3 U2 O4 101.15(17) . 3_676
O4 U2 O4 72.26(18) . 3_676
O3 U2 N102 91.0(2) . .
O4 U2 N102 93.80(19) . .
O4 U2 N102 142.86(17) 3_676 .
O3 U2 N103 90.21(19) . .
O4 U2 N103 95.80(19) . .
O4 U2 N103 143.63(18) 3_676 .
N102 U2 N103 70.09(19) . .
O3 U2 N101 74.00(19) . .
O4 U2 N101 103.63(18) . .
O4 U2 N101 82.82(17) 3_676 .
N102 U2 N101 66.88(19) . .
N103 U2 N101 133.52(19) . .
O3 U2 N104 73.38(19) . .
O4 U2 N104 106.44(19) . .
O4 U2 N104 84.18(16) 3_676 .
N102 U2 N104 132.95(18) . .
N103 U2 N104 66.01(18) . .
N101 U2 N104 141.63(19) . .
O3 U2 U2 133.29(13) . 3_676
O4 U2 U2 40.11(12) . 3_676
O4 U2 U2 32.15(11) 3_676 3_676
N102 U2 U2 125.18(13) . 3_676
N103 U2 U2 126.95(14) . 3_676
N101 U2 U2 92.70(12) . 3_676
N104 U2 U2 95.13(12) . 3_676
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 N1 1.298(9) .
C1 C2 1.414(10) .
C1 H1 0.9500 .
C2 C3 1.386(10) .
C2 N2 1.394(9) .
C3 C4 1.382(10) .
C3 H3 0.9500 .
C4 C5 1.404(10) .
C4 H4 0.9500 .
C5 N2 1.380(9) .
C5 C6 1.512(10) .
C6 C8 1.522(10) .
C6 C9 1.524(10) .
C6 C7 1.535(10) .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 H8A 0.9800 .
C8 H8B 0.9800 .
C8 H8C 0.9800 .
C9 N3 1.365(9) .
C9 C10 1.377(11) .
C10 C11 1.373(10) .
C10 H10 0.9500 .
C11 C12 1.398(11) .
C11 H11 0.9500 .
C12 N3 1.394(9) .
C12 C13 1.415(10) .
C13 N4 1.313(9) .
C13 H13 0.9500 .
C14 C21 1.381(10) .
C14 C15 1.406(10) .
C14 N4 1.427(9) .
C15 C16 1.374(10) .
C15 H15 0.9500 .
C16 C19 1.420(11) .
C16 C17 1.493(11) .
C17 H17A 0.9800 .
C17 H17B 0.9800 .
C17 H17C 0.9800 .
C18 C19 1.510(11) .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 C20 1.376(11) .
C20 C21 1.403(10) .
C20 H20 0.9500 .
C21 N5 1.443(9) .
C22 N5 1.303(9) .
C22 C23 1.423(11) .
C22 H22 0.9500 .
C23 C24 1.360(12) .
C23 N6 1.371(10) .
C24 C25 1.376(13) .
C24 H24 0.9500 .
C25 C26 1.378(13) .
C25 H25 0.9500 .
C26 N6 1.369(10) .
C26 C27 1.495(13) .
C27 C30 1.506(12) .
C27 C28 1.525(11) .
C27 C29 1.548(12) .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 H29A 0.9800 .
C29 H29B 0.9800 .
C29 H29C 0.9800 .
C30 N7 1.366(10) .
C30 C31 1.398(12) .
C31 C32 1.394(13) .
C31 H31 0.9500 .
C32 C33 1.378(11) .
C32 H32 0.9500 .
C33 N7 1.376(10) .
C33 C34 1.423(12) .
C34 N8 1.283(9) .
C34 H34 0.9500 .
C35 C36 1.396(10) .
C35 C42 1.404(9) .
C35 N8 1.451(9) .
C36 C37 1.402(10) .
C36 H36 0.9500 .
C37 C40 1.408(10) .
C37 C38 1.490(10) .
C38 H38A 0.9800 .
C38 H38B 0.9800 .
C38 H38C 0.9800 .
C39 C40 1.493(11) .
C39 H39A 0.9800 .
C39 H39B 0.9800 .
C39 H39C 0.9800 .
C40 C41 1.389(10) .
C41 C42 1.393(10) .
C41 H41 0.9500 .
C42 N1 1.423(9) .
C43 N9 1.336(11) .
C43 C44 1.388(13) .
C43 H43 0.9500 .
C44 C45 1.366(15) .
C44 H44 0.9500 .
C45 C46 1.355(16) .
C45 H45 0.9500 .
C46 C47 1.358(13) .
C46 H46 0.9500 .
C47 N9 1.333(10) .
C47 H47 0.9500 .
C48 N10 1.342(9) .
C48 C49 1.399(11) .
C48 H48 0.9500 .
C49 C50 1.375(12) .
C49 H49 0.9500 .
C50 C51 1.378(11) .
C50 H50 0.9500 .
C51 C52 1.369(11) .
C51 H51 0.9500 .
C52 N10 1.325(10) .
C52 H52 0.9500 .
C101 N101 1.311(8) .
C101 C102 1.402(10) .
C101 H101 0.9500 .
C102 N102 1.397(9) .
C102 C103 1.401(10) .
C103 C104 1.380(11) .
C103 H103 0.9500 .
C104 C105 1.409(11) .
C104 H104 0.9500 .
C105 N102 1.355(8) .
C105 C106 1.508(11) .
C106 C109 1.513(10) .
C106 C108 1.532(9) .
C106 C107 1.538(10) .
C107 H10A 0.9800 .
C107 H10B 0.9800 .
C107 H10C 0.9800 .
C108 H10D 0.9800 .
C108 H10E 0.9800 .
C108 H10F 0.9800 .
C109 N103 1.365(8) .
C109 C110 1.388(10) .
C110 C111 1.363(10) .
C110 H110 0.9500 .
C111 C112 1.388(9) .
C111 H111 0.9500 .
C112 N103 1.367(8) .
C112 C113 1.447(10) .
C113 N104 1.289(8) .
C113 H113 0.9500 .
C114 C115 1.399(10) .
C114 C121 1.402(10) .
C114 N104 1.430(8) .
C115 C116 1.379(9) .
C115 H115 0.9500 .
C116 C119 1.392(10) .
C116 C117 1.515(10) .
C117 H11A 0.9800 .
C117 H11B 0.9800 .
C117 H11C 0.9800 .
C118 C119 1.505(10) .
C118 H11D 0.9800 .
C118 H11E 0.9800 .
C118 H11F 0.9800 .
C119 C120 1.381(10) .
C120 C121 1.406(9) .
C120 H120 0.9500 .
C121 N105 1.429(9) .
C122 N105 1.305(9) .
C122 C123 1.417(10) .
C122 H122 0.9500 .
C123 N106 1.367(10) .
C123 C124 1.410(10) .
C124 C125 1.370(12) .
C124 H124 0.9500 .
C125 C126 1.413(11) .
C125 H125 0.9500 .
C126 N106 1.354(9) .
C126 C127 1.520(12) .
C127 C130 1.538(12) .
C127 C129 1.548(11) .
C127 C128 1.551(11) .
C128 H12A 0.9800 .
C128 H12B 0.9800 .
C128 H12C 0.9800 .
C129 H12D 0.9800 .
C129 H12E 0.9800 .
C129 H12F 0.9800 .
C130 C131 1.345(12) .
C130 N107 1.355(9) .
C131 C132 1.381(13) .
C131 H131 0.9500 .
C132 C133 1.401(12) .
C132 H132 0.9500 .
C133 N107 1.385(10) .
C133 C134 1.391(11) .
C134 N108 1.311(10) .
C134 H134 0.9500 .
C135 C142 1.388(9) .
C135 C136 1.402(10) .
C135 N108 1.444(9) .
C136 C137 1.400(10) .
C136 H136 0.9500 .
C137 C140 1.389(11) .
C137 C138 1.522(11) .
C138 H13A 0.9800 .
C138 H13B 0.9800 .
C138 H13C 0.9800 .
C139 C140 1.497(10) .
C139 H13D 0.9800 .
C139 H13E 0.9800 .
C139 H13F 0.9800 .
C140 C141 1.380(10) .
C141 C142 1.384(9) .
C141 H141 0.9500 .
C142 N101 1.432(8) .
C143 N109 1.352(10) .
C143 C144 1.386(11) .
C143 H143 0.9500 .
C144 C145 1.378(13) .
C144 H144 0.9500 .
C145 C146 1.369(13) .
C145 H145 0.9500 .
C146 C147 1.378(12) .
C146 H146 0.9500 .
C147 N109 1.323(10) .
C147 H147 0.9500 .
C200 C201 1.294(18) .
C200 N200 1.390(17) .
C200 H200 0.9500 .
C201 C202 1.261(19) .
C201 H201 0.9500 .
C202 C203 1.19(2) .
C202 H202 0.9500 .
C203 C204 1.42(2) .
C203 H203 0.9500 .
C204 N200 1.37(2) .
C204 H204 0.9500 .
N110 C152 1.30(3) .
N110 C148 1.37(3) .
N110 Dy2 2.47(2) .
C148 C149 1.37(2) .
C148 H148 0.9500 .
C149 C150 1.36(3) .
C149 H149 0.9500 .
C150 C151 1.32(3) .
C150 H150 0.9500 .
C152 C151 1.41(3) .
C152 H152 0.9500 .
C151 H151 0.9500 .
N111 C153 1.27(3) .
N111 C157 1.34(3) .
N111 Dy2 2.46(2) .
C153 C154 1.44(3) .
C153 H153 0.9500 .
C154 C155 1.38(3) .
C154 H154 0.9500 .
C155 C156 1.40(3) .
C155 H155 0.9500 .
C156 C157 1.35(2) .
C156 H156 0.9500 .
C157 H157 0.9500 .
N1 U1 2.573(5) .
N2 U1 2.470(6) .
N3 U1 2.438(6) .
N4 U1 2.590(6) .
N5 Dy1 2.517(6) .
N6 Dy1 2.365(7) .
N7 Dy1 2.371(6) .
N8 Dy1 2.590(6) .
N9 Dy1 2.450(7) .
N10 Dy1 2.533(7) .
N101 U2 2.555(6) .
N102 U2 2.474(6) .
N103 U2 2.490(5) .
N104 U2 2.586(6) .
N105 Dy2 2.554(6) .
N106 Dy2 2.386(6) .
N107 Dy2 2.389(7) .
N108 Dy2 2.559(6) .
N109 Dy2 2.463(6) .
O1 U1 1.901(4) .
O1 Dy1 2.179(4) .
O2 U1 1.942(4) .
O2 U1 2.330(5) 3_557
O3 U2 1.905(5) .
O3 Dy2 2.198(5) .
O4 U2 1.944(4) .
O4 U2 2.354(4) 3_676
U1 O2 2.330(5) 3_557
U1 U1 3.4587(9) 3_557
U2 O4 2.354(4) 3_676
U2 U2 3.4798(6) 3_676
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N1 C1 C2 C3 -178.3(8) . .
N1 C1 C2 N2 8.8(11) . .
N2 C2 C3 C4 -1.9(9) . .
C1 C2 C3 C4 -175.0(8) . .
C2 C3 C4 C5 1.1(9) . .
C3 C4 C5 N2 0.0(9) . .
C3 C4 C5 C6 -180.0(8) . .
N2 C5 C6 C8 175.6(7) . .
C4 C5 C6 C8 -4.4(12) . .
N2 C5 C6 C9 55.0(10) . .
C4 C5 C6 C9 -125.1(8) . .
N2 C5 C6 C7 -64.2(9) . .
C4 C5 C6 C7 115.8(9) . .
C5 C6 C9 N3 -59.7(9) . .
C8 C6 C9 N3 179.3(7) . .
C7 C6 C9 N3 59.2(9) . .
C5 C6 C9 C10 119.3(9) . .
C8 C6 C9 C10 -1.7(12) . .
C7 C6 C9 C10 -121.9(9) . .
N3 C9 C10 C11 0.3(9) . .
C6 C9 C10 C11 -178.7(7) . .
C9 C10 C11 C12 -1.1(9) . .
C10 C11 C12 N3 1.4(9) . .
C10 C11 C12 C13 176.2(8) . .
N3 C12 C13 N4 -3.6(11) . .
C11 C12 C13 N4 -177.9(8) . .
C21 C14 C15 C16 2.3(12) . .
N4 C14 C15 C16 -179.7(7) . .
C14 C15 C16 C19 -1.5(12) . .
C14 C15 C16 C17 179.6(8) . .
C15 C16 C19 C20 0.8(12) . .
C17 C16 C19 C20 179.8(8) . .
C15 C16 C19 C18 -175.1(8) . .
C17 C16 C19 C18 3.9(13) . .
C16 C19 C20 C21 -1.0(13) . .
C18 C19 C20 C21 175.0(8) . .
C15 C14 C21 C20 -2.3(11) . .
N4 C14 C21 C20 179.8(7) . .
C15 C14 C21 N5 172.3(7) . .
N4 C14 C21 N5 -5.7(11) . .
C19 C20 C21 C14 1.8(12) . .
C19 C20 C21 N5 -173.2(7) . .
N5 C22 C23 C24 166.8(9) . .
N5 C22 C23 N6 -12.2(12) . .
N6 C23 C24 C25 0.2(12) . .
C22 C23 C24 C25 -178.9(9) . .
C23 C24 C25 C26 -0.1(13) . .
C24 C25 C26 N6 0.0(12) . .
C24 C25 C26 C27 -178.7(9) . .
N6 C26 C27 C30 -13.0(13) . .
C25 C26 C27 C30 165.5(9) . .
N6 C26 C27 C28 -135.5(9) . .
C25 C26 C27 C28 43.0(14) . .
N6 C26 C27 C29 107.1(10) . .
C25 C26 C27 C29 -74.4(12) . .
C26 C27 C30 N7 38.9(12) . .
C28 C27 C30 N7 161.6(8) . .
C29 C27 C30 N7 -82.1(11) . .
C26 C27 C30 C31 -146.0(9) . .
C28 C27 C30 C31 -23.3(13) . .
C29 C27 C30 C31 93.0(11) . .
N7 C30 C31 C32 -0.8(11) . .
C27 C30 C31 C32 -176.5(9) . .
C30 C31 C32 C33 -0.1(11) . .
C31 C32 C33 N7 1.0(11) . .
C31 C32 C33 C34 -168.7(9) . .
N7 C33 C34 N8 0.9(13) . .
C32 C33 C34 N8 169.5(9) . .
C42 C35 C36 C37 -1.2(11) . .
N8 C35 C36 C37 174.9(7) . .
C35 C36 C37 C40 0.0(12) . .
C35 C36 C37 C38 -180.0(7) . .
C36 C37 C40 C41 0.2(11) . .
C38 C37 C40 C41 -179.8(7) . .
C36 C37 C40 C39 -178.7(7) . .
C38 C37 C40 C39 1.3(12) . .
C37 C40 C41 C42 0.8(11) . .
C39 C40 C41 C42 179.7(7) . .
C40 C41 C42 C35 -2.0(11) . .
C40 C41 C42 N1 -179.0(6) . .
C36 C35 C42 C41 2.1(10) . .
N8 C35 C42 C41 -173.8(6) . .
C36 C35 C42 N1 179.0(6) . .
N8 C35 C42 N1 3.1(11) . .
N9 C43 C44 C45 0.4(15) . .
C43 C44 C45 C46 0.0(19) . .
C44 C45 C46 C47 0(2) . .
C45 C46 C47 N9 -0.9(19) . .
N10 C48 C49 C50 -1.3(13) . .
C48 C49 C50 C51 -0.7(13) . .
C49 C50 C51 C52 1.5(13) . .
C50 C51 C52 N10 -0.5(14) . .
N101 C101 C102 N102 -4.5(11) . .
N101 C101 C102 C103 176.5(7) . .
N102 C102 C103 C104 -0.8(9) . .
C101 C102 C103 C104 178.3(8) . .
C102 C103 C104 C105 0.6(9) . .
C103 C104 C105 N102 -0.2(9) . .
C103 C104 C105 C106 -178.6(7) . .
N102 C105 C106 C109 -55.1(9) . .
C104 C105 C106 C109 123.2(8) . .
N102 C105 C106 C108 -176.3(7) . .
C104 C105 C106 C108 2.0(11) . .
N102 C105 C106 C107 64.7(9) . .
C104 C105 C106 C107 -116.9(8) . .
C105 C106 C109 N103 54.9(10) . .
C108 C106 C109 N103 176.6(7) . .
C107 C106 C109 N103 -65.7(9) . .
C105 C106 C109 C110 -121.0(9) . .
C108 C106 C109 C110 0.7(13) . .
C107 C106 C109 C110 118.3(9) . .
N103 C109 C110 C111 1.7(10) . .
C106 C109 C110 C111 178.0(8) . .
C109 C110 C111 C112 -0.9(10) . .
C110 C111 C112 N103 -0.3(10) . .
C110 C111 C112 C113 -176.5(8) . .
N103 C112 C113 N104 6.1(12) . .
C111 C112 C113 N104 -178.0(8) . .
C121 C114 C115 C116 -2.7(11) . .
N104 C114 C115 C116 178.3(6) . .
C114 C115 C116 C119 -0.8(11) . .
C114 C115 C116 C117 -179.2(7) . .
C115 C116 C119 C120 3.4(11) . .
C117 C116 C119 C120 -178.2(7) . .
C115 C116 C119 C118 -178.2(7) . .
C117 C116 C119 C118 0.3(11) . .
C116 C119 C120 C121 -2.5(12) . .
C118 C119 C120 C121 179.0(7) . .
C115 C114 C121 C120 3.5(10) . .
N104 C114 C121 C120 -177.5(7) . .
C115 C114 C121 N105 -170.3(7) . .
N104 C114 C121 N105 8.7(11) . .
C119 C120 C121 C114 -0.9(11) . .
C119 C120 C121 N105 173.1(7) . .
N105 C122 C123 N106 3.4(12) . .
N105 C122 C123 C124 -177.2(8) . .
N106 C123 C124 C125 -0.7(10) . .
C122 C123 C124 C125 179.9(8) . .
C123 C124 C125 C126 1.5(10) . .
C124 C125 C126 N106 -1.8(10) . .
C124 C125 C126 C127 -176.3(8) . .
N106 C126 C127 C130 31.9(12) . .
C125 C126 C127 C130 -154.5(8) . .
N106 C126 C127 C129 -88.9(10) . .
C125 C126 C127 C129 84.8(10) . .
N106 C126 C127 C128 152.2(8) . .
C125 C126 C127 C128 -34.1(12) . .
C126 C127 C130 C131 151.9(9) . .
C129 C127 C130 C131 -86.9(12) . .
C128 C127 C130 C131 29.1(12) . .
C126 C127 C130 N107 -34.6(11) . .
C129 C127 C130 N107 86.5(10) . .
C128 C127 C130 N107 -157.5(7) . .
N107 C130 C131 C132 1.0(12) . .
C127 C130 C131 C132 175.0(8) . .
C130 C131 C132 C133 -1.2(12) . .
C131 C132 C133 N107 1.0(11) . .
C131 C132 C133 C134 176.1(9) . .
N107 C133 C134 N108 -5.8(13) . .
C132 C133 C134 N108 179.6(8) . .
C142 C135 C136 C137 -0.2(11) . .
N108 C135 C136 C137 -177.2(7) . .
C135 C136 C137 C140 0.3(12) . .
C135 C136 C137 C138 179.6(8) . .
C136 C137 C140 C141 1.7(12) . .
C138 C137 C140 C141 -177.6(9) . .
C136 C137 C140 C139 178.3(8) . .
C138 C137 C140 C139 -1.0(13) . .
C137 C140 C141 C142 -4.0(12) . .
C139 C140 C141 C142 179.4(7) . .
C140 C141 C142 C135 4.2(11) . .
C140 C141 C142 N101 -177.2(7) . .
C136 C135 C142 C141 -2.0(11) . .
N108 C135 C142 C141 174.7(7) . .
C136 C135 C142 N101 179.4(7) . .
N108 C135 C142 N101 -3.9(11) . .
N109 C143 C144 C145 0.5(14) . .
C143 C144 C145 C146 -1.8(15) . .
C144 C145 C146 C147 2.1(16) . .
C145 C146 C147 N109 -1.0(16) . .
N200 C200 C201 C202 -2(4) . .
C200 C201 C202 C203 2(5) . .
C201 C202 C203 C204 -2(4) . .
C202 C203 C204 N200 1(4) . .
C152 N110 C148 C149 1(4) . .
Dy2 N110 C148 C149 -171.8(16) . .
N110 C148 C149 C150 -1(3) . .
C148 C149 C150 C151 4(4) . .
C148 N110 C152 C151 -4(4) . .
Dy2 N110 C152 C151 169.1(19) . .
C149 C150 C151 C152 -7(4) . .
N110 C152 C151 C150 7(4) . .
C157 N111 C153 C154 -2(4) . .
Dy2 N111 C153 C154 -168(2) . .
N111 C153 C154 C155 6(4) . .
C153 C154 C155 C156 -9(3) . .
C154 C155 C156 C157 10(3) . .
C153 N111 C157 C156 3(3) . .
Dy2 N111 C157 C156 167.6(15) . .
C155 C156 C157 N111 -7(3) . .
C2 C1 N1 C42 -170.0(7) . .
C2 C1 N1 U1 -20.3(9) . .
C41 C42 N1 C1 -125.8(8) . .
C35 C42 N1 C1 57.3(10) . .
C41 C42 N1 U1 86.4(7) . .
C35 C42 N1 U1 -90.4(7) . .
C4 C5 N2 C2 -1.2(8) . .
C6 C5 N2 C2 178.8(7) . .
C4 C5 N2 U1 163.4(5) . .
C6 C5 N2 U1 -16.6(11) . .
C3 C2 N2 C5 1.9(8) . .
C1 C2 N2 C5 176.3(7) . .
C3 C2 N2 U1 -165.8(5) . .
C1 C2 N2 U1 8.5(9) . .
C10 C9 N3 C12 0.6(8) . .
C6 C9 N3 C12 179.7(7) . .
C10 C9 N3 U1 -154.0(5) . .
C6 C9 N3 U1 25.2(11) . .
C11 C12 N3 C9 -1.2(8) . .
C13 C12 N3 C9 -176.7(7) . .
C11 C12 N3 U1 159.4(5) . .
C13 C12 N3 U1 -16.0(9) . .
C12 C13 N4 C14 167.1(7) . .
C12 C13 N4 U1 19.5(9) . .
C21 C14 N4 C13 -51.0(10) . .
C15 C14 N4 C13 131.0(8) . .
C21 C14 N4 U1 92.5(8) . .
C15 C14 N4 U1 -85.5(8) . .
C23 C22 N5 C21 164.1(7) . .
C23 C22 N5 Dy1 0.2(10) . .
C14 C21 N5 C22 129.7(8) . .
C20 C21 N5 C22 -55.7(10) . .
C14 C21 N5 Dy1 -69.7(9) . .
C20 C21 N5 Dy1 104.9(7) . .
C25 C26 N6 C23 0.2(10) . .
C27 C26 N6 C23 178.9(8) . .
C25 C26 N6 Dy1 155.2(7) . .
C27 C26 N6 Dy1 -26.1(13) . .
C24 C23 N6 C26 -0.2(10) . .
C22 C23 N6 C26 179.0(7) . .
C24 C23 N6 Dy1 -161.4(7) . .
C22 C23 N6 Dy1 17.8(9) . .
C31 C30 N7 C33 1.4(10) . .
C27 C30 N7 C33 177.3(8) . .
C31 C30 N7 Dy1 155.2(6) . .
C27 C30 N7 Dy1 -29.0(12) . .
C32 C33 N7 C30 -1.5(10) . .
C34 C33 N7 C30 168.9(8) . .
C32 C33 N7 Dy1 -161.4(6) . .
C34 C33 N7 Dy1 9.0(10) . .
C33 C34 N8 C35 -163.9(7) . .
C33 C34 N8 Dy1 -9.1(10) . .
C36 C35 N8 C34 45.0(9) . .
C42 C35 N8 C34 -139.1(7) . .
C36 C35 N8 Dy1 -103.6(7) . .
C42 C35 N8 Dy1 72.3(8) . .
C46 C47 N9 C43 1.3(14) . .
C46 C47 N9 Dy1 -176.9(8) . .
C44 C43 N9 C47 -1.0(13) . .
C44 C43 N9 Dy1 177.2(7) . .
C51 C52 N10 C48 -1.4(13) . .
C51 C52 N10 Dy1 168.3(7) . .
C49 C48 N10 C52 2.2(12) . .
C49 C48 N10 Dy1 -168.3(6) . .
C102 C101 N101 C142 170.9(6) . .
C102 C101 N101 U2 19.0(8) . .
C141 C142 N101 C101 124.1(7) . .
C135 C142 N101 C101 -57.3(9) . .
C141 C142 N101 U2 -87.1(7) . .
C135 C142 N101 U2 91.5(7) . .
C104 C105 N102 C102 -0.3(8) . .
C106 C105 N102 C102 178.3(7) . .
C104 C105 N102 U2 -160.6(5) . .
C106 C105 N102 U2 18.0(11) . .
C103 C102 N102 C105 0.7(8) . .
C101 C102 N102 C105 -178.5(6) . .
C103 C102 N102 U2 166.0(5) . .
C101 C102 N102 U2 -13.2(8) . .
C110 C109 N103 C112 -1.9(9) . .
C106 C109 N103 C112 -178.5(7) . .
C110 C109 N103 U2 159.1(6) . .
C106 C109 N103 U2 -17.6(12) . .
C111 C112 N103 C109 1.4(9) . .
C113 C112 N103 C109 178.0(7) . .
C111 C112 N103 U2 -164.0(5) . .
C113 C112 N103 U2 12.7(9) . .
C112 C113 N104 C114 -169.1(7) . .
C112 C113 N104 U2 -20.5(9) . .
C115 C114 N104 C113 -129.4(7) . .
C121 C114 N104 C113 51.7(10) . .
C115 C114 N104 U2 84.7(7) . .
C121 C114 N104 U2 -94.3(7) . .
C123 C122 N105 C121 -162.9(7) . .
C123 C122 N105 Dy2 -2.8(9) . .
C114 C121 N105 C122 -135.5(8) . .
C120 C121 N105 C122 50.8(10) . .
C114 C121 N105 Dy2 68.2(9) . .
C120 C121 N105 Dy2 -105.5(7) . .
C125 C126 N106 C123 1.4(9) . .
C127 C126 N106 C123 175.8(8) . .
C125 C126 N106 Dy2 -177.3(6) . .
C127 C126 N106 Dy2 -2.8(13) . .
C124 C123 N106 C126 -0.5(9) . .
C122 C123 N106 C126 179.1(7) . .
C124 C123 N106 Dy2 178.5(5) . .
C122 C123 N106 Dy2 -1.9(9) . .
C131 C130 N107 C133 -0.4(10) . .
C127 C130 N107 C133 -174.8(7) . .
C131 C130 N107 Dy2 -175.5(7) . .
C127 C130 N107 Dy2 10.1(13) . .
C134 C133 N107 C130 -175.9(7) . .
C132 C133 N107 C130 -0.4(9) . .
C134 C133 N107 Dy2 0.6(10) . .
C132 C133 N107 Dy2 176.1(5) . .
C133 C134 N108 C135 166.9(7) . .
C133 C134 N108 Dy2 7.1(9) . .
C142 C135 N108 C134 135.9(8) . .
C136 C135 N108 C134 -47.3(9) . .
C142 C135 N108 Dy2 -68.6(9) . .
C136 C135 N108 Dy2 108.2(7) . .
C146 C147 N109 C143 -0.3(13) . .
C146 C147 N109 Dy2 170.9(7) . .
C144 C143 N109 C147 0.6(12) . .
C144 C143 N109 Dy2 -170.3(6) . .
C203 C204 N200 C200 -1(3) . .
C201 C200 N200 C204 2(3) . .
U1 O1 Dy1 N6 4(7) . .
U1 O1 Dy1 N7 -139(6) . .
U1 O1 Dy1 N9 113(6) . .
U1 O1 Dy1 N5 41(6) . .
U1 O1 Dy1 N10 -58(6) . .
U1 O1 Dy1 N8 -179(100) . .
C26 N6 Dy1 O1 -126.4(8) . .
C23 N6 Dy1 O1 26.8(7) . .
C26 N6 Dy1 N7 29.0(8) . .
C23 N6 Dy1 N7 -177.8(6) . .
C26 N6 Dy1 N9 120.1(8) . .
C23 N6 Dy1 N9 -86.7(6) . .
C26 N6 Dy1 N5 -165.6(9) . .
C23 N6 Dy1 N5 -12.4(5) . .
C26 N6 Dy1 N10 -63.9(8) . .
C23 N6 Dy1 N10 89.3(6) . .
C26 N6 Dy1 N8 57.0(9) . .
C23 N6 Dy1 N8 -149.8(5) . .
C30 N7 Dy1 O1 157.2(7) . .
C33 N7 Dy1 O1 -50.3(7) . .
C30 N7 Dy1 N6 -1.1(7) . .
C33 N7 Dy1 N6 151.4(6) . .
C30 N7 Dy1 N9 -90.5(8) . .
C33 N7 Dy1 N9 62.0(5) . .
C30 N7 Dy1 N5 -22.5(9) . .
C33 N7 Dy1 N5 130.0(5) . .
C30 N7 Dy1 N10 77.7(8) . .
C33 N7 Dy1 N10 -129.8(5) . .
C30 N7 Dy1 N8 -161.6(8) . .
C33 N7 Dy1 N8 -9.2(5) . .
C47 N9 Dy1 O1 173.1(6) . .
C43 N9 Dy1 O1 -4.9(7) . .
C47 N9 Dy1 N6 -40.4(7) . .
C43 N9 Dy1 N6 141.5(7) . .
C47 N9 Dy1 N7 32.0(7) . .
C43 N9 Dy1 N7 -146.1(7) . .
C47 N9 Dy1 N5 -109.6(7) . .
C43 N9 Dy1 N5 72.3(7) . .
C47 N9 Dy1 N10 -60.0(14) . .
C43 N9 Dy1 N10 121.9(11) . .
C47 N9 Dy1 N8 101.0(7) . .
C43 N9 Dy1 N8 -77.1(7) . .
C22 N5 Dy1 O1 -151.7(5) . .
C21 N5 Dy1 O1 46.7(5) . .
C22 N5 Dy1 N6 6.4(5) . .
C21 N5 Dy1 N6 -155.2(6) . .
C22 N5 Dy1 N7 28.1(7) . .
C21 N5 Dy1 N7 -133.5(6) . .
C22 N5 Dy1 N9 101.6(6) . .
C21 N5 Dy1 N9 -59.9(6) . .
C22 N5 Dy1 N10 -69.3(5) . .
C21 N5 Dy1 N10 129.1(6) . .
C22 N5 Dy1 N8 145.9(5) . .
C21 N5 Dy1 N8 -15.7(7) . .
C52 N10 Dy1 O1 127.0(7) . .
C48 N10 Dy1 O1 -63.4(6) . .
C52 N10 Dy1 N6 -21.5(7) . .
C48 N10 Dy1 N6 148.1(6) . .
C52 N10 Dy1 N7 -93.7(7) . .
C48 N10 Dy1 N7 76.0(6) . .
C52 N10 Dy1 N9 -1.6(15) . .
C48 N10 Dy1 N9 168.1(10) . .
C52 N10 Dy1 N5 46.3(7) . .
C48 N10 Dy1 N5 -144.0(6) . .
C52 N10 Dy1 N8 -160.8(6) . .
C48 N10 Dy1 N8 8.8(6) . .
C34 N8 Dy1 O1 163.2(5) . .
C35 N8 Dy1 O1 -46.6(6) . .
C34 N8 Dy1 N6 -18.9(7) . .
C35 N8 Dy1 N6 131.4(6) . .
C34 N8 Dy1 N7 9.5(5) . .
C35 N8 Dy1 N7 159.7(6) . .
C34 N8 Dy1 N9 -88.0(5) . .
C35 N8 Dy1 N9 62.2(6) . .
C34 N8 Dy1 N5 -133.0(5) . .
C35 N8 Dy1 N5 17.2(7) . .
C34 N8 Dy1 N10 87.6(5) . .
C35 N8 Dy1 N10 -122.2(6) . .
U2 O3 Dy2 N106 141(17) . .
U2 O3 Dy2 N107 -86(17) . .
U2 O3 Dy2 N111 -145(17) . .
U2 O3 Dy2 N109 26(17) . .
U2 O3 Dy2 N110 -160(17) . .
U2 O3 Dy2 N105 100(17) . .
U2 O3 Dy2 N108 -44(17) . .
C126 N106 Dy2 O3 135.4(7) . .
C123 N106 Dy2 O3 -43.2(7) . .
C126 N106 Dy2 N107 -15.3(8) . .
C123 N106 Dy2 N107 166.2(6) . .
C126 N106 Dy2 N111 65.1(9) . .
C123 N106 Dy2 N111 -113.4(8) . .
C126 N106 Dy2 N109 -107.7(8) . .
C123 N106 Dy2 N109 73.8(6) . .
C126 N106 Dy2 N110 76.0(9) . .
C123 N106 Dy2 N110 -102.6(7) . .
C126 N106 Dy2 N105 179.0(8) . .
C123 N106 Dy2 N105 0.4(5) . .
C126 N106 Dy2 N108 -36.3(9) . .
C123 N106 Dy2 N108 145.1(5) . .
C130 N107 Dy2 O3 -138.9(7) . .
C133 N107 Dy2 O3 46.2(7) . .
C130 N107 Dy2 N106 11.4(8) . .
C133 N107 Dy2 N106 -163.4(6) . .
C130 N107 Dy2 N111 -80.4(9) . .
C133 N107 Dy2 N111 104.8(7) . .
C130 N107 Dy2 N109 106.9(8) . .
C133 N107 Dy2 N109 -68.0(5) . .
C130 N107 Dy2 N110 -67.1(9) . .
C133 N107 Dy2 N110 118.0(7) . .
C130 N107 Dy2 N105 31.8(9) . .
C133 N107 Dy2 N105 -143.1(5) . .
C130 N107 Dy2 N108 176.9(8) . .
C133 N107 Dy2 N108 2.1(5) . .
C153 N111 Dy2 O3 -78.2(18) . .
C157 N111 Dy2 O3 117.1(18) . .
C153 N111 Dy2 N106 63.7(18) . .
C157 N111 Dy2 N106 -101.0(17) . .
C153 N111 Dy2 N107 135.5(18) . .
C157 N111 Dy2 N107 -29.2(17) . .
C153 N111 Dy2 N109 -170(3) . .
C157 N111 Dy2 N109 25(5) . .
C153 N111 Dy2 N110 18(3) . .
C157 N111 Dy2 N110 -147(5) . .
C153 N111 Dy2 N105 -3.3(19) . .
C157 N111 Dy2 N105 -168.0(16) . .
C153 N111 Dy2 N108 -156.7(17) . .
C157 N111 Dy2 N108 38.6(18) . .
C147 N109 Dy2 O3 -167.6(6) . .
C143 N109 Dy2 O3 3.5(6) . .
C147 N109 Dy2 N106 48.3(6) . .
C143 N109 Dy2 N106 -140.7(6) . .
C147 N109 Dy2 N107 -23.9(6) . .
C143 N109 Dy2 N107 147.1(6) . .
C147 N109 Dy2 N111 -78(3) . .
C143 N109 Dy2 N111 93(3) . .
C147 N109 Dy2 N110 83(5) . .
C143 N109 Dy2 N110 -106(5) . .
C147 N109 Dy2 N105 115.1(6) . .
C143 N109 Dy2 N105 -73.8(6) . .
C147 N109 Dy2 N108 -91.3(6) . .
C143 N109 Dy2 N108 79.7(6) . .
C152 N110 Dy2 O3 67.2(19) . .
C148 N110 Dy2 O3 -120.6(19) . .
C152 N110 Dy2 N106 -147(2) . .
C148 N110 Dy2 N106 25.3(18) . .
C152 N110 Dy2 N107 -75(2) . .
C148 N110 Dy2 N107 97.2(19) . .
C152 N110 Dy2 N111 -14(3) . .
C148 N110 Dy2 N111 158(5) . .
C152 N110 Dy2 N109 178(4) . .
C148 N110 Dy2 N109 -10(7) . .
C152 N110 Dy2 N105 146.2(19) . .
C148 N110 Dy2 N105 -42(2) . .
C152 N110 Dy2 N108 -8(2) . .
C148 N110 Dy2 N108 164.1(17) . .
C122 N105 Dy2 O3 154.5(5) . .
C121 N105 Dy2 O3 -48.2(6) . .
C122 N105 Dy2 N106 1.2(5) . .
C121 N105 Dy2 N106 158.5(6) . .
C122 N105 Dy2 N107 -19.5(7) . .
C121 N105 Dy2 N107 137.8(6) . .
C122 N105 Dy2 N111 81.0(7) . .
C121 N105 Dy2 N111 -121.7(8) . .
C122 N105 Dy2 N109 -101.1(5) . .
C121 N105 Dy2 N109 56.2(6) . .
C122 N105 Dy2 N110 75.6(7) . .
C121 N105 Dy2 N110 -127.1(8) . .
C122 N105 Dy2 N108 -142.7(5) . .
C121 N105 Dy2 N108 14.6(8) . .
C134 N108 Dy2 O3 -158.0(5) . .
C135 N108 Dy2 O3 45.4(6) . .
C134 N108 Dy2 N106 16.6(7) . .
C135 N108 Dy2 N106 -140.0(6) . .
C134 N108 Dy2 N107 -4.7(5) . .
C135 N108 Dy2 N107 -161.3(6) . .
C134 N108 Dy2 N111 -81.3(7) . .
C135 N108 Dy2 N111 122.2(8) . .
C134 N108 Dy2 N109 96.6(5) . .
C135 N108 Dy2 N109 -59.9(6) . .
C134 N108 Dy2 N110 -82.7(8) . .
C135 N108 Dy2 N110 120.7(8) . .
C134 N108 Dy2 N105 139.2(5) . .
C135 N108 Dy2 N105 -17.3(7) . .
Dy1 O1 U1 O2 -112(6) . .
Dy1 O1 U1 O2 -111(6) . 3_557
Dy1 O1 U1 N3 33(6) . .
Dy1 O1 U1 N2 105(6) . .
Dy1 O1 U1 N1 169(6) . .
Dy1 O1 U1 N4 -33(6) . .
Dy1 O1 U1 U1 -111(6) . 3_557
U1 O2 U1 O1 2(2) 3_557 .
U1 O2 U1 O2 0.0 3_557 3_557
U1 O2 U1 N3 -143.8(2) 3_557 .
U1 O2 U1 N2 144.5(2) 3_557 .
U1 O2 U1 N1 78.7(2) 3_557 .
U1 O2 U1 N4 -76.0(2) 3_557 .
C9 N3 U1 O1 97.6(7) . .
C12 N3 U1 O1 -55.4(5) . .
C9 N3 U1 O2 -85.2(7) . .
C12 N3 U1 O2 121.9(5) . .
C9 N3 U1 O2 -151.3(6) . 3_557
C12 N3 U1 O2 55.8(6) . 3_557
C9 N3 U1 N2 8.3(7) . .
C12 N3 U1 N2 -144.6(5) . .
C9 N3 U1 N1 30.0(8) . .
C12 N3 U1 N1 -122.9(5) . .
C9 N3 U1 N4 170.5(8) . .
C12 N3 U1 N4 17.5(5) . .
C9 N3 U1 U1 -112.7(7) . 3_557
C12 N3 U1 U1 94.4(5) . 3_557
C5 N2 U1 O1 -102.9(7) . .
C2 N2 U1 O1 60.1(5) . .
C5 N2 U1 O2 80.0(7) . .
C2 N2 U1 O2 -117.0(5) . .
C5 N2 U1 O2 146.4(6) . 3_557
C2 N2 U1 O2 -50.6(6) . 3_557
C5 N2 U1 N3 -12.7(6) . .
C2 N2 U1 N3 150.2(6) . .
C5 N2 U1 N1 -175.7(7) . .
C2 N2 U1 N1 -12.8(5) . .
C5 N2 U1 N4 -36.5(8) . .
C2 N2 U1 N4 126.4(5) . .
C5 N2 U1 U1 107.3(7) . 3_557
C2 N2 U1 U1 -89.8(5) . 3_557
C1 N1 U1 O1 -80.1(5) . .
C42 N1 U1 O1 69.0(5) . .
C1 N1 U1 O2 104.9(5) . .
C42 N1 U1 O2 -106.1(5) . .
C1 N1 U1 O2 174.7(5) . 3_557
C42 N1 U1 O2 -36.2(5) . 3_557
C1 N1 U1 N3 -6.1(6) . .
C42 N1 U1 N3 143.0(5) . .
C1 N1 U1 N2 16.6(5) . .
C42 N1 U1 N2 165.6(6) . .
C1 N1 U1 N4 -116.4(5) . .
C42 N1 U1 N4 32.6(7) . .
C1 N1 U1 U1 144.0(5) . 3_557
C42 N1 U1 U1 -67.0(5) . 3_557
C13 N4 U1 O1 77.4(5) . .
C14 N4 U1 O1 -67.7(6) . .
C13 N4 U1 O2 -107.5(5) . .
C14 N4 U1 O2 107.4(6) . .
C13 N4 U1 O2 -176.6(5) . 3_557
C14 N4 U1 O2 38.3(6) . 3_557
C13 N4 U1 N3 -19.2(5) . .
C14 N4 U1 N3 -164.3(6) . .
C13 N4 U1 N2 5.2(6) . .
C14 N4 U1 N2 -139.9(6) . .
C13 N4 U1 N1 113.7(5) . .
C14 N4 U1 N1 -31.3(7) . .
C13 N4 U1 U1 -146.1(5) . 3_557
C14 N4 U1 U1 68.8(6) . 3_557
Dy2 O3 U2 O4 -18(18) . .
Dy2 O3 U2 O4 -27(17) . 3_676
Dy2 O3 U2 N102 118(17) . .
Dy2 O3 U2 N103 -172(100) . .
Dy2 O3 U2 N101 52(17) . .
Dy2 O3 U2 N104 -107(17) . .
Dy2 O3 U2 U2 -26(17) . 3_676
U2 O4 U2 O3 -9.3(18) 3_676 .
U2 O4 U2 O4 0.0 3_676 3_676
U2 O4 U2 N102 -144.8(2) 3_676 .
U2 O4 U2 N103 144.8(2) 3_676 .
U2 O4 U2 N101 -77.7(2) 3_676 .
U2 O4 U2 N104 78.1(2) 3_676 .
C105 N102 U2 O3 102.4(7) . .
C102 N102 U2 O3 -56.7(5) . .
C105 N102 U2 O4 -82.3(7) . .
C102 N102 U2 O4 118.6(5) . .
C105 N102 U2 O4 -147.6(6) . 3_676
C102 N102 U2 O4 53.3(6) . 3_676
C105 N102 U2 N103 12.5(7) . .
C102 N102 U2 N103 -146.6(5) . .
C105 N102 U2 N101 174.5(8) . .
C102 N102 U2 N101 15.4(4) . .
C105 N102 U2 N104 34.4(8) . .
C102 N102 U2 N104 -124.7(5) . .
C105 N102 U2 U2 -109.3(7) . 3_676
C102 N102 U2 U2 91.6(5) . 3_676
C109 N103 U2 O3 -103.5(7) . .
C112 N103 U2 O3 56.0(5) . .
C109 N103 U2 O4 79.4(7) . .
C112 N103 U2 O4 -121.1(5) . .
C109 N103 U2 O4 147.1(6) . 3_676
C112 N103 U2 O4 -53.3(7) . 3_676
C109 N103 U2 N102 -12.6(7) . .
C112 N103 U2 N102 147.0(6) . .
C109 N103 U2 N101 -35.7(8) . .
C112 N103 U2 N101 123.9(5) . .
C109 N103 U2 N104 -175.2(8) . .
C112 N103 U2 N104 -15.7(5) . .
C109 N103 U2 U2 107.0(7) . 3_676
C112 N103 U2 U2 -93.4(5) . 3_676
C101 N101 U2 O3 80.3(5) . .
C142 N101 U2 O3 -69.3(5) . .
C101 N101 U2 O4 -106.1(5) . .
C142 N101 U2 O4 104.3(5) . .
C101 N101 U2 O4 -175.8(5) . 3_676
C142 N101 U2 O4 34.6(5) . 3_676
C101 N101 U2 N102 -17.8(5) . .
C142 N101 U2 N102 -167.4(6) . .
C101 N101 U2 N103 5.8(6) . .
C142 N101 U2 N103 -143.8(5) . .
C101 N101 U2 N104 113.1(5) . .
C142 N101 U2 N104 -36.5(6) . .
C101 N101 U2 U2 -145.2(5) . 3_676
C142 N101 U2 U2 65.2(5) . 3_676
C113 N104 U2 O3 -79.3(5) . .
C114 N104 U2 O3 67.5(5) . .
C113 N104 U2 O4 107.7(5) . .
C114 N104 U2 O4 -105.5(5) . .
C113 N104 U2 O4 177.2(5) . 3_676
C114 N104 U2 O4 -36.0(5) . 3_676
C113 N104 U2 N102 -4.0(6) . .
C114 N104 U2 N102 142.8(5) . .
C113 N104 U2 N103 18.6(5) . .
C114 N104 U2 N103 165.4(6) . .
C113 N104 U2 N101 -112.1(5) . .
C114 N104 U2 N101 34.7(7) . .
C113 N104 U2 U2 147.0(5) . 3_676
C114 N104 U2 U2 -66.3(5) . 3_676
