#------------------------------------------------------------------------------
#$Date: 2019-11-02 07:49:39 +0200 (Sat, 02 Nov 2019) $
#$Revision: 221008 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/78/4127836.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4127836
loop_
_publ_author_name
'Chiu, Tzu-Hao'
'Liao, Jian-Hong'
'Gam, Franck'
'Chantrenne, Isaac'
'Kahlal, Samia'
'Saillard, Jean-Yves'
'Liu, C. W.'
_publ_section_title
;
 Homoleptic Platinum/Silver Superatoms Protected by Dithiolates: Linear
 Assemblies of Two and Three Centered Icosahedra Isolobal to
 Ne₂ and I₃<sup/>.
;
_journal_issue                   33
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              12957
_journal_page_last               12961
_journal_paper_doi               10.1021/jacs.9b05000
_journal_volume                  141
_journal_year                    2019
_chemical_formula_sum            'C75 H175 Ag20 O24 P12 Pt S24'
_chemical_formula_weight         4954.71
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                90
_cell_angle_beta                 109.4720(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   30.0959(9)
_cell_length_b                   17.3885(6)
_cell_length_c                   29.7671(9)
_cell_measurement_reflns_used    9934
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      26.87
_cell_measurement_theta_min      2.34
_cell_volume                     14686.8(8)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0647
_diffrn_reflns_av_unetI/netI     0.0614
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       35
_diffrn_reflns_limit_h_min       -35
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            91527
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.661
_exptl_absorpt_coefficient_mu    4.070
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_correction_T_min  0.6215
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.241
_exptl_crystal_description       plate
_exptl_crystal_F_000             9596
_exptl_crystal_size_max          0.090
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.020
_refine_diff_density_max         2.274
_refine_diff_density_min         -1.630
_refine_diff_density_rms         0.175
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1451
_refine_ls_number_reflns         25813
_refine_ls_number_restraints     433
_refine_ls_restrained_S_all      1.024
_refine_ls_R_factor_all          0.0735
_refine_ls_R_factor_gt           0.0409
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0256P)²+93.7091P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0796
_refine_ls_wR_factor_ref         0.0937
_reflns_Friedel_coverage         0.000
_reflns_number_gt                18405
_reflns_number_total             25813
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja9b05000_si_002.cif
_cod_data_source_block           1
_cod_database_code               4127836
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.711
_shelx_estimated_absorpt_t_max   0.923
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.76318(2) 0.36291(3) 0.27039(2) 0.02135(14) Uani 1 1 d . . . . .
Ag2 Ag 0.75699(2) 0.44129(3) 0.18278(2) 0.02064(14) Uani 1 1 d . . . . .
Ag3 Ag 0.84402(2) 0.45229(3) 0.26780(2) 0.01999(14) Uani 1 1 d . . . . .
Ag4 Ag 0.81421(2) 0.45709(3) 0.34927(2) 0.02249(14) Uani 1 1 d . . . . .
Ag5 Ag 0.70989(2) 0.45031(4) 0.31481(2) 0.02439(15) Uani 1 1 d . . . . .
Ag6 Ag 0.67600(2) 0.44743(4) 0.21093(2) 0.02385(14) Uani 1 1 d . . . . .
Ag7 Ag 0.67388(2) 0.58978(4) 0.26062(3) 0.02932(16) Uani 1 1 d . . . . .
Ag8 Ag 0.70436(2) 0.58658(4) 0.17746(2) 0.02809(16) Uani 1 1 d . . . . .
Ag9 Ag 0.80853(2) 0.58665(3) 0.21205(2) 0.02250(14) Uani 1 1 d . . . . .
Ag10 Ag 0.84217(2) 0.59729(3) 0.31372(2) 0.02189(14) Uani 1 1 d . . . . .
Ag11 Ag 0.75887(2) 0.59442(4) 0.34356(2) 0.02431(15) Uani 1 1 d . . . . .
Ag12 Ag 0.75618(2) 0.67751(4) 0.25945(2) 0.02986(16) Uani 1 1 d . . . . .
Ag13 Ag 0.85703(2) 0.58223(4) 0.41697(2) 0.02646(15) Uani 1 1 d . . . . .
Ag14 Ag 0.81902(3) 0.74246(4) 0.35248(3) 0.03237(17) Uani 1 1 d . . . . .
Ag15 Ag 0.75259(3) 0.71972(4) 0.16102(3) 0.03604(19) Uani 0.91 1 d . . P A 1
Ag21 Ag 0.7013(3) 0.7256(4) 0.3122(3) 0.03604(19) Uani 0.09 1 d . . P A 2
Ag16 Ag 0.75566(2) 0.55232(4) 0.11066(3) 0.03315(17) Uani 1 1 d . . . . .
Ag17 Ag 0.84881(2) 0.46738(4) 0.16832(2) 0.02999(16) Uani 1 1 d . . . . .
Ag18 Ag 0.81533(2) 0.30726(4) 0.21028(2) 0.02734(15) Uani 1 1 d . . . . .
Ag19 Ag 0.66689(2) 0.30528(4) 0.26283(2) 0.02956(16) Uani 1 1 d . . . . .
Ag20 Ag 0.60384(2) 0.46216(4) 0.26089(3) 0.03524(18) Uani 1 1 d . . . . .
C1 C 0.7591(4) 0.1110(6) 0.1704(4) 0.044(2) Uani 1 1 d . . . . .
H1A H 0.766138 0.164700 0.164008 0.052 Uiso 1 1 calc R U . . .
H1B H 0.728061 0.096537 0.147350 0.052 Uiso 1 1 calc R U . . .
C2 C 0.7971(4) 0.0573(6) 0.1657(4) 0.056(3) Uani 1 1 d . . . . .
H2A H 0.792349 0.005481 0.177122 0.068 Uiso 1 1 calc R U . . .
H2B H 0.794271 0.052953 0.131733 0.068 Uiso 1 1 calc R U . . .
C3 C 0.8450(4) 0.0846(8) 0.1933(5) 0.087(5) Uani 1 1 d . . . . .
H3A H 0.850442 0.134765 0.181061 0.130 Uiso 1 1 calc R U . . .
H3B H 0.868320 0.047631 0.190118 0.130 Uiso 1 1 calc R U . . .
H3C H 0.847857 0.089514 0.226940 0.130 Uiso 1 1 calc R U . . .
C4 C 0.6945(3) 0.0785(6) 0.2773(4) 0.043(2) Uani 1 1 d . . . . .
H4A H 0.697161 0.037364 0.255382 0.051 Uiso 1 1 calc R U . . .
H4B H 0.665519 0.108372 0.261328 0.051 Uiso 1 1 calc R U . . .
C5 C 0.6919(4) 0.0442(7) 0.3219(4) 0.067(4) Uani 1 1 d . . . . .
H5A H 0.685838 0.085008 0.342384 0.080 Uiso 1 1 calc R U . . .
H5B H 0.722248 0.019280 0.339655 0.080 Uiso 1 1 calc R U . . .
C6 C 0.6522(4) -0.0153(8) 0.3100(5) 0.084(5) Uani 1 1 d . . . . .
H6A H 0.622273 0.009388 0.292047 0.127 Uiso 1 1 calc R U . . .
H6B H 0.649926 -0.036904 0.339632 0.127 Uiso 1 1 calc R U . . .
H6C H 0.658908 -0.056634 0.290850 0.127 Uiso 1 1 calc R U . . .
C7 C 0.8448(3) 0.2773(6) 0.0625(3) 0.039(2) Uani 1 1 d . . . . .
H7A H 0.864332 0.324406 0.066984 0.047 Uiso 1 1 calc R U . . .
H7B H 0.826512 0.271912 0.028173 0.047 Uiso 1 1 calc R U . . .
C8 C 0.8754(3) 0.2080(6) 0.0801(3) 0.044(2) Uani 1 1 d . . . . .
H8A H 0.898859 0.205114 0.063411 0.052 Uiso 1 1 calc R U . . .
H8B H 0.892878 0.214472 0.114518 0.052 Uiso 1 1 calc R U . . .
C9 C 0.8486(4) 0.1340(6) 0.0728(5) 0.066(4) Uani 1 1 d . . . . .
H9A H 0.824893 0.136608 0.088649 0.099 Uiso 1 1 calc R U . . .
H9B H 0.870414 0.091537 0.086259 0.099 Uiso 1 1 calc R U . . .
H9C H 0.832977 0.125246 0.038582 0.099 Uiso 1 1 calc R U . . .
C10 C 0.7024(3) 0.3732(7) 0.0022(4) 0.061(3) Uani 1 1 d D . . . .
H10A H 0.702383 0.378586 -0.030905 0.074 Uiso 1 1 calc R U . . .
H10B H 0.705973 0.425108 0.016709 0.074 Uiso 1 1 calc R U . . .
C11 C 0.6561(4) 0.3377(8) 0.0020(6) 0.105(5) Uani 1 1 d D . . . .
H11A H 0.656729 0.330226 0.035211 0.126 Uiso 1 1 calc R U . . .
H11B H 0.651939 0.286740 -0.013691 0.126 Uiso 1 1 calc R U . . .
C12 C 0.6150(5) 0.3902(9) -0.0245(6) 0.125(7) Uani 1 1 d D . . . .
H12A H 0.617748 0.438956 -0.007288 0.187 Uiso 1 1 calc R U . . .
H12B H 0.585190 0.365175 -0.026608 0.187 Uiso 1 1 calc R U . . .
H12C H 0.615677 0.400134 -0.056691 0.187 Uiso 1 1 calc R U . . .
C13 C 0.9395(3) 0.2425(5) 0.3001(3) 0.033(2) Uani 1 1 d . . . . .
H13A H 0.923176 0.197799 0.281087 0.039 Uiso 1 1 calc R U . . .
H13B H 0.915353 0.275869 0.306049 0.039 Uiso 1 1 calc R U . . .
C14 C 0.9730(4) 0.2152(7) 0.3464(4) 0.049(3) Uani 1 1 d . . . . .
H14A H 0.987694 0.260080 0.366284 0.059 Uiso 1 1 calc R U . . .
H14B H 0.998362 0.184825 0.340552 0.059 Uiso 1 1 calc R U . . .
C15 C 0.9482(4) 0.1660(7) 0.3729(4) 0.069(4) Uani 1 1 d . . . . .
H15A H 0.923974 0.196645 0.379893 0.103 Uiso 1 1 calc R U . . .
H15B H 0.971231 0.147871 0.402847 0.103 Uiso 1 1 calc R U . . .
H15C H 0.933493 0.121748 0.353204 0.103 Uiso 1 1 calc R U . . .
C16 C 0.9981(3) 0.3517(5) 0.1949(3) 0.029(2) Uani 1 1 d . . . . .
H16A H 0.971512 0.322466 0.172867 0.035 Uiso 1 1 calc R U . . .
H16B H 1.023764 0.315207 0.210814 0.035 Uiso 1 1 calc R U . . .
C17 C 1.0153(4) 0.4113(6) 0.1678(4) 0.042(2) Uani 1 1 d . . . . .
H17A H 1.040259 0.442430 0.190650 0.050 Uiso 1 1 calc R U . . .
H17B H 1.029595 0.384777 0.146454 0.050 Uiso 1 1 calc R U . . .
C18 C 0.9770(5) 0.4641(7) 0.1384(4) 0.067(4) Uani 1 1 d . . . . .
H18A H 0.952528 0.433823 0.115057 0.100 Uiso 1 1 calc R U . . .
H18B H 0.990327 0.501329 0.121705 0.100 Uiso 1 1 calc R U . . .
H18C H 0.963157 0.491468 0.159306 0.100 Uiso 1 1 calc R U . . .
C19 C 0.8207(4) 0.2637(6) 0.4189(5) 0.068(3) Uani 1 1 d D . . . .
H19A H 0.833011 0.261822 0.391949 0.081 Uiso 1 1 calc R U . . .
H19B H 0.792644 0.297439 0.408960 0.081 Uiso 1 1 calc R U . . .
C20 C 0.8040(6) 0.1841(7) 0.4247(6) 0.126(7) Uani 1 1 d D . . . .
H20A H 0.781851 0.186576 0.442990 0.151 Uiso 1 1 calc R U . . .
H20B H 0.786972 0.161868 0.393041 0.151 Uiso 1 1 calc R U . . .
C21 C 0.8449(6) 0.1344(9) 0.4504(6) 0.122(6) Uani 1 1 d D . . . .
H21A H 0.868054 0.135662 0.433702 0.183 Uiso 1 1 calc R U . . .
H21B H 0.834130 0.081410 0.451257 0.183 Uiso 1 1 calc R U . . .
H21C H 0.859583 0.153344 0.482986 0.183 Uiso 1 1 calc R U . . .
C22 C 0.9442(3) 0.4598(5) 0.5061(3) 0.036(2) Uani 1 1 d . . . . .
H22A H 0.935174 0.492471 0.477237 0.043 Uiso 1 1 calc R U . . .
H22B H 0.977859 0.446246 0.514207 0.043 Uiso 1 1 calc R U . . .
C23 C 0.9374(4) 0.5039(6) 0.5462(4) 0.049(3) Uani 1 1 d . . . . .
H23A H 0.949408 0.473334 0.575882 0.059 Uiso 1 1 calc R U . . .
H23B H 0.903356 0.513069 0.539595 0.059 Uiso 1 1 calc R U . . .
C24 C 0.9634(4) 0.5812(7) 0.5531(5) 0.070(4) Uani 1 1 d . . . . .
H24A H 0.997435 0.572080 0.563054 0.105 Uiso 1 1 calc R U . . .
H24B H 0.956051 0.611116 0.577641 0.105 Uiso 1 1 calc R U . . .
H24C H 0.953278 0.609811 0.523015 0.105 Uiso 1 1 calc R U . . .
C25 C 0.5949(4) 0.2382(6) 0.3653(4) 0.053(3) Uani 1 1 d . . . . .
H25A H 0.626527 0.215381 0.380359 0.063 Uiso 1 1 calc R U . . .
H25B H 0.577866 0.235560 0.388530 0.063 Uiso 1 1 calc R U . . .
C26 C 0.5692(4) 0.1934(6) 0.3228(4) 0.056(3) Uani 1 1 d . . . . .
H26A H 0.588059 0.191134 0.301286 0.067 Uiso 1 1 calc R U . . .
H26B H 0.539158 0.219869 0.305676 0.067 Uiso 1 1 calc R U . . .
C27 C 0.5586(4) 0.1126(6) 0.3348(4) 0.058(3) Uani 1 1 d . . . . .
H27A H 0.588092 0.086958 0.353148 0.087 Uiso 1 1 calc R U . . .
H27B H 0.543392 0.084007 0.305344 0.087 Uiso 1 1 calc R U . . .
H27C H 0.537570 0.114462 0.353810 0.087 Uiso 1 1 calc R U . . .
C28 C 0.7083(5) 0.3807(11) 0.4538(4) 0.108(7) Uani 1 1 d D . . . .
H28A H 0.715459 0.425215 0.436650 0.130 Uiso 1 1 calc R U . . .
H28B H 0.732103 0.340571 0.455469 0.130 Uiso 1 1 calc R U . . .
C29 C 0.7140(5) 0.4050(13) 0.5023(5) 0.145(9) Uani 1 1 d D . . . .
H29A H 0.714159 0.461931 0.502153 0.175 Uiso 1 1 calc R U . . .
H29B H 0.745955 0.388664 0.522374 0.175 Uiso 1 1 calc R U . . .
C30 C 0.6815(5) 0.3814(9) 0.5280(5) 0.101(5) Uani 1 1 d D . . . .
H30A H 0.655553 0.351168 0.506660 0.152 Uiso 1 1 calc R U . . .
H30B H 0.668849 0.427303 0.538559 0.152 Uiso 1 1 calc R U . . .
H30C H 0.698749 0.350232 0.555781 0.152 Uiso 1 1 calc R U . . .
C31 C 0.5912(4) 0.2352(7) 0.0989(4) 0.055(3) Uani 1 1 d . . . . .
H31A H 0.620781 0.262777 0.101539 0.066 Uiso 1 1 calc R U . . .
H31B H 0.597741 0.179344 0.099683 0.066 Uiso 1 1 calc R U . . .
C32 C 0.5555(4) 0.2546(8) 0.0538(5) 0.076(4) Uani 1 1 d . . . . .
H32A H 0.567336 0.240345 0.027658 0.091 Uiso 1 1 calc R U . . .
H32B H 0.550819 0.311069 0.052498 0.091 Uiso 1 1 calc R U . . .
C33 C 0.5078(4) 0.2158(8) 0.0450(4) 0.078(4) Uani 1 1 d . . . . .
H33A H 0.512390 0.160295 0.050244 0.117 Uiso 1 1 calc R U . . .
H33B H 0.487487 0.225361 0.012149 0.117 Uiso 1 1 calc R U . . .
H33C H 0.492916 0.236828 0.067070 0.117 Uiso 1 1 calc R U . . .
C34 C 0.4922(3) 0.4232(6) 0.1357(5) 0.073(4) Uani 1 1 d D . . . .
H34A H 0.500001 0.466929 0.118391 0.087 Uiso 1 1 calc R U . . .
H34B H 0.501539 0.436551 0.169961 0.087 Uiso 1 1 calc R U . . .
C35 C 0.4388(3) 0.4043(9) 0.1153(6) 0.146(8) Uani 1 1 d D . . . .
H35A H 0.431872 0.352044 0.124453 0.175 Uiso 1 1 calc R U . . .
H35B H 0.419639 0.442428 0.125583 0.175 Uiso 1 1 calc R U . . .
C36 C 0.4310(7) 0.4100(13) 0.0628(6) 0.199(12) Uani 1 1 d D . . . .
H36A H 0.397873 0.399260 0.044738 0.298 Uiso 1 1 calc R U . . .
H36B H 0.438989 0.461996 0.055243 0.298 Uiso 1 1 calc R U . . .
H36C H 0.451095 0.372549 0.054125 0.298 Uiso 1 1 calc R U . . .
C37 C 0.6347(4) 0.7759(6) 0.0161(4) 0.051(3) Uani 1 1 d . . . . .
H37A H 0.650872 0.812212 0.041941 0.061 Uiso 1 1 calc R U . . .
H37B H 0.600636 0.776714 0.011639 0.061 Uiso 1 1 calc R U . . .
C38 C 0.6422(4) 0.8000(7) -0.0287(4) 0.065(3) Uani 1 1 d . . . . .
H38A H 0.626660 0.762633 -0.054202 0.078 Uiso 1 1 calc R U . . .
H38B H 0.676327 0.799633 -0.023909 0.078 Uiso 1 1 calc R U . . .
C39 C 0.6229(5) 0.8783(8) -0.0441(5) 0.080(4) Uani 1 1 d . . . . .
H39A H 0.588948 0.878536 -0.049647 0.120 Uiso 1 1 calc R U . . .
H39B H 0.628708 0.892158 -0.073537 0.120 Uiso 1 1 calc R U . . .
H39C H 0.638493 0.915559 -0.019087 0.120 Uiso 1 1 calc R U . . .
C40 C 0.5643(9) 0.6031(19) 0.0779(13) 0.052(5) Uani 0.5 1 d D . P B 1
H40A H 0.581892 0.601817 0.112556 0.062 Uiso 0.5 1 calc R U P B 1
H40B H 0.561061 0.549933 0.065250 0.062 Uiso 0.5 1 calc R U P B 1
C41 C 0.5164(9) 0.6410(16) 0.0676(13) 0.054(4) Uani 0.5 1 d D . P B 1
H41A H 0.496889 0.607200 0.080285 0.064 Uiso 0.5 1 calc R U P B 1
H41B H 0.501011 0.643218 0.032591 0.064 Uiso 0.5 1 calc R U P B 1
C42 C 0.5154(11) 0.7220(13) 0.0875(10) 0.092(6) Uani 0.5 1 d D . P B 1
H42A H 0.514762 0.718413 0.120113 0.138 Uiso 0.5 1 calc R U P B 1
H42B H 0.487215 0.749198 0.067499 0.138 Uiso 0.5 1 calc R U P B 1
H42C H 0.543601 0.750264 0.087543 0.138 Uiso 0.5 1 calc R U P B 1
C40B C 0.5625(9) 0.622(2) 0.0834(12) 0.052(5) Uani 0.5 1 d D . P B 2
H40C H 0.567025 0.655816 0.111172 0.062 Uiso 0.5 1 calc R U P B 2
H40D H 0.575139 0.570177 0.095388 0.062 Uiso 0.5 1 calc R U P B 2
C41B C 0.5114(9) 0.6156(18) 0.0554(12) 0.054(4) Uani 0.5 1 d D . P B 2
H41C H 0.499304 0.664362 0.038687 0.064 Uiso 0.5 1 calc R U P B 2
H41D H 0.492836 0.601956 0.076114 0.064 Uiso 0.5 1 calc R U P B 2
C42B C 0.5099(11) 0.5505(15) 0.0196(10) 0.092(6) Uani 0.5 1 d D . P B 2
H42D H 0.532644 0.561327 0.003399 0.138 Uiso 0.5 1 calc R U P B 2
H42E H 0.478127 0.547295 -0.003904 0.138 Uiso 0.5 1 calc R U P B 2
H42F H 0.517820 0.501492 0.036730 0.138 Uiso 0.5 1 calc R U P B 2
C43 C 0.9067(3) 0.7893(6) 0.1940(4) 0.045(3) Uani 1 1 d . . . . .
H43A H 0.938947 0.771675 0.197347 0.055 Uiso 1 1 calc R U . . .
H43B H 0.898737 0.771056 0.221847 0.055 Uiso 1 1 calc R U . . .
C44 C 0.9039(4) 0.8762(6) 0.1908(4) 0.056(3) Uani 1 1 d . . . . .
H44A H 0.870782 0.892033 0.184589 0.067 Uiso 1 1 calc R U . . .
H44B H 0.923056 0.898049 0.221904 0.067 Uiso 1 1 calc R U . . .
C45 C 0.9201(4) 0.9085(7) 0.1537(4) 0.060(3) Uani 1 1 d . . . . .
H45A H 0.954210 0.900801 0.162350 0.089 Uiso 1 1 calc R U . . .
H45B H 0.913083 0.963682 0.150539 0.089 Uiso 1 1 calc R U . . .
H45C H 0.903990 0.882800 0.123330 0.089 Uiso 1 1 calc R U . . .
C46 C 0.8808(6) 0.6757(10) 0.0582(5) 0.130(7) Uani 1 1 d D . . . .
H46A H 0.892088 0.729561 0.061535 0.156 Uiso 1 1 calc R U . . .
H46B H 0.847004 0.675146 0.038390 0.156 Uiso 1 1 calc R U . . .
C47 C 0.9094(5) 0.6265(8) 0.0354(5) 0.083(4) Uani 1 1 d D . . . .
H47A H 0.912246 0.654272 0.007484 0.099 Uiso 1 1 calc R U . . .
H47B H 0.941538 0.620083 0.058601 0.099 Uiso 1 1 calc R U . . .
C48 C 0.8888(7) 0.5473(10) 0.0194(6) 0.150(8) Uani 1 1 d D . . . .
H48A H 0.885957 0.519010 0.046713 0.225 Uiso 1 1 calc R U . . .
H48B H 0.909674 0.519114 0.005929 0.225 Uiso 1 1 calc R U . . .
H48C H 0.857657 0.552804 -0.004931 0.225 Uiso 1 1 calc R U . . .
C49 C 0.9807(3) 0.6391(6) 0.3100(3) 0.039(2) Uani 1 1 d D . . . .
H49A H 0.959425 0.664859 0.281137 0.047 Uiso 1 1 calc R U . . .
H49B H 0.967065 0.588263 0.312787 0.047 Uiso 1 1 calc R U . . .
C50 C 1.0285(3) 0.6285(5) 0.3051(3) 0.037(2) Uani 1 1 d D . . . .
H50A H 1.049556 0.601095 0.333344 0.045 Uiso 1 1 calc R U . . .
H50B H 1.042596 0.679246 0.303066 0.045 Uiso 1 1 calc R U . . .
C51 C 1.0229(3) 0.5822(6) 0.2603(3) 0.044(3) Uani 1 1 d D . . . .
H51A H 1.007521 0.533131 0.261943 0.066 Uiso 1 1 calc R U . . .
H51B H 1.054031 0.572459 0.257692 0.066 Uiso 1 1 calc R U . . .
H51C H 1.003614 0.611174 0.232375 0.066 Uiso 1 1 calc R U . . .
C52 C 0.9974(4) 0.7240(6) 0.4529(3) 0.049(3) Uani 1 1 d D . . . .
H52A H 1.025682 0.720253 0.443068 0.059 Uiso 1 1 calc R U . . .
H52B H 0.991931 0.672996 0.464924 0.059 Uiso 1 1 calc R U . . .
C53 C 1.0056(5) 0.7831(6) 0.4920(4) 0.080(4) Uani 1 1 d D . . . .
H53A H 1.033238 0.767195 0.519340 0.096 Uiso 1 1 calc R U . . .
H53B H 0.977899 0.783870 0.502797 0.096 Uiso 1 1 calc R U . . .
C54 C 1.0140(5) 0.8640(7) 0.4773(4) 0.090(5) Uani 1 1 d D . . . .
H54A H 1.041482 0.864031 0.466558 0.134 Uiso 1 1 calc R U . . .
H54B H 1.019874 0.898730 0.504610 0.134 Uiso 1 1 calc R U . . .
H54C H 0.986220 0.881493 0.451317 0.134 Uiso 1 1 calc R U . . .
C55 C 0.7325(7) 0.8231(9) 0.4574(9) 0.112(8) Uani 0.7 1 d D . P C 1
H55A H 0.727863 0.791629 0.483223 0.134 Uiso 0.7 1 calc R U P C 1
H55B H 0.705675 0.810766 0.428397 0.134 Uiso 0.7 1 calc R U P C 1
C56 C 0.7238(10) 0.9057(9) 0.4696(8) 0.107(7) Uani 0.7 1 d D . P C 1
H56A H 0.690017 0.915673 0.464106 0.129 Uiso 0.7 1 calc R U P C 1
H56B H 0.742620 0.919232 0.502793 0.129 Uiso 0.7 1 calc R U P C 1
C57 C 0.7409(11) 0.9465(12) 0.4340(10) 0.131(9) Uani 0.7 1 d D . P C 1
H57A H 0.771071 0.971691 0.450540 0.197 Uiso 0.7 1 calc R U P C 1
H57B H 0.717703 0.985229 0.417063 0.197 Uiso 0.7 1 calc R U P C 1
H57C H 0.745145 0.909199 0.411029 0.197 Uiso 0.7 1 calc R U P C 1
C55B C 0.7717(11) 0.8631(14) 0.4511(13) 0.112(8) Uani 0.3 1 d D . P C 2
H55C H 0.783680 0.873651 0.424568 0.134 Uiso 0.3 1 calc R U P C 2
H55D H 0.798608 0.872809 0.480553 0.134 Uiso 0.3 1 calc R U P C 2
C56B C 0.7391(19) 0.928(3) 0.449(3) 0.107(7) Uani 0.3 1 d D . P C 2
H56C H 0.753406 0.957239 0.479198 0.129 Uiso 0.3 1 calc R U P C 2
H56D H 0.741320 0.962212 0.423298 0.129 Uiso 0.3 1 calc R U P C 2
C57B C 0.6883(18) 0.923(3) 0.443(2) 0.131(9) Uani 0.3 1 d D . P C 2
H57D H 0.675420 0.974655 0.442735 0.197 Uiso 0.3 1 calc R U P C 2
H57E H 0.671764 0.897746 0.412180 0.197 Uiso 0.3 1 calc R U P C 2
H57F H 0.683985 0.892717 0.468702 0.197 Uiso 0.3 1 calc R U P C 2
C58 C 0.8085(5) 0.6192(8) 0.5245(4) 0.077(4) Uani 1 1 d D . . . .
H58A H 0.842910 0.616915 0.530968 0.092 Uiso 1 1 calc R U . . .
H58B H 0.793733 0.579905 0.499994 0.092 Uiso 1 1 calc R U . . .
C59 C 0.7991(4) 0.5980(9) 0.5689(5) 0.097(5) Uani 1 1 d D . . . .
H59A H 0.820977 0.628029 0.595348 0.116 Uiso 1 1 calc R U . . .
H59B H 0.807465 0.543086 0.575447 0.116 Uiso 1 1 calc R U . . .
C60 C 0.7505(4) 0.6091(8) 0.5704(5) 0.075(4) Uani 1 1 d D . . . .
H60A H 0.735788 0.653279 0.550502 0.113 Uiso 1 1 calc R U . . .
H60B H 0.751981 0.618596 0.603305 0.113 Uiso 1 1 calc R U . . .
H60C H 0.731734 0.562837 0.558312 0.113 Uiso 1 1 calc R U . . .
C61 C 0.5777(4) 0.7880(7) 0.2194(5) 0.072(4) Uani 1 1 d . . . . .
H61A H 0.590238 0.766194 0.195324 0.087 Uiso 1 1 calc R U . . .
H61B H 0.604405 0.806739 0.246797 0.087 Uiso 1 1 calc R U . . .
C62 C 0.5431(5) 0.8534(8) 0.1979(6) 0.104(6) Uani 1 1 d . . . . .
H62A H 0.559299 0.892282 0.184624 0.124 Uiso 1 1 calc R U . . .
H62B H 0.516582 0.832489 0.171153 0.124 Uiso 1 1 calc R U . . .
C63 C 0.5241(5) 0.8913(7) 0.2311(7) 0.114(7) Uani 1 1 d . . . . .
H63A H 0.506918 0.853818 0.243580 0.171 Uiso 1 1 calc R U . . .
H63B H 0.502631 0.932462 0.214510 0.171 Uiso 1 1 calc R U . . .
H63C H 0.549980 0.913244 0.257436 0.171 Uiso 1 1 calc R U . . .
C64 C 0.5250(4) 0.6629(6) 0.3181(4) 0.046(3) Uani 1 1 d . . . . .
H64A H 0.506798 0.710566 0.306515 0.055 Uiso 1 1 calc R U . . .
H64B H 0.554882 0.676759 0.343252 0.055 Uiso 1 1 calc R U . . .
C65 C 0.4974(4) 0.6092(7) 0.3374(4) 0.057(3) Uani 1 1 d . . . . .
H65A H 0.494555 0.631625 0.366905 0.068 Uiso 1 1 calc R U . . .
H65B H 0.514955 0.560296 0.346064 0.068 Uiso 1 1 calc R U . . .
C66 C 0.4489(4) 0.5922(7) 0.3036(4) 0.063(3) Uani 1 1 d . . . . .
H66A H 0.431744 0.640535 0.293244 0.095 Uiso 1 1 calc R U . . .
H66B H 0.431888 0.560285 0.319613 0.095 Uiso 1 1 calc R U . . .
H66C H 0.451300 0.564699 0.275744 0.095 Uiso 1 1 calc R U . . .
C67 C 0.6963(4) 0.9217(8) 0.1789(4) 0.069(4) Uani 1 1 d D . . . .
H67A H 0.706620 0.887808 0.157544 0.083 Uiso 1 1 calc R U . . .
H67B H 0.714613 0.970009 0.183163 0.083 Uiso 1 1 calc R U . . .
C68 C 0.6445(4) 0.9397(7) 0.1558(4) 0.073(4) Uani 1 1 d D . . . .
H68A H 0.626681 0.890844 0.148645 0.088 Uiso 1 1 calc R U . . .
H68B H 0.633530 0.968770 0.178686 0.088 Uiso 1 1 calc R U . . .
C69 C 0.6336(5) 0.9857(11) 0.1105(5) 0.140(8) Uani 1 1 d D . . . .
H69A H 0.637298 1.040609 0.118198 0.209 Uiso 1 1 calc R U . . .
H69B H 0.601039 0.975538 0.090138 0.209 Uiso 1 1 calc R U . . .
H69C H 0.655194 0.970802 0.093628 0.209 Uiso 1 1 calc R U . . .
C70 C 0.8253(5) 0.9530(9) 0.2996(5) 0.093(4) Uani 1 1 d D . . . .
H70A H 0.837414 0.996174 0.285305 0.111 Uiso 1 1 calc R U . . .
H70B H 0.842855 0.905906 0.297147 0.111 Uiso 1 1 calc R U . . .
C71 C 0.8323(5) 0.9703(13) 0.3517(5) 0.178(11) Uani 1 1 d D . . . .
H71A H 0.820281 1.022530 0.354151 0.214 Uiso 1 1 calc R U . . .
H71B H 0.813696 0.933258 0.363366 0.214 Uiso 1 1 calc R U . . .
C72 C 0.8835(5) 0.9655(10) 0.3830(5) 0.104(5) Uani 1 1 d D . . . .
H72A H 0.895935 0.914520 0.379772 0.157 Uiso 1 1 calc R U . . .
H72B H 0.885932 0.974051 0.416277 0.157 Uiso 1 1 calc R U . . .
H72C H 0.901670 1.004913 0.373205 0.157 Uiso 1 1 calc R U . . .
C73 C 0.5204(5) 0.0109(8) 0.9930(4) 0.079(4) Uani 1 1 d D . . . .
H73A H 0.538860 -0.036052 0.992377 0.095 Uiso 1 1 calc R U . . .
H73B H 0.540920 0.045582 1.017600 0.095 Uiso 1 1 calc R U . . .
C74 C 0.5081(4) 0.0505(9) 0.9448(5) 0.093(5) Uani 1 1 d D . . . .
H74A H 0.487440 0.095017 0.944374 0.112 Uiso 1 1 calc R U . . .
H74B H 0.489893 0.014183 0.919765 0.112 Uiso 1 1 calc R U . . .
C75 C 0.5507(5) 0.0785(10) 0.9325(6) 0.112(6) Uani 1 1 d D . . . .
H75A H 0.573000 0.103793 0.960337 0.168 Uiso 1 1 calc R U . . .
H75B H 0.540355 0.115173 0.906001 0.168 Uiso 1 1 calc R U . . .
H75C H 0.566109 0.034597 0.923181 0.168 Uiso 1 1 calc R U . . .
O1 O 0.7588(2) 0.1034(3) 0.2189(2) 0.0302(14) Uani 1 1 d . . . . .
O2 O 0.7359(2) 0.1293(3) 0.2888(2) 0.0306(14) Uani 1 1 d . . . . .
O3 O 0.81312(19) 0.2817(3) 0.09057(19) 0.0246(13) Uani 1 1 d . . . . .
O4 O 0.7410(2) 0.3252(4) 0.0289(2) 0.0337(15) Uani 1 1 d . . . . .
O5 O 0.9635(2) 0.2846(3) 0.2738(2) 0.0287(14) Uani 1 1 d . . . . .
O6 O 0.98272(19) 0.3921(3) 0.2306(2) 0.0264(13) Uani 1 1 d . . . . .
O7 O 0.8556(2) 0.3015(4) 0.4575(2) 0.0405(16) Uani 1 1 d . . . . .
O8 O 0.9161(2) 0.3902(3) 0.4963(2) 0.0316(14) Uani 1 1 d . . . . .
O9 O 0.6000(2) 0.3190(4) 0.3534(2) 0.0395(16) Uani 1 1 d . . . . .
O10 O 0.6642(2) 0.3521(4) 0.4269(2) 0.051(2) Uani 1 1 d . . . . .
O11 O 0.5764(2) 0.2557(3) 0.1400(2) 0.0362(15) Uani 1 1 d . . . . .
O12 O 0.5163(2) 0.3537(4) 0.1291(2) 0.0409(17) Uani 1 1 d . . . . .
O13 O 0.6534(2) 0.6977(4) 0.0293(2) 0.0409(16) Uani 1 1 d . . . . .
O14 O 0.5877(2) 0.6525(4) 0.0531(2) 0.0429(17) Uani 1 1 d D . . . .
O15 O 0.8739(3) 0.7604(5) 0.1513(3) 0.096(4) Uani 1 1 d . . . . .
O16 O 0.8870(3) 0.6440(7) 0.1021(3) 0.102(4) Uani 1 1 d . . . . .
O17 O 0.98437(19) 0.6851(3) 0.3517(2) 0.0255(13) Uani 1 1 d . . . . .
O18 O 0.95710(19) 0.7453(3) 0.4125(2) 0.0301(14) Uani 1 1 d . . . . .
O19 O 0.7673(4) 0.7947(5) 0.4504(3) 0.091(3) Uani 1 1 d D . . . .
O20 O 0.7926(2) 0.6910(4) 0.5055(2) 0.0444(17) Uani 1 1 d . . . . .
O21 O 0.5509(2) 0.7312(4) 0.2346(3) 0.0453(18) Uani 1 1 d . . . . .
O22 O 0.5347(2) 0.6243(3) 0.2791(2) 0.0349(15) Uani 1 1 d . . . . .
O23 O 0.7056(3) 0.8877(6) 0.2206(3) 0.088(3) Uani 1 1 d . . . . .
O24 O 0.7773(3) 0.9426(4) 0.2752(3) 0.068(2) Uani 1 1 d . . . . .
P1 P 0.74615(8) 0.17279(13) 0.24676(8) 0.0244(5) Uani 1 1 d . . . . .
P2 P 0.77415(8) 0.34617(13) 0.08125(8) 0.0243(5) Uani 1 1 d . . . . .
P3 P 0.94158(7) 0.36214(12) 0.24735(8) 0.0208(5) Uani 1 1 d . . . . .
P4 P 0.87465(8) 0.38296(13) 0.44710(8) 0.0269(5) Uani 1 1 d . . . . .
P5 P 0.64990(9) 0.35785(17) 0.37072(9) 0.0393(7) Uani 1 1 d . . . . .
P6 P 0.57087(8) 0.34021(14) 0.15709(9) 0.0313(6) Uani 1 1 d . . . . .
P7 P 0.64341(8) 0.65479(15) 0.07137(10) 0.0378(6) Uani 1 1 d . . . . .
P8 P 0.86040(10) 0.67356(17) 0.13711(9) 0.0429(7) Uani 1 1 d . . . . .
P9 P 0.93965(8) 0.68867(13) 0.36898(8) 0.0235(5) Uani 1 1 d . . . . .
P10 P 0.78374(9) 0.70968(15) 0.45107(9) 0.0362(6) Uani 1 1 d . . . . .
P11 P 0.57461(8) 0.65446(15) 0.26018(9) 0.0339(6) Uani 1 1 d . . . . .
P12 P 0.75738(10) 0.86364(14) 0.25545(10) 0.0401(7) Uani 1 1 d . . . . .
Pt1 Pt 0.75884(2) 0.51974(2) 0.26221(2) 0.01678(7) Uani 1 1 d . . . . .
S1 S 0.80495(8) 0.23311(12) 0.27963(8) 0.0282(5) Uani 1 1 d . . . . .
S2 S 0.69155(8) 0.22961(13) 0.20405(8) 0.0302(5) Uani 1 1 d . . . . .
S3 S 0.80133(8) 0.45154(13) 0.07915(8) 0.0289(5) Uani 1 1 d . . . . .
S4 S 0.74136(7) 0.32477(12) 0.12805(8) 0.0253(5) Uani 1 1 d . . . . .
S5 S 0.93147(7) 0.43783(13) 0.29207(8) 0.0255(5) Uani 1 1 d . . . . .
S6 S 0.88690(7) 0.33400(13) 0.18858(8) 0.0260(5) Uani 1 1 d . . . . .
S7 S 0.89543(8) 0.38189(13) 0.39121(8) 0.0302(5) Uani 1 1 d . . . . .
S8 S 0.82434(8) 0.46275(13) 0.44283(8) 0.0274(5) Uani 1 1 d . . . . .
S9 S 0.69756(9) 0.29801(17) 0.35136(9) 0.0431(7) Uani 1 1 d . . . . .
S10 S 0.64149(9) 0.46796(16) 0.35103(9) 0.0432(7) Uani 1 1 d . . . . .
S11 S 0.57891(8) 0.32981(14) 0.22699(9) 0.0323(5) Uani 1 1 d . . . . .
S12 S 0.60973(8) 0.41583(15) 0.13754(9) 0.0391(6) Uani 1 1 d . . . . .
S13 S 0.66745(9) 0.54732(15) 0.07539(11) 0.0515(8) Uani 1 1 d . . . . .
S14 S 0.66398(9) 0.71569(15) 0.13227(10) 0.0453(7) Uani 1 1 d . . . . .
S15 S 0.79080(9) 0.68010(14) 0.10033(10) 0.0435(7) Uani 1 1 d . . . . .
S16 S 0.88422(9) 0.60467(15) 0.19321(8) 0.0374(6) Uani 1 1 d . . . . .
S17 S 0.88644(8) 0.73931(13) 0.31843(8) 0.0298(5) Uani 1 1 d . . . . .
S18 S 0.92744(7) 0.58133(12) 0.38646(8) 0.0267(5) Uani 1 1 d . . . . .
S19 S 0.84650(9) 0.71799(14) 0.44077(8) 0.0352(6) Uani 1 1 d . . . . .
S20 S 0.73559(10) 0.6407(2) 0.41067(10) 0.0614(9) Uani 1 1 d . . . . .
S21 S 0.57701(9) 0.57833(15) 0.20985(9) 0.0398(6) Uani 1 1 d . . . . .
S22 S 0.63492(9) 0.67340(17) 0.31082(11) 0.0520(8) Uani 1 1 d . . . . .
S23 S 0.79633(9) 0.81561(15) 0.22057(10) 0.0424(6) Uani 1 1 d . . . . .
S24 S 0.74102(9) 0.80037(15) 0.30323(11) 0.0467(7) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
S1 Ag1 Pt1 153.82(6) .
S1 Ag1 Ag5 139.30(6) .
Pt1 Ag1 Ag5 59.339(19) .
S1 Ag1 Ag4 107.94(6) .
Pt1 Ag1 Ag4 59.887(19) .
Ag5 Ag1 Ag4 62.74(2) .
S1 Ag1 Ag2 113.26(6) .
Pt1 Ag1 Ag2 57.559(18) .
Ag5 Ag1 Ag2 106.94(3) .
Ag4 Ag1 Ag2 109.06(3) .
S1 Ag1 Ag3 95.11(5) .
Pt1 Ag1 Ag3 58.733(18) .
Ag5 Ag1 Ag3 109.51(3) .
Ag4 Ag1 Ag3 59.34(2) .
Ag2 Ag1 Ag3 61.81(2) .
S1 Ag1 Ag18 54.93(5) .
Pt1 Ag1 Ag18 107.22(2) .
Ag5 Ag1 Ag18 165.75(3) .
Ag4 Ag1 Ag18 116.35(3) .
Ag2 Ag1 Ag18 59.23(2) .
Ag3 Ag1 Ag18 62.24(2) .
S1 Ag1 Ag19 98.12(5) .
Pt1 Ag1 Ag19 108.03(2) .
Ag5 Ag1 Ag19 62.11(2) .
Ag4 Ag1 Ag19 119.62(3) .
Ag2 Ag1 Ag19 108.60(3) .
Ag3 Ag1 Ag19 166.12(3) .
Ag18 Ag1 Ag19 123.20(3) .
S1 Ag1 Ag6 142.69(6) .
Pt1 Ag1 Ag6 57.007(18) .
Ag5 Ag1 Ag6 59.70(2) .
Ag4 Ag1 Ag6 109.13(3) .
Ag2 Ag1 Ag6 57.24(2) .
Ag3 Ag1 Ag6 107.21(3) .
Ag18 Ag1 Ag6 110.08(3) .
Ag19 Ag1 Ag6 59.28(2) .
S4 Ag2 Pt1 154.70(6) .
S4 Ag2 Ag6 103.06(5) .
Pt1 Ag2 Ag6 59.532(19) .
S4 Ag2 Ag18 60.03(5) .
Pt1 Ag2 Ag18 109.08(3) .
Ag6 Ag2 Ag18 116.85(3) .
S4 Ag2 Ag16 95.91(6) .
Pt1 Ag2 Ag16 107.69(3) .
Ag6 Ag2 Ag16 113.35(3) .
Ag18 Ag2 Ag16 127.81(3) .
S4 Ag2 Ag1 98.32(5) .
Pt1 Ag2 Ag1 58.332(18) .
Ag6 Ag2 Ag1 63.52(2) .
Ag18 Ag2 Ag1 60.70(2) .
Ag16 Ag2 Ag1 165.77(3) .
S4 Ag2 Ag9 147.23(5) .
Pt1 Ag2 Ag9 56.937(18) .
Ag6 Ag2 Ag9 107.52(3) .
Ag18 Ag2 Ag9 113.67(3) .
Ag16 Ag2 Ag9 61.27(2) .
Ag1 Ag2 Ag9 105.58(3) .
S4 Ag2 Ag8 131.66(6) .
Pt1 Ag2 Ag8 58.166(19) .
Ag6 Ag2 Ag8 59.02(2) .
Ag18 Ag2 Ag8 167.23(3) .
Ag16 Ag2 Ag8 60.86(2) .
Ag1 Ag2 Ag8 108.85(3) .
Ag9 Ag2 Ag8 60.14(2) .
S4 Ag2 Ag17 90.64(5) .
Pt1 Ag2 Ag17 107.43(2) .
Ag6 Ag2 Ag17 166.30(3) .
Ag18 Ag2 Ag17 69.80(2) .
Ag16 Ag2 Ag17 64.64(2) .
Ag1 Ag2 Ag17 114.78(3) .
Ag9 Ag2 Ag17 59.16(2) .
Ag8 Ag2 Ag17 111.67(3) .
S4 Ag2 Ag3 121.16(5) .
Pt1 Ag2 Ag3 58.061(18) .
Ag6 Ag2 Ag3 110.23(3) .
Ag18 Ag2 Ag3 61.88(2) .
Ag16 Ag2 Ag3 112.34(3) .
Ag1 Ag2 Ag3 59.37(2) .
Ag9 Ag2 Ag3 57.72(2) .
Ag8 Ag2 Ag3 107.10(3) .
Ag17 Ag2 Ag3 61.08(2) .
S5 Ag3 Pt1 157.42(6) .
S5 Ag3 Ag4 110.88(6) .
Pt1 Ag3 Ag4 59.498(18) .
S5 Ag3 Ag9 113.81(6) .
Pt1 Ag3 Ag9 57.351(18) .
Ag4 Ag3 Ag9 107.88(3) .
S5 Ag3 Ag10 97.82(5) .
Pt1 Ag3 Ag10 59.603(18) .
Ag4 Ag3 Ag10 60.61(2) .
Ag9 Ag3 Ag10 59.80(2) .
S5 Ag3 Ag1 138.42(6) .
Pt1 Ag3 Ag1 57.526(18) .
Ag4 Ag3 Ag1 59.37(2) .
Ag9 Ag3 Ag1 107.34(3) .
Ag10 Ag3 Ag1 107.86(3) .
S5 Ag3 Ag2 141.43(6) .
Pt1 Ag3 Ag2 56.153(17) .
Ag4 Ag3 Ag2 106.69(2) .
Ag9 Ag3 Ag2 60.46(2) .
Ag10 Ag3 Ag2 107.99(2) .
Ag1 Ag3 Ag2 58.82(2) .
S5 Ag3 Ag18 98.92(5) .
Pt1 Ag3 Ag18 103.66(2) .
Ag4 Ag3 Ag18 113.35(3) .
Ag9 Ag3 Ag18 111.96(3) .
Ag10 Ag3 Ag18 163.24(3) .
Ag1 Ag3 Ag18 58.90(2) .
Ag2 Ag3 Ag18 57.23(2) .
S5 Ag3 Ag17 84.40(5) .
Pt1 Ag3 Ag17 104.45(2) .
Ag4 Ag3 Ag17 163.92(3) .
Ag9 Ag3 Ag17 59.41(2) .
Ag10 Ag3 Ag17 113.83(3) .
Ag1 Ag3 Ag17 112.69(3) .
Ag2 Ag3 Ag17 59.29(2) .
Ag18 Ag3 Ag17 67.28(2) .
S7 Ag4 S8 76.47(7) .
S7 Ag4 Pt1 142.23(5) .
S8 Ag4 Pt1 140.36(5) .
S7 Ag4 Ag3 83.42(5) .
S8 Ag4 Ag3 156.65(5) .
Pt1 Ag4 Ag3 58.814(18) .
S7 Ag4 Ag1 105.06(5) .
S8 Ag4 Ag1 135.55(5) .
Pt1 Ag4 Ag1 57.964(18) .
Ag3 Ag4 Ag1 61.29(2) .
S7 Ag4 Ag11 148.11(6) .
S8 Ag4 Ag11 83.98(5) .
Pt1 Ag4 Ag11 57.866(19) .
Ag3 Ag4 Ag11 108.25(3) .
Ag1 Ag4 Ag11 106.54(3) .
S7 Ag4 Ag10 104.47(6) .
S8 Ag4 Ag10 113.58(5) .
Pt1 Ag4 Ag10 59.210(18) .
Ag3 Ag4 Ag10 60.10(2) .
Ag1 Ag4 Ag10 108.97(3) .
Ag11 Ag4 Ag10 60.87(2) .
S7 Ag4 Ag13 85.35(5) .
S8 Ag4 Ag13 52.85(5) .
Pt1 Ag4 Ag13 109.60(2) .
Ag3 Ag4 Ag13 114.33(3) .
Ag1 Ag4 Ag13 167.55(3) .
Ag11 Ag4 Ag13 62.76(2) .
Ag10 Ag4 Ag13 60.97(2) .
S7 Ag4 Ag5 146.83(6) .
S8 Ag4 Ag5 95.78(5) .
Pt1 Ag4 Ag5 57.221(18) .
Ag3 Ag4 Ag5 107.56(3) .
Ag1 Ag4 Ag5 58.32(2) .
Ag11 Ag4 Ag5 59.20(2) .
Ag10 Ag4 Ag5 108.11(3) .
Ag13 Ag4 Ag5 115.89(3) .
S10 Ag5 Pt1 144.78(7) .
S10 Ag5 Ag1 153.07(6) .
Pt1 Ag5 Ag1 58.542(18) .
S10 Ag5 Ag11 99.70(6) .
Pt1 Ag5 Ag11 58.154(19) .
Ag1 Ag5 Ag11 106.91(3) .
S10 Ag5 Ag7 86.14(7) .
Pt1 Ag5 Ag7 59.485(19) .
Ag1 Ag5 Ag7 110.58(3) .
Ag11 Ag5 Ag7 60.06(2) .
S10 Ag5 Ag6 112.97(7) .
Pt1 Ag5 Ag6 57.997(18) .
Ag1 Ag5 Ag6 63.17(2) .
Ag11 Ag5 Ag6 107.01(3) .
Ag7 Ag5 Ag6 59.55(2) .
S10 Ag5 S9 75.01(8) .
Pt1 Ag5 S9 139.71(6) .
Ag1 Ag5 S9 81.39(5) .
Ag11 Ag5 S9 142.05(6) .
Ag7 Ag5 S9 152.50(6) .
Ag6 Ag5 S9 109.58(6) .
S10 Ag5 Ag4 137.25(6) .
Pt1 Ag5 Ag4 58.297(18) .
Ag1 Ag5 Ag4 58.94(2) .
Ag11 Ag5 Ag4 59.04(2) .
Ag7 Ag5 Ag4 108.30(3) .
Ag6 Ag5 Ag4 108.88(3) .
S9 Ag5 Ag4 99.09(5) .
S10 Ag5 Ag19 92.70(6) .
Pt1 Ag5 Ag19 107.08(2) .
Ag1 Ag5 Ag19 61.66(2) .
Ag11 Ag5 Ag19 165.20(3) .
Ag7 Ag5 Ag19 113.28(3) .
Ag6 Ag5 Ag19 60.19(2) .
S9 Ag5 Ag19 49.43(5) .
Ag4 Ag5 Ag19 115.78(3) .
S10 Ag5 Ag20 52.31(6) .
Pt1 Ag5 Ag20 109.46(3) .
Ag1 Ag5 Ag20 116.36(3) .
Ag11 Ag5 Ag20 115.88(3) .
Ag7 Ag5 Ag20 61.57(2) .
Ag6 Ag5 Ag20 60.70(2) .
S9 Ag5 Ag20 90.95(5) .
Ag4 Ag5 Ag20 167.75(3) .
Ag19 Ag5 Ag20 66.02(2) .
S12 Ag6 Pt1 154.54(6) .
S12 Ag6 Ag2 104.47(7) .
Pt1 Ag6 Ag2 58.115(18) .
S12 Ag6 Ag8 97.27(6) .
Pt1 Ag6 Ag8 59.048(19) .
Ag2 Ag6 Ag8 62.70(2) .
S12 Ag6 Ag7 119.44(7) .
Pt1 Ag6 Ag7 59.779(19) .
Ag2 Ag6 Ag7 110.55(3) .
Ag8 Ag6 Ag7 60.89(2) .
S12 Ag6 Ag5 146.36(6) .
Pt1 Ag6 Ag5 58.169(18) .
Ag2 Ag6 Ag5 106.45(3) .
Ag8 Ag6 Ag5 108.43(3) .
Ag7 Ag6 Ag5 60.20(2) .
S12 Ag6 Ag19 95.00(6) .
Pt1 Ag6 Ag19 108.33(3) .
Ag2 Ag6 Ag19 111.09(3) .
Ag8 Ag6 Ag19 167.35(3) .
Ag7 Ag6 Ag19 115.06(3) .
Ag5 Ag6 Ag19 61.57(2) .
S12 Ag6 Ag1 134.15(7) .
Pt1 Ag6 Ag1 56.438(17) .
Ag2 Ag6 Ag1 59.24(2) .
Ag8 Ag6 Ag1 108.38(3) .
Ag7 Ag6 Ag1 106.26(3) .
Ag5 Ag6 Ag1 57.13(2) .
Ag19 Ag6 Ag1 60.19(2) .
S12 Ag6 Ag20 87.34(7) .
Pt1 Ag6 Ag20 110.76(3) .
Ag2 Ag6 Ag20 168.20(3) .
Ag8 Ag6 Ag20 116.57(3) .
Ag7 Ag6 Ag20 62.27(2) .
Ag5 Ag6 Ag20 62.08(2) .
Ag19 Ag6 Ag20 67.02(2) .
Ag1 Ag6 Ag20 112.32(3) .
S22 Ag7 Ag21 47.43(18) .
S22 Ag7 S21 76.40(8) .
Ag21 Ag7 S21 114.83(17) .
S22 Ag7 Pt1 143.59(6) .
Ag21 Ag7 Pt1 104.88(17) .
S21 Ag7 Pt1 138.74(6) .
S22 Ag7 Ag6 148.70(7) .
Ag21 Ag7 Ag6 162.35(17) .
S21 Ag7 Ag6 81.96(6) .
Pt1 Ag7 Ag6 57.638(18) .
S22 Ag7 Ag11 86.26(6) .
Ag21 Ag7 Ag11 59.56(16) .
S21 Ag7 Ag11 157.17(6) .
Pt1 Ag7 Ag11 57.365(19) .
Ag6 Ag7 Ag11 107.15(3) .
S22 Ag7 Ag8 145.21(8) .
Ag21 Ag7 Ag8 111.42(17) .
S21 Ag7 Ag8 96.07(6) .
Pt1 Ag7 Ag8 57.665(19) .
Ag6 Ag7 Ag8 58.85(2) .
Ag11 Ag7 Ag8 106.58(3) .
S22 Ag7 Ag5 107.46(8) .
Ag21 Ag7 Ag5 114.40(17) .
S21 Ag7 Ag5 111.51(6) .
Pt1 Ag7 Ag5 57.535(18) .
Ag6 Ag7 Ag5 60.25(2) .
Ag11 Ag7 Ag5 59.53(2) .
Ag8 Ag7 Ag5 106.87(3) .
S22 Ag7 Ag12 105.03(7) .
Ag21 Ag7 Ag12 57.82(17) .
S21 Ag7 Ag12 139.77(6) .
Pt1 Ag7 Ag12 57.139(18) .
Ag6 Ag7 Ag12 106.11(3) .
Ag11 Ag7 Ag12 59.02(2) .
Ag8 Ag7 Ag12 59.41(2) .
Ag5 Ag7 Ag12 106.33(3) .
S22 Ag7 Ag20 87.79(7) .
Ag21 Ag7 Ag20 133.63(17) .
S21 Ag7 Ag20 50.06(6) .
Pt1 Ag7 Ag20 107.95(3) .
Ag6 Ag7 Ag20 60.93(2) .
Ag11 Ag7 Ag20 115.46(3) .
Ag8 Ag7 Ag20 113.60(3) .
Ag5 Ag7 Ag20 61.62(2) .
Ag12 Ag7 Ag20 165.06(3) .
S14 Ag8 Pt1 147.00(7) .
S14 Ag8 Ag6 138.11(6) .
Pt1 Ag8 Ag6 58.696(19) .
S14 Ag8 Ag15 53.80(6) .
Pt1 Ag8 Ag15 108.42(3) .
Ag6 Ag8 Ag15 166.92(3) .
S14 Ag8 Ag12 89.56(6) .
Pt1 Ag8 Ag12 58.030(19) .
Ag6 Ag8 Ag12 108.00(3) .
Ag15 Ag8 Ag12 62.60(3) .
S14 Ag8 Ag7 101.03(7) .
Pt1 Ag8 Ag7 59.44(2) .
Ag6 Ag8 Ag7 60.26(2) .
Ag15 Ag8 Ag7 116.84(3) .
Ag12 Ag8 Ag7 60.40(2) .
S14 Ag8 S13 74.07(8) .
Pt1 Ag8 S13 138.46(6) .
Ag6 Ag8 S13 96.30(6) .
Ag15 Ag8 S13 92.84(6) .
Ag12 Ag8 S13 155.43(6) .
Ag7 Ag8 S13 139.77(6) .
S14 Ag8 Ag9 115.07(6) .
Pt1 Ag8 Ag9 56.276(18) .
Ag6 Ag8 Ag9 106.54(3) .
Ag15 Ag8 Ag9 61.27(2) .
Ag12 Ag8 Ag9 59.63(2) .
Ag7 Ag8 Ag9 107.56(3) .
S13 Ag8 Ag9 110.54(6) .
S14 Ag8 Ag16 94.70(7) .
Pt1 Ag8 Ag16 104.19(2) .
Ag6 Ag8 Ag16 110.37(3) .
Ag15 Ag8 Ag16 68.86(3) .
Ag12 Ag8 Ag16 114.99(3) .
Ag7 Ag8 Ag16 163.42(3) .
S13 Ag8 Ag16 50.33(6) .
Ag9 Ag8 Ag16 60.22(2) .
S14 Ag8 Ag2 152.15(7) .
Pt1 Ag8 Ag2 56.497(18) .
Ag6 Ag8 Ag2 58.28(2) .
Ag15 Ag8 Ag2 114.03(3) .
Ag12 Ag8 Ag2 107.07(3) .
Ag7 Ag8 Ag2 106.59(3) .
S13 Ag8 Ag2 82.44(6) .
Ag9 Ag8 Ag2 59.66(2) .
Ag16 Ag8 Ag2 58.23(2) .
S16 Ag9 Pt1 151.27(6) .
S16 Ag9 Ag3 92.29(6) .
Pt1 Ag9 Ag3 59.737(18) .
S16 Ag9 Ag10 101.45(6) .
Pt1 Ag9 Ag10 60.602(19) .
Ag3 Ag9 Ag10 60.43(2) .
S16 Ag9 Ag12 135.32(6) .
Pt1 Ag9 Ag12 58.45(2) .
Ag3 Ag9 Ag12 108.70(3) .
Ag10 Ag9 Ag12 60.60(2) .
S16 Ag9 Ag17 56.83(6) .
Pt1 Ag9 Ag17 109.21(2) .
Ag3 Ag9 Ag17 63.11(2) .
Ag10 Ag9 Ag17 117.71(3) .
Ag12 Ag9 Ag17 167.31(3) .
S16 Ag9 Ag2 117.63(6) .
Pt1 Ag9 Ag2 57.287(18) .
Ag3 Ag9 Ag2 61.82(2) .
Ag10 Ag9 Ag2 109.56(3) .
Ag12 Ag9 Ag2 107.04(3) .
Ag17 Ag9 Ag2 60.91(2) .
S16 Ag9 Ag8 148.01(6) .
Pt1 Ag9 Ag8 58.294(19) .
Ag3 Ag9 Ag8 110.46(3) .
Ag10 Ag9 Ag8 109.20(3) .
Ag12 Ag9 Ag8 59.05(2) .
Ag17 Ag9 Ag8 113.23(3) .
Ag2 Ag9 Ag8 60.20(2) .
S16 Ag9 Ag15 100.86(6) .
Pt1 Ag9 Ag15 107.14(3) .
Ag3 Ag9 Ag15 166.84(3) .
Ag10 Ag9 Ag15 115.59(3) .
Ag12 Ag9 Ag15 61.15(2) .
Ag17 Ag9 Ag15 125.13(3) .
Ag2 Ag9 Ag15 111.44(3) .
Ag8 Ag9 Ag15 57.77(2) .
S16 Ag9 Ag16 90.95(6) .
Pt1 Ag9 Ag16 105.51(2) .
Ag3 Ag9 Ag16 113.34(3) .
Ag10 Ag9 Ag16 166.10(3) .
Ag12 Ag9 Ag16 114.17(3) .
Ag17 Ag9 Ag16 64.20(2) .
Ag2 Ag9 Ag16 58.30(2) .
Ag8 Ag9 Ag16 59.90(2) .
Ag15 Ag9 Ag16 67.37(2) .
S18 Ag10 S17 75.30(6) .
S18 Ag10 Pt1 143.68(5) .
S17 Ag10 Pt1 141.02(5) .
S18 Ag10 Ag9 136.96(5) .
S17 Ag10 Ag9 96.04(5) .
Pt1 Ag10 Ag9 56.952(18) .
S18 Ag10 Ag3 97.13(5) .
S17 Ag10 Ag3 135.69(6) .
Pt1 Ag10 Ag3 58.350(18) .
Ag9 Ag10 Ag3 59.77(2) .
S18 Ag10 Ag4 86.34(5) .
S17 Ag10 Ag4 157.06(5) .
Pt1 Ag10 Ag4 58.638(18) .
Ag9 Ag10 Ag4 106.81(3) .
Ag3 Ag10 Ag4 59.29(2) .
S18 Ag10 Ag12 154.75(5) .
S17 Ag10 Ag12 85.70(5) .
Pt1 Ag10 Ag12 57.333(19) .
Ag9 Ag10 Ag12 60.51(2) .
Ag3 Ag10 Ag12 108.10(3) .
Ag4 Ag10 Ag12 107.09(3) .
S18 Ag10 Ag11 115.22(5) .
S17 Ag10 Ag11 116.32(5) .
Pt1 Ag10 Ag11 57.202(18) .
Ag9 Ag10 Ag11 106.46(3) .
Ag3 Ag10 Ag11 106.47(3) .
Ag4 Ag10 Ag11 59.43(2) .
Ag12 Ag10 Ag11 58.89(2) .
S18 Ag10 Ag14 93.33(5) .
S17 Ag10 Ag14 52.71(5) .
Pt1 Ag10 Ag14 109.85(2) .
Ag9 Ag10 Ag14 114.98(3) .
Ag3 Ag10 Ag14 168.20(3) .
Ag4 Ag10 Ag14 116.25(3) .
Ag12 Ag10 Ag14 61.66(2) .
Ag11 Ag10 Ag14 63.80(2) .
S18 Ag10 Ag13 53.12(5) .
S17 Ag10 Ag13 96.99(5) .
Pt1 Ag10 Ag13 108.79(2) .
Ag9 Ag10 Ag13 165.68(3) .
Ag3 Ag10 Ag13 113.25(3) .
Ag4 Ag10 Ag13 60.54(2) .
Ag12 Ag10 Ag13 114.63(3) .
Ag11 Ag10 Ag13 62.13(2) .
Ag14 Ag10 Ag13 69.18(2) .
S20 Ag11 Pt1 162.35(7) .
S20 Ag11 Ag21 72.28(19) .
Pt1 Ag11 Ag21 105.68(17) .
S20 Ag11 Ag12 127.66(9) .
Pt1 Ag11 Ag12 58.477(19) .
Ag21 Ag11 Ag12 57.98(17) .
S20 Ag11 Ag4 122.51(9) .
Pt1 Ag11 Ag4 59.410(19) .
Ag21 Ag11 Ag4 164.93(18) .
Ag12 Ag11 Ag4 108.44(3) .
S20 Ag11 Ag5 105.57(8) .
Pt1 Ag11 Ag5 58.579(19) .
Ag21 Ag11 Ag5 113.95(16) .
Ag12 Ag11 Ag5 108.38(3) .
Ag4 Ag11 Ag5 61.76(2) .
S20 Ag11 Ag7 106.90(7) .
Pt1 Ag11 Ag7 59.747(19) .
Ag21 Ag11 Ag7 58.18(17) .
Ag12 Ag11 Ag7 60.75(2) .
Ag4 Ag11 Ag7 110.78(3) .
Ag5 Ag11 Ag7 60.41(2) .
S20 Ag11 Ag10 138.17(7) .
Pt1 Ag11 Ag10 59.279(18) .
Ag21 Ag11 Ag10 112.26(17) .
Ag12 Ag11 Ag10 60.28(2) .
Ag4 Ag11 Ag10 59.71(2) .
Ag5 Ag11 Ag10 109.22(3) .
Ag7 Ag11 Ag10 110.08(3) .
S20 Ag11 Ag13 84.88(7) .
Pt1 Ag11 Ag13 108.38(2) .
Ag21 Ag11 Ag13 129.43(17) .
Ag12 Ag11 Ag13 113.61(3) .
Ag4 Ag11 Ag13 59.74(2) .
Ag5 Ag11 Ag13 115.47(3) .
Ag7 Ag11 Ag13 168.10(3) .
Ag10 Ag11 Ag13 59.58(2) .
S20 Ag11 Ag14 88.59(8) .
Pt1 Ag11 Ag14 107.22(2) .
Ag21 Ag11 Ag14 68.62(16) .
Ag12 Ag11 Ag14 60.23(2) .
Ag4 Ag11 Ag14 111.87(3) .
Ag5 Ag11 Ag14 165.78(3) .
Ag7 Ag11 Ag14 114.75(3) .
Ag10 Ag11 Ag14 58.54(2) .
Ag13 Ag11 Ag14 66.26(2) .
S24 Ag12 Pt1 143.91(7) .
S24 Ag12 Ag21 39.99(17) .
Pt1 Ag12 Ag21 107.62(16) .
S24 Ag12 Ag11 86.30(7) .
Pt1 Ag12 Ag11 58.56(2) .
Ag21 Ag12 Ag11 60.29(16) .
S24 Ag12 Ag8 137.03(7) .
Pt1 Ag12 Ag8 58.710(19) .
Ag21 Ag12 Ag8 112.91(17) .
Ag11 Ag12 Ag8 108.17(3) .
S24 Ag12 Ag9 153.74(7) .
Pt1 Ag12 Ag9 57.061(18) .
Ag21 Ag12 Ag9 164.68(16) .
Ag11 Ag12 Ag9 106.72(3) .
Ag8 Ag12 Ag9 61.32(2) .
S24 Ag12 Ag10 112.63(7) .
Pt1 Ag12 Ag10 59.506(19) .
Ag21 Ag12 Ag10 114.80(17) .
Ag11 Ag12 Ag10 60.84(2) .
Ag8 Ag12 Ag10 109.66(3) .
Ag9 Ag12 Ag10 58.89(2) .
S24 Ag12 Ag7 97.53(6) .
Pt1 Ag12 Ag7 59.59(2) .
Ag21 Ag12 Ag7 58.71(17) .
Ag11 Ag12 Ag7 60.23(2) .
Ag8 Ag12 Ag7 60.20(2) .
Ag9 Ag12 Ag7 108.73(3) .
Ag10 Ag12 Ag7 110.12(3) .
S24 Ag12 Ag15 109.40(7) .
Pt1 Ag12 Ag15 105.43(3) .
Ag11 Ag12 Ag15 163.98(3) .
Ag8 Ag12 Ag15 58.21(2) .
Ag9 Ag12 Ag15 60.38(2) .
Ag10 Ag12 Ag15 113.39(3) .
Ag7 Ag12 Ag15 112.75(3) .
S24 Ag12 Ag14 52.82(6) .
Pt1 Ag12 Ag14 110.17(3) .
Ag21 Ag12 Ag14 70.98(17) .
Ag11 Ag12 Ag14 63.83(2) .
Ag8 Ag12 Ag14 168.71(3) .
Ag9 Ag12 Ag14 112.03(3) .
Ag10 Ag12 Ag14 59.89(2) .
Ag7 Ag12 Ag14 117.47(3) .
Ag15 Ag12 Ag14 128.13(3) .
S19 Ag13 S8 125.98(8) .
S19 Ag13 S18 107.56(8) .
S8 Ag13 S18 123.63(7) .
S19 Ag13 Ag4 144.72(6) .
S8 Ag13 Ag4 58.42(5) .
S18 Ag13 Ag4 88.75(5) .
S19 Ag13 Ag10 102.67(6) .
S8 Ag13 Ag10 116.67(6) .
S18 Ag13 Ag10 59.44(5) .
Ag4 Ag13 Ag10 58.49(2) .
S19 Ag13 Ag11 87.33(6) .
S8 Ag13 Ag11 83.83(5) .
S18 Ag13 Ag11 117.70(6) .
Ag4 Ag13 Ag11 57.49(2) .
Ag10 Ag13 Ag11 58.28(2) .
S19 Ag13 Ag14 48.07(6) .
S8 Ag13 Ag14 139.72(6) .
S18 Ag13 Ag14 88.11(5) .
Ag4 Ag13 Ag14 103.48(3) .
Ag10 Ag13 Ag14 55.24(2) .
Ag11 Ag13 Ag14 57.82(2) .
S19 Ag14 S24 126.32(9) .
S19 Ag14 S17 112.54(8) .
S24 Ag14 S17 119.07(9) .
S19 Ag14 Ag10 103.03(6) .
S24 Ag14 Ag10 114.12(7) .
S17 Ag14 Ag10 60.30(5) .
S19 Ag14 Ag12 141.84(6) .
S24 Ag14 Ag12 55.75(7) .
S17 Ag14 Ag12 88.02(6) .
Ag10 Ag14 Ag12 58.45(2) .
S19 Ag14 Ag11 85.89(6) .
S24 Ag14 Ag11 83.02(7) .
S17 Ag14 Ag11 117.76(6) .
Ag10 Ag14 Ag11 57.66(2) .
Ag12 Ag14 Ag11 55.95(2) .
S19 Ag14 Ag21 107.40(16) .
S24 Ag14 Ag21 32.91(15) .
S17 Ag14 Ag21 137.82(16) .
Ag10 Ag14 Ag21 98.30(14) .
Ag12 Ag14 Ag21 51.12(15) .
Ag11 Ag14 Ag21 51.76(13) .
S19 Ag14 Ag13 48.08(6) .
S24 Ag14 Ag13 137.37(7) .
S17 Ag14 Ag13 92.56(5) .
Ag10 Ag14 Ag13 55.58(2) .
Ag12 Ag14 Ag13 101.81(3) .
Ag11 Ag14 Ag13 55.92(2) .
Ag21 Ag14 Ag13 104.47(14) .
S23 Ag15 S14 120.93(9) .
S23 Ag15 S15 115.75(9) .
S14 Ag15 S15 115.51(10) .
S23 Ag15 Ag8 127.09(7) .
S14 Ag15 Ag8 59.64(6) .
S15 Ag15 Ag8 106.15(6) .
S23 Ag15 Ag9 94.78(7) .
S14 Ag15 Ag9 120.60(7) .
S15 Ag15 Ag9 80.69(6) .
Ag8 Ag15 Ag9 60.96(2) .
S23 Ag15 Ag12 68.01(7) .
S14 Ag15 Ag12 90.82(7) .
S15 Ag15 Ag12 138.97(7) .
Ag8 Ag15 Ag12 59.19(2) .
Ag9 Ag15 Ag12 58.47(2) .
S23 Ag15 Ag16 146.64(7) .
S14 Ag15 Ag16 90.45(7) .
S15 Ag15 Ag16 49.26(6) .
Ag8 Ag15 Ag16 56.95(2) .
Ag9 Ag15 Ag16 56.33(2) .
Ag12 Ag15 Ag16 103.43(3) .
S24 Ag21 S22 157.5(5) .
S24 Ag21 Ag12 65.9(3) .
S22 Ag21 Ag12 125.5(4) .
S24 Ag21 Ag7 127.2(4) .
S22 Ag21 Ag7 62.4(2) .
Ag12 Ag21 Ag7 63.47(18) .
S24 Ag21 Ag11 105.1(3) .
S22 Ag21 Ag11 97.3(3) .
Ag12 Ag21 Ag11 61.73(17) .
Ag7 Ag21 Ag11 62.26(17) .
S24 Ag21 Ag14 48.1(2) .
S22 Ag21 Ag14 153.5(3) .
Ag12 Ag21 Ag14 57.90(15) .
Ag7 Ag21 Ag14 110.7(3) .
Ag11 Ag21 Ag14 59.62(15) .
S13 Ag16 S15 114.05(9) .
S13 Ag16 S3 116.13(9) .
S15 Ag16 S3 104.91(8) .
S13 Ag16 Ag2 92.20(7) .
S15 Ag16 Ag2 141.22(7) .
S3 Ag16 Ag2 86.51(5) .
S13 Ag16 Ag8 64.63(8) .
S15 Ag16 Ag8 103.81(7) .
S3 Ag16 Ag8 147.10(6) .
Ag2 Ag16 Ag8 60.91(2) .
S13 Ag16 Ag9 124.51(8) .
S15 Ag16 Ag9 80.92(7) .
S3 Ag16 Ag9 109.60(6) .
Ag2 Ag16 Ag9 60.43(2) .
Ag8 Ag16 Ag9 59.89(2) .
S13 Ag16 Ag17 147.45(7) .
S15 Ag16 Ag17 98.47(7) .
S3 Ag16 Ag17 52.55(5) .
Ag2 Ag16 Ag17 59.11(2) .
Ag8 Ag16 Ag17 107.44(3) .
Ag9 Ag16 Ag17 57.16(2) .
S13 Ag16 Ag15 92.00(7) .
S15 Ag16 Ag15 49.68(7) .
S3 Ag16 Ag15 149.68(6) .
Ag2 Ag16 Ag15 104.43(3) .
Ag8 Ag16 Ag15 54.19(2) .
Ag9 Ag16 Ag15 56.30(2) .
Ag17 Ag16 Ag15 108.90(3) .
S6 Ag17 S3 101.32(7) .
S6 Ag17 S16 130.48(8) .
S3 Ag17 S16 115.00(8) .
S6 Ag17 Ag9 139.13(6) .
S3 Ag17 Ag9 111.43(6) .
S16 Ag17 Ag9 54.29(6) .
S6 Ag17 Ag2 101.07(5) .
S3 Ag17 Ag2 84.81(6) .
S16 Ag17 Ag2 114.13(6) .
Ag9 Ag17 Ag2 59.93(2) .
S6 Ag17 Ag3 81.66(5) .
S3 Ag17 Ag3 143.96(6) .
S16 Ag17 Ag3 87.12(6) .
Ag9 Ag17 Ag3 57.48(2) .
Ag2 Ag17 Ag3 59.63(2) .
S6 Ag17 Ag16 143.48(6) .
S3 Ag17 Ag16 52.91(5) .
S16 Ag17 Ag16 86.02(6) .
Ag9 Ag17 Ag16 58.64(2) .
Ag2 Ag17 Ag16 56.25(2) .
Ag3 Ag17 Ag16 104.58(3) .
S6 Ag17 Ag18 47.65(5) .
S3 Ag17 Ag18 99.39(5) .
S16 Ag17 Ag18 143.02(6) .
Ag9 Ag17 Ag18 101.74(3) .
Ag2 Ag17 Ag18 53.67(2) .
Ag3 Ag17 Ag18 56.15(2) .
Ag16 Ag17 Ag18 105.77(3) .
S6 Ag18 S1 131.07(8) .
S6 Ag18 S4 105.35(7) .
S1 Ag18 S4 120.16(7) .
S6 Ag18 Ag2 105.93(6) .
S1 Ag18 Ag2 114.51(6) .
S4 Ag18 Ag2 54.06(5) .
S6 Ag18 Ag1 141.96(6) .
S1 Ag18 Ag1 55.35(5) .
S4 Ag18 Ag1 93.94(5) .
Ag2 Ag18 Ag1 60.07(2) .
S6 Ag18 Ag3 83.23(5) .
S1 Ag18 Ag3 93.02(6) .
S4 Ag18 Ag3 114.31(5) .
Ag2 Ag18 Ag3 60.89(2) .
Ag1 Ag18 Ag3 58.85(2) .
S6 Ag18 Ag17 49.66(5) .
S1 Ag18 Ag17 149.41(6) .
S4 Ag18 Ag17 80.15(5) .
Ag2 Ag18 Ag17 56.53(2) .
Ag1 Ag18 Ag17 104.14(3) .
Ag3 Ag18 Ag17 56.58(2) .
S9 Ag19 S2 128.66(9) .
S9 Ag19 S11 114.86(8) .
S2 Ag19 S11 107.85(8) .
S9 Ag19 Ag6 121.75(7) .
S2 Ag19 Ag6 88.48(6) .
S11 Ag19 Ag6 84.60(6) .
S9 Ag19 Ag1 85.96(6) .
S2 Ag19 Ag1 73.92(6) .
S11 Ag19 Ag1 145.14(6) .
Ag6 Ag19 Ag1 60.53(2) .
S9 Ag19 Ag5 63.56(7) .
S2 Ag19 Ag5 128.65(6) .
S11 Ag19 Ag5 106.51(6) .
Ag6 Ag19 Ag5 58.24(2) .
Ag1 Ag19 Ag5 56.23(2) .
S9 Ag19 Ag20 93.93(7) .
S2 Ag19 Ag20 136.52(6) .
S11 Ag19 Ag20 48.95(5) .
Ag6 Ag19 Ag20 57.19(2) .
Ag1 Ag19 Ag20 105.03(3) .
Ag5 Ag19 Ag20 57.70(2) .
S21 Ag20 S11 120.13(9) .
S21 Ag20 S10 123.39(9) .
S11 Ag20 S10 115.24(9) .
S21 Ag20 Ag6 84.77(6) .
S11 Ag20 Ag6 83.84(6) .
S10 Ag20 Ag6 112.44(6) .
S21 Ag20 Ag7 59.67(6) .
S11 Ag20 Ag7 140.60(6) .
S10 Ag20 Ag7 84.78(6) .
Ag6 Ag20 Ag7 56.80(2) .
S21 Ag20 Ag5 116.28(6) .
S11 Ag20 Ag5 105.49(6) .
S10 Ag20 Ag5 55.25(6) .
Ag6 Ag20 Ag5 57.22(2) .
Ag7 Ag20 Ag5 56.80(2) .
S21 Ag20 Ag19 138.14(6) .
S11 Ag20 Ag19 49.34(5) .
S10 Ag20 Ag19 87.88(7) .
Ag6 Ag20 Ag19 55.79(2) .
Ag7 Ag20 Ag19 101.89(3) .
Ag5 Ag20 Ag19 56.28(2) .
O1 C1 C2 106.8(8) .
C3 C2 C1 112.1(9) .
O2 C4 C5 109.1(9) .
C4 C5 C6 109.6(11) .
O3 C7 C8 106.4(7) .
C9 C8 C7 113.7(9) .
O4 C10 C11 109.7(9) .
C10 C11 C12 109.9(11) .
O5 C13 C14 111.0(7) .
C13 C14 C15 111.2(9) .
O6 C16 C17 107.8(7) .
C18 C17 C16 113.3(8) .
O7 C19 C20 121.0(11) .
C21 C20 C19 109.9(13) .
O8 C22 C23 111.5(8) .
C22 C23 C24 111.0(9) .
C26 C25 O9 111.6(9) .
C25 C26 C27 112.5(9) .
O10 C28 C29 116.6(10) .
C28 C29 C30 123.3(12) .
C32 C31 O11 111.9(10) .
C31 C32 C33 114.8(11) .
O12 C34 C35 105.6(8) .
C36 C35 C34 100.0(14) .
O13 C37 C38 110.0(9) .
C37 C38 C39 112.0(11) .
O14 C40 C41 103(2) .
C40 C41 C42 117(2) .
O14 C40B C41B 109(3) .
C40B C41B C42B 103(3) .
O15 C43 C44 106.8(9) .
C45 C44 C43 113.9(10) .
O16 C46 C47 106.2(11) .
C48 C47 C46 114.7(14) .
O17 C49 C50 110.3(7) .
C49 C50 C51 108.7(7) .
O18 C52 C53 110.1(8) .
C52 C53 C54 114.2(10) .
O19 C55 C56 129.7(17) .
C57 C56 C55 98.7(8) .
O19 C55B C56B 134(4) .
C57B C56B C55B 127(5) .
O20 C58 C59 116.3(10) .
C58 C59 C60 118.2(11) .
O21 C61 C62 105.5(9) .
C63 C62 C61 114.9(14) .
O22 C64 C65 107.9(8) .
C64 C65 C66 114.1(10) .
O23 C67 C68 112.6(10) .
C69 C68 C67 113.8(11) .
O24 C70 C71 108.8(12) .
C72 C71 C70 112.6(13) .
C73 C73 C74 114.7(13) 3_657
C73 C74 C75 114.2(11) .
C1 O1 P1 122.3(5) .
C4 O2 P1 118.5(6) .
C7 O3 P2 121.6(5) .
C10 O4 P2 122.5(6) .
C13 O5 P3 120.1(5) .
C16 O6 P3 122.8(5) .
C19 O7 P4 117.9(6) .
C22 O8 P4 118.8(5) .
C25 O9 P5 119.8(6) .
C28 O10 P5 117.1(6) .
C31 O11 P6 125.7(6) .
C34 O12 P6 121.6(6) .
C37 O13 P7 119.5(6) .
C40 O14 P7 118.3(12) .
C40B O14 P7 120.3(12) .
C43 O15 P8 128.1(7) .
C46 O16 P8 123.6(9) .
C49 O17 P9 117.8(5) .
C52 O18 P9 118.9(5) .
C55B O19 P10 156(2) .
C55 O19 P10 131.4(11) .
C58 O20 P10 121.1(7) .
C61 O21 P11 121.2(6) .
C64 O22 P11 120.8(6) .
C67 O23 P12 125.2(8) .
C70 O24 P12 121.3(9) .
O2 P1 O1 101.3(3) .
O2 P1 S2 114.2(3) .
O1 P1 S2 109.8(3) .
O2 P1 S1 103.7(3) .
O1 P1 S1 109.0(3) .
S2 P1 S1 117.47(14) .
O3 P2 O4 101.3(3) .
O3 P2 S4 104.9(2) .
O4 P2 S4 110.4(3) .
O3 P2 S3 111.4(2) .
O4 P2 S3 107.9(3) .
S4 P2 S3 119.47(14) .
O6 P3 O5 101.4(3) .
O6 P3 S5 108.0(2) .
O5 P3 S5 111.4(2) .
O6 P3 S6 107.8(2) .
O5 P3 S6 107.9(2) .
S5 P3 S6 118.86(13) .
O8 P4 O7 96.6(3) .
O8 P4 S7 114.2(3) .
O7 P4 S7 113.1(3) .
O8 P4 S8 110.2(3) .
O7 P4 S8 108.1(3) .
S7 P4 S8 113.32(14) .
O9 P5 O10 102.2(3) .
O9 P5 S10 107.6(3) .
O10 P5 S10 109.5(3) .
O9 P5 S9 112.4(3) .
O10 P5 S9 107.6(3) .
S10 P5 S9 116.52(16) .
O11 P6 O12 99.7(3) .
O11 P6 S12 112.8(3) .
O12 P6 S12 110.9(3) .
O11 P6 S11 105.0(3) .
O12 P6 S11 107.5(3) .
S12 P6 S11 118.96(15) .
O13 P7 O14 101.5(3) .
O13 P7 S13 109.3(3) .
O14 P7 S13 108.6(3) .
O13 P7 S14 112.7(3) .
O14 P7 S14 107.2(3) .
S13 P7 S14 116.32(16) .
O15 P8 O16 109.9(6) .
O15 P8 S16 111.3(3) .
O16 P8 S16 103.7(4) .
O15 P8 S15 102.6(4) .
O16 P8 S15 108.7(3) .
S16 P8 S15 120.60(16) .
O18 P9 O17 101.8(3) .
O18 P9 S17 107.9(3) .
O17 P9 S17 108.9(2) .
O18 P9 S18 114.2(3) .
O17 P9 S18 107.2(2) .
S17 P9 S18 115.81(14) .
O19 P10 O20 98.7(4) .
O19 P10 S20 114.0(5) .
O20 P10 S20 109.9(3) .
O19 P10 S19 103.9(4) .
O20 P10 S19 108.9(3) .
S20 P10 S19 119.33(15) .
O22 P11 O21 100.1(3) .
O22 P11 S22 113.7(3) .
O21 P11 S22 112.4(3) .
O22 P11 S21 105.5(3) .
O21 P11 S21 108.5(3) .
S22 P11 S21 115.31(15) .
O24 P12 O23 100.6(5) .
O24 P12 S24 112.3(4) .
O23 P12 S24 100.8(4) .
O24 P12 S23 110.6(4) .
O23 P12 S23 112.6(4) .
S24 P12 S23 118.10(16) .
Ag9 Pt1 Ag2 65.78(2) .
Ag9 Pt1 Ag1 117.34(2) .
Ag2 Pt1 Ag1 64.11(2) .
Ag9 Pt1 Ag12 64.49(2) .
Ag2 Pt1 Ag12 118.96(2) .
Ag1 Pt1 Ag12 176.80(2) .
Ag9 Pt1 Ag11 116.46(2) .
Ag2 Pt1 Ag11 177.75(2) .
Ag1 Pt1 Ag11 113.98(2) .
Ag12 Pt1 Ag11 62.96(2) .
Ag9 Pt1 Ag6 117.10(2) .
Ag2 Pt1 Ag6 62.353(19) .
Ag1 Pt1 Ag6 66.55(2) .
Ag12 Pt1 Ag6 115.31(2) .
Ag11 Pt1 Ag6 116.00(2) .
Ag9 Pt1 Ag5 178.77(2) .
Ag2 Pt1 Ag5 114.49(2) .
Ag1 Pt1 Ag5 62.12(2) .
Ag12 Pt1 Ag5 116.00(2) .
Ag11 Pt1 Ag5 63.27(2) .
Ag6 Pt1 Ag5 63.83(2) .
Ag9 Pt1 Ag8 65.43(2) .
Ag2 Pt1 Ag8 65.34(2) .
Ag1 Pt1 Ag8 119.75(2) .
Ag12 Pt1 Ag8 63.26(2) .
Ag11 Pt1 Ag8 115.55(2) .
Ag6 Pt1 Ag8 62.26(2) .
Ag5 Pt1 Ag8 115.79(2) .
Ag9 Pt1 Ag3 62.912(19) .
Ag2 Pt1 Ag3 65.786(19) .
Ag1 Pt1 Ag3 63.741(19) .
Ag12 Pt1 Ag3 116.21(2) .
Ag11 Pt1 Ag3 114.73(2) .
Ag6 Pt1 Ag3 119.21(2) .
Ag5 Pt1 Ag3 116.01(2) .
Ag8 Pt1 Ag3 119.19(2) .
Ag9 Pt1 Ag4 114.30(2) .
Ag2 Pt1 Ag4 116.42(2) .
Ag1 Pt1 Ag4 62.149(19) .
Ag12 Pt1 Ag4 114.83(2) .
Ag11 Pt1 Ag4 62.72(2) .
Ag6 Pt1 Ag4 119.07(2) .
Ag5 Pt1 Ag4 64.48(2) .
Ag8 Pt1 Ag4 178.07(2) .
Ag3 Pt1 Ag4 61.687(19) .
Ag9 Pt1 Ag10 62.45(2) .
Ag2 Pt1 Ag10 118.17(2) .
Ag1 Pt1 Ag10 114.97(2) .
Ag12 Pt1 Ag10 63.16(2) .
Ag11 Pt1 Ag10 63.520(19) .
Ag6 Pt1 Ag10 178.47(2) .
Ag5 Pt1 Ag10 116.64(2) .
Ag8 Pt1 Ag10 116.49(2) .
Ag3 Pt1 Ag10 62.046(19) .
Ag4 Pt1 Ag10 62.152(19) .
Ag9 Pt1 Ag7 118.07(2) .
Ag2 Pt1 Ag7 116.59(2) .
Ag1 Pt1 Ag7 116.63(2) .
Ag12 Pt1 Ag7 63.28(2) .
Ag11 Pt1 Ag7 62.89(2) .
Ag6 Pt1 Ag7 62.58(2) .
Ag5 Pt1 Ag7 62.98(2) .
Ag8 Pt1 Ag7 62.89(2) .
Ag3 Pt1 Ag7 177.60(2) .
Ag4 Pt1 Ag7 116.20(2) .
Ag10 Pt1 Ag7 116.19(2) .
P1 S1 Ag18 101.32(11) .
P1 S1 Ag1 94.99(10) .
Ag18 S1 Ag1 69.72(6) .
P1 S2 Ag19 101.00(11) .
P2 S3 Ag17 99.02(11) .
P2 S3 Ag16 109.53(11) .
Ag17 S3 Ag16 74.55(6) .
P2 S4 Ag2 105.67(11) .
P2 S4 Ag18 101.68(10) .
Ag2 S4 Ag18 65.91(5) .
P3 S5 Ag3 104.91(11) .
P3 S6 Ag18 110.23(11) .
P3 S6 Ag17 98.94(10) .
Ag18 S6 Ag17 82.68(7) .
P4 S7 Ag4 83.77(10) .
P4 S8 Ag13 102.90(11) .
P4 S8 Ag4 82.23(10) .
Ag13 S8 Ag4 68.73(6) .
P5 S9 Ag19 103.27(13) .
P5 S9 Ag5 80.16(12) .
Ag19 S9 Ag5 67.01(7) .
P5 S10 Ag20 103.91(12) .
P5 S10 Ag5 88.20(12) .
Ag20 S10 Ag5 72.44(7) .
P6 S11 Ag20 104.33(12) .
P6 S11 Ag19 101.41(11) .
Ag20 S11 Ag19 81.70(7) .
P6 S12 Ag6 105.65(12) .
P7 S13 Ag16 107.74(13) .
P7 S13 Ag8 81.32(12) .
Ag16 S13 Ag8 65.04(7) .
P7 S14 Ag15 107.11(14) .
P7 S14 Ag8 87.89(12) .
Ag15 S14 Ag8 66.56(6) .
P8 S15 Ag16 106.61(13) .
P8 S15 Ag15 105.29(14) .
Ag16 S15 Ag15 81.06(8) .
P8 S16 Ag9 99.28(13) .
P8 S16 Ag17 108.26(12) .
Ag9 S16 Ag17 68.88(6) .
P9 S17 Ag14 104.71(11) .
P9 S17 Ag10 84.10(10) .
Ag14 S17 Ag10 66.99(6) .
P9 S18 Ag13 109.29(11) .
P9 S18 Ag10 84.60(10) .
Ag13 S18 Ag10 67.45(5) .
P10 S19 Ag14 99.94(12) .
P10 S19 Ag13 100.83(12) .
Ag14 S19 Ag13 83.84(7) .
P10 S20 Ag11 110.28(14) .
P11 S21 Ag20 99.41(13) .
P11 S21 Ag7 80.89(11) .
Ag20 S21 Ag7 70.27(7) .
P11 S22 Ag21 133.7(3) .
P11 S22 Ag7 86.79(12) .
Ag21 S22 Ag7 70.2(2) .
P12 S23 Ag15 113.08(14) .
Ag21 S24 P12 145.2(3) .
Ag21 S24 Ag14 99.0(3) .
P12 S24 Ag14 103.43(13) .
Ag21 S24 Ag12 74.1(3) .
P12 S24 Ag12 88.26(12) .
Ag14 S24 Ag12 71.43(7) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 S1 2.553(2) .
Ag1 Pt1 2.7371(7) .
Ag1 Ag5 2.8362(9) .
Ag1 Ag4 2.8547(9) .
Ag1 Ag2 2.8931(9) .
Ag1 Ag3 2.9095(8) .
Ag1 Ag18 2.9112(9) .
Ag1 Ag19 3.0031(9) .
Ag1 Ag6 3.0135(9) .
Ag2 S4 2.544(2) .
Ag2 Pt1 2.7140(7) .
Ag2 Ag6 2.8314(9) .
Ag2 Ag18 2.8682(9) .
Ag2 Ag16 2.8777(9) .
Ag2 Ag9 2.9417(9) .
Ag2 Ag8 2.9579(9) .
Ag2 Ag17 2.9701(9) .
Ag2 Ag3 2.9803(8) .
Ag3 S5 2.499(2) .
Ag3 Pt1 2.7731(6) .
Ag3 Ag4 2.8538(9) .
Ag3 Ag9 2.8585(9) .
Ag3 Ag10 2.8776(9) .
Ag3 Ag18 3.0085(9) .
Ag3 Ag17 3.0237(9) .
Ag4 S7 2.685(2) .
Ag4 S8 2.700(2) .
Ag4 Pt1 2.7930(7) .
Ag4 Ag11 2.8838(9) .
Ag4 Ag10 2.8921(9) .
Ag4 Ag13 2.9537(9) .
Ag4 Ag5 2.9626(9) .
Ag5 S10 2.641(2) .
Ag5 Pt1 2.7601(7) .
Ag5 Ag11 2.8887(9) .
Ag5 Ag7 2.9143(10) .
Ag5 Ag6 2.9157(9) .
Ag5 S9 2.933(3) .
Ag5 Ag19 3.0155(9) .
Ag5 Ag20 3.0641(10) .
Ag6 S12 2.479(2) .
Ag6 Pt1 2.7549(7) .
Ag6 Ag8 2.8537(9) .
Ag6 Ag7 2.8952(9) .
Ag6 Ag19 2.9755(10) .
Ag6 Ag20 3.0241(9) .
Ag7 S22 2.625(3) .
Ag7 Ag21 2.788(8) .
Ag7 S21 2.808(3) .
Ag7 Pt1 2.8182(7) .
Ag7 Ag11 2.9040(9) .
Ag7 Ag8 2.9131(10) .
Ag7 Ag12 2.9189(10) .
Ag7 Ag20 3.0626(10) .
Ag8 S14 2.690(3) .
Ag8 Pt1 2.7652(7) .
Ag8 Ag15 2.8601(10) .
Ag8 Ag12 2.8898(9) .
Ag8 S13 2.946(3) .
Ag8 Ag9 2.9560(9) .
Ag8 Ag16 2.9563(10) .
Ag9 S16 2.540(2) .
Ag9 Pt1 2.7034(7) .
Ag9 Ag10 2.8593(9) .
Ag9 Ag12 2.9071(9) .
Ag9 Ag17 2.9185(9) .
Ag9 Ag15 2.9650(10) .
Ag9 Ag16 2.9659(9) .
Ag10 S18 2.765(2) .
Ag10 S17 2.787(2) .
Ag10 Pt1 2.8099(7) .
Ag10 Ag12 2.9096(9) .
Ag10 Ag11 2.9256(9) .
Ag10 Ag14 2.9536(9) .
Ag10 Ag13 2.9659(9) .
Ag11 S20 2.462(3) .
Ag11 Pt1 2.7475(7) .
Ag11 Ag21 2.829(8) .
Ag11 Ag12 2.8684(10) .
Ag11 Ag13 3.0404(9) .
Ag11 Ag14 3.1070(9) .
Ag12 S24 2.620(3) .
Ag12 Pt1 2.7451(7) .
Ag12 Ag21 2.761(8) .
Ag12 Ag15 2.9873(11) .
Ag12 Ag14 3.0050(10) .
Ag13 S19 2.515(2) .
Ag13 S8 2.526(2) .
Ag13 S18 2.569(2) .
Ag13 Ag14 3.3604(9) .
Ag14 S19 2.515(3) .
Ag14 S24 2.526(3) .
Ag14 S17 2.553(2) .
Ag14 Ag21 3.354(8) .
Ag15 S23 2.470(3) .
Ag15 S14 2.515(3) .
Ag15 S15 2.539(3) .
Ag15 Ag16 3.2895(11) .
Ag21 S24 1.845(8) .
Ag21 S22 2.182(8) .
Ag16 S13 2.510(3) .
Ag16 S15 2.523(3) .
Ag16 S3 2.588(2) .
Ag16 Ag17 3.1273(10) .
Ag17 S6 2.568(2) .
Ag17 S3 2.576(2) .
Ag17 S16 2.619(2) .
Ag17 Ag18 3.3416(9) .
Ag18 S6 2.490(2) .
Ag18 S1 2.540(2) .
Ag18 S4 2.722(2) .
Ag19 S9 2.488(3) .
Ag19 S2 2.492(2) .
Ag19 S11 2.539(2) .
Ag19 Ag20 3.3123(10) .
Ag20 S21 2.495(3) .
Ag20 S11 2.525(2) .
Ag20 S10 2.543(3) .
C1 O1 1.454(11) .
C1 C2 1.517(13) .
C2 C3 1.477(16) .
C4 O2 1.471(10) .
C4 C5 1.483(14) .
C5 C6 1.531(15) .
C7 O3 1.465(10) .
C7 C8 1.501(13) .
C8 C9 1.496(15) .
C10 O4 1.437(11) .
C10 C11 1.523(9) .
C11 C12 1.529(9) .
C13 O5 1.433(10) .
C13 C14 1.489(12) .
C14 C15 1.518(14) .
C16 O6 1.471(9) .
C16 C17 1.507(12) .
C17 C18 1.505(14) .
C19 O7 1.430(12) .
C19 C20 1.503(9) .
C20 C21 1.492(9) .
C22 O8 1.448(10) .
C22 C23 1.487(13) .
C23 C24 1.534(14) .
C25 C26 1.466(14) .
C25 O9 1.469(12) .
C26 C27 1.509(14) .
C28 O10 1.393(12) .
C28 C29 1.458(9) .
C29 C30 1.485(9) .
C31 C32 1.453(15) .
C31 O11 1.478(11) .
C32 C33 1.528(16) .
C34 O12 1.455(11) .
C34 C35 1.554(9) .
C35 C36 1.507(10) .
C37 O13 1.473(11) .
C37 C38 1.483(14) .
C38 C39 1.489(16) .
C40 O14 1.459(16) .
C40 C41 1.522(9) .
C41 C42 1.532(10) .
C40B O14 1.462(16) .
C40B C41B 1.488(19) .
C41B C42B 1.543(19) .
C43 O15 1.416(11) .
C43 C44 1.514(14) .
C44 C45 1.461(14) .
C46 O16 1.372(14) .
C46 C47 1.524(9) .
C47 C48 1.519(9) .
C49 O17 1.450(10) .
C49 C50 1.503(8) .
C50 C51 1.519(8) .
C52 O18 1.444(10) .
C52 C53 1.509(8) .
C53 C54 1.519(9) .
C55 O19 1.236(17) .
C55 C56 1.524(9) .
C56 C57 1.503(10) .
C55B O19 1.20(2) .
C55B C56B 1.49(2) .
C56B C57B 1.48(2) .
C58 O20 1.387(12) .
C58 C59 1.486(9) .
C59 C60 1.493(9) .
C61 O21 1.442(12) .
C61 C62 1.529(17) .
C62 C63 1.453(19) .
C64 O22 1.451(11) .
C64 C65 1.486(14) .
C65 C66 1.501(15) .
C67 O23 1.318(13) .
C67 C68 1.512(9) .
C68 C69 1.506(9) .
C70 O24 1.394(15) .
C70 C71 1.524(9) .
C71 C72 1.513(9) .
C73 C73 1.47(2) 3_657
C73 C74 1.522(9) .
C74 C75 1.527(9) .
O1 P1 1.581(6) .
O2 P1 1.578(6) .
O3 P2 1.578(6) .
O4 P2 1.586(6) .
O5 P3 1.590(6) .
O6 P3 1.570(6) .
O7 P4 1.596(6) .
O8 P4 1.580(6) .
O9 P5 1.570(6) .
O10 P5 1.586(7) .
O11 P6 1.582(6) .
O12 P6 1.592(6) .
O13 P7 1.572(7) .
O14 P7 1.582(6) .
O15 P8 1.584(8) .
O16 P8 1.597(9) .
O17 P9 1.594(6) .
O18 P9 1.571(6) .
O19 P10 1.557(8) .
O20 P10 1.587(7) .
O21 P11 1.583(7) .
O22 P11 1.578(6) .
O23 P12 1.613(9) .
O24 P12 1.536(8) .
P1 S2 1.975(3) .
P1 S1 2.009(3) .
P2 S4 1.992(3) .
P2 S3 2.016(3) .
P3 S5 1.967(3) .
P3 S6 2.022(3) .
P4 S7 1.963(3) .
P4 S8 2.026(3) .
P5 S10 1.994(4) .
P5 S9 2.006(4) .
P6 S12 1.972(3) .
P6 S11 2.021(4) .
P7 S13 1.993(4) .
P7 S14 2.011(4) .
P8 S16 1.985(4) .
P8 S15 2.017(4) .
P9 S17 1.999(3) .
P9 S18 2.004(3) .
P10 S20 1.956(4) .
P10 S19 2.017(4) .
P11 S22 1.962(4) .
P11 S21 2.018(4) .
P12 S24 1.985(4) .
P12 S23 1.990(4) .
