#------------------------------------------------------------------------------
#$Date: 2017-03-01 23:07:20 +0200 (Wed, 01 Mar 2017) $
#$Revision: 192604 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/55/4125550.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4125550
loop_
_publ_author_name
'Travieso-Puente, Raquel'
'Budzak, Simon'
'Chen, Juan'
'Stacko, Peter'
'Jastrzebski, Johann T. B. H.'
'Jacquemin, Denis'
'Otten, Edwin'
_publ_section_title
;
 Arylazoindazole Photoswitches: Facile Synthesis and Functionalization via
 SNAr Substitution.
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_paper_doi               10.1021/jacs.6b12585
_journal_year                    2017
_chemical_formula_sum            'C22 H16 F4 N4'
_chemical_formula_weight         412.39
_space_group_crystal_system      orthorhombic
_space_group_IT_number           60
_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   13.194(3)
_cell_length_b                   38.114(7)
_cell_length_c                   14.650(3)
_cell_measurement_reflns_used    9942
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      53.220
_cell_measurement_theta_min      5.962
_cell_volume                     7367(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0714
_diffrn_reflns_av_unetI/netI     0.0350
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       47
_diffrn_reflns_limit_k_min       -42
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            123195
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.372
_diffrn_reflns_theta_min         2.781
_exptl_absorpt_coefficient_mu    0.119
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_correction_T_min  0.6966
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.487
_exptl_crystal_description       needle
_exptl_crystal_F_000             3392
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.03
_refine_diff_density_max         0.281
_refine_diff_density_min         -0.281
_refine_diff_density_rms         0.056
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.093
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     547
_refine_ls_number_reflns         7546
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.093
_refine_ls_R_factor_all          0.0963
_refine_ls_R_factor_gt           0.0537
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0423P)²+7.1992P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1132
_refine_ls_wR_factor_ref         0.1274
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5108
_reflns_number_total             7546
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja6b12585_si_002.cif
_cod_data_source_block           mo_molan107b_0m_b
_cod_database_code               4125550
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z-1/2'
'-x-1/2, y-1/2, z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
F1_1 F 0.39588(10) 0.32624(3) 0.59516(8) 0.0226(3) Uani 1 1 d . .
F2_1 F 0.39338(10) 0.38943(3) 0.67844(8) 0.0239(3) Uani 1 1 d . .
F3_1 F 0.38175(10) 0.44928(3) 0.58322(9) 0.0223(3) Uani 1 1 d . .
F4_1 F 0.37340(10) 0.44859(3) 0.39763(9) 0.0212(3) Uani 1 1 d . .
N1_1 N 0.38844(14) 0.32790(5) 0.38788(12) 0.0150(4) Uani 1 1 d . .
N2_1 N 0.38528(14) 0.33989(5) 0.29991(12) 0.0160(4) Uani 1 1 d . .
N3_1 N 0.37566(14) 0.39799(5) 0.23208(13) 0.0174(4) Uani 1 1 d . .
N4_1 N 0.36329(14) 0.38337(5) 0.15541(13) 0.0159(4) Uani 1 1 d . .
C1_1 C 0.40121(17) 0.29116(6) 0.40382(15) 0.0168(5) Uani 1 1 d . .
C2_1 C 0.32890(18) 0.27301(6) 0.45387(16) 0.0209(5) Uani 1 1 d . .
H2_1 H 0.2723 0.2849 0.4794 0.025 Uiso 1 1 calc R U
C3_1 C 0.3409(2) 0.23729(6) 0.46580(17) 0.0266(6) Uani 1 1 d . .
H3_1 H 0.2926 0.2245 0.5005 0.032 Uiso 1 1 calc R U
C4_1 C 0.4226(2) 0.22015(6) 0.42766(17) 0.0310(7) Uani 1 1 d . .
H4_1 H 0.4299 0.1956 0.4358 0.037 Uiso 1 1 calc R U
C5_1 C 0.4940(2) 0.23852(7) 0.37760(18) 0.0323(7) Uani 1 1 d . .
H5_1 H 0.5499 0.2265 0.3514 0.039 Uiso 1 1 calc R U
C6_1 C 0.48375(19) 0.27446(6) 0.36573(16) 0.0249(6) Uani 1 1 d . .
H6_1 H 0.5327 0.2873 0.3320 0.030 Uiso 1 1 calc R U
C7_1 C 0.37961(16) 0.37455(6) 0.30592(15) 0.0146(5) Uani 1 1 d . .
C8_1 C 0.38034(16) 0.38607(6) 0.39873(15) 0.0147(5) Uani 1 1 d . .
C9_1 C 0.37790(17) 0.41821(6) 0.44398(15) 0.0158(5) Uani 1 1 d . .
C10_1 C 0.38284(17) 0.41881(6) 0.53723(16) 0.0172(5) Uani 1 1 d . .
C11_1 C 0.38763(17) 0.38763(6) 0.58688(15) 0.0169(5) Uani 1 1 d . .
C12_1 C 0.38900(16) 0.35570(6) 0.54486(15) 0.0159(5) Uani 1 1 d . .
C13_1 C 0.38518(16) 0.35490(6) 0.44946(15) 0.0151(5) Uani 1 1 d . .
C14_1 C 0.36349(16) 0.40587(6) 0.07897(15) 0.0150(5) Uani 1 1 d . .
C15_1 C 0.36978(16) 0.44302(6) 0.08047(15) 0.0161(5) Uani 1 1 d . .
C16_1 C 0.37591(16) 0.46033(6) -0.00247(15) 0.0182(5) Uani 1 1 d . .
H16_1 H 0.3814 0.4852 -0.0023 0.022 Uiso 1 1 calc R U
C17_1 C 0.37447(17) 0.44305(6) -0.08605(16) 0.0182(5) Uani 1 1 d . .
C18_1 C 0.36445(17) 0.40661(6) -0.08579(15) 0.0172(5) Uani 1 1 d . .
H18_1 H 0.3616 0.3944 -0.1423 0.021 Uiso 1 1 calc R U
C19_1 C 0.35853(16) 0.38772(6) -0.00505(15) 0.0166(5) Uani 1 1 d . .
C20_1 C 0.36986(19) 0.46505(6) 0.16590(16) 0.0217(5) Uani 1 1 d . .
H20A_1 H 0.3653 0.4899 0.1494 0.033 Uiso 1 1 calc R U
H20B_1 H 0.4327 0.4609 0.1999 0.033 Uiso 1 1 calc R U
H20C_1 H 0.3116 0.4587 0.2040 0.033 Uiso 1 1 calc R U
C21_1 C 0.38535(19) 0.46322(7) -0.17372(16) 0.0254(6) Uani 1 1 d . .
H21A_1 H 0.3714 0.4477 -0.2255 0.038 Uiso 1 1 calc R U
H21B_1 H 0.4545 0.4724 -0.1786 0.038 Uiso 1 1 calc R U
H21C_1 H 0.3371 0.4828 -0.1742 0.038 Uiso 1 1 calc R U
C22_1 C 0.34725(18) 0.34847(6) -0.00886(16) 0.0211(5) Uani 1 1 d . .
H22A_1 H 0.3549 0.3405 -0.0721 0.032 Uiso 1 1 calc R U
H22B_1 H 0.2801 0.3418 0.0138 0.032 Uiso 1 1 calc R U
H22C_1 H 0.3995 0.3375 0.0292 0.032 Uiso 1 1 calc R U
F1_2 F 0.12264(10) 0.44815(3) 0.29531(9) 0.0235(3) Uani 1 1 d . .
F2_2 F 0.11029(10) 0.44750(3) 0.11016(9) 0.0239(3) Uani 1 1 d . .
F3_2 F 0.10788(10) 0.38671(3) 0.01761(8) 0.0219(3) Uani 1 1 d . .
F4_2 F 0.11748(10) 0.32444(3) 0.10330(8) 0.0205(3) Uani 1 1 d . .
N1_2 N 0.13454(13) 0.32748(5) 0.31121(12) 0.0148(4) Uani 1 1 d . .
N2_2 N 0.13633(13) 0.34045(5) 0.39822(12) 0.0157(4) Uani 1 1 d . .
N3_2 N 0.13276(14) 0.39922(5) 0.46300(12) 0.0170(4) Uani 1 1 d . .
N4_2 N 0.13878(14) 0.38469(5) 0.54052(13) 0.0172(4) Uani 1 1 d . .
C1_2 C 0.13977(17) 0.29042(6) 0.29866(15) 0.0163(5) Uani 1 1 d . .
C2_2 C 0.20602(18) 0.27608(6) 0.23586(15) 0.0197(5) Uani 1 1 d . .
H2_2 H 0.2484 0.2907 0.1999 0.024 Uiso 1 1 calc R U
C3_2 C 0.20939(19) 0.23987(6) 0.22641(16) 0.0244(6) Uani 1 1 d . .
H3_2 H 0.2532 0.2296 0.1823 0.029 Uiso 1 1 calc R U
C4_2 C 0.1500(2) 0.21861(6) 0.28029(16) 0.0265(6) Uani 1 1 d . .
H4_2 H 0.1536 0.1938 0.2737 0.032 Uiso 1 1 calc R U
C5_2 C 0.08497(19) 0.23317(6) 0.34401(17) 0.0236(6) Uani 1 1 d . .
H5_2 H 0.0444 0.2184 0.3814 0.028 Uiso 1 1 calc R U
C6_2 C 0.07910(17) 0.26935(6) 0.35311(15) 0.0189(5) Uani 1 1 d . .
H6_2 H 0.0340 0.2796 0.3962 0.023 Uiso 1 1 calc R U
C7_2 C 0.13328(16) 0.37501(6) 0.39024(15) 0.0144(5) Uani 1 1 d . .
C8_2 C 0.12952(16) 0.38554(6) 0.29669(15) 0.0147(5) Uani 1 1 d . .
C9_2 C 0.12407(17) 0.41744(6) 0.25019(16) 0.0165(5) Uani 1 1 d . .
C10_2 C 0.11719(17) 0.41734(6) 0.15692(16) 0.0174(5) Uani 1 1 d . .
C11_2 C 0.11561(16) 0.38567(6) 0.10897(15) 0.0162(5) Uani 1 1 d . .
C12_2 C 0.12144(16) 0.35414(6) 0.15241(15) 0.0151(5) Uani 1 1 d . .
C13_2 C 0.12998(16) 0.35404(6) 0.24783(15) 0.0144(5) Uani 1 1 d . .
C14_2 C 0.13749(16) 0.40725(6) 0.61706(15) 0.0155(5) Uani 1 1 d . .
C15_2 C 0.13742(17) 0.44444(6) 0.61645(16) 0.0180(5) Uani 1 1 d . .
C16_2 C 0.13368(17) 0.46122(6) 0.70030(15) 0.0197(5) Uani 1 1 d . .
H16_2 H 0.1342 0.4861 0.7011 0.024 Uiso 1 1 calc R U
C17_2 C 0.12927(17) 0.44367(6) 0.78319(16) 0.0207(5) Uani 1 1 d . .
C18_2 C 0.13187(17) 0.40703(6) 0.78187(15) 0.0199(5) Uani 1 1 d . .
H18_2 H 0.1305 0.3945 0.8379 0.024 Uiso 1 1 calc R U
C19_2 C 0.13645(17) 0.38863(6) 0.70041(15) 0.0180(5) Uani 1 1 d . .
C20_2 C 0.13985(19) 0.46658(6) 0.53126(16) 0.0219(5) Uani 1 1 d . .
H20A_2 H 0.1458 0.4914 0.5481 0.033 Uiso 1 1 calc R U
H20B_2 H 0.0772 0.4630 0.4966 0.033 Uiso 1 1 calc R U
H20C_2 H 0.1981 0.4598 0.4937 0.033 Uiso 1 1 calc R U
C21_2 C 0.12236(19) 0.46352(7) 0.87164(16) 0.0266(6) Uani 1 1 d . .
H21A_2 H 0.1033 0.4474 0.9208 0.040 Uiso 1 1 calc R U
H21B_2 H 0.0710 0.4820 0.8662 0.040 Uiso 1 1 calc R U
H21C_2 H 0.1882 0.4741 0.8856 0.040 Uiso 1 1 calc R U
C22_2 C 0.1377(2) 0.34900(6) 0.70196(17) 0.0269(6) Uani 1 1 d . .
H22A_2 H 0.1429 0.3408 0.7652 0.040 Uiso 1 1 calc R U
H22B_2 H 0.1960 0.3405 0.6670 0.040 Uiso 1 1 calc R U
H22C_2 H 0.0750 0.3400 0.6747 0.040 Uiso 1 1 calc R U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N2_1 N1_1 C13_1 111.63(17)
N2_1 N1_1 C1_1 118.99(17)
C13_1 N1_1 C1_1 129.22(18)
C7_1 N2_1 N1_1 105.78(18)
N4_1 N3_1 C7_1 114.12(18)
N3_1 N4_1 C14_1 115.92(18)
C6_1 C1_1 C2_1 121.8(2)
C6_1 C1_1 N1_1 118.6(2)
C2_1 C1_1 N1_1 119.6(2)
C3_1 C2_1 C1_1 118.6(2)
C4_1 C3_1 C2_1 120.3(2)
C3_1 C4_1 C5_1 120.5(2)
C4_1 C5_1 C6_1 120.0(3)
C1_1 C6_1 C5_1 118.8(2)
N2_1 C7_1 N3_1 125.8(2)
N2_1 C7_1 C8_1 111.65(19)
N3_1 C7_1 C8_1 122.5(2)
C9_1 C8_1 C13_1 119.6(2)
C9_1 C8_1 C7_1 136.3(2)
C13_1 C8_1 C7_1 104.13(19)
F4_1 C9_1 C10_1 119.5(2)
F4_1 C9_1 C8_1 121.21(19)
C10_1 C9_1 C8_1 119.3(2)
F3_1 C10_1 C9_1 121.0(2)
F3_1 C10_1 C11_1 118.4(2)
C9_1 C10_1 C11_1 120.6(2)
F2_1 C11_1 C12_1 119.6(2)
F2_1 C11_1 C10_1 118.6(2)
C12_1 C11_1 C10_1 121.7(2)
F1_1 C12_1 C11_1 119.87(19)
F1_1 C12_1 C13_1 122.1(2)
C11_1 C12_1 C13_1 118.0(2)
N1_1 C13_1 C12_1 132.3(2)
N1_1 C13_1 C8_1 106.80(18)
C12_1 C13_1 C8_1 120.8(2)
N4_1 C14_1 C19_1 113.19(19)
N4_1 C14_1 C15_1 126.5(2)
C19_1 C14_1 C15_1 120.3(2)
C16_1 C15_1 C14_1 117.7(2)
C16_1 C15_1 C20_1 117.6(2)
C14_1 C15_1 C20_1 124.7(2)
C15_1 C16_1 C17_1 123.1(2)
C16_1 C17_1 C18_1 118.1(2)
C16_1 C17_1 C21_1 120.6(2)
C18_1 C17_1 C21_1 121.4(2)
C19_1 C18_1 C17_1 121.6(2)
C18_1 C19_1 C14_1 119.1(2)
C18_1 C19_1 C22_1 119.3(2)
C14_1 C19_1 C22_1 121.6(2)
N2_2 N1_2 C13_2 111.35(17)
N2_2 N1_2 C1_2 118.52(17)
C13_2 N1_2 C1_2 130.12(18)
C7_2 N2_2 N1_2 106.09(17)
N4_2 N3_2 C7_2 113.06(18)
N3_2 N4_2 C14_2 116.42(18)
C2_2 C1_2 C6_2 121.3(2)
C2_2 C1_2 N1_2 120.5(2)
C6_2 C1_2 N1_2 118.1(2)
C1_2 C2_2 C3_2 118.7(2)
C4_2 C3_2 C2_2 120.7(2)
C3_2 C4_2 C5_2 120.3(2)
C4_2 C5_2 C6_2 119.9(2)
C1_2 C6_2 C5_2 119.2(2)
N2_2 C7_2 N3_2 125.8(2)
N2_2 C7_2 C8_2 111.42(19)
N3_2 C7_2 C8_2 122.8(2)
C9_2 C8_2 C13_2 119.9(2)
C9_2 C8_2 C7_2 135.6(2)
C13_2 C8_2 C7_2 104.47(19)
F1_2 C9_2 C10_2 119.5(2)
F1_2 C9_2 C8_2 121.28(19)
C10_2 C9_2 C8_2 119.2(2)
F2_2 C10_2 C9_2 120.8(2)
F2_2 C10_2 C11_2 118.9(2)
C9_2 C10_2 C11_2 120.3(2)
F3_2 C11_2 C12_2 119.7(2)
F3_2 C11_2 C10_2 118.5(2)
C12_2 C11_2 C10_2 121.8(2)
F4_2 C12_2 C11_2 119.44(19)
F4_2 C12_2 C13_2 122.3(2)
C11_2 C12_2 C13_2 118.2(2)
N1_2 C13_2 C8_2 106.67(18)
N1_2 C13_2 C12_2 132.7(2)
C8_2 C13_2 C12_2 120.5(2)
C19_2 C14_2 N4_2 112.36(19)
C19_2 C14_2 C15_2 120.5(2)
N4_2 C14_2 C15_2 127.1(2)
C16_2 C15_2 C14_2 117.1(2)
C16_2 C15_2 C20_2 118.5(2)
C14_2 C15_2 C20_2 124.4(2)
C15_2 C16_2 C17_2 123.7(2)
C16_2 C17_2 C18_2 118.0(2)
C16_2 C17_2 C21_2 121.0(2)
C18_2 C17_2 C21_2 121.1(2)
C19_2 C18_2 C17_2 121.3(2)
C18_2 C19_2 C14_2 119.4(2)
C18_2 C19_2 C22_2 119.6(2)
C14_2 C19_2 C22_2 121.0(2)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
F1_1 C12_1 1.346(2)
F2_1 C11_1 1.345(3)
F3_1 C10_1 1.343(3)
F4_1 C9_1 1.344(3)
N1_1 N2_1 1.368(2)
N1_1 C13_1 1.369(3)
N1_1 C1_1 1.429(3)
N2_1 C7_1 1.326(3)
N3_1 N4_1 1.264(3)
N3_1 C7_1 1.404(3)
N4_1 C14_1 1.410(3)
C1_1 C6_1 1.379(3)
C1_1 C2_1 1.388(3)
C2_1 C3_1 1.382(3)
C3_1 C4_1 1.379(4)
C4_1 C5_1 1.384(4)
C5_1 C6_1 1.388(3)
C7_1 C8_1 1.429(3)
C8_1 C9_1 1.393(3)
C8_1 C13_1 1.403(3)
C9_1 C10_1 1.368(3)
C10_1 C11_1 1.395(3)
C11_1 C12_1 1.364(3)
C12_1 C13_1 1.399(3)
C14_1 C19_1 1.413(3)
C14_1 C15_1 1.419(3)
C15_1 C16_1 1.385(3)
C15_1 C20_1 1.507(3)
C16_1 C17_1 1.390(3)
C17_1 C18_1 1.395(3)
C17_1 C21_1 1.504(3)
C18_1 C19_1 1.387(3)
C19_1 C22_1 1.504(3)
F1_2 C9_2 1.344(3)
F2_2 C10_2 1.341(3)
F3_2 C11_2 1.343(3)
F4_2 C12_2 1.342(2)
N1_2 N2_2 1.367(2)
N1_2 C13_2 1.375(3)
N1_2 C1_2 1.426(3)
N2_2 C7_2 1.323(3)
N3_2 N4_2 1.266(3)
N3_2 C7_2 1.410(3)
N4_2 C14_2 1.413(3)
C1_2 C2_2 1.382(3)
C1_2 C6_2 1.386(3)
C2_2 C3_2 1.388(3)
C3_2 C4_2 1.376(3)
C4_2 C5_2 1.384(4)
C5_2 C6_2 1.388(3)
C7_2 C8_2 1.429(3)
C8_2 C9_2 1.395(3)
C8_2 C13_2 1.398(3)
C9_2 C10_2 1.369(3)
C10_2 C11_2 1.397(3)
C11_2 C12_2 1.362(3)
C12_2 C13_2 1.403(3)
C14_2 C19_2 1.412(3)
C14_2 C15_2 1.417(3)
C15_2 C16_2 1.386(3)
C15_2 C20_2 1.507(3)
C16_2 C17_2 1.388(3)
C17_2 C18_2 1.397(3)
C17_2 C21_2 1.503(3)
C18_2 C19_2 1.386(3)
C19_2 C22_2 1.511(3)
