#------------------------------------------------------------------------------
#$Date: 2016-03-22 21:19:14 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179017 $
#$URL: svn://www.crystallography.net/cod/cif/4/12/15/4121512.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4121512
loop_
_publ_author_name
'Abe, Yoko'
'Tanaka, Hideyuki'
'Guo, Yunlong'
'Matsuo, Yutaka'
'Nakamura, Eiichi'
_publ_section_title
;
 Mobility of long-lived fullerene radical in solid state and nonlinear
 temperature dependence.
;
_journal_issue                   9
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              3366
_journal_page_last               3369
_journal_paper_doi               10.1021/ja500340f
_journal_volume                  136
_journal_year                    2014
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C79 H30 Cl3 O1 Si1'
_chemical_formula_sum            'C79 H30 Cl3 O Si'
_chemical_formula_weight         1129.47
_chemical_name_systematic
;
 C60CH2SiMe2C6H4EHOdimer_CHCl3
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2012-11-23
_cell_angle_alpha                113.04
_cell_angle_beta                 92.89
_cell_angle_gamma                105.44
_cell_formula_units_Z            2
_cell_length_a                   10.003
_cell_length_b                   15.818
_cell_length_c                   17.837
_cell_measurement_reflns_used    29134
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      68.23
_cell_measurement_theta_min      3.19
_cell_measurement_wavelength     1.5418
_cell_volume                     2465.116
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR2004 (Giacovazzo et al, 2004)'
_diffrn_ambient_temperature      153(2)
_diffrn_measured_fraction_theta_full 0.977
_diffrn_measured_fraction_theta_max 0.977
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0.1082
_diffrn_reflns_av_unetI/netI     0.1251
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            29134
_diffrn_reflns_theta_full        68.23
_diffrn_reflns_theta_max         68.23
_diffrn_reflns_theta_min         3.19
_exptl_absorpt_coefficient_mu    2.362
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.522
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1154
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.591
_refine_diff_density_min         -0.409
_refine_diff_density_rms         0.1
_refine_ls_extinction_coef       0.0043(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.078
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     714
_refine_ls_number_reflns         8808
_refine_ls_number_restraints     13
_refine_ls_restrained_S_all      1.088
_refine_ls_R_factor_all          0.2565
_refine_ls_R_factor_gt           0.1366
_refine_ls_shift/su_max          0.049
_refine_ls_shift/su_mean         0.003
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.2000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3477
_refine_ls_wR_factor_ref         0.4407
_reflns_number_gt                2706
_reflns_number_total             8808
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ja500340f_si_002.cif
_cod_data_source_block           EHOdimer
_cod_original_cell_volume        2465.1
_cod_database_code               4121512
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
O O 0.4124(7) 0.2573(5) 0.2987(5) 0.124(2) Uani 1 1 d . A 1
Si Si 0.4489(2) 0.11239(16) 0.36070(18) 0.1024(10) Uani 1 1 d . A 1
Cl1 Cl -0.2122(3) 0.27696(19) 0.2547(2) 0.1477(12) Uani 1 1 d . B 1
Cl2 Cl 0.0069(3) 0.40951(18) 0.3942(2) 0.1475(12) Uani 1 1 d . B 1
Cl3 Cl -0.0884(3) 0.2060(2) 0.3560(2) 0.1542(13) Uani 1 1 d . B 1
C1 C 0.1461(8) -0.0142(6) 0.3248(5) 0.093(3) Uani 1 1 d . A 1
C2 C 0.1762(8) -0.0721(6) 0.3721(6) 0.093(3) Uani 1 1 d . A 1
C3 C 0.1023(8) -0.0835(5) 0.4306(5) 0.087(2) Uani 1 1 d . A 1
C4 C -0.0188(8) -0.0438(5) 0.4584(5) 0.080(2) Uani 1 1 d . . 1
C5 C -0.0770(8) -0.0245(5) 0.3880(6) 0.089(3) Uani 1 1 d . A 1
C6 C -0.0041(9) -0.0135(5) 0.3273(6) 0.094(3) Uani 1 1 d . A 1
C7 C 0.1608(18) -0.0859(12) 0.2438(11) 0.066(5) Uiso 0.5 1 d P A 1
C8 C 0.2241(14) -0.1603(10) 0.2368(10) 0.048(4) Uiso 0.5 1 d P A 1
C9 C 0.2291(16) -0.1424(11) 0.3212(13) 0.049(5) Uiso 0.5 1 d P A 1
C10 C 0.2111(18) -0.2244(14) 0.3373(13) 0.072(6) Uiso 0.5 1 d P A 1
C11 C 0.1358(19) -0.2420(13) 0.4076(11) 0.083(5) Uiso 0.5 1 d P A 1
C12 C 0.079(3) -0.1684(17) 0.4475(13) 0.083(7) Uiso 0.5 1 d P A 1
C13 C -0.113(2) -0.2079(16) 0.4553(14) 0.073(7) Uiso 0.5 1 d P A 1
C14 C -0.1452(19) -0.1258(11) 0.4457(11) 0.059(5) Uiso 0.5 1 d P A 1
C15 C -0.266(2) -0.1490(13) 0.4116(14) 0.059(5) Uiso 0.5 1 d P A 1
C16 C -0.325(3) -0.1159(18) 0.341(2) 0.119(8) Uiso 0.5 1 d P A 1
C17 C -0.2278(18) -0.0560(11) 0.3408(13) 0.068(5) Uiso 0.5 1 d P A 1
C18 C -0.230(2) -0.0720(13) 0.2615(15) 0.070(6) Uiso 0.5 1 d P A 1
C19 C -0.0984(19) -0.0363(13) 0.2334(12) 0.074(7) Uiso 0.5 1 d P A 1
C20 C -0.058(2) -0.0853(18) 0.1623(17) 0.096(8) Uiso 0.5 1 d P A 1
C21 C 0.0704(19) -0.1148(13) 0.1643(13) 0.082(5) Uiso 0.5 1 d P A 1
C22 C 0.041(4) -0.210(2) 0.0959(19) 0.092(10) Uiso 0.5 1 d P A 1
C23 C 0.129(2) -0.3061(16) 0.1226(15) 0.087(7) Uiso 0.5 1 d P A 1
C24 C 0.1984(18) -0.2450(13) 0.1768(12) 0.072(5) Uiso 0.5 1 d P A 1
C25 C 0.186(2) -0.332(2) 0.216(2) 0.080(7) Uiso 0.5 1 d P A 1
C26 C 0.182(2) -0.3237(18) 0.278(2) 0.081(7) Uiso 0.5 1 d P A 1
C27 C 0.080(2) -0.3931(15) 0.2914(16) 0.090(6) Uiso 0.5 1 d P A 1
C28 C 0.056(3) -0.3435(19) 0.3754(19) 0.094(7) Uiso 0.5 1 d P A 1
C29 C -0.086(4) -0.3687(19) 0.3939(15) 0.104(8) Uiso 0.5 1 d P A 1
C30 C -0.140(2) -0.2932(15) 0.4433(12) 0.090(6) Uiso 0.5 1 d P A 1
C31 C -0.291(3) -0.3306(13) 0.4010(12) 0.071(5) Uiso 0.5 1 d P A 1
C32 C -0.3567(17) -0.2625(17) 0.3946(11) 0.068(5) Uiso 0.5 1 d P A 1
C33 C -0.440(2) -0.2907(14) 0.3289(15) 0.086(6) Uiso 0.5 1 d P A 1
C34 C -0.433(2) -0.2095(19) 0.3142(18) 0.095(8) Uiso 0.5 1 d P A 1
C35 C -0.427(2) -0.1935(15) 0.238(2) 0.076(6) Uiso 0.5 1 d P A 1
C36 C 0.115(3) -0.0775(17) 0.2197(18) 0.103(8) Uiso 0.5 1 d P A 1
C37 C -0.282(3) -0.1998(19) 0.1093(16) 0.115(9) Uiso 0.5 1 d P A 1
C38 C -0.093(2) -0.1564(18) 0.1125(14) 0.099(6) Uiso 0.5 1 d P A 1
C39 C -0.093(3) -0.2398(19) 0.0613(14) 0.106(7) Uiso 0.5 1 d P A 1
C40 C -0.180(3) -0.3414(17) 0.0342(13) 0.084(7) Uiso 0.5 1 d P A 1
C41 C -0.1256(18) -0.4041(12) 0.0332(11) 0.057(6) Uani 0.5 1 d P A 1
C42 C 0.026(2) -0.3736(12) 0.0672(11) 0.067(5) Uiso 0.5 1 d P A 1
C43 C 0.071(2) -0.4155(14) 0.1292(13) 0.084(5) Uiso 0.5 1 d P A 1
C44 C -0.0187(13) -0.4712(8) 0.1355(7) 0.121(3) Uiso 1 1 d . A 1
C45 C -0.024(2) -0.4704(13) 0.2265(13) 0.079(6) Uiso 0.5 1 d P A 1
C46 C -0.1571(10) -0.4973(5) 0.2471(7) 0.103(3) Uani 1 1 d . A 1
C47 C -0.190(2) -0.4520(18) 0.3344(17) 0.089(8) Uiso 0.5 1 d P A 1
C48 C -0.3239(18) -0.4238(12) 0.3319(12) 0.075(5) Uiso 0.5 1 d P A 1
C49 C -0.352(2) -0.4585(15) 0.2793(17) 0.092(6) Uiso 0.5 1 d P A 1
C50 C -0.4735(17) -0.3797(12) 0.2650(12) 0.061(4) Uiso 0.5 1 d P A 1
C51 C -0.4847(8) -0.3915(7) 0.1659(7) 0.107(3) Uani 1 1 d . A 1
C52 C -0.1253(17) -0.1350(13) 0.4696(11) 0.060(5) Uiso 0.5 1 d P A 1
C53 C -0.447(3) -0.3167(18) 0.1219(18) 0.098(8) Uiso 0.5 1 d P A 1
C54 C -0.3447(13) -0.3643(8) 0.0560(8) 0.138(4) Uani 1 1 d . A 1
C55 C -0.3483(9) -0.4500(7) 0.0635(6) 0.109(3) Uani 1 1 d . A 1
C56 C -0.2248(11) -0.4744(6) 0.0545(6) 0.107(3) Uani 1 1 d . A 1
C57 C -0.1699(10) -0.5110(7) 0.1093(8) 0.111(3) Uani 1 1 d . A 1
C58 C -0.2477(12) -0.5244(6) 0.1688(7) 0.105(3) Uani 1 1 d . A 1
C59 C -0.3708(12) -0.5024(6) 0.1804(8) 0.112(4) Uani 1 1 d . A 1
C60 C -0.4218(10) -0.4653(6) 0.1259(8) 0.112(4) Uani 1 1 d . A 1
C61 C 0.2550(7) 0.0911(5) 0.3530(5) 0.096(3) Uani 1 1 d . A 1
H61A H 0.2394 0.1309 0.407 0.115 Uiso 1 1 calc R A 1
H61B H 0.2282 0.1166 0.3153 0.115 Uiso 1 1 calc R A 1
C62 C 0.5174(9) 0.0651(6) 0.4337(6) 0.108(3) Uani 1 1 d . A 1
H62A H 0.6171 0.0771 0.4362 0.163 Uiso 1 1 calc R A 1
H62B H 0.4712 -0.0031 0.4134 0.163 Uiso 1 1 calc R A 1
H62C H 0.4982 0.0976 0.488 0.163 Uiso 1 1 calc R A 1
C63 C 0.5009(9) 0.0591(6) 0.2592(5) 0.113(3) Uani 1 1 d . A 1
H63A H 0.6011 0.0715 0.2664 0.169 Uiso 1 1 calc R A 1
H63B H 0.4742 0.0874 0.2244 0.169 Uiso 1 1 calc R A 1
H63C H 0.4546 -0.0094 0.2338 0.169 Uiso 1 1 calc R A 1
C64 C 0.5282(10) 0.2491(7) 0.4149(8) 0.100(3) Uani 1 1 d . A 1
C65 C 0.5010(10) 0.3070(8) 0.3750(8) 0.111(3) Uani 1 1 d . A 1
C66 C 0.5576(11) 0.4070(7) 0.4111(8) 0.116(3) Uani 1 1 d . A 1
H66 H 0.5391 0.4443 0.3849 0.14 Uiso 1 1 calc R A 1
C67 C 0.6454(10) 0.4498(8) 0.4902(9) 0.125(4) Uani 1 1 d . A 1
H67 H 0.6874 0.5165 0.5155 0.15 Uiso 1 1 calc R A 1
C68 C 0.6694(10) 0.3955(7) 0.5298(7) 0.110(3) Uani 1 1 d . A 1
H68 H 0.723 0.4257 0.5827 0.132 Uiso 1 1 calc R A 1
C69 C 0.6153(9) 0.2972(6) 0.4924(7) 0.101(3) Uani 1 1 d . A 1
H69 H 0.6369 0.2613 0.5192 0.121 Uiso 1 1 calc R A 1
C70 C 0.3722(13) 0.3157(9) 0.2643(7) 0.147(4) Uiso 1 1 d D A 1
H70A H 0.4542 0.3587 0.2567 0.177 Uiso 1 1 calc R A 1
H70B H 0.3204 0.3542 0.2999 0.177 Uiso 1 1 calc R A 1
C71 C 0.2759(14) 0.2421(10) 0.1785(9) 0.176(5) Uani 1 1 d D A 1
H71 H 0.1938 0.2046 0.1922 0.211 Uiso 1 1 calc R A 1
C72 C 0.3284(18) 0.1671(12) 0.1142(10) 0.229(7) Uiso 1 1 d D A 1
H72A H 0.255 0.1293 0.0657 0.275 Uiso 1 1 calc R A 1
H72B H 0.3461 0.1235 0.1366 0.275 Uiso 1 1 calc R A 1
C74 C 0.548(3) 0.1537(18) 0.033(2) 0.227(16) Uiso 0.5 1 d PD A 1
H74A H 0.5074 0.1249 -0.0249 0.273 Uiso 1 1 calc R A 1
H74B H 0.562 0.1044 0.0495 0.273 Uiso 1 1 calc R A 1
C75 C 0.6890(19) 0.2416(14) 0.0561(13) 0.117(6) Uiso 0.5 1 d PD A 1
H75A H 0.76 0.2181 0.0281 0.176 Uiso 1 1 calc R A 1
H75B H 0.7214 0.271 0.1148 0.176 Uiso 1 1 calc R A 1
H75C H 0.6704 0.2885 0.0391 0.176 Uiso 1 1 calc R A 1
C73 C 0.4628(18) 0.2117(14) 0.0879(12) 0.198(8) Uiso 0.75 1 d PD A 1
H73A H 0.4378 0.2489 0.0604 0.238 Uiso 1 1 calc R A 1
H73B H 0.5273 0.258 0.1386 0.238 Uiso 1 1 calc R A 1
C76 C 0.219(3) 0.2933(17) 0.1368(14) 0.193(11) Uiso 0.5 1 d PD A 1
H76A H 0.2894 0.3157 0.1075 0.232 Uiso 1 1 calc R A 1
H76B H 0.137 0.2476 0.0959 0.232 Uiso 1 1 calc R A 1
C77 C 0.181(2) 0.3738(14) 0.1906(13) 0.152(8) Uiso 0.5 1 d PD A 1
H77A H 0.1768 0.4154 0.1637 0.229 Uiso 1 1 calc R A 1
H77B H 0.2494 0.4091 0.2405 0.229 Uiso 1 1 calc R A 1
H77C H 0.09 0.3512 0.2038 0.229 Uiso 1 1 calc R A 1
C78 C -0.1323(10) 0.3048(6) 0.3583(6) 0.120(3) Uani 1 1 d . B 1
H78 H -0.2027 0.3153 0.3943 0.143 Uiso 1 1 calc R B 1
C101 C 0.000(2) -0.4588(14) 0.2649(14) 0.076(6) Uiso 0.5 1 d P A 1
C102 C -0.4925(17) -0.3595(14) 0.2408(14) 0.075(6) Uiso 0.5 1 d P A 1
C103 C 0.185(3) -0.349(2) 0.245(2) 0.117(14) Uiso 0.5 1 d P A 1
C104 C -0.2207(17) -0.0709(11) 0.3767(11) 0.064(4) Uiso 0.5 1 d P A 1
C105 C -0.312(2) -0.0986(15) 0.2863(15) 0.100(6) Uiso 0.5 1 d P A 1
C106 C -0.225(2) -0.4551(13) 0.3070(13) 0.070(6) Uiso 0.5 1 d P A 1
C107 C 0.0331(17) -0.3952(11) 0.0919(12) 0.056(4) Uiso 0.5 1 d P A 1
C108 C 0.189(2) -0.3087(16) 0.3261(17) 0.098(7) Uiso 0.5 1 d P A 1
C109 C -0.437(3) -0.226(2) 0.196(3) 0.102(8) Uiso 0.5 1 d P A 1
C110 C -0.006(4) -0.225(3) 0.081(2) 0.113(13) Uiso 0.5 1 d P A 1
C111 C -0.418(2) -0.4006(16) 0.3020(15) 0.102(6) Uiso 0.5 1 d P A 1
C112 C -0.307(3) -0.1299(16) 0.3822(18) 0.095(7) Uiso 0.5 1 d P A 1
C113 C -0.469(2) -0.3184(17) 0.1524(15) 0.083(7) Uiso 0.5 1 d P A 1
C114 C 0.119(3) -0.169(2) 0.4285(16) 0.106(9) Uiso 0.5 1 d P A 1
C115 C -0.191(2) -0.1779(10) 0.1009(9) 0.065(4) Uiso 0.5 1 d P A 1
C116 C -0.0892(18) -0.0450(11) 0.2603(12) 0.053(5) Uiso 0.5 1 d P A 1
C117 C 0.170(3) -0.339(2) 0.175(2) 0.130(12) Uiso 0.5 1 d P A 1
C118 C -0.128(3) -0.322(2) 0.0345(16) 0.111(10) Uiso 0.5 1 d P A 1
C119 C -0.024(2) -0.0818(13) 0.1912(13) 0.077(6) Uiso 0.5 1 d P A 1
C120 C -0.313(2) -0.1734(15) 0.1390(16) 0.078(5) Uiso 0.5 1 d P A 1
C121 C 0.2112(18) -0.2778(17) 0.1973(12) 0.074(5) Uiso 0.5 1 d P A 1
C122 C -0.213(3) -0.3017(16) 0.4212(13) 0.088(6) Uiso 0.5 1 d P A 1
C123 C 0.070(2) -0.3780(18) 0.337(2) 0.085(6) Uiso 0.5 1 d P A 1
C124 C -0.423(5) -0.223(4) 0.160(3) 0.20(2) Uiso 0.5 1 d P A 1
C125 C -0.4344(17) -0.2044(13) 0.2750(19) 0.067(5) Uiso 0.5 1 d P A 1
C126 C -0.345(2) -0.3094(18) 0.3839(12) 0.079(6) Uiso 0.5 1 d P A 1
C127 C -0.4610(18) -0.2686(17) 0.2980(13) 0.081(5) Uiso 0.5 1 d P A 1
C128 C 0.029(3) -0.2268(18) 0.4490(13) 0.116(7) Uiso 0.5 1 d P A 1
C129 C -0.163(3) -0.381(2) 0.3846(17) 0.119(9) Uiso 0.5 1 d P A 1
C130 C -0.374(2) -0.2263(15) 0.3768(13) 0.083(5) Uiso 0.5 1 d P A 1
C131 C 0.105(3) -0.224(2) 0.1139(14) 0.093(7) Uiso 0.5 1 d P A 1
C132 C 0.069(2) -0.4394(13) 0.1980(13) 0.093(5) Uiso 0.5 1 d P A 1
C133 C -0.006(4) -0.342(2) 0.4000(16) 0.112(8) Uiso 0.5 1 d P A 1
C134 C -0.264(3) -0.3053(18) 0.0445(13) 0.113(6) Uiso 0.5 1 d P A 1
C135 C 0.240(2) -0.1529(18) 0.3432(13) 0.079(7) Uiso 0.5 1 d P A 1
C136 C 0.2385(17) -0.1827(14) 0.2596(13) 0.079(6) Uiso 0.5 1 d P A 1
C137 C 0.176(2) -0.1424(14) 0.1938(14) 0.092(5) Uiso 0.5 1 d P A 1
C138 C 0.209(2) -0.2165(15) 0.3746(16) 0.088(7) Uiso 0.5 1 d P A 1
C139 C -0.248(3) -0.079(2) 0.2282(18) 0.115(11) Uiso 0.5 1 d P A 1
C140 C -0.3348(18) -0.1481(13) 0.1930(12) 0.071(4) Uiso 0.5 1 d P A 1
C141 C -0.384(2) -0.2965(15) 0.0871(13) 0.092(5) Uiso 0.5 1 d P A 1
C142 C 0.109(2) -0.274(2) 0.1075(13) 0.082(6) Uiso 0.5 1 d P A 1
C143 C -0.267(2) -0.1636(16) 0.4357(14) 0.092(9) Uiso 0.5 1 d P A 1
C144 C -0.067(3) -0.2018(18) 0.4683(15) 0.094(9) Uiso 0.5 1 d P A 1
C145 C -0.4087(17) -0.4495(12) 0.2525(11) 0.064(4) Uiso 0.5 1 d P A 1
C146 C -0.078(3) -0.401(2) 0.0517(18) 0.098(11) Uiso 0.5 1 d P A 1
C201 C -0.005(4) 0.128(3) 0.105(3) 0.128(13) Uiso 0.25 1 d P C 2
C202 C -0.370(3) 0.187(2) -0.0163(19) 0.062(8) Uiso 0.25 1 d P . 2
C203 C -0.220(3) 0.104(2) 0.043(2) 0.094(10) Uiso 0.25 1 d P . 2
C204 C 0.123(4) 0.182(3) 0.184(2) 0.120(12) Uiso 0.25 1 d P C 2
C205 C 0.169(6) 0.078(4) 0.055(3) 0.172(19) Uiso 0.25 1 d P D 2
C206 C 0.610(3) 0.234(2) 0.011(2) 0.076(9) Uiso 0.25 1 d P . 2
C207 C 0.458(6) 0.107(4) 0.006(3) 0.157(18) Uiso 0.25 1 d P . 2
C208 C -0.337(4) 0.153(3) 0.008(2) 0.101(11) Uiso 0.25 1 d P . 2
C209 C 0.569(2) 0.0819(17) -0.0743(15) 0.053(6) Uiso 0.25 1 d P . 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C65 O C70 115.5(9) . .
C63 Si C61 112.6(4) . .
C63 Si C64 113.3(4) . .
C61 Si C64 104.1(4) . .
C63 Si C62 109.6(4) . .
C61 Si C62 111.6(4) . .
C64 Si C62 105.3(5) . .
C7 C1 C6 111.8(9) . .
C7 C1 C2 93.5(9) . .
C6 C1 C2 108.0(7) . .
C7 C1 C61 113.6(8) . .
C6 C1 C61 112.7(7) . .
C2 C1 C61 115.7(7) . .
C7 C1 C36 23.4(9) . .
C6 C1 C36 93.3(10) . .
C2 C1 C36 113.6(10) . .
C61 C1 C36 111.3(9) . .
C3 C2 C9 122.5(11) . .
C3 C2 C135 106.3(11) . .
C9 C2 C135 19.4(11) . .
C3 C2 C1 122.2(8) . .
C9 C2 C1 108.1(11) . .
C135 C2 C1 127.4(11) . .
C2 C3 C114 101.2(13) . .
C2 C3 C12 122.3(12) . .
C114 C3 C12 21.5(13) . .
C2 C3 C4 126.5(8) . .
C114 C3 C4 126.5(13) . .
C12 C3 C4 105.6(11) . .
C14 C4 C4 117.3(10) . 2_556
C14 C4 C3 108.6(8) . .
C4 C4 C3 115.0(8) 2_556 .
C14 C4 C5 94.3(9) . .
C4 C4 C5 112.9(8) 2_556 .
C3 C4 C5 106.5(7) . .
C14 C4 C52 19.4(9) . .
C4 C4 C52 107.6(10) 2_556 .
C3 C4 C52 100.7(8) . .
C5 C4 C52 113.6(9) . .
C6 C5 C104 125.6(11) . .
C6 C5 C4 124.3(8) . .
C104 C5 C4 101.9(11) . .
C6 C5 C17 98.5(11) . .
C104 C5 C17 29.9(8) . .
C4 C5 C17 131.7(10) . .
C116 C6 C5 109.8(11) . .
C116 C6 C1 119.8(11) . .
C5 C6 C1 123.9(9) . .
C116 C6 C19 11.8(11) . .
C5 C6 C19 118.7(10) . .
C1 C6 C19 114.5(9) . .
C36 C7 C137 93(3) . .
C36 C7 C8 138(4) . .
C137 C7 C8 46.6(14) . .
C36 C7 C21 29(3) . .
C137 C7 C21 64.7(16) . .
C8 C7 C21 109.1(15) . .
C36 C7 C1 97(3) . .
C137 C7 C1 169(2) . .
C8 C7 C1 122.8(15) . .
C21 C7 C1 124.2(16) . .
C36 C7 C136 147(3) . .
C137 C7 C136 58.6(17) . .
C8 C7 C136 12.9(9) . .
C21 C7 C136 118.5(14) . .
C1 C7 C136 110.7(12) . .
C136 C8 C137 164(3) . .
C136 C8 C24 83(3) . .
C137 C8 C24 86.0(19) . .
C136 C8 C9 45(2) . .
C137 C8 C9 138.3(19) . .
C24 C8 C9 124.5(18) . .
C136 C8 C7 138(3) . .
C137 C8 C7 45.9(14) . .
C24 C8 C7 128.6(18) . .
C9 C8 C7 93.9(13) . .
C136 C8 C121 56(2) . .
C137 C8 C121 111.7(18) . .
C24 C8 C121 26.4(10) . .
C9 C8 C121 99.1(15) . .
C7 C8 C121 148.8(14) . .
C136 C8 C135 37(3) . .
C137 C8 C135 146.3(17) . .
C24 C8 C135 117.0(16) . .
C9 C8 C135 8.7(12) . .
C7 C8 C135 102.5(13) . .
C121 C8 C135 91.1(14) . .
C136 C8 C36 147(3) . .
C137 C8 C36 33.7(16) . .
C24 C8 C36 115.5(17) . .
C9 C8 C36 105.0(13) . .
C7 C8 C36 13.1(12) . .
C121 C8 C36 137.4(14) . .
C135 C8 C36 113.4(12) . .
C135 C9 C136 120(5) . .
C135 C9 C2 94(4) . .
C136 C9 C2 145(2) . .
C135 C9 C10 37(4) . .
C136 C9 C10 90.0(18) . .
C2 C9 C10 116.4(15) . .
C135 C9 C8 146(5) . .
C136 C9 C8 26.7(13) . .
C2 C9 C8 119.5(15) . .
C10 C9 C8 114.8(16) . .
C135 C9 C138 23(4) . .
C136 C9 C138 109.0(18) . .
C2 C9 C138 99.4(14) . .
C10 C9 C138 19.1(10) . .
C8 C9 C138 133.8(15) . .
C138 C10 C135 99(4) . .
C138 C10 C108 85(3) . .
C135 C10 C108 173(3) . .
C138 C10 C9 114(4) . .
C135 C10 C9 16.8(16) . .
C108 C10 C9 161(2) . .
C138 C10 C26 118(4) . .
C135 C10 C26 143(3) . .
C108 C10 C26 33.3(14) . .
C9 C10 C26 128(2) . .
C138 C10 C11 28(3) . .
C135 C10 C11 115(2) . .
C108 C10 C11 70.4(17) . .
C9 C10 C11 125.2(16) . .
C26 C10 C11 99.5(19) . .
C138 C10 C136 151(4) . .
C135 C10 C136 51.5(18) . .
C108 C10 C136 124(2) . .
C9 C10 C136 37.0(8) . .
C26 C10 C136 91.4(19) . .
C11 C10 C136 155.7(15) . .
C138 C10 C114 37(3) . .
C135 C10 C114 80.8(19) . .
C108 C10 C114 105.4(19) . .
C9 C10 C114 89.6(15) . .
C26 C10 C114 130.1(18) . .
C11 C10 C114 35.6(9) . .
C136 C10 C114 123.4(15) . .
C138 C10 C103 127(4) . .
C135 C10 C103 133(2) . .
C108 C10 C103 42.4(18) . .
C9 C10 C103 118.7(17) . .
C26 C10 C103 9.7(19) . .
C11 C10 C103 109.1(17) . .
C136 C10 C103 82.1(15) . .
C114 C10 C103 138.6(17) . .
C138 C11 C114 85(2) . .
C138 C11 C128 145(2) . .
C114 C11 C128 61.1(19) . .
C138 C11 C12 106(2) . .
C114 C11 C12 21.4(17) . .
C128 C11 C12 40.0(12) . .
C138 C11 C28 121(2) . .
C114 C11 C28 140(2) . .
C128 C11 C28 85(2) . .
C12 C11 C28 123(2) . .
C138 C11 C10 16.0(16) . .
C114 C11 C10 90(2) . .
C128 C11 C10 142.8(18) . .
C12 C11 C10 110.3(19) . .
C28 C11 C10 108.0(18) . .
C138 C11 C108 53.9(16) . .
C114 C11 C108 134(2) . .
C128 C11 C108 148.5(19) . .
C12 C11 C108 151.1(19) . .
C28 C11 C108 67.4(18) . .
C10 C11 C108 44.7(10) . .
C138 C11 C133 144(2) . .
C114 C11 C133 118(2) . .
C128 C11 C133 60.2(15) . .
C12 C11 C133 98.9(17) . .
C28 C11 C133 25.3(13) . .
C10 C11 C133 129.2(15) . .
C108 C11 C133 92.3(16) . .
C138 C11 C123 101.3(19) . .
C114 C11 C123 149(2) . .
C128 C11 C123 103.6(18) . .
C12 C11 C123 138.0(17) . .
C28 C11 C123 19.4(13) . .
C10 C11 C123 89.2(13) . .
C108 C11 C123 48.0(12) . .
C133 C11 C123 44.4(13) . .
C114 C12 C128 117(6) . .
C114 C12 C11 50(5) . .
C128 C12 C11 68(2) . .
C114 C12 C3 73(5) . .
C128 C12 C3 158(3) . .
C11 C12 C3 123(2) . .
C114 C12 C144 156(5) . .
C128 C12 C144 49(2) . .
C11 C12 C144 115(2) . .
C3 C12 C144 113.6(18) . .
C114 C12 C13 149(5) . .
C128 C12 C13 54(2) . .
C11 C12 C13 115.9(19) . .
C3 C12 C13 106.7(14) . .
C144 C12 C13 10.5(13) . .
C114 C12 C138 19(5) . .
C128 C12 C138 98(2) . .
C11 C12 C138 31.0(10) . .
C3 C12 C138 92.3(15) . .
C144 C12 C138 141.8(19) . .
C13 C12 C138 138.6(15) . .
C52 C13 C30 161(3) . .
C52 C13 C122 131(3) . .
C30 C13 C122 32.6(13) . .
C52 C13 C14 18.1(13) . .
C30 C13 C14 153(2) . .
C122 C13 C14 121(2) . .
C52 C13 C128 123(2) . .
C30 C13 C128 75.8(18) . .
C122 C13 C128 104(2) . .
C14 C13 C128 124.9(18) . .
C52 C13 C12 94.1(17) . .
C30 C13 C12 105.0(19) . .
C122 C13 C12 130.1(19) . .
C14 C13 C12 95.5(15) . .
C128 C13 C12 29.6(10) . .
C52 C13 C143 45.4(14) . .
C30 C13 C143 118(2) . .
C122 C13 C143 85.9(17) . .
C14 C13 C143 37.5(10) . .
C128 C13 C143 158.8(18) . .
C12 C13 C143 132.0(16) . .
C52 C14 C143 102(3) . .
C52 C14 C15 129(4) . .
C143 C14 C15 27.1(14) . .
C52 C14 C4 97(3) . .
C143 C14 C4 154.0(19) . .
C15 C14 C4 132(2) . .
C52 C14 C13 40(3) . .
C143 C14 C13 91.8(17) . .
C15 C14 C13 111.7(19) . .
C4 C14 C13 113.9(15) . .
C52 C14 C144 33(3) . .
C143 C14 C144 104.8(18) . .
C15 C14 C144 125.4(18) . .
C4 C14 C144 100.6(13) . .
C13 C14 C144 13.7(13) . .
C52 C14 C112 146(4) . .
C143 C14 C112 44.9(16) . .
C15 C14 C112 18.4(14) . .
C4 C14 C112 113.8(13) . .
C13 C14 C112 127.7(16) . .
C144 C14 C112 141.2(14) . .
C52 C14 C104 169(4) . .
C143 C14 C104 78.3(17) . .
C15 C14 C104 52.2(15) . .
C4 C14 C104 80.3(10) . .
C13 C14 C104 150.9(15) . .
C144 C14 C104 157.4(14) . .
C112 C14 C104 33.8(8) . .
C143 C15 C112 149(5) . .
C143 C15 C14 72(4) . .
C112 C15 C14 135(3) . .
C143 C15 C130 80(4) . .
C112 C15 C130 83(3) . .
C14 C15 C130 139(3) . .
C143 C15 C104 156(4) . .
C112 C15 C104 45(2) . .
C14 C15 C104 90.2(16) . .
C130 C15 C104 124(2) . .
C143 C15 C52 57(4) . .
C112 C15 C52 149(3) . .
C14 C15 C52 15.4(12) . .
C130 C15 C52 127(2) . .
C104 C15 C52 105.1(15) . .
C143 C15 C16 159(4) . .
C112 C15 C16 11(2) . .
C14 C15 C16 128(2) . .
C130 C15 C16 85(2) . .
C104 C15 C16 38.9(11) . .
C52 C15 C16 143.1(16) . .
C143 C15 C32 56(3) . .
C112 C15 C32 110(3) . .
C14 C15 C32 112(2) . .
C130 C15 C32 27.7(11) . .
C104 C15 C32 148.3(19) . .
C52 C15 C32 99.4(17) . .
C16 C15 C32 112.2(17) . .
C112 C16 C104 70(3) . .
C112 C16 C105 161(4) . .
C104 C16 C105 96(3) . .
C112 C16 C17 110(3) . .
C104 C16 C17 39.8(15) . .
C105 C16 C17 57(2) . .
C112 C16 C34 80(3) . .
C104 C16 C34 146(4) . .
C105 C16 C34 108(3) . .
C17 C16 C34 160(3) . .
C112 C16 C125 108(4) . .
C104 C16 C125 157(2) . .
C105 C16 C125 80(3) . .
C17 C16 C125 135(3) . .
C34 C16 C125 28.4(12) . .
C112 C16 C15 11(2) . .
C104 C16 C15 65(2) . .
C105 C16 C15 151(2) . .
C17 C16 C15 104(2) . .
C34 C16 C15 82(2) . .
C125 C16 C15 108(2) . .
C112 C16 C35 130(3) . .
C104 C16 C35 145(3) . .
C105 C16 C35 56(2) . .
C17 C16 C35 112(3) . .
C34 C16 C35 52.0(15) . .
C125 C16 C35 23.6(12) . .
C15 C16 C35 128.0(18) . .
C112 C16 C18 142(3) . .
C104 C16 C18 77(2) . .
C105 C16 C18 20.4(15) . .
C17 C16 C18 40.2(17) . .
C34 C16 C18 122(2) . .
C125 C16 C18 95(2) . .
C15 C16 C18 131.8(16) . .
C35 C16 C18 71.8(17) . .
C104 C17 C105 122(3) . .
C104 C17 C16 64(2) . .
C105 C17 C16 59.5(18) . .
C104 C17 C18 152(2) . .
C105 C17 C18 48.1(16) . .
C16 C17 C18 105(2) . .
C104 C17 C5 64(2) . .
C105 C17 C5 153.5(18) . .
C16 C17 C5 126(2) . .
C18 C17 C5 112.4(15) . .
C104 C17 C112 35.4(18) . .
C105 C17 C112 87.7(18) . .
C16 C17 C112 29.0(16) . .
C18 C17 C112 129.6(17) . .
C5 C17 C112 98.3(17) . .
C104 C17 C139 154(2) . .
C105 C17 C139 44(2) . .
C16 C17 C139 102(3) . .
C18 C17 C139 4.9(15) . .
C5 C17 C139 117.2(14) . .
C112 C17 C139 127.7(17) . .
C139 C18 C105 112(5) . .
C139 C18 C17 164(5) . .
C105 C18 C17 53.8(17) . .
C139 C18 C116 96(5) . .
C105 C18 C116 150(3) . .
C17 C18 C116 100.1(19) . .
C139 C18 C140 45(4) . .
C105 C18 C140 73.4(19) . .
C17 C18 C140 125.5(19) . .
C116 C18 C140 124.3(19) . .
C139 C18 C19 75(4) . .
C105 C18 C19 172(3) . .
C17 C18 C19 119.7(19) . .
C116 C18 C19 22.1(11) . .
C140 C18 C19 111.3(19) . .
C139 C18 C16 134(5) . .
C105 C18 C16 22.7(17) . .
C17 C18 C16 34.3(11) . .
C116 C18 C16 127.0(19) . .
C140 C18 C16 91.2(16) . .
C19 C18 C16 149(2) . .
C139 C18 C104 165(5) . .
C105 C18 C104 52.9(19) . .
C17 C18 C104 10.2(9) . .
C116 C18 C104 98.4(16) . .
C140 C18 C104 120.7(16) . .
C19 C18 C104 119.6(17) . .
C16 C18 C104 31.1(8) . .
C116 C19 C119 96(3) . .
C116 C19 C20 118(4) . .
C119 C19 C20 25.3(14) . .
C116 C19 C139 88(3) . .
C119 C19 C139 123(2) . .
C20 C19 C139 110(2) . .
C116 C19 C18 67(3) . .
C119 C19 C18 129.9(18) . .
C20 C19 C18 125.6(18) . .
C139 C19 C18 22.4(13) . .
C116 C19 C6 28(3) . .
C119 C19 C6 94.2(16) . .
C20 C19 C6 119.5(17) . .
C139 C19 C6 111.2(17) . .
C18 C19 C6 89.0(14) . .
C119 C20 C38 115(5) . .
C119 C20 C19 67(4) . .
C38 C20 C19 138(3) . .
C119 C20 C21 53(3) . .
C38 C20 C21 79(2) . .
C19 C20 C21 120(2) . .
C119 C20 C115 127(4) . .
C38 C20 C115 32.4(14) . .
C19 C20 C115 109.7(18) . .
C21 C20 C115 110.2(19) . .
C119 C20 C116 53(4) . .
C38 C20 C116 131(2) . .
C19 C20 C116 16.9(11) . .
C21 C20 C116 106.2(18) . .
C115 C20 C116 110.1(15) . .
C119 C20 C36 28(3) . .
C38 C20 C36 105(2) . .
C19 C20 C36 92.5(18) . .
C21 C20 C36 28.6(10) . .
C115 C20 C36 131.7(17) . .
C116 C20 C36 79.9(14) . .
C36 C21 C119 82(2) . .
C36 C21 C137 63(2) . .
C119 C21 C137 137(2) . .
C36 C21 C22 143(3) . .
C119 C21 C22 122(2) . .
C137 C21 C22 82(2) . .
C36 C21 C7 20.6(19) . .
C119 C21 C7 98.7(19) . .
C137 C21 C7 42.3(10) . .
C22 C21 C7 122(2) . .
C36 C21 C20 102(3) . .
C119 C21 C20 22.2(14) . .
C137 C21 C20 158(2) . .
C22 C21 C20 107(2) . .
C7 C21 C20 121(2) . .
C36 C21 C38 136(2) . .
C119 C21 C38 56.4(15) . .
C137 C21 C38 143.3(17) . .
C22 C21 C38 67.8(19) . .
C7 C21 C38 146.3(14) . .
C20 C21 C38 39.4(10) . .
C36 C21 C110 151(3) . .
C119 C21 C110 108(2) . .
C137 C21 C110 95(2) . .
C22 C21 C110 14(2) . .
C7 C21 C110 132.8(19) . .
C20 C21 C110 92.8(18) . .
C38 C21 C110 53.4(15) . .
C36 C21 C131 116(2) . .
C119 C21 C131 141.8(18) . .
C137 C21 C131 54.5(13) . .
C22 C21 C131 27.8(15) . .
C7 C21 C131 95.4(14) . .
C20 C21 C131 133.2(19) . .
C38 C21 C131 94.1(16) . .
C110 C21 C131 41.4(17) . .
C131 C22 C39 147(4) . .
C131 C22 C142 25(2) . .
C39 C22 C142 123(2) . .
C131 C22 C21 96(4) . .
C39 C22 C21 108(3) . .
C142 C22 C21 117(3) . .
C131 C22 C38 150(4) . .
C39 C22 C38 46.6(16) . .
C142 C22 C38 151(2) . .
C21 C22 C38 61.5(16) . .
C131 C22 C137 49(3) . .
C39 C22 C137 147(2) . .
C142 C22 C137 71(2) . .
C21 C22 C137 47.3(13) . .
C38 C22 C137 106.0(18) . .
C131 C22 C118 114(4) . .
C39 C22 C118 33.5(13) . .
C142 C22 C118 89.6(18) . .
C21 C22 C118 136(2) . .
C38 C22 C118 77.9(19) . .
C137 C22 C118 146.3(19) . .
C142 C23 C24 91(3) . .
C142 C23 C42 86(3) . .
C24 C23 C42 168(2) . .
C142 C23 C117 160(4) . .
C24 C23 C117 71(2) . .
C42 C23 C117 109(3) . .
C142 C23 C107 113(4) . .
C24 C23 C107 147(3) . .
C42 C23 C107 29.0(11) . .
C117 C23 C107 80(2) . .
C142 C23 C121 125(3) . .
C24 C23 C121 34.4(13) . .
C42 C23 C121 145(3) . .
C117 C23 C121 36.9(17) . .
C107 C23 C121 116(2) . .
C142 C23 C131 15(3) . .
C24 C23 C131 77(2) . .
C42 C23 C131 99(2) . .
C117 C23 C131 146(2) . .
C107 C23 C131 124(2) . .
C121 C23 C131 111(2) . .
C142 C23 C43 144(3) . .
C24 C23 C43 117(3) . .
C42 C23 C43 61.8(14) . .
C117 C23 C43 47.2(17) . .
C107 C23 C43 33.0(11) . .
C121 C23 C43 83.5(19) . .
C131 C23 C43 151.8(17) . .
C142 C23 C25 149(3) . .
C24 C23 C25 62.8(18) . .
C42 C23 C25 116(2) . .
C117 C23 C25 10.8(18) . .
C107 C23 C25 87(2) . .
C121 C23 C25 29.2(12) . .
C131 C23 C25 135.0(17) . .
C43 C23 C25 54.5(14) . .
C121 C24 C23 93(3) . .
C121 C24 C8 105(3) . .
C23 C24 C8 151(2) . .
C121 C24 C142 126(3) . .
C23 C24 C142 33.3(15) . .
C8 C24 C142 122(2) . .
C121 C24 C136 77(2) . .
C23 C24 C136 155(2) . .
C8 C24 C136 28.7(10) . .
C142 C24 C136 146(2) . .
C121 C24 C117 31(2) . .
C23 C24 C117 62.1(18) . .
C8 C24 C117 132(2) . .
C142 C24 C117 95(2) . .
C136 C24 C117 105(2) . .
C121 C24 C131 151(3) . .
C23 C24 C131 61.1(19) . .
C8 C24 C131 94.9(17) . .
C142 C24 C131 27.9(13) . .
C136 C24 C131 121.7(19) . .
C117 C24 C131 122(2) . .
C121 C24 C137 145(3) . .
C23 C24 C137 115(2) . .
C8 C24 C137 40.7(10) . .
C142 C24 C137 82.4(19) . .
C136 C24 C137 69.0(14) . .
C117 C24 C137 157.8(16) . .
C131 C24 C137 54.6(13) . .
C121 C24 C25 12.9(19) . .
C23 C24 C25 84(2) . .
C8 C24 C25 110.1(19) . .
C142 C24 C25 115(2) . .
C136 C24 C25 82.2(17) . .
C117 C24 C25 22.6(16) . .
C131 C24 C25 138.9(17) . .
C137 C24 C25 144.4(16) . .
C103 C25 C117 152(8) . .
C103 C25 C121 152(7) . .
C117 C25 C121 56(4) . .
C103 C25 C26 29(4) . .
C117 C25 C26 164(4) . .
C121 C25 C26 126(3) . .
C103 C25 C132 61(4) . .
C117 C25 C132 92(4) . .
C121 C25 C132 144(3) . .
C26 C25 C132 80(2) . .
C103 C25 C43 110(5) . .
C117 C25 C43 43(4) . .
C121 C25 C43 97(3) . .
C26 C25 C43 127(2) . .
C132 C25 C43 49.6(12) . .
C103 C25 C24 156(6) . .
C117 C25 C24 51(4) . .
C121 C25 C24 9.8(15) . .
C26 C25 C24 128(3) . .
C132 C25 C24 135(2) . .
C43 C25 C24 89(2) . .
C103 C25 C108 31(4) . .
C117 C25 C108 166(4) . .
C121 C25 C108 122(3) . .
C26 C25 C108 4.4(17) . .
C132 C25 C108 84.3(19) . .
C43 C25 C108 131(2) . .
C24 C25 C108 124.8(18) . .
C103 C25 C23 163(5) . .
C117 C25 C23 21(4) . .
C121 C25 C23 41.1(19) . .
C26 C25 C23 149(2) . .
C132 C25 C23 103.7(19) . .
C43 C25 C23 55.7(15) . .
C24 C25 C23 33.6(9) . .
C108 C25 C23 148.8(17) . .
C103 C26 C108 152(7) . .
C103 C26 C25 33(5) . .
C108 C26 C25 170(4) . .
C103 C26 C27 96(5) . .
C108 C26 C27 71(3) . .
C25 C26 C27 119(3) . .
C103 C26 C10 145(6) . .
C108 C26 C10 58(3) . .
C25 C26 C10 114(3) . .
C27 C26 C10 117(3) . .
C103 C26 C117 35(5) . .
C108 C26 C117 172(4) . .
C25 C26 C117 6.2(18) . .
C27 C26 C117 115(3) . .
C10 C26 C117 114(2) . .
C103 C26 C132 45(5) . .
C108 C26 C132 125(3) . .
C25 C26 C132 65(2) . .
C27 C26 C132 54.2(15) . .
C10 C26 C132 154.3(18) . .
C117 C26 C132 62.3(18) . .
C103 C26 C138 162(6) . .
C108 C26 C138 40(2) . .
C25 C26 C138 132(3) . .
C27 C26 C138 102(2) . .
C10 C26 C138 17.7(12) . .
C117 C26 C138 132(2) . .
C132 C26 C138 151.0(18) . .
C103 C26 C121 59(5) . .
C108 C26 C121 145(3) . .
C25 C26 C121 26.4(19) . .
C27 C26 C121 139(2) . .
C10 C26 C121 87.7(17) . .
C117 C26 C121 27.3(11) . .
C132 C26 C121 89.1(18) . .
C138 C26 C121 105.4(16) . .
C103 C26 C123 118(5) . .
C108 C26 C123 49(2) . .
C25 C26 C123 141(2) . .
C27 C26 C123 22.5(12) . .
C10 C26 C123 96(2) . .
C117 C26 C123 136(2) . .
C132 C26 C123 76.7(14) . .
C138 C26 C123 79.8(19) . .
C121 C26 C123 153.9(16) . .
C123 C27 C101 98(3) . .
C123 C27 C108 82(3) . .
C101 C27 C108 178(2) . .
C123 C27 C26 115(3) . .
C101 C27 C26 147(3) . .
C108 C27 C26 33.6(14) . .
C123 C27 C45 120(3) . .
C101 C27 C45 25.1(15) . .
C108 C27 C45 156(2) . .
C26 C27 C45 122(3) . .
C123 C27 C28 14(2) . .
C101 C27 C28 106(2) . .
C108 C27 C28 74.8(18) . .
C26 C27 C28 105(2) . .
C45 C27 C28 123.8(19) . .
C123 C27 C132 167(3) . .
C101 C27 C132 68.9(19) . .
C108 C27 C132 111(2) . .
C26 C27 C132 78(2) . .
C45 C27 C132 46.8(11) . .
C28 C27 C132 164.1(17) . .
C123 C27 C103 135(4) . .
C101 C27 C103 126(3) . .
C108 C27 C103 53.6(19) . .
C26 C27 C103 21.4(19) . .
C45 C27 C103 104(2) . .
C28 C27 C103 127(2) . .
C132 C27 C103 57.4(16) . .
C123 C28 C133 136(5) . .
C123 C28 C11 120(4) . .
C133 C28 C11 102(5) . .
C123 C28 C29 117(3) . .
C133 C28 C29 20(3) . .
C11 C28 C29 118(3) . .
C123 C28 C27 15(3) . .
C133 C28 C27 139(4) . .
C11 C28 C27 109(2) . .
C29 C28 C27 119(2) . .
C123 C28 C108 58(3) . .
C133 C28 C108 160(4) . .
C11 C28 C108 61.5(15) . .
C29 C28 C108 159.1(19) . .
C27 C28 C108 49.9(14) . .
C123 C28 C128 158(4) . .
C133 C28 C128 57(4) . .
C11 C28 C128 45.1(14) . .
C29 C28 C128 73(2) . .
C27 C28 C128 142.7(17) . .
C108 C28 C128 105.2(16) . .
C123 C28 C101 26(2) . .
C133 C28 C101 112(4) . .
C11 C28 C101 137(2) . .
C29 C28 C101 91.8(16) . .
C27 C28 C101 29.8(10) . .
C108 C28 C101 79.6(17) . .
C128 C28 C101 149.5(16) . .
C129 C29 C133 161(6) . .
C129 C29 C47 48(3) . .
C133 C29 C47 139(4) . .
C129 C29 C30 66(4) . .
C133 C29 C30 103(4) . .
C47 C29 C30 114(3) . .
C129 C29 C28 153(4) . .
C133 C29 C28 20(3) . .
C47 C29 C28 119(2) . .
C30 C29 C28 119(3) . .
C129 C29 C106 44(3) . .
C133 C29 C106 136(4) . .
C47 C29 C106 14.0(12) . .
C30 C29 C106 107(2) . .
C28 C29 C106 116.6(18) . .
C129 C29 C122 45(3) . .
C133 C29 C122 121(4) . .
C47 C29 C122 92(2) . .
C30 C29 C122 23.3(12) . .
C28 C29 C122 132(2) . .
C106 C29 C122 84.2(18) . .
C129 C29 C123 139(4) . .
C133 C29 C123 40(3) . .
C47 C29 C123 98.7(19) . .
C30 C29 C123 137(2) . .
C28 C29 C123 20.1(11) . .
C106 C29 C123 97.8(15) . .
C122 C29 C123 142.6(17) . .
C129 C29 C128 118(4) . .
C133 C29 C128 48(3) . .
C47 C29 C128 156(2) . .
C30 C29 C128 56.0(15) . .
C28 C29 C128 64(2) . .
C106 C29 C128 141.5(16) . .
C122 C29 C128 73.8(15) . .
C123 C29 C128 82.5(19) . .
C122 C30 C13 87(3) . .
C122 C30 C144 108(3) . .
C13 C30 C144 20.8(17) . .
C122 C30 C129 80(3) . .
C13 C30 C129 143(2) . .
C144 C30 C129 144(2) . .
C122 C30 C29 109(3) . .
C13 C30 C29 132(2) . .
C144 C30 C29 121(2) . .
C129 C30 C29 30.6(15) . .
C122 C30 C31 12(2) . .
C13 C30 C31 100(2) . .
C144 C30 C31 120(2) . .
C129 C30 C31 71.8(18) . .
C29 C30 C31 102(2) . .
C122 C30 C128 136(3) . .
C13 C30 C128 59.9(17) . .
C144 C30 C128 42.4(14) . .
C129 C30 C128 108(2) . .
C29 C30 C128 79.9(19) . .
C31 C30 C128 147.0(15) . .
C122 C30 C133 128(3) . .
C13 C30 C133 112(2) . .
C144 C30 C133 97(2) . .
C129 C30 C133 55.1(17) . .
C29 C30 C133 25.1(14) . .
C31 C30 C133 124.0(16) . .
C128 C30 C133 55.0(14) . .
C122 C31 C126 124(4) . .
C122 C31 C32 107(3) . .
C126 C31 C32 20(2) . .
C122 C31 C48 119(3) . .
C126 C31 C48 99(3) . .
C32 C31 C48 118(2) . .
C122 C31 C30 12(2) . .
C126 C31 C30 136(3) . .
C32 C31 C30 118.4(17) . .
C48 C31 C30 112.2(16) . .
C122 C31 C129 57(3) . .
C126 C31 C129 148(3) . .
C32 C31 C129 150.7(15) . .
C48 C31 C129 63.5(14) . .
C30 C31 C129 48.8(13) . .
C122 C31 C111 145(3) . .
C126 C31 C111 56(3) . .
C32 C31 C111 76.2(17) . .
C48 C31 C111 42.6(11) . .
C30 C31 C111 146.6(14) . .
C129 C31 C111 103.0(15) . .
C126 C32 C130 145(4) . .
C126 C32 C33 95(3) . .
C130 C32 C33 57(2) . .
C126 C32 C31 22(2) . .
C130 C32 C31 157(2) . .
C33 C32 C31 116(2) . .
C126 C32 C143 133(3) . .
C130 C32 C143 65(2) . .
C33 C32 C143 121(2) . .
C31 C32 C143 113.2(17) . .
C126 C32 C15 139(3) . .
C130 C32 C15 49(2) . .
C33 C32 C15 103(2) . .
C31 C32 C15 123.2(16) . .
C143 C32 C15 18.8(12) . .
C126 C32 C122 45(2) . .
C130 C32 C122 142(2) . .
C33 C32 C122 133(2) . .
C31 C32 C122 24.2(9) . .
C143 C32 C122 89.2(15) . .
C15 C32 C122 99.3(15) . .
C126 C32 C127 108(3) . .
C130 C32 C127 41(2) . .
C33 C32 C127 16.3(12) . .
C31 C32 C127 128.4(17) . .
C143 C32 C127 104.5(18) . .
C15 C32 C127 86.6(15) . .
C122 C32 C127 139.0(14) . .
C127 C33 C130 99(3) . .
C127 C33 C32 138(3) . .
C130 C33 C32 39.7(14) . .
C127 C33 C50 90(3) . .
C130 C33 C50 157(2) . .
C32 C33 C50 125(2) . .
C127 C33 C34 32(2) . .
C130 C33 C34 67.3(18) . .
C32 C33 C34 107(2) . .
C50 C33 C34 121(2) . .
C127 C33 C102 63(3) . .
C130 C33 C102 154(2) . .
C32 C33 C102 149(2) . .
C50 C33 C102 27.0(11) . .
C34 C33 C102 94(2) . .
C127 C33 C126 157(3) . .
C130 C33 C126 68(2) . .
C32 C33 C126 29.3(12) . .
C50 C33 C126 96.0(19) . .
C34 C33 C126 132(2) . .
C102 C33 C126 121.2(19) . .
C127 C33 C111 127(3) . .
C130 C33 C111 124(2) . .
C32 C33 C111 87.4(19) . .
C50 C33 C111 38.0(11) . .
C34 C33 C111 151.2(19) . .
C102 C33 C111 64.5(14) . .
C126 C33 C111 58.2(14) . .
C127 C33 C125 19(2) . .
C130 C33 C125 81(2) . .
C32 C33 C125 119.7(18) . .
C50 C33 C125 103.9(18) . .
C34 C33 C125 16.9(12) . .
C102 C33 C125 77.8(15) . .
C126 C33 C125 140.0(15) . .
C111 C33 C125 135.3(16) . .
C125 C34 C127 102(4) . .
C125 C34 C130 154(3) . .
C127 C34 C130 75(3) . .
C125 C34 C33 130(4) . .
C127 C34 C33 31(2) . .
C130 C34 C33 44.5(13) . .
C125 C34 C16 81(3) . .
C127 C34 C16 154(3) . .
C130 C34 C16 91(2) . .
C33 C34 C16 133(3) . .
C125 C34 C35 4(2) . .
C127 C34 C35 105(3) . .
C130 C34 C35 151.9(18) . .
C33 C34 C35 132(2) . .
C16 C34 C35 77(2) . .
C125 C34 C112 112(4) . .
C127 C34 C112 132(4) . .
C130 C34 C112 58.9(18) . .
C33 C34 C112 102(2) . .
C16 C34 C112 32.9(14) . .
C35 C34 C112 108(2) . .
C125 C34 C109 13(2) . .
C127 C34 C109 90(3) . .
C130 C34 C109 145.9(17) . .
C33 C34 C109 116.9(19) . .
C16 C34 C109 90(2) . .
C35 C34 C109 15.3(12) . .
C112 C34 C109 119(2) . .
C109 C35 C125 128(5) . .
C109 C35 C124 21(4) . .
C125 C35 C124 149(4) . .
C109 C35 C34 131(4) . .
C125 C35 C34 4(2) . .
C124 C35 C34 151(3) . .
C109 C35 C140 70(4) . .
C125 C35 C140 148(3) . .
C124 C35 C140 50(2) . .
C34 C35 C140 144.6(19) . .
C109 C35 C105 129(4) . .
C125 C35 C105 93(3) . .
C124 C35 C105 110(3) . .
C34 C35 C105 89(2) . .
C140 C35 C105 60.5(14) . .
C109 C35 C16 155(4) . .
C125 C35 C16 55(3) . .
C124 C35 C16 144(3) . .
C34 C35 C16 51.3(16) . .
C140 C35 C16 97.0(17) . .
C105 C35 C16 38.0(12) . .
C109 C35 C127 106(4) . .
C125 C35 C127 22(2) . .
C124 C35 C127 127(3) . .
C34 C35 C127 25.2(10) . .
C140 C35 C127 150.7(15) . .
C105 C35 C127 112(2) . .
C16 C35 C127 74.4(18) . .
C109 C35 C113 27(3) . .
C125 C35 C113 101(3) . .
C124 C35 C113 48(3) . .
C34 C35 C113 104.3(16) . .
C140 C35 C113 93.0(19) . .
C105 C35 C113 144.4(18) . .
C16 C35 C113 142.5(17) . .
C127 C35 C113 79.2(12) . .
C7 C36 C21 130(4) . .
C7 C36 C137 55(3) . .
C21 C36 C137 77(2) . .
C7 C36 C119 151(4) . .
C21 C36 C119 58(2) . .
C137 C36 C119 129(3) . .
C7 C36 C1 60(3) . .
C21 C36 C1 163(3) . .
C137 C36 C1 114(2) . .
C119 C36 C1 106.2(17) . .
C7 C36 C20 160(3) . .
C21 C36 C20 49(2) . .
C137 C36 C20 123(2) . .
C119 C36 C20 11.0(13) . .
C1 C36 C20 115.9(16) . .
C7 C36 C8 29(3) . .
C21 C36 C8 102(2) . .
C137 C36 C8 27.3(13) . .
C119 C36 C8 141.5(17) . .
C1 C36 C8 87.5(14) . .
C20 C36 C8 142.0(16) . .
C120 C37 C115 126(5) . .
C120 C37 C141 98(4) . .
C115 C37 C141 135(3) . .
C120 C37 C140 15(2) . .
C115 C37 C140 123(3) . .
C141 C37 C140 95(2) . .
C120 C37 C134 152(4) . .
C115 C37 C134 80(3) . .
C141 C37 C134 54.9(15) . .
C140 C37 C134 143.8(19) . .
C120 C37 C124 43(3) . .
C115 C37 C124 160(3) . .
C141 C37 C124 55(2) . .
C140 C37 C124 40.7(17) . .
C134 C37 C124 109(2) . .
C120 C37 C38 121(4) . .
C115 C37 C38 11.3(16) . .
C141 C37 C38 134(2) . .
C140 C37 C38 115.1(17) . .
C134 C37 C38 82.6(18) . .
C124 C37 C38 149(2) . .
C115 C38 C20 109(3) . .
C115 C38 C39 89(3) . .
C20 C38 C39 161(3) . .
C115 C38 C119 119(2) . .
C20 C38 C119 21.7(17) . .
C39 C38 C119 141(2) . .
C115 C38 C110 122(3) . .
C20 C38 C110 127(3) . .
C39 C38 C110 34.0(15) . .
C119 C38 C110 110(2) . .
C115 C38 C21 161(2) . .
C20 C38 C21 61.2(18) . .
C39 C38 C21 99.4(19) . .
C119 C38 C21 46.2(11) . .
C110 C38 C21 65.5(18) . .
C115 C38 C22 136(3) . .
C20 C38 C22 112(2) . .
C39 C38 C22 48.8(17) . .
C119 C38 C22 95.5(17) . .
C110 C38 C22 14.8(18) . .
C21 C38 C22 50.7(12) . .
C115 C38 C37 11.3(15) . .
C20 C38 C37 105(2) . .
C39 C38 C37 92(2) . .
C119 C38 C37 111.4(16) . .
C110 C38 C37 122(2) . .
C21 C38 C37 149.7(15) . .
C22 C38 C37 134.5(19) . .
C110 C39 C118 102(4) . .
C110 C39 C38 89(4) . .
C118 C39 C38 153(3) . .
C110 C39 C22 4(4) . .
C118 C39 C22 106(3) . .
C38 C39 C22 85(2) . .
C110 C39 C40 117(4) . .
C118 C39 C40 18(2) . .
C38 C39 C40 138(2) . .
C22 C39 C40 120(2) . .
C110 C39 C115 124(4) . .
C118 C39 C115 123(3) . .
C38 C39 C115 36.4(12) . .
C22 C39 C115 120(2) . .
C40 C39 C115 105.6(18) . .
C110 C39 C134 152(4) . .
C118 C39 C134 58(2) . .
C38 C39 C134 102(2) . .
C22 C39 C134 153.3(19) . .
C40 C39 C134 40.8(11) . .
C115 C39 C134 66.2(14) . .
C118 C40 C134 119(6) . .
C118 C40 C41 84(6) . .
C134 C40 C41 155(3) . .
C118 C40 C39 41(5) . .
C134 C40 C39 80(2) . .
C41 C40 C39 121(2) . .
C118 C40 C146 75(6) . .
C134 C40 C146 157(3) . .
C41 C40 C146 14.5(14) . .
C39 C40 C146 108(2) . .
C118 C40 C54 159(6) . .
C134 C40 C54 42.9(16) . .
C41 C40 C54 112.0(18) . .
C39 C40 C54 118(2) . .
C146 C40 C54 118.7(19) . .
C118 C40 C110 26(5) . .
C134 C40 C110 100(2) . .
C41 C40 C110 99.0(18) . .
C39 C40 C110 22.2(14) . .
C146 C40 C110 85.8(18) . .
C54 C40 C110 133.9(17) . .
C146 C41 C40 130(5) . .
C146 C41 C118 112(5) . .
C40 C41 C118 23.6(16) . .
C146 C41 C56 98(6) . .
C40 C41 C56 108.6(16) . .
C118 C41 C56 131.2(18) . .
C146 C41 C42 21(5) . .
C40 C41 C42 118.8(17) . .
C118 C41 C42 97.1(17) . .
C56 C41 C42 118.7(17) . .
C146 C41 C107 2(4) . .
C40 C41 C107 131.4(15) . .
C118 C41 C107 113.2(18) . .
C56 C41 C107 98.1(14) . .
C42 C41 C107 20.7(8) . .
C107 C42 C146 96(3) . .
C107 C42 C23 81(3) . .
C146 C42 C23 144(3) . .
C107 C42 C142 110(3) . .
C146 C42 C142 127(3) . .
C23 C42 C142 30.5(12) . .
C107 C42 C41 107(3) . .
C146 C42 C41 11(3) . .
C23 C42 C41 145.0(16) . .
C142 C42 C41 121.8(17) . .
C107 C42 C43 10(2) . .
C146 C42 C43 106(3) . .
C23 C42 C43 72.7(18) . .
C142 C42 C43 102.3(17) . .
C41 C42 C43 117.3(16) . .
C107 C43 C44 107(2) . .
C107 C43 C117 101(3) . .
C44 C43 C117 139(3) . .
C107 C43 C132 153(2) . .
C44 C43 C132 56.1(13) . .
C117 C43 C132 87(2) . .
C107 C43 C42 7.0(15) . .
C44 C43 C42 113.7(19) . .
C117 C43 C42 95(2) . .
C132 C43 C42 158.2(15) . .
C107 C43 C25 120(2) . .
C44 C43 C25 118(2) . .
C117 C43 C25 22(2) . .
C132 C43 C25 64.7(16) . .
C42 C43 C25 114.7(18) . .
C107 C43 C23 51.3(17) . .
C44 C43 C23 147.9(18) . .
C117 C43 C23 49.7(18) . .
C132 C43 C23 131.7(17) . .
C42 C43 C23 45.5(11) . .
C25 C43 C23 69.8(17) . .
C107 C43 C103 135(2) . .
C44 C43 C103 101.6(18) . .
C117 C43 C103 40(2) . .
C132 C43 C103 46.9(13) . .
C42 C43 C103 131.4(16) . .
C25 C43 C103 17.8(13) . .
C23 C43 C103 87.3(15) . .
C43 C44 C132 74.4(16) . .
C43 C44 C57 137.9(17) . .
C132 C44 C57 139.3(14) . .
C43 C44 C45 117.6(16) . .
C132 C44 C45 46.0(10) . .
C57 C44 C45 93.9(11) . .
C43 C44 C107 33.0(11) . .
C132 C44 C107 105.0(14) . .
C57 C44 C107 105.1(11) . .
C45 C44 C107 140.0(11) . .
C101 C45 C132 107(3) . .
C101 C45 C46 86(3) . .
C132 C45 C46 163(2) . .
C101 C45 C27 43(3) . .
C132 C45 C27 70.9(17) . .
C46 C45 C27 115.7(18) . .
C101 C45 C44 156(4) . .
C132 C45 C44 48.7(13) . .
C46 C45 C44 117.4(15) . .
C27 C45 C44 115.3(17) . .
C101 C45 C123 27(3) . .
C132 C45 C123 91.3(17) . .
C46 C45 C123 96.1(14) . .
C27 C45 C123 20.4(11) . .
C44 C45 C123 134.1(14) . .
C106 C46 C45 135.4(13) . .
C106 C46 C58 105.7(13) . .
C45 C46 C58 100.4(12) . .
C106 C46 C101 116.8(14) . .
C45 C46 C101 25.7(9) . .
C58 C46 C101 126.1(12) . .
C106 C46 C47 21.3(12) . .
C45 C46 C47 123.8(14) . .
C58 C46 C47 126.7(12) . .
C101 C46 C47 100.5(13) . .
C106 C47 C129 112(5) . .
C106 C47 C29 128(4) . .
C129 C47 C29 30.4(18) . .
C106 C47 C48 51(4) . .
C129 C47 C48 77(2) . .
C29 C47 C48 106(2) . .
C106 C47 C46 60(4) . .
C129 C47 C46 137(2) . .
C29 C47 C46 117.3(19) . .
C48 C47 C46 111.0(18) . .
C106 C47 C49 25(3) . .
C129 C47 C49 102(2) . .
C29 C47 C49 128(2) . .
C48 C47 C49 28.6(9) . .
C46 C47 C49 83.4(15) . .
C49 C48 C106 75(2) . .
C49 C48 C111 67(2) . .
C106 C48 C111 136(2) . .
C49 C48 C31 148(3) . .
C106 C48 C31 118.5(19) . .
C111 C48 C31 86.5(19) . .
C49 C48 C145 27.5(19) . .
C106 C48 C145 99.7(19) . .
C111 C48 C145 39.8(11) . .
C31 C48 C145 123.5(17) . .
C49 C48 C47 94(3) . .
C106 C48 C47 20.6(14) . .
C111 C48 C47 156(2) . .
C31 C48 C47 104.4(17) . .
C145 C48 C47 120.1(19) . .
C49 C48 C129 128(3) . .
C106 C48 C129 55.4(16) . .
C111 C48 C129 143.1(19) . .
C31 C48 C129 64.9(16) . .
C145 C48 C129 144.8(15) . .
C47 C48 C129 39.6(11) . .
C49 C48 C126 123(3) . .
C106 C48 C126 135.9(16) . .
C111 C48 C126 59.6(15) . .
C31 C48 C126 26.9(10) . .
C145 C48 C126 97.0(14) . .
C47 C48 C126 127.9(16) . .
C129 C48 C126 89.0(15) . .
C49 C48 C122 149(2) . .
C106 C48 C122 98.0(16) . .
C111 C48 C122 102.5(18) . .
C31 C48 C122 20.6(11) . .
C145 C48 C122 133.5(14) . .
C47 C48 C122 84.7(14) . .
C129 C48 C122 45.2(12) . .
C126 C48 C122 44.1(11) . .
C145 C49 C48 123(4) . .
C145 C49 C111 51(2) . .
C48 C49 C111 72(2) . .
C145 C49 C106 156(3) . .
C48 C49 C106 66(2) . .
C111 C49 C106 132(3) . .
C145 C49 C59 59(2) . .
C48 C49 C59 165(2) . .
C111 C49 C59 108(3) . .
C106 C49 C59 107.2(18) . .
C145 C49 C47 164(2) . .
C48 C49 C47 57(2) . .
C111 C49 C47 127(3) . .
C106 C49 C47 10.4(14) . .
C59 C49 C47 117.0(17) . .
C102 C50 C111 165(3) . .
C102 C50 C33 87(3) . .
C111 C50 C33 89(2) . .
C102 C50 C145 133(3) . .
C111 C50 C145 43.4(15) . .
C33 C50 C145 128(2) . .
C102 C50 C127 56(2) . .
C111 C50 C127 118(2) . .
C33 C50 C127 30.5(11) . .
C145 C50 C127 148.8(15) . .
C102 C50 C51 39(2) . .
C111 C50 C51 136.1(19) . .
C33 C50 C51 120.2(18) . .
C145 C50 C51 94.8(12) . .
C127 C50 C51 91.1(15) . .
C102 C51 C113 101.7(18) . .
C102 C51 C60 124.0(15) . .
C113 C51 C60 124.1(15) . .
C102 C51 C53 119.3(16) . .
C113 C51 C53 18.5(14) . .
C60 C51 C53 106.2(13) . .
C102 C51 C50 19.9(11) . .
C113 C51 C50 119.2(16) . .
C60 C51 C50 104.3(11) . .
C53 C51 C50 135.1(13) . .
C14 C52 C13 122(4) . .
C14 C52 C144 134(4) . .
C13 C52 C144 19.8(17) . .
C14 C52 C143 56(3) . .
C13 C52 C143 99(2) . .
C144 C52 C143 119(2) . .
C14 C52 C15 36(3) . .
C13 C52 C15 108.8(19) . .
C144 C52 C15 128.0(18) . .
C143 C52 C15 19.8(11) . .
C14 C52 C4 64(3) . .
C13 C52 C4 127.8(17) . .
C144 C52 C4 114.0(15) . .
C143 C52 C4 117.2(17) . .
C15 C52 C4 98.6(13) . .
C113 C53 C141 160(5) . .
C113 C53 C124 86(5) . .
C141 C53 C124 81(3) . .
C113 C53 C109 59(4) . .
C141 C53 C109 106(3) . .
C124 C53 C109 27(2) . .
C113 C53 C51 41(4) . .
C141 C53 C51 144(3) . .
C124 C53 C51 125(3) . .
C109 C53 C51 98(2) . .
C113 C53 C54 140(4) . .
C141 C53 C54 43.6(17) . .
C124 C53 C54 122(3) . .
C109 C53 C54 139(2) . .
C51 C53 C54 101.4(14) . .
C134 C54 C141 77.8(17) . .
C134 C54 C55 136.8(18) . .
C141 C54 C55 139.1(17) . .
C134 C54 C53 111.2(18) . .
C141 C54 C53 34.9(12) . .
C55 C54 C53 104.6(13) . .
C134 C54 C40 41.1(13) . .
C141 C54 C40 116.2(16) . .
C55 C54 C40 95.8(12) . .
C53 C54 C40 143.0(13) . .
C56 C55 C54 115.0(11) . .
C56 C55 C60 117.5(11) . .
C54 C55 C60 115.0(10) . .
C55 C56 C57 120.8(10) . .
C55 C56 C41 108.3(12) . .
C57 C56 C41 118.7(12) . .
C55 C56 C146 122.6(14) . .
C57 C56 C146 99.5(14) . .
C41 C56 C146 19.2(14) . .
C58 C57 C44 116.0(12) . .
C58 C57 C56 118.4(10) . .
C44 C57 C56 113.3(11) . .
C59 C58 C57 123.5(12) . .
C59 C58 C46 112.4(10) . .
C57 C58 C46 112.1(10) . .
C58 C59 C145 128.8(13) . .
C58 C59 C60 116.9(11) . .
C145 C59 C60 100.3(12) . .
C58 C59 C49 100.4(13) . .
C145 C59 C49 30.0(9) . .
C60 C59 C49 127.8(12) . .
C55 C60 C51 112.6(11) . .
C55 C60 C59 122.8(10) . .
C51 C60 C59 113.7(11) . .
C1 C61 Si 121.9(6) . .
C69 C64 C65 117.3(9) . .
C69 C64 Si 123.2(8) . .
C65 C64 Si 119.5(9) . .
O C65 C66 122.0(12) . .
O C65 C64 115.9(10) . .
C66 C65 C64 122.0(11) . .
C65 C66 C67 116.8(11) . .
C68 C67 C66 121.7(10) . .
C69 C68 C67 120.5(11) . .
C68 C69 C64 121.6(10) . .
O C70 C71 104.9(10) . .
C76 C71 C72 107.8(14) . .
C76 C71 C70 111.0(13) . .
C72 C71 C70 121.1(12) . .
C71 C72 C73 113.3(14) . .
C73 C74 C75 96.8(16) . .
C74 C73 C72 124.3(16) . .
C77 C76 C71 114.9(18) . .
Cl2 C78 Cl3 114.3(6) . .
Cl2 C78 Cl1 109.7(6) . .
Cl3 C78 Cl1 108.1(5) . .
C45 C101 C27 112(4) . .
C45 C101 C123 140(4) . .
C27 C101 C123 33.8(15) . .
C45 C101 C46 69(3) . .
C27 C101 C46 140(2) . .
C123 C101 C46 120.4(17) . .
C45 C101 C132 48(3) . .
C27 C101 C132 70.8(19) . .
C123 C101 C132 104.6(19) . .
C46 C101 C132 115.9(17) . .
C45 C101 C28 140(3) . .
C27 C101 C28 44.4(17) . .
C123 C101 C28 13.2(12) . .
C46 C101 C28 107.2(13) . .
C132 C101 C28 113.6(16) . .
C50 C102 C51 121(3) . .
C50 C102 C127 99(3) . .
C51 C102 C127 131(2) . .
C50 C102 C33 66(3) . .
C51 C102 C33 153.3(16) . .
C127 C102 C33 32.6(11) . .
C50 C102 C111 9.2(19) . .
C51 C102 C111 119.1(16) . .
C127 C102 C111 95.7(18) . .
C33 C102 C111 63.7(14) . .
C50 C102 C145 32(2) . .
C51 C102 C145 89.9(13) . .
C127 C102 C145 122.5(18) . .
C33 C102 C145 92.2(15) . .
C111 C102 C145 29.8(8) . .
C50 C102 C113 152(3) . .
C51 C102 C113 39.2(10) . .
C127 C102 C113 92.3(17) . .
C33 C102 C113 121.8(16) . .
C111 C102 C113 144.9(13) . .
C145 C102 C113 122.7(14) . .
C26 C103 C25 118(7) . .
C26 C103 C117 130(6) . .
C25 C103 C117 15(4) . .
C26 C103 C108 16(4) . .
C25 C103 C108 133(6) . .
C117 C103 C108 146(3) . .
C26 C103 C132 119(6) . .
C25 C103 C132 96(5) . .
C117 C103 C132 82(3) . .
C108 C103 C132 115(3) . .
C26 C103 C27 62(5) . .
C25 C103 C27 141(5) . .
C117 C103 C27 134(3) . .
C108 C103 C27 55.5(17) . .
C132 C103 C27 59.8(17) . .
C26 C103 C121 104(5) . .
C25 C103 C121 17(4) . .
C117 C103 C121 31.6(17) . .
C108 C103 C121 118(2) . .
C132 C103 C121 112(3) . .
C27 C103 C121 144(2) . .
C26 C103 C10 25(4) . .
C25 C103 C10 95(5) . .
C117 C103 C10 109(2) . .
C108 C103 C10 38.3(13) . .
C132 C103 C10 137(2) . .
C27 C103 C10 86(2) . .
C121 C103 C10 79.6(16) . .
C26 C103 C43 139(6) . .
C25 C103 C43 52(4) . .
C117 C103 C43 38.0(17) . .
C108 C103 C43 149(2) . .
C132 C103 C43 44.5(13) . .
C27 C103 C43 100(2) . .
C121 C103 C43 68.4(17) . .
C10 C103 C43 133.5(19) . .
C17 C104 C16 76(3) . .
C17 C104 C112 121(3) . .
C16 C104 C112 45.7(19) . .
C17 C104 C5 86(2) . .
C16 C104 C5 156(3) . .
C112 C104 C5 148(2) . .
C17 C104 C15 149(3) . .
C16 C104 C15 76(2) . .
C112 C104 C15 31.6(17) . .
C5 C104 C15 116.9(15) . .
C17 C104 C105 34.3(17) . .
C16 C104 C105 42.8(19) . .
C112 C104 C105 88(2) . .
C5 C104 C105 115.5(17) . .
C15 C104 C105 115.0(16) . .
C17 C104 C14 158(2) . .
C16 C104 C14 113(3) . .
C112 C104 C14 69(2) . .
C5 C104 C14 79.5(10) . .
C15 C104 C14 37.7(9) . .
C105 C104 C14 143.8(13) . .
C17 C104 C18 17.9(16) . .
C16 C104 C18 72(2) . .
C112 C104 C18 115(2) . .
C5 C104 C18 86.0(12) . .
C15 C104 C18 135.4(13) . .
C105 C104 C18 29.5(9) . .
C14 C104 C18 142.4(10) . .
C18 C105 C17 78(2) . .
C18 C105 C16 137(3) . .
C17 C105 C16 63(2) . .
C18 C105 C139 23(2) . .
C17 C105 C139 101(3) . .
C16 C105 C139 158(3) . .
C18 C105 C140 66(2) . .
C17 C105 C140 142(2) . .
C16 C105 C140 141(2) . .
C139 C105 C140 45.7(13) . .
C18 C105 C35 123(3) . .
C17 C105 C35 146(3) . .
C16 C105 C35 86(2) . .
C139 C105 C35 104(2) . .
C140 C105 C35 58.6(16) . .
C18 C105 C104 98(2) . .
C17 C105 C104 23.2(12) . .
C16 C105 C104 40.9(16) . .
C139 C105 C104 121(2) . .
C140 C105 C104 149.8(15) . .
C35 C105 C104 123(2) . .
C18 C105 C125 143(2) . .
C17 C105 C125 122(2) . .
C16 C105 C125 60(2) . .
C139 C105 C125 128(2) . .
C140 C105 C125 83.1(16) . .
C35 C105 C125 25.5(11) . .
C104 C105 C125 98.6(19) . .
C18 C105 C112 129(2) . .
C17 C105 C112 58.3(16) . .
C16 C105 C112 8.1(16) . .
C139 C105 C112 150(2) . .
C140 C105 C112 140.0(16) . .
C35 C105 C112 89.4(19) . .
C104 C105 C112 35.3(9) . .
C125 C105 C112 64.0(16) . .
C18 C105 C109 108(2) . .
C17 C105 C109 152(2) . .
C16 C105 C109 99(2) . .
C139 C105 C109 89.0(19) . .
C140 C105 C109 43.4(13) . .
C35 C105 C109 15.7(13) . .
C104 C105 C109 132.4(18) . .
C125 C105 C109 39.7(13) . .
C112 C105 C109 101.5(16) . .
C47 C106 C48 108(4) . .
C47 C106 C49 145(5) . .
C48 C106 C49 39.4(12) . .
C47 C106 C46 99(4) . .
C48 C106 C46 153(2) . .
C49 C106 C46 114(2) . .
C47 C106 C129 46(4) . .
C48 C106 C129 77.1(18) . .
C49 C106 C129 115(2) . .
C46 C106 C129 126(2) . .
C47 C106 C29 38(3) . .
C48 C106 C29 98.4(18) . .
C49 C106 C29 135.0(19) . .
C46 C106 C29 104.6(16) . .
C129 C106 C29 21.5(14) . .
C42 C107 C43 163(4) . .
C42 C107 C146 52(2) . .
C43 C107 C146 145(3) . .
C42 C107 C23 70(3) . .
C43 C107 C23 96(2) . .
C146 C107 C23 113(3) . .
C42 C107 C44 157(3) . .
C43 C107 C44 40.2(15) . .
C146 C107 C44 105(2) . .
C23 C107 C44 130(2) . .
C42 C107 C117 119(3) . .
C43 C107 C117 46.5(18) . .
C146 C107 C117 153(2) . .
C23 C107 C117 49.2(14) . .
C44 C107 C117 83.1(18) . .
C42 C107 C142 50(2) . .
C43 C107 C142 117(2) . .
C146 C107 C142 91(2) . .
C23 C107 C142 22.4(13) . .
C44 C107 C142 146.6(14) . .
C117 C107 C142 70.9(15) . .
C42 C107 C41 52(3) . .
C43 C107 C41 145(2) . .
C146 C107 C41 0.8(18) . .
C23 C107 C41 113.3(19) . .
C44 C107 C41 104.8(10) . .
C117 C107 C41 153.8(15) . .
C142 C107 C41 91.1(14) . .
C26 C108 C10 89(3) . .
C26 C108 C138 117(3) . .
C10 C108 C138 28.3(13) . .
C26 C108 C103 12(3) . .
C10 C108 C103 99(2) . .
C138 C108 C103 128(3) . .
C26 C108 C27 75(3) . .
C10 C108 C27 138(2) . .
C138 C108 C27 138(2) . .
C103 C108 C27 71(2) . .
C26 C108 C123 106(3) . .
C10 C108 C123 132(2) . .
C138 C108 C123 115(2) . .
C103 C108 C123 103(2) . .
C27 C108 C123 31.8(12) . .
C26 C108 C11 141(3) . .
C10 C108 C11 64.9(16) . .
C138 C108 C11 40.1(13) . .
C103 C108 C11 152(2) . .
C27 C108 C11 104.1(18) . .
C123 C108 C11 76.1(18) . .
C26 C108 C28 125(3) . .
C10 C108 C28 111(2) . .
C138 C108 C28 90.8(19) . .
C103 C108 C28 125(2) . .
C27 C108 C28 55.3(14) . .
C123 C108 C28 25.1(11) . .
C11 C108 C28 51.1(13) . .
C26 C108 C25 6(2) . .
C10 C108 C25 84.5(19) . .
C138 C108 C25 113(2) . .
C103 C108 C25 15.0(17) . .
C27 C108 C25 80.9(19) . .
C123 C108 C25 112(2) . .
C11 C108 C25 139.7(16) . .
C28 C108 C25 130.3(17) . .
C124 C109 C35 136(8) . .
C124 C109 C125 162(7) . .
C35 C109 C125 26(3) . .
C124 C109 C113 84(7) . .
C35 C109 C113 139(5) . .
C125 C109 C113 112(3) . .
C124 C109 C140 57(5) . .
C35 C109 C140 82(4) . .
C125 C109 C140 105(3) . .
C113 C109 C140 132(3) . .
C124 C109 C53 61(6) . .
C35 C109 C53 160(5) . .
C125 C109 C53 134(3) . .
C113 C109 C53 23.6(16) . .
C140 C109 C53 110(3) . .
C124 C109 C120 31(5) . .
C35 C109 C120 111(4) . .
C125 C109 C120 132(2) . .
C113 C109 C120 103(3) . .
C140 C109 C120 29.5(11) . .
C53 C109 C120 81(2) . .
C124 C109 C34 166(7) . .
C35 C109 C34 33(3) . .
C125 C109 C34 7.2(13) . .
C113 C109 C34 105(2) . .
C140 C109 C34 110(3) . .
C53 C109 C34 127(2) . .
C120 C109 C34 135(2) . .
C124 C109 C105 104(6) . .
C35 C109 C105 35(3) . .
C125 C109 C105 57(2) . .
C113 C109 C105 152(2) . .
C140 C109 C105 47.8(15) . .
C53 C109 C105 148(2) . .
C120 C109 C105 76.3(14) . .
C34 C109 C105 62.4(17) . .
C124 C109 C141 37(5) . .
C35 C109 C141 158(4) . .
C125 C109 C141 152(2) . .
C113 C109 C141 51.4(19) . .
C140 C109 C141 81(2) . .
C53 C109 C141 28.2(13) . .
C120 C109 C141 52.4(14) . .
C34 C109 C141 145.4(17) . .
C105 C109 C141 124.4(17) . .
C39 C110 C131 163(5) . .
C39 C110 C38 57(3) . .
C131 C110 C38 130(3) . .
C39 C110 C118 45(3) . .
C131 C110 C118 120(3) . .
C38 C110 C118 99(3) . .
C39 C110 C142 141(4) . .
C131 C110 C142 24.1(14) . .
C38 C110 C142 146(3) . .
C118 C110 C142 96(2) . .
C39 C110 C21 118(4) . .
C131 C110 C21 70(2) . .
C38 C110 C21 61.1(17) . .
C118 C110 C21 152(3) . .
C142 C110 C21 92(2) . .
C39 C110 C40 41(3) . .
C131 C110 C40 124(3) . .
C38 C110 C40 92(2) . .
C118 C110 C40 8.5(15) . .
C142 C110 C40 100(2) . .
C21 C110 C40 144(2) . .
C145 C111 C50 87(3) . .
C145 C111 C49 41.0(17) . .
C50 C111 C49 127(3) . .
C145 C111 C48 82(2) . .
C50 C111 C48 162(2) . .
C49 C111 C48 40.8(15) . .
C145 C111 C126 149(3) . .
C50 C111 C126 108(2) . .
C49 C111 C126 114(3) . .
C48 C111 C126 76(2) . .
C145 C111 C33 135(3) . .
C50 C111 C33 53.4(16) . .
C49 C111 C33 154.4(18) . .
C48 C111 C33 130(2) . .
C126 C111 C33 54.7(14) . .
C145 C111 C102 87(2) . .
C50 C111 C102 6.0(12) . .
C49 C111 C102 126(2) . .
C48 C111 C102 157.3(18) . .
C126 C111 C102 105.4(18) . .
C33 C111 C102 51.8(13) . .
C145 C111 C31 129(3) . .
C50 C111 C31 132(2) . .
C49 C111 C31 90(2) . .
C48 C111 C31 50.9(14) . .
C126 C111 C31 25.4(10) . .
C33 C111 C31 79.9(14) . .
C102 C111 C31 129.1(15) . .
C15 C112 C16 157(4) . .
C15 C112 C104 104(3) . .
C16 C112 C104 64(2) . .
C15 C112 C143 12(2) . .
C16 C112 C143 168(3) . .
C104 C112 C143 114(3) . .
C15 C112 C130 62(2) . .
C16 C112 C130 121(3) . .
C104 C112 C130 155(2) . .
C143 C112 C130 55.8(16) . .
C15 C112 C34 115(3) . .
C16 C112 C34 67(3) . .
C104 C112 C34 128(3) . .
C143 C112 C34 110(2) . .
C130 C112 C34 54.5(14) . .
C15 C112 C17 125(3) . .
C16 C112 C17 41(2) . .
C104 C112 C17 23.2(13) . .
C143 C112 C17 136(2) . .
C130 C112 C17 151.3(19) . .
C34 C112 C17 106(2) . .
C15 C112 C14 26.9(19) . .
C16 C112 C14 137(3) . .
C104 C112 C14 76.9(19) . .
C143 C112 C14 37.6(14) . .
C130 C112 C14 88(2) . .
C34 C112 C14 137(2) . .
C17 C112 C14 98.5(15) . .
C15 C112 C125 130(3) . .
C16 C112 C125 48(3) . .
C104 C112 C125 108(3) . .
C143 C112 C125 127.6(18) . .
C130 C112 C125 72.8(15) . .
C34 C112 C125 20.2(11) . .
C17 C112 C125 86.0(19) . .
C14 C112 C125 142.7(14) . .
C15 C112 C105 147(3) . .
C16 C112 C105 11(2) . .
C104 C112 C105 57.0(18) . .
C143 C112 C105 158.9(18) . .
C130 C112 C105 123(2) . .
C34 C112 C105 72(2) . .
C17 C112 C105 34.1(9) . .
C14 C112 C105 126.5(14) . .
C125 C112 C105 52.1(15) . .
C53 C113 C51 121(5) . .
C53 C113 C109 97(5) . .
C51 C113 C109 137(3) . .
C53 C113 C124 69(4) . .
C51 C113 C124 162(3) . .
C109 C113 C124 29(2) . .
C53 C113 C141 12(3) . .
C51 C113 C141 125.0(19) . .
C109 C113 C141 88(2) . .
C124 C113 C141 61(2) . .
C53 C113 C35 111(5) . .
C51 C113 C35 122.4(19) . .
C109 C113 C35 14.5(19) . .
C124 C113 C35 43(2) . .
C141 C113 C35 101.2(17) . .
C53 C113 C102 156(4) . .
C51 C113 C102 39.1(11) . .
C109 C113 C102 98(2) . .
C124 C113 C102 127(3) . .
C141 C113 C102 152.6(15) . .
C35 C113 C102 84.0(13) . .
C12 C114 C11 108(6) . .
C12 C114 C128 41(4) . .
C11 C114 C128 68(2) . .
C12 C114 C3 85(6) . .
C11 C114 C3 163(3) . .
C128 C114 C3 123(3) . .
C12 C114 C138 154(6) . .
C11 C114 C138 45.4(15) . .
C128 C114 C138 113(3) . .
C3 C114 C138 120(2) . .
C12 C114 C10 157(6) . .
C11 C114 C10 54.5(18) . .
C128 C114 C10 118(2) . .
C3 C114 C10 109.6(16) . .
C138 C114 C10 14.8(11) . .
C12 C114 C144 18(4) . .
C11 C114 C144 98(2) . .
C128 C114 C144 31.3(15) . .
C3 C114 C144 91.6(17) . .
C138 C114 C144 141(2) . .
C10 C114 C144 139.9(17) . .
C37 C115 C38 157(3) . .
C37 C115 C120 23(2) . .
C38 C115 C120 142(2) . .
C37 C115 C39 127(3) . .
C38 C115 C39 55(2) . .
C120 C115 C39 146.9(17) . .
C37 C115 C20 130(2) . .
C38 C115 C20 38.2(17) . .
C120 C115 C20 108.1(15) . .
C39 C115 C20 92.7(17) . .
C37 C115 C134 69(2) . .
C38 C115 C134 113(2) . .
C120 C115 C134 91.3(16) . .
C39 C115 C134 60.0(13) . .
C20 C115 C134 148.3(16) . .
C19 C116 C6 141(4) . .
C19 C116 C18 91(4) . .
C6 C116 C18 118.5(18) . .
C19 C116 C119 61(3) . .
C6 C116 C119 110.7(17) . .
C18 C116 C119 125.9(19) . .
C19 C116 C139 71(3) . .
C6 C116 C139 140.0(18) . .
C18 C116 C139 21.7(13) . .
C119 C116 C139 107.1(19) . .
C19 C116 C20 45(3) . .
C6 C116 C20 128.8(15) . .
C18 C116 C20 110.9(18) . .
C119 C116 C20 19.0(12) . .
C139 C116 C20 90.4(16) . .
C25 C117 C121 81(5) . .
C25 C117 C43 115(5) . .
C121 C117 C43 154(5) . .
C25 C117 C23 148(5) . .
C121 C117 C23 74(3) . .
C43 C117 C23 83(3) . .
C25 C117 C103 14(4) . .
C121 C117 C103 95(4) . .
C43 C117 C103 102(3) . .
C23 C117 C103 158(3) . .
C25 C117 C24 106(5) . .
C121 C117 C24 28(2) . .
C43 C117 C24 128(3) . .
C23 C117 C24 46.6(15) . .
C103 C117 C24 120(3) . .
C25 C117 C107 141(5) . .
C121 C117 C107 123(4) . .
C43 C117 C107 32.5(13) . .
C23 C117 C107 50.6(17) . .
C103 C117 C107 131(3) . .
C24 C117 C107 96(2) . .
C25 C117 C26 9(3) . .
C121 C117 C26 83(3) . .
C43 C117 C26 110(3) . .
C23 C117 C26 144(3) . .
C103 C117 C26 14.6(17) . .
C24 C117 C26 107(2) . .
C107 C117 C26 133(2) . .
C25 C117 C132 66(4) . .
C121 C117 C132 142(4) . .
C43 C117 C132 50.0(17) . .
C23 C117 C132 129(3) . .
C103 C117 C132 52.5(18) . .
C24 C117 C132 153(2) . .
C107 C117 C132 80.1(18) . .
C26 C117 C132 61.0(17) . .
C25 C117 C142 141(5) . .
C121 C117 C142 68(3) . .
C43 C117 C142 88(3) . .
C23 C117 C142 7.1(14) . .
C103 C117 C142 151(2) . .
C24 C117 C142 40.8(14) . .
C107 C117 C142 55.5(16) . .
C26 C117 C142 137(2) . .
C132 C117 C142 131(2) . .
C40 C118 C39 121(6) . .
C40 C118 C41 72(6) . .
C39 C118 C41 153(3) . .
C40 C118 C134 42(5) . .
C39 C118 C134 80(2) . .
C41 C118 C134 114(3) . .
C40 C118 C110 145(6) . .
C39 C118 C110 32.4(18) . .
C41 C118 C110 124(3) . .
C134 C118 C110 110(3) . .
C40 C118 C146 87(6) . .
C39 C118 C146 136(3) . .
C41 C118 C146 18.3(14) . .
C134 C118 C146 126(3) . .
C110 C118 C146 105(2) . .
C40 C118 C22 148(6) . .
C39 C118 C22 40(2) . .
C41 C118 C22 116(2) . .
C134 C118 C22 117(2) . .
C110 C118 C22 8(2) . .
C146 C118 C22 97.6(19) . .
C20 C119 C21 104(4) . .
C20 C119 C19 87(4) . .
C21 C119 C19 167(3) . .
C20 C119 C116 108(4) . .
C21 C119 C116 147(2) . .
C19 C119 C116 23.1(12) . .
C20 C119 C38 43(3) . .
C21 C119 C38 77.5(17) . .
C19 C119 C38 116(2) . .
C116 C119 C38 125.9(18) . .
C20 C119 C36 141(4) . .
C21 C119 C36 40.4(13) . .
C19 C119 C36 126(2) . .
C116 C119 C36 109(2) . .
C38 C119 C36 117(2) . .
C37 C120 C140 154(4) . .
C37 C120 C124 117(4) . .
C140 C120 C124 59(2) . .
C37 C120 C115 32(3) . .
C140 C120 C115 138(2) . .
C124 C120 C115 145(3) . .
C37 C120 C139 132(4) . .
C140 C120 C139 40.9(16) . .
C124 C120 C139 100(3) . .
C115 C120 C139 102.1(16) . .
C37 C120 C141 59(3) . .
C140 C120 C141 114(2) . .
C124 C120 C141 58(2) . .
C115 C120 C141 89.9(17) . .
C139 C120 C141 147.7(18) . .
C37 C120 C109 123(4) . .
C140 C120 C109 46.5(19) . .
C124 C120 C109 15(2) . .
C115 C120 C109 144.9(16) . .
C139 C120 C109 86.5(19) . .
C141 C120 C109 67.7(16) . .
C24 C121 C117 122(4) . .
C24 C121 C25 157(3) . .
C117 C121 C25 43(3) . .
C24 C121 C23 53(2) . .
C117 C121 C23 69(3) . .
C25 C121 C23 110(3) . .
C24 C121 C136 71(2) . .
C117 C121 C136 154(4) . .
C25 C121 C136 116(3) . .
C23 C121 C136 120(2) . .
C24 C121 C103 161(3) . .
C117 C121 C103 54(4) . .
C25 C121 C103 11(3) . .
C23 C121 C103 120(2) . .
C136 C121 C103 106.0(19) . .
C24 C121 C8 48(2) . .
C117 C121 C8 157(3) . .
C25 C121 C8 137(3) . .
C23 C121 C8 98(2) . .
C136 C121 C8 23.1(9) . .
C103 C121 C8 127.3(18) . .
C24 C121 C26 150(3) . .
C117 C121 C26 70(3) . .
C25 C121 C26 28(2) . .
C23 C121 C26 129.9(18) . .
C136 C121 C26 88.7(17) . .
C103 C121 C26 17.6(14) . .
C8 C121 C26 109.8(15) . .
C24 C121 C142 35(2) . .
C117 C121 C142 87(3) . .
C25 C121 C142 126(2) . .
C23 C121 C142 18.4(12) . .
C136 C121 C142 102.2(19) . .
C103 C121 C142 134.8(19) . .
C8 C121 C142 79.9(15) . .
C26 C121 C142 140.0(14) . .
C30 C122 C31 155(5) . .
C30 C122 C126 176(4) . .
C31 C122 C126 28(2) . .
C30 C122 C129 68(3) . .
C31 C122 C129 95(3) . .
C126 C122 C129 117(3) . .
C30 C122 C13 60(3) . .
C31 C122 C13 144(3) . .
C126 C122 C13 116(2) . .
C129 C122 C13 118(3) . .
C30 C122 C144 47(3) . .
C31 C122 C144 157(3) . .
C126 C122 C144 129(2) . .
C129 C122 C144 106(2) . .
C13 C122 C144 13.3(15) . .
C30 C122 C32 154(3) . .
C31 C122 C32 49(2) . .
C126 C122 C32 21.7(10) . .
C129 C122 C32 137(3) . .
C13 C122 C32 94.7(17) . .
C144 C122 C32 108.0(17) . .
C30 C122 C29 48(2) . .
C31 C122 C29 117(3) . .
C126 C122 C29 136(2) . .
C129 C122 C29 21.5(15) . .
C13 C122 C29 96(2) . .
C144 C122 C29 85.0(19) . .
C32 C122 C29 152.4(17) . .
C30 C122 C48 124(3) . .
C31 C122 C48 41(2) . .
C126 C122 C48 60.8(18) . .
C129 C122 C48 56.2(16) . .
C13 C122 C48 154.8(17) . .
C144 C122 C48 154.7(16) . .
C32 C122 C48 82.0(16) . .
C29 C122 C48 77.1(14) . .
C28 C123 C27 150(5) . .
C28 C123 C101 141(4) . .
C27 C123 C101 48(2) . .
C28 C123 C133 22(3) . .
C27 C123 C133 150(3) . .
C101 C123 C133 120(2) . .
C28 C123 C108 97(3) . .
C27 C123 C108 66(3) . .
C101 C123 C108 114(3) . .
C133 C123 C108 118(3) . .
C28 C123 C26 116(3) . .
C27 C123 C26 43(2) . .
C101 C123 C26 90(2) . .
C133 C123 C26 133(2) . .
C108 C123 C26 24.3(11) . .
C28 C123 C29 43(3) . .
C27 C123 C29 136(3) . .
C101 C123 C29 98.8(16) . .
C133 C123 C29 20.8(13) . .
C108 C123 C29 135(2) . .
C26 C123 C29 142.3(16) . .
C28 C123 C11 41(3) . .
C27 C123 C11 116(3) . .
C101 C123 C11 154.3(18) . .
C133 C123 C11 62(2) . .
C108 C123 C11 55.9(14) . .
C26 C123 C11 75.3(14) . .
C29 C123 C11 81.2(19) . .
C28 C123 C45 140(3) . .
C27 C123 C45 39(2) . .
C101 C123 C45 12.4(11) . .
C133 C123 C45 121.6(18) . .
C108 C123 C45 105(2) . .
C26 C123 C45 80.9(17) . .
C29 C123 C45 101.5(15) . .
C11 C123 C45 142.2(14) . .
C109 C124 C140 94(6) . .
C109 C124 C35 22(5) . .
C140 C124 C35 74(3) . .
C109 C124 C53 92(7) . .
C140 C124 C53 144(4) . .
C35 C124 C53 113(4) . .
C109 C124 C120 134(7) . .
C140 C124 C120 44(2) . .
C35 C124 C120 116(4) . .
C53 C124 C120 112(4) . .
C109 C124 C113 67(6) . .
C140 C124 C113 145(4) . .
C35 C124 C113 89(3) . .
C53 C124 C113 25.5(18) . .
C120 C124 C113 133(4) . .
C109 C124 C141 127(7) . .
C140 C124 C141 114(4) . .
C35 C124 C141 144(3) . .
C53 C124 C141 39.9(19) . .
C120 C124 C141 74(3) . .
C113 C124 C141 65(3) . .
C109 C124 C37 141(6) . .
C140 C124 C37 62(3) . .
C35 C124 C37 130(3) . .
C53 C124 C37 92(3) . .
C120 C124 C37 20.4(15) . .
C113 C124 C37 114(3) . .
C141 C124 C37 53.3(19) . .
C109 C124 C125 12(5) . .
C140 C124 C125 82(3) . .
C35 C124 C125 11.2(14) . .
C53 C124 C125 102(3) . .
C120 C124 C125 123(3) . .
C113 C124 C125 78(2) . .
C141 C124 C125 134(3) . .
C37 C124 C125 133(3) . .
C34 C125 C35 172(5) . .
C34 C125 C127 42(3) . .
C35 C125 C127 144(3) . .
C34 C125 C109 160(4) . .
C35 C125 C109 25(2) . .
C127 C125 C109 119(2) . .
C34 C125 C16 71(3) . .
C35 C125 C16 101(4) . .
C127 C125 C16 109(3) . .
C109 C125 C16 122(3) . .
C34 C125 C105 111(3) . .
C35 C125 C105 61(3) . .
C127 C125 C105 145(2) . .
C109 C125 C105 83(2) . .
C16 C125 C105 39.9(14) . .
C34 C125 C33 33(3) . .
C35 C125 C33 151(3) . .
C127 C125 C33 12.3(14) . .
C109 C125 C33 126.6(19) . .
C16 C125 C33 97(2) . .
C105 C125 C33 132.6(16) . .
C34 C125 C112 47(3) . .
C35 C125 C112 125(3) . .
C127 C125 C112 84(2) . .
C109 C125 C112 141(2) . .
C16 C125 C112 24.7(14) . .
C105 C125 C112 63.8(12) . .
C33 C125 C112 72.3(15) . .
C34 C125 C124 164(3) . .
C35 C125 C124 20(3) . .
C127 C125 C124 125(2) . .
C109 C125 C124 6(2) . .
C16 C125 C124 116(3) . .
C105 C125 C124 77(2) . .
C33 C125 C124 131.4(18) . .
C112 C125 C124 135.9(19) . .
C32 C126 C31 138(4) . .
C32 C126 C122 114(3) . .
C31 C126 C122 27.5(18) . .
C32 C126 C130 18(2) . .
C31 C126 C130 149(3) . .
C122 C126 C130 122(2) . .
C32 C126 C33 56(3) . .
C31 C126 C33 164(3) . .
C122 C126 C33 153.7(19) . .
C130 C126 C33 41.5(11) . .
C32 C126 C111 123(3) . .
C31 C126 C111 98(3) . .
C122 C126 C111 118(2) . .
C130 C126 C111 107.7(18) . .
C33 C126 C111 67.2(16) . .
C32 C126 C48 165(3) . .
C31 C126 C48 54(2) . .
C122 C126 C48 75.1(19) . .
C130 C126 C48 146.8(17) . .
C33 C126 C48 110.4(17) . .
C111 C126 C48 44.1(12) . .
C32 C126 C143 31(2) . .
C31 C126 C143 109(3) . .
C122 C126 C143 82.8(14) . .
C130 C126 C143 40.7(12) . .
C33 C126 C143 82.0(17) . .
C111 C126 C143 144.5(19) . .
C48 C126 C143 151.0(14) . .
C33 C127 C34 118(4) . .
C33 C127 C125 149(3) . .
C34 C127 C125 36(2) . .
C33 C127 C102 84(3) . .
C34 C127 C102 154(4) . .
C125 C127 C102 118(2) . .
C33 C127 C130 47(2) . .
C34 C127 C130 71(3) . .
C125 C127 C130 103(2) . .
C102 C127 C130 128(2) . .
C33 C127 C50 59(2) . .
C34 C127 C50 165(3) . .
C125 C127 C50 140(2) . .
C102 C127 C50 24.9(11) . .
C130 C127 C50 103(2) . .
C33 C127 C35 155(3) . .
C34 C127 C35 50(3) . .
C125 C127 C35 13.4(14) . .
C102 C127 C35 104.5(18) . .
C130 C127 C35 114.4(18) . .
C50 C127 C35 126.5(17) . .
C33 C127 C32 26(2) . .
C34 C127 C32 92(3) . .
C125 C127 C32 124(2) . .
C102 C127 C32 106.5(19) . .
C130 C127 C32 21.8(10) . .
C50 C127 C32 82.0(15) . .
C35 C127 C32 132.9(15) . .
C12 C128 C144 94(3) . .
C12 C128 C114 22(2) . .
C144 C128 C114 114(3) . .
C12 C128 C11 72(2) . .
C144 C128 C11 160(3) . .
C114 C128 C11 50.7(15) . .
C12 C128 C13 97(3) . .
C144 C128 C13 12.2(18) . .
C114 C128 C13 114(2) . .
C11 C128 C13 151.4(19) . .
C12 C128 C133 142(3) . .
C144 C128 C133 114(3) . .
C114 C128 C133 121(3) . .
C11 C128 C133 73(2) . .
C13 C128 C133 106(2) . .
C12 C128 C30 140(3) . .
C144 C128 C30 50.1(18) . .
C114 C128 C30 152(2) . .
C11 C128 C30 136(2) . .
C13 C128 C30 44.3(11) . .
C133 C128 C30 64.8(18) . .
C12 C128 C28 119(3) . .
C144 C128 C28 135(2) . .
C114 C128 C28 98(2) . .
C11 C128 C28 49.5(14) . .
C13 C128 C28 124.9(17) . .
C133 C128 C28 23.8(13) . .
C30 C128 C28 87.4(15) . .
C12 C128 C29 152(3) . .
C144 C128 C29 94(2) . .
C114 C128 C29 136(2) . .
C11 C128 C29 93(2) . .
C13 C128 C29 85.5(16) . .
C133 C128 C29 20.8(13) . .
C30 C128 C29 44.2(12) . .
C28 C128 C29 43.4(13) . .
C29 C129 C47 102(4) . .
C29 C129 C30 83(4) . .
C47 C129 C30 175(4) . .
C29 C129 C106 115(4) . .
C47 C129 C106 22.1(17) . .
C30 C129 C106 153(3) . .
C29 C129 C122 114(5) . .
C47 C129 C122 142(3) . .
C30 C129 C122 32.4(14) . .
C106 C129 C122 122(3) . .
C29 C129 C133 10(3) . .
C47 C129 C133 106(3) . .
C30 C129 C133 78(2) . .
C106 C129 C133 116(2) . .
C122 C129 C133 107(2) . .
C29 C129 C48 161(4) . .
C47 C129 C48 64(2) . .
C30 C129 C48 111(2) . .
C106 C129 C48 47.4(13) . .
C122 C129 C48 79(2) . .
C133 C129 C48 157.0(19) . .
C29 C129 C31 142(5) . .
C47 C129 C31 115(3) . .
C30 C129 C31 59.4(17) . .
C106 C129 C31 98(2) . .
C122 C129 C31 27.8(12) . .
C133 C129 C31 134(2) . .
C48 C129 C31 51.6(12) . .
C32 C130 C33 83(3) . .
C32 C130 C15 104(3) . .
C33 C130 C15 157(2) . .
C32 C130 C143 82(3) . .
C33 C130 C143 162(3) . .
C15 C130 C143 24.7(14) . .
C32 C130 C34 151(3) . .
C33 C130 C34 68(2) . .
C15 C130 C34 101(2) . .
C143 C130 C34 125(2) . .
C32 C130 C127 117(3) . .
C33 C130 C127 34.1(14) . .
C15 C130 C127 131(2) . .
C143 C130 C127 156(2) . .
C34 C130 C127 34.1(12) . .
C32 C130 C112 139(3) . .
C33 C130 C112 133(3) . .
C15 C130 C112 35.1(12) . .
C143 C130 C112 58.3(17) . .
C34 C130 C112 66.6(19) . .
C127 C130 C112 100(2) . .
C32 C130 C126 16.5(19) . .
C33 C130 C126 70.7(19) . .
C15 C130 C126 111(2) . .
C143 C130 C126 93(2) . .
C34 C130 C126 136(2) . .
C127 C130 C126 103.1(18) . .
C112 C130 C126 144(2) . .
C142 C131 C22 129(5) . .
C142 C131 C110 115(4) . .
C22 C131 C110 14(3) . .
C142 C131 C23 14(3) . .
C22 C131 C23 139(4) . .
C110 C131 C23 125(3) . .
C142 C131 C137 118(4) . .
C22 C131 C137 107(4) . .
C110 C131 C137 118(3) . .
C23 C131 C137 104(2) . .
C142 C131 C24 55(3) . .
C22 C131 C24 159(4) . .
C110 C131 C24 154(2) . .
C23 C131 C24 41.5(11) . .
C137 C131 C24 62.8(15) . .
C142 C131 C21 156(3) . .
C22 C131 C21 56(3) . .
C110 C131 C21 68(2) . .
C23 C131 C21 145.4(18) . .
C137 C131 C21 50.5(14) . .
C24 C131 C21 111.1(17) . .
C45 C132 C44 85.3(18) . .
C45 C132 C43 131(2) . .
C44 C132 C43 49.5(11) . .
C45 C132 C103 124(2) . .
C44 C132 C103 136(2) . .
C43 C132 C103 89(2) . .
C45 C132 C101 24.6(13) . .
C44 C132 C101 109.9(18) . .
C43 C132 C101 152.7(18) . .
C103 C132 C101 103(2) . .
C45 C132 C27 62.3(15) . .
C44 C132 C27 139.6(17) . .
C43 C132 C27 140.8(17) . .
C103 C132 C27 62.8(18) . .
C101 C132 C27 40.3(10) . .
C45 C132 C25 139(2) . .
C44 C132 C25 113.0(19) . .
C43 C132 C25 65.8(16) . .
C103 C132 C25 22.9(18) . .
C101 C132 C25 122.3(19) . .
C27 C132 C25 82.5(18) . .
C45 C132 C26 108.5(18) . .
C44 C132 C26 140.0(16) . .
C43 C132 C26 99.3(16) . .
C103 C132 C26 16.0(18) . .
C101 C132 C26 88.2(15) . .
C27 C132 C26 48.0(13) . .
C25 C132 C26 34.8(14) . .
C45 C132 C117 148.5(18) . .
C44 C132 C117 91.8(17) . .
C43 C132 C117 43.5(13) . .
C103 C132 C117 45.1(18) . .
C101 C132 C117 141.4(18) . .
C27 C132 C117 103.4(18) . .
C25 C132 C117 22.3(13) . .
C26 C132 C117 56.7(15) . .
C29 C133 C28 140(6) . .
C29 C133 C123 119(4) . .
C28 C133 C123 21(3) . .
C29 C133 C129 9(3) . .
C28 C133 C129 139(4) . .
C123 C133 C129 120(2) . .
C29 C133 C128 112(4) . .
C28 C133 C128 99(4) . .
C123 C133 C128 119(3) . .
C129 C133 C128 105(2) . .
C29 C133 C11 152(4) . .
C28 C133 C11 53(4) . .
C123 C133 C11 73(2) . .
C129 C133 C11 142.9(19) . .
C128 C133 C11 46.7(13) . .
C29 C133 C30 52(3) . .
C28 C133 C30 153(4) . .
C123 C133 C30 155.6(19) . .
C129 C133 C30 46.6(15) . .
C128 C133 C30 60.2(15) . .
C11 C133 C30 105.9(16) . .
C40 C134 C54 96(2) . .
C40 C134 C118 18(2) . .
C54 C134 C118 114(3) . .
C40 C134 C141 143(3) . .
C54 C134 C141 52.0(13) . .
C118 C134 C141 154(2) . .
C40 C134 C37 138(3) . .
C54 C134 C37 106(2) . .
C118 C134 C37 124(2) . .
C141 C134 C37 55.7(14) . .
C40 C134 C39 60(2) . .
C54 C134 C39 146(2) . .
C118 C134 C39 41.6(13) . .
C141 C134 C39 136(2) . .
C37 C134 C39 84.0(18) . .
C40 C134 C115 112(2) . .
C54 C134 C115 133.3(19) . .
C118 C134 C115 94.9(18) . .
C141 C134 C115 86.3(16) . .
C37 C134 C115 30.8(10) . .
C39 C134 C115 53.8(13) . .
C9 C135 C10 126(5) . .
C9 C135 C138 149(5) . .
C10 C135 C138 28.4(15) . .
C9 C135 C136 42(3) . .
C10 C135 C136 92(2) . .
C138 C135 C136 120(2) . .
C9 C135 C2 66(4) . .
C10 C135 C2 135(2) . .
C138 C135 C2 117.6(19) . .
C136 C135 C2 108.1(19) . .
C9 C135 C8 25(4) . .
C10 C135 C8 106(2) . .
C138 C135 C8 134(2) . .
C136 C135 C8 16.9(10) . .
C2 C135 C8 91.5(13) . .
C8 C136 C9 108(3) . .
C8 C136 C24 68(2) . .
C9 C136 C24 159(2) . .
C8 C136 C135 126(3) . .
C9 C136 C135 18.5(15) . .
C24 C136 C135 156.6(19) . .
C8 C136 C121 101(3) . .
C9 C136 C121 144(2) . .
C24 C136 C121 32.1(10) . .
C135 C136 C121 129(2) . .
C8 C136 C137 10.0(19) . .
C9 C136 C137 111(2) . .
C24 C136 C137 61.9(13) . .
C135 C136 C137 130(2) . .
C121 C136 C137 93.6(16) . .
C8 C136 C10 153(3) . .
C9 C136 C10 53.1(15) . .
C24 C136 C10 121.5(16) . .
C135 C136 C10 36.7(11) . .
C121 C136 C10 92.2(16) . .
C137 C136 C10 148.8(13) . .
C8 C136 C7 29(2) . .
C9 C136 C7 80.0(17) . .
C24 C136 C7 92.2(15) . .
C135 C136 C7 98.5(18) . .
C121 C136 C7 122.6(16) . .
C137 C136 C7 31.4(8) . .
C10 C136 C7 126.1(13) . .
C7 C137 C8 88(2) . .
C7 C137 C36 32.3(16) . .
C8 C137 C36 119(3) . .
C7 C137 C21 73.0(18) . .
C8 C137 C21 153(2) . .
C36 C137 C21 40.9(14) . .
C7 C137 C131 144(2) . .
C8 C137 C131 115(2) . .
C36 C137 C131 115(3) . .
C21 C137 C131 75(2) . .
C7 C137 C24 137(2) . .
C8 C137 C24 53.3(14) . .
C36 C137 C24 155.5(17) . .
C21 C137 C24 134.0(19) . .
C131 C137 C24 62.6(16) . .
C7 C137 C136 90(2) . .
C8 C137 C136 6.3(12) . .
C36 C137 C136 120(2) . .
C21 C137 C136 150.1(16) . .
C131 C137 C136 110.3(19) . .
C24 C137 C136 49.1(11) . .
C7 C137 C22 121(2) . .
C8 C137 C22 136(2) . .
C36 C137 C22 91(2) . .
C21 C137 C22 50.4(14) . .
C131 C137 C22 24.6(14) . .
C24 C137 C22 85.9(16) . .
C136 C137 C22 130.1(16) . .
C7 C137 C142 151.3(18) . .
C8 C137 C142 95.1(17) . .
C36 C137 C142 131(2) . .
C21 C137 C142 93.4(18) . .
C131 C137 C142 20.2(13) . .
C24 C137 C142 42.6(11) . .
C136 C137 C142 90.2(14) . .
C22 C137 C142 43.6(15) . .
C10 C138 C11 136(4) . .
C10 C138 C135 52(3) . .
C11 C138 C135 142(2) . .
C10 C138 C108 67(3) . .
C11 C138 C108 86(2) . .
C135 C138 C108 119(3) . .
C10 C138 C114 129(4) . .
C11 C138 C114 49.4(15) . .
C135 C138 C114 94(2) . .
C108 C138 C114 131(2) . .
C10 C138 C9 47(3) . .
C11 C138 C9 139(2) . .
C135 C138 C9 8.4(13) . .
C108 C138 C9 114(2) . .
C114 C138 C9 94.4(16) . .
C10 C138 C26 44(3) . .
C11 C138 C26 103(2) . .
C135 C138 C26 97(2) . .
C108 C138 C26 22.7(13) . .
C114 C138 C26 136.4(18) . .
C9 C138 C26 91.0(15) . .
C10 C138 C12 132(3) . .
C11 C138 C12 42.6(16) . .
C135 C138 C12 100.9(18) . .
C108 C138 C12 124.5(19) . .
C114 C138 C12 6.9(16) . .
C9 C138 C12 100.6(13) . .
C26 C138 C12 132.4(15) . .
C18 C139 C140 114(5) . .
C18 C139 C105 45(4) . .
C140 C139 C105 75(2) . .
C18 C139 C19 82(5) . .
C140 C139 C19 141(3) . .
C105 C139 C19 127(3) . .
C18 C139 C116 63(4) . .
C140 C139 C116 139(2) . .
C105 C139 C116 106(2) . .
C19 C139 C116 21.3(10) . .
C18 C139 C120 137(5) . .
C140 C139 C120 33.8(13) . .
C105 C139 C120 108(2) . .
C19 C139 C120 110(2) . .
C116 C139 C120 118.8(19) . .
C18 C139 C17 12(4) . .
C140 C139 C17 108(2) . .
C105 C139 C17 34.9(12) . .
C19 C139 C17 93.0(19) . .
C116 C139 C17 73.7(15) . .
C120 C139 C17 136.3(19) . .
C120 C140 C139 105(2) . .
C120 C140 C124 77(3) . .
C139 C140 C124 175(3) . .
C120 C140 C109 104(3) . .
C139 C140 C109 147(3) . .
C124 C140 C109 29(2) . .
C120 C140 C18 121(2) . .
C139 C140 C18 21.2(16) . .
C124 C140 C18 154(3) . .
C109 C140 C18 126(2) . .
C120 C140 C35 132(2) . .
C139 C140 C35 120(2) . .
C124 C140 C35 57(3) . .
C109 C140 C35 28.4(14) . .
C18 C140 C35 100.0(17) . .
C120 C140 C105 159(2) . .
C139 C140 C105 59.0(18) . .
C124 C140 C105 118(3) . .
C109 C140 C105 89(2) . .
C18 C140 C105 40.1(10) . .
C35 C140 C105 60.8(15) . .
C120 C140 C37 10.8(17) . .
C139 C140 C37 104(2) . .
C124 C140 C37 77(3) . .
C109 C140 C37 101(2) . .
C18 C140 C37 117.4(17) . .
C35 C140 C37 128.2(18) . .
C105 C140 C37 150.8(17) . .
C53 C141 C54 102(2) . .
C53 C141 C134 148(3) . .
C54 C141 C134 50.3(13) . .
C53 C141 C37 127(3) . .
C54 C141 C37 117(2) . .
C134 C141 C37 69.4(17) . .
C53 C141 C124 59(3) . .
C54 C141 C124 153(3) . .
C134 C141 C124 139(3) . .
C37 C141 C124 72(2) . .
C53 C141 C113 8(2) . .
C54 C141 C113 104.0(18) . .
C134 C141 C113 146.7(18) . .
C37 C141 C113 120.8(19) . .
C124 C141 C113 54(2) . .
C53 C141 C120 106(2) . .
C54 C141 C120 138.1(19) . .
C134 C141 C120 92.6(17) . .
C37 C141 C120 23.3(12) . .
C124 C141 C120 48(2) . .
C113 C141 C120 99.9(16) . .
C53 C141 C109 46(2) . .
C54 C141 C109 137.4(18) . .
C134 C141 C109 142.9(17) . .
C37 C141 C109 82.1(18) . .
C124 C141 C109 16(2) . .
C113 C141 C109 40.2(11) . .
C120 C141 C109 59.9(14) . .
C23 C142 C131 151(5) . .
C23 C142 C24 55(2) . .
C131 C142 C24 97(3) . .
C23 C142 C22 162(3) . .
C131 C142 C22 27(3) . .
C24 C142 C22 121(3) . .
C23 C142 C42 64(3) . .
C131 C142 C42 140(4) . .
C24 C142 C42 118(3) . .
C22 C142 C42 114(2) . .
C23 C142 C110 154(3) . .
C131 C142 C110 41(3) . .
C24 C142 C110 132(3) . .
C22 C142 C110 14.7(18) . .
C42 C142 C110 99.0(19) . .
C23 C142 C107 45(3) . .
C131 C142 C107 153(3) . .
C24 C142 C107 98(2) . .
C22 C142 C107 128(2) . .
C42 C142 C107 20.8(10) . .
C110 C142 C107 114.0(19) . .
C23 C142 C121 36(2) . .
C131 C142 C121 115(3) . .
C24 C142 C121 19.5(11) . .
C22 C142 C121 136(2) . .
C42 C142 C121 99(2) . .
C110 C142 C121 144.5(19) . .
C107 C142 C121 78.2(16) . .
C23 C142 C137 109(3) . .
C131 C142 C137 42(3) . .
C24 C142 C137 55.0(14) . .
C22 C142 C137 66(2) . .
C42 C142 C137 157.7(16) . .
C110 C142 C137 79(2) . .
C107 C142 C137 142.1(16) . .
C121 C142 C137 73.1(13) . .
C23 C142 C117 13(3) . .
C131 C142 C117 139(4) . .
C24 C142 C117 44.4(15) . .
C22 C142 C117 152.3(18) . .
C42 C142 C117 73.8(19) . .
C110 C142 C117 150.5(18) . .
C107 C142 C117 53.6(15) . .
C121 C142 C117 24.9(10) . .
C137 C142 C117 97.0(16) . .
C15 C143 C14 80(4) . .
C15 C143 C130 76(4) . .
C14 C143 C130 141(2) . .
C15 C143 C112 19(3) . .
C14 C143 C112 97(2) . .
C130 C143 C112 65.9(16) . .
C15 C143 C52 103(4) . .
C14 C143 C52 22.7(12) . .
C130 C143 C52 149(2) . .
C112 C143 C52 120(2) . .
C15 C143 C32 105(4) . .
C14 C143 C32 134(2) . .
C130 C143 C32 33.4(11) . .
C112 C143 C32 98.8(17) . .
C52 C143 C32 125(2) . .
C15 C143 C13 118(4) . .
C14 C143 C13 50.7(14) . .
C130 C143 C13 117.3(17) . .
C112 C143 C13 136.3(19) . .
C52 C143 C13 35.1(10) . .
C32 C143 C13 89.7(16) . .
C15 C143 C126 111(4) . .
C14 C143 C126 119.9(17) . .
C130 C143 C126 46.6(14) . .
C112 C143 C126 109.1(16) . .
C52 C143 C126 109.6(16) . .
C32 C143 C126 15.3(11) . .
C13 C143 C126 74.4(12) . .
C128 C144 C30 87(3) . .
C128 C144 C52 141(3) . .
C30 C144 C52 123(2) . .
C128 C144 C12 37.6(15) . .
C30 C144 C12 123(2) . .
C52 C144 C12 104(2) . .
C128 C144 C122 107(2) . .
C30 C144 C122 25.1(12) . .
C52 C144 C122 98.6(19) . .
C12 C144 C122 135(2) . .
C128 C144 C14 133(2) . .
C30 C144 C14 119(2) . .
C52 C144 C14 13.1(10) . .
C12 C144 C14 99.5(17) . .
C122 C144 C14 93.9(15) . .
C128 C144 C114 35.0(19) . .
C30 C144 C114 118(2) . .
C52 C144 C114 105.8(18) . .
C12 C144 C114 6.1(14) . .
C122 C144 C114 128.9(17) . .
C14 C144 C114 99.9(15) . .
C49 C145 C111 88(3) . .
C49 C145 C59 91(3) . .
C111 C145 C59 166(2) . .
C49 C145 C50 136(3) . .
C111 C145 C50 49.3(18) . .
C59 C145 C50 126.9(17) . .
C49 C145 C48 30(2) . .
C111 C145 C48 58.4(19) . .
C59 C145 C48 119.8(17) . .
C50 C145 C48 106.6(16) . .
C49 C145 C102 147(3) . .
C111 C145 C102 63(2) . .
C59 C145 C102 112.0(13) . .
C50 C145 C102 15.0(11) . .
C48 C145 C102 118.9(15) . .
C41 C146 C42 148(7) . .
C41 C146 C107 177(6) . .
C42 C146 C107 31.7(15) . .
C41 C146 C56 63(5) . .
C42 C146 C56 149(3) . .
C107 C146 C56 117(3) . .
C41 C146 C118 49(4) . .
C42 C146 C118 106(3) . .
C107 C146 C118 132(3) . .
C56 C146 C118 103(2) . .
C41 C146 C40 35(4) . .
C42 C146 C40 124(3) . .
C107 C146 C40 146(3) . .
C56 C146 C40 84.7(18) . .
C118 C146 C40 18.5(13) . .
C206 C202 C208 120(6) 1_455 .
C206 C202 C209 143(4) 1_455 1_455
C208 C202 C209 73(4) . 1_455
C206 C202 C207 88(4) 1_455 1_455
C208 C202 C207 74(4) . 1_455
C209 C202 C207 61(2) 1_455 1_455
C202 C206 C208 32(3) 1_655 1_655
C209 C207 C208 46.8(19) . 1_655
C209 C207 C202 45.8(17) . 1_655
C208 C207 C202 26.8(13) 1_655 1_655
C202 C208 C206 28(3) . 1_455
C202 C208 C209 71(4) . 1_455
C206 C208 C209 93(3) 1_455 1_455
C202 C208 C203 160(4) . .
C206 C208 C203 153(3) 1_455 .
C209 C208 C203 113(3) 1_455 .
C202 C208 C207 79(4) . 1_455
C206 C208 C207 75(2) 1_455 1_455
C209 C208 C207 62(2) 1_455 1_455
C203 C208 C207 121(3) . 1_455
C202 C209 C208 35.6(16) 1_655 1_655
C202 C209 C207 73(2) 1_655 .
C208 C209 C207 71(2) 1_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
O C65 1.387(11) .
O C70 1.419(12) .
Si C63 1.842(9) .
Si C61 1.867(8) .
Si C64 1.901(10) .
Si C62 1.915(10) .
Cl1 C78 1.809(11) .
Cl2 C78 1.716(9) .
Cl3 C78 1.720(10) .
C1 C7 1.491(19) .
C1 C6 1.508(11) .
C1 C2 1.538(12) .
C1 C61 1.593(10) .
C1 C36 1.71(3) .
C2 C3 1.350(11) .
C2 C9 1.383(18) .
C2 C135 1.50(2) .
C3 C114 1.40(3) .
C3 C12 1.45(3) .
C3 C4 1.525(10) .
C4 C14 1.483(17) .
C4 C4 1.524(14) 2_556
C4 C5 1.525(12) .
C4 C52 1.640(19) .
C5 C6 1.377(11) .
C5 C104 1.392(17) .
C5 C17 1.54(2) .
C6 C116 1.268(18) .
C6 C19 1.74(2) .
C7 C36 0.68(3) .
C7 C137 1.04(2) .
C7 C8 1.45(3) .
C7 C21 1.48(3) .
C7 C136 2.00(3) .
C8 C136 0.67(2) .
C8 C137 1.052(19) .
C8 C24 1.29(2) .
C8 C9 1.41(3) .
C8 C121 1.68(3) .
C8 C135 1.85(3) .
C8 C36 2.01(3) .
C9 C135 0.50(3) .
C9 C136 1.06(2) .
C9 C10 1.40(3) .
C9 C138 1.76(3) .
C10 C138 0.63(3) .
C10 C135 1.05(2) .
C10 C108 1.22(3) .
C10 C26 1.45(3) .
C10 C11 1.57(3) .
C10 C136 1.76(3) .
C10 C114 1.93(3) .
C10 C103 1.95(4) .
C11 C138 1.06(2) .
C11 C114 1.13(3) .
C11 C128 1.35(3) .
C11 C12 1.39(3) .
C11 C28 1.45(3) .
C11 C108 1.64(3) .
C11 C133 1.78(4) .
C11 C123 1.92(3) .
C12 C114 0.53(3) .
C12 C128 0.94(3) .
C12 C144 1.53(4) .
C12 C13 1.88(3) .
C12 C138 1.97(3) .
C13 C52 1.12(2) .
C13 C30 1.23(3) .
C13 C122 1.42(3) .
C13 C14 1.49(3) .
C13 C128 1.52(3) .
C13 C143 1.92(3) .
C14 C52 0.55(2) .
C14 C143 1.17(3) .
C14 C15 1.21(2) .
C14 C144 1.75(3) .
C14 C112 1.90(4) .
C14 C104 1.98(3) .
C15 C143 0.56(3) .
C15 C112 0.84(3) .
C15 C130 1.30(3) .
C15 C104 1.57(3) .
C15 C52 1.61(3) .
C15 C16 1.67(4) .
C15 C32 1.68(3) .
C16 C112 0.86(3) .
C16 C104 1.08(3) .
C16 C105 1.12(3) .
C16 C17 1.16(3) .
C16 C34 1.46(3) .
C16 C125 1.52(3) .
C16 C35 1.82(4) .
C16 C18 1.99(4) .
C17 C104 0.77(2) .
C17 C105 1.10(2) .
C17 C18 1.33(3) .
C17 C112 1.67(3) .
C17 C139 1.89(3) .
C18 C139 0.57(3) .
C18 C105 1.01(2) .
C18 C116 1.37(2) .
C18 C140 1.44(3) .
C18 C19 1.49(3) .
C18 C104 2.04(3) .
C19 C116 0.56(2) .
C19 C119 1.25(2) .
C19 C20 1.35(3) .
C19 C139 1.45(3) .
C20 C119 0.58(3) .
C20 C38 1.07(2) .
C20 C21 1.48(3) .
C20 C115 1.64(3) .
C20 C116 1.69(3) .
C20 C36 1.92(4) .
C21 C36 0.94(3) .
C21 C119 1.23(2) .
C21 C137 1.40(2) .
C21 C22 1.46(3) .
C21 C38 1.66(3) .
C21 C110 1.73(4) .
C21 C131 1.75(4) .
C22 C131 0.82(3) .
C22 C39 1.33(4) .
C22 C142 1.42(4) .
C22 C38 1.75(4) .
C22 C137 1.88(4) .
C22 C118 1.97(4) .
C23 C142 0.73(3) .
C23 C24 1.09(2) .
C23 C42 1.29(2) .
C23 C117 1.33(3) .
C23 C107 1.35(2) .
C23 C121 1.37(3) .
C23 C131 1.44(3) .
C23 C43 1.73(3) .
C23 C25 1.96(4) .
C24 C121 0.77(2) .
C24 C142 1.33(3) .
C24 C136 1.38(3) .
C24 C117 1.42(4) .
C24 C131 1.61(4) .
C24 C137 1.61(3) .
C24 C25 1.76(4) .
C25 C103 0.66(4) .
C25 C117 0.70(4) .
C25 C121 1.02(3) .
C25 C26 1.06(4) .
C25 C132 1.68(3) .
C25 C43 1.70(4) .
C25 C108 1.85(4) .
C26 C103 0.57(5) .
C26 C108 0.79(3) .
C26 C27 1.39(3) .
C26 C117 1.75(4) .
C26 C132 1.83(3) .
C26 C138 1.83(4) .
C26 C121 1.85(4) .
C26 C123 1.86(4) .
C27 C123 0.78(3) .
C27 C101 1.04(2) .
C27 C108 1.36(3) .
C27 C45 1.42(3) .
C27 C28 1.46(3) .
C27 C132 1.52(3) .
C27 C103 1.56(4) .
C28 C123 0.73(3) .
C28 C133 0.78(3) .
C28 C29 1.46(4) .
C28 C108 1.72(4) .
C28 C128 1.90(4) .
C28 C101 2.01(4) .
C29 C129 0.73(3) .
C29 C133 0.77(3) .
C29 C47 1.42(4) .
C29 C30 1.43(3) .
C29 C106 1.82(4) .
C29 C122 1.83(4) .
C29 C123 1.90(4) .
C29 C128 2.03(4) .
C30 C122 0.77(3) .
C30 C144 1.31(3) .
C30 C129 1.32(3) .
C30 C31 1.51(3) .
C30 C128 1.71(3) .
C30 C133 1.78(4) .
C31 C122 0.78(2) .
C31 C126 0.80(2) .
C31 C32 1.44(3) .
C31 C48 1.44(2) .
C31 C129 1.67(4) .
C31 C111 1.86(4) .
C32 C126 0.73(2) .
C32 C130 0.80(2) .
C32 C33 1.25(3) .
C32 C143 1.44(3) .
C32 C122 1.82(3) .
C32 C127 1.92(3) .
C33 C127 0.81(2) .
C33 C130 1.05(2) .
C33 C50 1.36(2) .
C33 C34 1.39(3) .
C33 C102 1.48(3) .
C33 C126 1.50(3) .
C33 C111 1.69(3) .
C33 C125 1.94(4) .
C34 C125 0.73(3) .
C34 C127 0.82(2) .
C34 C130 1.38(3) .
C34 C35 1.47(3) .
C34 C112 1.56(3) .
C34 C109 2.02(4) .
C35 C109 0.71(3) .
C35 C125 0.74(3) .
C35 C124 1.29(5) .
C35 C140 1.48(3) .
C35 C105 1.51(3) .
C35 C127 1.87(3) .
C35 C113 1.88(3) .
C36 C137 1.27(3) .
C36 C119 1.43(3) .
C37 C120 0.68(3) .
C37 C115 0.92(2) .
C37 C141 1.48(3) .
C37 C140 1.59(3) .
C37 C134 1.68(3) .
C37 C124 1.75(5) .
C37 C38 1.81(3) .
C38 C115 0.929(19) .
C38 C39 1.28(3) .
C38 C119 1.42(3) .
C38 C110 1.53(4) .
C39 C110 0.85(4) .
C39 C118 1.13(3) .
C39 C40 1.48(4) .
C39 C115 1.57(3) .
C39 C134 1.68(3) .
C40 C118 0.52(4) .
C40 C134 1.12(3) .
C40 C41 1.25(3) .
C40 C146 1.65(4) .
C40 C54 1.69(3) .
C40 C110 2.01(4) .
C41 C146 0.54(3) .
C41 C118 1.30(4) .
C41 C56 1.46(2) .
C41 C42 1.48(3) .
C41 C107 1.80(3) .
C42 C107 0.66(2) .
C42 C146 1.00(3) .
C42 C142 1.43(3) .
C42 C43 1.59(3) .
C43 C107 0.945(19) .
C43 C44 1.120(17) .
C43 C117 1.28(3) .
C43 C132 1.42(3) .
C43 C103 2.02(4) .
C44 C132 1.222(18) .
C44 C57 1.447(13) .
C44 C45 1.62(2) .
C44 C107 1.66(2) .
C45 C101 0.65(2) .
C45 C132 1.17(2) .
C45 C46 1.40(2) .
C45 C123 1.94(4) .
C46 C106 1.35(2) .
C46 C58 1.468(13) .
C46 C101 1.50(2) .
C46 C47 1.53(3) .
C47 C106 0.56(3) .
C47 C129 1.08(3) .
C47 C48 1.52(3) .
C47 C49 1.80(4) .
C48 C49 0.87(2) .
C48 C106 1.24(2) .
C48 C111 1.26(3) .
C48 C145 1.46(3) .
C48 C129 1.65(3) .
C48 C126 1.76(3) .
C48 C122 1.94(3) .
C49 C145 0.80(2) .
C49 C111 1.22(3) .
C49 C106 1.32(3) .
C49 C59 1.60(3) .
C50 C102 0.68(2) .
C50 C111 1.04(2) .
C50 C145 1.37(3) .
C50 C127 1.59(3) .
C50 C51 1.70(2) .
C51 C102 1.245(19) .
C51 C113 1.24(2) .
C51 C60 1.432(13) .
C51 C53 1.64(3) .
C52 C144 1.33(3) .
C52 C143 1.39(3) .
C53 C113 0.60(3) .
C53 C141 0.98(3) .
C53 C124 1.31(5) .
C53 C109 1.49(5) .
C53 C54 1.68(3) .
C54 C134 1.16(2) .
C54 C141 1.18(2) .
C54 C55 1.405(14) .
C55 C56 1.389(12) .
C55 C60 1.426(13) .
C56 C57 1.467(14) .
C56 C146 1.63(3) .
C57 C58 1.395(14) .
C58 C59 1.370(13) .
C59 C145 1.368(19) .
C59 C60 1.452(14) .
C64 C69 1.398(12) .
C64 C65 1.428(13) .
C65 C66 1.388(12) .
C66 C67 1.425(14) .
C67 C68 1.365(14) .
C68 C69 1.363(11) .
C70 C71 1.577(15) .
C71 C76 1.486(15) .
C71 C72 1.524(13) .
C72 C73 1.530(14) .
C74 C73 1.523(17) .
C74 C75 1.593(18) .
C76 C77 1.426(16) .
C101 C123 1.39(3) .
C101 C132 1.50(3) .
C102 C127 1.34(2) .
C102 C111 1.70(3) .
C102 C145 1.90(3) .
C102 C113 1.93(3) .
C103 C117 1.32(5) .
C103 C108 1.33(4) .
C103 C132 1.48(3) .
C103 C121 1.63(4) .
C104 C112 1.13(2) .
C104 C105 1.65(3) .
C105 C139 1.34(4) .
C105 C140 1.51(3) .
C105 C125 1.72(3) .
C105 C112 1.96(4) .
C105 C109 2.04(4) .
C106 C129 1.39(4) .
C107 C146 1.26(3) .
C107 C117 1.73(4) .
C107 C142 1.77(3) .
C108 C138 1.32(3) .
C108 C123 1.47(3) .
C109 C124 0.68(5) .
C109 C125 1.31(4) .
C109 C113 1.29(3) .
C109 C140 1.40(3) .
C109 C120 1.87(4) .
C109 C141 2.00(5) .
C110 C131 1.23(4) .
C110 C118 1.56(4) .
C110 C142 1.69(4) .
C111 C145 0.95(2) .
C111 C126 1.56(3) .
C112 C143 1.36(4) .
C112 C130 1.46(3) .
C112 C125 1.96(4) .
C113 C124 1.40(6) .
C113 C141 1.56(3) .
C114 C128 1.27(3) .
C114 C138 1.48(3) .
C114 C144 2.03(4) .
C115 C120 1.43(3) .
C115 C134 1.78(3) .
C116 C119 1.42(3) .
C116 C139 1.53(3) .
C117 C121 0.85(3) .
C117 C132 1.85(4) .
C117 C142 2.03(4) .
C118 C134 1.45(4) .
C118 C146 1.59(4) .
C120 C140 0.95(2) .
C120 C124 1.34(5) .
C120 C139 1.64(4) .
C120 C141 1.71(3) .
C121 C136 1.42(2) .
C121 C142 1.89(3) .
C122 C126 1.40(3) .
C122 C129 1.41(3) .
C122 C144 1.71(4) .
C123 C133 1.40(4) .
C124 C140 1.17(5) .
C124 C141 1.52(5) .
C124 C125 1.97(5) .
C125 C127 1.21(3) .
C126 C130 1.47(3) .
C126 C143 2.02(3) .
C127 C130 1.42(3) .
C128 C144 1.15(3) .
C128 C133 1.61(3) .
C129 C133 1.49(4) .
C130 C143 1.32(3) .
C131 C142 0.76(3) .
C131 C137 1.47(3) .
C134 C141 1.47(3) .
C135 C138 1.31(3) .
C135 C136 1.37(3) .
C136 C137 1.70(3) .
C137 C142 1.95(3) .
C139 C140 1.12(3) .
C201 C204 1.64(5) .
C202 C206 0.80(3) 1_455
C202 C208 0.92(4) .
C202 C209 1.51(4) 1_455
C202 C207 2.01(6) 1_455
C203 C208 1.77(5) .
C206 C202 0.80(3) 1_655
C206 C208 1.49(5) 1_655
C207 C209 1.84(6) .
C207 C208 1.98(7) 1_655
C207 C202 2.01(6) 1_655
C208 C206 1.49(5) 1_455
C208 C209 1.52(4) 1_455
C208 C207 1.97(7) 1_455
C209 C202 1.51(4) 1_655
C209 C208 1.52(4) 1_655
