#------------------------------------------------------------------------------
#$Date: 2019-11-03 12:52:03 +0200 (Sun, 03 Nov 2019) $
#$Revision: 221450 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/12/83/4128327.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4128327
loop_
_publ_author_name
'Takano, Shinjiro'
'Ito, Shun'
'Tsukuda, Tatsuya'
_publ_section_title
;
 Efficient and Selective Conversion of Phosphine-Protected
 (MAu₈)²⁺ (M = Pd, Pt) Superatoms to
 Thiolate-Protected (MAu₁₂)⁶⁺ or Alkynyl-Protected
 (MAu₁₂)⁴⁺ Superatoms via Hydride Doping.
;
_journal_issue                   40
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              15994
_journal_page_last               16002
_journal_paper_doi               10.1021/jacs.9b08055
_journal_volume                  141
_journal_year                    2019
_chemical_formula_sum            'C229 H96 Au24 Cl2 F108 P2 Pt'
_chemical_formula_weight         9954.18
_space_group_crystal_system      monoclinic
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yac'
_space_group_name_H-M_alt        'P 1 2/n 1'
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                90
_cell_angle_beta                 95.690(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   17.464(3)
_cell_length_b                   20.626(4)
_cell_length_c                   35.907(7)
_cell_measurement_reflns_used    30375
_cell_measurement_temperature    93(2)
_cell_measurement_theta_max      25.3
_cell_measurement_theta_min      1.8
_cell_volume                     12870(4)
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_diffrn_ambient_temperature      93(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Rigaku AFC11 with Saturn724+'
_diffrn_measurement_method       ω
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0950
_diffrn_reflns_av_unetI/netI     0.0625
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       43
_diffrn_reflns_limit_l_min       -43
_diffrn_reflns_number            137266
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.306
_diffrn_reflns_theta_min         1.975
_diffrn_source                   'Rotating anode'
_exptl_absorpt_coefficient_mu    14.315
_exptl_absorpt_correction_T_max  0.283
_exptl_absorpt_correction_T_min  0.108
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'NUMABS (Rigaku, 1999)'
_exptl_crystal_colour            Black
_exptl_crystal_density_diffrn    2.569
_exptl_crystal_description       Prism
_exptl_crystal_F_000             8960
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.12
_refine_diff_density_max         4.050
_refine_diff_density_min         -2.515
_refine_diff_density_rms         0.289
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.122
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1605
_refine_ls_number_reflns         23360
_refine_ls_number_restraints     866
_refine_ls_restrained_S_all      1.111
_refine_ls_R_factor_all          0.0699
_refine_ls_R_factor_gt           0.0627
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0708P)²+164.0974P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1612
_refine_ls_wR_factor_ref         0.1668
_reflns_Friedel_coverage         0.000
_reflns_number_gt                21080
_reflns_number_total             23360
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja9b08055_si_008.cif
_cod_data_source_block           shelxs_sq
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Numerical' changed to
'numerical' according to
/home/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_database_code               4128327
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x+1/2, -y, z+1/2'
'-x, -y, -z'
'-x-1/2, y, -z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.17408(3) 0.19239(3) 0.67895(2) 0.03314(14) Uani 1 1 d . . . . .
Au2 Au 0.11057(3) 0.12536(3) 0.73872(2) 0.03316(14) Uani 1 1 d . . . . .
Au3 Au 0.25514(3) 0.07959(3) 0.71025(2) 0.03379(14) Uani 1 1 d . . . . .
Au4 Au 0.34229(3) 0.19136(3) 0.69124(2) 0.03207(14) Uani 1 1 d . . . . .
Au5 Au 0.25610(3) 0.30726(3) 0.71024(2) 0.03194(14) Uani 1 1 d . . . . .
Au6 Au 0.11485(3) 0.26452(3) 0.73966(2) 0.03196(13) Uani 1 1 d . . . . .
Au7 Au 0.00089(4) 0.19973(3) 0.66690(2) 0.03958(15) Uani 1 1 d . . . . .
Au8 Au 0.26450(4) 0.26675(3) 0.62134(2) 0.04200(16) Uani 1 1 d . . . . .
Au9 Au 0.10726(3) 0.33337(3) 0.65432(2) 0.03633(14) Uani 1 1 d . . . . .
Au10 Au 0.14043(3) -0.02100(3) 0.74272(2) 0.03486(14) Uani 1 1 d . . . . .
Au11 Au 0.41335(3) 0.06507(3) 0.68165(2) 0.03866(15) Uani 1 1 d . . . . .
Au12 Au 0.40761(4) 0.33405(3) 0.67770(2) 0.04562(17) Uani 1 1 d . . . . .
Pt1 Pt 0.250000 0.19348(3) 0.750000 0.02982(17) Uani 1 2 d S T P . .
P1 P 0.1307(2) 0.30897(18) 0.38691(10) 0.0347(8) Uani 1 1 d . . . . .
C1A C -0.0068(8) 0.1328(8) 0.7030(4) 0.042(4) Uani 1 1 d . . . . .
C1B C -0.0245(8) 0.0914(7) 0.7264(4) 0.035(3) Uani 1 1 d . . . . .
C1C C -0.0680(6) 0.0441(4) 0.7483(3) 0.041(3) Uani 1 1 d G . . . .
C1D C -0.0754(6) -0.0195(5) 0.7356(2) 0.053(4) Uani 1 1 d G . . . .
H1D H -0.052733 -0.032318 0.713748 0.063 Uiso 1 1 calc R U . . .
C1E C -0.1160(6) -0.0643(3) 0.7548(3) 0.044(4) Uani 1 1 d G . . . .
C1F C -0.1491(6) -0.0455(4) 0.7868(3) 0.045(4) Uani 1 1 d G . . . .
H1F H -0.176879 -0.076178 0.799935 0.054 Uiso 1 1 calc R U . . .
C1G C -0.1417(6) 0.0180(5) 0.7995(2) 0.046(4) Uani 1 1 d G . . . .
C1H C -0.1011(6) 0.0628(4) 0.7802(3) 0.044(4) Uani 1 1 d G . . . .
H1H H -0.096065 0.106297 0.788866 0.052 Uiso 1 1 calc R U . . .
C1I C -0.1252(10) -0.1323(8) 0.7409(5) 0.047(4) Uani 1 1 d . . . . .
F1A F -0.1899(6) -0.1416(5) 0.7188(3) 0.068(3) Uani 1 1 d . . . . .
F1B F -0.1285(9) -0.1760(5) 0.7690(3) 0.097(5) Uani 1 1 d . . . . .
F1C F -0.0701(7) -0.1518(6) 0.7211(5) 0.105(5) Uani 1 1 d . . . . .
C1J C -0.1778(10) 0.0371(9) 0.8337(5) 0.052(4) Uani 1 1 d . . . . .
F1D F -0.2555(6) 0.0416(6) 0.8266(3) 0.073(3) Uani 1 1 d . . . . .
F1E F -0.1636(6) -0.0063(5) 0.8615(3) 0.063(3) Uani 1 1 d . . . . .
F1F F -0.1537(7) 0.0942(5) 0.8474(3) 0.075(3) Uani 1 1 d . . . . .
C2A C 0.0163(11) 0.2852(7) 0.6303(4) 0.050(4) Uani 1 1 d . . . . .
C2B C -0.0393(9) 0.2539(8) 0.6150(4) 0.046(4) Uani 1 1 d . . . . .
C2C C -0.1049(5) 0.2391(5) 0.5892(3) 0.047(4) Uani 1 1 d G . . . .
C2D C -0.1282(6) 0.2844(4) 0.5617(3) 0.059(5) Uani 1 1 d G . . . .
H2D H -0.100157 0.323590 0.560055 0.071 Uiso 1 1 calc R U . . .
C2E C -0.1926(7) 0.2724(6) 0.5367(3) 0.069(6) Uani 1 1 d G . . . .
C2F C -0.2336(5) 0.2151(7) 0.5392(3) 0.079(8) Uani 1 1 d G . . . .
H2F H -0.277622 0.206820 0.522090 0.095 Uiso 1 1 calc R U . . .
C2G C -0.2103(7) 0.1698(6) 0.5667(3) 0.086(7) Uani 1 1 d G U . . .
C2H C -0.1460(7) 0.1818(5) 0.5917(3) 0.058(5) Uani 1 1 d G . . . .
H2H H -0.130019 0.150884 0.610480 0.069 Uiso 1 1 calc R U . . .
C2I C -0.2145(15) 0.3236(11) 0.5050(6) 0.090(6) Uani 1 1 d . . . . .
F2A F -0.2142(8) 0.3827(6) 0.5207(4) 0.095(4) Uani 1 1 d . . . . .
F2B F -0.2872(10) 0.3136(7) 0.4908(6) 0.153(7) Uani 1 1 d . . . . .
F2C F -0.1741(12) 0.3196(8) 0.4783(4) 0.130(6) Uani 1 1 d . . . . .
C2J C -0.2522(17) 0.1037(16) 0.5682(6) 0.115(6) Uani 1 1 d . U . . .
F2D F -0.2262(9) 0.0668(7) 0.5938(4) 0.113(5) Uani 1 1 d . U . . .
F2E F -0.3262(10) 0.1148(12) 0.5717(4) 0.176(8) Uani 1 1 d . U . . .
F2F F -0.2521(15) 0.0753(10) 0.5346(4) 0.196(9) Uani 1 1 d . U . . .
C3A C 0.1927(8) 0.3900(7) 0.6768(3) 0.035(3) Uani 1 1 d . . . . .
C3B C 0.2476(9) 0.4183(7) 0.6909(4) 0.038(3) Uani 1 1 d . . . . .
C3C C 0.2988(5) 0.4760(4) 0.7002(2) 0.036(3) Uani 1 1 d G . . . .
C3D C 0.2959(6) 0.5280(4) 0.6754(2) 0.042(4) Uani 1 1 d G . . . .
H3D H 0.263983 0.525828 0.652450 0.051 Uiso 1 1 calc R U . . .
C3E C 0.3397(6) 0.5831(4) 0.6843(3) 0.049(4) Uani 1 1 d G . . . .
C3F C 0.3864(5) 0.5863(4) 0.7179(3) 0.046(4) Uani 1 1 d G . . . .
H3F H 0.416377 0.623941 0.724022 0.055 Uiso 1 1 calc R U . . .
C3G C 0.3893(5) 0.5343(5) 0.7427(2) 0.049(4) Uani 1 1 d G . . . .
C3H C 0.3454(6) 0.4792(4) 0.7338(2) 0.040(3) Uani 1 1 d G . . . .
H3H H 0.347401 0.443657 0.750722 0.048 Uiso 1 1 calc R U . . .
C3I C 0.3382(14) 0.6394(10) 0.6576(7) 0.079(5) Uani 1 1 d . U . . .
F3A F 0.2803(8) 0.6792(7) 0.6638(5) 0.125(5) Uani 1 1 d D U . . .
F3B F 0.3969(8) 0.6758(7) 0.6617(5) 0.131(6) Uani 1 1 d D U . . .
F3C F 0.3229(15) 0.6221(7) 0.6230(4) 0.187(9) Uani 1 1 d D U . . .
C3J C 0.4325(18) 0.5415(14) 0.7807(8) 0.123(7) Uani 1 1 d . U . . .
F3D F 0.5130(9) 0.5245(10) 0.7732(5) 0.178(8) Uani 1 1 d D U . . .
F3E F 0.4456(14) 0.5974(8) 0.7898(4) 0.194(9) Uani 1 1 d D U . . .
F3F F 0.4219(8) 0.4992(7) 0.8043(3) 0.105(5) Uani 1 1 d D U . . .
C4A C 0.1850(9) 0.1975(8) 0.6162(4) 0.043(4) Uani 1 1 d . . . . .
C4B C 0.1333(10) 0.1559(7) 0.6118(4) 0.039(4) Uani 1 1 d . . . . .
C4C C 0.0737(5) 0.1127(4) 0.5965(2) 0.042(4) Uani 1 1 d G . . . .
C4D C 0.0403(6) 0.1244(4) 0.5604(2) 0.048(4) Uani 1 1 d G . . . .
H4D H 0.055957 0.160903 0.546879 0.057 Uiso 1 1 calc R U . . .
C4E C -0.0159(6) 0.0828(5) 0.5440(2) 0.048(4) Uani 1 1 d G . . . .
C4F C -0.0388(6) 0.0294(4) 0.5638(3) 0.055(4) Uani 1 1 d G . . . .
H4F H -0.077186 0.000971 0.552644 0.066 Uiso 1 1 calc R U . . .
C4G C -0.0054(6) 0.0177(4) 0.6000(2) 0.047(4) Uani 1 1 d G . . . .
C4H C 0.0508(6) 0.0593(5) 0.6163(2) 0.051(4) Uani 1 1 d G . . . .
H4H H 0.073619 0.051293 0.641022 0.061 Uiso 1 1 calc R U . . .
C4I C -0.0507(13) 0.0959(10) 0.5045(5) 0.070(4) Uani 1 1 d . . . . .
F4A F -0.0886(7) 0.1504(6) 0.5020(3) 0.073(3) Uani 1 1 d . . . . .
F4B F 0.0064(8) 0.1046(6) 0.4811(3) 0.088(3) Uani 1 1 d . . . . .
F4C F -0.0870(10) 0.0484(7) 0.4893(3) 0.112(5) Uani 1 1 d . . . . .
C4J C -0.0336(11) -0.0373(9) 0.6217(5) 0.059(4) Uani 1 1 d . . . . .
F4D F -0.0963(7) -0.0235(6) 0.6391(3) 0.080(3) Uani 1 1 d . . . . .
F4E F 0.0187(7) -0.0581(6) 0.6499(4) 0.091(4) Uani 1 1 d . . . . .
F4F F -0.0538(7) -0.0887(5) 0.5999(3) 0.072(3) Uani 1 1 d . . . . .
C5A C 0.3407(9) 0.3396(8) 0.6211(4) 0.044(4) Uani 1 1 d . . . . .
C5B C 0.3847(9) 0.3869(8) 0.6231(4) 0.044(4) Uani 1 1 d . . . . .
C5C C 0.4246(7) 0.4446(6) 0.6133(4) 0.049(4) Uani 1 1 d D . . . .
C5D C 0.4066(11) 0.4721(9) 0.5788(5) 0.100(8) Uani 1 1 d D . . . .
H5D H 0.378075 0.449080 0.559088 0.120 Uiso 1 1 calc R U . A 1
C5EA C 0.4319(13) 0.5355(10) 0.5738(6) 0.097(5) Uani 0.5 1 d D U P B 1
C5EB C 0.4522(12) 0.5219(10) 0.5649(6) 0.097(5) Uani 0.5 1 d D U P B 2
C5F C 0.4999(12) 0.5554(9) 0.5933(7) 0.119(9) Uani 1 1 d D . . . .
H5F H 0.532178 0.586350 0.583019 0.143 Uiso 1 1 calc R U . B 1
C5G C 0.5192(9) 0.5292(9) 0.6275(7) 0.074(5) Uani 1 1 d D . . . .
C5H C 0.4816(8) 0.4738(9) 0.6378(5) 0.060(4) Uani 1 1 d D . . . .
H5H H 0.494790 0.455424 0.661881 0.072 Uiso 1 1 calc R U . . .
C5IA C 0.3890(14) 0.5775(13) 0.5473(8) 0.096(4) Uani 0.5 1 d D U P B 1
F5AA F 0.3938(17) 0.5483(13) 0.5142(8) 0.104(5) Uani 0.5 1 d D U P B 1
F5BA F 0.4210(15) 0.6348(11) 0.5467(7) 0.103(6) Uani 0.5 1 d D U P B 1
F5CA F 0.3138(13) 0.5803(13) 0.5461(7) 0.099(6) Uani 0.5 1 d D U P B 1
C5IB C 0.4461(16) 0.5374(14) 0.5233(6) 0.097(4) Uani 0.5 1 d D U P B 2
F5AB F 0.4296(14) 0.4881(11) 0.4978(7) 0.098(5) Uani 0.5 1 d D U P B 2
F5BB F 0.5057(12) 0.5667(12) 0.5088(7) 0.091(5) Uani 0.5 1 d D U P B 2
F5CB F 0.3895(15) 0.5805(13) 0.5127(8) 0.101(5) Uani 0.5 1 d D U P B 2
C5J C 0.5800(11) 0.5567(14) 0.6547(8) 0.102(6) Uani 1 1 d . . . . .
F5D F 0.5548(8) 0.5886(8) 0.6815(5) 0.117(5) Uani 1 1 d . . . . .
F5E F 0.6331(9) 0.5194(9) 0.6665(7) 0.200(10) Uani 1 1 d . . . . .
F5F F 0.6191(10) 0.6073(10) 0.6384(6) 0.171(7) Uani 1 1 d . . . . .
C6A C 0.1922(9) -0.0156(7) 0.6953(4) 0.040(3) Uani 1 1 d . . . . .
C6B C 0.2261(9) -0.0103(7) 0.6668(4) 0.038(3) Uani 1 1 d . . . . .
C6C C 0.2537(5) -0.0232(4) 0.63092(18) 0.032(3) Uani 1 1 d G . . . .
C6D C 0.2696(6) -0.0870(3) 0.6219(2) 0.041(4) Uani 1 1 d G . . . .
H6D H 0.265118 -0.120480 0.639704 0.049 Uiso 1 1 calc R U . . .
C6E C 0.2920(5) -0.1018(3) 0.5868(2) 0.034(3) Uani 1 1 d G . . . .
C6F C 0.2986(5) -0.0528(4) 0.56073(17) 0.037(3) Uani 1 1 d G . . . .
H6F H 0.313884 -0.062906 0.536747 0.044 Uiso 1 1 calc R U . . .
C6G C 0.2827(6) 0.0110(4) 0.5698(2) 0.043(4) Uani 1 1 d G . . . .
C6H C 0.2603(6) 0.0258(3) 0.6049(2) 0.036(3) Uani 1 1 d G . . . .
H6H H 0.249471 0.069455 0.611023 0.043 Uiso 1 1 calc R U . . .
C6I C 0.3091(10) -0.1698(8) 0.5761(4) 0.046(3) Uani 1 1 d . . . . .
F6A F 0.2478(6) -0.1974(5) 0.5576(3) 0.064(3) Uani 1 1 d D . . . .
F6B F 0.3648(6) -0.1756(5) 0.5546(3) 0.072(3) Uani 1 1 d D . . . .
F6C F 0.3269(8) -0.2075(5) 0.6062(3) 0.081(3) Uani 1 1 d D . . . .
C6J C 0.2823(19) 0.0632(10) 0.5405(6) 0.096(6) Uani 1 1 d . . . . .
F6D F 0.2657(12) 0.1179(6) 0.5491(4) 0.140(7) Uani 1 1 d D . . . .
F6E F 0.2895(11) 0.0433(6) 0.5086(3) 0.122(5) Uani 1 1 d D . . . .
F6F F 0.3711(11) 0.0832(9) 0.5437(5) 0.156(6) Uani 1 1 d D . . . .
C7A C 0.4249(8) 0.1495(7) 0.6548(4) 0.038(3) Uani 1 1 d . . . . .
C7B C 0.4478(9) 0.1873(7) 0.6315(4) 0.043(4) Uani 1 1 d . . . . .
C7C C 0.4759(8) 0.2297(6) 0.6037(3) 0.045(4) Uani 1 1 d D . . . .
C7D C 0.5330(8) 0.2759(7) 0.6109(4) 0.042(4) Uani 1 1 d D . . . .
H7D H 0.558088 0.279284 0.635487 0.051 Uiso 1 1 calc R U . . .
C7E C 0.5546(8) 0.3170(7) 0.5838(4) 0.040(3) Uani 1 1 d D . . . .
C7F C 0.5185(10) 0.3115(8) 0.5474(4) 0.062(5) Uani 1 1 d D . . . .
H7F H 0.530581 0.341116 0.528618 0.075 Uiso 1 1 calc R U . C 1
C7GA C 0.4650(12) 0.2629(10) 0.5388(5) 0.116(6) Uani 0.55 1 d D U P D 1
C7GB C 0.4532(13) 0.2717(11) 0.5403(5) 0.116(6) Uani 0.45 1 d D U P D 2
C7H C 0.4397(12) 0.2263(9) 0.5676(4) 0.075(6) Uani 1 1 d D . . . .
H7H H 0.396631 0.198357 0.562493 0.090 Uiso 1 1 calc R U . D 1
C7I C 0.6156(10) 0.3647(8) 0.5915(4) 0.048(3) Uani 1 1 d . . . . .
F7A F 0.6277(5) 0.3808(5) 0.6281(2) 0.053(2) Uani 1 1 d . . . . .
F7B F 0.6836(6) 0.3444(6) 0.5817(3) 0.074(3) Uani 1 1 d . . . . .
F7C F 0.6010(6) 0.4196(5) 0.5727(3) 0.073(3) Uani 1 1 d . . . . .
C7JA C 0.4376(17) 0.2505(16) 0.4992(6) 0.118(5) Uani 0.5 1 d D U P D 1
F7DA F 0.394(2) 0.1977(15) 0.4954(9) 0.127(7) Uani 0.5 1 d D U P D 1
F7EA F 0.3954(19) 0.3009(15) 0.4864(9) 0.128(6) Uani 0.5 1 d D U P D 1
F7FA F 0.4921(15) 0.2450(15) 0.4762(6) 0.119(6) Uani 0.5 1 d D U P D 1
C7JB C 0.3999(18) 0.2766(17) 0.5052(7) 0.121(5) Uani 0.5 1 d D U P D 2
F7DB F 0.382(2) 0.2195(15) 0.4887(9) 0.128(6) Uani 0.5 1 d D U P D 2
F7EB F 0.3267(18) 0.2981(17) 0.5058(8) 0.146(7) Uani 0.5 1 d D U P D 2
F7FB F 0.4291(19) 0.3130(16) 0.4790(7) 0.123(6) Uani 0.5 1 d D U P D 2
C8A C 0.4109(8) -0.0325(7) 0.7095(4) 0.039(3) Uani 1 1 d . . . . .
C8B C 0.4374(8) -0.0380(8) 0.6800(4) 0.037(3) Uani 1 1 d . . . . .
C8C C 0.4754(6) -0.0715(4) 0.6502(2) 0.043(4) Uani 1 1 d G . . . .
C8D C 0.4847(6) -0.0396(4) 0.6168(3) 0.047(4) Uani 1 1 d G . . . .
H8D H 0.467076 0.003749 0.613181 0.056 Uiso 1 1 calc R U . . .
C8E C 0.5198(6) -0.0711(6) 0.5888(2) 0.064(6) Uani 1 1 d G . . . .
C8F C 0.5456(6) -0.1345(6) 0.5941(2) 0.071(6) Uani 1 1 d G . . . .
H8F H 0.569558 -0.155995 0.574989 0.086 Uiso 1 1 calc R U . . .
C8G C 0.5363(6) -0.1664(4) 0.6275(3) 0.050(4) Uani 1 1 d G . . . .
C8H C 0.5012(6) -0.1349(4) 0.6555(2) 0.043(4) Uani 1 1 d G . . . .
H8H H 0.494886 -0.156650 0.678321 0.051 Uiso 1 1 calc R U . . .
C8I C 0.5292(13) -0.0389(14) 0.5523(6) 0.089(5) Uani 1 1 d . U . . .
F8A F 0.5930(7) -0.0359(11) 0.5433(4) 0.164(8) Uani 1 1 d D U . . .
F8B F 0.4739(8) -0.0473(8) 0.5281(4) 0.121(5) Uani 1 1 d D U . . .
F8C F 0.5167(14) 0.0336(9) 0.5563(5) 0.176(7) Uani 1 1 d D U . . .
C8J C 0.5635(14) -0.2353(12) 0.6342(9) 0.093(6) Uani 1 1 d . U . . .
F8D F 0.5157(13) -0.2749(8) 0.6110(5) 0.164(7) Uani 1 1 d D U . . .
F8E F 0.6277(10) -0.2454(8) 0.6233(8) 0.233(11) Uani 1 1 d D U . . .
F8F F 0.5553(11) -0.2605(8) 0.6652(4) 0.132(6) Uani 1 1 d D U . . .
C9A C 0.0371(9) 0.3231(8) 0.7730(4) 0.044(4) Uani 1 1 d . . . . .
C9B C -0.0039(10) 0.3194(7) 0.7431(4) 0.045(4) Uani 1 1 d . . . . .
C9C C -0.0689(5) 0.3265(5) 0.7139(2) 0.043(4) Uani 1 1 d G . . . .
C9D C -0.0717(5) 0.3785(5) 0.6891(3) 0.052(4) Uani 1 1 d G . . . .
H9D H -0.031346 0.409573 0.690807 0.062 Uiso 1 1 calc R U . . .
C9E C -0.1334(7) 0.3849(5) 0.6618(3) 0.057(5) Uani 1 1 d G . . . .
C9F C -0.1924(5) 0.3394(6) 0.6592(3) 0.056(5) Uani 1 1 d G . . . .
H9F H -0.234594 0.343729 0.640580 0.067 Uiso 1 1 calc R U . . .
C9G C -0.1896(5) 0.2874(5) 0.6840(3) 0.055(4) Uani 1 1 d G . . . .
C9H C -0.1279(6) 0.2810(4) 0.7113(3) 0.052(4) Uani 1 1 d G . . . .
H9H H -0.125986 0.245551 0.728262 0.062 Uiso 1 1 calc R U . . .
C9I C -0.1352(12) 0.4404(9) 0.6336(5) 0.063(4) Uani 1 1 d . . . . .
F9A F -0.0875(7) 0.4880(6) 0.6441(3) 0.087(4) Uani 1 1 d . . . . .
F9B F -0.1182(11) 0.4216(6) 0.6013(3) 0.119(6) Uani 1 1 d . . . . .
F9C F -0.2049(8) 0.4669(6) 0.6291(5) 0.112(5) Uani 1 1 d . . . . .
C9J C -0.2550(12) 0.2406(11) 0.6815(6) 0.072(4) Uani 1 1 d . . . . .
F9D F -0.2821(6) 0.2260(6) 0.6475(3) 0.080(3) Uani 1 1 d . . . . .
F9E F -0.3157(9) 0.2638(9) 0.6977(4) 0.126(5) Uani 1 1 d . . . . .
F9F F -0.2388(9) 0.1847(8) 0.6989(5) 0.139(6) Uani 1 1 d . . . . .
C10A C 0.0301(4) 0.3007(5) 0.3919(3) 0.041(4) Uani 1 1 d G . . . .
C10B C 0.0029(5) 0.2497(5) 0.4122(3) 0.050(4) Uani 1 1 d G . . . .
H10B H 0.037730 0.218435 0.423554 0.059 Uiso 1 1 calc R U . . .
C10C C -0.0753(6) 0.2445(5) 0.4160(3) 0.065(5) Uani 1 1 d G . . . .
H10C H -0.093939 0.209715 0.429895 0.078 Uiso 1 1 calc R U . . .
C10D C -0.1263(4) 0.2903(6) 0.3995(4) 0.080(7) Uani 1 1 d G . . . .
H10D H -0.179739 0.286795 0.402049 0.096 Uiso 1 1 calc R U . . .
C10E C -0.0990(5) 0.3413(5) 0.3792(3) 0.059(5) Uani 1 1 d G . . . .
H10E H -0.133871 0.372597 0.367862 0.071 Uiso 1 1 calc R U . . .
C10F C -0.0208(6) 0.3465(5) 0.3754(3) 0.051(4) Uani 1 1 d G . . . .
H10F H -0.002202 0.381319 0.361521 0.061 Uiso 1 1 calc R U . . .
C10G C 0.1397(6) 0.3323(5) 0.33892(19) 0.039(3) Uani 1 1 d G . . . .
C10H C 0.1886(6) 0.3822(5) 0.3304(2) 0.051(4) Uani 1 1 d G . . . .
H10H H 0.218313 0.404546 0.349949 0.061 Uiso 1 1 calc R U . . .
C10I C 0.1940(6) 0.3993(5) 0.2933(3) 0.059(5) Uani 1 1 d G . . . .
H10I H 0.227415 0.433351 0.287509 0.071 Uiso 1 1 calc R U . . .
C10J C 0.1505(7) 0.3665(6) 0.2647(2) 0.060(5) Uani 1 1 d G . . . .
H10J H 0.154174 0.378231 0.239391 0.072 Uiso 1 1 calc R U . . .
C10K C 0.1016(7) 0.3167(6) 0.2732(2) 0.065(5) Uani 1 1 d G . . . .
H10K H 0.071829 0.294307 0.253713 0.078 Uiso 1 1 calc R U . . .
C10L C 0.0962(6) 0.2996(5) 0.3103(3) 0.056(5) Uani 1 1 d G . . . .
H10L H 0.062726 0.265501 0.316152 0.067 Uiso 1 1 calc R U . . .
C10M C 0.1727(5) 0.3698(5) 0.4180(3) 0.042(4) Uani 1 1 d G . . . .
C10N C 0.2524(5) 0.3746(5) 0.4231(3) 0.057(5) Uani 1 1 d G . . . .
H10N H 0.283351 0.344599 0.411250 0.068 Uiso 1 1 calc R U . . .
C10O C 0.2869(5) 0.4233(6) 0.4457(4) 0.067(5) Uani 1 1 d G . . . .
H10O H 0.341425 0.426635 0.449211 0.080 Uiso 1 1 calc R U . . .
C10P C 0.2417(7) 0.4672(5) 0.4631(3) 0.065(5) Uani 1 1 d G . . . .
H10P H 0.265271 0.500541 0.478495 0.078 Uiso 1 1 calc R U . . .
C10Q C 0.1620(6) 0.4624(5) 0.4579(3) 0.067(5) Uani 1 1 d G . . . .
H10Q H 0.131041 0.492412 0.469819 0.080 Uiso 1 1 calc R U . . .
C10R C 0.1275(5) 0.4137(6) 0.4354(3) 0.055(5) Uani 1 1 d G . . . .
H10R H 0.072965 0.410376 0.431858 0.066 Uiso 1 1 calc R U . . .
C10S C 0.1804(6) 0.2346(4) 0.3975(3) 0.041(3) Uani 1 1 d G . . . .
C10T C 0.1951(6) 0.1925(5) 0.3689(2) 0.045(4) Uani 1 1 d G . . . .
H10T H 0.182173 0.204658 0.343550 0.054 Uiso 1 1 calc R U . . .
C10U C 0.2289(7) 0.1326(5) 0.3774(3) 0.068(5) Uani 1 1 d G . . . .
H10U H 0.238983 0.103773 0.357804 0.081 Uiso 1 1 calc R U . . .
C10V C 0.2479(7) 0.1148(4) 0.4145(4) 0.062(5) Uani 1 1 d G . . . .
H10V H 0.270928 0.073828 0.420270 0.074 Uiso 1 1 calc R U . . .
C10W C 0.2331(7) 0.1569(5) 0.4431(3) 0.066(5) Uani 1 1 d G . . . .
H10W H 0.246063 0.144767 0.468483 0.079 Uiso 1 1 calc R U . . .
C10X C 0.1993(7) 0.2169(5) 0.4347(2) 0.053(4) Uani 1 1 d G . . . .
H10X H 0.189254 0.245653 0.454230 0.064 Uiso 1 1 calc R U . . .
Cl20 Cl 0.0543(5) 0.2910(4) 0.5092(2) 0.0522(19) Uiso 0.5 1 d D U P . .
Cl21 Cl 0.2108(10) 0.3291(9) 0.5257(5) 0.126(5) Uiso 0.5 1 d D U P . .
C22 C 0.1252(11) 0.315(2) 0.5396(12) 0.075(11) Uiso 0.5 1 d D U P . .
H22A H 0.131627 0.282332 0.559693 0.090 Uiso 0.5 1 calc R U P . .
H22B H 0.108250 0.355769 0.551128 0.090 Uiso 0.5 1 calc R U P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C4A Au1 C4B 29.1(5) . .
C4A Au1 Pt1 146.5(4) . .
C4B Au1 Pt1 159.7(3) . .
C4A Au1 Au2 146.9(5) . .
C4B Au1 Au2 118.1(3) . .
Pt1 Au1 Au2 59.82(2) . .
C4A Au1 Au3 109.6(4) . .
C4B Au1 Au3 102.1(3) . .
Pt1 Au1 Au3 58.32(2) . .
Au2 Au1 Au3 62.09(2) . .
C4A Au1 Au6 141.8(4) . .
C4B Au1 Au6 140.3(4) . .
Pt1 Au1 Au6 58.46(2) . .
Au2 Au1 Au6 59.57(2) . .
Au3 Au1 Au6 108.45(2) . .
C4A Au1 Au4 88.2(4) . .
C4B Au1 Au4 108.8(4) . .
Pt1 Au1 Au4 58.465(16) . .
Au2 Au1 Au4 109.91(2) . .
Au3 Au1 Au4 59.36(2) . .
Au6 Au1 Au4 108.44(2) . .
C4A Au1 Au5 104.8(5) . .
C4B Au1 Au5 132.7(3) . .
Pt1 Au1 Au5 57.80(2) . .
Au2 Au1 Au5 108.24(2) . .
Au3 Au1 Au5 107.41(3) . .
Au6 Au1 Au5 59.80(2) . .
Au4 Au1 Au5 60.233(19) . .
C4A Au1 Au7 92.1(4) . .
C4B Au1 Au7 72.4(4) . .
Pt1 Au1 Au7 121.05(2) . .
Au2 Au1 Au7 71.02(2) . .
Au3 Au1 Au7 122.77(2) . .
Au6 Au1 Au7 69.89(2) . .
Au4 Au1 Au7 177.50(3) . .
Au5 Au1 Au7 117.31(2) . .
C4A Au1 Au8 39.4(5) . .
C4B Au1 Au8 68.4(4) . .
Pt1 Au1 Au8 112.35(3) . .
Au2 Au1 Au8 171.97(3) . .
Au3 Au1 Au8 113.08(3) . .
Au6 Au1 Au8 119.00(3) . .
Au4 Au1 Au8 62.49(2) . .
Au5 Au1 Au8 66.28(2) . .
Au7 Au1 Au8 116.46(2) . .
C4A Au1 Au9 75.6(4) . .
C4B Au1 Au9 87.0(3) . .
Pt1 Au1 Au9 111.98(2) . .
Au2 Au1 Au9 118.94(2) . .
Au3 Au1 Au9 169.12(3) . .
Au6 Au1 Au9 66.35(2) . .
Au4 Au1 Au9 112.24(2) . .
Au5 Au1 Au9 61.73(2) . .
Au7 Au1 Au9 65.473(19) . .
Au8 Au1 Au9 64.46(2) . .
C1A Au2 C1B 30.4(5) . .
C1A Au2 Pt1 139.1(4) . .
C1B Au2 Pt1 166.5(4) . .
C1A Au2 Au1 86.6(4) . .
C1B Au2 Au1 116.0(3) . .
Pt1 Au2 Au1 58.127(17) . .
C1A Au2 Au6 87.7(4) . .
C1B Au2 Au6 108.1(4) . .
Pt1 Au2 Au6 58.43(2) . .
Au1 Au2 Au6 61.005(19) . .
C1A Au2 Au4 127.5(3) . 4_657
C1B Au2 Au4 118.3(3) . 4_657
Pt1 Au2 Au4 58.206(16) . 4_657
Au1 Au2 Au4 108.94(3) . 4_657
Au6 Au2 Au4 61.101(19) . 4_657
C1A Au2 Au3 124.6(3) . .
C1B Au2 Au3 132.9(3) . .
Pt1 Au2 Au3 56.89(2) . .
Au1 Au2 Au3 59.37(2) . .
Au6 Au2 Au3 107.44(2) . .
Au4 Au2 Au3 105.62(2) 4_657 .
C1A Au2 Au3 164.0(4) . 4_657
C1B Au2 Au3 134.6(4) . 4_657
Pt1 Au2 Au3 56.74(2) . 4_657
Au1 Au2 Au3 105.87(3) . 4_657
Au6 Au2 Au3 106.93(2) . 4_657
Au4 Au2 Au3 58.58(2) 4_657 4_657
Au3 Au2 Au3 57.82(2) . 4_657
C1A Au2 Au10 103.2(4) . .
C1B Au2 Au10 83.3(4) . .
Pt1 Au2 Au10 110.20(3) . .
Au1 Au2 Au10 115.69(2) . .
Au6 Au2 Au10 168.54(3) . .
Au4 Au2 Au10 112.87(2) 4_657 .
Au3 Au2 Au10 63.673(18) . .
Au3 Au2 Au10 62.589(19) 4_657 .
C1A Au2 Au11 109.6(4) . 4_657
C1B Au2 Au11 80.9(3) . 4_657
Pt1 Au2 Au11 104.79(2) . 4_657
Au1 Au2 Au11 162.89(3) . 4_657
Au6 Au2 Au11 112.67(2) . 4_657
Au4 Au2 Au11 57.10(2) 4_657 4_657
Au3 Au2 Au11 112.13(2) . 4_657
Au3 Au2 Au11 59.33(2) 4_657 4_657
Au10 Au2 Au11 67.044(18) . 4_657
C6A Au3 C6B 30.1(5) . .
C6A Au3 Pt1 144.5(4) . .
C6B Au3 Pt1 164.2(4) . .
C6A Au3 Au3 99.0(4) . 4_657
C6B Au3 Au3 127.1(3) . 4_657
Pt1 Au3 Au3 58.513(15) . 4_657
C6A Au3 Au4 152.1(4) . .
C6B Au3 Au4 122.5(3) . .
Pt1 Au3 Au4 59.042(19) . .
Au3 Au3 Au4 108.74(2) 4_657 .
C6A Au3 Au1 113.2(4) . .
C6B Au3 Au1 107.4(4) . .
Pt1 Au3 Au1 58.37(2) . .
Au3 Au3 Au1 108.02(2) 4_657 .
Au4 Au3 Au1 60.92(2) . .
C6A Au3 Au2 87.0(4) . .
C6B Au3 Au2 109.3(4) . .
Pt1 Au3 Au2 58.547(16) . .
Au3 Au3 Au2 61.31(2) 4_657 .
Au4 Au3 Au2 108.31(3) . .
Au1 Au3 Au2 58.54(2) . .
C6A Au3 Au2 138.2(4) . 4_657
C6B Au3 Au2 137.1(4) . 4_657
Pt1 Au3 Au2 58.391(16) . 4_657
Au3 Au3 Au2 60.87(2) 4_657 4_657
Au4 Au3 Au2 59.38(2) . 4_657
Au1 Au3 Au2 107.99(2) . 4_657
Au2 Au3 Au2 109.36(3) . 4_657
C6A Au3 Au11 105.5(4) . .
C6B Au3 Au11 81.3(4) . .
Pt1 Au3 Au11 109.55(2) . .
Au3 Au3 Au11 118.73(3) 4_657 .
Au4 Au3 Au11 58.83(2) . .
Au1 Au3 Au11 111.85(2) . .
Au2 Au3 Au11 167.00(3) . .
Au2 Au3 Au11 63.60(2) 4_657 .
C6A Au3 Au10 78.4(4) . 4_657
C6B Au3 Au10 85.1(4) . 4_657
Pt1 Au3 Au10 109.37(2) . 4_657
Au3 Au3 Au10 63.697(19) 4_657 4_657
Au4 Au3 Au10 111.32(3) . 4_657
Au1 Au3 Au10 167.36(2) . 4_657
Au2 Au3 Au10 119.53(2) . 4_657
Au2 Au3 Au10 59.98(2) 4_657 4_657
Au11 Au3 Au10 67.66(2) . 4_657
C6A Au3 Au10 38.9(4) . .
C6B Au3 Au10 69.0(3) . .
Pt1 Au3 Au10 108.18(2) . .
Au3 Au3 Au10 62.193(18) 4_657 .
Au4 Au3 Au10 166.97(2) . .
Au1 Au3 Au10 111.41(3) . .
Au2 Au3 Au10 59.60(2) . .
Au2 Au3 Au10 117.79(2) 4_657 .
Au11 Au3 Au10 132.98(3) . .
Au10 Au3 Au10 74.08(3) 4_657 .
C7A Au4 Pt1 156.1(4) . .
C7A Au4 Au3 102.6(4) . .
Pt1 Au4 Au3 58.20(2) . .
C7A Au4 Au2 100.5(4) . 4_657
Pt1 Au4 Au2 59.09(2) . 4_657
Au3 Au4 Au2 62.04(2) . 4_657
C7A Au4 Au11 43.4(4) . .
Pt1 Au4 Au11 112.88(3) . .
Au3 Au4 Au11 63.57(2) . .
Au2 Au4 Au11 66.23(2) 4_657 .
C7A Au4 Au1 128.0(4) . .
Pt1 Au4 Au1 57.694(17) . .
Au3 Au4 Au1 59.72(2) . .
Au2 Au4 Au1 109.14(2) 4_657 .
Au11 Au4 Au1 114.87(2) . .
C7A Au4 Au6 124.9(4) . 4_657
Pt1 Au4 Au6 57.928(19) . 4_657
Au3 Au4 Au6 107.89(2) . 4_657
Au2 Au4 Au6 58.87(2) 4_657 4_657
Au11 Au4 Au6 118.83(2) . 4_657
Au1 Au4 Au6 106.96(2) . 4_657
C7A Au4 Au5 146.3(4) . .
Pt1 Au4 Au5 57.48(2) . .
Au3 Au4 Au5 107.51(3) . .
Au2 Au4 Au5 106.72(2) 4_657 .
Au11 Au4 Au5 170.27(3) . .
Au1 Au4 Au5 60.00(2) . .
Au6 Au4 Au5 58.656(19) 4_657 .
C7A Au4 Au8 88.7(4) . .
Pt1 Au4 Au8 111.16(3) . .
Au3 Au4 Au8 112.84(3) . .
Au2 Au4 Au8 170.18(3) 4_657 .
Au11 Au4 Au8 120.13(2) . .
Au1 Au4 Au8 61.856(19) . .
Au6 Au4 Au8 118.30(3) 4_657 .
Au5 Au4 Au8 65.96(2) . .
C7A Au4 Au12 90.4(4) . .
Pt1 Au4 Au12 110.00(2) . .
Au3 Au4 Au12 166.69(3) . .
Au2 Au4 Au12 119.08(2) 4_657 .
Au11 Au4 Au12 129.66(3) . .
Au1 Au4 Au12 109.69(2) . .
Au6 Au4 Au12 65.94(2) 4_657 .
Au5 Au4 Au12 59.19(2) . .
Au8 Au4 Au12 63.75(2) . .
C3A Au5 C3B 29.3(5) . .
C3A Au5 Pt1 149.2(4) . .
C3B Au5 Pt1 164.0(3) . .
C3A Au5 Au6 149.1(3) . 4_657
C3B Au5 Au6 119.8(3) . 4_657
Pt1 Au5 Au6 58.894(16) . 4_657
C3A Au5 Au5 115.9(4) . 4_657
C3B Au5 Au5 106.2(3) . 4_657
Pt1 Au5 Au5 58.428(15) . 4_657
Au6 Au5 Au5 60.76(2) 4_657 4_657
C3A Au5 Au6 91.9(4) . .
C3B Au5 Au6 111.3(4) . .
Pt1 Au5 Au6 58.453(16) . .
Au6 Au5 Au6 108.61(3) 4_657 .
Au5 Au5 Au6 59.53(2) 4_657 .
C3A Au5 Au1 101.9(3) . .
C3B Au5 Au1 130.4(3) . .
Pt1 Au5 Au1 57.86(2) . .
Au6 Au5 Au1 108.31(2) 4_657 .
Au5 Au5 Au1 107.33(2) 4_657 .
Au6 Au5 Au1 59.733(19) . .
C3A Au5 Au4 135.3(4) . .
C3B Au5 Au4 136.8(4) . .
Pt1 Au5 Au4 58.312(19) . .
Au6 Au5 Au4 60.60(2) 4_657 .
Au5 Au5 Au4 108.627(19) 4_657 .
Au6 Au5 Au4 108.01(2) . .
Au1 Au5 Au4 59.76(2) . .
C3A Au5 Au12 93.2(4) . .
C3B Au5 Au12 75.3(4) . .
Pt1 Au5 Au12 115.65(2) . .
Au6 Au5 Au12 68.86(2) 4_657 .
Au5 Au5 Au12 122.13(3) 4_657 .
Au6 Au5 Au12 172.82(3) . .
Au1 Au5 Au12 114.15(2) . .
Au4 Au5 Au12 64.82(2) . .
C3A Au5 Au9 39.0(3) . .
C3B Au5 Au9 68.3(3) . .
Pt1 Au5 Au9 113.69(2) . .
Au6 Au5 Au9 171.89(2) 4_657 .
Au5 Au5 Au9 119.39(3) 4_657 .
Au6 Au5 Au9 67.08(2) . .
Au1 Au5 Au9 63.64(2) . .
Au4 Au5 Au9 113.43(2) . .
Au12 Au5 Au9 114.52(2) . .
C3A Au5 Au8 75.5(4) . .
C3B Au5 Au8 88.3(3) . .
Pt1 Au5 Au8 106.97(2) . .
Au6 Au5 Au8 114.68(2) 4_657 .
Au5 Au5 Au8 165.320(15) 4_657 .
Au6 Au5 Au8 113.10(2) . .
Au1 Au5 Au8 59.635(18) . .
Au4 Au5 Au8 59.965(18) . .
Au12 Au5 Au8 63.495(19) . .
Au9 Au5 Au8 62.92(2) . .
C9A Au6 C9B 30.7(5) . .
C9A Au6 Pt1 139.8(4) . .
C9B Au6 Pt1 168.7(4) . .
C9A Au6 Au2 121.8(4) . .
C9B Au6 Au2 117.1(4) . .
Pt1 Au6 Au2 59.60(2) . .
C9A Au6 Au5 88.8(4) . 4_657
C9B Au6 Au5 117.1(4) . 4_657
Pt1 Au6 Au5 58.31(2) . 4_657
Au2 Au6 Au5 109.35(2) . 4_657
C9A Au6 Au1 161.9(4) . .
C9B Au6 Au1 131.2(4) . .
Pt1 Au6 Au1 57.948(17) . .
Au2 Au6 Au1 59.427(19) . .
Au5 Au6 Au1 108.06(3) 4_657 .
C9A Au6 Au5 127.4(4) . .
C9B Au6 Au5 130.5(4) . .
Pt1 Au6 Au5 57.88(2) . .
Au2 Au6 Au5 108.67(2) . .
Au5 Au6 Au5 59.71(2) 4_657 .
Au1 Au6 Au5 60.47(2) . .
C9A Au6 Au4 86.8(4) . 4_657
C9B Au6 Au4 110.6(4) . 4_657
Pt1 Au6 Au4 58.190(16) . 4_657
Au2 Au6 Au4 60.033(19) . 4_657
Au5 Au6 Au4 60.75(2) 4_657 4_657
Au1 Au6 Au4 106.87(3) . 4_657
Au5 Au6 Au4 107.92(2) . 4_657
C9A Au6 Au12 33.9(4) . 4_657
C9B Au6 Au12 64.6(4) . 4_657
Pt1 Au6 Au12 106.28(2) . 4_657
Au2 Au6 Au12 115.64(2) . 4_657
Au5 Au6 Au12 57.94(2) 4_657 4_657
Au1 Au6 Au12 164.18(3) . 4_657
Au5 Au6 Au12 111.64(2) . 4_657
Au4 Au6 Au12 60.96(2) 4_657 4_657
C9A Au6 Au9 106.6(4) . .
C9B Au6 Au9 83.7(4) . .
Pt1 Au6 Au9 107.51(2) . .
Au2 Au6 Au9 114.34(2) . .
Au5 Au6 Au9 113.40(2) 4_657 .
Au1 Au6 Au9 61.26(2) . .
Au5 Au6 Au9 60.070(18) . .
Au4 Au6 Au9 165.70(2) 4_657 .
Au12 Au6 Au9 128.85(3) 4_657 .
C1A Au7 C2B 153.5(6) . .
C1A Au7 C2A 173.2(6) . .
C2B Au7 C2A 32.5(6) . .
C1A Au7 Au1 90.2(4) . .
C2B Au7 Au1 112.0(4) . .
C2A Au7 Au1 86.9(5) . .
C1A Au7 Au9 139.3(4) . .
C2B Au7 Au9 67.1(4) . .
C2A Au7 Au9 34.6(4) . .
Au1 Au7 Au9 60.226(19) . .
C4A Au8 C5A 174.0(6) . .
C4A Au8 Au1 46.8(4) . .
C5A Au8 Au1 138.4(4) . .
C4A Au8 Au4 87.8(4) . .
C5A Au8 Au4 98.0(4) . .
Au1 Au8 Au4 55.66(2) . .
C4A Au8 Au5 100.0(4) . .
C5A Au8 Au5 84.7(4) . .
Au1 Au8 Au5 54.085(18) . .
Au4 Au8 Au5 54.073(18) . .
C4A Au8 Au12 145.6(4) . .
C5A Au8 Au12 40.4(4) . .
Au1 Au8 Au12 101.47(2) . .
Au4 Au8 Au12 59.09(2) . .
Au5 Au8 Au12 54.334(18) . .
C2A Au9 C3A 174.1(6) . .
C2A Au9 Au5 139.2(4) . .
C3A Au9 Au5 46.5(4) . .
C2A Au9 Au1 85.5(5) . .
C3A Au9 Au1 100.4(4) . .
Au5 Au9 Au1 54.630(17) . .
C2A Au9 Au6 98.2(4) . .
C3A Au9 Au6 85.4(4) . .
Au5 Au9 Au6 52.848(17) . .
Au1 Au9 Au6 52.386(15) . .
C2A Au9 Au7 39.4(4) . .
C3A Au9 Au7 145.1(4) . .
Au5 Au9 Au7 101.77(2) . .
Au1 Au9 Au7 54.30(2) . .
Au6 Au9 Au7 60.461(17) . .
C6A Au10 C8A 176.4(6) . 4_657
C6A Au10 Au2 89.7(4) . .
C8A Au10 Au2 93.9(4) 4_657 .
C6A Au10 Au3 97.6(4) . 4_657
C8A Au10 Au3 84.5(4) 4_657 4_657
Au2 Au10 Au3 57.43(2) . 4_657
C6A Au10 Au3 45.6(4) . .
C8A Au10 Au3 137.2(4) 4_657 .
Au2 Au10 Au3 56.724(19) . .
Au3 Au10 Au3 54.11(2) 4_657 .
C7A Au11 C8B 143.8(5) . .
C7A Au11 C8A 174.5(5) . .
C8B Au11 C8A 31.6(5) . .
C7A Au11 Au4 49.3(4) . .
C8B Au11 Au4 164.4(3) . .
C8A Au11 Au4 135.9(3) . .
C7A Au11 Au3 102.3(4) . .
C8B Au11 Au3 106.8(3) . .
C8A Au11 Au3 83.1(4) . .
Au4 Au11 Au3 57.595(19) . .
C7A Au11 Au2 96.9(4) . 4_657
C8B Au11 Au2 116.8(3) . 4_657
C8A Au11 Au2 86.5(4) . 4_657
Au4 Au11 Au2 56.667(18) . 4_657
Au3 Au11 Au2 57.068(18) . 4_657
C9A Au12 C5A 176.0(6) 4_657 .
C9A Au12 C5B 151.8(6) 4_657 .
C5A Au12 C5B 32.1(6) . .
C9A Au12 Au5 90.1(4) 4_657 .
C5A Au12 Au5 87.8(4) . .
C5B Au12 Au5 109.7(4) . .
C9A Au12 Au4 84.7(5) 4_657 .
C5A Au12 Au4 91.3(4) . .
C5B Au12 Au4 122.8(4) . .
Au5 Au12 Au4 55.989(18) . .
C9A Au12 Au6 40.1(4) 4_657 4_657
C5A Au12 Au6 136.6(4) . 4_657
C5B Au12 Au6 162.6(4) . 4_657
Au5 Au12 Au6 53.199(17) . 4_657
Au4 Au12 Au6 53.098(17) . 4_657
C9A Au12 Au8 140.7(4) 4_657 .
C5A Au12 Au8 35.4(4) . .
C5B Au12 Au8 67.5(4) . .
Au5 Au12 Au8 62.17(2) . .
Au4 Au12 Au8 57.158(19) . .
Au6 Au12 Au8 102.19(2) 4_657 .
Au5 Pt1 Au5 63.14(3) 4_657 .
Au5 Pt1 Au3 179.644(17) 4_657 .
Au5 Pt1 Au3 116.94(2) . .
Au5 Pt1 Au3 116.94(2) 4_657 4_657
Au5 Pt1 Au3 179.645(17) . 4_657
Au3 Pt1 Au3 62.97(3) . 4_657
Au5 Pt1 Au1 64.343(19) 4_657 4_657
Au5 Pt1 Au1 116.55(3) . 4_657
Au3 Pt1 Au1 115.80(3) . 4_657
Au3 Pt1 Au1 63.309(19) 4_657 4_657
Au5 Pt1 Au1 116.55(3) 4_657 .
Au5 Pt1 Au1 64.343(19) . .
Au3 Pt1 Au1 63.311(19) . .
Au3 Pt1 Au1 115.80(3) 4_657 .
Au1 Pt1 Au1 179.06(4) 4_657 .
Au5 Pt1 Au6 62.79(2) 4_657 .
Au5 Pt1 Au6 63.67(2) . .
Au3 Pt1 Au6 116.902(19) . .
Au3 Pt1 Au6 116.687(19) 4_657 .
Au1 Pt1 Au6 116.96(2) 4_657 .
Au1 Pt1 Au6 63.594(17) . .
Au5 Pt1 Au6 63.67(2) 4_657 4_657
Au5 Pt1 Au6 62.80(2) . 4_657
Au3 Pt1 Au6 116.688(19) . 4_657
Au3 Pt1 Au6 116.900(19) 4_657 4_657
Au1 Pt1 Au6 63.592(17) 4_657 4_657
Au1 Pt1 Au6 116.96(2) . 4_657
Au6 Pt1 Au6 116.18(4) . 4_657
Au5 Pt1 Au4 64.205(18) 4_657 4_657
Au5 Pt1 Au4 117.52(3) . 4_657
Au3 Pt1 Au4 115.53(3) . 4_657
Au3 Pt1 Au4 62.752(18) 4_657 4_657
Au1 Pt1 Au4 63.84(2) 4_657 4_657
Au1 Pt1 Au4 116.14(2) . 4_657
Au6 Pt1 Au4 63.882(18) . 4_657
Au6 Pt1 Au4 117.18(2) 4_657 4_657
Au5 Pt1 Au4 117.52(3) 4_657 .
Au5 Pt1 Au4 64.204(19) . .
Au3 Pt1 Au4 62.754(19) . .
Au3 Pt1 Au4 115.53(3) 4_657 .
Au1 Pt1 Au4 116.14(2) 4_657 .
Au1 Pt1 Au4 63.84(2) . .
Au6 Pt1 Au4 117.19(2) . .
Au6 Pt1 Au4 63.883(18) 4_657 .
Au4 Pt1 Au4 178.19(4) 4_657 .
Au5 Pt1 Au2 115.438(19) 4_657 4_657
Au5 Pt1 Au2 115.080(19) . 4_657
Au3 Pt1 Au2 64.87(2) . 4_657
Au3 Pt1 Au2 64.57(2) 4_657 4_657
Au1 Pt1 Au2 62.054(17) 4_657 4_657
Au1 Pt1 Au2 117.41(2) . 4_657
Au6 Pt1 Au2 178.09(3) . 4_657
Au6 Pt1 Au2 61.97(2) 4_657 4_657
Au4 Pt1 Au2 116.28(2) 4_657 4_657
Au4 Pt1 Au2 62.703(18) . 4_657
Au5 Pt1 Au2 115.079(19) 4_657 .
Au5 Pt1 Au2 115.436(19) . .
Au3 Pt1 Au2 64.57(2) . .
Au3 Pt1 Au2 64.87(2) 4_657 .
Au1 Pt1 Au2 117.42(2) 4_657 .
Au1 Pt1 Au2 62.053(17) . .
Au6 Pt1 Au2 61.97(2) . .
Au6 Pt1 Au2 178.09(3) 4_657 .
Au4 Pt1 Au2 62.704(18) 4_657 .
Au4 Pt1 Au2 116.28(2) . .
Au2 Pt1 Au2 119.89(4) 4_657 .
C10S P1 C10M 108.0(5) . .
C10S P1 C10A 110.9(5) . .
C10M P1 C10A 110.4(5) . .
C10S P1 C10G 110.3(5) . .
C10M P1 C10G 109.8(5) . .
C10A P1 C10G 107.4(5) . .
C1B C1A Au7 169.6(13) . .
C1B C1A Au2 81.2(10) . .
Au7 C1A Au2 107.9(7) . .
C1A C1B C1C 163.6(14) . .
C1A C1B Au2 68.4(9) . .
C1C C1B Au2 128.0(9) . .
C1D C1C C1H 120.0 . .
C1D C1C C1B 118.5(8) . .
C1H C1C C1B 121.5(8) . .
C1C C1D C1E 120.0 . .
C1F C1E C1D 120.0 . .
C1F C1E C1I 119.9(9) . .
C1D C1E C1I 120.1(9) . .
C1E C1F C1G 120.0 . .
C1H C1G C1F 120.0 . .
C1H C1G C1J 120.9(9) . .
C1F C1G C1J 119.1(9) . .
C1G C1H C1C 120.0 . .
F1C C1I F1A 104.9(14) . .
F1C C1I F1B 106.7(15) . .
F1A C1I F1B 104.5(14) . .
F1C C1I C1E 114.1(13) . .
F1A C1I C1E 113.2(13) . .
F1B C1I C1E 112.6(13) . .
F1F C1J F1E 106.7(14) . .
F1F C1J F1D 106.4(15) . .
F1E C1J F1D 107.0(13) . .
F1F C1J C1G 113.3(12) . .
F1E C1J C1G 112.0(14) . .
F1D C1J C1G 111.0(14) . .
C2B C2A Au9 178.4(16) . .
C2B C2A Au7 73.5(10) . .
Au9 C2A Au7 106.0(7) . .
C2A C2B C2C 158.8(16) . .
C2A C2B Au7 74.1(10) . .
C2C C2B Au7 126.9(11) . .
C2D C2C C2H 120.0 . .
C2D C2C C2B 118.4(10) . .
C2H C2C C2B 121.6(10) . .
C2E C2D C2C 120.0 . .
C2D C2E C2F 120.0 . .
C2D C2E C2I 118.1(12) . .
C2F C2E C2I 121.8(12) . .
C2G C2F C2E 120.0 . .
C2F C2G C2H 120.0 . .
C2F C2G C2J 120.6(14) . .
C2H C2G C2J 119.2(15) . .
C2G C2H C2C 120.0 . .
F2C C2I F2B 106.6(19) . .
F2C C2I F2A 114(3) . .
F2B C2I F2A 105.4(18) . .
F2C C2I C2E 113.2(17) . .
F2B C2I C2E 109(2) . .
F2A C2I C2E 108.4(15) . .
F2D C2J F2E 109(2) . .
F2D C2J F2F 111(3) . .
F2E C2J F2F 104(2) . .
F2D C2J C2G 115.1(18) . .
F2E C2J C2G 108(3) . .
F2F C2J C2G 108.1(18) . .
C3B C3A Au9 173.6(13) . .
C3B C3A Au5 79.4(9) . .
Au9 C3A Au5 94.5(6) . .
C3A C3B C3C 156.4(14) . .
C3A C3B Au5 71.2(10) . .
C3C C3B Au5 132.4(9) . .
C3D C3C C3H 120.0 . .
C3D C3C C3B 119.0(7) . .
C3H C3C C3B 120.9(7) . .
C3E C3D C3C 120.0 . .
C3F C3E C3D 120.0 . .
C3F C3E C3I 119.3(11) . .
C3D C3E C3I 120.7(10) . .
C3E C3F C3G 120.0 . .
C3F C3G C3H 120.0 . .
C3F C3G C3J 119.2(11) . .
C3H C3G C3J 120.4(10) . .
C3G C3H C3C 120.0 . .
F3B C3I F3C 111(2) . .
F3B C3I F3A 103.4(19) . .
F3C C3I F3A 103.9(19) . .
F3B C3I C3E 115.0(16) . .
F3C C3I C3E 112.8(17) . .
F3A C3I C3E 109.5(18) . .
F3E C3J F3F 121(3) . .
F3E C3J F3D 97(2) . .
F3F C3J F3D 99(2) . .
F3E C3J C3G 114(2) . .
F3F C3J C3G 117.1(16) . .
F3D C3J C3G 102(2) . .
C4B C4A Au8 177.1(13) . .
C4B C4A Au1 87.8(10) . .
Au8 C4A Au1 93.9(6) . .
C4A C4B C4C 164.7(13) . .
C4A C4B Au1 63.1(8) . .
C4C C4B Au1 131.7(8) . .
C4D C4C C4H 120.0 . .
C4D C4C C4B 118.0(8) . .
C4H C4C C4B 122.0(8) . .
C4E C4D C4C 120.0 . .
C4D C4E C4F 120.0 . .
C4D C4E C4I 119.2(10) . .
C4F C4E C4I 120.8(10) . .
C4G C4F C4E 120.0 . .
C4H C4G C4F 120.0 . .
C4H C4G C4J 120.3(9) . .
C4F C4G C4J 119.6(10) . .
C4G C4H C4C 120.0 . .
F4C C4I F4A 114(2) . .
F4C C4I F4B 101.4(16) . .
F4A C4I F4B 103.8(16) . .
F4C C4I C4E 114.1(16) . .
F4A C4I C4E 111.9(14) . .
F4B C4I C4E 110.4(17) . .
F4F C4J F4D 105.0(15) . .
F4F C4J F4E 107.6(16) . .
F4D C4J F4E 103.8(14) . .
F4F C4J C4G 112.1(13) . .
F4D C4J C4G 114.1(15) . .
F4E C4J C4G 113.5(14) . .
C5B C5A Au8 175.0(13) . .
C5B C5A Au12 74.1(10) . .
Au8 C5A Au12 104.2(7) . .
C5A C5B C5C 161.7(16) . .
C5A C5B Au12 73.9(10) . .
C5C C5B Au12 124.4(11) . .
C5D C5C C5H 118.4(13) . .
C5D C5C C5B 119.2(13) . .
C5H C5C C5B 122.4(14) . .
C5C C5D C5EA 117.1(15) . .
C5C C5D C5EB 122.0(15) . .
C5F C5EA C5D 118.7(16) . .
C5F C5EA C5IA 121.4(18) . .
C5D C5EA C5IA 119.8(19) . .
C5D C5EB C5F 114.1(15) . .
C5D C5EB C5IB 120.6(19) . .
C5F C5EB C5IB 125.3(19) . .
C5G C5F C5EA 117.8(15) . .
C5G C5F C5EB 122.0(14) . .
C5F C5G C5H 119.3(15) . .
C5F C5G C5J 123(2) . .
C5H C5G C5J 118(2) . .
C5G C5H C5C 120.8(18) . .
F5BA C5IA F5CA 113(3) . .
F5BA C5IA F5AA 109(2) . .
F5CA C5IA F5AA 98(2) . .
F5BA C5IA C5EA 111(2) . .
F5CA C5IA C5EA 120(2) . .
F5AA C5IA C5EA 104(2) . .
F5BB C5IB F5CB 100(2) . .
F5BB C5IB F5AB 101.1(19) . .
F5CB C5IB F5AB 101(2) . .
F5BB C5IB C5EB 119(2) . .
F5CB C5IB C5EB 113(2) . .
F5AB C5IB C5EB 119(2) . .
F5E C5J F5D 111(3) . .
F5E C5J F5F 103(2) . .
F5D C5J F5F 98(2) . .
F5E C5J C5G 117(2) . .
F5D C5J C5G 114.5(17) . .
F5F C5J C5G 111(3) . .
C6B C6A Au10 177.5(13) . .
C6B C6A Au3 82.0(9) . .
Au10 C6A Au3 95.5(6) . .
C6A C6B C6C 162.2(14) . .
C6A C6B Au3 67.9(9) . .
C6C C6B Au3 129.9(8) . .
C6D C6C C6H 120.0 . .
C6D C6C C6B 118.3(8) . .
C6H C6C C6B 121.6(8) . .
C6C C6D C6E 120.0 . .
C6F C6E C6D 120.0 . .
C6F C6E C6I 118.5(8) . .
C6D C6E C6I 121.5(8) . .
C6E C6F C6G 120.0 . .
C6F C6G C6H 120.0 . .
C6F C6G C6J 120.2(9) . .
C6H C6G C6J 119.6(9) . .
C6G C6H C6C 120.0 . .
F6B C6I F6A 106.0(13) . .
F6B C6I F6C 107.1(14) . .
F6A C6I F6C 105.3(13) . .
F6B C6I C6E 114.8(13) . .
F6A C6I C6E 111.1(13) . .
F6C C6I C6E 111.9(12) . .
F6D C6J F6E 126.4(19) . .
F6D C6J C6G 118.3(15) . .
F6E C6J C6G 114.6(16) . .
F6D C6J F6F 90(2) . .
F6E C6J F6F 87.9(18) . .
C6G C6J F6F 101.3(19) . .
C7B C7A Au11 157.5(13) . .
C7B C7A Au4 115.2(12) . .
Au11 C7A Au4 87.3(6) . .
C7A C7B C7C 178.0(16) . .
C7D C7C C7H 117.6(11) . .
C7D C7C C7B 125.0(12) . .
C7H C7C C7B 117.3(12) . .
C7E C7D C7C 122.5(13) . .
C7D C7E C7F 118.8(12) . .
C7D C7E C7I 122.2(13) . .
C7F C7E C7I 119.0(12) . .
C7GA C7F C7E 120.0(12) . .
C7E C7F C7GB 120.0(12) . .
C7F C7GA C7H 119.0(15) . .
C7F C7GA C7JA 119.2(17) . .
C7H C7GA C7JA 121.8(19) . .
C7H C7GB C7JB 120.2(19) . .
C7H C7GB C7F 117.1(15) . .
C7JB C7GB C7F 122.7(17) . .
C7GB C7H C7C 121.9(15) . .
C7C C7H C7GA 121.2(15) . .
F7C C7I F7B 105.3(13) . .
F7C C7I F7A 106.8(14) . .
F7B C7I F7A 105.9(13) . .
F7C C7I C7E 112.4(13) . .
F7B C7I C7E 112.9(14) . .
F7A C7I C7E 113.0(13) . .
F7FA C7JA F7DA 108(2) . .
F7FA C7JA F7EA 105(2) . .
F7DA C7JA F7EA 108(2) . .
F7FA C7JA C7GA 116(2) . .
F7DA C7JA C7GA 112(3) . .
F7EA C7JA C7GA 108(2) . .
F7DB C7JB F7FB 105(2) . .
F7DB C7JB F7EB 97(2) . .
F7FB C7JB F7EB 105(2) . .
F7DB C7JB C7GB 114(2) . .
F7FB C7JB C7GB 112(2) . .
F7EB C7JB C7GB 121(2) . .
C8B C8A Au10 176.1(13) . 4_657
C8B C8A Au11 70.4(10) . .
Au10 C8A Au11 107.5(6) 4_657 .
C8A C8B C8C 156.4(15) . .
C8A C8B Au11 78.0(10) . .
C8C C8B Au11 125.3(9) . .
C8D C8C C8H 120.0 . .
C8D C8C C8B 120.0(8) . .
C8H C8C C8B 120.0(8) . .
C8C C8D C8E 120.0 . .
C8F C8E C8D 120.0 . .
C8F C8E C8I 118.5(14) . .
C8D C8E C8I 121.5(14) . .
C8E C8F C8G 120.0 . .
C8H C8G C8F 120.0 . .
C8H C8G C8J 118.6(13) . .
C8F C8G C8J 121.4(13) . .
C8G C8H C8C 120.0 . .
F8A C8I F8B 120.1(19) . .
F8A C8I C8E 117(2) . .
F8B C8I C8E 113.9(17) . .
F8A C8I F8C 97(2) . .
F8B C8I F8C 95(2) . .
C8E C8I F8C 108.9(17) . .
F8E C8J F8F 113(3) . .
F8E C8J F8D 103(2) . .
F8F C8J F8D 100(2) . .
F8E C8J C8G 113(2) . .
F8F C8J C8G 118(2) . .
F8D C8J C8G 107(2) . .
C9B C9A Au12 173.6(13) . 4_657
C9B C9A Au6 80.4(10) . .
Au12 C9A Au6 106.0(7) 4_657 .
C9A C9B C9C 162.5(14) . .
C9A C9B Au6 68.8(10) . .
C9C C9B Au6 128.6(9) . .
C9D C9C C9H 120.0 . .
C9D C9C C9B 120.5(9) . .
C9H C9C C9B 119.5(9) . .
C9C C9D C9E 120.0 . .
C9F C9E C9D 120.0 . .
C9F C9E C9I 119.8(10) . .
C9D C9E C9I 120.2(10) . .
C9G C9F C9E 120.0 . .
C9F C9G C9H 120.0 . .
C9F C9G C9J 118.9(11) . .
C9H C9G C9J 121.0(11) . .
C9G C9H C9C 120.0 . .
F9B C9I F9A 106.6(19) . .
F9B C9I F9C 107.8(16) . .
F9A C9I F9C 106.0(16) . .
F9B C9I C9E 112.3(15) . .
F9A C9I C9E 113.4(13) . .
F9C C9I C9E 110.3(17) . .
F9D C9J F9F 106.3(19) . .
F9D C9J F9E 104.9(17) . .
F9F C9J F9E 104.3(19) . .
F9D C9J C9G 114.2(16) . .
F9F C9J C9G 114.1(17) . .
F9E C9J C9G 112.0(18) . .
C10B C10A C10F 120.0 . .
C10B C10A P1 121.0(6) . .
C10F C10A P1 119.0(6) . .
C10A C10B C10C 120.0 . .
C10B C10C C10D 120.0 . .
C10E C10D C10C 120.0 . .
C10D C10E C10F 120.0 . .
C10E C10F C10A 120.0 . .
C10H C10G C10L 120.0 . .
C10H C10G P1 121.2(5) . .
C10L C10G P1 118.8(5) . .
C10G C10H C10I 120.0 . .
C10J C10I C10H 120.0 . .
C10K C10J C10I 120.0 . .
C10J C10K C10L 120.0 . .
C10K C10L C10G 120.0 . .
C10N C10M C10R 120.0 . .
C10N C10M P1 118.5(6) . .
C10R C10M P1 121.4(6) . .
C10O C10N C10M 120.0 . .
C10P C10O C10N 120.0 . .
C10O C10P C10Q 120.0 . .
C10R C10Q C10P 120.0 . .
C10Q C10R C10M 120.0 . .
C10T C10S C10X 120.0 . .
C10T C10S P1 120.1(6) . .
C10X C10S P1 119.8(6) . .
C10S C10T C10U 120.0 . .
C10T C10U C10V 120.0 . .
C10W C10V C10U 120.0 . .
C10V C10W C10X 120.0 . .
C10W C10X C10S 120.0 . .
Cl20 C22 Cl21 120(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Au1 C4A 2.283(13) .
Au1 C4B 2.557(14) .
Au1 Pt1 2.7563(7) .
Au1 Au2 2.8672(8) .
Au1 Au3 2.8923(9) .
Au1 Au6 2.9127(8) .
Au1 Au4 2.9271(9) .
Au1 Au5 2.9342(9) .
Au1 Au7 3.0164(10) .
Au1 Au8 3.1260(9) .
Au1 Au9 3.2241(9) .
Au2 C1A 2.312(15) .
Au2 C1B 2.458(13) .
Au2 Pt1 2.8057(8) .
Au2 Au6 2.8713(10) .
Au2 Au4 2.9061(8) 4_657
Au2 Au3 2.9702(9) .
Au2 Au3 2.9827(9) 4_657
Au2 Au10 3.0644(10) .
Au2 Au11 3.1832(9) 4_657
Au3 C6A 2.286(14) .
Au3 C6B 2.445(13) .
Au3 Pt1 2.7548(9) .
Au3 Au3 2.8778(11) 4_657
Au3 Au4 2.8816(9) .
Au3 Au11 3.0564(9) .
Au3 Au10 3.1417(9) 4_657
Au3 Au10 3.1842(8) .
Au4 C7A 2.217(14) .
Au4 Pt1 2.7795(7) .
Au4 Au11 2.9204(9) .
Au4 Au6 2.9368(8) 4_657
Au4 Au5 2.9410(8) .
Au4 Au8 3.1442(9) .
Au4 Au12 3.2109(10) .
Au5 C3A 2.306(13) .
Au5 C3B 2.394(15) .
Au5 Pt1 2.7544(9) .
Au5 Au6 2.8790(9) 4_657
Au5 Au5 2.8841(12) 4_657
Au5 Au6 2.9147(9) .
Au5 Au12 3.0472(9) .
Au5 Au9 3.1693(9) .
Au5 Au8 3.3169(9) .
Au6 C9A 2.248(14) .
Au6 C9B 2.377(15) .
Au6 Pt1 2.7716(8) .
Au6 Au12 3.3536(10) 4_657
Au6 Au9 3.3683(9) .
Au7 C1A 1.908(17) .
Au7 C2B 2.226(17) .
Au7 C2A 2.233(15) .
Au7 Au9 3.3792(9) .
Au8 C4A 1.987(19) .
Au8 C5A 2.008(17) .
Au8 Au12 3.3564(9) .
Au9 C2A 1.996(18) .
Au9 C3A 2.000(14) .
Au10 C6A 2.008(15) .
Au10 C8A 2.025(14) 4_657
Au11 C7A 2.009(16) .
Au11 C8B 2.168(16) .
Au11 C8A 2.251(15) .
Au12 C9A 1.945(17) 4_657
Au12 C5A 2.243(14) .
Au12 C5B 2.245(15) .
P1 C10S 1.784(8) .
P1 C10M 1.787(8) .
P1 C10A 1.792(8) .
P1 C10G 1.811(7) .
C1A C1B 1.26(2) .
C1B C1C 1.504(16) .
C1C C1D 1.3900 .
C1C C1H 1.3900 .
C1D C1E 1.3900 .
C1E C1F 1.3900 .
C1E C1I 1.492(17) .
C1F C1G 1.3900 .
C1G C1H 1.3900 .
C1G C1J 1.490(17) .
C1I F1C 1.315(19) .
C1I F1A 1.328(19) .
C1I F1B 1.360(19) .
C1J F1F 1.33(2) .
C1J F1E 1.344(18) .
C1J F1D 1.36(2) .
C2A C2B 1.25(2) .
C2B C2C 1.433(18) .
C2C C2D 1.3900 .
C2C C2H 1.3900 .
C2D C2E 1.3900 .
C2E C2F 1.3900 .
C2E C2I 1.57(3) .
C2F C2G 1.3900 .
C2G C2H 1.3900 .
C2G C2J 1.55(3) .
C2I F2C 1.25(3) .
C2I F2B 1.34(3) .
C2I F2A 1.34(2) .
C2J F2D 1.24(3) .
C2J F2E 1.33(4) .
C2J F2F 1.34(3) .
C3A C3B 1.193(19) .
C3B C3C 1.505(16) .
C3C C3D 1.3900 .
C3C C3H 1.3900 .
C3D C3E 1.3900 .
C3E C3F 1.3900 .
C3E C3I 1.50(2) .
C3F C3G 1.3900 .
C3G C3H 1.3900 .
C3G C3J 1.50(2) .
C3I F3B 1.27(2) .
C3I F3C 1.30(3) .
C3I F3A 1.34(3) .
C3J F3E 1.22(3) .
C3J F3F 1.24(2) .
C3J F3D 1.50(4) .
C4A C4B 1.24(2) .
C4B C4C 1.438(18) .
C4C C4D 1.3900 .
C4C C4H 1.3900 .
C4D C4E 1.3900 .
C4E C4F 1.3900 .
C4E C4I 1.51(2) .
C4F C4G 1.3900 .
C4G C4H 1.3900 .
C4G C4J 1.489(19) .
C4I F4C 1.26(2) .
C4I F4A 1.30(2) .
C4I F4B 1.38(2) .
C4J F4F 1.344(19) .
C4J F4D 1.34(2) .
C4J F4E 1.36(2) .
C5A C5B 1.24(2) .
C5B C5C 1.44(2) .
C5C C5D 1.373(15) .
C5C C5H 1.398(15) .
C5D C5EA 1.397(17) .
C5D C5EB 1.419(16) .
C5EA C5F 1.380(18) .
C5EA C5IA 1.441(18) .
C5EB C5F 1.429(19) .
C5EB C5IB 1.521(18) .
C5F C5G 1.35(3) .
C5G C5H 1.39(3) .
C5G C5J 1.48(3) .
C5IA F5BA 1.308(18) .
C5IA F5CA 1.312(18) .
C5IA F5AA 1.340(19) .
C5IB F5BB 1.352(19) .
C5IB F5CB 1.356(19) .
C5IB F5AB 1.379(19) .
F5AB F5BB 1.63(4) 3_666
C5J F5E 1.25(3) .
C5J F5D 1.28(3) .
C5J F5F 1.41(3) .
C6A C6B 1.238(19) .
C6B C6C 1.444(14) .
C6C C6D 1.3900 .
C6C C6H 1.3900 .
C6D C6E 1.3900 .
C6E C6F 1.3900 .
C6E C6I 1.492(17) .
C6F C6G 1.3900 .
C6G C6H 1.3900 .
C6G C6J 1.50(2) .
C6I F6B 1.305(17) .
C6I F6A 1.331(19) .
C6I F6C 1.344(19) .
C6J F6D 1.21(2) .
C6J F6E 1.23(2) .
C6J F6F 1.60(3) .
C7A C7B 1.24(2) .
C7B C7C 1.449(18) .
C7C C7D 1.385(15) .
C7C C7H 1.386(15) .
C7D C7E 1.369(19) .
C7E C7F 1.40(2) .
C7E C7I 1.46(2) .
C7F C7GA 1.384(18) .
C7F C7GB 1.406(19) .
C7GA C7H 1.388(16) .
C7GA C7JA 1.475(18) .
C7GB C7H 1.393(16) .
C7GB C7JB 1.494(18) .
C7I F7C 1.329(18) .
C7I F7B 1.340(19) .
C7I F7A 1.351(18) .
C7JA F7FA 1.325(19) .
C7JA F7DA 1.329(19) .
C7JA F7EA 1.330(19) .
C7JB F7DB 1.341(19) .
C7JB F7FB 1.344(19) .
C7JB F7EB 1.354(19) .
C8A C8B 1.206(19) .
C8B C8C 1.484(15) .
C8C C8D 1.3900 .
C8C C8H 1.3900 .
C8D C8E 1.3900 .
C8E C8F 1.3900 .
C8E C8I 1.49(2) .
C8F C8G 1.3900 .
C8G C8H 1.3900 .
C8G C8J 1.51(3) .
C8I F8A 1.19(2) .
C8I F8B 1.24(2) .
C8I F8C 1.52(3) .
C8J F8E 1.24(3) .
C8J F8F 1.25(3) .
C8J F8D 1.39(3) .
C9A C9B 1.23(2) .
C9B C9C 1.475(18) .
C9C C9D 1.3900 .
C9C C9H 1.3900 .
C9D C9E 1.3900 .
C9E C9F 1.3900 .
C9E C9I 1.53(2) .
C9F C9G 1.3900 .
C9G C9H 1.3900 .
C9G C9J 1.49(2) .
C9I F9B 1.28(2) .
C9I F9A 1.32(2) .
C9I F9C 1.33(2) .
C9J F9D 1.30(2) .
C9J F9F 1.33(2) .
C9J F9E 1.35(2) .
C10A C10B 1.3900 .
C10A C10F 1.3900 .
C10B C10C 1.3900 .
C10C C10D 1.3900 .
C10D C10E 1.3900 .
C10E C10F 1.3900 .
C10G C10H 1.3900 .
C10G C10L 1.3900 .
C10H C10I 1.3900 .
C10I C10J 1.3900 .
C10J C10K 1.3900 .
C10K C10L 1.3900 .
C10M C10N 1.3900 .
C10M C10R 1.3900 .
C10N C10O 1.3900 .
C10O C10P 1.3900 .
C10P C10Q 1.3900 .
C10Q C10R 1.3900 .
C10S C10T 1.3900 .
C10S C10X 1.3900 .
C10T C10U 1.3900 .
C10U C10V 1.3900 .
C10V C10W 1.3900 .
C10W C10X 1.3900 .
Cl20 C22 1.64(3) .
Cl21 C22 1.65(3) .
