#------------------------------------------------------------------------------
#$Date: 2019-11-26 01:02:59 +0200 (Tue, 26 Nov 2019) $
#$Revision: 242229 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/13/22/4132208.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4132208
loop_
_publ_author_name
'Zhang, Jun'
'Kosaka, Wataru'
'Sugimoto, Kunihisa'
'Miyasaka, Hitoshi'
_publ_section_title
;
 Magnetic Sponge Behavior via Electronic State Modulations.
;
_journal_issue                   16
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              5644
_journal_page_last               5652
_journal_paper_doi               10.1021/jacs.8b02428
_journal_volume                  140
_journal_year                    2018
_chemical_formula_moiety         'C70 H24 Cl24 N4 O16 Ru4'
_chemical_formula_sum            'C70 H24 Cl24 N4 O16 Ru4'
_chemical_formula_weight         2432.13
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                96.129(4)
_cell_angle_beta                 99.372(6)
_cell_angle_gamma                109.695(7)
_cell_formula_units_Z            1
_cell_length_a                   11.008(4)
_cell_length_b                   13.982(6)
_cell_length_c                   16.198(6)
_cell_measurement_reflns_used    6710
_cell_measurement_temperature    103
_cell_measurement_theta_max      31.33
_cell_measurement_theta_min      1.85
_cell_volume                     2280.6(15)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'CrystalStructure 4.2.5'
_computing_publication_material  'CrystalStructure 4.2.5 (Rigaku, 2017)'
_computing_structure_refinement  'SHELXL Version 2014/7 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXT Version 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      103
_diffrn_detector_area_resol_mean 7.111
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  'Rigaku Saturn724'
_diffrn_measurement_method       ω
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0619
_diffrn_reflns_Laue_measured_fraction_full 0.983
_diffrn_reflns_Laue_measured_fraction_max 0.983
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            15709
_diffrn_reflns_point_group_measured_fraction_full 0.983
_diffrn_reflns_point_group_measured_fraction_max 0.983
_diffrn_reflns_theta_full        24.999
_diffrn_reflns_theta_max         24.999
_diffrn_reflns_theta_min         1.294
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.413
_exptl_absorpt_correction_T_max  0.978
_exptl_absorpt_correction_T_min  0.801
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'REQAB (Rigaku, 1998)'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.771
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1184.00
_exptl_crystal_size_max          0.088
_exptl_crystal_size_mid          0.033
_exptl_crystal_size_min          0.016
_refine_diff_density_max         2.35
_refine_diff_density_min         -1.13
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.078
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     694
_refine_ls_number_reflns         7905
_refine_ls_number_restraints     300
_refine_ls_R_factor_all          0.1018
_refine_ls_R_factor_gt           0.0749
_refine_ls_shift/su_max          0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²)+(0.1199P)²+8.4224P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1966
_refine_ls_wR_factor_ref         0.2307
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5798
_reflns_number_total             7905
_reflns_threshold_expression     F²>2.0σ(F²)
_cod_data_source_file            ja8b02428_si_002.cif
_cod_data_source_block           Ru2-235-Cl3PhCO2-TCNQMe2_comp2-dry
_cod_original_cell_volume        2280.6(16)
_cod_database_code               4132208
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 +X,+Y,+Z
2 -X,-Y,-Z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Ru1 Ru 0.48211(6) 0.92514(5) 0.45595(4) 0.0299(2) Uani 1 1 d . . .
Ru2 Ru 0.50300(6) 0.52336(5) 0.07021(4) 0.0320(2) Uani 1 1 d . . .
Cl1 Cl 0.5065(4) 0.9914(3) 0.18239(18) 0.0783(9) Uani 1 1 d . . .
Cl2 Cl 0.5909(4) 1.1444(4) 0.0584(2) 0.1068(15) Uani 1 1 d . . .
Cl3 Cl 0.7676(4) 1.4660(3) 0.3135(3) 0.1054(15) Uani 1 1 d . . .
Cl4A Cl 0.8201(3) 0.8168(3) 0.5591(2) 0.0484(9) Uani 0.7 1 d . . P
Cl4B Cl 0.9643(11) 1.2494(9) 0.6337(13) 0.119(6) Uani 0.3 1 d . . P
Cl5 Cl 1.1124(3) 0.8595(3) 0.6147(3) 0.0833(11) Uani 1 1 d . . .
Cl6 Cl 1.2231(3) 1.2648(3) 0.6814(3) 0.1086(15) Uani 1 1 d . . .
Cl7A Cl 0.7610(4) 0.8698(3) 0.1494(2) 0.0676(10) Uani 0.8 1 d . U P
Cl7B Cl 0.7156(12) 0.7832(9) -0.1688(7) 0.043(2) Uani 0.2 1 d . U P
Cl8A Cl 0.8936(4) 1.0872(3) 0.1083(2) 0.0647(9) Uani 0.8 1 d . U P
Cl8B Cl 0.8599(12) 1.0201(9) -0.1485(7) 0.046(2) Uani 0.2 1 d . U P
Cl9A Cl 0.7716(3) 0.9341(3) -0.2242(2) 0.0570(8) Uani 0.8 1 d . U P
Cl9B Cl 0.8612(12) 1.0707(8) 0.1807(7) 0.043(2) Uani 0.2 1 d . U P
Cl10 Cl 0.2262(4) 0.7004(4) 0.0978(4) 0.0652(12) Uani 0.6 1 d . U P
Cl11 Cl -0.0435(4) 0.7231(4) 0.0450(4) 0.0708(13) Uani 0.6 1 d . U P
Cl12 Cl -0.1444(5) 0.4800(5) -0.2516(4) 0.0836(15) Uani 0.6 1 d . U P
Cl13 Cl 0.0687(11) 0.2856(11) -0.1453(10) 0.140(3) Uani 0.4 1 d . U P
Cl14 Cl -0.2005(11) 0.2881(12) -0.2289(11) 0.153(4) Uani 0.4 1 d . U P
Cl15 Cl -0.0941(9) 0.6651(9) -0.0913(8) 0.106(3) Uani 0.4 1 d . U P
O1 O 0.5355(6) 1.0054(5) 0.3628(4) 0.0366(13) Uani 1 1 d . . .
O2 O 0.5663(6) 1.1516(4) 0.4483(4) 0.0375(14) Uani 1 1 d . . .
O3 O 0.6732(5) 0.9412(5) 0.4995(4) 0.0347(13) Uani 1 1 d . . .
O4 O 0.7071(5) 1.0873(4) 0.5865(4) 0.0340(13) Uani 1 1 d . . .
O5 O 0.5986(7) 0.6736(5) 0.0617(4) 0.0453(15) Uani 1 1 d . . .
O6 O 0.5927(5) 0.6275(4) -0.0753(4) 0.0345(13) Uani 1 1 d . . .
O7 O 0.3246(6) 0.5395(5) 0.0371(5) 0.0496(17) Uani 1 1 d . . .
O8 O 0.3217(6) 0.4956(6) -0.0992(4) 0.054(2) Uani 1 1 d . . .
N1 N 0.4537(8) 0.7763(6) 0.3814(5) 0.0461(19) Uani 1 1 d . . .
N2 N 0.4939(9) 0.5542(6) 0.2056(5) 0.051(2) Uani 1 1 d . . .
C1 C 0.5642(8) 1.1013(7) 0.3770(6) 0.036(2) Uani 1 1 d . . .
C2 C 0.6007(9) 1.1636(8) 0.3079(6) 0.045(2) Uani 1 1 d . . .
C3 C 0.5788(10) 1.1214(10) 0.2234(7) 0.060(3) Uani 1 1 d . . .
C4 C 0.6174(12) 1.1915(14) 0.1657(8) 0.076(4) Uani 1 1 d . . .
C5 C 0.6750(12) 1.2955(13) 0.1943(10) 0.080(5) Uani 1 1 d . . .
H5 H 0.6995 1.3414 0.1556 0.096 Uiso 1 1 calc R U .
C6 C 0.6967(11) 1.3322(11) 0.2773(11) 0.079(4) Uani 1 1 d . . .
C7 C 0.6592(10) 1.2700(8) 0.3358(8) 0.057(3) Uani 1 1 d . . .
H7 H 0.6727 1.2987 0.3939 0.069 Uiso 1 1 calc R U .
C8 C 0.7458(8) 1.0189(7) 0.5570(6) 0.039(2) Uani 1 1 d . . .
C9 C 0.8861(8) 1.0288(8) 0.5884(5) 0.040(2) Uani 1 1 d . . .
C10 C 0.9249(8) 0.9444(7) 0.5878(6) 0.041(2) Uani 1 1 d . . .
C11 C 1.0598(10) 0.9618(8) 0.6149(6) 0.049(2) Uani 1 1 d . . .
C12 C 1.1493(9) 1.0590(10) 0.6432(6) 0.056(3) Uani 1 1 d . . .
H12 H 1.2400 1.0695 0.6615 0.067 Uiso 1 1 calc R U .
C13 C 1.1098(10) 1.1413(9) 0.6455(7) 0.058(3) Uani 1 1 d . . .
C14 C 0.9769(9) 1.1304(8) 0.6178(7) 0.053(3) Uani 1 1 d . . .
C15 C 0.6238(8) 0.6945(7) -0.0094(5) 0.0355(19) Uani 1 1 d . . .
C16 C 0.6984(9) 0.8039(7) -0.0186(6) 0.0423(15) Uani 1 1 d . U .
C17A C 0.7542(16) 0.8824(12) 0.0459(8) 0.0507(19) Uani 0.8 1 d . U P
C18A C 0.8173(13) 0.9837(11) 0.0264(9) 0.0509(18) Uani 0.8 1 d . U P
C18B C 0.814(5) 0.985(3) 0.083(3) 0.040(3) Uani 0.2 1 d . U P
C19A C 0.8202(16) 0.9992(10) -0.0551(11) 0.048(2) Uani 0.8 1 d . U P
C19B C 0.849(5) 1.033(4) 0.008(3) 0.041(3) Uani 0.2 1 d . U P
C20A C 0.7635(12) 0.9153(9) -0.1210(8) 0.0454(17) Uani 0.8 1 d . U P
C20B C 0.823(7) 0.968(4) -0.061(4) 0.042(3) Uani 0.2 1 d . U P
C21A C 0.6988(12) 0.8150(10) -0.1073(8) 0.0409(18) Uani 0.8 1 d . U P
C21B C 0.740(5) 0.855(4) -0.072(3) 0.042(2) Uani 0.2 1 d . U P
C22A C 0.2744(10) 0.5243(10) -0.0389(9) 0.069(4) Uani 1 1 d . . .
C23A C 0.1549(17) 0.5614(16) -0.0517(13) 0.052(2) Uani 0.6 1 d . U P
C23B C 0.124(4) 0.492(4) -0.084(4) 0.117(4) Uani 0.4 1 d . U P
C24A C 0.1287(17) 0.6356(15) 0.0013(15) 0.059(2) Uani 0.6 1 d . U P
C24B C 0.098(4) 0.580(4) -0.060(4) 0.112(4) Uani 0.4 1 d . U P
C25A C 0.0074(17) 0.6492(14) -0.0210(15) 0.062(2) Uani 0.6 1 d . U P
C25B C -0.037(4) 0.568(4) -0.103(4) 0.113(3) Uani 0.4 1 d . U P
C26A C -0.074(2) 0.5972(18) -0.1009(16) 0.065(2) Uani 0.6 1 d . U P
C26B C -0.131(4) 0.475(4) -0.154(4) 0.124(4) Uani 0.4 1 d . U P
C27A C -0.047(2) 0.5354(19) -0.1505(15) 0.068(2) Uani 0.6 1 d . U P
C27B C -0.083(4) 0.400(4) -0.169(4) 0.135(3) Uani 0.4 1 d . U P
C28A C 0.0691(16) 0.5140(16) -0.1311(13) 0.056(2) Uani 0.6 1 d . U P
C28B C 0.038(4) 0.413(4) -0.143(4) 0.130(3) Uani 0.4 1 d . U P
C29 C 0.4602(8) 0.6952(7) 0.3688(5) 0.0328(18) Uani 1 1 d . . .
C30 C 0.4688(8) 0.5993(6) 0.3563(5) 0.0307(17) Uani 1 1 d . . .
C31 C 0.4804(8) 0.5693(6) 0.2742(5) 0.0336(18) Uani 1 1 d . . .
C32 C 0.4838(7) 0.5452(6) 0.4279(5) 0.0291(17) Uani 1 1 d . . .
C33 C 0.4573(8) 0.4391(6) 0.4176(5) 0.0325(18) Uani 1 1 d . . .
C34 C 0.4016(10) 0.3683(7) 0.3325(6) 0.044(2) Uani 1 1 d . . .
H34A H 0.3943 0.4091 0.2877 0.053 Uiso 1 1 calc R U .
H34B H 0.4604 0.3311 0.3221 0.053 Uiso 1 1 calc R U .
H34C H 0.3140 0.3186 0.3326 0.053 Uiso 1 1 calc R U .
C35 C 0.5241(8) 0.6034(6) 0.5094(5) 0.0321(18) Uani 1 1 d . . .
H35 H 0.5396 0.6752 0.5156 0.038 Uiso 1 1 calc R U .
C17B C 0.751(6) 0.884(4) 0.076(3) 0.039(3) Uani 0.2 1 d . U P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
H H 0.0000 0.0000
;
International Tables for Crystallography
(Vol. C, Table 6.1.1.4)
;
N N 0.0061 0.0033
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
O O 0.0106 0.0060
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
Cl Cl 0.1484 0.1585
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
Ru Ru -1.2594 0.8363
;
International Tables for Crystallography
(Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Ru1 O1 178.2(2) 2_676 .
O2 Ru1 O4 91.9(2) 2_676 2_676
O1 Ru1 O4 89.3(2) . 2_676
O2 Ru1 O3 88.5(2) 2_676 .
O1 Ru1 O3 90.2(2) . .
O4 Ru1 O3 178.7(2) 2_676 .
O2 Ru1 N1 87.1(3) 2_676 .
O1 Ru1 N1 94.1(3) . .
O4 Ru1 N1 93.3(3) 2_676 .
O3 Ru1 N1 88.0(3) . .
O2 Ru1 Ru1 88.54(18) 2_676 2_676
O1 Ru1 Ru1 90.11(18) . 2_676
O4 Ru1 Ru1 89.56(17) 2_676 2_676
O3 Ru1 Ru1 89.18(17) . 2_676
N1 Ru1 Ru1 174.9(2) . 2_676
O8 Ru2 O6 89.9(3) 2_665 2_665
O8 Ru2 O5 90.1(3) 2_665 .
O6 Ru2 O5 178.5(2) 2_665 .
O8 Ru2 O7 178.1(3) 2_665 .
O6 Ru2 O7 89.4(2) 2_665 .
O5 Ru2 O7 90.5(3) . .
O8 Ru2 N2 92.7(3) 2_665 .
O6 Ru2 N2 85.9(3) 2_665 .
O5 Ru2 N2 95.7(3) . .
O7 Ru2 N2 89.0(3) . .
O8 Ru2 Ru2 89.0(2) 2_665 2_665
O6 Ru2 Ru2 88.95(16) 2_665 2_665
O5 Ru2 Ru2 89.51(18) . 2_665
O7 Ru2 Ru2 89.3(2) . 2_665
N2 Ru2 Ru2 174.6(2) . 2_665
C17B Cl7A C17A 5(3) . .
C17B Cl7A C18B 40(3) . .
C17A Cl7A C18B 42.8(15) . .
C21A Cl7B C21B 17.8(18) . .
C21A Cl7B C20A 51.7(9) . .
C21B Cl7B C20A 40.7(16) . .
C21A Cl7B Cl9A 97.6(9) . .
C21B Cl7B Cl9A 88.6(16) . .
C20A Cl7B Cl9A 47.9(5) . .
Cl9B Cl8A C18B 82(2) . .
Cl9B Cl8A C19B 139.9(19) . .
C18B Cl8A C19B 59(2) . .
Cl9B Cl8A C18A 114.5(8) . .
C18B Cl8A C18A 32.2(19) . .
C19B Cl8A C18A 26.5(16) . .
Cl9A Cl8B C20A 65.4(6) . .
Cl9A Cl8B C19A 113.8(8) . .
C20A Cl8B C19A 49.5(7) . .
Cl9A Cl8B C20B 104(2) . .
C20A Cl8B C20B 39(2) . .
C19A Cl8B C20B 15(2) . .
Cl8B Cl9A C20A 60.0(6) . .
Cl8B Cl9A Cl7B 105.4(5) . .
C20A Cl9A Cl7B 50.0(5) . .
Cl8A Cl9B C18B 50.5(15) . .
C24A Cl10 Cl14 135.5(7) . 2_565
C25A Cl11 Cl13 130.5(9) . 2_565
C25A Cl11 Cl15 45.0(7) . .
Cl13 Cl11 Cl15 151.9(6) 2_565 .
C26B Cl12 C27A 35.1(18) . .
C26B Cl12 C27B 42(2) . .
C27A Cl12 C27B 56.3(16) . .
Cl11 Cl13 C28B 92.4(18) 2_565 .
C27B Cl14 Cl10 71(2) . 2_565
C26A Cl15 C25A 62.3(16) . .
C26A Cl15 C25B 9(2) . .
C25A Cl15 C25B 57(2) . .
C26A Cl15 Cl11 107.8(16) . .
C25A Cl15 Cl11 50.7(9) . .
C25B Cl15 Cl11 105(2) . .
C26A Cl15 C27A 17.9(15) . .
C25A Cl15 C27A 75.0(11) . .
C25B Cl15 C27A 19(2) . .
Cl11 Cl15 C27A 123.9(7) . .
C1 O1 Ru1 118.3(6) . .
C1 O2 Ru1 119.4(5) . 2_676
C8 O3 Ru1 118.4(5) . .
C8 O4 Ru1 119.1(6) . 2_676
C15 O5 Ru2 118.4(6) . .
C15 O6 Ru2 119.6(5) . 2_665
C22A O7 Ru2 117.8(7) . .
C22A O8 Ru2 118.4(6) . 2_665
C29 N1 Ru1 156.6(7) . .
C31 N2 Ru2 175.4(8) . .
O1 C1 O2 123.6(8) . .
O1 C1 C2 119.8(9) . .
O2 C1 C2 116.6(8) . .
C3 C2 C7 121.2(9) . .
C3 C2 C1 124.2(10) . .
C7 C2 C1 114.6(9) . .
C2 C3 C4 117.1(12) . .
C2 C3 Cl1 124.8(8) . .
C4 C3 Cl1 118.1(11) . .
C5 C4 C3 120.9(13) . .
C5 C4 Cl2 119.2(10) . .
C3 C4 Cl2 119.8(13) . .
C6 C5 C4 119.5(11) . .
C6 C5 H5 120.3 . .
C4 C5 H5 120.3 . .
C5 C6 C7 122.8(14) . .
C5 C6 Cl3 119.4(10) . .
C7 C6 Cl3 117.7(13) . .
C6 C7 C2 118.4(13) . .
C6 C7 H7 120.8 . .
C2 C7 H7 120.8 . .
O4 C8 O3 123.8(8) . .
O4 C8 C9 118.8(8) . .
O3 C8 C9 117.4(8) . .
C10 C9 C14 121.9(8) . .
C10 C9 C8 122.5(9) . .
C14 C9 C8 115.6(9) . .
C9 C10 C11 118.4(9) . .
C9 C10 Cl4A 125.4(7) . .
C11 C10 Cl4A 116.2(7) . .
C12 C11 C10 120.8(10) . .
C12 C11 Cl5 119.2(8) . .
C10 C11 Cl5 120.0(8) . .
C11 C12 C13 120.4(9) . .
C11 C12 H12 119.8 . .
C13 C12 H12 119.8 . .
C12 C13 C14 122.2(10) . .
C12 C13 Cl6 120.5(9) . .
C14 C13 Cl6 117.3(9) . .
C13 C14 C9 116.3(10) . .
C13 C14 Cl4B 108.9(8) . .
C9 C14 Cl4B 134.7(9) . .
O6 C15 O5 123.5(8) . .
O6 C15 C16 115.8(8) . .
O5 C15 C16 120.7(8) . .
C21B C16 C17A 94(3) . .
C21B C16 C21A 30(2) . .
C17A C16 C21A 123.4(10) . .
C21B C16 C15 141(3) . .
C17A C16 C15 124.2(10) . .
C21A C16 C15 112.3(9) . .
C21B C16 C17B 107(3) . .
C17A C16 C17B 13(2) . .
C21A C16 C17B 136.3(19) . .
C15 C16 C17B 111.2(19) . .
C16 C17A C18B 155(2) . .
C16 C17A C18A 117.6(12) . .
C18B C17A C18A 37.9(19) . .
C16 C17A Cl7A 123.9(11) . .
C18B C17A Cl7A 81(2) . .
C18A C17A Cl7A 118.4(11) . .
C16 C17A C21B 40.7(16) . .
C18B C17A C21B 115(3) . .
C18A C17A C21B 77.2(17) . .
Cl7A C17A C21B 163.1(18) . .
C19B C18A C18B 123(5) . .
C19B C18A C19A 48(4) . .
C18B C18A C19A 169(3) . .
C19B C18A C20B 64(4) . .
C18B C18A C20B 173(4) . .
C19A C18A C20B 18(2) . .
C19B C18A C17A 170(4) . .
C18B C18A C17A 67(3) . .
C19A C18A C17A 121.8(13) . .
C20B C18A C17A 106(2) . .
C19B C18A C17B 174(5) . .
C18B C18A C17B 52(3) . .
C19A C18A C17B 137(2) . .
C20B C18A C17B 122(3) . .
C17A C18A C17B 15.7(19) . .
C19B C18A Cl8A 71(4) . .
C18B C18A Cl8A 52(3) . .
C19A C18A Cl8A 119.0(12) . .
C20B C18A Cl8A 133(3) . .
C17A C18A Cl8A 119.2(11) . .
C17B C18A Cl8A 104(2) . .
C18A C18B C17B 96(4) . .
C18A C18B Cl8A 95(4) . .
C17B C18B Cl8A 166(5) . .
C18A C18B C17A 75(3) . .
C17B C18B C17A 21(2) . .
Cl8A C18B C17A 167(4) . .
C18A C18B C19B 26(3) . .
C17B C18B C19B 122(5) . .
Cl8A C18B C19B 70(3) . .
C17A C18B C19B 101(4) . .
C18A C18B Cl9B 142(4) . .
C17B C18B Cl9B 122(4) . .
Cl8A C18B Cl9B 47.1(15) . .
C17A C18B Cl9B 143(3) . .
C19B C18B Cl9B 116(3) . .
C18A C18B Cl7A 130(4) . .
C17B C18B Cl7A 36(2) . .
Cl8A C18B Cl7A 131(3) . .
C17A C18B Cl7A 56.3(16) . .
C19B C18B Cl7A 156(4) . .
Cl9B C18B Cl7A 87(2) . .
C19B C19A C18A 34(3) . .
C19B C19A C20A 153(3) . .
C18A C19A C20A 119.2(13) . .
C19B C19A Cl8B 140(3) . .
C18A C19A Cl8B 166.7(14) . .
C20A C19A Cl8B 64.4(9) . .
C19B C19A C21B 113(3) . .
C18A C19A C21B 78.9(18) . .
C20A C19A C21B 40.4(16) . .
Cl8B C19A C21B 102.9(18) . .
C18A C19B C19A 97(5) . .
C18A C19B C20B 84(5) . .
C19A C19B C20B 18(3) . .
C18A C19B C18B 31(3) . .
C19A C19B C18B 128(5) . .
C20B C19B C18B 115(5) . .
C18A C19B Cl8A 83(4) . .
C19A C19B Cl8A 179(5) . .
C20B C19B Cl8A 163(5) . .
C18B C19B Cl8A 52(2) . .
C20B C20A C21B 81(4) . .
C20B C20A C19A 16(3) . .
C21B C20A C19A 92(3) . .
C20B C20A C21A 112(3) . .
C21B C20A C21A 31(2) . .
C19A C20A C21A 122.4(13) . .
C20B C20A Cl8B 73(3) . .
C21B C20A Cl8B 151(3) . .
C19A C20A Cl8B 66.1(9) . .
C21A C20A Cl8B 166.5(12) . .
C20B C20A Cl9A 128(3) . .
C21B C20A Cl9A 148(3) . .
C19A C20A Cl9A 119.3(10) . .
C21A C20A Cl9A 118.3(10) . .
Cl8B C20A Cl9A 54.5(6) . .
C20B C20A Cl7B 140(3) . .
C21B C20A Cl7B 66(3) . .
C19A C20A Cl7B 154.9(11) . .
C21A C20A Cl7B 38.6(7) . .
Cl8B C20A Cl7B 129.5(9) . .
Cl9A C20A Cl7B 82.2(7) . .
C20A C20B C19B 158(7) . .
C20A C20B C18A 138(5) . .
C19B C20B C18A 33(3) . .
C20A C20B C21B 53(3) . .
C19B C20B C21B 123(5) . .
C18A C20B C21B 91(4) . .
C20A C20B Cl8B 68(3) . .
C19B C20B Cl8B 116(4) . .
C18A C20B Cl8B 149(4) . .
C21B C20B Cl8B 120(4) . .
C21B C21A Cl7B 134(5) . .
C21B C21A C20A 60(4) . .
Cl7B C21A C20A 89.6(11) . .
C21B C21A C16 57(4) . .
Cl7B C21A C16 145.6(12) . .
C20A C21A C16 115.6(12) . .
C21A C21B C20A 89(5) . .
C21A C21B C16 94(5) . .
C20A C21B C16 167(5) . .
C21A C21B C20B 135(6) . .
C20A C21B C20B 46(3) . .
C16 C21B C20B 130(5) . .
C21A C21B Cl7B 28(3) . .
C20A C21B Cl7B 73(3) . .
C16 C21B Cl7B 114(4) . .
C20B C21B Cl7B 116(4) . .
C21A C21B C17A 138(5) . .
C20A C21B C17A 129(4) . .
C16 C21B C17A 45.1(19) . .
C20B C21B C17A 85(4) . .
Cl7B C21B C17A 157(3) . .
C21A C21B C19A 135(5) . .
C20A C21B C19A 48(2) . .
C16 C21B C19A 126(4) . .
C20B C21B C19A 9(3) . .
Cl7B C21B C19A 120(3) . .
C17A C21B C19A 82(2) . .
O7 C22A O8 125.5(9) . .
O7 C22A C23A 109.9(13) . .
O8 C22A C23A 124.0(12) . .
O7 C22A C23B 129(2) . .
O8 C22A C23B 101(2) . .
C23A C22A C23B 35.9(18) . .
C24B C23A C23B 107(6) . .
C24B C23A C28A 67(5) . .
C23B C23A C28A 47(3) . .
C24B C23A C24A 52(5) . .
C23B C23A C24A 148(3) . .
C28A C23A C24A 119.5(17) . .
C24B C23A C22A 177(5) . .
C23B C23A C22A 73(3) . .
C28A C23A C22A 111.0(18) . .
C24A C23A C22A 129.5(18) . .
C23A C23B C28A 89(5) . .
C23A C23B C28B 153(5) . .
C28A C23B C28B 66(4) . .
C23A C23B C24B 32(3) . .
C28A C23B C24B 64(3) . .
C28B C23B C24B 122(4) . .
C23A C23B C22A 71(3) . .
C28A C23B C22A 138(5) . .
C28B C23B C22A 135(4) . .
C24B C23B C22A 102(4) . .
C24B C24A C25A 86(3) . .
C24B C24A C23A 32(2) . .
C25A C24A C23A 119(2) . .
C24B C24A Cl10 157(3) . .
C25A C24A Cl10 116.7(17) . .
C23A C24A Cl10 124.2(14) . .
C23A C24B C24A 96(6) . .
C23A C24B C28A 80(5) . .
C24A C24B C28A 176(4) . .
C23A C24B C23B 42(4) . .
C24A C24B C23B 132(5) . .
C28A C24B C23B 45(3) . .
C23A C24B C25B 152(7) . .
C24A C24B C25B 110(4) . .
C28A C24B C25B 74(4) . .
C23B C24B C25B 110(5) . .
C23A C24B C25A 149(7) . .
C24A C24B C25A 54(2) . .
C28A C24B C25A 130(3) . .
C23B C24B C25A 155(4) . .
C25B C24B C25A 57(3) . .
C23A C24B C27A 129(6) . .
C24A C24B C27A 135(4) . .
C28A C24B C27A 49(2) . .
C23B C24B C27A 89(4) . .
C25B C24B C27A 25(2) . .
C25A C24B C27A 82(2) . .
C23A C24B C26A 166(6) . .
C24A C24B C26A 97(3) . .
C28A C24B C26A 87(3) . .
C23B C24B C26A 124(4) . .
C25B C24B C26A 14(3) . .
C25A C24B C26A 43.6(14) . .
C27A C24B C26A 38.0(14) . .
C24A C25A C26A 118(2) . .
C24A C25A C25B 93(2) . .
C26A C25A C25B 25.8(16) . .
C24A C25A Cl15 147.4(19) . .
C26A C25A Cl15 41.0(11) . .
C25B C25A Cl15 66(2) . .
C24A C25A Cl11 122.4(18) . .
C26A C25A Cl11 119.9(15) . .
C25B C25A Cl11 144(2) . .
Cl15 C25A Cl11 84.4(10) . .
C24A C25A C24B 39.8(18) . .
C26A C25A C24B 78(2) . .
C25B C25A C24B 53(2) . .
Cl15 C25A C24B 113(2) . .
Cl11 C25A C24B 162(2) . .
C26A C25B C27A 115(8) . .
C26A C25B C26B 101(6) . .
C27A C25B C26B 44(4) . .
C26A C25B C24B 133(8) . .
C27A C25B C24B 104(5) . .
C26B C25B C24B 125(5) . .
C26A C25B C25A 66(6) . .
C27A C25B C25A 166(6) . .
C26B C25B C25A 150(5) . .
C24B C25B C25A 70(3) . .
C26A C25B C28A 163(8) . .
C27A C25B C28A 56(4) . .
C26B C25B C28A 82(4) . .
C24B C25B C28A 49(3) . .
C25A C25B C28A 119(3) . .
C26A C25B Cl15 14(4) . .
C27A C25B Cl15 120(6) . .
C26B C25B Cl15 114(3) . .
C24B C25B Cl15 121(4) . .
C25A C25B Cl15 57(2) . .
C28A C25B Cl15 154(4) . .
C25B C26A Cl15 157(6) . .
C25B C26A C27A 36(6) . .
Cl15 C26A C27A 147(2) . .
C25B C26A C25A 89(6) . .
Cl15 C26A C25A 76.7(19) . .
C27A C26A C25A 123(2) . .
C25B C26A C26B 56(5) . .
Cl15 C26A C26B 145(3) . .
C27A C26A C26B 36.5(18) . .
C25A C26A C26B 135(2) . .
C25B C26A C24B 33(6) . .
Cl15 C26A C24B 127(2) . .
C27A C26A C24B 65(2) . .
C25A C26A C24B 58.4(19) . .
C26B C26A C24B 88(2) . .
C27A C26B C27B 98(4) . .
C27A C26B C25B 34(3) . .
C27B C26B C25B 114(4) . .
C27A C26B Cl12 82(4) . .
C27B C26B Cl12 87(4) . .
C25B C26B Cl12 112(5) . .
C27A C26B C26A 48(3) . .
C27B C26B C26A 137(4) . .
C25B C26B C26A 22.9(19) . .
Cl12 C26B C26A 107(3) . .
C27A C26B C28A 39(2) . .
C27B C26B C28A 62(3) . .
C25B C26B C28A 55(3) . .
Cl12 C26B C28A 94(2) . .
C26A C26B C28A 77(2) . .
C25B C27A C26B 102(5) . .
C25B C27A C26A 29(4) . .
C26B C27A C26A 96(4) . .
C25B C27A C28A 95(4) . .
C26B C27A C28A 114(4) . .
C26A C27A C28A 122(2) . .
C25B C27A Cl12 149(4) . .
C26B C27A Cl12 63(4) . .
C26A C27A Cl12 121.6(18) . .
C28A C27A Cl12 115.8(19) . .
C25B C27A C27B 122(5) . .
C26B C27A C27B 48(3) . .
C26A C27A C27B 136(3) . .
C28A C27A C27B 69.4(19) . .
Cl12 C27A C27B 69(2) . .
C25B C27A C24B 50(4) . .
C26B C27A C24B 125(4) . .
C26A C27A C24B 77(2) . .
C28A C27A C24B 45.2(18) . .
Cl12 C27A C24B 160(2) . .
C27B C27A C24B 102(2) . .
C25B C27A Cl15 41(4) . .
C26B C27A Cl15 102(3) . .
C26A C27A Cl15 14.7(11) . .
C28A C27A Cl15 128.7(18) . .
Cl12 C27A Cl15 112.4(10) . .
C27B C27A Cl15 147(2) . .
C24B C27A Cl15 84.6(19) . .
C28B C27B C26B 122(5) . .
C28B C27B Cl14 125(5) . .
C26B C27B Cl14 113(3) . .
C28B C27B C27A 91(4) . .
C26B C27B C27A 34(2) . .
Cl14 C27B C27A 140(3) . .
C28B C27B C28A 46(3) . .
C26B C27B C28A 78(3) . .
Cl14 C27B C28A 163(4) . .
C27A C27B C28A 45.4(16) . .
C28B C27B Cl12 124(5) . .
C26B C27B Cl12 51(3) . .
Cl14 C27B Cl12 89(2) . .
C27A C27B Cl12 54.3(18) . .
C28A C27B Cl12 88(3) . .
C23B C28A C24B 71(4) . .
C23B C28A C28B 68(4) . .
C24B C28A C28B 130(4) . .
C23B C28A C27A 142(3) . .
C24B C28A C27A 86(2) . .
C28B C28A C27A 109(2) . .
C23B C28A C23A 43(3) . .
C24B C28A C23A 32.1(17) . .
C28B C28A C23A 111(3) . .
C27A C28A C23A 118(2) . .
C23B C28A C25B 118(4) . .
C24B C28A C25B 57(3) . .
C28B C28A C25B 121(3) . .
C27A C28A C25B 29(2) . .
C23A C28A C25B 89(2) . .
C23B C28A C27B 104(4) . .
C24B C28A C27B 126(3) . .
C28B C28A C27B 44(2) . .
C27A C28A C27B 65(2) . .
C23A C28A C27B 135(2) . .
C25B C28A C27B 83(2) . .
C23B C28A C26B 125(3) . .
C24B C28A C26B 98(3) . .
C28B C28A C26B 83(2) . .
C27A C28A C26B 26.9(18) . .
C23A C28A C26B 125(2) . .
C25B C28A C26B 44(2) . .
C27B C28A C26B 40(2) . .
C27B C28B C28A 90(4) . .
C27B C28B C23B 124(5) . .
C28A C28B C23B 46(3) . .
C27B C28B Cl13 113(4) . .
C28A C28B Cl13 157(3) . .
C23B C28B Cl13 115(4) . .
N1 C29 C30 178.3(9) . .
C29 C30 C31 112.8(7) . .
C29 C30 C32 120.9(7) . .
C31 C30 C32 125.7(7) . .
N2 C31 C30 173.5(9) . .
C35 C32 C33 119.5(7) . .
C35 C32 C30 117.4(7) . .
C33 C32 C30 123.1(7) . .
C35 C33 C32 117.7(7) 2_666 .
C35 C33 C34 118.9(8) 2_666 .
C32 C33 C34 123.2(7) . .
C33 C34 H34A 109.5 . .
C33 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
C33 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
C32 C35 C33 122.7(7) . 2_666
C32 C35 H35 118.6 . .
C33 C35 H35 118.6 2_666 .
Cl7A C17B C18B 104(4) . .
Cl7A C17B C16 134(4) . .
C18B C17B C16 122(4) . .
Cl7A C17B C18A 135(4) . .
C18B C17B C18A 33(2) . .
C16 C17B C18A 89(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ru1 O2 2.020(6) 2_676
Ru1 O1 2.021(6) .
Ru1 O4 2.026(5) 2_676
Ru1 O3 2.034(6) .
Ru1 N1 2.188(8) .
Ru1 Ru1 2.2798(15) 2_676
Ru2 O8 2.022(6) 2_665
Ru2 O6 2.033(6) 2_665
Ru2 O5 2.039(6) .
Ru2 O7 2.044(6) .
Ru2 N2 2.214(8) .
Ru2 Ru2 2.2825(15) 2_665
Cl1 C3 1.724(14) .
Cl2 C4 1.733(14) .
Cl3 C6 1.757(16) .
Cl4A C10 1.730(10) .
Cl4B C14 1.712(16) .
Cl5 C11 1.716(11) .
Cl6 C13 1.724(11) .
Cl7A C17B 1.22(5) .
Cl7A C17A 1.696(13) .
Cl7A C18B 2.01(4) .
Cl7B C21A 1.115(17) .
Cl7B C21B 1.70(5) .
Cl7B C20A 1.786(17) .
Cl7B Cl9A 2.312(11) .
Cl8A Cl9B 1.303(12) .
Cl8A C18B 1.37(5) .
Cl8A C19B 1.64(5) .
Cl8A C18A 1.723(13) .
Cl8B Cl9A 1.550(12) .
Cl8B C20A 1.648(16) .
Cl8B C19A 1.67(2) .
Cl8B C20B 1.70(6) .
Cl9A C20A 1.730(12) .
Cl9B C18B 1.76(5) .
Cl10 C24A 1.71(2) .
Cl10 Cl14 2.183(18) 2_565
Cl11 C25A 1.70(2) .
Cl11 Cl13 1.702(17) 2_565
Cl11 Cl15 2.181(15) .
Cl12 C26B 1.57(6) .
Cl12 C27A 1.74(2) .
Cl12 C27B 2.01(6) .
Cl13 Cl11 1.702(17) 2_565
Cl13 C28B 1.91(6) .
Cl14 C27B 1.72(5) .
Cl14 Cl10 2.183(18) 2_565
Cl15 C26A 1.04(2) .
Cl15 C25A 1.55(2) .
Cl15 C25B 1.69(5) .
Cl15 C27A 2.21(3) .
O1 C1 1.255(11) .
O2 C1 1.279(11) .
O2 Ru1 2.020(6) 2_676
O3 C8 1.282(11) .
O4 C8 1.252(11) .
O4 Ru1 2.027(5) 2_676
O5 C15 1.269(10) .
O6 C15 1.259(10) .
O6 Ru2 2.033(6) 2_665
O7 C22A 1.230(14) .
O8 C22A 1.268(15) .
O8 Ru2 2.022(6) 2_665
N1 C29 1.159(11) .
N2 C31 1.152(11) .
C1 C2 1.516(11) .
C2 C3 1.380(16) .
C2 C7 1.396(15) .
C3 C4 1.434(15) .
C4 C5 1.37(2) .
C5 C6 1.34(2) .
C5 H5 0.9500 .
C6 C7 1.373(15) .
C7 H7 0.9500 .
C8 C9 1.498(11) .
C9 C10 1.383(13) .
C9 C14 1.409(14) .
C10 C11 1.406(13) .
C11 C12 1.358(15) .
C12 C13 1.360(16) .
C12 H12 0.9500 .
C13 C14 1.409(15) .
C15 C16 1.509(13) .
C16 C21B 1.22(5) .
C16 C17A 1.329(17) .
C16 C21A 1.462(15) .
C16 C17B 1.69(5) .
C17A C18B 1.38(5) .
C17A C18A 1.45(2) .
C17A C21B 1.87(5) .
C18A C19B 0.77(4) .
C18A C18B 0.92(4) .
C18A C19A 1.36(2) .
C18A C20B 1.43(7) .
C18A C17B 1.70(5) .
C18B C17B 1.34(7) .
C18B C19B 1.49(6) .
C19A C19B 1.03(5) .
C19A C20A 1.39(2) .
C19A C21B 1.88(5) .
C19B C20B 1.29(8) .
C20A C20B 1.11(6) .
C20A C21B 1.22(5) .
C20A C21A 1.403(17) .
C20B C21B 1.52(8) .
C21A C21B 0.73(5) .
C22A C23A 1.56(2) .
C22A C23B 1.58(4) .
C23A C24B 0.76(4) .
C23A C23B 0.97(5) .
C23A C28A 1.41(3) .
C23A C24A 1.41(3) .
C23B C28A 1.04(5) .
C23B C28B 1.35(6) .
C23B C24B 1.39(7) .
C24A C24B 1.12(5) .
C24A C25A 1.41(2) .
C24B C28A 1.32(6) .
C24B C25B 1.48(6) .
C24B C25A 1.74(5) .
C24B C27A 1.86(5) .
C24B C26A 2.00(5) .
C25A C26A 1.41(3) .
C25A C25B 1.55(6) .
C25B C26A 0.67(5) .
C25B C27A 0.82(6) .
C25B C26B 1.43(7) .
C25B C28A 1.68(5) .
C26A C27A 1.26(3) .
C26A C26B 1.69(6) .
C26B C27A 1.01(5) .
C26B C27B 1.34(6) .
C26B C28A 2.04(4) .
C27A C28A 1.40(3) .
C27A C27B 1.78(6) .
C27B C28B 1.28(5) .
C27B C28A 1.84(5) .
C28A C28B 1.32(5) .
C29 C30 1.371(12) .
C30 C31 1.391(12) .
C30 C32 1.468(10) .
C32 C35 1.392(11) .
C32 C33 1.397(11) .
C33 C35 1.395(11) 2_666
C33 C34 1.510(12) .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
C35 C33 1.395(11) 2_666
C35 H35 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C19A Cl8B Cl9A C20A -11.0(8) . .
C20B Cl8B Cl9A C20A 1(2) . .
C20A Cl8B Cl9A Cl7B -21.6(7) . .
C19A Cl8B Cl9A Cl7B -32.6(10) . .
C20B Cl8B Cl9A Cl7B -20(2) . .
C19B Cl8A Cl9B C18B 13(3) . .
C18A Cl8A Cl9B C18B 3(2) . .
Ru1 O1 C1 O2 2.6(11) . .
Ru1 O1 C1 C2 -178.1(5) . .
Ru1 O2 C1 O1 -1.2(11) 2_676 .
Ru1 O2 C1 C2 179.6(5) 2_676 .
O1 C1 C2 C3 14.2(13) . .
O2 C1 C2 C3 -166.6(8) . .
O1 C1 C2 C7 -166.1(8) . .
O2 C1 C2 C7 13.2(11) . .
C7 C2 C3 C4 -0.7(14) . .
C1 C2 C3 C4 179.0(8) . .
C7 C2 C3 Cl1 -179.6(7) . .
C1 C2 C3 Cl1 0.1(14) . .
C2 C3 C4 C5 0.9(15) . .
Cl1 C3 C4 C5 179.9(9) . .
C2 C3 C4 Cl2 -179.1(7) . .
Cl1 C3 C4 Cl2 -0.1(12) . .
C3 C4 C5 C6 0.5(17) . .
Cl2 C4 C5 C6 -179.5(9) . .
C4 C5 C6 C7 -2.4(18) . .
C4 C5 C6 Cl3 -178.7(8) . .
C5 C6 C7 C2 2.6(17) . .
Cl3 C6 C7 C2 179.0(7) . .
C3 C2 C7 C6 -1.0(14) . .
C1 C2 C7 C6 179.3(9) . .
Ru1 O4 C8 O3 1.5(11) 2_676 .
Ru1 O4 C8 C9 179.7(5) 2_676 .
Ru1 O3 C8 O4 -2.1(11) . .
Ru1 O3 C8 C9 179.7(5) . .
O4 C8 C9 C10 153.6(8) . .
O3 C8 C9 C10 -28.1(12) . .
O4 C8 C9 C14 -27.1(12) . .
O3 C8 C9 C14 151.2(8) . .
C14 C9 C10 C11 -2.1(14) . .
C8 C9 C10 C11 177.2(8) . .
C14 C9 C10 Cl4A 175.8(8) . .
C8 C9 C10 Cl4A -4.9(13) . .
C9 C10 C11 C12 1.8(14) . .
Cl4A C10 C11 C12 -176.3(8) . .
C9 C10 C11 Cl5 -179.7(7) . .
Cl4A C10 C11 Cl5 2.2(11) . .
C10 C11 C12 C13 -0.2(15) . .
Cl5 C11 C12 C13 -178.7(9) . .
C11 C12 C13 C14 -1.1(16) . .
C11 C12 C13 Cl6 -180.0(8) . .
C12 C13 C14 C9 0.8(16) . .
Cl6 C13 C14 C9 179.7(8) . .
C12 C13 C14 Cl4B 177.9(12) . .
Cl6 C13 C14 Cl4B -3.2(13) . .
C10 C9 C14 C13 0.8(14) . .
C8 C9 C14 C13 -178.5(9) . .
C10 C9 C14 Cl4B -175.3(13) . .
C8 C9 C14 Cl4B 5.4(18) . .
Ru2 O6 C15 O5 -0.1(11) 2_665 .
Ru2 O6 C15 C16 178.1(5) 2_665 .
Ru2 O5 C15 O6 0.2(12) . .
Ru2 O5 C15 C16 -177.9(6) . .
O6 C15 C16 C21B 3(4) . .
O5 C15 C16 C21B -179(4) . .
O6 C15 C16 C17A -170.9(11) . .
O5 C15 C16 C17A 7.4(16) . .
O6 C15 C16 C21A 11.2(12) . .
O5 C15 C16 C21A -170.6(9) . .
O6 C15 C16 C17B -173(2) . .
O5 C15 C16 C17B 5(2) . .
C21B C16 C17A C18B 17(6) . .
C21A C16 C17A C18B 11(6) . .
C15 C16 C17A C18B -167(5) . .
C17B C16 C17A C18B -158(14) . .
C21B C16 C17A C18A 7(3) . .
C21A C16 C17A C18A 0(2) . .
C15 C16 C17A C18A -177.3(11) . .
C17B C16 C17A C18A -169(11) . .
C21B C16 C17A Cl7A -171(3) . .
C21A C16 C17A Cl7A -177.0(10) . .
C15 C16 C17A Cl7A 5(2) . .
C17B C16 C17A Cl7A 14(10) . .
C21A C16 C17A C21B -6(3) . .
C15 C16 C17A C21B 176(3) . .
C17B C16 C17A C21B -175(11) . .
C17B Cl7A C17A C16 -119(35) . .
C18B Cl7A C17A C16 -177(3) . .
C17B Cl7A C17A C18B 58(34) . .
C17B Cl7A C17A C18A 64(34) . .
C18B Cl7A C17A C18A 6(2) . .
C17B Cl7A C17A C21B -140(37) . .
C18B Cl7A C17A C21B 162(7) . .
C16 C17A C18A C19B -8(25) . .
C18B C17A C18A C19B 179(100) . .
Cl7A C17A C18A C19B 169(24) . .
C21B C17A C18A C19B -4(24) . .
C16 C17A C18A C18B 173(4) . .
Cl7A C17A C18A C18B -9(3) . .
C21B C17A C18A C18B 178(4) . .
C16 C17A C18A C19A 0(2) . .
C18B C17A C18A C19A -173(4) . .
Cl7A C17A C18A C19A 177.6(12) . .
C21B C17A C18A C19A 5(2) . .
C16 C17A C18A C20B -10(3) . .
C18B C17A C18A C20B 176(5) . .
Cl7A C17A C18A C20B 167(3) . .
C21B C17A C18A C20B -6(4) . .
C16 C17A C18A C17B 170(10) . .
C18B C17A C18A C17B -3(9) . .
Cl7A C17A C18A C17B -12(8) . .
C21B C17A C18A C17B 175(9) . .
C16 C17A C18A Cl8A -178.8(10) . .
C18B C17A C18A Cl8A 8(3) . .
Cl7A C17A C18A Cl8A -1.2(18) . .
C21B C17A C18A Cl8A -174.3(19) . .
Cl9B Cl8A C18A C19B 166(4) . .
C18B Cl8A C18A C19B 172(6) . .
Cl9B Cl8A C18A C18B -6(4) . .
C19B Cl8A C18A C18B -172(6) . .
Cl9B Cl8A C18A C19A 165.2(12) . .
C18B Cl8A C18A C19A 172(4) . .
C19B Cl8A C18A C19A -1(4) . .
Cl9B Cl8A C18A C20B 179(4) . .
C18B Cl8A C18A C20B -174(6) . .
C19B Cl8A C18A C20B 14(5) . .
Cl9B Cl8A C18A C17A -16.0(15) . .
C18B Cl8A C18A C17A -10(4) . .
C19B Cl8A C18A C17A 178(5) . .
Cl9B Cl8A C18A C17B -13(2) . .
C18B Cl8A C18A C17B -7(4) . .
C19B Cl8A C18A C17B -179(5) . .
C19B C18A C18B C17B 179(5) . .
C19A C18A C18B C17B 146(17) . .
C17A C18A C18B C17B -1(3) . .
Cl8A C18A C18B C17B -172(5) . .
C19B C18A C18B Cl8A -9(7) . .
C19A C18A C18B Cl8A -42(20) . .
C17A C18A C18B Cl8A 171(3) . .
C17B C18A C18B Cl8A 172(5) . .
C19B C18A C18B C17A -180(5) . .
C19A C18A C18B C17A 147(17) . .
C17B C18A C18B C17A 1(3) . .
Cl8A C18A C18B C17A -171(3) . .
C19A C18A C18B C19B -33(16) . .
C17A C18A C18B C19B 180(5) . .
C17B C18A C18B C19B -179(5) . .
Cl8A C18A C18B C19B 9(7) . .
C19B C18A C18B Cl9B -2(10) . .
C19A C18A C18B Cl9B -35(23) . .
C17A C18A C18B Cl9B 178(8) . .
C17B C18A C18B Cl9B 179(9) . .
Cl8A C18A C18B Cl9B 7(4) . .
C19B C18A C18B Cl7A -171(5) . .
C19A C18A C18B Cl7A 156(14) . .
C17A C18A C18B Cl7A 9(3) . .
C17B C18A C18B Cl7A 10(3) . .
Cl8A C18A C18B Cl7A -162(7) . .
Cl9B Cl8A C18B C18A 174(4) . .
C19B Cl8A C18B C18A 4(3) . .
Cl9B Cl8A C18B C17B -42(19) . .
C19B Cl8A C18B C17B 148(20) . .
C18A Cl8A C18B C17B 144(22) . .
Cl9B Cl8A C18B C17A -145(17) . .
C19B Cl8A C18B C17A 45(16) . .
C18A Cl8A C18B C17A 41(15) . .
Cl9B Cl8A C18B C19B 170(3) . .
C18A Cl8A C18B C19B -4(3) . .
C19B Cl8A C18B Cl9B -170(3) . .
C18A Cl8A C18B Cl9B -174(4) . .
Cl9B Cl8A C18B Cl7A -24(3) . .
C19B Cl8A C18B Cl7A 166(5) . .
C18A Cl8A C18B Cl7A 162(7) . .
C16 C17A C18B C18A -15(7) . .
Cl7A C17A C18B C18A 172(3) . .
C21B C17A C18B C18A -3(4) . .
C16 C17A C18B C17B 163(11) . .
C18A C17A C18B C17B 177(9) . .
Cl7A C17A C18B C17B -11(8) . .
C21B C17A C18B C17B 175(9) . .
C16 C17A C18B Cl8A -58(20) . .
C18A C17A C18B Cl8A -43(15) . .
Cl7A C17A C18B Cl8A 129(17) . .
C21B C17A C18B Cl8A -45(18) . .
C16 C17A C18B C19B -15(8) . .
C18A C17A C18B C19B 0(2) . .
Cl7A C17A C18B C19B 172(3) . .
C21B C17A C18B C19B -3(4) . .
C16 C17A C18B Cl9B 167(3) . .
C18A C17A C18B Cl9B -178(8) . .
Cl7A C17A C18B Cl9B -6(5) . .
C21B C17A C18B Cl9B 179(5) . .
C16 C17A C18B Cl7A 174(5) . .
C18A C17A C18B Cl7A -172(3) . .
C21B C17A C18B Cl7A -174(2) . .
Cl8A Cl9B C18B C18A -10(6) . .
Cl8A Cl9B C18B C17B 169(5) . .
Cl8A Cl9B C18B C17A 167(7) . .
Cl8A Cl9B C18B C19B -10(3) . .
Cl8A Cl9B C18B Cl7A 162(3) . .
C18B C18A C19A C19B 38(18) . .
C20B C18A C19A C19B -144(12) . .
C17A C18A C19A C19B -178(6) . .
C17B C18A C19A C19B 178(6) . .
Cl8A C18A C19A C19B 1(5) . .
C19B C18A C19A C20A 177(5) . .
C18B C18A C19A C20A -145(18) . .
C20B C18A C19A C20A 33(10) . .
C17A C18A C19A C20A -1(2) . .
C17B C18A C19A C20A -5(4) . .
Cl8A C18A C19A C20A 177.4(11) . .
C19B C18A C19A Cl8B 74(7) . .
C18B C18A C19A Cl8B 112(18) . .
C20B C18A C19A Cl8B -69(10) . .
C17A C18A C19A Cl8B -104(5) . .
C17B C18A C19A Cl8B -108(6) . .
Cl8A C18A C19A Cl8B 75(6) . .
C19B C18A C19A C21B 174(6) . .
C18B C18A C19A C21B -149(18) . .
C20B C18A C19A C21B 30(10) . .
C17A C18A C19A C21B -5(2) . .
C17B C18A C19A C21B -8(4) . .
Cl8A C18A C19A C21B 174.3(19) . .
Cl9A Cl8B C19A C19B -180(5) . .
C20A Cl8B C19A C19B 167(5) . .
C20B Cl8B C19A C19B 128(12) . .
Cl9A Cl8B C19A C18A 122(5) . .
C20A Cl8B C19A C18A 109(6) . .
C20B Cl8B C19A C18A 70(11) . .
Cl9A Cl8B C19A C20A 13.2(10) . .
C20B Cl8B C19A C20A -39(10) . .
Cl9A Cl8B C19A C21B 26(2) . .
C20A Cl8B C19A C21B 12.6(18) . .
C20B Cl8B C19A C21B -27(10) . .
C18B C18A C19B C19A -172(4) . .
C20B C18A C19B C19A 12(4) . .
C17A C18A C19B C19A 10(27) . .
Cl8A C18A C19B C19A -179(5) . .
C18B C18A C19B C20B 176(5) . .
C19A C18A C19B C20B -12(4) . .
C17A C18A C19B C20B -2(26) . .
Cl8A C18A C19B C20B 169(4) . .
C19A C18A C19B C18B 172(4) . .
C20B C18A C19B C18B -176(5) . .
C17A C18A C19B C18B -178(100) . .
Cl8A C18A C19B C18B -7(6) . .
C18B C18A C19B Cl8A 7(5) . .
C19A C18A C19B Cl8A 179(5) . .
C20B C18A C19B Cl8A -169(4) . .
C17A C18A C19B Cl8A -171(23) . .
C20A C19A C19B C18A -7(10) . .
Cl8B C19A C19B C18A -160(3) . .
C21B C19A C19B C18A -7(6) . .
C18A C19A C19B C20B 42(13) . .
C20A C19A C19B C20B 35(11) . .
Cl8B C19A C19B C20B -118(13) . .
C21B C19A C19B C20B 35(12) . .
C18A C19A C19B C18B -5(3) . .
C20A C19A C19B C18B -12(11) . .
Cl8B C19A C19B C18B -165(3) . .
C21B C19A C19B C18B -12(7) . .
C17B C18B C19B C18A -1(6) . .
Cl8A C18B C19B C18A 171(7) . .
C17A C18B C19B C18A 0(5) . .
Cl9B C18B C19B C18A 179(7) . .
Cl7A C18B C19B C18A 18(10) . .
C18A C18B C19B C19A 10(5) . .
C17B C18B C19B C19A 9(8) . .
Cl8A C18B C19B C19A -179(6) . .
C17A C18B C19B C19A 10(7) . .
Cl9B C18B C19B C19A -171(4) . .
Cl7A C18B C19B C19A 28(13) . .
C18A C18B C19B C20B -4(6) . .
C17B C18B C19B C20B -5(8) . .
Cl8A C18B C19B C20B 167(5) . .
C17A C18B C19B C20B -4(6) . .
Cl9B C18B C19B C20B 175(5) . .
Cl7A C18B C19B C20B 13(12) . .
C18A C18B C19B Cl8A -171(7) . .
C17B C18B C19B Cl8A -171(6) . .
C17A C18B C19B Cl8A -170(4) . .
Cl9B C18B C19B Cl8A 8(2) . .
Cl7A C18B C19B Cl8A -153(9) . .
Cl9B Cl8A C19B C18A -20(6) . .
C18B Cl8A C19B C18A -5(4) . .
Cl9B Cl8A C19B C20B -60(18) . .
C18B Cl8A C19B C20B -45(16) . .
C18A Cl8A C19B C20B -40(15) . .
Cl9B Cl8A C19B C18B -15(4) . .
C18A Cl8A C19B C18B 5(4) . .
C19B C19A C20A C20B -48(14) . .
C18A C19A C20A C20B -53(14) . .
Cl8B C19A C20A C20B 113(14) . .
C21B C19A C20A C20B -48(14) . .
C19B C19A C20A C21B 0(8) . .
C18A C19A C20A C21B -5(3) . .
Cl8B C19A C20A C21B 161(3) . .
C19B C19A C20A C21A 7(8) . .
C18A C19A C20A C21A 2(2) . .
Cl8B C19A C20A C21A 168.0(14) . .
C21B C19A C20A C21A 7(3) . .
C19B C19A C20A Cl8B -161(7) . .
C18A C19A C20A Cl8B -165.6(16) . .
C21B C19A C20A Cl8B -161(3) . .
C19B C19A C20A Cl9A -174(7) . .
C18A C19A C20A Cl9A -177.9(11) . .
Cl8B C19A C20A Cl9A -12.4(10) . .
C21B C19A C20A Cl9A -173(3) . .
C19B C19A C20A Cl7B -27(9) . .
C18A C19A C20A Cl7B -32(4) . .
Cl8B C19A C20A Cl7B 134(3) . .
C21B C19A C20A Cl7B -27(3) . .
Cl9A Cl8B C20A C20B 178(4) . .
C19A Cl8B C20A C20B -15(4) . .
Cl9A Cl8B C20A C21B 150(6) . .
C19A Cl8B C20A C21B -43(6) . .
C20B Cl8B C20A C21B -27(7) . .
Cl9A Cl8B C20A C19A -166.7(10) . .
C20B Cl8B C20A C19A 15(4) . .
Cl9A Cl8B C20A C21A 62(5) . .
C19A Cl8B C20A C21A -131(5) . .
C20B Cl8B C20A C21A -116(6) . .
C19A Cl8B C20A Cl9A 166.7(10) . .
C20B Cl8B C20A Cl9A -178(4) . .
Cl9A Cl8B C20A Cl7B 36.6(11) . .
C19A Cl8B C20A Cl7B -156.7(15) . .
C20B Cl8B C20A Cl7B -141(4) . .
Cl8B Cl9A C20A C20B -3(4) . .
Cl7B Cl9A C20A C20B 150(5) . .
Cl8B Cl9A C20A C21B -153(5) . .
Cl7B Cl9A C20A C21B -1(5) . .
Cl8B Cl9A C20A C19A 13.9(11) . .
Cl7B Cl9A C20A C19A 166.3(14) . .
Cl8B Cl9A C20A C21A -166.4(13) . .
Cl7B Cl9A C20A C21A -14.1(8) . .
Cl7B Cl9A C20A Cl8B 152.3(9) . .
Cl8B Cl9A C20A Cl7B -152.3(9) . .
C21A Cl7B C20A C20B 58(6) . .
C21B Cl7B C20A C20B 39(6) . .
Cl9A Cl7B C20A C20B -142(6) . .
C21A Cl7B C20A C21B 20(3) . .
Cl9A Cl7B C20A C21B 179(3) . .
C21A Cl7B C20A C19A 49(3) . .
C21B Cl7B C20A C19A 30(4) . .
Cl9A Cl7B C20A C19A -151(3) . .
C21B Cl7B C20A C21A -20(3) . .
Cl9A Cl7B C20A C21A 159.9(12) . .
C21A Cl7B C20A Cl8B 170.8(16) . .
C21B Cl7B C20A Cl8B 151(3) . .
Cl9A Cl7B C20A Cl8B -29.3(9) . .
C21A Cl7B C20A Cl9A -159.9(12) . .
C21B Cl7B C20A Cl9A -179(3) . .
C21B C20A C20B C19B -86(16) . .
C19A C20A C20B C19B 45(13) . .
C21A C20A C20B C19B -86(16) . .
Cl8B C20A C20B C19B 107(16) . .
Cl9A C20A C20B C19B 109(15) . .
Cl7B C20A C20B C19B -121(14) . .
C21B C20A C20B C18A -33(8) . .
C19A C20A C20B C18A 98(18) . .
C21A C20A C20B C18A -34(9) . .
Cl8B C20A C20B C18A 160(9) . .
Cl9A C20A C20B C18A 162(5) . .
Cl7B C20A C20B C18A -69(10) . .
C19A C20A C20B C21B 131(14) . .
C21A C20A C20B C21B 0(3) . .
Cl8B C20A C20B C21B -167(3) . .
Cl9A C20A C20B C21B -165(4) . .
Cl7B C20A C20B C21B -35(5) . .
C21B C20A C20B Cl8B 167(3) . .
C19A C20A C20B Cl8B -62(13) . .
C21A C20A C20B Cl8B 166.9(14) . .
Cl9A C20A C20B Cl8B 2(4) . .
Cl7B C20A C20B Cl8B 132(4) . .
C18A C19B C20B C20A 80(16) . .
C19A C19B C20B C20A -59(16) . .
C18B C19B C20B C20A 82(16) . .
Cl8A C19B C20B C20A 120(18) . .
C19A C19B C20B C18A -139(13) . .
C18B C19B C20B C18A 2(3) . .
Cl8A C19B C20B C18A 40(14) . .
C18A C19B C20B C21B 9(8) . .
C19A C19B C20B C21B -130(16) . .
C18B C19B C20B C21B 11(9) . .
Cl8A C19B C20B C21B 49(20) . .
C18A C19B C20B Cl8B 177(5) . .
C19A C19B C20B Cl8B 38(9) . .
C18B C19B C20B Cl8B 179(4) . .
Cl8A C19B C20B Cl8B -143(14) . .
C19B C18A C20B C20A -146(10) . .
C19A C18A C20B C20A -117(16) . .
C17A C18A C20B C20A 33(9) . .
C17B C18A C20B C20A 33(10) . .
Cl8A C18A C20B C20A -161(5) . .
C19A C18A C20B C19B 30(10) . .
C17A C18A C20B C19B 180(5) . .
C17B C18A C20B C19B 180(5) . .
Cl8A C18A C20B C19B -14(6) . .
C19B C18A C20B C21B -172(6) . .
C19A C18A C20B C21B -143(13) . .
C17A C18A C20B C21B 7(4) . .
C17B C18A C20B C21B 7(5) . .
Cl8A C18A C20B C21B 173(2) . .
C19B C18A C20B Cl8B -5(9) . .
C19A C18A C20B Cl8B 24(4) . .
C17A C18A C20B Cl8B 174(9) . .
C17B C18A C20B Cl8B 174(8) . .
Cl8A C18A C20B Cl8B -20(12) . .
Cl9A Cl8B C20B C20A -2(4) . .
C19A Cl8B C20B C20A 130(13) . .
Cl9A Cl8B C20B C19B -158(5) . .
C20A Cl8B C20B C19B -156(8) . .
C19A Cl8B C20B C19B -27(7) . .
Cl9A Cl8B C20B C18A -155(9) . .
C20A Cl8B C20B C18A -153(12) . .
C19A Cl8B C20B C18A -23(4) . .
Cl9A Cl8B C20B C21B 10(6) . .
C20A Cl8B C20B C21B 12(3) . .
C19A Cl8B C20B C21B 141(14) . .
C20A Cl7B C21A C21B -46(6) . .
Cl9A Cl7B C21A C21B -60(6) . .
C21B Cl7B C21A C20A 46(6) . .
Cl9A Cl7B C21A C20A -14.9(9) . .
C21B Cl7B C21A C16 -93(7) . .
C20A Cl7B C21A C16 -139(3) . .
Cl9A Cl7B C21A C16 -154(2) . .
C20B C20A C21A C21B 0(6) . .
C19A C20A C21A C21B -14(5) . .
Cl8B C20A C21A C21B 112(7) . .
Cl9A C20A C21A C21B 167(5) . .
Cl7B C20A C21A C21B 144(5) . .
C20B C20A C21A Cl7B -144(4) . .
C21B C20A C21A Cl7B -144(5) . .
C19A C20A C21A Cl7B -157.6(14) . .
Cl8B C20A C21A Cl7B -32(5) . .
Cl9A C20A C21A Cl7B 22.7(13) . .
C20B C20A C21A C16 12(4) . .
C21B C20A C21A C16 12(5) . .
C19A C20A C21A C16 -1.9(18) . .
Cl8B C20A C21A C16 124(5) . .
Cl9A C20A C21A C16 178.5(8) . .
Cl7B C20A C21A C16 155.7(16) . .
C17A C16 C21A C21B 13(5) . .
C15 C16 C21A C21B -169(5) . .
C17B C16 C21A C21B 16(6) . .
C21B C16 C21A Cl7B 121(6) . .
C17A C16 C21A Cl7B 134(2) . .
C15 C16 C21A Cl7B -48(3) . .
C17B C16 C21A Cl7B 137(3) . .
C21B C16 C21A C20A -12(5) . .
C17A C16 C21A C20A 0.5(17) . .
C15 C16 C21A C20A 178.4(9) . .
C17B C16 C21A C20A 4(3) . .
Cl7B C21A C21B C20A 55(6) . .
C16 C21A C21B C20A -167(5) . .
Cl7B C21A C21B C16 -137(3) . .
C20A C21A C21B C16 167(5) . .
Cl7B C21A C21B C20B 55(11) . .
C20A C21A C21B C20B 0(6) . .
C16 C21A C21B C20B -167(11) . .
C20A C21A C21B Cl7B -55(6) . .
C16 C21A C21B Cl7B 137(3) . .
Cl7B C21A C21B C17A -149(4) . .
C20A C21A C21B C17A 156(9) . .
C16 C21A C21B C17A -11(5) . .
Cl7B C21A C21B C19A 68(10) . .
C20A C21A C21B C19A 12(4) . .
C16 C21A C21B C19A -155(9) . .
C20B C20A C21B C21A -180(6) . .
C19A C20A C21B C21A 168(4) . .
Cl8B C20A C21B C21A -153(3) . .
Cl9A C20A C21B C21A -23(8) . .
Cl7B C20A C21B C21A -24(4) . .
C20B C20A C21B C16 80(23) . .
C19A C20A C21B C16 68(23) . .
C21A C20A C21B C16 -100(24) . .
Cl8B C20A C21B C16 106(22) . .
Cl9A C20A C21B C16 -123(21) . .
Cl7B C20A C21B C16 -124(24) . .
C19A C20A C21B C20B -12(4) . .
C21A C20A C21B C20B 180(6) . .
Cl8B C20A C21B C20B 27(6) . .
Cl9A C20A C21B C20B 157(6) . .
Cl7B C20A C21B C20B 156(4) . .
C20B C20A C21B Cl7B -156(4) . .
C19A C20A C21B Cl7B -167.8(15) . .
C21A C20A C21B Cl7B 24(4) . .
Cl8B C20A C21B Cl7B -129(5) . .
Cl9A C20A C21B Cl7B 1(5) . .
C20B C20A C21B C17A 21(5) . .
C19A C20A C21B C17A 9(4) . .
C21A C20A C21B C17A -159(8) . .
Cl8B C20A C21B C17A 48(8) . .
Cl9A C20A C21B C17A 178.0(14) . .
Cl7B C20A C21B C17A 177(5) . .
C20B C20A C21B C19A 12(4) . .
C21A C20A C21B C19A -168(4) . .
Cl8B C20A C21B C19A 38(5) . .
Cl9A C20A C21B C19A 169(5) . .
Cl7B C20A C21B C19A 167.8(15) . .
C17A C16 C21B C21A -169(5) . .
C15 C16 C21B C21A 16(8) . .
C17B C16 C21B C21A -168(4) . .
C17A C16 C21B C20A -69(23) . .
C21A C16 C21B C20A 100(24) . .
C15 C16 C21B C20A 116(22) . .
C17B C16 C21B C20A -68(23) . .
C17A C16 C21B C20B -1(6) . .
C21A C16 C21B C20B 168(10) . .
C15 C16 C21B C20B -176(4) . .
C17B C16 C21B C20B 0(7) . .
C17A C16 C21B Cl7B 170(3) . .
C21A C16 C21B Cl7B -20(2) . .
C15 C16 C21B Cl7B -4(6) . .
C17B C16 C21B Cl7B 172(3) . .
C21A C16 C21B C17A 169(5) . .
C15 C16 C21B C17A -175(4) . .
C17B C16 C21B C17A 1(3) . .
C17A C16 C21B C19A -11(4) . .
C21A C16 C21B C19A 158(8) . .
C15 C16 C21B C19A 174.3(14) . .
C17B C16 C21B C19A -10(5) . .
C20A C20B C21B C21A 0(9) . .
C19B C20B C21B C21A 154(8) . .
C18A C20B C21B C21A 159(8) . .
Cl8B C20B C21B C21A -13(12) . .
C19B C20B C21B C20A 154(8) . .
C18A C20B C21B C20A 158(6) . .
Cl8B C20B C21B C20A -14(3) . .
C20A C20B C21B C16 -163(6) . .
C19B C20B C21B C16 -10(10) . .
C18A C20B C21B C16 -5(7) . .
Cl8B C20B C21B C16 -177(4) . .
C20A C20B C21B Cl7B 26(4) . .
C19B C20B C21B Cl7B 179(5) . .
C18A C20B C21B Cl7B -176(3) . .
Cl8B C20B C21B Cl7B 12(7) . .
C20A C20B C21B C17A -164(4) . .
C19B C20B C21B C17A -10(7) . .
C18A C20B C21B C17A -5(3) . .
Cl8B C20B C21B C17A -178(4) . .
C20A C20B C21B C19A -95(19) . .
C19B C20B C21B C19A 58(17) . .
C18A C20B C21B C19A 63(18) . .
Cl8B C20B C21B C19A -109(21) . .
C20A Cl7B C21B C21A 121(7) . .
Cl9A Cl7B C21B C21A 120(6) . .
C21A Cl7B C21B C20A -121(7) . .
Cl9A Cl7B C21B C20A 0(2) . .
C21A Cl7B C21B C16 47(5) . .
C20A Cl7B C21B C16 168(6) . .
Cl9A Cl7B C21B C16 168(4) . .
C21A Cl7B C21B C20B -140(9) . .
C20A Cl7B C21B C20B -19(3) . .
Cl9A Cl7B C21B C20B -20(4) . .
C21A Cl7B C21B C17A 65(8) . .
C20A Cl7B C21B C17A -174(11) . .
Cl9A Cl7B C21B C17A -174(9) . .
C21A Cl7B C21B C19A -131(8) . .
C20A Cl7B C21B C19A -10.4(13) . .
Cl9A Cl7B C21B C19A -11(3) . .
C16 C17A C21B C21A 16(7) . .
C18B C17A C21B C21A -156(8) . .
C18A C17A C21B C21A -158(9) . .
Cl7A C17A C21B C21A 44(13) . .
C16 C17A C21B C20A 164(6) . .
C18B C17A C21B C20A -8(6) . .
C18A C17A C21B C20A -10(4) . .
Cl7A C17A C21B C20A -168(4) . .
C18B C17A C21B C16 -172(3) . .
C18A C17A C21B C16 -174(3) . .
Cl7A C17A C21B C16 28(8) . .
C16 C17A C21B C20B 179(5) . .
C18B C17A C21B C20B 7(4) . .
C18A C17A C21B C20B 5(3) . .
Cl7A C17A C21B C20B -153(6) . .
C16 C17A C21B Cl7B -23(7) . .
C18B C17A C21B Cl7B 164(8) . .
C18A C17A C21B Cl7B 163(9) . .
Cl7A C17A C21B Cl7B 4(14) . .
C16 C17A C21B C19A 171(3) . .
C18B C17A C21B C19A -1(3) . .
C18A C17A C21B C19A -2.8(13) . .
Cl7A C17A C21B C19A -161(5) . .
C19B C19A C21B C21A 163(8) . .
C18A C19A C21B C21A 159(8) . .
C20A C19A C21B C21A -17(6) . .
Cl8B C19A C21B C21A -34(8) . .
C19B C19A C21B C20A 180(4) . .
C18A C19A C21B C20A 176(3) . .
Cl8B C19A C21B C20A -18(2) . .
C19B C19A C21B C16 15(6) . .
C18A C19A C21B C16 11(4) . .
C20A C19A C21B C16 -165(6) . .
Cl8B C19A C21B C16 177(4) . .
C19B C19A C21B C20B -104(19) . .
C18A C19A C21B C20B -108(19) . .
C20A C19A C21B C20B 77(19) . .
Cl8B C19A C21B C20B 59(19) . .
C19B C19A C21B Cl7B -167(4) . .
C18A C19A C21B Cl7B -171(3) . .
C20A C19A C21B Cl7B 13.5(17) . .
Cl8B C19A C21B Cl7B -4(4) . .
C19B C19A C21B C17A 7(4) . .
C18A C19A C21B C17A 3.0(14) . .
C20A C19A C21B C17A -173(3) . .
Cl8B C19A C21B C17A 169.5(14) . .
Ru2 O7 C22A O8 2.8(15) . .
Ru2 O7 C22A C23A -168.7(8) . .
Ru2 O7 C22A C23B 156(3) . .
Ru2 O8 C22A O7 -2.0(16) 2_665 .
Ru2 O8 C22A C23A 168.3(11) 2_665 .
Ru2 O8 C22A C23B -161(2) 2_665 .
O7 C22A C23A C23B -130(4) . .
O8 C22A C23A C23B 58(4) . .
O7 C22A C23A C28A -159.3(12) . .
O8 C22A C23A C28A 29.0(19) . .
C23B C22A C23A C28A -29(4) . .
O7 C22A C23A C24A 24(2) . .
O8 C22A C23A C24A -147.4(17) . .
C23B C22A C23A C24A 154(5) . .
C24B C23A C23B C28A 35(6) . .
C24A C23A C23B C28A 77(8) . .
C22A C23A C23B C28A -142(4) . .
C24B C23A C23B C28B 13(15) . .
C28A C23A C23B C28B -22(11) . .
C24A C23A C23B C28B 55(19) . .
C22A C23A C23B C28B -164(14) . .
C28A C23A C23B C24B -35(6) . .
C24A C23A C23B C24B 42(7) . .
C22A C23A C23B C24B -177(5) . .
C24B C23A C23B C22A 177(5) . .
C28A C23A C23B C22A 142(4) . .
C24A C23A C23B C22A -141(6) . .
O7 C22A C23B C23A 68(4) . .
O8 C22A C23B C23A -134(3) . .
O7 C22A C23B C28A 134(6) . .
O8 C22A C23B C28A -68(7) . .
C23A C22A C23B C28A 66(7) . .
O7 C22A C23B C28B -122(6) . .
O8 C22A C23B C28B 36(7) . .
C23A C22A C23B C28B 170(10) . .
O7 C22A C23B C24B 69(5) . .
O8 C22A C23B C24B -132(4) . .
C23A C22A C23B C24B 2(3) . .
C23B C23A C24A C24B -55(9) . .
C28A C23A C24A C24B 1(5) . .
C22A C23A C24A C24B 177(6) . .
C24B C23A C24A C25A 9(5) . .
C23B C23A C24A C25A -46(8) . .
C28A C23A C24A C25A 9(2) . .
C22A C23A C24A C25A -174.6(15) . .
C24B C23A C24A Cl10 -179(5) . .
C23B C23A C24A Cl10 126(8) . .
C28A C23A C24A Cl10 -178.7(13) . .
C22A C23A C24A Cl10 -2(3) . .
Cl14 Cl10 C24A C24B -119(8) 2_565 .
Cl14 Cl10 C24A C25A 54.1(18) 2_565 .
Cl14 Cl10 C24A C23A -118.1(16) 2_565 .
C23B C23A C24B C24A 153(5) . .
C28A C23A C24B C24A -179(5) . .
C23B C23A C24B C28A -27(5) . .
C24A C23A C24B C28A 179(5) . .
C28A C23A C24B C23B 27(5) . .
C24A C23A C24B C23B -153(5) . .
C23B C23A C24B C25B -5(15) . .
C28A C23A C24B C25B 23(12) . .
C24A C23A C24B C25B -158(16) . .
C23B C23A C24B C25A 142(9) . .
C28A C23A C24B C25A 169(11) . .
C24A C23A C24B C25A -12(7) . .
C23B C23A C24B C27A -22(8) . .
C28A C23A C24B C27A 5(4) . .
C24A C23A C24B C27A -176(8) . .
C23B C23A C24B C26A -4(26) . .
C28A C23A C24B C26A 23(23) . .
C24A C23A C24B C26A -157(27) . .
C25A C24A C24B C23A -172(4) . .
Cl10 C24A C24B C23A 1(11) . .
C25A C24A C24B C23B -149(6) . .
C23A C24A C24B C23B 24(4) . .
Cl10 C24A C24B C23B 25(12) . .
C25A C24A C24B C25B -3(4) . .
C23A C24A C24B C25B 169(8) . .
Cl10 C24A C24B C25B 171(5) . .
C23A C24A C24B C25A 172(4) . .
Cl10 C24A C24B C25A 174(8) . .
C25A C24A C24B C27A 3(5) . .
C23A C24A C24B C27A 175(9) . .
Cl10 C24A C24B C27A 177(3) . .
C25A C24A C24B C26A 2(2) . .
C23A C24A C24B C26A 175(6) . .
Cl10 C24A C24B C26A 176(6) . .
C28A C23B C24B C23A -140(7) . .
C28B C23B C24B C23A -173(8) . .
C22A C23B C24B C23A -3(5) . .
C23A C23B C24B C24A -37(6) . .
C28A C23B C24B C24A -177(6) . .
C28B C23B C24B C24A 150(6) . .
C22A C23B C24B C24A -40(7) . .
C23A C23B C24B C28A 140(7) . .
C28B C23B C24B C28A -33(5) . .
C22A C23B C24B C28A 137(5) . .
C23A C23B C24B C25B 178(8) . .
C28A C23B C24B C25B 37(4) . .
C28B C23B C24B C25B 5(8) . .
C22A C23B C24B C25B 175(4) . .
C23A C23B C24B C25A -129(14) . .
C28A C23B C24B C25A 91(11) . .
C28B C23B C24B C25A 58(14) . .
C22A C23B C24B C25A -132(10) . .
C23A C23B C24B C27A 163(6) . .
C28A C23B C24B C27A 23(2) . .
C28B C23B C24B C27A -10(6) . .
C22A C23B C24B C27A 160(3) . .
C23A C23B C24B C26A 179(8) . .
C28A C23B C24B C26A 39(4) . .
C28B C23B C24B C26A 6(8) . .
C22A C23B C24B C26A 176(3) . .
C24B C24A C25A C26A -3(3) . .
C23A C24A C25A C26A -8(3) . .
Cl10 C24A C25A C26A 179.4(14) . .
C24B C24A C25A C25B 3(4) . .
C23A C24A C25A C25B -2(3) . .
Cl10 C24A C25A C25B -174(2) . .
C24B C24A C25A Cl15 -44(4) . .
C23A C24A C25A Cl15 -48(4) . .
Cl10 C24A C25A Cl15 139(3) . .
C24B C24A C25A Cl11 175(3) . .
C23A C24A C25A Cl11 170.9(14) . .
Cl10 C24A C25A Cl11 -2(2) . .
C23A C24A C25A C24B -5(3) . .
Cl10 C24A C25A C24B -177(4) . .
C26A Cl15 C25A C24A 61(3) . .
C25B Cl15 C25A C24A 53(4) . .
Cl11 Cl15 C25A C24A -148(3) . .
C27A Cl15 C25A C24A 48(3) . .
C25B Cl15 C25A C26A -8(3) . .
Cl11 Cl15 C25A C26A 151.3(16) . .
C27A Cl15 C25A C26A -13.5(14) . .
C26A Cl15 C25A C25B 8(3) . .
Cl11 Cl15 C25A C25B 160(2) . .
C27A Cl15 C25A C25B -5(2) . .
C26A Cl15 C25A Cl11 -151.3(16) . .
C25B Cl15 C25A Cl11 -160(2) . .
C27A Cl15 C25A Cl11 -164.8(9) . .
C26A Cl15 C25A C24B 32(2) . .
C25B Cl15 C25A C24B 24(3) . .
Cl11 Cl15 C25A C24B -176(2) . .
C27A Cl15 C25A C24B 19(2) . .
Cl13 Cl11 C25A C24A -58.2(18) 2_565 .
Cl15 Cl11 C25A C24A 160(2) . .
Cl13 Cl11 C25A C26A 120.5(15) 2_565 .
Cl15 Cl11 C25A C26A -21.3(12) . .
Cl13 Cl11 C25A C25B 109(4) 2_565 .
Cl15 Cl11 C25A C25B -33(4) . .
Cl13 Cl11 C25A Cl15 141.8(8) 2_565 .
Cl13 Cl11 C25A C24B -49(7) 2_565 .
Cl15 Cl11 C25A C24B 169(7) . .
C23A C24B C25A C24A 14(8) . .
C28A C24B C25A C24A -180(7) . .
C23B C24B C25A C24A 112(12) . .
C25B C24B C25A C24A 176(5) . .
C27A C24B C25A C24A -178(4) . .
C26A C24B C25A C24A -177(3) . .
C23A C24B C25A C26A -169(11) . .
C24A C24B C25A C26A 177(3) . .
C28A C24B C25A C26A -3(4) . .
C23B C24B C25A C26A -71(11) . .
C25B C24B C25A C26A -7(3) . .
C27A C24B C25A C26A -1.0(15) . .
C23A C24B C25A C25B -162(12) . .
C24A C24B C25A C25B -176(5) . .
C28A C24B C25A C25B 4(4) . .
C23B C24B C25A C25B -64(11) . .
C27A C24B C25A C25B 6(3) . .
C26A C24B C25A C25B 7(3) . .
C23A C24B C25A Cl15 170(10) . .
C24A C24B C25A Cl15 156(2) . .
C28A C24B C25A Cl15 -24(5) . .
C23B C24B C25A Cl15 -92(11) . .
C25B C24B C25A Cl15 -28(3) . .
C27A C24B C25A Cl15 -22(2) . .
C26A C24B C25A Cl15 -21.0(14) . .
C23A C24B C25A Cl11 2(16) . .
C24A C24B C25A Cl11 -12(8) . .
C28A C24B C25A Cl11 168(4) . .
C23B C24B C25A Cl11 100(12) . .
C25B C24B C25A Cl11 164(6) . .
C27A C24B C25A Cl11 170(5) . .
C26A C24B C25A Cl11 171(6) . .
C23A C24B C25B C26A 179(13) . .
C24A C24B C25B C26A 23(12) . .
C28A C24B C25B C26A -158(11) . .
C23B C24B C25B C26A 176(10) . .
C25A C24B C25B C26A 19(9) . .
C27A C24B C25B C26A -147(15) . .
C23A C24B C25B C27A -34(16) . .
C24A C24B C25B C27A 170(6) . .
C28A C24B C25B C27A -10(5) . .
C23B C24B C25B C27A -37(8) . .
C25A C24B C25B C27A 167(7) . .
C26A C24B C25B C27A 147(15) . .
C23A C24B C25B C26B 10(17) . .
C24A C24B C25B C26B -147(6) . .
C28A C24B C25B C26B 33(6) . .
C23B C24B C25B C26B 6(8) . .
C25A C24B C25B C26B -150(7) . .
C27A C24B C25B C26B 43(5) . .
C26A C24B C25B C26B -169(15) . .
C23A C24B C25B C25A 160(14) . .
C24A C24B C25B C25A 3(4) . .
C28A C24B C25B C25A -177(3) . .
C23B C24B C25B C25A 156(5) . .
C27A C24B C25B C25A -167(7) . .
C26A C24B C25B C25A -19(9) . .
C23A C24B C25B C28A -23(12) . .
C24A C24B C25B C28A -180(6) . .
C23B C24B C25B C28A -27(3) . .
C25A C24B C25B C28A 177(3) . .
C27A C24B C25B C28A 10(5) . .
C26A C24B C25B C28A 158(11) . .
C23A C24B C25B Cl15 -173(12) . .
C24A C24B C25B Cl15 30(7) . .
C28A C24B C25B Cl15 -150(4) . .
C23B C24B C25B Cl15 -176(4) . .
C25A C24B C25B Cl15 27(3) . .
C27A C24B C25B Cl15 -139(9) . .
C26A C24B C25B Cl15 8(7) . .
C24A C25A C25B C26A -167(5) . .
Cl15 C25A C25B C26A -13(4) . .
Cl11 C25A C25B C26A 24(8) . .
C24B C25A C25B C26A -165(7) . .
C24A C25A C25B C27A -71(25) . .
C26A C25A C25B C27A 96(27) . .
Cl15 C25A C25B C27A 83(25) . .
Cl11 C25A C25B C27A 120(23) . .
C24B C25A C25B C27A -69(24) . .
C24A C25A C25B C26B 123(8) . .
C26A C25A C25B C26B -70(8) . .
Cl15 C25A C25B C26B -82(8) . .
Cl11 C25A C25B C26B -46(11) . .
C24B C25A C25B C26B 126(10) . .
C24A C25A C25B C24B -2(3) . .
C26A C25A C25B C24B 165(7) . .
Cl15 C25A C25B C24B 152(3) . .
Cl11 C25A C25B C24B -171(3) . .
C24A C25A C25B C28A -5(4) . .
C26A C25A C25B C28A 162(8) . .
Cl15 C25A C25B C28A 149(4) . .
Cl11 C25A C25B C28A -174.1(18) . .
C24B C25A C25B C28A -3(3) . .
C24A C25A C25B Cl15 -154.5(16) . .
C26A C25A C25B Cl15 13(4) . .
Cl11 C25A C25B Cl15 36(4) . .
C24B C25A C25B Cl15 -152(3) . .
C25A Cl15 C25B C26A 124(19) . .
Cl11 Cl15 C25B C26A 108(18) . .
C27A Cl15 C25B C26A -72(17) . .
C26A Cl15 C25B C27A 72(17) . .
C25A Cl15 C25B C27A -164(7) . .
Cl11 Cl15 C25B C27A 180(5) . .
C26A Cl15 C25B C26B 22(15) . .
C25A Cl15 C25B C26B 147(6) . .
Cl11 Cl15 C25B C26B 130(4) . .
C27A Cl15 C25B C26B -49(5) . .
C26A Cl15 C25B C24B -155(21) . .
C25A Cl15 C25B C24B -31(4) . .
Cl11 Cl15 C25B C24B -47(5) . .
C27A Cl15 C25B C24B 133(9) . .
C26A Cl15 C25B C25A -124(19) . .
Cl11 Cl15 C25B C25A -16.3(18) . .
C27A Cl15 C25B C25A 164(7) . .
C26A Cl15 C25B C28A 146(25) . .
C25A Cl15 C25B C28A -90(9) . .
Cl11 Cl15 C25B C28A -106(9) . .
C27A Cl15 C25B C28A 74(10) . .
C27A C25B C26A Cl15 -115(16) . .
C26B C25B C26A Cl15 -159(14) . .
C24B C25B C26A Cl15 29(25) . .
C25A C25B C26A Cl15 50(17) . .
C28A C25B C26A Cl15 -60(38) . .
C26B C25B C26A C27A -44(6) . .
C24B C25B C26A C27A 145(15) . .
C25A C25B C26A C27A 165(7) . .
C28A C25B C26A C27A 55(24) . .
Cl15 C25B C26A C27A 115(16) . .
C27A C25B C26A C25A -165(7) . .
C26B C25B C26A C25A 151(5) . .
C24B C25B C26A C25A -20(9) . .
C28A C25B C26A C25A -110(26) . .
Cl15 C25B C26A C25A -50(17) . .
C27A C25B C26A C26B 44(6) . .
C24B C25B C26A C26B -171(13) . .
C25A C25B C26A C26B -151(5) . .
C28A C25B C26A C26B 99(27) . .
Cl15 C25B C26A C26B 159(14) . .
C27A C25B C26A C24B -145(15) . .
C26B C25B C26A C24B 171(13) . .
C25A C25B C26A C24B 20(9) . .
C28A C25B C26A C24B -90(26) . .
Cl15 C25B C26A C24B -29(25) . .
C25A Cl15 C26A C25B -51(18) . .
Cl11 Cl15 C26A C25B -74(18) . .
C27A Cl15 C26A C25B 81(17) . .
C25A Cl15 C26A C27A -133(5) . .
C25B Cl15 C26A C27A -81(17) . .
Cl11 Cl15 C26A C27A -156(4) . .
C25B Cl15 C26A C25A 51(18) . .
Cl11 Cl15 C26A C25A -23.0(12) . .
C27A Cl15 C26A C25A 133(5) . .
C25A Cl15 C26A C26B 159(5) . .
C25B Cl15 C26A C26B -150(20) . .
Cl11 Cl15 C26A C26B 136(4) . .
C27A Cl15 C26A C26B -68(6) . .
C25A Cl15 C26A C24B -32(2) . .
C25B Cl15 C26A C24B 19(17) . .
Cl11 Cl15 C26A C24B -55(3) . .
C27A Cl15 C26A C24B 100(5) . .
C24A C25A C26A C25B 15(6) . .
Cl15 C25A C26A C25B 162(6) . .
Cl11 C25A C26A C25B -164(5) . .
C24B C25A C26A C25B 13(6) . .
C24A C25A C26A Cl15 -147.7(18) . .
C25B C25A C26A Cl15 -162(6) . .
Cl11 C25A C26A Cl15 33.5(18) . .
C24B C25A C26A Cl15 -150(2) . .
C24A C25A C26A C27A 4(3) . .
C25B C25A C26A C27A -11(5) . .
Cl15 C25A C26A C27A 152(3) . .
Cl11 C25A C26A C27A -174.9(18) . .
C24B C25A C26A C27A 2(3) . .
C24A C25A C26A C26B 49(4) . .
C25B C25A C26A C26B 35(6) . .
Cl15 C25A C26A C26B -163(4) . .
Cl11 C25A C26A C26B -130(3) . .
C24B C25A C26A C26B 47(4) . .
C24A C25A C26A C24B 2(2) . .
C25B C25A C26A C24B -13(6) . .
Cl15 C25A C26A C24B 150(2) . .
Cl11 C25A C26A C24B -177(2) . .
C26A C25B C26B C27A 114(9) . .
C24B C25B C26B C27A -73(7) . .
C25A C25B C26B C27A 175(12) . .
C28A C25B C26B C27A -49(4) . .
Cl15 C25B C26B C27A 109(7) . .
C26A C25B C26B C27B -180(7) . .
C27A C25B C26B C27B 66(7) . .
C24B C25B C26B C27B -8(9) . .
C25A C25B C26B C27B -119(8) . .
C28A C25B C26B C27B 17(6) . .
Cl15 C25B C26B C27B 175(4) . .
C26A C25B C26B Cl12 84(7) . .
C27A C25B C26B Cl12 -31(5) . .
C24B C25B C26B Cl12 -104(6) . .
C25A C25B C26B Cl12 144(7) . .
C28A C25B C26B Cl12 -80(3) . .
Cl15 C25B C26B Cl12 78(5) . .
C27A C25B C26B C26A -114(9) . .
C24B C25B C26B C26A 172(11) . .
C25A C25B C26B C26A 61(7) . .
C28A C25B C26B C26A -163(8) . .
Cl15 C25B C26B C26A -5(4) . .
C26A C25B C26B C28A 163(8) . .
C27A C25B C26B C28A 49(4) . .
C24B C25B C26B C28A -25(4) . .
C25A C25B C26B C28A -136(10) . .
Cl15 C25B C26B C28A 158(5) . .
C27B Cl12 C26B C27A 98(4) . .
C27A Cl12 C26B C27B -98(4) . .
C27A Cl12 C26B C25B 17(3) . .
C27B Cl12 C26B C25B 115(5) . .
C27A Cl12 C26B C26A 41(2) . .
C27B Cl12 C26B C26A 139(4) . .
C27A Cl12 C26B C28A -37(2) . .
C27B Cl12 C26B C28A 62(3) . .
C25B C26A C26B C27A -44(7) . .
Cl15 C26A C26B C27A 123(5) . .
C25A C26A C26B C27A -87(5) . .
C24B C26A C26B C27A -48(3) . .
C25B C26A C26B C27B 0(9) . .
Cl15 C26A C26B C27B 167(6) . .
C27A C26A C26B C27B 44(6) . .
C25A C26A C26B C27B -43(9) . .
C24B C26A C26B C27B -4(7) . .
Cl15 C26A C26B C25B 166(9) . .
C27A C26A C26B C25B 44(7) . .
C25A C26A C26B C25B -43(7) . .
C24B C26A C26B C25B -5(7) . .
C25B C26A C26B Cl12 -104(8) . .
Cl15 C26A C26B Cl12 62(5) . .
C27A C26A C26B Cl12 -61(3) . .
C25A C26A C26B Cl12 -148(2) . .
C24B C26A C26B Cl12 -109(3) . .
C25B C26A C26B C28A -14(7) . .
Cl15 C26A C26B C28A 152(4) . .
C27A C26A C26B C28A 30(2) . .
C25A C26A C26B C28A -57(3) . .
C24B C26A C26B C28A -19(2) . .
C26A C25B C27A C26B -80(9) . .
C24B C25B C27A C26B 126(5) . .
C25A C25B C27A C26B -170(23) . .
C28A C25B C27A C26B 116(4) . .
Cl15 C25B C27A C26B -95(6) . .
C26B C25B C27A C26A 80(9) . .
C24B C25B C27A C26A -154(11) . .
C25A C25B C27A C26A -89(27) . .
C28A C25B C27A C26A -164(7) . .
Cl15 C25B C27A C26A -15(4) . .
C26A C25B C27A C28A 164(7) . .
C26B C25B C27A C28A -116(4) . .
C24B C25B C27A C28A 9(5) . .
C25A C25B C27A C28A 74(25) . .
Cl15 C25B C27A C28A 149(4) . .
C26A C25B C27A Cl12 -23(16) . .
C26B C25B C27A Cl12 57(9) . .
C24B C25B C27A Cl12 -178(6) . .
C25A C25B C27A Cl12 -113(21) . .
C28A C25B C27A Cl12 173(10) . .
Cl15 C25B C27A Cl12 -38(13) . .
C26A C25B C27A C27B -128(7) . .
C26B C25B C27A C27B -48(4) . .
C24B C25B C27A C27B 78(6) . .
C25A C25B C27A C27B 143(22) . .
C28A C25B C27A C27B 69(3) . .
Cl15 C25B C27A C27B -142(4) . .
C26A C25B C27A C24B 154(11) . .
C26B C25B C27A C24B -126(5) . .
C25A C25B C27A C24B 65(23) . .
C28A C25B C27A C24B -9(5) . .
Cl15 C25B C27A C24B 140(8) . .
C26A C25B C27A Cl15 15(4) . .
C26B C25B C27A Cl15 95(6) . .
C24B C25B C27A Cl15 -140(8) . .
C25A C25B C27A Cl15 -75(25) . .
C28A C25B C27A Cl15 -149(4) . .
C27B C26B C27A C25B -123(6) . .
Cl12 C26B C27A C25B 151(5) . .
C26A C26B C27A C25B 29(4) . .
C28A C26B C27A C25B -101(5) . .
C27B C26B C27A C26A -152(4) . .
C25B C26B C27A C26A -29(4) . .
Cl12 C26B C27A C26A 123(2) . .
C28A C26B C27A C26A -130(4) . .
C27B C26B C27A C28A -22(6) . .
C25B C26B C27A C28A 101(5) . .
Cl12 C26B C27A C28A -108(3) . .
C26A C26B C27A C28A 130(4) . .
C27B C26B C27A Cl12 86(4) . .
C25B C26B C27A Cl12 -151(5) . .
C26A C26B C27A Cl12 -123(2) . .
C28A C26B C27A Cl12 108(3) . .
C25B C26B C27A C27B 123(6) . .
Cl12 C26B C27A C27B -86(4) . .
C26A C26B C27A C27B 152(4) . .
C28A C26B C27A C27B 22(6) . .
C27B C26B C27A C24B -73(6) . .
C25B C26B C27A C24B 50(5) . .
Cl12 C26B C27A C24B -159(3) . .
C26A C26B C27A C24B 78(4) . .
C28A C26B C27A C24B -51(3) . .
C27B C26B C27A Cl15 -165(4) . .
C25B C26B C27A Cl15 -42(4) . .
Cl12 C26B C27A Cl15 109.2(17) . .
C26A C26B C27A Cl15 -13.5(12) . .
C28A C26B C27A Cl15 -143(4) . .
Cl15 C26A C27A C25B 139(10) . .
C25A C26A C27A C25B 18(9) . .
C26B C26A C27A C25B -104(9) . .
C24B C26A C27A C25B 20(9) . .
C25B C26A C27A C26B 104(9) . .
Cl15 C26A C27A C26B -116(5) . .
C25A C26A C27A C26B 123(4) . .
C24B C26A C27A C26B 124(4) . .
C25B C26A C27A C28A -19(9) . .
Cl15 C26A C27A C28A 120(4) . .
C25A C26A C27A C28A -1(3) . .
C26B C26A C27A C28A -124(4) . .
C24B C26A C27A C28A 1(2) . .
C25B C26A C27A Cl12 166(9) . .
Cl15 C26A C27A Cl12 -54(5) . .
C25A C26A C27A Cl12 -175.4(16) . .
C26B C26A C27A Cl12 62(3) . .
C24B C26A C27A Cl12 -174(3) . .
C25B C26A C27A C27B 74(9) . .
Cl15 C26A C27A C27B -147(4) . .
C25A C26A C27A C27B 92(4) . .
C26B C26A C27A C27B -31(4) . .
C24B C26A C27A C27B 94(4) . .
C25B C26A C27A C24B -20(9) . .
Cl15 C26A C27A C24B 119(4) . .
C25A C26A C27A C24B -2(3) . .
C26B C26A C27A C24B -124(4) . .
C25B C26A C27A Cl15 -139(10) . .
C25A C26A C27A Cl15 -121(5) . .
C26B C26A C27A Cl15 116(5) . .
C24B C26A C27A Cl15 -119(4) . .
C26B Cl12 C27A C25B -67(10) . .
C27B Cl12 C27A C25B -119(10) . .
C27B Cl12 C27A C26B -52(3) . .
C26B Cl12 C27A C26A -80(4) . .
C27B Cl12 C27A C26A -132(3) . .
C26B Cl12 C27A C28A 106(4) . .
C27B Cl12 C27A C28A 53(2) . .
C26B Cl12 C27A C27B 52(3) . .
C26B Cl12 C27A C24B 119(8) . .
C27B Cl12 C27A C24B 66(6) . .
C26B Cl12 C27A Cl15 -92(4) . .
C27B Cl12 C27A Cl15 -145(2) . .
C23A C24B C27A C25B 160(10) . .
C24A C24B C27A C25B -14(8) . .
C28A C24B C27A C25B 167(7) . .
C23B C24B C27A C25B 146(7) . .
C25A C24B C27A C25B -11(6) . .
C26A C24B C27A C25B -12(6) . .
C23A C24B C27A C26B 85(8) . .
C24A C24B C27A C26B -89(7) . .
C28A C24B C27A C26B 91(5) . .
C23B C24B C27A C26B 70(6) . .
C25B C24B C27A C26B -76(7) . .
C25A C24B C27A C26B -87(5) . .
C26A C24B C27A C26B -88(5) . .
C23A C24B C27A C26A 173(7) . .
C24A C24B C27A C26A -1(6) . .
C28A C24B C27A C26A 179(3) . .
C23B C24B C27A C26A 158(3) . .
C25B C24B C27A C26A 12(6) . .
C25A C24B C27A C26A 1.1(17) . .
C23A C24B C27A C28A -6(5) . .
C24A C24B C27A C28A 180(7) . .
C23B C24B C27A C28A -21(3) . .
C25B C24B C27A C28A -167(7) . .
C25A C24B C27A C28A -178(3) . .
C26A C24B C27A C28A -179(3) . .
C23A C24B C27A Cl12 -23(12) . .
C24A C24B C27A Cl12 163(4) . .
C28A C24B C27A Cl12 -17(7) . .
C23B C24B C27A Cl12 -38(8) . .
C25B C24B C27A Cl12 176(9) . .
C25A C24B C27A Cl12 165(5) . .
C26A C24B C27A Cl12 164(7) . .
C23A C24B C27A C27B 38(7) . .
C24A C24B C27A C27B -136(6) . .
C28A C24B C27A C27B 44(3) . .
C23B C24B C27A C27B 23(4) . .
C25B C24B C27A C27B -122(7) . .
C25A C24B C27A C27B -134(2) . .
C26A C24B C27A C27B -135(3) . .
C23A C24B C27A Cl15 -174(7) . .
C24A C24B C27A Cl15 12(6) . .
C28A C24B C27A Cl15 -168(2) . .
C23B C24B C27A Cl15 171(3) . .
C25B C24B C27A Cl15 25(6) . .
C25A C24B C27A Cl15 14.0(15) . .
C26A C24B C27A Cl15 12.9(11) . .
C27A C26B C27B C28B 28(8) . .
C25B C26B C27B C28B -3(9) . .
Cl12 C26B C27B C28B 109(6) . .
C26A C26B C27B C28B -3(11) . .
C28A C26B C27B C28B 13(5) . .
C27A C26B C27B Cl14 -150(4) . .
C25B C26B C27B Cl14 178(4) . .
Cl12 C26B C27B Cl14 -69(4) . .
C26A C26B C27B Cl14 178(5) . .
C28A C26B C27B Cl14 -166(5) . .
C25B C26B C27B C27A -31(3) . .
Cl12 C26B C27B C27A 81(4) . .
C26A C26B C27B C27A -31(4) . .
C28A C26B C27B C27A -15(4) . .
C27A C26B C27B C28A 15(4) . .
C25B C26B C27B C28A -16(5) . .
Cl12 C26B C27B C28A 97(2) . .
C26A C26B C27B C28A -16(7) . .
C27A C26B C27B Cl12 -81(4) . .
C25B C26B C27B Cl12 -112(6) . .
C26A C26B C27B Cl12 -112(7) . .
C28A C26B C27B Cl12 -97(2) . .
Cl10 Cl14 C27B C28B 104(6) 2_565 .
Cl10 Cl14 C27B C26B -78(5) 2_565 .
Cl10 Cl14 C27B C27A -103(5) 2_565 .
Cl10 Cl14 C27B C28A 156(13) 2_565 .
Cl10 Cl14 C27B Cl12 -124.5(18) 2_565 .
C25B C27A C27B C28B -81(6) . .
C26B C27A C27B C28B -157(7) . .
C26A C27A C27B C28B -114(4) . .
C28A C27A C27B C28B 2(4) . .
Cl12 C27A C27B C28B 132(4) . .
C24B C27A C27B C28B -30(4) . .
Cl15 C27A C27B C28B -129(4) . .
C25B C27A C27B C26B 76(7) . .
C26A C27A C27B C26B 43(6) . .
C28A C27A C27B C26B 158(6) . .
Cl12 C27A C27B C26B -72(5) . .
C24B C27A C27B C26B 126(5) . .
Cl15 C27A C27B C26B 28(6) . .
C25B C27A C27B Cl14 121(7) . .
C26B C27A C27B Cl14 45(6) . .
C26A C27A C27B Cl14 88(7) . .
C28A C27A C27B Cl14 -156(6) . .
Cl12 C27A C27B Cl14 -26(5) . .
C24B C27A C27B Cl14 172(5) . .
Cl15 C27A C27B Cl14 73(7) . .
C25B C27A C27B C28A -82(5) . .
C26B C27A C27B C28A -158(6) . .
C26A C27A C27B C28A -116(3) . .
Cl12 C27A C27B C28A 129.6(19) . .
C24B C27A C27B C28A -32(2) . .
Cl15 C27A C27B C28A -131(4) . .
C25B C27A C27B Cl12 148(5) . .
C26B C27A C27B Cl12 72(5) . .
C26A C27A C27B Cl12 115(3) . .
C28A C27A C27B Cl12 -129.6(19) . .
C24B C27A C27B Cl12 -162(2) . .
Cl15 C27A C27B Cl12 100(4) . .
C23A C23B C28A C24B -20(3) . .
C28B C23B C28A C24B 150(4) . .
C22A C23B C28A C24B -80(7) . .
C23A C23B C28A C28B -169(5) . .
C24B C23B C28A C28B -150(4) . .
C22A C23B C28A C28B 131(7) . .
C23A C23B C28A C27A -76(7) . .
C28B C23B C28A C27A 94(6) . .
C24B C23B C28A C27A -56(6) . .
C22A C23B C28A C27A -136(5) . .
C28B C23B C28A C23A 169(5) . .
C24B C23B C28A C23A 20(3) . .
C22A C23B C28A C23A -60(6) . .
C23A C23B C28A C25B -54(5) . .
C28B C23B C28A C25B 115(4) . .
C24B C23B C28A C25B -35(4) . .
C22A C23B C28A C25B -114(6) . .
C23A C23B C28A C27B -143(3) . .
C28B C23B C28A C27B 26(3) . .
C24B C23B C28A C27B -124(3) . .
C22A C23B C28A C27B 157(6) . .
C23A C23B C28A C26B -105(4) . .
C28B C23B C28A C26B 64(4) . .
C24B C23B C28A C26B -86(4) . .
C22A C23B C28A C26B -165(5) . .
C23A C24B C28A C23B 26(4) . .
C25B C24B C28A C23B -143(4) . .
C25A C24B C28A C23B -147(5) . .
C27A C24B C28A C23B -149(3) . .
C26A C24B C28A C23B -149(4) . .
C23A C24B C28A C28B 63(5) . .
C23B C24B C28A C28B 38(4) . .
C25B C24B C28A C28B -106(4) . .
C25A C24B C28A C28B -109(5) . .
C27A C24B C28A C28B -112(3) . .
C26A C24B C28A C28B -111(3) . .
C23A C24B C28A C27A 175(4) . .
C23B C24B C28A C27A 149(3) . .
C25B C24B C28A C27A 6(3) . .
C25A C24B C28A C27A 2(4) . .
C26A C24B C28A C27A 0.5(17) . .
C23B C24B C28A C23A -26(4) . .
C25B C24B C28A C23A -169(6) . .
C25A C24B C28A C23A -172(8) . .
C27A C24B C28A C23A -175(4) . .
C26A C24B C28A C23A -174(5) . .
C23A C24B C28A C25B 169(6) . .
C23B C24B C28A C25B 143(4) . .
C25A C24B C28A C25B -3(4) . .
C27A C24B C28A C25B -6(3) . .
C26A C24B C28A C25B -5(3) . .
C23A C24B C28A C27B 120(4) . .
C23B C24B C28A C27B 94(4) . .
C25B C24B C28A C27B -49(4) . .
C25A C24B C28A C27B -53(6) . .
C27A C24B C28A C27B -55(3) . .
C26A C24B C28A C27B -55(4) . .
C23A C24B C28A C26B 151(4) . .
C23B C24B C28A C26B 125(4) . .
C25B C24B C28A C26B -18(3) . .
C25A C24B C28A C26B -22(5) . .
C27A C24B C28A C26B -24.3(19) . .
C26A C24B C28A C26B -24(2) . .
C25B C27A C28A C23B 42(8) . .
C26B C27A C28A C23B -64(8) . .
C26A C27A C28A C23B 51(7) . .
Cl12 C27A C28A C23B -134(6) . .
C27B C27A C28A C23B -81(7) . .
C24B C27A C28A C23B 52(7) . .
Cl15 C27A C28A C23B 67(7) . .
C25B C27A C28A C24B -10(5) . .
C26B C27A C28A C24B -116(5) . .
C26A C27A C28A C24B -1(3) . .
Cl12 C27A C28A C24B 174(3) . .
C27B C27A C28A C24B -133(3) . .
Cl15 C27A C28A C24B 15(3) . .
C25B C27A C28A C28B 121(6) . .
C26B C27A C28A C28B 16(5) . .
C26A C27A C28A C28B 130(4) . .
Cl12 C27A C28A C28B -55(3) . .
C27B C27A C28A C28B -2(4) . .
C24B C27A C28A C28B 131(4) . .
Cl15 C27A C28A C28B 146(3) . .
C25B C27A C28A C23A -7(5) . .
C26B C27A C28A C23A -112(4) . .
C26A C27A C28A C23A 2(3) . .
Cl12 C27A C28A C23A 176.8(13) . .
C27B C27A C28A C23A -130(3) . .
C24B C27A C28A C23A 3(2) . .
Cl15 C27A C28A C23A 18(3) . .
C26B C27A C28A C25B -105(6) . .
C26A C27A C28A C25B 9(4) . .
Cl12 C27A C28A C25B -176(6) . .
C27B C27A C28A C25B -123(5) . .
C24B C27A C28A C25B 10(5) . .
Cl15 C27A C28A C25B 26(4) . .
C25B C27A C28A C27B 123(5) . .
C26B C27A C28A C27B 17(5) . .
C26A C27A C28A C27B 132(3) . .
Cl12 C27A C28A C27B -53(2) . .
C24B C27A C28A C27B 133(3) . .
Cl15 C27A C28A C27B 148(3) . .
C25B C27A C28A C26B 105(6) . .
C26A C27A C28A C26B 115(5) . .
Cl12 C27A C28A C26B -71(4) . .
C27B C27A C28A C26B -17(5) . .
C24B C27A C28A C26B 116(5) . .
Cl15 C27A C28A C26B 131(5) . .
C24B C23A C28A C23B -143(6) . .
C24A C23A C28A C23B -144(4) . .
C22A C23A C28A C23B 39(4) . .
C23B C23A C28A C24B 143(6) . .
C24A C23A C28A C24B -1(4) . .
C22A C23A C28A C24B -177(5) . .
C24B C23A C28A C28B -133(5) . .
C23B C23A C28A C28B 11(5) . .
C24A C23A C28A C28B -133(3) . .
C22A C23A C28A C28B 50(3) . .
C24B C23A C28A C27A -6(5) . .
C23B C23A C28A C27A 138(4) . .
C24A C23A C28A C27A -6(2) . .
C22A C23A C28A C27A 176.9(15) . .
C24B C23A C28A C25B -9(5) . .
C23B C23A C28A C25B 134(5) . .
C24A C23A C28A C25B -10(3) . .
C22A C23A C28A C25B 173(2) . .
C24B C23A C28A C27B -88(5) . .
C23B C23A C28A C27B 56(5) . .
C24A C23A C28A C27B -88(3) . .
C22A C23A C28A C27B 95(3) . .
C24B C23A C28A C26B -36(5) . .
C23B C23A C28A C26B 107(5) . .
C24A C23A C28A C26B -37(3) . .
C22A C23A C28A C26B 146(2) . .
C26A C25B C28A C23B 145(26) . .
C27A C25B C28A C23B -152(6) . .
C26B C25B C28A C23B -113(5) . .
C24B C25B C28A C23B 40(5) . .
C25A C25B C28A C23B 43(6) . .
Cl15 C25B C28A C23B 117(9) . .
C26A C25B C28A C24B 105(27) . .
C27A C25B C28A C24B 168(6) . .
C26B C25B C28A C24B -153(5) . .
C25A C25B C28A C24B 3(4) . .
Cl15 C25B C28A C24B 77(9) . .
C26A C25B C28A C28B -135(25) . .
C27A C25B C28A C28B -72(6) . .
C26B C25B C28A C28B -33(5) . .
C24B C25B C28A C28B 120(5) . .
C25A C25B C28A C28B 123(4) . .
Cl15 C25B C28A C28B -163(8) . .
C26A C25B C28A C27A -63(25) . .
C26B C25B C28A C27A 39(4) . .
C24B C25B C28A C27A -168(6) . .
C25A C25B C28A C27A -165(8) . .
Cl15 C25B C28A C27A -91(10) . .
C26A C25B C28A C23A 111(26) . .
C27A C25B C28A C23A 174(5) . .
C26B C25B C28A C23A -147(3) . .
C24B C25B C28A C23A 6(3) . .
C25A C25B C28A C23A 9(4) . .
Cl15 C25B C28A C23A 83(9) . .
C26A C25B C28A C27B -113(26) . .
C27A C25B C28A C27B -50(5) . .
C26B C25B C28A C27B -11(4) . .
C24B C25B C28A C27B 142(4) . .
C25A C25B C28A C27B 145(4) . .
Cl15 C25B C28A C27B -141(9) . .
C26A C25B C28A C26B -102(27) . .
C27A C25B C28A C26B -39(4) . .
C24B C25B C28A C26B 153(5) . .
C25A C25B C28A C26B 156(6) . .
Cl15 C25B C28A C26B -130(11) . .
C28B C27B C28A C23B -36(5) . .
C26B C27B C28A C23B 129(5) . .
Cl14 C27B C28A C23B -100(13) . .
C27A C27B C28A C23B 141(4) . .
Cl12 C27B C28A C23B -180(3) . .
C28B C27B C28A C24B -113(5) . .
C26B C27B C28A C24B 52(5) . .
Cl14 C27B C28A C24B -177(11) . .
C27A C27B C28A C24B 64(4) . .
Cl12 C27B C28A C24B 103(4) . .
C26B C27B C28A C28B 165(6) . .
Cl14 C27B C28A C28B -64(12) . .
C27A C27B C28A C28B 177(5) . .
Cl12 C27B C28A C28B -144(5) . .
C28B C27B C28A C27A -177(5) . .
C26B C27B C28A C27A -12(3) . .
Cl14 C27B C28A C27A 118(13) . .
Cl12 C27B C28A C27A 38.8(15) . .
C28B C27B C28A C23A -72(5) . .
C26B C27B C28A C23A 93(4) . .
Cl14 C27B C28A C23A -136(11) . .
C27A C27B C28A C23A 105(3) . .
Cl12 C27B C28A C23A 144(2) . .
C28B C27B C28A C25B -153(5) . .
C26B C27B C28A C25B 12(4) . .
Cl14 C27B C28A C25B 143(13) . .
C27A C27B C28A C25B 24(2) . .
Cl12 C27B C28A C25B 63(3) . .
C28B C27B C28A C26B -165(6) . .
Cl14 C27B C28A C26B 131(14) . .
C27A C27B C28A C26B 12(3) . .
Cl12 C27B C28A C26B 51(3) . .
C26B C27B C28B C28A -17(7) . .
Cl14 C27B C28B C28A 161(5) . .
C27A C27B C28B C28A -2(4) . .
Cl12 C27B C28B C28A 45(5) . .
C26B C27B C28B C23B 15(11) . .
Cl14 C27B C28B C23B -167(5) . .
C27A C27B C28B C23B 30(7) . .
C28A C27B C28B C23B 32(5) . .
Cl12 C27B C28B C23B 77(8) . .
C26B C27B C28B Cl13 163(5) . .
Cl14 C27B C28B Cl13 -18(7) . .
C27A C27B C28B Cl13 179(3) . .
C28A C27B C28B Cl13 -179(6) . .
Cl12 C27B C28B Cl13 -134(4) . .
C23B C28A C28B C27B 142(5) . .
C24B C28A C28B C27B 104(5) . .
C27A C28A C28B C27B 3(5) . .
C23A C28A C28B C27B 134(4) . .
C25B C28A C28B C27B 32(6) . .
C26B C28A C28B C27B 10(4) . .
C24B C28A C28B C23B -38(4) . .
C27A C28A C28B C23B -140(4) . .
C23A C28A C28B C23B -8(3) . .
C25B C28A C28B C23B -110(4) . .
C27B C28A C28B C23B -142(5) . .
C26B C28A C28B C23B -133(4) . .
C23B C28A C28B Cl13 -39(10) . .
C24B C28A C28B Cl13 -78(12) . .
C27A C28A C28B Cl13 -179(10) . .
C23A C28A C28B Cl13 -47(12) . .
C25B C28A C28B Cl13 -150(9) . .
C27B C28A C28B Cl13 178(14) . .
C26B C28A C28B Cl13 -172(11) . .
C23A C23B C28B C27B -24(18) . .
C28A C23B C28B C27B -48(7) . .
C24B C23B C28B C27B -16(10) . .
C22A C23B C28B C27B 178(5) . .
C23A C23B C28B C28A 24(12) . .
C24B C23B C28B C28A 32(5) . .
C22A C23B C28B C28A -134(7) . .
C23A C23B C28B Cl13 -172(11) . .
C28A C23B C28B Cl13 164(4) . .
C24B C23B C28B Cl13 -164(4) . .
C22A C23B C28B Cl13 30(9) . .
C29 C30 C32 C35 -16.9(12) . .
C31 C30 C32 C35 153.5(8) . .
C29 C30 C32 C33 161.9(8) . .
C31 C30 C32 C33 -27.7(13) . .
C35 C32 C33 C35 -1.6(13) . 2_666
C30 C32 C33 C35 179.7(8) . 2_666
C35 C32 C33 C34 174.4(8) . .
C30 C32 C33 C34 -4.4(13) . .
C33 C32 C35 C33 1.6(14) . 2_666
C30 C32 C35 C33 -179.5(8) . 2_666
C17A Cl7A C17B C18B -117(36) . .
C17A Cl7A C17B C16 52(31) . .
C18B Cl7A C17B C16 169(9) . .
C17A Cl7A C17B C18A -107(37) . .
C18B Cl7A C17B C18A 10(3) . .
C18A C18B C17B Cl7A 167(4) . .
Cl8A C18B C17B Cl7A 23(21) . .
C17A C18B C17B Cl7A 164(11) . .
C19B C18B C17B Cl7A 167(4) . .
Cl9B C18B C17B Cl7A -12(6) . .
C18A C18B C17B C16 -4(6) . .
Cl8A C18B C17B C16 -148(17) . .
C17A C18B C17B C16 -7(4) . .
C19B C18B C17B C16 -4(7) . .
Cl9B C18B C17B C16 177(3) . .
Cl7A C18B C17B C16 -171(7) . .
Cl8A C18B C17B C18A -144(22) . .
C17A C18B C17B C18A -2(9) . .
C19B C18B C17B C18A 0(3) . .
Cl9B C18B C17B C18A -179(7) . .
Cl7A C18B C17B C18A -167(4) . .
C21B C16 C17B Cl7A -162(6) . .
C17A C16 C17B Cl7A -157(16) . .
C21A C16 C17B Cl7A -170(4) . .
C15 C16 C17B Cl7A 15(6) . .
C21B C16 C17B C18B 6(6) . .
C17A C16 C17B C18B 11(7) . .
C21A C16 C17B C18B -3(7) . .
C15 C16 C17B C18B -177(4) . .
C21B C16 C17B C18A 4(4) . .
C17A C16 C17B C18A 9(9) . .
C21A C16 C17B C18A -5(4) . .
C15 C16 C17B C18A -179.1(14) . .
C18B C18A C17B Cl7A -18(6) . .
C19A C18A C17B Cl7A 171(4) . .
C20B C18A C17B Cl7A 158(6) . .
C17A C18A C17B Cl7A 159(14) . .
Cl8A C18A C17B Cl7A -12(6) . .
C19A C18A C17B C18B -171(5) . .
C20B C18A C17B C18B 176(5) . .
C17A C18A C17B C18B 177(11) . .
Cl8A C18A C17B C18B 7(4) . .
C18B C18A C17B C16 176(5) . .
C19A C18A C17B C16 5(4) . .
C20B C18A C17B C16 -8(5) . .
C17A C18A C17B C16 -7(7) . .
Cl8A C18A C17B C16 -177.0(16) . .
