#------------------------------------------------------------------------------
#$Date: 2019-11-25 16:33:10 +0200 (Mon, 25 Nov 2019) $
#$Revision: 241331 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/13/10/4131019.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4131019
loop_
_publ_author_name
'Hau, Sam C. K.'
'Yeung, Margaret C.-L.'
'Yam, Vivian W.-W.'
'Mak, Thomas C. W.'
_publ_section_title
;
 Assembly of Heterometallic Silver(I)-Copper(I) Alkyl-1,3-diynyl Clusters
 via Inner-Core Expansion.
;
_journal_issue                   41
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              13732
_journal_page_last               13739
_journal_paper_doi               10.1021/jacs.6b08674
_journal_volume                  138
_journal_year                    2016
_chemical_formula_sum            'C178 H160 Ag10 Cu2 F12 P8'
_chemical_formula_weight         3980.60
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                112.706(2)
_cell_angle_beta                 98.107(2)
_cell_angle_gamma                93.650(2)
_cell_formula_units_Z            1
_cell_length_a                   15.5936(18)
_cell_length_b                   16.7877(18)
_cell_length_c                   17.1552(19)
_cell_measurement_reflns_used    9842
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      28.00
_cell_measurement_theta_min      2.41
_cell_volume                     4067.0(8)
_computing_cell_refinement       SAINT(Bruker,2001)
_computing_data_collection       APEX2(Bruker,2003)
_computing_data_reduction        APEX2(Bruker,2003)
_computing_molecular_graphics    DIAMOND
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'Bruker APEX II CCD diffractometer'
_diffrn_measurement_method       'φ and ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0840
_diffrn_reflns_av_sigmaI/netI    0.0855
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            51534
_diffrn_reflns_theta_full        25.25
_diffrn_reflns_theta_max         25.25
_diffrn_reflns_theta_min         1.31
_exptl_absorpt_coefficient_mu    1.574
_exptl_absorpt_correction_T_max  0.7437
_exptl_absorpt_correction_T_min  0.5717
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.625
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1984
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.925
_refine_diff_density_min         -1.749
_refine_diff_density_rms         0.274
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     955
_refine_ls_number_reflns         14360
_refine_ls_number_restraints     109
_refine_ls_restrained_S_all      1.095
_refine_ls_R_factor_all          0.1180
_refine_ls_R_factor_gt           0.1016
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1959P)²+12.3017P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2574
_refine_ls_wR_factor_ref         0.2867
_reflns_number_gt                11395
_reflns_number_total             14360
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja6b08674_si_002.cif
_cod_data_source_block           7
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      'P-1   '
_cod_database_code               4131019
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu 0.30399(6) 0.99126(5) 0.49728(6) 0.0240(2) Uani 1 1 d .
Ag1 Ag 0.34604(6) 1.10488(5) 0.65922(4) 0.0499(3) Uani 1 1 d .
Ag2 Ag 0.34866(6) 0.83257(5) 0.43705(5) 0.0513(3) Uani 1 1 d .
Ag3 Ag 0.24980(4) 1.04766(4) 0.37465(4) 0.0334(2) Uani 1 1 d .
Ag4 Ag 0.44679(7) 1.11728(6) 0.50795(6) 0.0438(3) Uani 0.85 1 d P
Ag4' Ag 0.4921(5) 1.0918(3) 0.4782(3) 0.0457(13) Uani 0.15 1 d P
Ag5 Ag 0.45277(7) 0.95210(6) 0.37194(6) 0.0678(3) Uani 1 1 d .
P1 P 0.35705(15) 1.15010(14) 0.81082(13) 0.0321(5) Uani 1 1 d .
P2 P 0.32457(15) 0.68478(13) 0.42681(14) 0.0323(5) Uani 1 1 d .
P3 P 0.11661(13) 1.07407(13) 0.30468(13) 0.0287(4) Uani 1 1 d .
C1 C 0.3574(5) 0.9494(5) 0.5820(5) 0.0299(17) Uani 1 1 d .
C2 C 0.3742(5) 0.9137(5) 0.6329(5) 0.0301(17) Uani 1 1 d .
C3 C 0.3912(6) 0.8757(5) 0.6889(6) 0.0346(19) Uani 1 1 d .
C4 C 0.4025(7) 0.8432(6) 0.7412(6) 0.046(2) Uani 1 1 d .
C5 C 0.4149(11) 0.8022(8) 0.8018(8) 0.075(4) Uani 1 1 d .
H5A H 0.3564 0.7952 0.8177 0.090 Uiso 1 1 calc R
C6 C 0.4763(10) 0.8621(10) 0.8863(8) 0.079(4) Uani 1 1 d .
H6A H 0.4547 0.9186 0.9097 0.119 Uiso 1 1 calc R
H6B H 0.5353 0.8703 0.8749 0.119 Uiso 1 1 calc R
H6C H 0.4777 0.8352 0.9280 0.119 Uiso 1 1 calc R
C7 C 0.4382(14) 0.7140(12) 0.7628(13) 0.109(6) Uani 1 1 d U
H7A H 0.3953 0.6798 0.7109 0.163 Uiso 1 1 calc R
H7B H 0.4386 0.6863 0.8038 0.163 Uiso 1 1 calc R
H7C H 0.4963 0.7169 0.7478 0.163 Uiso 1 1 calc R
C8 C 0.2506(6) 0.9050(5) 0.3799(5) 0.0319(18) Uani 1 1 d .
C9 C 0.2054(6) 0.8559(5) 0.3127(6) 0.0334(18) Uani 1 1 d .
C10 C 0.1488(7) 0.8059(6) 0.2386(6) 0.045(2) Uani 1 1 d .
C11 C 0.0958(8) 0.7640(7) 0.1757(7) 0.057(3) Uani 1 1 d .
C12 C 0.0289(10) 0.7171(7) 0.0965(8) 0.072(4) Uani 1 1 d .
H12A H 0.0490 0.7301 0.0494 0.086 Uiso 1 1 calc R
C13 C 0.0209(12) 0.6193(10) 0.0690(11) 0.093(5) Uani 1 1 d U
H13A H 0.0781 0.5997 0.0609 0.140 Uiso 1 1 calc R
H13B H -0.0208 0.5909 0.0149 0.140 Uiso 1 1 calc R
H13C H 0.0003 0.6040 0.1135 0.140 Uiso 1 1 calc R
C14 C -0.0584(11) 0.7515(11) 0.1077(12) 0.099(5) Uani 1 1 d U
H14A H -0.0503 0.8148 0.1256 0.148 Uiso 1 1 calc R
H14B H -0.0817 0.7373 0.1516 0.148 Uiso 1 1 calc R
H14C H -0.0996 0.7246 0.0530 0.148 Uiso 1 1 calc R
C15 C 0.2775(6) 1.1155(6) 0.5344(5) 0.0340(19) Uani 1 1 d .
C16 C 0.2393(6) 1.1783(5) 0.5624(5) 0.0312(17) Uani 1 1 d .
C17 C 0.1917(6) 1.2473(6) 0.5937(6) 0.040(2) Uani 1 1 d .
C18 C 0.1478(7) 1.3041(6) 0.6220(6) 0.047(2) Uani 1 1 d .
C19 C 0.0874(8) 1.3685(7) 0.6553(7) 0.065(4) Uani 1 1 d .
H19A H 0.1221 1.4187 0.7059 0.079 Uiso 1 1 calc R
C20 C 0.0516(10) 1.4038(9) 0.5904(10) 0.083(4) Uani 1 1 d .
H20A H 0.1001 1.4287 0.5728 0.125 Uiso 1 1 calc R
H20B H 0.0153 1.4492 0.6163 0.125 Uiso 1 1 calc R
H20C H 0.0161 1.3566 0.5401 0.125 Uiso 1 1 calc R
C21 C 0.0170(13) 1.3310(12) 0.6879(12) 0.102(5) Uani 1 1 d U
H21A H 0.0439 1.3092 0.7296 0.153 Uiso 1 1 calc R
H21B H -0.0202 1.2831 0.6396 0.153 Uiso 1 1 calc R
H21C H -0.0185 1.3764 0.7155 0.153 Uiso 1 1 calc R
C22 C 0.4084(5) 1.0684(6) 0.3665(6) 0.0365(19) Uani 1 1 d .
C23 C 0.3794(5) 1.1026(5) 0.3194(5) 0.0317(18) Uani 1 1 d .
C24 C 0.3533(6) 1.1449(6) 0.2667(6) 0.037(2) Uani 1 1 d .
C25 C 0.3293(6) 1.1823(6) 0.2222(7) 0.044(2) Uani 1 1 d .
C26 C 0.3033(8) 1.2309(7) 0.1706(7) 0.054(3) Uani 1 1 d .
H26A H 0.3451 1.2238 0.1299 0.065 Uiso 1 1 calc R
C27 C 0.2129(8) 1.1952(10) 0.1176(8) 0.069(3) Uani 1 1 d .
H27A H 0.2112 1.1332 0.0818 0.103 Uiso 1 1 calc R
H27B H 0.1987 1.2267 0.0808 0.103 Uiso 1 1 calc R
H27C H 0.1703 1.2025 0.1559 0.103 Uiso 1 1 calc R
C28 C 0.3113(11) 1.3274(8) 0.2278(10) 0.081(4) Uani 1 1 d .
H28A H 0.3709 1.3474 0.2605 0.122 Uiso 1 1 calc R
H28B H 0.2700 1.3366 0.2676 0.122 Uiso 1 1 calc R
H28C H 0.2982 1.3603 0.1921 0.122 Uiso 1 1 calc R
C29 C 0.4878(6) 0.8288(6) 0.3624(6) 0.039(2) Uani 1 1 d .
C30 C 0.5008(7) 0.7575(7) 0.3160(8) 0.054(3) Uani 1 1 d .
C31 C 0.5177(11) 0.6781(9) 0.2657(11) 0.083(4) Uani 1 1 d U
C32 C 0.5428(13) 0.6104(12) 0.2329(13) 0.102(5) Uani 1 1 d U
C33 C 0.5739(16) 0.5191(16) 0.1851(16) 0.133(8) Uani 1 1 d DU
H33A H 0.6021 0.5210 0.1369 0.160 Uiso 1 1 calc R
C34 C 0.4993(15) 0.4568(13) 0.1512(14) 0.120(6) Uani 1 1 d U
H34A H 0.5164 0.3993 0.1206 0.180 Uiso 1 1 calc R
H34B H 0.4589 0.4719 0.1113 0.180 Uiso 1 1 calc R
H34C H 0.4704 0.4557 0.1980 0.180 Uiso 1 1 calc R
C35 C 0.6425(18) 0.5060(19) 0.2513(18) 0.167(10) Uani 1 1 d DU
H35A H 0.6644 0.4501 0.2243 0.251 Uiso 1 1 calc R
H35B H 0.6158 0.5062 0.2998 0.251 Uiso 1 1 calc R
H35C H 0.6911 0.5533 0.2720 0.251 Uiso 1 1 calc R
C36 C 0.4712(7) 1.1688(6) 0.8611(6) 0.041(2) Uani 1 1 d .
C37 C 0.5172(7) 1.0963(7) 0.8419(7) 0.052(3) Uani 1 1 d .
H37A H 0.4867 1.0395 0.8097 0.063 Uiso 1 1 calc R
C38 C 0.6066(8) 1.1067(8) 0.8692(10) 0.085(5) Uani 1 1 d .
H38A H 0.6384 1.0583 0.8508 0.101 Uiso 1 1 calc R
C39 C 0.6473(11) 1.1853(11) 0.9215(12) 0.097(5) Uani 1 1 d U
H39A H 0.7065 1.1905 0.9475 0.116 Uiso 1 1 calc R
C40 C 0.6058(10) 1.2615(10) 0.9398(12) 0.095(5) Uani 1 1 d U
H40A H 0.6375 1.3179 0.9710 0.114 Uiso 1 1 calc R
C41 C 0.5163(8) 1.2496(8) 0.9100(9) 0.073(4) Uani 1 1 d .
H41A H 0.4856 1.2990 0.9240 0.088 Uiso 1 1 calc R
C42 C 0.3068(6) 1.0674(6) 0.8398(6) 0.0349(18) Uani 1 1 d .
C43 C 0.3317(7) 1.0629(7) 0.9190(6) 0.047(2) Uani 1 1 d .
H43A H 0.3760 1.1053 0.9609 0.057 Uiso 1 1 calc R
C44 C 0.2929(9) 0.9977(8) 0.9375(8) 0.063(3) Uani 1 1 d .
H44A H 0.3098 0.9951 0.9918 0.076 Uiso 1 1 calc R
C45 C 0.2275(9) 0.9347(7) 0.8742(10) 0.071(4) Uani 1 1 d .
H45A H 0.2008 0.8891 0.8860 0.085 Uiso 1 1 calc R
C46 C 0.2028(7) 0.9387(7) 0.7981(8) 0.054(3) Uani 1 1 d .
H46A H 0.1588 0.8960 0.7561 0.065 Uiso 1 1 calc R
C47 C 0.2418(6) 1.0060(7) 0.7800(7) 0.048(2) Uani 1 1 d .
H47A H 0.2232 1.0092 0.7262 0.058 Uiso 1 1 calc R
C48 C 0.3141(6) 1.2510(5) 0.8668(6) 0.0355(19) Uani 1 1 d .
C49 C 0.2836(7) 1.2972(6) 0.8193(6) 0.049(2) Uani 1 1 d .
H49A H 0.2852 1.2760 0.7596 0.058 Uiso 1 1 calc R
C50 C 0.2504(8) 1.3759(7) 0.8601(7) 0.057(3) Uani 1 1 d .
H50A H 0.2277 1.4066 0.8271 0.069 Uiso 1 1 calc R
C51 C 0.2505(8) 1.4090(7) 0.9470(7) 0.056(3) Uani 1 1 d .
H51A H 0.2315 1.4640 0.9747 0.067 Uiso 1 1 calc R
C52 C 0.2781(8) 1.3623(7) 0.9929(7) 0.060(3) Uani 1 1 d .
H52A H 0.2744 1.3825 1.0521 0.072 Uiso 1 1 calc R
C53 C 0.3121(7) 1.2840(7) 0.9526(6) 0.049(2) Uani 1 1 d .
H53A H 0.3342 1.2535 0.9859 0.058 Uiso 1 1 calc R
C54 C 0.2623(6) 0.6693(6) 0.5037(6) 0.040(2) Uani 1 1 d .
C55 C 0.2034(7) 0.7261(7) 0.5340(7) 0.055(3) Uani 1 1 d .
H55A H 0.1956 0.7716 0.5148 0.065 Uiso 1 1 calc R
C56 C 0.1551(8) 0.7167(9) 0.5932(8) 0.068(3) Uani 1 1 d .
H56A H 0.1139 0.7555 0.6137 0.082 Uiso 1 1 calc R
C57 C 0.1670(9) 0.6512(11) 0.6219(8) 0.077(4) Uani 1 1 d .
H57A H 0.1337 0.6446 0.6619 0.092 Uiso 1 1 calc R
C58 C 0.2268(10) 0.5960(10) 0.5927(9) 0.076(4) Uani 1 1 d .
H58A H 0.2350 0.5509 0.6125 0.091 Uiso 1 1 calc R
C59 C 0.2760(8) 0.6053(8) 0.5339(8) 0.059(3) Uani 1 1 d .
H59A H 0.3186 0.5676 0.5148 0.070 Uiso 1 1 calc R
C60 C 0.4256(6) 0.6413(5) 0.4440(5) 0.0319(17) Uani 1 1 d .
C61 C 0.4884(6) 0.6918(6) 0.5135(6) 0.041(2) Uani 1 1 d .
H61A H 0.4768 0.7468 0.5517 0.050 Uiso 1 1 calc R
C62 C 0.5684(7) 0.6640(7) 0.5289(7) 0.054(3) Uani 1 1 d .
H62A H 0.6123 0.7005 0.5758 0.064 Uiso 1 1 calc R
C63 C 0.5832(9) 0.5823(9) 0.4748(11) 0.087(5) Uani 1 1 d .
H63A H 0.6383 0.5632 0.4838 0.105 Uiso 1 1 calc R
C64 C 0.5202(10) 0.5295(9) 0.4095(11) 0.093(6) Uani 1 1 d .
H64A H 0.5297 0.4717 0.3763 0.111 Uiso 1 1 calc R
C65 C 0.4421(8) 0.5581(7) 0.3901(8) 0.066(3) Uani 1 1 d .
H65A H 0.4001 0.5221 0.3412 0.080 Uiso 1 1 calc R
C66 C 0.2629(6) 0.6097(5) 0.3221(6) 0.038(2) Uani 1 1 d .
C67 C 0.2023(8) 0.5418(7) 0.3112(7) 0.056(3) Uani 1 1 d .
H67A H 0.1931 0.5292 0.3591 0.067 Uiso 1 1 calc R
C68 C 0.1543(8) 0.4912(6) 0.2297(8) 0.057(3) Uani 1 1 d .
H68A H 0.1106 0.4457 0.2229 0.069 Uiso 1 1 calc R
C69 C 0.1690(8) 0.5059(7) 0.1601(7) 0.057(3) Uani 1 1 d .
H69A H 0.1371 0.4705 0.1045 0.069 Uiso 1 1 calc R
C70 C 0.2311(10) 0.5731(10) 0.1719(8) 0.083(4) Uani 1 1 d .
H70A H 0.2430 0.5832 0.1234 0.100 Uiso 1 1 calc R
C71 C 0.2773(8) 0.6271(8) 0.2535(7) 0.060(3) Uani 1 1 d .
H71A H 0.3180 0.6752 0.2610 0.071 Uiso 1 1 calc R
C72 C 0.1084(6) 1.1851(6) 0.3171(6) 0.0362(19) Uani 1 1 d .
C73 C 0.1666(7) 1.2515(6) 0.3839(6) 0.046(2) Uani 1 1 d .
H73A H 0.2122 1.2362 0.4164 0.055 Uiso 1 1 calc R
C74 C 0.1590(9) 1.3398(7) 0.4038(10) 0.070(4) Uani 1 1 d .
H74A H 0.1981 1.3843 0.4497 0.084 Uiso 1 1 calc R
C75 C 0.0924(11) 1.3601(9) 0.3543(12) 0.085(5) Uani 1 1 d .
H75A H 0.0850 1.4195 0.3683 0.102 Uiso 1 1 calc R
C76 C 0.0361(9) 1.2956(9) 0.2846(10) 0.070(4) Uani 1 1 d .
H76A H -0.0068 1.3119 0.2503 0.084 Uiso 1 1 calc R
C77 C 0.0424(7) 1.2075(8) 0.2649(7) 0.051(3) Uani 1 1 d .
H77A H 0.0039 1.1635 0.2180 0.062 Uiso 1 1 calc R
C78 C 0.0271(5) 1.0485(5) 0.3517(6) 0.0328(18) Uani 1 1 d .
C79 C -0.0078(7) 0.9629(6) 0.3285(6) 0.044(2) Uani 1 1 d .
H79A H 0.0106 0.9177 0.2829 0.052 Uiso 1 1 calc R
C80 C -0.0701(7) 0.9423(7) 0.3717(7) 0.051(2) Uani 1 1 d .
H80A H -0.0949 0.8836 0.3545 0.061 Uiso 1 1 calc R
C81 C -0.0951(7) 1.0072(8) 0.4386(7) 0.052(3) Uani 1 1 d .
H81A H -0.1359 0.9934 0.4692 0.063 Uiso 1 1 calc R
C82 C -0.0614(7) 1.0914(8) 0.4614(7) 0.054(3) Uani 1 1 d .
H82A H -0.0799 1.1358 0.5076 0.065 Uiso 1 1 calc R
C83 C -0.0015(6) 1.1144(7) 0.4196(6) 0.043(2) Uani 1 1 d .
H83A H 0.0203 1.1739 0.4362 0.051 Uiso 1 1 calc R
C84 C 0.0867(6) 1.0059(5) 0.1905(5) 0.0323(18) Uani 1 1 d .
C85 C 0.0019(7) 0.9891(7) 0.1454(6) 0.053(3) Uani 1 1 d .
H85A H -0.0439 1.0135 0.1743 0.063 Uiso 1 1 calc R
C86 C -0.0161(11) 0.9368(10) 0.0583(9) 0.085(5) Uani 1 1 d .
H86A H -0.0740 0.9271 0.0274 0.102 Uiso 1 1 calc R
C87 C 0.0490(10) 0.8986(8) 0.0158(7) 0.064(3) Uani 1 1 d .
H87A H 0.0359 0.8621 -0.0437 0.077 Uiso 1 1 calc R
C88 C 0.1323(9) 0.9137(8) 0.0600(7) 0.061(3) Uani 1 1 d .
H88A H 0.1771 0.8868 0.0311 0.073 Uiso 1 1 calc R
C89 C 0.1522(7) 0.9676(7) 0.1462(6) 0.043(2) Uani 1 1 d .
H89A H 0.2109 0.9788 0.1757 0.052 Uiso 1 1 calc R
P4 P -0.1475(4) 1.3692(3) 0.1261(3) 0.1023(15) Uani 1 1 d U
F1 F -0.1102(9) 1.4148(7) 0.2263(7) 0.121(3) Uani 1 1 d U
F2 F -0.0489(8) 1.3558(8) 0.1155(7) 0.122(3) Uani 1 1 d U
F3 F -0.1778(9) 1.3246(10) 0.0253(8) 0.154(5) Uani 1 1 d U
F4 F -0.1268(12) 1.4610(9) 0.1224(10) 0.166(5) Uani 1 1 d U
F5 F -0.1552(12) 1.2784(10) 0.1341(12) 0.184(6) Uani 1 1 d U
F6 F -0.2388(15) 1.3914(15) 0.1316(15) 0.229(9) Uani 1 1 d U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Cu1 C8 119.0(3) . .
C1 Cu1 C15 120.4(3) . .
C8 Cu1 C15 119.0(3) . .
C1 Cu1 Ag2 63.3(2) . .
C8 Cu1 Ag2 59.0(2) . .
C15 Cu1 Ag2 173.6(2) . .
C1 Cu1 Ag1 62.5(2) . .
C8 Cu1 Ag1 169.7(3) . .
C15 Cu1 Ag1 58.0(2) . .
Ag2 Cu1 Ag1 125.18(4) . .
C1 Cu1 Ag3 172.9(3) . .
C8 Cu1 Ag3 60.7(2) . .
C15 Cu1 Ag3 62.1(2) . .
Ag2 Cu1 Ag3 113.55(4) . .
Ag1 Cu1 Ag3 119.27(4) . .
C1 Cu1 Ag4 100.1(2) . .
C8 Cu1 Ag4 116.3(3) . .
C15 Cu1 Ag4 64.7(2) . .
Ag2 Cu1 Ag4 110.22(5) . .
Ag1 Cu1 Ag4 72.22(4) . .
Ag3 Cu1 Ag4 74.74(3) . .
C15 Ag1 P1 147.1(2) . .
C15 Ag1 C1 92.1(3) . .
P1 Ag1 C1 114.14(19) . .
C15 Ag1 Cu1 47.4(2) . .
P1 Ag1 Cu1 154.18(7) . .
C1 Ag1 Cu1 44.76(18) . .
C15 Ag1 Ag4 55.4(2) . .
P1 Ag1 Ag4 144.26(7) . .
C1 Ag1 Ag4 80.8(2) . .
Cu1 Ag1 Ag4 57.53(3) . .
C8 Ag2 P2 127.1(2) . .
C8 Ag2 C1 89.5(3) . .
P2 Ag2 C1 116.08(19) . .
C8 Ag2 Cu1 46.64(19) . .
P2 Ag2 Cu1 147.22(7) . .
C1 Ag2 Cu1 44.74(17) . .
C8 Ag2 Ag4' 121.9(2) . 2_676
P2 Ag2 Ag4' 110.96(12) . 2_676
C1 Ag2 Ag4' 63.8(3) . 2_676
Cu1 Ag2 Ag4' 85.34(14) . 2_676
C8 Ag2 C29 105.9(3) . .
P2 Ag2 C29 102.0(2) . .
C1 Ag2 C29 116.9(3) . .
Cu1 Ag2 C29 110.62(19) . .
Ag4' Ag2 C29 56.1(3) 2_676 .
C8 Ag2 Ag5 71.0(2) . .
P2 Ag2 Ag5 143.14(6) . .
C1 Ag2 Ag5 93.45(19) . .
Cu1 Ag2 Ag5 69.56(3) . .
Ag4' Ag2 Ag5 61.25(11) 2_676 .
C29 Ag2 Ag5 42.21(19) . .
C8 Ag2 Ag4 126.6(2) . 2_676
P2 Ag2 Ag4 103.93(6) . 2_676
C1 Ag2 Ag4 79.9(2) . 2_676
Cu1 Ag2 Ag4 98.18(4) . 2_676
Ag4' Ag2 Ag4 16.15(15) 2_676 2_676
C29 Ag2 Ag4 41.7(2) . 2_676
Ag5 Ag2 Ag4 57.89(3) . 2_676
P3 Ag3 C8 116.5(2) . .
P3 Ag3 C15 115.9(2) . .
C8 Ag3 C15 89.3(3) . .
P3 Ag3 C22 135.2(2) . .
C8 Ag3 C22 95.8(3) . .
C15 Ag3 C22 93.3(3) . .
P3 Ag3 C23 107.9(2) . .
C8 Ag3 C23 117.1(3) . .
C15 Ag3 C23 109.1(3) . .
C22 Ag3 C23 27.4(3) . .
P3 Ag3 Cu1 139.41(6) . .
C8 Ag3 Cu1 45.57(19) . .
C15 Ag3 Cu1 45.9(2) . .
C22 Ag3 Cu1 85.3(2) . .
C23 Ag3 Cu1 112.46(19) . .
Ag4' Ag4 C29 101.9(4) . 2_676
Ag4' Ag4 C22 67.2(4) . .
C29 Ag4 C22 166.8(3) 2_676 .
Ag4' Ag4 Ag5 46.9(3) . .
C29 Ag4 Ag5 130.2(3) 2_676 .
C22 Ag4 Ag5 47.7(2) . .
Ag4' Ag4 Cu1 114.0(3) . .
C29 Ag4 Cu1 106.2(2) 2_676 .
C22 Ag4 Cu1 85.6(2) . .
Ag5 Ag4 Cu1 69.86(3) . .
Ag4' Ag4 Ag5 76.7(3) . 2_676
C29 Ag4 Ag5 44.4(2) 2_676 2_676
C22 Ag4 Ag5 134.0(2) . 2_676
Ag5 Ag4 Ag5 86.73(4) . 2_676
Cu1 Ag4 Ag5 83.93(4) . 2_676
Ag4' Ag4 Ag2 50.5(3) . 2_676
C29 Ag4 Ag2 56.6(3) 2_676 2_676
C22 Ag4 Ag2 110.4(2) . 2_676
Ag5 Ag4 Ag2 95.54(5) . 2_676
Cu1 Ag4 Ag2 142.66(4) . 2_676
Ag5 Ag4 Ag2 60.44(3) 2_676 2_676
Ag4' Ag4 Ag1 138.9(3) . .
C29 Ag4 Ag1 60.0(2) 2_676 .
C22 Ag4 Ag1 133.1(2) . .
Ag5 Ag4 Ag1 114.19(4) . .
Cu1 Ag4 Ag1 50.25(3) . .
Ag5 Ag4 Ag1 64.78(3) 2_676 .
Ag2 Ag4 Ag1 114.74(3) 2_676 .
Ag4 Ag4' C22 87.3(5) . .
Ag4 Ag4' Ag5 115.6(4) . .
C22 Ag4' Ag5 58.4(3) . .
Ag4 Ag4' C29 56.1(3) . 2_676
C22 Ag4' C29 142.7(5) . 2_676
Ag5 Ag4' C29 140.4(3) . 2_676
Ag4 Ag4' Ag2 113.3(3) . 2_676
C22 Ag4' Ag2 141.8(4) . 2_676
Ag5 Ag4' Ag2 127.5(3) . 2_676
C29 Ag4' Ag2 62.1(2) 2_676 2_676
Ag4 Ag4' Ag5 85.0(3) . 2_676
C22 Ag4' Ag5 149.8(3) . 2_676
Ag5 Ag4' Ag5 99.44(16) . 2_676
C29 Ag4' Ag5 44.7(2) 2_676 2_676
Ag2 Ag4' Ag5 67.14(11) 2_676 2_676
C29 Ag5 C22 173.2(4) . .
C29 Ag5 Ag4' 132.6(3) . .
C22 Ag5 Ag4' 54.3(3) . .
C29 Ag5 Ag4 136.5(3) . .
C22 Ag5 Ag4 49.9(3) . .
Ag4' Ag5 Ag4 17.48(19) . .
C29 Ag5 Ag4' 55.8(3) . 2_676
C22 Ag5 Ag4' 130.3(3) . 2_676
Ag4' Ag5 Ag4' 80.56(16) . 2_676
Ag4 Ag5 Ag4' 80.68(12) . 2_676
C29 Ag5 Ag4 44.2(3) . 2_676
C22 Ag5 Ag4 142.5(3) . 2_676
Ag4' Ag5 Ag4 88.62(13) . 2_676
Ag4 Ag5 Ag4 93.26(4) . 2_676
Ag4' Ag5 Ag4 18.28(15) 2_676 2_676
C29 Ag5 Ag2 57.3(3) . .
C22 Ag5 Ag2 122.7(2) . .
Ag4' Ag5 Ag2 111.23(15) . .
Ag4 Ag5 Ag2 98.81(3) . .
Ag4' Ag5 Ag2 51.61(12) 2_676 .
Ag4 Ag5 Ag2 61.67(3) 2_676 .
C42 P1 C36 105.1(4) . .
C42 P1 C48 107.3(4) . .
C36 P1 C48 104.9(4) . .
C42 P1 Ag1 112.8(3) . .
C36 P1 Ag1 109.6(3) . .
C48 P1 Ag1 116.2(3) . .
C60 P2 C54 104.3(4) . .
C60 P2 C66 106.9(4) . .
C54 P2 C66 103.9(4) . .
C60 P2 Ag2 112.6(3) . .
C54 P2 Ag2 115.6(3) . .
C66 P2 Ag2 112.5(3) . .
C72 P3 C78 103.7(4) . .
C72 P3 C84 107.0(4) . .
C78 P3 C84 105.0(4) . .
C72 P3 Ag3 116.8(3) . .
C78 P3 Ag3 108.5(3) . .
C84 P3 Ag3 114.7(3) . .
C2 C1 Cu1 166.7(7) . .
C2 C1 Ag1 111.1(6) . .
Cu1 C1 Ag1 72.8(2) . .
C2 C1 Ag2 105.2(6) . .
Cu1 C1 Ag2 71.9(3) . .
Ag1 C1 Ag2 143.7(3) . .
C1 C2 C3 178.9(9) . .
C4 C3 C2 176.5(10) . .
C3 C4 C5 178.5(11) . .
C4 C5 C7 112.4(12) . .
C4 C5 C6 111.8(10) . .
C7 C5 C6 114.5(14) . .
C4 C5 H5A 105.8 . .
C7 C5 H5A 105.8 . .
C6 C5 H5A 105.8 . .
C5 C6 H6A 109.5 . .
C5 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C5 C7 H7A 109.5 . .
C5 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C5 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
C9 C8 Cu1 169.3(8) . .
C9 C8 Ag2 112.0(6) . .
Cu1 C8 Ag2 74.4(3) . .
C9 C8 Ag3 104.3(6) . .
Cu1 C8 Ag3 73.8(3) . .
Ag2 C8 Ag3 137.1(4) . .
C8 C9 C10 174.7(10) . .
C11 C10 C9 176.6(13) . .
C10 C11 C12 176.2(12) . .
C11 C12 C13 112.1(11) . .
C11 C12 C14 110.8(13) . .
C13 C12 C14 112.2(13) . .
C11 C12 H12A 107.2 . .
C13 C12 H12A 107.2 . .
C14 C12 H12A 107.2 . .
C12 C13 H13A 109.5 . .
C12 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
C12 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
C12 C14 H14A 109.5 . .
C12 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C12 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C16 C15 Cu1 159.6(7) . .
C16 C15 Ag1 102.5(6) . .
Cu1 C15 Ag1 74.6(3) . .
C16 C15 Ag3 112.4(6) . .
Cu1 C15 Ag3 72.0(3) . .
Ag1 C15 Ag3 145.1(4) . .
C15 C16 C17 177.0(10) . .
C18 C17 C16 176.5(11) . .
C17 C18 C19 175.2(13) . .
C18 C19 C21 110.5(11) . .
C18 C19 C20 111.9(10) . .
C21 C19 C20 113.0(12) . .
C18 C19 H19A 107.0 . .
C21 C19 H19A 107.0 . .
C20 C19 H19A 107.0 . .
C19 C20 H20A 109.5 . .
C19 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C19 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
C19 C21 H21A 109.5 . .
C19 C21 H21B 109.5 . .
H21A C21 H21B 109.5 . .
C19 C21 H21C 109.5 . .
H21A C21 H21C 109.5 . .
H21B C21 H21C 109.5 . .
C23 C22 Ag4' 142.9(8) . .
C23 C22 Ag5 145.1(8) . .
Ag4' C22 Ag5 67.4(3) . .
C23 C22 Ag4 132.5(7) . .
Ag4' C22 Ag4 25.6(2) . .
Ag5 C22 Ag4 82.4(3) . .
C23 C22 Ag3 81.0(6) . .
Ag4' C22 Ag3 114.6(4) . .
Ag5 C22 Ag3 102.6(3) . .
Ag4 C22 Ag3 91.8(3) . .
C22 C23 C24 175.2(9) . .
C22 C23 Ag3 71.6(5) . .
C24 C23 Ag3 112.9(6) . .
C25 C24 C23 178.5(11) . .
C24 C25 C26 177.3(11) . .
C25 C26 C27 111.3(10) . .
C25 C26 C28 109.9(9) . .
C27 C26 C28 112.6(11) . .
C25 C26 H26A 107.6 . .
C27 C26 H26A 107.6 . .
C28 C26 H26A 107.6 . .
C26 C27 H27A 109.5 . .
C26 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C26 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C26 C28 H28A 109.5 . .
C26 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C26 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C30 C29 Ag4 118.7(8) . 2_676
C30 C29 Ag5 146.8(9) . .
Ag4 C29 Ag5 91.4(4) 2_676 .
C30 C29 Ag4' 133.6(8) . 2_676
Ag4 C29 Ag4' 22.00(19) 2_676 2_676
Ag5 C29 Ag4' 79.4(3) . 2_676
C30 C29 Ag2 115.3(7) . .
Ag4 C29 Ag2 81.8(3) 2_676 .
Ag5 C29 Ag2 80.5(3) . .
Ag4' C29 Ag2 61.8(3) 2_676 .
C29 C30 C31 178.2(15) . .
C32 C31 C30 169(2) . .
C31 C32 C33 177(2) . .
C34 C33 C35 116(2) . .
C34 C33 C32 107(2) . .
C35 C33 C32 106(2) . .
C34 C33 H33A 109.0 . .
C35 C33 H33A 109.0 . .
C32 C33 H33A 109.0 . .
C33 C34 H34A 109.5 . .
C33 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
C33 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
C33 C35 H35A 109.5 . .
C33 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
C33 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
C41 C36 C37 118.4(10) . .
C41 C36 P1 123.9(8) . .
C37 C36 P1 117.5(7) . .
C38 C37 C36 120.8(10) . .
C38 C37 H37A 119.6 . .
C36 C37 H37A 119.6 . .
C39 C38 C37 119.0(12) . .
C39 C38 H38A 120.5 . .
C37 C38 H38A 120.5 . .
C38 C39 C40 122.5(15) . .
C38 C39 H39A 118.8 . .
C40 C39 H39A 118.8 . .
C41 C40 C39 116.7(14) . .
C41 C40 H40A 121.6 . .
C39 C40 H40A 121.6 . .
C36 C41 C40 121.9(12) . .
C36 C41 H41A 119.1 . .
C40 C41 H41A 119.1 . .
C47 C42 C43 119.0(9) . .
C47 C42 P1 118.1(7) . .
C43 C42 P1 122.9(7) . .
C44 C43 C42 120.8(10) . .
C44 C43 H43A 119.6 . .
C42 C43 H43A 119.6 . .
C43 C44 C45 118.9(11) . .
C43 C44 H44A 120.5 . .
C45 C44 H44A 120.5 . .
C46 C45 C44 120.7(11) . .
C46 C45 H45A 119.6 . .
C44 C45 H45A 119.6 . .
C45 C46 C47 120.2(11) . .
C45 C46 H46A 119.9 . .
C47 C46 H46A 119.9 . .
C42 C47 C46 120.4(10) . .
C42 C47 H47A 119.8 . .
C46 C47 H47A 119.8 . .
C53 C48 C49 118.7(8) . .
C53 C48 P1 123.7(7) . .
C49 C48 P1 117.7(7) . .
C48 C49 C50 119.6(9) . .
C48 C49 H49A 120.2 . .
C50 C49 H49A 120.2 . .
C51 C50 C49 120.8(9) . .
C51 C50 H50A 119.6 . .
C49 C50 H50A 119.6 . .
C52 C51 C50 119.4(10) . .
C52 C51 H51A 120.3 . .
C50 C51 H51A 120.3 . .
C51 C52 C53 119.9(10) . .
C51 C52 H52A 120.1 . .
C53 C52 H52A 120.1 . .
C48 C53 C52 121.5(9) . .
C48 C53 H53A 119.2 . .
C52 C53 H53A 119.2 . .
C55 C54 C59 120.2(10) . .
C55 C54 P2 118.1(8) . .
C59 C54 P2 121.7(8) . .
C54 C55 C56 119.8(11) . .
C54 C55 H55A 120.1 . .
C56 C55 H55A 120.1 . .
C57 C56 C55 120.2(11) . .
C57 C56 H56A 119.9 . .
C55 C56 H56A 119.9 . .
C58 C57 C56 119.6(11) . .
C58 C57 H57A 120.2 . .
C56 C57 H57A 120.2 . .
C57 C58 C59 120.6(12) . .
C57 C58 H58A 119.7 . .
C59 C58 H58A 119.7 . .
C54 C59 C58 119.6(11) . .
C54 C59 H59A 120.2 . .
C58 C59 H59A 120.2 . .
C61 C60 C65 118.8(9) . .
C61 C60 P2 118.0(6) . .
C65 C60 P2 123.2(7) . .
C60 C61 C62 121.2(9) . .
C60 C61 H61A 119.4 . .
C62 C61 H61A 119.4 . .
C63 C62 C61 118.9(10) . .
C63 C62 H62A 120.6 . .
C61 C62 H62A 120.6 . .
C64 C63 C62 120.8(11) . .
C64 C63 H63A 119.6 . .
C62 C63 H63A 119.6 . .
C63 C64 C65 121.0(11) . .
C63 C64 H64A 119.5 . .
C65 C64 H64A 119.5 . .
C64 C65 C60 119.1(11) . .
C64 C65 H65A 120.4 . .
C60 C65 H65A 120.4 . .
C71 C66 C67 120.3(9) . .
C71 C66 P2 116.0(7) . .
C67 C66 P2 123.6(8) . .
C66 C67 C68 119.8(11) . .
C66 C67 H67A 120.1 . .
C68 C67 H67A 120.1 . .
C69 C68 C67 121.0(10) . .
C69 C68 H68A 119.5 . .
C67 C68 H68A 119.5 . .
C68 C69 C70 118.4(10) . .
C68 C69 H69A 120.8 . .
C70 C69 H69A 120.8 . .
C69 C70 C71 121.6(12) . .
C69 C70 H70A 119.2 . .
C71 C70 H70A 119.2 . .
C66 C71 C70 118.8(11) . .
C66 C71 H71A 120.6 . .
C70 C71 H71A 120.6 . .
C73 C72 C77 119.6(9) . .
C73 C72 P3 117.7(7) . .
C77 C72 P3 122.6(8) . .
C74 C73 C72 121.4(11) . .
C74 C73 H73A 119.3 . .
C72 C73 H73A 119.3 . .
C75 C74 C73 118.0(13) . .
C75 C74 H74A 121.0 . .
C73 C74 H74A 121.0 . .
C74 C75 C76 121.9(11) . .
C74 C75 H75A 119.1 . .
C76 C75 H75A 119.1 . .
C77 C76 C75 120.5(12) . .
C77 C76 H76A 119.8 . .
C75 C76 H76A 119.8 . .
C76 C77 C72 118.5(12) . .
C76 C77 H77A 120.8 . .
C72 C77 H77A 120.8 . .
C79 C78 C83 118.6(8) . .
C79 C78 P3 120.5(7) . .
C83 C78 P3 120.5(7) . .
C78 C79 C80 120.6(9) . .
C78 C79 H79A 119.7 . .
C80 C79 H79A 119.7 . .
C81 C80 C79 119.7(10) . .
C81 C80 H80A 120.1 . .
C79 C80 H80A 120.1 . .
C82 C81 C80 119.9(10) . .
C82 C81 H81A 120.1 . .
C80 C81 H81A 120.1 . .
C81 C82 C83 122.2(10) . .
C81 C82 H82A 118.9 . .
C83 C82 H82A 118.9 . .
C82 C83 C78 119.1(10) . .
C82 C83 H83A 120.5 . .
C78 C83 H83A 120.5 . .
C85 C84 C89 118.4(9) . .
C85 C84 P3 123.1(7) . .
C89 C84 P3 118.5(7) . .
C84 C85 C86 120.0(12) . .
C84 C85 H85A 120.0 . .
C86 C85 H85A 120.0 . .
C87 C86 C85 120.8(13) . .
C87 C86 H86A 119.6 . .
C85 C86 H86A 119.6 . .
C88 C87 C86 119.5(10) . .
C88 C87 H87A 120.2 . .
C86 C87 H87A 120.2 . .
C87 C88 C89 120.7(11) . .
C87 C88 H88A 119.7 . .
C89 C88 H88A 119.7 . .
C88 C89 C84 120.5(10) . .
C88 C89 H89A 119.7 . .
C84 C89 H89A 119.7 . .
F6 P4 F5 101.1(12) . .
F6 P4 F3 87.4(10) . .
F5 P4 F3 92.1(9) . .
F6 P4 F4 85.7(11) . .
F5 P4 F4 172.7(10) . .
F3 P4 F4 91.1(9) . .
F6 P4 F1 96.3(10) . .
F5 P4 F1 88.9(8) . .
F3 P4 F1 175.9(8) . .
F4 P4 F1 87.5(7) . .
F6 P4 F2 172.1(11) . .
F5 P4 F2 86.5(8) . .
F3 P4 F2 90.3(7) . .
F4 P4 F2 86.8(8) . .
F1 P4 F2 85.8(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 C1 1.954(8) .
Cu1 C8 1.992(8) .
Cu1 C15 2.022(9) .
Cu1 Ag2 2.6389(11) .
Cu1 Ag1 2.6500(11) .
Cu1 Ag3 2.6786(11) .
Cu1 Ag4 2.9077(14) .
Ag1 C15 2.330(8) .
Ag1 P1 2.388(2) .
Ag1 C1 2.460(8) .
Ag1 Ag4 3.2821(14) .
Ag2 C8 2.348(8) .
Ag2 P2 2.419(2) .
Ag2 C1 2.480(8) .
Ag2 Ag4' 2.654(6) 2_676
Ag2 C29 2.662(10) .
Ag2 Ag5 3.1203(13) .
Ag2 Ag4 3.1574(14) 2_676
Ag3 P3 2.403(2) .
Ag3 C8 2.432(8) .
Ag3 C15 2.488(8) .
Ag3 C22 2.506(8) .
Ag3 C23 2.609(8) .
Ag4 Ag4' 0.957(8) .
Ag4 C29 2.120(10) 2_676
Ag4 C22 2.215(9) .
Ag4 Ag5 2.8708(15) .
Ag4 Ag5 3.0382(12) 2_676
Ag4 Ag2 3.1573(14) 2_676
Ag4' C22 2.044(10) .
Ag4' Ag5 2.324(5) .
Ag4' C29 2.499(11) 2_676
Ag4' Ag2 2.654(6) 2_676
Ag4' Ag5 2.969(5) 2_676
Ag5 C29 2.125(9) .
Ag5 C22 2.144(8) .
Ag5 Ag4' 2.969(5) 2_676
Ag5 Ag4 3.0382(12) 2_676
P1 C42 1.814(9) .
P1 C36 1.815(10) .
P1 C48 1.819(9) .
P2 C60 1.812(9) .
P2 C54 1.828(10) .
P2 C66 1.831(9) .
P3 C72 1.808(9) .
P3 C78 1.815(9) .
P3 C84 1.818(8) .
C1 C2 1.246(11) .
C2 C3 1.349(12) .
C3 C4 1.218(13) .
C4 C5 1.451(15) .
C5 C7 1.46(2) .
C5 C6 1.546(19) .
C5 H5A 1.0000 .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 C9 1.212(12) .
C9 C10 1.365(13) .
C10 C11 1.196(14) .
C11 C12 1.491(15) .
C12 C13 1.514(18) .
C12 C14 1.52(2) .
C12 H12A 1.0000 .
C13 H13A 0.9800 .
C13 H13B 0.9800 .
C13 H13C 0.9800 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 C16 1.211(12) .
C16 C17 1.385(12) .
C17 C18 1.198(13) .
C18 C19 1.480(13) .
C19 C21 1.51(2) .
C19 C20 1.510(18) .
C19 H19A 1.0000 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 H21A 0.9800 .
C21 H21B 0.9800 .
C21 H21C 0.9800 .
C22 C23 1.215(12) .
C23 C24 1.384(12) .
C24 C25 1.198(13) .
C25 C26 1.454(14) .
C26 C27 1.510(17) .
C26 C28 1.521(16) .
C26 H26A 1.0000 .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 C30 1.204(14) .
C29 Ag4 2.120(10) 2_676
C29 Ag4' 2.499(11) 2_676
C30 C31 1.346(18) .
C31 C32 1.18(2) .
C32 C33 1.58(3) .
C33 C34 1.40(3) .
C33 C35 1.537(10) .
C33 H33A 1.0000 .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
C35 H35A 0.9800 .
C35 H35B 0.9800 .
C35 H35C 0.9800 .
C36 C41 1.369(15) .
C36 C37 1.405(13) .
C37 C38 1.383(16) .
C37 H37A 0.9500 .
C38 C39 1.330(19) .
C38 H38A 0.9500 .
C39 C40 1.42(2) .
C39 H39A 0.9500 .
C40 C41 1.390(19) .
C40 H40A 0.9500 .
C41 H41A 0.9500 .
C42 C47 1.378(14) .
C42 C43 1.392(13) .
C43 C44 1.380(15) .
C43 H43A 0.9500 .
C44 C45 1.41(2) .
C44 H44A 0.9500 .
C45 C46 1.338(19) .
C45 H45A 0.9500 .
C46 C47 1.407(15) .
C46 H46A 0.9500 .
C47 H47A 0.9500 .
C48 C53 1.364(13) .
C48 C49 1.384(13) .
C49 C50 1.406(15) .
C49 H49A 0.9500 .
C50 C51 1.376(16) .
C50 H50A 0.9500 .
C51 C52 1.357(16) .
C51 H51A 0.9500 .
C52 C53 1.406(14) .
C52 H52A 0.9500 .
C53 H53A 0.9500 .
C54 C55 1.373(14) .
C54 C59 1.377(14) .
C55 C56 1.395(17) .
C55 H55A 0.9500 .
C56 C57 1.38(2) .
C56 H56A 0.9500 .
C57 C58 1.364(19) .
C57 H57A 0.9500 .
C58 C59 1.400(16) .
C58 H58A 0.9500 .
C59 H59A 0.9500 .
C60 C61 1.372(13) .
C60 C65 1.410(13) .
C61 C62 1.385(14) .
C61 H61A 0.9500 .
C62 C63 1.383(17) .
C62 H62A 0.9500 .
C63 C64 1.348(19) .
C63 H63A 0.9500 .
C64 C65 1.380(16) .
C64 H64A 0.9500 .
C65 H65A 0.9500 .
C66 C71 1.362(15) .
C66 C67 1.368(15) .
C67 C68 1.395(15) .
C67 H67A 0.9500 .
C68 C69 1.356(17) .
C68 H68A 0.9500 .
C69 C70 1.371(18) .
C69 H69A 0.9500 .
C70 C71 1.397(15) .
C70 H70A 0.9500 .
C71 H71A 0.9500 .
C72 C73 1.405(14) .
C72 C77 1.431(13) .
C73 C74 1.404(15) .
C73 H73A 0.9500 .
C74 C75 1.39(2) .
C74 H74A 0.9500 .
C75 C76 1.40(2) .
C75 H75A 0.9500 .
C76 C77 1.398(16) .
C76 H76A 0.9500 .
C77 H77A 0.9500 .
C78 C79 1.385(13) .
C78 C83 1.412(13) .
C79 C80 1.404(14) .
C79 H79A 0.9500 .
C80 C81 1.367(16) .
C80 H80A 0.9500 .
C81 C82 1.360(16) .
C81 H81A 0.9500 .
C82 C83 1.375(14) .
C82 H82A 0.9500 .
C83 H83A 0.9500 .
C84 C85 1.386(13) .
C84 C89 1.401(13) .
C85 C86 1.387(17) .
C85 H85A 0.9500 .
C86 C87 1.38(2) .
C86 H86A 0.9500 .
C87 C88 1.363(18) .
C87 H87A 0.9500 .
C88 C89 1.380(15) .
C88 H88A 0.9500 .
C89 H89A 0.9500 .
P4 F6 1.50(2) .
P4 F5 1.581(16) .
P4 F3 1.582(14) .
P4 F4 1.583(15) .
P4 F1 1.588(12) .
P4 F2 1.594(13) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Cu1 Ag1 C15 -177.3(4) . .
C8 Cu1 Ag1 C15 -76.2(13) . .
Ag2 Cu1 Ag1 C15 173.4(3) . .
Ag3 Cu1 Ag1 C15 10.6(3) . .
Ag4 Cu1 Ag1 C15 70.8(3) . .
C1 Cu1 Ag1 P1 -41.4(3) . .
C8 Cu1 Ag1 P1 59.7(13) . .
C15 Cu1 Ag1 P1 135.9(3) . .
Ag2 Cu1 Ag1 P1 -50.73(18) . .
Ag3 Cu1 Ag1 P1 146.45(15) . .
Ag4 Cu1 Ag1 P1 -153.32(16) . .
C8 Cu1 Ag1 C1 101.1(13) . .
C15 Cu1 Ag1 C1 177.3(4) . .
Ag2 Cu1 Ag1 C1 -9.4(3) . .
Ag3 Cu1 Ag1 C1 -172.2(3) . .
Ag4 Cu1 Ag1 C1 -112.0(3) . .
C1 Cu1 Ag1 Ag4 112.0(3) . .
C8 Cu1 Ag1 Ag4 -146.9(13) . .
C15 Cu1 Ag1 Ag4 -70.8(3) . .
Ag2 Cu1 Ag1 Ag4 102.59(6) . .
Ag3 Cu1 Ag1 Ag4 -60.23(4) . .
C1 Cu1 Ag2 C8 159.4(4) . .
C15 Cu1 Ag2 C8 -73(2) . .
Ag1 Cu1 Ag2 C8 168.7(3) . .
Ag3 Cu1 Ag2 C8 -27.6(3) . .
Ag4 Cu1 Ag2 C8 -109.2(3) . .
C1 Cu1 Ag2 P2 65.6(3) . .
C8 Cu1 Ag2 P2 -93.9(3) . .
C15 Cu1 Ag2 P2 -167(2) . .
Ag1 Cu1 Ag2 P2 74.86(13) . .
Ag3 Cu1 Ag2 P2 -121.46(12) . .
Ag4 Cu1 Ag2 P2 156.90(11) . .
C8 Cu1 Ag2 C1 -159.4(4) . .
C15 Cu1 Ag2 C1 127(2) . .
Ag1 Cu1 Ag2 C1 9.3(3) . .
Ag3 Cu1 Ag2 C1 173.0(3) . .
Ag4 Cu1 Ag2 C1 91.3(3) . .
C1 Cu1 Ag2 Ag4' -56.9(3) . 2_676
C8 Cu1 Ag2 Ag4' 143.7(3) . 2_676
C15 Cu1 Ag2 Ag4' 70(2) . 2_676
Ag1 Cu1 Ag2 Ag4' -47.57(13) . 2_676
Ag3 Cu1 Ag2 Ag4' 116.11(13) . 2_676
Ag4 Cu1 Ag2 Ag4' 34.47(13) . 2_676
C1 Cu1 Ag2 C29 -107.9(4) . .
C8 Cu1 Ag2 C29 92.7(4) . .
C15 Cu1 Ag2 C29 19(2) . .
Ag1 Cu1 Ag2 C29 -98.6(2) . .
Ag3 Cu1 Ag2 C29 65.1(2) . .
Ag4 Cu1 Ag2 C29 -16.6(2) . .
C1 Cu1 Ag2 Ag5 -117.9(3) . .
C8 Cu1 Ag2 Ag5 82.7(3) . .
C15 Cu1 Ag2 Ag5 9(2) . .
Ag1 Cu1 Ag2 Ag5 -108.58(5) . .
Ag3 Cu1 Ag2 Ag5 55.10(4) . .
Ag4 Cu1 Ag2 Ag5 -26.54(4) . .
C1 Cu1 Ag2 Ag4 -66.7(3) . 2_676
C8 Cu1 Ag2 Ag4 133.9(3) . 2_676
C15 Cu1 Ag2 Ag4 61(2) . 2_676
Ag1 Cu1 Ag2 Ag4 -57.39(6) . 2_676
Ag3 Cu1 Ag2 Ag4 106.29(4) . 2_676
Ag4 Cu1 Ag2 Ag4 24.65(5) . 2_676
C1 Cu1 Ag3 P3 169.0(19) . .
C8 Cu1 Ag3 P3 79.4(3) . .
C15 Cu1 Ag3 P3 -78.6(3) . .
Ag2 Cu1 Ag3 P3 106.54(9) . .
Ag1 Cu1 Ag3 P3 -88.73(10) . .
Ag4 Cu1 Ag3 P3 -147.68(9) . .
C1 Cu1 Ag3 C8 89.6(19) . .
C15 Cu1 Ag3 C8 -158.0(4) . .
Ag2 Cu1 Ag3 C8 27.1(3) . .
Ag1 Cu1 Ag3 C8 -168.2(3) . .
Ag4 Cu1 Ag3 C8 132.9(3) . .
C1 Cu1 Ag3 C15 -112.4(19) . .
C8 Cu1 Ag3 C15 158.0(4) . .
Ag2 Cu1 Ag3 C15 -174.9(3) . .
Ag1 Cu1 Ag3 C15 -10.1(3) . .
Ag4 Cu1 Ag3 C15 -69.1(3) . .
C1 Cu1 Ag3 C22 -13.2(19) . .
C8 Cu1 Ag3 C22 -102.8(4) . .
C15 Cu1 Ag3 C22 99.2(3) . .
Ag2 Cu1 Ag3 C22 -75.7(2) . .
Ag1 Cu1 Ag3 C22 89.1(2) . .
Ag4 Cu1 Ag3 C22 30.1(2) . .
C1 Cu1 Ag3 C23 -17.1(19) . .
C8 Cu1 Ag3 C23 -106.6(3) . .
C15 Cu1 Ag3 C23 95.3(3) . .
Ag2 Cu1 Ag3 C23 -79.5(2) . .
Ag1 Cu1 Ag3 C23 85.2(2) . .
Ag4 Cu1 Ag3 C23 26.3(2) . .
C1 Cu1 Ag4 Ag4' 77.9(4) . .
C8 Cu1 Ag4 Ag4' -51.7(4) . .
C15 Cu1 Ag4 Ag4' -163.1(4) . .
Ag2 Cu1 Ag4 Ag4' 12.8(3) . .
Ag1 Cu1 Ag4 Ag4' 134.6(3) . .
Ag3 Cu1 Ag4 Ag4' -97.1(3) . .
C1 Cu1 Ag4 C29 -33.4(4) . 2_676
C8 Cu1 Ag4 C29 -163.0(4) . 2_676
C15 Cu1 Ag4 C29 85.6(4) . 2_676
Ag2 Cu1 Ag4 C29 -98.5(3) . 2_676
Ag1 Cu1 Ag4 C29 23.3(3) . 2_676
Ag3 Cu1 Ag4 C29 151.5(3) . 2_676
C1 Cu1 Ag4 C22 140.5(3) . .
C8 Cu1 Ag4 C22 10.9(3) . .
C15 Cu1 Ag4 C22 -100.5(3) . .
Ag2 Cu1 Ag4 C22 75.4(2) . .
Ag1 Cu1 Ag4 C22 -162.9(2) . .
Ag3 Cu1 Ag4 C22 -34.6(2) . .
C1 Cu1 Ag4 Ag5 94.1(2) . .
C8 Cu1 Ag4 Ag5 -35.5(3) . .
C15 Cu1 Ag4 Ag5 -146.9(3) . .
Ag2 Cu1 Ag4 Ag5 28.99(4) . .
Ag1 Cu1 Ag4 Ag5 150.77(4) . .
Ag3 Cu1 Ag4 Ag5 -80.94(3) . .
C1 Cu1 Ag4 Ag5 5.4(2) . 2_676
C8 Cu1 Ag4 Ag5 -124.2(3) . 2_676
C15 Cu1 Ag4 Ag5 124.4(3) . 2_676
Ag2 Cu1 Ag4 Ag5 -59.75(4) . 2_676
Ag1 Cu1 Ag4 Ag5 62.03(3) . 2_676
Ag3 Cu1 Ag4 Ag5 -169.68(4) . 2_676
C1 Cu1 Ag4 Ag2 22.2(3) . 2_676
C8 Cu1 Ag4 Ag2 -107.4(3) . 2_676
C15 Cu1 Ag4 Ag2 141.2(3) . 2_676
Ag2 Cu1 Ag4 Ag2 -42.88(9) . 2_676
Ag1 Cu1 Ag4 Ag2 78.89(7) . 2_676
Ag3 Cu1 Ag4 Ag2 -152.82(8) . 2_676
C1 Cu1 Ag4 Ag1 -56.6(2) . .
C8 Cu1 Ag4 Ag1 173.7(3) . .
C15 Cu1 Ag4 Ag1 62.4(3) . .
Ag2 Cu1 Ag4 Ag1 -121.78(5) . .
Ag3 Cu1 Ag4 Ag1 128.29(4) . .
C15 Ag1 Ag4 Ag4' -139.1(5) . .
P1 Ag1 Ag4 Ag4' 78.9(5) . .
C1 Ag1 Ag4 Ag4' -40.1(5) . .
Cu1 Ag1 Ag4 Ag4' -81.5(4) . .
C15 Ag1 Ag4 C29 148.4(4) . 2_676
P1 Ag1 Ag4 C29 6.4(3) . 2_676
C1 Ag1 Ag4 C29 -112.6(3) . 2_676
Cu1 Ag1 Ag4 C29 -154.1(3) . 2_676
C15 Ag1 Ag4 C22 -33.8(4) . .
P1 Ag1 Ag4 C22 -175.8(3) . .
C1 Ag1 Ag4 C22 65.1(4) . .
Cu1 Ag1 Ag4 C22 23.7(3) . .
C15 Ag1 Ag4 Ag5 -87.7(3) . .
P1 Ag1 Ag4 Ag5 130.27(11) . .
C1 Ag1 Ag4 Ag5 11.25(19) . .
Cu1 Ag1 Ag4 Ag5 -30.17(4) . .
C15 Ag1 Ag4 Cu1 -57.6(3) . .
P1 Ag1 Ag4 Cu1 160.44(11) . .
C1 Ag1 Ag4 Cu1 41.42(19) . .
C15 Ag1 Ag4 Ag5 -161.4(3) . 2_676
P1 Ag1 Ag4 Ag5 56.56(11) . 2_676
C1 Ag1 Ag4 Ag5 -62.46(19) . 2_676
Cu1 Ag1 Ag4 Ag5 -103.88(4) . 2_676
C15 Ag1 Ag4 Ag2 163.4(3) . 2_676
P1 Ag1 Ag4 Ag2 21.39(12) . 2_676
C1 Ag1 Ag4 Ag2 -97.63(19) . 2_676
Cu1 Ag1 Ag4 Ag2 -139.05(5) . 2_676
C29 Ag4 Ag4' C22 -172.3(3) 2_676 .
Ag5 Ag4 Ag4' C22 52.8(3) . .
Cu1 Ag4 Ag4' C22 73.8(3) . .
Ag5 Ag4 Ag4' C22 150.8(3) 2_676 .
Ag2 Ag4 Ag4' C22 -146.7(4) 2_676 .
Ag1 Ag4 Ag4' C22 130.1(4) . .
C29 Ag4 Ag4' Ag5 135.0(3) 2_676 .
C22 Ag4 Ag4' Ag5 -52.8(3) . .
Cu1 Ag4 Ag4' Ag5 21.0(4) . .
Ag5 Ag4 Ag4' Ag5 98.1(3) 2_676 .
Ag2 Ag4 Ag4' Ag5 160.5(5) 2_676 .
Ag1 Ag4 Ag4' Ag5 77.4(5) . .
C22 Ag4 Ag4' C29 172.3(3) . 2_676
Ag5 Ag4 Ag4' C29 -135.0(3) . 2_676
Cu1 Ag4 Ag4' C29 -114.0(3) . 2_676
Ag5 Ag4 Ag4' C29 -36.9(3) 2_676 2_676
Ag2 Ag4 Ag4' C29 25.6(4) 2_676 2_676
Ag1 Ag4 Ag4' C29 -57.6(4) . 2_676
C29 Ag4 Ag4' Ag2 -25.6(4) 2_676 2_676
C22 Ag4 Ag4' Ag2 146.7(4) . 2_676
Ag5 Ag4 Ag4' Ag2 -160.5(5) . 2_676
Cu1 Ag4 Ag4' Ag2 -139.52(16) . 2_676
Ag5 Ag4 Ag4' Ag2 -62.4(2) 2_676 2_676
Ag1 Ag4 Ag4' Ag2 -83.2(4) . 2_676
C29 Ag4 Ag4' Ag5 36.9(3) 2_676 2_676
C22 Ag4 Ag4' Ag5 -150.8(3) . 2_676
Ag5 Ag4 Ag4' Ag5 -98.1(3) . 2_676
Cu1 Ag4 Ag4' Ag5 -77.07(16) . 2_676
Ag2 Ag4 Ag4' Ag5 62.4(2) 2_676 2_676
Ag1 Ag4 Ag4' Ag5 -20.7(4) . 2_676
Ag4 Ag4' Ag5 C29 -111.2(5) . .
C22 Ag4' Ag5 C29 179.7(4) . .
C29 Ag4' Ag5 C29 -44.1(9) 2_676 .
Ag2 Ag4' Ag5 C29 46.1(5) 2_676 .
Ag5 Ag4' Ag5 C29 -22.3(5) 2_676 .
Ag4 Ag4' Ag5 C22 69.1(5) . .
C29 Ag4' Ag5 C22 136.1(8) 2_676 .
Ag2 Ag4' Ag5 C22 -133.6(4) 2_676 .
Ag5 Ag4' Ag5 C22 158.0(4) 2_676 .
C22 Ag4' Ag5 Ag4 -69.1(5) . .
C29 Ag4' Ag5 Ag4 67.1(6) 2_676 .
Ag2 Ag4' Ag5 Ag4 157.3(6) 2_676 .
Ag5 Ag4' Ag5 Ag4 88.9(4) 2_676 .
Ag4 Ag4' Ag5 Ag4' -88.9(4) . 2_676
C22 Ag4' Ag5 Ag4' -158.0(4) . 2_676
C29 Ag4' Ag5 Ag4' -21.8(5) 2_676 2_676
Ag2 Ag4' Ag5 Ag4' 68.4(2) 2_676 2_676
Ag5 Ag4' Ag5 Ag4' 0.0 2_676 2_676
Ag4 Ag4' Ag5 Ag4 -105.4(4) . 2_676
C22 Ag4' Ag5 Ag4 -174.5(3) . 2_676
C29 Ag4' Ag5 Ag4 -38.3(6) 2_676 2_676
Ag2 Ag4' Ag5 Ag4 51.9(2) 2_676 2_676
Ag5 Ag4' Ag5 Ag4 -16.49(17) 2_676 2_676
Ag4 Ag4' Ag5 Ag2 -46.7(4) . .
C22 Ag4' Ag5 Ag2 -115.7(3) . .
C29 Ag4' Ag5 Ag2 20.4(7) 2_676 .
Ag2 Ag4' Ag5 Ag2 110.6(2) 2_676 .
Ag5 Ag4' Ag5 Ag2 42.3(2) 2_676 .
Ag4' Ag4 Ag5 C29 85.8(5) . .
C29 Ag4 Ag5 C29 20.8(7) 2_676 .
C22 Ag4 Ag5 C29 -176.6(5) . .
Cu1 Ag4 Ag5 C29 -73.8(4) . .
Ag5 Ag4 Ag5 C29 10.9(4) 2_676 .
Ag2 Ag4 Ag5 C29 70.8(4) 2_676 .
Ag1 Ag4 Ag5 C29 -49.5(4) . .
Ag4' Ag4 Ag5 C22 -97.6(5) . .
C29 Ag4 Ag5 C22 -162.6(4) 2_676 .
Cu1 Ag4 Ag5 C22 102.8(3) . .
Ag5 Ag4 Ag5 C22 -172.5(3) 2_676 .
Ag2 Ag4 Ag5 C22 -112.6(3) 2_676 .
Ag1 Ag4 Ag5 C22 127.1(3) . .
C29 Ag4 Ag5 Ag4' -65.0(5) 2_676 .
C22 Ag4 Ag5 Ag4' 97.6(5) . .
Cu1 Ag4 Ag5 Ag4' -159.6(4) . .
Ag5 Ag4 Ag5 Ag4' -74.9(4) 2_676 .
Ag2 Ag4 Ag5 Ag4' -15.0(4) 2_676 .
Ag1 Ag4 Ag5 Ag4' -135.3(4) . .
Ag4' Ag4 Ag5 Ag4' 88.2(4) . 2_676
C29 Ag4 Ag5 Ag4' 23.2(3) 2_676 2_676
C22 Ag4 Ag5 Ag4' -174.2(3) . 2_676
Cu1 Ag4 Ag5 Ag4' -71.43(14) . 2_676
Ag5 Ag4 Ag5 Ag4' 13.30(13) 2_676 2_676
Ag2 Ag4 Ag5 Ag4' 73.17(14) 2_676 2_676
Ag1 Ag4 Ag5 Ag4' -47.12(14) . 2_676
Ag4' Ag4 Ag5 Ag4 74.9(4) . 2_676
C29 Ag4 Ag5 Ag4 9.9(3) 2_676 2_676
C22 Ag4 Ag5 Ag4 172.5(3) . 2_676
Cu1 Ag4 Ag5 Ag4 -84.73(4) . 2_676
Ag5 Ag4 Ag5 Ag4 0.0 2_676 2_676
Ag2 Ag4 Ag5 Ag4 59.87(3) 2_676 2_676
Ag1 Ag4 Ag5 Ag4 -60.43(4) . 2_676
Ag4' Ag4 Ag5 Ag2 136.7(4) . .
C29 Ag4 Ag5 Ag2 71.7(3) 2_676 .
C22 Ag4 Ag5 Ag2 -125.7(3) . .
Cu1 Ag4 Ag5 Ag2 -22.91(3) . .
Ag5 Ag4 Ag5 Ag2 61.82(3) 2_676 .
Ag2 Ag4 Ag5 Ag2 121.70(3) 2_676 .
Ag1 Ag4 Ag5 Ag2 1.40(5) . .
C8 Ag2 Ag5 C29 -144.3(4) . .
P2 Ag2 Ag5 C29 -17.1(3) . .
C1 Ag2 Ag5 C29 127.5(4) . .
Cu1 Ag2 Ag5 C29 166.0(3) . .
Ag4' Ag2 Ag5 C29 70.0(4) 2_676 .
Ag4 Ag2 Ag5 C29 51.6(3) 2_676 .
C8 Ag2 Ag5 C22 27.6(4) . .
P2 Ag2 Ag5 C22 154.8(3) . .
C1 Ag2 Ag5 C22 -60.7(4) . .
Cu1 Ag2 Ag5 C22 -22.1(3) . .
Ag4' Ag2 Ag5 C22 -118.2(3) 2_676 .
C29 Ag2 Ag5 C22 171.9(4) . .
Ag4 Ag2 Ag5 C22 -136.5(3) 2_676 .
C8 Ag2 Ag5 Ag4' 88.0(3) . .
P2 Ag2 Ag5 Ag4' -144.9(2) . .
C1 Ag2 Ag5 Ag4' -0.3(3) . .
Cu1 Ag2 Ag5 Ag4' 38.22(18) . .
Ag4' Ag2 Ag5 Ag4' -57.8(3) 2_676 .
C29 Ag2 Ag5 Ag4' -127.8(4) . .
Ag4 Ag2 Ag5 Ag4' -76.19(19) 2_676 .
C8 Ag2 Ag5 Ag4 75.2(2) . .
P2 Ag2 Ag5 Ag4 -157.66(10) . .
C1 Ag2 Ag5 Ag4 -13.11(19) . .
Cu1 Ag2 Ag5 Ag4 25.45(4) . .
Ag4' Ag2 Ag5 Ag4 -70.61(19) 2_676 .
C29 Ag2 Ag5 Ag4 -140.6(3) . .
Ag4 Ag2 Ag5 Ag4 -88.96(5) 2_676 .
C8 Ag2 Ag5 Ag4' 145.8(3) . 2_676
P2 Ag2 Ag5 Ag4' -87.0(2) . 2_676
C1 Ag2 Ag5 Ag4' 57.5(3) . 2_676
Cu1 Ag2 Ag5 Ag4' 96.06(18) . 2_676
C29 Ag2 Ag5 Ag4' -70.0(4) . 2_676
Ag4 Ag2 Ag5 Ag4' -18.35(17) 2_676 2_676
C8 Ag2 Ag5 Ag4 164.1(2) . 2_676
P2 Ag2 Ag5 Ag4 -68.69(11) . 2_676
C1 Ag2 Ag5 Ag4 75.85(19) . 2_676
Cu1 Ag2 Ag5 Ag4 114.41(4) . 2_676
Ag4' Ag2 Ag5 Ag4 18.35(17) 2_676 2_676
C29 Ag2 Ag5 Ag4 -51.6(3) . 2_676
C15 Ag1 P1 C42 104.4(5) . .
C1 Ag1 P1 C42 -35.7(4) . .
Cu1 Ag1 P1 C42 -5.0(4) . .
Ag4 Ag1 P1 C42 -144.6(3) . .
C15 Ag1 P1 C36 -138.9(5) . .
C1 Ag1 P1 C36 81.0(4) . .
Cu1 Ag1 P1 C36 111.7(3) . .
Ag4 Ag1 P1 C36 -27.9(3) . .
C15 Ag1 P1 C48 -20.2(5) . .
C1 Ag1 P1 C48 -160.2(4) . .
Cu1 Ag1 P1 C48 -129.6(3) . .
Ag4 Ag1 P1 C48 90.9(4) . .
C8 Ag2 P2 C60 159.0(4) . .
C1 Ag2 P2 C60 -89.9(4) . .
Cu1 Ag2 P2 C60 -135.5(3) . .
Ag4' Ag2 P2 C60 -19.7(3) 2_676 .
C29 Ag2 P2 C60 38.3(4) . .
Ag5 Ag2 P2 C60 49.9(3) . .
Ag4 Ag2 P2 C60 -4.5(3) 2_676 .
C8 Ag2 P2 C54 -81.1(4) . .
C1 Ag2 P2 C54 29.9(4) . .
Cu1 Ag2 P2 C54 -15.7(4) . .
Ag4' Ag2 P2 C54 100.1(4) 2_676 .
C29 Ag2 P2 C54 158.1(4) . .
Ag5 Ag2 P2 C54 169.7(3) . .
Ag4 Ag2 P2 C54 115.3(4) 2_676 .
C8 Ag2 P2 C66 38.1(4) . .
C1 Ag2 P2 C66 149.1(4) . .
Cu1 Ag2 P2 C66 103.6(3) . .
Ag4' Ag2 P2 C66 -140.7(4) 2_676 .
C29 Ag2 P2 C66 -82.7(4) . .
Ag5 Ag2 P2 C66 -71.1(4) . .
Ag4 Ag2 P2 C66 -125.4(3) 2_676 .
C8 Ag3 P3 C72 169.3(4) . .
C15 Ag3 P3 C72 66.1(4) . .
C22 Ag3 P3 C72 -59.3(4) . .
C23 Ag3 P3 C72 -56.5(4) . .
Cu1 Ag3 P3 C72 117.6(3) . .
C8 Ag3 P3 C78 52.6(4) . .
C15 Ag3 P3 C78 -50.5(4) . .
C22 Ag3 P3 C78 -175.9(4) . .
C23 Ag3 P3 C78 -173.2(4) . .
Cu1 Ag3 P3 C78 0.9(3) . .
C8 Ag3 P3 C84 -64.4(4) . .
C15 Ag3 P3 C84 -167.5(4) . .
C22 Ag3 P3 C84 67.0(4) . .
C23 Ag3 P3 C84 69.8(4) . .
Cu1 Ag3 P3 C84 -116.1(3) . .
C8 Cu1 C1 C2 -59(3) . .
C15 Cu1 C1 C2 106(3) . .
Ag2 Cu1 C1 C2 -79(3) . .
Ag1 Cu1 C1 C2 109(3) . .
Ag3 Cu1 C1 C2 -145(2) . .
Ag4 Cu1 C1 C2 173(3) . .
C8 Cu1 C1 Ag1 -168.4(3) . .
C15 Cu1 C1 Ag1 -2.7(4) . .
Ag2 Cu1 C1 Ag1 171.4(3) . .
Ag3 Cu1 C1 Ag1 106.0(19) . .
Ag4 Cu1 C1 Ag1 63.76(16) . .
C8 Cu1 C1 Ag2 20.1(4) . .
C15 Cu1 C1 Ag2 -174.1(3) . .
Ag1 Cu1 C1 Ag2 -171.4(3) . .
Ag3 Cu1 C1 Ag2 -65.5(19) . .
Ag4 Cu1 C1 Ag2 -107.68(12) . .
C15 Ag1 C1 C2 -164.5(7) . .
P1 Ag1 C1 C2 -4.9(7) . .
Cu1 Ag1 C1 C2 -166.5(8) . .
Ag4 Ag1 C1 C2 141.0(6) . .
C15 Ag1 C1 Cu1 2.0(3) . .
P1 Ag1 C1 Cu1 161.61(14) . .
Ag4 Ag1 C1 Cu1 -52.43(19) . .
C15 Ag1 C1 Ag2 15.8(7) . .
P1 Ag1 C1 Ag2 175.4(5) . .
Cu1 Ag1 C1 Ag2 13.8(4) . .
Ag4 Ag1 C1 Ag2 -38.6(6) . .
C8 Ag2 C1 C2 151.7(6) . .
P2 Ag2 C1 C2 19.8(7) . .
Cu1 Ag2 C1 C2 166.5(8) . .
Ag4' Ag2 C1 C2 -82.0(6) 2_676 .
C29 Ag2 C1 C2 -100.7(6) . .
Ag5 Ag2 C1 C2 -137.5(6) . .
Ag4 Ag2 C1 C2 -80.9(6) 2_676 .
C8 Ag2 C1 Cu1 -14.8(3) . .
P2 Ag2 C1 Cu1 -146.71(15) . .
Ag4' Ag2 C1 Cu1 111.6(3) 2_676 .
C29 Ag2 C1 Cu1 92.8(3) . .
Ag5 Ag2 C1 Cu1 56.1(2) . .
Ag4 Ag2 C1 Cu1 112.6(2) 2_676 .
C8 Ag2 C1 Ag1 -28.7(6) . .
P2 Ag2 C1 Ag1 -160.6(5) . .
Cu1 Ag2 C1 Ag1 -13.9(4) . .
Ag4' Ag2 C1 Ag1 97.7(6) 2_676 .
C29 Ag2 C1 Ag1 78.9(7) . .
Ag5 Ag2 C1 Ag1 42.2(6) . .
Ag4 Ag2 C1 Ag1 98.7(6) 2_676 .
Cu1 C1 C2 C3 -59(50) . .
Ag1 C1 C2 C3 46(49) . .
Ag2 C1 C2 C3 -134(49) . .
C1 C2 C3 C4 8(59) . .
C2 C3 C4 C5 99(50) . .
C3 C4 C5 C7 39(49) . .
C3 C4 C5 C6 169(100) . .
C1 Cu1 C8 C9 107(4) . .
C15 Cu1 C8 C9 -59(4) . .
Ag2 Cu1 C8 C9 128(4) . .
Ag1 Cu1 C8 C9 11(5) . .
Ag3 Cu1 C8 C9 -81(4) . .
Ag4 Cu1 C8 C9 -133(4) . .
C1 Cu1 C8 Ag2 -21.0(4) . .
C15 Cu1 C8 Ag2 173.0(3) . .
Ag1 Cu1 C8 Ag2 -116.6(12) . .
Ag3 Cu1 C8 Ag2 150.8(3) . .
Ag4 Cu1 C8 Ag2 98.77(18) . .
C1 Cu1 C8 Ag3 -171.9(3) . .
C15 Cu1 C8 Ag3 22.2(4) . .
Ag2 Cu1 C8 Ag3 -150.8(3) . .
Ag1 Cu1 C8 Ag3 92.5(13) . .
Ag4 Cu1 C8 Ag3 -52.1(2) . .
P2 Ag2 C8 C9 -33.6(8) . .
C1 Ag2 C8 C9 -156.6(7) . .
Cu1 Ag2 C8 C9 -171.0(8) . .
Ag4' Ag2 C8 C9 145.0(6) 2_676 .
C29 Ag2 C8 C9 85.5(7) . .
Ag5 Ag2 C8 C9 109.5(7) . .
Ag4 Ag2 C8 C9 126.3(6) 2_676 .
P2 Ag2 C8 Cu1 137.34(15) . .
C1 Ag2 C8 Cu1 14.3(3) . .
Ag4' Ag2 C8 Cu1 -44.0(4) 2_676 .
C29 Ag2 C8 Cu1 -103.6(3) . .
Ag5 Ag2 C8 Cu1 -79.5(2) . .
Ag4 Ag2 C8 Cu1 -62.7(3) 2_676 .
P2 Ag2 C8 Ag3 -179.3(4) . .
C1 Ag2 C8 Ag3 57.7(5) . .
Cu1 Ag2 C8 Ag3 43.4(4) . .
Ag4' Ag2 C8 Ag3 -0.6(7) 2_676 .
C29 Ag2 C8 Ag3 -60.2(6) . .
Ag5 Ag2 C8 Ag3 -36.1(5) . .
Ag4 Ag2 C8 Ag3 -19.3(6) 2_676 .
P3 Ag3 C8 C9 34.8(7) . .
C15 Ag3 C8 C9 153.6(7) . .
C22 Ag3 C8 C9 -113.2(7) . .
C23 Ag3 C8 C9 -95.2(7) . .
Cu1 Ag3 C8 C9 169.1(8) . .
P3 Ag3 C8 Cu1 -134.37(16) . .
C15 Ag3 C8 Cu1 -15.6(3) . .
C22 Ag3 C8 Cu1 77.7(3) . .
C23 Ag3 C8 Cu1 95.7(3) . .
P3 Ag3 C8 Ag2 -177.9(4) . .
C15 Ag3 C8 Ag2 -59.1(5) . .
C22 Ag3 C8 Ag2 34.1(6) . .
C23 Ag3 C8 Ag2 52.1(6) . .
Cu1 Ag3 C8 Ag2 -43.6(4) . .
Cu1 C8 C9 C10 31(13) . .
Ag2 C8 C9 C10 156(10) . .
Ag3 C8 C9 C10 -48(10) . .
C8 C9 C10 C11 -28(25) . .
C9 C10 C11 C12 73(32) . .
C10 C11 C12 C13 172(22) . .
C10 C11 C12 C14 -62(23) . .
C1 Cu1 C15 C16 -82(2) . .
C8 Cu1 C15 C16 84(2) . .
Ag2 Cu1 C15 C16 153.8(15) . .
Ag1 Cu1 C15 C16 -84(2) . .
Ag3 Cu1 C15 C16 106(2) . .
Ag4 Cu1 C15 C16 -169(2) . .
C1 Cu1 C15 Ag1 2.8(4) . .
C8 Cu1 C15 Ag1 168.5(3) . .
Ag2 Cu1 C15 Ag1 -122(2) . .
Ag3 Cu1 C15 Ag1 -169.6(3) . .
Ag4 Cu1 C15 Ag1 -84.10(19) . .
C1 Cu1 C15 Ag3 172.4(3) . .
C8 Cu1 C15 Ag3 -21.9(4) . .
Ag2 Cu1 C15 Ag3 48(2) . .
Ag1 Cu1 C15 Ag3 169.6(3) . .
Ag4 Cu1 C15 Ag3 85.47(16) . .
P1 Ag1 C15 C16 13.1(9) . .
C1 Ag1 C15 C16 157.2(7) . .
Cu1 Ag1 C15 C16 159.2(8) . .
Ag4 Ag1 C15 C16 -125.4(7) . .
P1 Ag1 C15 Cu1 -146.1(2) . .
C1 Ag1 C15 Cu1 -1.9(3) . .
Ag4 Ag1 C15 Cu1 75.4(2) . .
P1 Ag1 C15 Ag3 -163.6(4) . .
C1 Ag1 C15 Ag3 -19.4(7) . .
Cu1 Ag1 C15 Ag3 -17.5(5) . .
Ag4 Ag1 C15 Ag3 57.9(6) . .
P3 Ag3 C15 C16 -23.9(8) . .
C8 Ag3 C15 C16 -143.2(7) . .
C22 Ag3 C15 C16 121.0(7) . .
C23 Ag3 C15 C16 98.2(7) . .
Cu1 Ag3 C15 C16 -158.7(8) . .
P3 Ag3 C15 Cu1 134.87(16) . .
C8 Ag3 C15 Cu1 15.5(3) . .
C22 Ag3 C15 Cu1 -80.2(3) . .
C23 Ag3 C15 Cu1 -103.1(3) . .
P3 Ag3 C15 Ag1 152.6(6) . .
C8 Ag3 C15 Ag1 33.3(7) . .
C22 Ag3 C15 Ag1 -62.5(7) . .
C23 Ag3 C15 Ag1 -85.3(7) . .
Cu1 Ag3 C15 Ag1 17.8(5) . .
Cu1 C15 C16 C17 -17(19) . .
Ag1 C15 C16 C17 -96(18) . .
Ag3 C15 C16 C17 82(18) . .
C15 C16 C17 C18 25(30) . .
C16 C17 C18 C19 -26(26) . .
C17 C18 C19 C21 27(13) . .
C17 C18 C19 C20 -100(13) . .
Ag4 Ag4' C22 C23 80.2(13) . .
Ag5 Ag4' C22 C23 -157.3(13) . .
C29 Ag4' C22 C23 69.6(15) 2_676 .
Ag2 Ag4' C22 C23 -45.3(16) 2_676 .
Ag5 Ag4' C22 C23 155.3(10) 2_676 .
Ag4 Ag4' C22 Ag5 -122.5(4) . .
C29 Ag4' C22 Ag5 -133.2(6) 2_676 .
Ag2 Ag4' C22 Ag5 112.0(6) 2_676 .
Ag5 Ag4' C22 Ag5 -47.4(8) 2_676 .
Ag5 Ag4' C22 Ag4 122.5(4) . .
C29 Ag4' C22 Ag4 -10.6(5) 2_676 .
Ag2 Ag4' C22 Ag4 -125.5(7) 2_676 .
Ag5 Ag4' C22 Ag4 75.2(8) 2_676 .
Ag4 Ag4' C22 Ag3 -28.5(5) . .
Ag5 Ag4' C22 Ag3 94.0(4) . .
C29 Ag4' C22 Ag3 -39.2(8) 2_676 .
Ag2 Ag4' C22 Ag3 -154.0(5) 2_676 .
Ag5 Ag4' C22 Ag3 46.6(10) 2_676 .
C29 Ag5 C22 C23 -22(4) . .
Ag4' Ag5 C22 C23 156.0(14) . .
Ag4 Ag5 C22 C23 177.5(14) . .
Ag4' Ag5 C22 C23 -175.0(11) 2_676 .
Ag4 Ag5 C22 C23 165.1(10) 2_676 .
Ag2 Ag5 C22 C23 -110.1(12) . .
C29 Ag5 C22 Ag4' -178(3) . .
Ag4 Ag5 C22 Ag4' 21.5(2) . .
Ag4' Ag5 C22 Ag4' 29.0(5) 2_676 .
Ag4 Ag5 C22 Ag4' 9.1(5) 2_676 .
Ag2 Ag5 C22 Ag4' 93.9(3) . .
C29 Ag5 C22 Ag4 160(3) . .
Ag4' Ag5 C22 Ag4 -21.5(2) . .
Ag4' Ag5 C22 Ag4 7.5(4) 2_676 .
Ag4 Ag5 C22 Ag4 -12.4(5) 2_676 .
Ag2 Ag5 C22 Ag4 72.4(3) . .
C29 Ag5 C22 Ag3 70(3) . .
Ag4' Ag5 C22 Ag3 -111.6(4) . .
Ag4 Ag5 C22 Ag3 -90.1(3) . .
Ag4' Ag5 C22 Ag3 -82.6(4) 2_676 .
Ag4 Ag5 C22 Ag3 -102.5(4) 2_676 .
Ag2 Ag5 C22 Ag3 -17.7(4) . .
Ag4' Ag4 C22 C23 -126.3(10) . .
C29 Ag4 C22 C23 -91.3(17) 2_676 .
Ag5 Ag4 C22 C23 -178.1(11) . .
Cu1 Ag4 C22 C23 115.3(9) . .
Ag5 Ag4 C22 C23 -167.6(8) 2_676 .
Ag2 Ag4 C22 C23 -99.5(9) 2_676 .
Ag1 Ag4 C22 C23 97.2(9) . .
C29 Ag4 C22 Ag4' 35.1(15) 2_676 .
Ag5 Ag4 C22 Ag4' -51.7(3) . .
Cu1 Ag4 C22 Ag4' -118.4(3) . .
Ag5 Ag4 C22 Ag4' -41.2(4) 2_676 .
Ag2 Ag4 C22 Ag4' 26.9(3) 2_676 .
Ag1 Ag4 C22 Ag4' -136.5(4) . .
Ag4' Ag4 C22 Ag5 51.7(3) . .
C29 Ag4 C22 Ag5 86.8(15) 2_676 .
Cu1 Ag4 C22 Ag5 -66.7(2) . .
Ag5 Ag4 C22 Ag5 10.5(4) 2_676 .
Ag2 Ag4 C22 Ag5 78.6(2) 2_676 .
Ag1 Ag4 C22 Ag5 -84.7(3) . .
Ag4' Ag4 C22 Ag3 154.2(4) . .
C29 Ag4 C22 Ag3 -170.7(13) 2_676 .
Ag5 Ag4 C22 Ag3 102.5(3) . .
Cu1 Ag4 C22 Ag3 35.82(19) . .
Ag5 Ag4 C22 Ag3 113.0(2) 2_676 .
Ag2 Ag4 C22 Ag3 -178.92(13) 2_676 .
Ag1 Ag4 C22 Ag3 17.8(4) . .
P3 Ag3 C22 C23 5.7(8) . .
C8 Ag3 C22 C23 143.3(6) . .
C15 Ag3 C22 C23 -127.0(6) . .
Cu1 Ag3 C22 C23 -172.2(6) . .
P3 Ag3 C22 Ag4' 150.4(3) . .
C8 Ag3 C22 Ag4' -72.0(4) . .
C15 Ag3 C22 Ag4' 17.7(4) . .
C23 Ag3 C22 Ag4' 144.7(9) . .
Cu1 Ag3 C22 Ag4' -27.6(4) . .
P3 Ag3 C22 Ag5 -138.9(2) . .
C8 Ag3 C22 Ag5 -1.3(4) . .
C15 Ag3 C22 Ag5 88.3(4) . .
C23 Ag3 C22 Ag5 -144.7(8) . .
Cu1 Ag3 C22 Ag5 43.1(3) . .
P3 Ag3 C22 Ag4 138.50(18) . .
C8 Ag3 C22 Ag4 -83.9(3) . .
C15 Ag3 C22 Ag4 5.8(3) . .
C23 Ag3 C22 Ag4 132.8(7) . .
Cu1 Ag3 C22 Ag4 -39.5(2) . .
Ag4' C22 C23 C24 43(12) . .
Ag5 C22 C23 C24 -99(12) . .
Ag4 C22 C23 C24 78(12) . .
Ag3 C22 C23 C24 162(12) . .
Ag4' C22 C23 Ag3 -119.3(12) . .
Ag5 C22 C23 Ag3 99.2(12) . .
Ag4 C22 C23 Ag3 -84.1(8) . .
P3 Ag3 C23 C22 -175.8(6) . .
C8 Ag3 C23 C22 -41.9(7) . .
C15 Ag3 C23 C22 57.5(6) . .
Cu1 Ag3 C23 C22 8.4(6) . .
P3 Ag3 C23 C24 5.8(7) . .
C8 Ag3 C23 C24 139.7(6) . .
C15 Ag3 C23 C24 -120.9(6) . .
C22 Ag3 C23 C24 -178.4(10) . .
Cu1 Ag3 C23 C24 -170.0(6) . .
C22 C23 C24 C25 -126(38) . .
Ag3 C23 C24 C25 35(40) . .
C23 C24 C25 C26 94(48) . .
C24 C25 C26 C27 -163(26) . .
C24 C25 C26 C28 -37(27) . .
C22 Ag5 C29 C30 30(4) . .
Ag4' Ag5 C29 C30 -147.9(14) . .
Ag4 Ag5 C29 C30 -171.9(13) . .
Ag4' Ag5 C29 C30 -174.7(17) 2_676 .
Ag4 Ag5 C29 C30 -156.1(17) 2_676 .
Ag2 Ag5 C29 C30 122.4(16) . .
C22 Ag5 C29 Ag4 -173(3) . 2_676
Ag4' Ag5 C29 Ag4 8.3(6) . 2_676
Ag4 Ag5 C29 Ag4 -15.7(5) . 2_676
Ag4' Ag5 C29 Ag4 -18.57(19) 2_676 2_676
Ag2 Ag5 C29 Ag4 -81.4(3) . 2_676
C22 Ag5 C29 Ag4' -155(3) . 2_676
Ag4' Ag5 C29 Ag4' 26.8(6) . 2_676
Ag4 Ag5 C29 Ag4' 2.8(5) . 2_676
Ag4 Ag5 C29 Ag4' 18.57(19) 2_676 2_676
Ag2 Ag5 C29 Ag4' -62.9(2) . 2_676
C22 Ag5 C29 Ag2 -92(3) . .
Ag4' Ag5 C29 Ag2 89.7(4) . .
Ag4 Ag5 C29 Ag2 65.7(4) . .
Ag4' Ag5 C29 Ag2 62.9(2) 2_676 .
Ag4 Ag5 C29 Ag2 81.4(3) 2_676 .
C8 Ag2 C29 C30 -114.2(9) . .
P2 Ag2 C29 C30 20.4(9) . .
C1 Ag2 C29 C30 148.1(8) . .
Cu1 Ag2 C29 C30 -163.3(8) . .
Ag4' Ag2 C29 C30 127.7(9) 2_676 .
Ag5 Ag2 C29 C30 -149.3(10) . .
Ag4 Ag2 C29 C30 117.9(9) 2_676 .
C8 Ag2 C29 Ag4 127.8(3) . 2_676
P2 Ag2 C29 Ag4 -97.6(2) . 2_676
C1 Ag2 C29 Ag4 30.1(4) . 2_676
Cu1 Ag2 C29 Ag4 78.8(2) . 2_676
Ag4' Ag2 C29 Ag4 9.77(16) 2_676 2_676
Ag5 Ag2 C29 Ag4 92.8(3) . 2_676
C8 Ag2 C29 Ag5 35.0(3) . .
P2 Ag2 C29 Ag5 169.62(19) . .
C1 Ag2 C29 Ag5 -62.7(3) . .
Cu1 Ag2 C29 Ag5 -14.0(3) . .
Ag4' Ag2 C29 Ag5 -83.0(3) 2_676 .
Ag4 Ag2 C29 Ag5 -92.8(3) 2_676 .
C8 Ag2 C29 Ag4' 118.1(3) . 2_676
P2 Ag2 C29 Ag4' -107.35(19) . 2_676
C1 Ag2 C29 Ag4' 20.4(3) . 2_676
Cu1 Ag2 C29 Ag4' 69.0(2) . 2_676
Ag5 Ag2 C29 Ag4' 83.0(3) . 2_676
Ag4 Ag2 C29 Ag4' -9.77(16) 2_676 2_676
Ag4 C29 C30 C31 -22(40) 2_676 .
Ag5 C29 C30 C31 131(39) . .
Ag4' C29 C30 C31 -42(40) 2_676 .
Ag2 C29 C30 C31 -116(39) . .
C29 C30 C31 C32 13(44) . .
C30 C31 C32 C33 -171(40) . .
C31 C32 C33 C34 -59(46) . .
C31 C32 C33 C35 177(100) . .
C42 P1 C36 C41 -130.5(11) . .
C48 P1 C36 C41 -17.6(12) . .
Ag1 P1 C36 C41 108.0(10) . .
C42 P1 C36 C37 55.4(9) . .
C48 P1 C36 C37 168.4(8) . .
Ag1 P1 C36 C37 -66.1(9) . .
C41 C36 C37 C38 -2.3(19) . .
P1 C36 C37 C38 172.1(11) . .
C36 C37 C38 C39 7(2) . .
C37 C38 C39 C40 -10(3) . .
C38 C39 C40 C41 9(3) . .
C37 C36 C41 C40 1(2) . .
P1 C36 C41 C40 -173.2(13) . .
C39 C40 C41 C36 -4(3) . .
C36 P1 C42 C47 -143.8(7) . .
C48 P1 C42 C47 104.9(8) . .
Ag1 P1 C42 C47 -24.4(8) . .
C36 P1 C42 C43 35.4(9) . .
C48 P1 C42 C43 -75.9(8) . .
Ag1 P1 C42 C43 154.8(7) . .
C47 C42 C43 C44 0.7(15) . .
P1 C42 C43 C44 -178.6(9) . .
C42 C43 C44 C45 0.4(17) . .
C43 C44 C45 C46 -0.8(18) . .
C44 C45 C46 C47 0.0(18) . .
C43 C42 C47 C46 -1.5(14) . .
P1 C42 C47 C46 177.8(8) . .
C45 C46 C47 C42 1.2(16) . .
C42 P1 C48 C53 50.0(10) . .
C36 P1 C48 C53 -61.4(10) . .
Ag1 P1 C48 C53 177.3(8) . .
C42 P1 C48 C49 -131.6(8) . .
C36 P1 C48 C49 117.0(8) . .
Ag1 P1 C48 C49 -4.2(9) . .
C53 C48 C49 C50 -1.0(16) . .
P1 C48 C49 C50 -179.5(9) . .
C48 C49 C50 C51 2.2(18) . .
C49 C50 C51 C52 -4(2) . .
C50 C51 C52 C53 5(2) . .
C49 C48 C53 C52 1.6(17) . .
P1 C48 C53 C52 -179.9(9) . .
C51 C52 C53 C48 -3.5(19) . .
C60 P2 C54 C55 151.9(8) . .
C66 P2 C54 C55 -96.2(9) . .
Ag2 P2 C54 C55 27.7(9) . .
C60 P2 C54 C59 -25.3(10) . .
C66 P2 C54 C59 86.7(9) . .
Ag2 P2 C54 C59 -149.5(8) . .
C59 C54 C55 C56 -2.4(17) . .
P2 C54 C55 C56 -179.6(9) . .
C54 C55 C56 C57 0.7(19) . .
C55 C56 C57 C58 0(2) . .
C56 C57 C58 C59 0(2) . .
C55 C54 C59 C58 2.8(18) . .
P2 C54 C59 C58 180.0(11) . .
C57 C58 C59 C54 -2(2) . .
C54 P2 C60 C61 -78.4(8) . .
C66 P2 C60 C61 171.9(7) . .
Ag2 P2 C60 C61 47.7(8) . .
C54 P2 C60 C65 100.8(10) . .
C66 P2 C60 C65 -8.9(11) . .
Ag2 P2 C60 C65 -133.1(9) . .
C65 C60 C61 C62 3.0(15) . .
P2 C60 C61 C62 -177.7(8) . .
C60 C61 C62 C63 -2.7(18) . .
C61 C62 C63 C64 -2(2) . .
C62 C63 C64 C65 6(3) . .
C63 C64 C65 C60 -5(3) . .
C61 C60 C65 C64 0.8(19) . .
P2 C60 C65 C64 -178.4(12) . .
C60 P2 C66 C71 -90.6(9) . .
C54 P2 C66 C71 159.3(9) . .
Ag2 P2 C66 C71 33.5(9) . .
C60 P2 C66 C67 92.4(9) . .
C54 P2 C66 C67 -17.7(10) . .
Ag2 P2 C66 C67 -143.5(8) . .
C71 C66 C67 C68 -1.0(17) . .
P2 C66 C67 C68 175.9(8) . .
C66 C67 C68 C69 2.7(18) . .
C67 C68 C69 C70 -1.4(19) . .
C68 C69 C70 C71 -2(2) . .
C67 C66 C71 C70 -1.8(19) . .
P2 C66 C71 C70 -178.9(11) . .
C69 C70 C71 C66 3(2) . .
C78 P3 C72 C73 101.9(8) . .
C84 P3 C72 C73 -147.5(7) . .
Ag3 P3 C72 C73 -17.4(8) . .
C78 P3 C72 C77 -74.6(8) . .
C84 P3 C72 C77 36.0(9) . .
Ag3 P3 C72 C77 166.1(7) . .
C77 C72 C73 C74 3.3(15) . .
P3 C72 C73 C74 -173.3(8) . .
C72 C73 C74 C75 -0.9(17) . .
C73 C74 C75 C76 -2.3(19) . .
C74 C75 C76 C77 3.2(19) . .
C75 C76 C77 C72 -0.7(16) . .
C73 C72 C77 C76 -2.4(14) . .
P3 C72 C77 C76 174.0(8) . .
C72 P3 C78 C79 156.9(8) . .
C84 P3 C78 C79 44.7(8) . .
Ag3 P3 C78 C79 -78.4(8) . .
C72 P3 C78 C83 -30.4(8) . .
C84 P3 C78 C83 -142.6(7) . .
Ag3 P3 C78 C83 94.3(7) . .
C83 C78 C79 C80 -0.1(14) . .
P3 C78 C79 C80 172.7(8) . .
C78 C79 C80 C81 -1.6(15) . .
C79 C80 C81 C82 2.0(16) . .
C80 C81 C82 C83 -0.7(16) . .
C81 C82 C83 C78 -1.0(15) . .
C79 C78 C83 C82 1.4(14) . .
P3 C78 C83 C82 -171.5(8) . .
C72 P3 C84 C85 -71.4(9) . .
C78 P3 C84 C85 38.4(9) . .
Ag3 P3 C84 C85 157.4(7) . .
C72 P3 C84 C89 109.5(7) . .
C78 P3 C84 C89 -140.8(7) . .
Ag3 P3 C84 C89 -21.8(8) . .
C89 C84 C85 C86 -1.1(16) . .
P3 C84 C85 C86 179.7(10) . .
C84 C85 C86 C87 2(2) . .
C85 C86 C87 C88 -1(2) . .
C86 C87 C88 C89 -0.9(19) . .
C87 C88 C89 C84 1.8(17) . .
C85 C84 C89 C88 -0.8(14) . .
P3 C84 C89 C88 178.5(8) . .
