#------------------------------------------------------------------------------
#$Date: 2020-10-31 01:49:47 +0200 (Sat, 31 Oct 2020) $
#$Revision: 258656 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/13/53/4135328.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4135328
loop_
_publ_author_name
'Kim, Jinwoo'
'Kim, Dongwook'
'Chang, Sukbok'
_publ_section_title
;
 Merging Two Functions in a Single Rh Catalyst System: Bimodular Conjugate
 for Light-Induced Oxidative Coupling
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_paper_doi               10.1021/jacs.0c09982
_journal_year                    2020
_chemical_formula_sum            'C44 H43 F18 N Rh Sb3'
_chemical_formula_weight         1395.95
_space_group_crystal_system      monoclinic
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yc'
_space_group_name_H-M_alt        'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                90
_cell_angle_beta                 108.36(3)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   36.655(7)
_cell_length_b                   9.3680(19)
_cell_length_c                   32.952(7)
_cell_measurement_reflns_used    105077
_cell_measurement_temperature    253(2)
_cell_measurement_theta_max      34.001
_cell_measurement_theta_min      0.487
_cell_volume                     10739(4)
_computing_cell_refinement       HKL3000sm
_computing_data_collection       'PAL BL2D-SMDC Program'
_computing_data_reduction        HKL3000sm
_computing_structure_refinement  SHELXL
_computing_structure_solution    SHELXS
_diffrn_ambient_temperature      253(2)
_diffrn_measured_fraction_theta_full 0.973
_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'Rayonix MX225HS CCD area detector'
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.850
_diffrn_reflns_av_R_equivalents  0.0895
_diffrn_reflns_av_unetI/netI     0.0877
_diffrn_reflns_Laue_measured_fraction_full 0.973
_diffrn_reflns_Laue_measured_fraction_max 0.973
_diffrn_reflns_limit_h_max       42
_diffrn_reflns_limit_h_min       -42
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            60520
_diffrn_reflns_point_group_measured_fraction_full 0.973
_diffrn_reflns_point_group_measured_fraction_max 0.973
_diffrn_reflns_theta_full        29.498
_diffrn_reflns_theta_max         29.498
_diffrn_reflns_theta_min         1.493
_diffrn_source                   'PLSII 2D bending magnet'
_exptl_absorpt_coefficient_mu    3.015
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.853
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'HKL3000sm Scalepack'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.727
_exptl_crystal_description       needle
_exptl_crystal_F_000             5392
_exptl_crystal_size_max          0.021
_exptl_crystal_size_mid          0.019
_exptl_crystal_size_min          0.014
_refine_diff_density_max         1.172
_refine_diff_density_min         -1.745
_refine_diff_density_rms         0.174
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.071
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1327
_refine_ls_number_reflns         17020
_refine_ls_number_restraints     2771
_refine_ls_restrained_S_all      1.088
_refine_ls_R_factor_all          0.2163
_refine_ls_R_factor_gt           0.1155
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3295
_refine_ls_wR_factor_ref         0.3865
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5870
_reflns_number_total             17020
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ja0c09982_si_004.cif
_cod_data_source_block           P20012_013_sq
_cod_original_sg_symbol_H-M      'P 2/c'
_cod_database_code               4135328
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.939
_shelx_estimated_absorpt_t_max   0.959
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1A Rh 0.94972(4) 0.6810(2) 0.39023(5) 0.1260(6) Uani 1 1 d . U . . .
C2A C 0.9185(4) 0.5528(11) 0.3336(4) 0.114(5) Uani 1 1 d DG U . . .
C3A C 0.9533(3) 0.6011(15) 0.3278(4) 0.124(6) Uani 1 1 d DG U . . .
C4A C 0.9531(3) 0.7527(15) 0.3283(4) 0.120(6) Uani 1 1 d DG U . . .
C5A C 0.9182(4) 0.7981(11) 0.3343(4) 0.117(6) Uani 1 1 d DG U . . .
C6A C 0.8968(3) 0.6745(16) 0.3376(4) 0.114(6) Uani 1 1 d G U . . .
C7A C 0.9085(6) 0.3937(14) 0.3271(7) 0.144(7) Uani 1 1 d D U . . .
H7AA H 0.884147 0.376221 0.332020 0.216 Uiso 1 1 calc R U . . .
H7AB H 0.906520 0.366418 0.298085 0.216 Uiso 1 1 calc R U . . .
H7AC H 0.928487 0.337826 0.347095 0.216 Uiso 1 1 calc R U . . .
C8A C 0.9884(5) 0.516(2) 0.3255(6) 0.142(7) Uani 1 1 d D U . . .
H8AA H 1.007532 0.580914 0.321402 0.213 Uiso 1 1 calc R U . . .
H8AB H 0.999332 0.463399 0.351990 0.213 Uiso 1 1 calc R U . . .
H8AC H 0.980588 0.449385 0.301796 0.213 Uiso 1 1 calc R U . . .
C9A C 0.9841(6) 0.851(2) 0.3205(7) 0.161(9) Uani 1 1 d D U . . .
H9AA H 0.977215 0.949686 0.322508 0.242 Uiso 1 1 calc R U . . .
H9AB H 1.008742 0.831163 0.341770 0.242 Uiso 1 1 calc R U . . .
H9AC H 0.985949 0.832470 0.292172 0.242 Uiso 1 1 calc R U . . .
C10A C 0.9059(5) 0.9556(14) 0.3337(5) 0.124(6) Uani 1 1 d D U . . .
H10A H 0.926409 1.016686 0.331213 0.186 Uiso 1 1 calc R U . . .
H10B H 0.882931 0.971784 0.309595 0.186 Uiso 1 1 calc R U . . .
H10C H 0.900497 0.977603 0.360067 0.186 Uiso 1 1 calc R U . . .
C11A C 0.8569(2) 0.6736(13) 0.3393(4) 0.098(5) Uani 1 1 d G U . . .
C12A C 0.8469(3) 0.6025(12) 0.3713(3) 0.106(5) Uani 1 1 d G U . . .
H12A H 0.865907 0.555685 0.393301 0.127 Uiso 1 1 calc R U . . .
C13A C 0.8089(3) 0.6008(13) 0.3709(3) 0.116(6) Uani 1 1 d G U . . .
H13A H 0.802133 0.552810 0.392536 0.139 Uiso 1 1 calc R U . . .
C14A C 0.7808(2) 0.6701(14) 0.3384(4) 0.117(6) Uani 1 1 d G U . . .
C15A C 0.7908(3) 0.7411(13) 0.3064(3) 0.108(5) Uani 1 1 d G U . . .
H15A H 0.771773 0.787987 0.284423 0.130 Uiso 1 1 calc R U . . .
C16A C 0.8288(3) 0.7428(13) 0.3068(3) 0.121(6) Uani 1 1 d G U . . .
H16A H 0.835547 0.790865 0.285187 0.145 Uiso 1 1 calc R U . . .
N17A N 0.7408(4) 0.6742(17) 0.3392(4) 0.114(4) Uani 1 1 d . U . . .
C18A C 0.7294(4) 0.8011(13) 0.3539(4) 0.104(5) Uani 1 1 d G U . . .
C19A C 0.7542(3) 0.9159(16) 0.3680(4) 0.126(6) Uani 1 1 d G U . . .
H19A H 0.780012 0.908761 0.368781 0.151 Uiso 1 1 calc R U . . .
C20A C 0.7409(4) 1.0412(13) 0.3811(3) 0.118(6) Uani 1 1 d G U . . .
H20A H 0.757684 1.118792 0.390601 0.141 Uiso 1 1 calc R U . . .
C21A C 0.7028(4) 1.0517(13) 0.3800(4) 0.145(7) Uani 1 1 d G U . . .
H21A H 0.693780 1.136472 0.388768 0.174 Uiso 1 1 calc R U . . .
C22A C 0.6780(3) 0.9370(17) 0.3659(4) 0.137(7) Uani 1 1 d G U . . .
H22A H 0.652202 0.944119 0.365113 0.164 Uiso 1 1 calc R U . . .
C23A C 0.6913(4) 0.8117(14) 0.3528(4) 0.136(7) Uani 1 1 d G U . . .
C24A C 0.6665(5) 0.684(2) 0.3408(5) 0.110(5) Uani 1 1 d . U . . .
C25A C 0.6818(4) 0.5593(13) 0.3297(4) 0.108(5) Uani 1 1 d G U . . .
C26A C 0.6589(3) 0.4383(17) 0.3188(4) 0.126(6) Uani 1 1 d G U . . .
H26A H 0.633710 0.439403 0.320377 0.151 Uiso 1 1 calc R U . . .
C27A C 0.6731(4) 0.3156(13) 0.3054(4) 0.153(8) Uani 1 1 d G U . . .
H27A H 0.657605 0.233699 0.298033 0.183 Uiso 1 1 calc R U . . .
C28A C 0.7103(4) 0.3139(13) 0.3031(4) 0.125(6) Uani 1 1 d G U . . .
H28A H 0.719948 0.230912 0.294054 0.150 Uiso 1 1 calc R U . . .
C29A C 0.7332(3) 0.4350(16) 0.3140(4) 0.139(7) Uani 1 1 d G U . . .
H29A H 0.758399 0.433828 0.312419 0.167 Uiso 1 1 calc R U . . .
C30A C 0.7190(3) 0.5577(13) 0.3274(4) 0.103(5) Uani 1 1 d G U . . .
C31A C 0.6255(3) 0.6963(15) 0.3418(5) 0.130(6) Uani 1 1 d G U . . .
C32A C 0.6164(4) 0.6576(15) 0.3781(4) 0.119(6) Uani 1 1 d DG U . . .
C33A C 0.5781(4) 0.6446(15) 0.3764(4) 0.131(6) Uani 1 1 d G U . . .
H33A H 0.571976 0.618417 0.400969 0.157 Uiso 1 1 calc R U . . .
C34A C 0.5490(3) 0.6705(17) 0.3382(6) 0.196(11) Uani 1 1 d DG U . . .
C35A C 0.5582(4) 0.7092(18) 0.3019(4) 0.169(9) Uani 1 1 d G U . . .
H35A H 0.538459 0.726680 0.276090 0.203 Uiso 1 1 calc R U . . .
C36A C 0.5964(5) 0.7221(16) 0.3037(4) 0.139(7) Uani 1 1 d DG U . . .
C37A C 0.6437(7) 0.618(3) 0.4223(6) 0.227(12) Uani 1 1 d D U . . .
H37A H 0.670098 0.628360 0.422389 0.340 Uiso 1 1 calc R U . . .
H37B H 0.639264 0.681053 0.443627 0.340 Uiso 1 1 calc R U . . .
H37C H 0.639185 0.520128 0.428845 0.340 Uiso 1 1 calc R U . . .
C38A C 0.5060(5) 0.656(4) 0.3348(11) 0.255(15) Uani 1 1 d D U . . .
H38A H 0.503912 0.628760 0.362320 0.383 Uiso 1 1 calc R U . . .
H38B H 0.493211 0.746920 0.326094 0.383 Uiso 1 1 calc R U . . .
H38C H 0.494074 0.583862 0.313707 0.383 Uiso 1 1 calc R U . . .
C39A C 0.6038(7) 0.776(3) 0.2632(5) 0.183(9) Uani 1 1 d D U . . .
H39A H 0.631248 0.781179 0.267969 0.274 Uiso 1 1 calc R U . . .
H39B H 0.592108 0.711590 0.239703 0.274 Uiso 1 1 calc R U . . .
H39C H 0.592650 0.870663 0.256181 0.274 Uiso 1 1 calc R U . . .
C40A C 0.9950(5) 0.7944(17) 0.4441(4) 0.135(7) Uani 1 1 d G U . . .
H40A H 1.009776 0.874358 0.437276 0.162 Uiso 1 1 calc R U . . .
C41A C 0.9600(5) 0.8214(14) 0.4506(4) 0.205(12) Uani 1 1 d G U . . .
H41A H 0.949882 0.920153 0.447688 0.246 Uiso 1 1 calc R U . . .
C42A C 0.9362(3) 0.709(2) 0.4533(4) 0.136(7) Uani 1 1 d G U . . .
H42A H 0.909469 0.728566 0.452535 0.164 Uiso 1 1 calc R U . . .
C43A C 0.9474(4) 0.5690(17) 0.4493(4) 0.165(8) Uani 1 1 d G U . . .
H43A H 0.928849 0.490123 0.446976 0.198 Uiso 1 1 calc R U . . .
C44A C 0.9824(5) 0.5419(14) 0.4427(4) 0.142(7) Uani 1 1 d G U . . .
H44A H 0.988890 0.443514 0.436533 0.171 Uiso 1 1 calc R U . . .
C45A C 1.0062(4) 0.655(2) 0.4401(4) 0.164(9) Uani 1 1 d DG U . . .
C46A C 1.0463(5) 0.632(3) 0.4340(9) 0.228(13) Uani 1 1 d D U . . .
H46A H 1.058177 0.723384 0.432954 0.342 Uiso 1 1 calc R U . . .
H46B H 1.062526 0.576270 0.457725 0.342 Uiso 1 1 calc R U . . .
H46C H 1.043091 0.580555 0.407462 0.342 Uiso 1 1 calc R U . . .
Rh1C Rh 0.81891(4) 0.87759(16) 0.57834(5) 0.1085(5) Uani 1 1 d . U . . .
C2C C 0.7753(3) 0.8039(12) 0.5208(3) 0.101(5) Uani 1 1 d DG U . . .
C3C C 0.8123(4) 0.7602(15) 0.5204(4) 0.122(6) Uani 1 1 d DG U . . .
C4C C 0.8284(3) 0.6709(14) 0.5564(4) 0.119(6) Uani 1 1 d DG U . . .
C5C C 0.8014(4) 0.6594(13) 0.5791(3) 0.110(5) Uani 1 1 d DG U . . .
C6C C 0.7686(3) 0.7416(14) 0.5570(4) 0.104(5) Uani 1 1 d G U . . .
C7C C 0.7477(5) 0.8924(18) 0.4855(5) 0.136(7) Uani 1 1 d D U . . .
H7CA H 0.760253 0.920692 0.464864 0.205 Uiso 1 1 calc R U . . .
H7CB H 0.725062 0.835978 0.471253 0.205 Uiso 1 1 calc R U . . .
H7CC H 0.740084 0.976913 0.497820 0.205 Uiso 1 1 calc R U . . .
C8C C 0.8333(5) 0.796(2) 0.4870(5) 0.138(7) Uani 1 1 d D U . . .
H8CA H 0.817239 0.857996 0.465178 0.206 Uiso 1 1 calc R U . . .
H8CB H 0.857499 0.842662 0.501307 0.206 Uiso 1 1 calc R U . . .
H8CC H 0.838127 0.707840 0.473944 0.206 Uiso 1 1 calc R U . . .
C9C C 0.8672(4) 0.591(2) 0.5708(7) 0.149(7) Uani 1 1 d D U . . .
H9CA H 0.881528 0.612218 0.551323 0.224 Uiso 1 1 calc R U . . .
H9CB H 0.881919 0.620543 0.599470 0.224 Uiso 1 1 calc R U . . .
H9CC H 0.862518 0.488676 0.570632 0.224 Uiso 1 1 calc R U . . .
C10C C 0.8056(5) 0.5727(19) 0.6204(4) 0.122(6) Uani 1 1 d D U . . .
H10D H 0.782610 0.584454 0.628689 0.183 Uiso 1 1 calc R U . . .
H10E H 0.809028 0.472493 0.615148 0.183 Uiso 1 1 calc R U . . .
H10F H 0.827719 0.606955 0.643145 0.183 Uiso 1 1 calc R U . . .
C11C C 0.7334(3) 0.7441(14) 0.5685(4) 0.096(5) Uani 1 1 d G U . . .
C12C C 0.7172(3) 0.8712(11) 0.5763(4) 0.130(6) Uani 1 1 d G U . . .
H12C H 0.730387 0.957827 0.577218 0.156 Uiso 1 1 calc R U . . .
C13C C 0.6815(4) 0.8703(12) 0.5827(4) 0.137(7) Uani 1 1 d G U . . .
H13C H 0.670539 0.956298 0.587986 0.165 Uiso 1 1 calc R U . . .
C14C C 0.6620(3) 0.7423(16) 0.5814(4) 0.119(6) Uani 1 1 d DG U . . .
C15C C 0.6782(3) 0.6152(12) 0.5736(4) 0.113(5) Uani 1 1 d G U . . .
H15C H 0.664987 0.528563 0.572709 0.136 Uiso 1 1 calc R U . . .
C16C C 0.7139(3) 0.6161(12) 0.5672(4) 0.120(6) Uani 1 1 d G U . . .
H16C H 0.724835 0.530088 0.561940 0.144 Uiso 1 1 calc R U . . .
N17C N 0.6227(3) 0.7409(15) 0.5823(4) 0.112(4) Uani 1 1 d D U . . .
C18C C 0.5928(3) 0.7819(13) 0.5479(3) 0.099(5) Uani 1 1 d DG U . . .
C19C C 0.5994(3) 0.8149(13) 0.5096(4) 0.107(5) Uani 1 1 d G U . . .
H19C H 0.624372 0.809054 0.507672 0.128 Uiso 1 1 calc R U . . .
C20C C 0.5690(4) 0.8567(13) 0.4743(3) 0.134(7) Uani 1 1 d G U . . .
H20C H 0.573441 0.878974 0.448435 0.161 Uiso 1 1 calc R U . . .
C21C C 0.5320(3) 0.8654(13) 0.4772(4) 0.125(6) Uani 1 1 d G U . . .
H21C H 0.511495 0.893573 0.453286 0.150 Uiso 1 1 calc R U . . .
C22C C 0.5255(3) 0.8324(14) 0.5154(4) 0.136(7) Uani 1 1 d G U . . .
H22C H 0.500477 0.838250 0.517374 0.163 Uiso 1 1 calc R U . . .
C23C C 0.5559(4) 0.7906(13) 0.5508(3) 0.110(5) Uani 1 1 d G U . . .
C24C C 0.5497(5) 0.7554(19) 0.5904(6) 0.105(5) Uani 1 1 d . U . . .
C25C C 0.5806(4) 0.7025(16) 0.6245(4) 0.136(7) Uani 1 1 d G U . . .
C26C C 0.5745(4) 0.6480(16) 0.6611(5) 0.144(7) Uani 1 1 d G U . . .
H26C H 0.549578 0.646655 0.663374 0.173 Uiso 1 1 calc R U . . .
C27C C 0.6053(5) 0.5954(17) 0.6942(4) 0.185(10) Uani 1 1 d G U . . .
H27C H 0.601160 0.558556 0.718954 0.223 Uiso 1 1 calc R U . . .
C28C C 0.6421(4) 0.5974(17) 0.6908(4) 0.193(10) Uani 1 1 d G U . . .
H28C H 0.662907 0.561844 0.713215 0.232 Uiso 1 1 calc R U . . .
C29C C 0.6482(3) 0.6519(16) 0.6542(5) 0.140(7) Uani 1 1 d G U . . .
H29C H 0.673070 0.653228 0.651894 0.168 Uiso 1 1 calc R U . . .
C30C C 0.6174(4) 0.7045(16) 0.6211(4) 0.131(7) Uani 1 1 d DG U . . .
C31C C 0.5101(3) 0.7654(17) 0.5933(4) 0.120(6) Uani 1 1 d G U . . .
C32C C 0.5027(4) 0.8817(14) 0.6157(4) 0.148(7) Uani 1 1 d DG U . . .
C33C C 0.4658(5) 0.9043(14) 0.6176(5) 0.176(9) Uani 1 1 d G U . . .
H33C H 0.460830 0.982942 0.632793 0.211 Uiso 1 1 calc R U . . .
C34C C 0.4364(3) 0.8107(18) 0.5972(5) 0.156(8) Uani 1 1 d DG U . . .
C35C C 0.4438(4) 0.6944(16) 0.5748(5) 0.149(7) Uani 1 1 d G U . . .
H35C H 0.423847 0.631092 0.560937 0.178 Uiso 1 1 calc R U . . .
C36C C 0.4807(4) 0.6718(13) 0.5728(4) 0.131(6) Uani 1 1 d DG U . . .
C37C C 0.5322(6) 0.998(2) 0.6374(7) 0.164(8) Uani 1 1 d D U . . .
H37D H 0.519455 1.072730 0.648131 0.246 Uiso 1 1 calc R U . . .
H37E H 0.543300 1.037501 0.616777 0.246 Uiso 1 1 calc R U . . .
H37F H 0.552357 0.955937 0.660958 0.246 Uiso 1 1 calc R U . . .
C38C C 0.3976(6) 0.844(3) 0.6049(10) 0.220(12) Uani 1 1 d D U . . .
H38D H 0.400158 0.931565 0.621446 0.330 Uiso 1 1 calc R U . . .
H38E H 0.377689 0.856386 0.577640 0.330 Uiso 1 1 calc R U . . .
H38F H 0.390856 0.766240 0.620473 0.330 Uiso 1 1 calc R U . . .
C39C C 0.4864(6) 0.546(2) 0.5456(6) 0.165(8) Uani 1 1 d D U . . .
H39D H 0.513166 0.541211 0.546767 0.247 Uiso 1 1 calc R U . . .
H39E H 0.479345 0.457614 0.556618 0.247 Uiso 1 1 calc R U . . .
H39F H 0.470360 0.559002 0.516189 0.247 Uiso 1 1 calc R U . . .
C40C C 0.8134(4) 1.0323(17) 0.6298(5) 0.168(8) Uani 1 1 d G U . . .
H40C H 0.792056 1.020628 0.641850 0.201 Uiso 1 1 calc R U . . .
C41C C 0.8076(3) 1.1111(14) 0.5925(5) 0.126(6) Uani 1 1 d G U . . .
H41C H 0.782140 1.154063 0.578252 0.151 Uiso 1 1 calc R U . . .
C42C C 0.8352(5) 1.1097(14) 0.5716(4) 0.134(7) Uani 1 1 d G U . . .
H42C H 0.829197 1.152706 0.542820 0.161 Uiso 1 1 calc R U . . .
C43C C 0.8685(4) 1.0295(17) 0.5880(5) 0.145(7) Uani 1 1 d G U . . .
H43C H 0.886301 1.017731 0.570987 0.174 Uiso 1 1 calc R U . . .
C44C C 0.8743(4) 0.9507(15) 0.6252(5) 0.139(7) Uani 1 1 d G U . . .
H44C H 0.896295 0.883981 0.634696 0.167 Uiso 1 1 calc R U . . .
C45C C 0.8467(5) 0.9521(15) 0.6461(4) 0.154(8) Uani 1 1 d DG U . . .
C46C C 0.8581(16) 0.873(6) 0.6896(10) 0.42(3) Uani 1 1 d D U . . .
H46D H 0.837177 0.879865 0.701699 0.634 Uiso 1 1 calc R U . . .
H46E H 0.863153 0.773628 0.685373 0.634 Uiso 1 1 calc R U . . .
H46F H 0.880957 0.916723 0.709003 0.634 Uiso 1 1 calc R U . . .
Sb1E Sb 0.90387(4) 0.67330(16) 0.19914(4) 0.1154(5) Uani 1 1 d D U . . .
F2E F 0.9537(2) 0.6543(12) 0.2313(3) 0.145(4) Uani 1 1 d D U . . .
F3E F 0.8893(4) 0.5851(17) 0.2393(4) 0.229(7) Uani 1 1 d D U . . .
F4E F 0.8543(2) 0.6973(11) 0.1659(3) 0.140(4) Uani 1 1 d D U . . .
F5E F 0.9174(4) 0.7693(16) 0.1593(4) 0.225(7) Uani 1 1 d D U . . .
F6E F 0.9011(4) 0.8396(12) 0.2256(4) 0.219(7) Uani 1 1 d D U . . .
F7E F 0.9042(4) 0.5044(10) 0.1758(4) 0.208(6) Uani 1 1 d D U . . .
Sb1F Sb 0.75249(5) 0.39110(17) 0.46867(5) 0.1408(6) Uani 1 1 d D U . . .
F2F F 0.7701(4) 0.2086(11) 0.4715(5) 0.205(6) Uani 1 1 d D U . . .
F3F F 0.7084(4) 0.3267(19) 0.4721(6) 0.267(8) Uani 1 1 d D U . . .
F4F F 0.7348(4) 0.5671(13) 0.4673(5) 0.232(7) Uani 1 1 d D U . . .
F5F F 0.8007(3) 0.4544(16) 0.4739(6) 0.241(7) Uani 1 1 d D U . . .
F6F F 0.7709(4) 0.3951(14) 0.5267(3) 0.193(5) Uani 1 1 d D U . . .
F7F F 0.7404(6) 0.392(2) 0.4150(4) 0.279(9) Uani 1 1 d D U . . .
Sb1G Sb 0.60089(18) 0.2544(7) 0.5755(2) 0.183(3) Uani 0.765(18) 1 d D U P A 1
F2G F 0.5617(6) 0.170(2) 0.5353(6) 0.235(11) Uani 0.765(18) 1 d D U P A 1
F3G F 0.5918(5) 0.4214(16) 0.5499(7) 0.175(8) Uani 0.765(18) 1 d D U P A 1
F4G F 0.6392(8) 0.328(3) 0.6183(8) 0.40(2) Uani 0.765(18) 1 d D U P A 1
F5G F 0.6117(5) 0.0824(15) 0.6019(6) 0.167(7) Uani 0.765(18) 1 d D U P A 1
F6G F 0.6317(6) 0.212(2) 0.5447(7) 0.228(10) Uani 0.765(18) 1 d D U P A 1
F7G F 0.5713(7) 0.288(2) 0.6063(8) 0.251(12) Uani 0.765(18) 1 d D U P A 1
Sb1H Sb 0.8733(4) 1.1778(17) 0.4444(5) 0.142(2) Uani 0.422(9) 1 d D U P B 1
F2H F 0.8389(7) 1.248(3) 0.3965(7) 0.167(5) Uani 0.422(9) 1 d D U P B 1
F3H F 0.9114(6) 1.202(3) 0.4236(9) 0.165(5) Uani 0.422(9) 1 d D U P B 1
F4H F 0.9062(7) 1.098(3) 0.4913(7) 0.175(5) Uani 0.422(9) 1 d D U P B 1
F5H F 0.8356(7) 1.145(3) 0.4669(9) 0.162(5) Uani 0.422(9) 1 d D U P B 1
F6H F 0.8643(7) 1.000(2) 0.4201(8) 0.159(5) Uani 0.422(9) 1 d D U P B 1
F7H F 0.8801(8) 1.336(2) 0.4710(8) 0.165(5) Uani 0.422(9) 1 d D U P B 1
Sb1I Sb 0.7845(4) 1.1747(16) 0.2392(4) 0.2050(16) Uani 0.518(8) 1 d D U P C 1
F2I F 0.7957(8) 1.251(3) 0.1939(7) 0.211(3) Uani 0.518(8) 1 d D U P C 1
F3I F 0.8314(5) 1.108(3) 0.2581(8) 0.211(3) Uani 0.518(8) 1 d D U P C 1
F4I F 0.7708(7) 1.102(3) 0.2822(7) 0.208(3) Uani 0.518(8) 1 d D U P C 1
F5I F 0.7373(5) 1.250(3) 0.2198(7) 0.211(3) Uani 0.518(8) 1 d D U P C 1
F6I F 0.8007(7) 1.334(2) 0.2714(8) 0.210(3) Uani 0.518(8) 1 d D U P C 1
F7I F 0.7657(7) 1.021(2) 0.2117(7) 0.215(3) Uani 0.518(8) 1 d D U P C 1
Sb1J Sb 1.0288(7) 1.182(3) 0.4115(7) 0.257(3) Uani 0.274(11) 1 d D U P D 1
F2J F 1.0712(11) 1.174(9) 0.401(2) 0.251(7) Uani 0.274(11) 1 d D U P D 1
F3J F 1.054(2) 1.293(6) 0.4516(16) 0.247(6) Uani 0.274(11) 1 d D U P D 1
F4J F 0.9964(17) 1.195(7) 0.439(2) 0.245(6) Uani 0.274(11) 1 d D U P D 1
F5J F 1.0088(16) 1.117(6) 0.3611(12) 0.253(4) Uani 0.274(11) 1 d D U P D 1
F6J F 1.0593(19) 1.042(6) 0.429(2) 0.236(7) Uani 0.274(11) 1 d D U P D 1
F7J F 1.0062(17) 1.332(4) 0.3865(16) 0.254(4) Uani 0.274(11) 1 d D U P D 1
Sb8G Sb 0.6013(4) 0.2517(15) 0.5743(3) 0.098(5) Uani 0.235(18) 1 d D U P A 2
F9G F 0.6075(12) 0.260(4) 0.6311(6) 0.14(2) Uani 0.235(18) 1 d D U P A 2
F10G F 0.5512(5) 0.230(4) 0.5643(13) 0.129(17) Uani 0.235(18) 1 d D U P A 2
F11G F 0.5950(12) 0.243(5) 0.5188(6) 0.16(2) Uani 0.235(18) 1 d D U P A 2
F12G F 0.6515(5) 0.277(4) 0.5862(12) 0.113(16) Uani 0.235(18) 1 d D U P A 2
F13G F 0.5950(13) 0.443(2) 0.5728(15) 0.21(4) Uani 0.235(18) 1 d D U P A 2
F14G F 0.6078(11) 0.070(2) 0.5761(13) 0.14(2) Uani 0.235(18) 1 d D U P A 2
Sb8H Sb 0.8789(3) 1.1807(12) 0.4470(3) 0.1331(17) Uani 0.578(9) 1 d D U P B 2
F9H F 0.8283(4) 1.181(2) 0.4190(7) 0.177(5) Uani 0.578(9) 1 d D U P B 2
F10H F 0.8682(6) 1.159(2) 0.4956(5) 0.162(4) Uani 0.578(9) 1 d D U P B 2
F11H F 0.9291(4) 1.183(2) 0.4755(6) 0.168(5) Uani 0.578(9) 1 d D U P B 2
F12H F 0.8887(6) 1.203(2) 0.3977(5) 0.172(5) Uani 0.578(9) 1 d D U P B 2
F13H F 0.8768(6) 1.3719(15) 0.4530(7) 0.172(5) Uani 0.578(9) 1 d D U P B 2
F14H F 0.8846(6) 0.9970(16) 0.4426(7) 0.174(5) Uani 0.578(9) 1 d D U P B 2
Sb8I Sb 0.7875(4) 1.1841(17) 0.2367(4) 0.2035(17) Uani 0.482(8) 1 d D U P C 2
F9I F 0.7443(6) 1.097(3) 0.2385(9) 0.210(3) Uani 0.482(8) 1 d D U P C 2
F10I F 0.7684(7) 1.163(3) 0.1796(5) 0.208(3) Uani 0.482(8) 1 d D U P C 2
F11I F 0.8300(6) 1.262(3) 0.2288(9) 0.210(3) Uani 0.482(8) 1 d D U P C 2
F12I F 0.8059(7) 1.194(3) 0.2922(5) 0.210(3) Uani 0.482(8) 1 d D U P C 2
F13I F 0.8100(8) 1.011(2) 0.2364(8) 0.213(3) Uani 0.482(8) 1 d D U P C 2
F14I F 0.7693(8) 1.355(2) 0.2317(9) 0.215(3) Uani 0.482(8) 1 d D U P C 2
Sb8J Sb 1.0309(2) 1.1738(10) 0.4271(2) 0.254(2) Uani 0.726(11) 1 d D U P D 2
F9J F 1.0442(6) 1.0060(17) 0.4103(7) 0.224(6) Uani 0.726(11) 1 d D U P D 2
F10J F 1.0464(7) 1.261(2) 0.3858(6) 0.244(5) Uani 0.726(11) 1 d D U P D 2
F11J F 1.0235(7) 1.3527(18) 0.4443(8) 0.261(6) Uani 0.726(11) 1 d D U P D 2
F12J F 1.0100(6) 1.105(2) 0.4633(6) 0.243(6) Uani 0.726(11) 1 d D U P D 2
F13J F 0.9843(5) 1.177(2) 0.3867(6) 0.245(5) Uani 0.726(11) 1 d D U P D 2
F14J F 1.0744(5) 1.192(3) 0.4645(6) 0.252(6) Uani 0.726(11) 1 d D U P D 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0051 0.0024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0095 0.0049 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0254 0.0152 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -0.7030 1.2730 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.2755 2.1319 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C5A Rh1A C6A 38.54(19) . . ?
C5A Rh1A C4A 38.2(2) . . ?
C6A Rh1A C4A 63.8(2) . . ?
C5A Rh1A C44A 173.7(5) . . ?
C6A Rh1A C44A 138.3(6) . . ?
C4A Rh1A C44A 137.8(6) . . ?
C5A Rh1A C2A 63.7(2) . . ?
C6A Rh1A C2A 37.90(19) . . ?
C4A Rh1A C2A 63.0(2) . . ?
C44A Rh1A C2A 110.6(5) . . ?
C5A Rh1A C3A 63.3(2) . . ?
C6A Rh1A C3A 63.1(2) . . ?
C4A Rh1A C3A 37.5(2) . . ?
C44A Rh1A C3A 110.6(5) . . ?
C2A Rh1A C3A 37.29(19) . . ?
C5A Rh1A C45A 145.1(6) . . ?
C6A Rh1A C45A 170.7(6) . . ?
C4A Rh1A C45A 114.4(5) . . ?
C44A Rh1A C45A 36.7(2) . . ?
C2A Rh1A C45A 132.9(6) . . ?
C3A Rh1A C45A 109.5(5) . . ?
C5A Rh1A C43A 146.1(6) . . ?
C6A Rh1A C43A 114.6(5) . . ?
C4A Rh1A C43A 169.9(6) . . ?
C44A Rh1A C43A 36.54(19) . . ?
C2A Rh1A C43A 109.2(4) . . ?
C3A Rh1A C43A 132.4(6) . . ?
C45A Rh1A C43A 65.5(3) . . ?
C5A Rh1A C40A 119.7(5) . . ?
C6A Rh1A C40A 152.9(6) . . ?
C4A Rh1A C40A 110.0(4) . . ?
C44A Rh1A C40A 65.1(3) . . ?
C2A Rh1A C40A 165.5(6) . . ?
C3A Rh1A C40A 129.4(5) . . ?
C45A Rh1A C40A 36.0(2) . . ?
C43A Rh1A C40A 76.1(2) . . ?
C5A Rh1A C42A 120.5(5) . . ?
C6A Rh1A C42A 109.6(4) . . ?
C4A Rh1A C42A 154.1(6) . . ?
C44A Rh1A C42A 64.8(3) . . ?
C2A Rh1A C42A 128.6(5) . . ?
C3A Rh1A C42A 164.5(6) . . ?
C45A Rh1A C42A 76.0(2) . . ?
C43A Rh1A C42A 35.67(18) . . ?
C40A Rh1A C42A 63.5(3) . . ?
C5A Rh1A C41A 110.3(4) . . ?
C6A Rh1A C41A 124.7(5) . . ?
C4A Rh1A C41A 125.8(5) . . ?
C44A Rh1A C41A 76.0(2) . . ?
C2A Rh1A C41A 159.3(6) . . ?
C3A Rh1A C41A 160.4(6) . . ?
C45A Rh1A C41A 64.2(3) . . ?
C43A Rh1A C41A 63.8(3) . . ?
C40A Rh1A C41A 35.23(19) . . ?
C42A Rh1A C41A 35.07(19) . . ?
C3A C2A C6A 108.0 . . ?
C3A C2A C7A 118.5(13) . . ?
C6A C2A C7A 132.6(13) . . ?
C3A C2A Rh1A 72.1(5) . . ?
C6A C2A Rh1A 69.0(5) . . ?
C7A C2A Rh1A 133.0(11) . . ?
C2A C3A C4A 108.0 . . ?
C2A C3A C8A 129.9(13) . . ?
C4A C3A C8A 121.9(13) . . ?
C2A C3A Rh1A 70.7(5) . . ?
C4A C3A Rh1A 69.7(5) . . ?
C8A C3A Rh1A 120.9(10) . . ?
C3A C4A C5A 108.0 . . ?
C3A C4A C9A 125.8(14) . . ?
C5A C4A C9A 126.1(14) . . ?
C3A C4A Rh1A 72.8(5) . . ?
C5A C4A Rh1A 69.2(5) . . ?
C9A C4A Rh1A 126.8(11) . . ?
C6A C5A C4A 108.0 . . ?
C6A C5A C10A 128.0(12) . . ?
C4A C5A C10A 123.9(12) . . ?
C6A C5A Rh1A 71.3(5) . . ?
C4A C5A Rh1A 72.6(5) . . ?
C10A C5A Rh1A 125.2(9) . . ?
C5A C6A C2A 108.0 . . ?
C5A C6A C11A 125.6(12) . . ?
C2A C6A C11A 126.0(12) . . ?
C5A C6A Rh1A 70.2(5) . . ?
C2A C6A Rh1A 73.1(5) . . ?
C11A C6A Rh1A 128.1(9) . . ?
C2A C7A H7AA 109.5 . . ?
C2A C7A H7AB 109.5 . . ?
H7AA C7A H7AB 109.5 . . ?
C2A C7A H7AC 109.5 . . ?
H7AA C7A H7AC 109.5 . . ?
H7AB C7A H7AC 109.5 . . ?
C3A C8A H8AA 109.5 . . ?
C3A C8A H8AB 109.5 . . ?
H8AA C8A H8AB 109.5 . . ?
C3A C8A H8AC 109.5 . . ?
H8AA C8A H8AC 109.5 . . ?
H8AB C8A H8AC 109.5 . . ?
C4A C9A H9AA 109.5 . . ?
C4A C9A H9AB 109.5 . . ?
H9AA C9A H9AB 109.5 . . ?
C4A C9A H9AC 109.5 . . ?
H9AA C9A H9AC 109.5 . . ?
H9AB C9A H9AC 109.5 . . ?
C5A C10A H10A 109.5 . . ?
C5A C10A H10B 109.5 . . ?
H10A C10A H10B 109.5 . . ?
C5A C10A H10C 109.5 . . ?
H10A C10A H10C 109.5 . . ?
H10B C10A H10C 109.5 . . ?
C12A C11A C16A 120.0 . . ?
C12A C11A C6A 122.1(9) . . ?
C16A C11A C6A 117.9(9) . . ?
C11A C12A C13A 120.0 . . ?
C11A C12A H12A 120.0 . . ?
C13A C12A H12A 120.0 . . ?
C14A C13A C12A 120.0 . . ?
C14A C13A H13A 120.0 . . ?
C12A C13A H13A 120.0 . . ?
C15A C14A C13A 120.0 . . ?
C15A C14A N17A 120.1(10) . . ?
C13A C14A N17A 119.9(10) . . ?
C14A C15A C16A 120.0 . . ?
C14A C15A H15A 120.0 . . ?
C16A C15A H15A 120.0 . . ?
C15A C16A C11A 120.0 . . ?
C15A C16A H16A 120.0 . . ?
C11A C16A H16A 120.0 . . ?
C30A N17A C18A 125.5(14) . . ?
C30A N17A C14A 118.7(14) . . ?
C18A N17A C14A 115.8(13) . . ?
C19A C18A C23A 120.0 . . ?
C19A C18A N17A 122.6(12) . . ?
C23A C18A N17A 117.3(12) . . ?
C20A C19A C18A 120.0 . . ?
C20A C19A H19A 120.0 . . ?
C18A C19A H19A 120.0 . . ?
C19A C20A C21A 120.0 . . ?
C19A C20A H20A 120.0 . . ?
C21A C20A H20A 120.0 . . ?
C22A C21A C20A 120.0 . . ?
C22A C21A H21A 120.0 . . ?
C20A C21A H21A 120.0 . . ?
C23A C22A C21A 120.0 . . ?
C23A C22A H22A 120.0 . . ?
C21A C22A H22A 120.0 . . ?
C22A C23A C18A 120.0 . . ?
C22A C23A C24A 121.3(12) . . ?
C18A C23A C24A 118.5(12) . . ?
C25A C24A C23A 118.9(15) . . ?
C25A C24A C31A 123.6(15) . . ?
C23A C24A C31A 117.5(15) . . ?
C24A C25A C26A 119.4(12) . . ?
C24A C25A C30A 120.5(12) . . ?
C26A C25A C30A 120.0 . . ?
C27A C26A C25A 120.0 . . ?
C27A C26A H26A 120.0 . . ?
C25A C26A H26A 120.0 . . ?
C28A C27A C26A 120.0 . . ?
C28A C27A H27A 120.0 . . ?
C26A C27A H27A 120.0 . . ?
C29A C28A C27A 120.0 . . ?
C29A C28A H28A 120.0 . . ?
C27A C28A H28A 120.0 . . ?
C28A C29A C30A 120.0 . . ?
C28A C29A H29A 120.0 . . ?
C30A C29A H29A 120.0 . . ?
N17A C30A C29A 121.2(12) . . ?
N17A C30A C25A 118.8(12) . . ?
C29A C30A C25A 120.0 . . ?
C32A C31A C36A 120.0 . . ?
C32A C31A C24A 120.5(12) . . ?
C36A C31A C24A 118.5(12) . . ?
C33A C32A C31A 120.0 . . ?
C33A C32A C37A 111.7(16) . . ?
C31A C32A C37A 128.3(16) . . ?
C32A C33A C34A 120.0 . . ?
C32A C33A H33A 120.0 . . ?
C34A C33A H33A 120.0 . . ?
C35A C34A C33A 120.0 . . ?
C35A C34A C38A 118.3(18) . . ?
C33A C34A C38A 121.7(18) . . ?
C36A C35A C34A 120.0 . . ?
C36A C35A H35A 120.0 . . ?
C34A C35A H35A 120.0 . . ?
C35A C36A C31A 120.0 . . ?
C35A C36A C39A 116.5(14) . . ?
C31A C36A C39A 123.4(14) . . ?
C32A C37A H37A 109.5 . . ?
C32A C37A H37B 109.5 . . ?
H37A C37A H37B 109.5 . . ?
C32A C37A H37C 109.5 . . ?
H37A C37A H37C 109.5 . . ?
H37B C37A H37C 109.5 . . ?
C34A C38A H38A 109.5 . . ?
C34A C38A H38B 109.5 . . ?
H38A C38A H38B 109.5 . . ?
C34A C38A H38C 109.5 . . ?
H38A C38A H38C 109.5 . . ?
H38B C38A H38C 109.5 . . ?
C36A C39A H39A 109.5 . . ?
C36A C39A H39B 109.5 . . ?
H39A C39A H39B 109.5 . . ?
C36A C39A H39C 109.5 . . ?
H39A C39A H39C 109.5 . . ?
H39B C39A H39C 109.5 . . ?
C41A C40A C45A 120.0 . . ?
C41A C40A Rh1A 74.0(4) . . ?
C45A C40A Rh1A 69.6(4) . . ?
C41A C40A H40A 119.6 . . ?
C45A C40A H40A 119.6 . . ?
Rh1A C40A H40A 119.6 . . ?
C40A C41A C42A 120.0 . . ?
C40A C41A Rh1A 70.8(4) . . ?
C42A C41A Rh1A 71.7(4) . . ?
C40A C41A H41A 119.4 . . ?
C42A C41A H41A 119.4 . . ?
Rh1A C41A H41A 119.4 . . ?
C43A C42A C41A 120.0 . . ?
C43A C42A Rh1A 69.8(4) . . ?
C41A C42A Rh1A 73.2(4) . . ?
C43A C42A H42A 119.5 . . ?
C41A C42A H42A 119.5 . . ?
Rh1A C42A H42A 119.5 . . ?
C42A C43A C44A 120.0 . . ?
C42A C43A Rh1A 74.5(5) . . ?
C44A C43A Rh1A 70.1(5) . . ?
C42A C43A H43A 119.7 . . ?
C44A C43A H43A 119.7 . . ?
Rh1A C43A H43A 119.7 . . ?
C43A C44A C45A 120.0 . . ?
C43A C44A Rh1A 73.4(5) . . ?
C45A C44A Rh1A 72.4(5) . . ?
C43A C44A H44A 119.8 . . ?
C45A C44A H44A 119.8 . . ?
Rh1A C44A H44A 119.8 . . ?
C44A C45A C40A 120.0 . . ?
C44A C45A C46A 122.6(18) . . ?
C40A C45A C46A 117.4(18) . . ?
C44A C45A Rh1A 70.9(5) . . ?
C40A C45A Rh1A 74.4(5) . . ?
C46A C45A Rh1A 128.2(14) . . ?
C45A C46A H46A 109.5 . . ?
C45A C46A H46B 109.5 . . ?
H46A C46A H46B 109.5 . . ?
C45A C46A H46C 109.5 . . ?
H46A C46A H46C 109.5 . . ?
H46B C46A H46C 109.5 . . ?
C5C Rh1C C4C 38.8(2) . . ?
C5C Rh1C C6C 38.42(19) . . ?
C4C Rh1C C6C 64.5(2) . . ?
C5C Rh1C C3C 64.7(2) . . ?
C4C Rh1C C3C 38.7(2) . . ?
C6C Rh1C C3C 64.3(2) . . ?
C5C Rh1C C2C 64.3(2) . . ?
C4C Rh1C C2C 64.5(2) . . ?
C6C Rh1C C2C 38.18(18) . . ?
C3C Rh1C C2C 38.35(18) . . ?
C5C Rh1C C44C 119.6(5) . . ?
C4C Rh1C C44C 107.6(4) . . ?
C6C Rh1C C44C 153.9(6) . . ?
C3C Rh1C C44C 126.4(5) . . ?
C2C Rh1C C44C 163.4(6) . . ?
C5C Rh1C C43C 146.3(5) . . ?
C4C Rh1C C43C 114.3(5) . . ?
C6C Rh1C C43C 169.7(5) . . ?
C3C Rh1C C43C 108.0(4) . . ?
C2C Rh1C C43C 131.5(5) . . ?
C44C Rh1C C43C 36.08(18) . . ?
C5C Rh1C C45C 109.1(4) . . ?
C4C Rh1C C45C 123.0(5) . . ?
C6C Rh1C C45C 125.2(5) . . ?
C3C Rh1C C45C 158.0(6) . . ?
C2C Rh1C C45C 160.5(6) . . ?
C44C Rh1C C45C 36.06(18) . . ?
C43C Rh1C C45C 64.6(3) . . ?
C5C Rh1C C42C 175.3(4) . . ?
C4C Rh1C C42C 139.1(5) . . ?
C6C Rh1C C42C 138.5(5) . . ?
C3C Rh1C C42C 111.1(4) . . ?
C2C Rh1C C42C 111.1(4) . . ?
C44C Rh1C C42C 64.4(3) . . ?
C43C Rh1C C42C 35.68(17) . . ?
C45C Rh1C C42C 75.6(2) . . ?
C5C Rh1C C40C 119.9(5) . . ?
C4C Rh1C C40C 152.6(6) . . ?
C6C Rh1C C40C 110.3(4) . . ?
C3C Rh1C C40C 166.2(6) . . ?
C2C Rh1C C40C 129.5(5) . . ?
C44C Rh1C C40C 64.3(3) . . ?
C43C Rh1C C40C 75.6(2) . . ?
C45C Rh1C C40C 35.65(19) . . ?
C42C Rh1C C40C 63.6(3) . . ?
C5C Rh1C C41C 146.1(5) . . ?
C4C Rh1C C41C 172.1(6) . . ?
C6C Rh1C C41C 115.8(4) . . ?
C3C Rh1C C41C 133.6(5) . . ?
C2C Rh1C C41C 110.5(4) . . ?
C44C Rh1C C41C 75.6(2) . . ?
C43C Rh1C C41C 63.8(3) . . ?
C45C Rh1C C41C 63.8(3) . . ?
C42C Rh1C C41C 35.29(17) . . ?
C40C Rh1C C41C 35.28(18) . . ?
C6C C2C C3C 108.0 . . ?
C6C C2C C7C 127.9(12) . . ?
C3C C2C C7C 123.9(12) . . ?
C6C C2C Rh1C 70.8(5) . . ?
C3C C2C Rh1C 70.0(5) . . ?
C7C C2C Rh1C 128.5(10) . . ?
C4C C3C C2C 108.0 . . ?
C4C C3C C8C 123.1(12) . . ?
C2C C3C C8C 128.8(12) . . ?
C4C C3C Rh1C 70.0(5) . . ?
C2C C3C Rh1C 71.7(5) . . ?
C8C C3C Rh1C 125.0(10) . . ?
C5C C4C C3C 108.0 . . ?
C5C C4C C9C 122.0(12) . . ?
C3C C4C C9C 130.0(12) . . ?
C5C C4C Rh1C 71.1(5) . . ?
C3C C4C Rh1C 71.3(5) . . ?
C9C C4C Rh1C 124.8(12) . . ?
C4C C5C C6C 108.0 . . ?
C4C C5C C10C 127.4(11) . . ?
C6C C5C C10C 124.6(11) . . ?
C4C C5C Rh1C 70.2(5) . . ?
C6C C5C Rh1C 71.7(5) . . ?
C10C C5C Rh1C 124.2(10) . . ?
C2C C6C C5C 108.0 . . ?
C2C C6C C11C 128.1(10) . . ?
C5C C6C C11C 123.5(11) . . ?
C2C C6C Rh1C 71.0(5) . . ?
C5C C6C Rh1C 69.9(5) . . ?
C11C C6C Rh1C 129.7(9) . . ?
C2C C7C H7CA 109.5 . . ?
C2C C7C H7CB 109.5 . . ?
H7CA C7C H7CB 109.5 . . ?
C2C C7C H7CC 109.5 . . ?
H7CA C7C H7CC 109.5 . . ?
H7CB C7C H7CC 109.5 . . ?
C3C C8C H8CA 109.5 . . ?
C3C C8C H8CB 109.5 . . ?
H8CA C8C H8CB 109.5 . . ?
C3C C8C H8CC 109.5 . . ?
H8CA C8C H8CC 109.5 . . ?
H8CB C8C H8CC 109.5 . . ?
C4C C9C H9CA 109.5 . . ?
C4C C9C H9CB 109.5 . . ?
H9CA C9C H9CB 109.5 . . ?
C4C C9C H9CC 109.5 . . ?
H9CA C9C H9CC 109.5 . . ?
H9CB C9C H9CC 109.5 . . ?
C5C C10C H10D 109.5 . . ?
C5C C10C H10E 109.5 . . ?
H10D C10C H10E 109.5 . . ?
C5C C10C H10F 109.5 . . ?
H10D C10C H10F 109.5 . . ?
H10E C10C H10F 109.5 . . ?
C12C C11C C16C 120.0 . . ?
C12C C11C C6C 121.8(10) . . ?
C16C C11C C6C 117.8(10) . . ?
C13C C12C C11C 120.0 . . ?
C13C C12C H12C 120.0 . . ?
C11C C12C H12C 120.0 . . ?
C12C C13C C14C 120.0 . . ?
C12C C13C H13C 120.0 . . ?
C14C C13C H13C 120.0 . . ?
C15C C14C C13C 120.0 . . ?
C15C C14C N17C 118.7(11) . . ?
C13C C14C N17C 120.8(11) . . ?
C16C C15C C14C 120.0 . . ?
C16C C15C H15C 120.0 . . ?
C14C C15C H15C 120.0 . . ?
C15C C16C C11C 120.0 . . ?
C15C C16C H16C 120.0 . . ?
C11C C16C H16C 120.0 . . ?
C18C N17C C30C 121.6(12) . . ?
C18C N17C C14C 121.6(12) . . ?
C30C N17C C14C 116.6(12) . . ?
N17C C18C C19C 119.6(10) . . ?
N17C C18C C23C 120.4(10) . . ?
C19C C18C C23C 120.0 . . ?
C20C C19C C18C 120.0 . . ?
C20C C19C H19C 120.0 . . ?
C18C C19C H19C 120.0 . . ?
C21C C20C C19C 120.0 . . ?
C21C C20C H20C 120.0 . . ?
C19C C20C H20C 120.0 . . ?
C20C C21C C22C 120.0 . . ?
C20C C21C H21C 120.0 . . ?
C22C C21C H21C 120.0 . . ?
C23C C22C C21C 120.0 . . ?
C23C C22C H22C 120.0 . . ?
C21C C22C H22C 120.0 . . ?
C22C C23C C18C 120.0 . . ?
C22C C23C C24C 121.0(11) . . ?
C18C C23C C24C 119.0(11) . . ?
C25C C24C C23C 119.4(14) . . ?
C25C C24C C31C 121.7(15) . . ?
C23C C24C C31C 118.6(14) . . ?
C26C C25C C30C 120.0 . . ?
C26C C25C C24C 120.9(13) . . ?
C30C C25C C24C 119.1(13) . . ?
C27C C26C C25C 120.0 . . ?
C27C C26C H26C 120.0 . . ?
C25C C26C H26C 120.0 . . ?
C26C C27C C28C 120.0 . . ?
C26C C27C H27C 120.0 . . ?
C28C C27C H27C 120.0 . . ?
C27C C28C C29C 120.0 . . ?
C27C C28C H28C 120.0 . . ?
C29C C28C H28C 120.0 . . ?
C30C C29C C28C 120.0 . . ?
C30C C29C H29C 120.0 . . ?
C28C C29C H29C 120.0 . . ?
C29C C30C C25C 120.0 . . ?
C29C C30C N17C 119.6(12) . . ?
C25C C30C N17C 119.8(12) . . ?
C32C C31C C36C 120.0 . . ?
C32C C31C C24C 116.2(13) . . ?
C36C C31C C24C 123.7(13) . . ?
C31C C32C C33C 120.0 . . ?
C31C C32C C37C 125.0(14) . . ?
C33C C32C C37C 114.9(14) . . ?
C34C C33C C32C 120.0 . . ?
C34C C33C H33C 120.0 . . ?
C32C C33C H33C 120.0 . . ?
C35C C34C C33C 120.0 . . ?
C35C C34C C38C 126.1(17) . . ?
C33C C34C C38C 113.8(17) . . ?
C34C C35C C36C 120.0 . . ?
C34C C35C H35C 120.0 . . ?
C36C C35C H35C 120.0 . . ?
C35C C36C C31C 120.0 . . ?
C35C C36C C39C 117.3(13) . . ?
C31C C36C C39C 122.6(13) . . ?
C32C C37C H37D 109.5 . . ?
C32C C37C H37E 109.5 . . ?
H37D C37C H37E 109.5 . . ?
C32C C37C H37F 109.5 . . ?
H37D C37C H37F 109.5 . . ?
H37E C37C H37F 109.5 . . ?
C34C C38C H38D 109.5 . . ?
C34C C38C H38E 109.5 . . ?
H38D C38C H38E 109.5 . . ?
C34C C38C H38F 109.5 . . ?
H38D C38C H38F 109.5 . . ?
H38E C38C H38F 109.5 . . ?
C36C C39C H39D 109.5 . . ?
C36C C39C H39E 109.5 . . ?
H39D C39C H39E 109.5 . . ?
C36C C39C H39F 109.5 . . ?
H39D C39C H39F 109.5 . . ?
H39E C39C H39F 109.5 . . ?
C41C C40C C45C 120.0 . . ?
C41C C40C Rh1C 72.9(4) . . ?
C45C C40C Rh1C 70.9(4) . . ?
C41C C40C H40C 119.6 . . ?
C45C C40C H40C 119.6 . . ?
Rh1C C40C H40C 119.6 . . ?
C42C C41C C40C 120.0 . . ?
C42C C41C Rh1C 71.7(4) . . ?
C40C C41C Rh1C 71.8(4) . . ?
C42C C41C H41C 119.6 . . ?
C40C C41C H41C 119.6 . . ?
Rh1C C41C H41C 119.6 . . ?
C43C C42C C41C 120.0 . . ?
C43C C42C Rh1C 70.9(4) . . ?
C41C C42C Rh1C 73.0(4) . . ?
C43C C42C H42C 119.6 . . ?
C41C C42C H42C 119.6 . . ?
Rh1C C42C H42C 119.6 . . ?
C44C C43C C42C 120.0 . . ?
C44C C43C Rh1C 71.4(4) . . ?
C42C C43C Rh1C 73.4(4) . . ?
C44C C43C H43C 119.7 . . ?
C42C C43C H43C 119.7 . . ?
Rh1C C43C H43C 119.7 . . ?
C43C C44C C45C 120.0 . . ?
C43C C44C Rh1C 72.6(4) . . ?
C45C C44C Rh1C 72.6(4) . . ?
C43C C44C H44C 119.8 . . ?
C45C C44C H44C 119.8 . . ?
Rh1C C44C H44C 119.8 . . ?
C44C C45C C40C 120.0 . . ?
C44C C45C C46C 115(2) . . ?
C40C C45C C46C 124(2) . . ?
C44C C45C Rh1C 71.3(4) . . ?
C40C C45C Rh1C 73.4(4) . . ?
C46C C45C Rh1C 132(2) . . ?
C45C C46C H46D 109.5 . . ?
C45C C46C H46E 109.5 . . ?
H46D C46C H46E 109.5 . . ?
C45C C46C H46F 109.5 . . ?
H46D C46C H46F 109.5 . . ?
H46E C46C H46F 109.5 . . ?
F7E Sb1E F3E 87.3(7) . . ?
F7E Sb1E F5E 95.2(7) . . ?
F3E Sb1E F5E 177.3(8) . . ?
F7E Sb1E F6E 175.0(7) . . ?
F3E Sb1E F6E 88.0(7) . . ?
F5E Sb1E F6E 89.5(7) . . ?
F7E Sb1E F4E 89.5(5) . . ?
F3E Sb1E F4E 91.6(6) . . ?
F5E Sb1E F4E 87.3(6) . . ?
F6E Sb1E F4E 89.2(5) . . ?
F7E Sb1E F2E 91.3(5) . . ?
F3E Sb1E F2E 90.2(5) . . ?
F5E Sb1E F2E 90.9(6) . . ?
F6E Sb1E F2E 90.2(5) . . ?
F4E Sb1E F2E 178.1(5) . . ?
F7F Sb1F F3F 97.2(9) . . ?
F7F Sb1F F4F 89.8(8) . . ?
F3F Sb1F F4F 89.1(7) . . ?
F7F Sb1F F6F 173.7(8) . . ?
F3F Sb1F F6F 89.1(7) . . ?
F4F Sb1F F6F 91.1(6) . . ?
F7F Sb1F F2F 91.7(8) . . ?
F3F Sb1F F2F 89.6(7) . . ?
F4F Sb1F F2F 178.1(8) . . ?
F6F Sb1F F2F 87.5(6) . . ?
F7F Sb1F F5F 91.4(8) . . ?
F3F Sb1F F5F 171.3(8) . . ?
F4F Sb1F F5F 92.1(7) . . ?
F6F Sb1F F5F 82.3(7) . . ?
F2F Sb1F F5F 89.0(7) . . ?
F7G Sb1G F3G 93.5(9) . . ?
F7G Sb1G F4G 86.9(11) . . ?
F3G Sb1G F4G 91.1(10) . . ?
F7G Sb1G F6G 177.3(10) . . ?
F3G Sb1G F6G 89.2(9) . . ?
F4G Sb1G F6G 93.2(11) . . ?
F7G Sb1G F2G 90.5(10) . . ?
F3G Sb1G F2G 93.0(9) . . ?
F4G Sb1G F2G 175.3(11) . . ?
F6G Sb1G F2G 89.2(10) . . ?
F7G Sb1G F5G 87.9(9) . . ?
F3G Sb1G F5G 178.3(8) . . ?
F4G Sb1G F5G 87.9(10) . . ?
F6G Sb1G F5G 89.5(8) . . ?
F2G Sb1G F5G 88.0(8) . . ?
F7H Sb1H F3H 94.7(12) . . ?
F7H Sb1H F5H 86.7(11) . . ?
F3H Sb1H F5H 177.1(13) . . ?
F7H Sb1H F4H 88.2(11) . . ?
F3H Sb1H F4H 89.3(11) . . ?
F5H Sb1H F4H 88.2(11) . . ?
F7H Sb1H F2H 94.7(12) . . ?
F3H Sb1H F2H 92.0(11) . . ?
F5H Sb1H F2H 90.4(11) . . ?
F4H Sb1H F2H 176.7(13) . . ?
F7H Sb1H F6H 174.3(13) . . ?
F3H Sb1H F6H 90.1(11) . . ?
F5H Sb1H F6H 88.4(11) . . ?
F4H Sb1H F6H 88.7(11) . . ?
F2H Sb1H F6H 88.3(11) . . ?
F7I Sb1I F3I 94.2(12) . . ?
F7I Sb1I F4I 86.2(11) . . ?
F3I Sb1I F4I 94.3(11) . . ?
F7I Sb1I F5I 87.6(11) . . ?
F3I Sb1I F5I 177.9(14) . . ?
F4I Sb1I F5I 87.1(11) . . ?
F7I Sb1I F6I 173.9(12) . . ?
F3I Sb1I F6I 89.1(11) . . ?
F4I Sb1I F6I 88.4(11) . . ?
F5I Sb1I F6I 89.3(11) . . ?
F7I Sb1I F2I 92.9(11) . . ?
F3I Sb1I F2I 88.9(11) . . ?
F4I Sb1I F2I 176.7(12) . . ?
F5I Sb1I F2I 89.7(11) . . ?
F6I Sb1I F2I 92.3(11) . . ?
F6J Sb1J F7J 165(4) . . ?
F6J Sb1J F3J 93(4) . . ?
F7J Sb1J F3J 86.6(18) . . ?
F6J Sb1J F2J 59(4) . . ?
F7J Sb1J F2J 106(4) . . ?
F3J Sb1J F2J 83(4) . . ?
F6J Sb1J F5J 95(3) . . ?
F7J Sb1J F5J 80.2(17) . . ?
F3J Sb1J F5J 159(3) . . ?
F2J Sb1J F5J 85.4(18) . . ?
F6J Sb1J F4J 111(4) . . ?
F7J Sb1J F4J 83.6(18) . . ?
F3J Sb1J F4J 82(4) . . ?
F2J Sb1J F4J 161(3) . . ?
F5J Sb1J F4J 113(4) . . ?
F7J F5J Sb1J 49.9(9) . . ?
F5J F7J Sb1J 49.9(9) . . ?
F14G Sb8G F11G 87.9(13) . . ?
F14G Sb8G F10G 90.9(13) . . ?
F11G Sb8G F10G 90.7(12) . . ?
F14G Sb8G F12G 90.2(12) . . ?
F11G Sb8G F12G 91.4(12) . . ?
F10G Sb8G F12G 177.7(14) . . ?
F14G Sb8G F13G 179.4(18) . . ?
F11G Sb8G F13G 92.5(13) . . ?
F10G Sb8G F13G 89.6(13) . . ?
F12G Sb8G F13G 89.3(13) . . ?
F14G Sb8G F9G 92.2(13) . . ?
F11G Sb8G F9G 179.6(14) . . ?
F10G Sb8G F9G 89.0(12) . . ?
F12G Sb8G F9G 89.0(12) . . ?
F13G Sb8G F9G 87.4(13) . . ?
F14H Sb8H F10H 91.7(9) . . ?
F14H Sb8H F11H 85.7(9) . . ?
F10H Sb8H F11H 90.6(9) . . ?
F14H Sb8H F12H 88.7(9) . . ?
F10H Sb8H F12H 178.8(11) . . ?
F11H Sb8H F12H 90.5(9) . . ?
F14H Sb8H F9H 95.3(10) . . ?
F10H Sb8H F9H 88.7(10) . . ?
F11H Sb8H F9H 178.9(11) . . ?
F12H Sb8H F9H 90.2(10) . . ?
F14H Sb8H F13H 175.9(11) . . ?
F10H Sb8H F13H 89.0(9) . . ?
F11H Sb8H F13H 90.3(9) . . ?
F12H Sb8H F13H 90.6(10) . . ?
F9H Sb8H F13H 88.8(9) . . ?
F14I Sb8I F12I 93.3(12) . . ?
F14I Sb8I F10I 89.5(11) . . ?
F12I Sb8I F10I 176.9(14) . . ?
F14I Sb8I F11I 86.6(11) . . ?
F12I Sb8I F11I 93.6(12) . . ?
F10I Sb8I F11I 87.9(11) . . ?
F14I Sb8I F9I 96.0(12) . . ?
F12I Sb8I F9I 92.5(11) . . ?
F10I Sb8I F9I 85.9(11) . . ?
F11I Sb8I F9I 173.3(13) . . ?
F14I Sb8I F13I 172.0(12) . . ?
F12I Sb8I F13I 91.6(11) . . ?
F10I Sb8I F13I 85.8(10) . . ?
F11I Sb8I F13I 86.8(11) . . ?
F9I Sb8I F13I 90.1(11) . . ?
F14J Sb8J F12J 93.3(10) . . ?
F14J Sb8J F11J 83.0(10) . . ?
F12J Sb8J F11J 89.3(10) . . ?
F14J Sb8J F10J 93.1(11) . . ?
F12J Sb8J F10J 171.7(11) . . ?
F11J Sb8J F10J 86.2(10) . . ?
F14J Sb8J F13J 173.1(11) . . ?
F12J Sb8J F13J 89.6(10) . . ?
F11J Sb8J F13J 90.8(10) . . ?
F10J Sb8J F13J 83.5(9) . . ?
F14J Sb8J F9J 91.7(10) . . ?
F12J Sb8J F9J 96.3(10) . . ?
F11J Sb8J F9J 172.5(11) . . ?
F10J Sb8J F9J 88.9(10) . . ?
F13J Sb8J F9J 94.2(10) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1A C5A 2.144(12) . ?
Rh1A C6A 2.158(12) . ?
Rh1A C4A 2.189(13) . ?
Rh1A C44A 2.195(13) . ?
Rh1A C2A 2.211(12) . ?
Rh1A C3A 2.230(13) . ?
Rh1A C45A 2.214(13) . ?
Rh1A C43A 2.237(12) . ?
Rh1A C40A 2.275(13) . ?
Rh1A C42A 2.297(13) . ?
Rh1A C41A 2.316(13) . ?
C2A C3A 1.4200 . ?
C2A C6A 1.4200 . ?
C2A C7A 1.534(9) . ?
C3A C4A 1.4200 . ?
C3A C8A 1.538(9) . ?
C4A C5A 1.4200 . ?
C4A C9A 1.546(9) . ?
C5A C6A 1.4200 . ?
C5A C10A 1.542(9) . ?
C6A C11A 1.483(12) . ?
C7A H7AA 0.9700 . ?
C7A H7AB 0.9700 . ?
C7A H7AC 0.9700 . ?
C8A H8AA 0.9700 . ?
C8A H8AB 0.9700 . ?
C8A H8AC 0.9700 . ?
C9A H9AA 0.9700 . ?
C9A H9AB 0.9700 . ?
C9A H9AC 0.9700 . ?
C10A H10A 0.9700 . ?
C10A H10B 0.9700 . ?
C10A H10C 0.9700 . ?
C11A C12A 1.3900 . ?
C11A C16A 1.3900 . ?
C12A C13A 1.3900 . ?
C12A H12A 0.9400 . ?
C13A C14A 1.3900 . ?
C13A H13A 0.9400 . ?
C14A C15A 1.3900 . ?
C14A N17A 1.475(16) . ?
C15A C16A 1.3900 . ?
C15A H15A 0.9400 . ?
C16A H16A 0.9400 . ?
N17A C30A 1.337(17) . ?
N17A C18A 1.396(17) . ?
C18A C19A 1.3900 . ?
C18A C23A 1.3900 . ?
C19A C20A 1.3900 . ?
C19A H19A 0.9400 . ?
C20A C21A 1.3900 . ?
C20A H20A 0.9400 . ?
C21A C22A 1.3900 . ?
C21A H21A 0.9400 . ?
C22A C23A 1.3900 . ?
C22A H22A 0.9400 . ?
C23A C24A 1.48(2) . ?
C24A C25A 1.39(2) . ?
C24A C31A 1.52(2) . ?
C25A C26A 1.3900 . ?
C25A C30A 1.3900 . ?
C26A C27A 1.3900 . ?
C26A H26A 0.9400 . ?
C27A C28A 1.3900 . ?
C27A H27A 0.9400 . ?
C28A C29A 1.3900 . ?
C28A H28A 0.9400 . ?
C29A C30A 1.3900 . ?
C29A H29A 0.9400 . ?
C31A C32A 1.3900 . ?
C31A C36A 1.3900 . ?
C32A C33A 1.3900 . ?
C32A C37A 1.529(10) . ?
C33A C34A 1.3900 . ?
C33A H33A 0.9400 . ?
C34A C35A 1.3900 . ?
C34A C38A 1.549(10) . ?
C35A C36A 1.3900 . ?
C35A H35A 0.9400 . ?
C36A C39A 1.529(10) . ?
C37A H37A 0.9700 . ?
C37A H37B 0.9700 . ?
C37A H37C 0.9700 . ?
C38A H38A 0.9700 . ?
C38A H38B 0.9700 . ?
C38A H38C 0.9700 . ?
C39A H39A 0.9700 . ?
C39A H39B 0.9700 . ?
C39A H39C 0.9700 . ?
C40A C41A 1.3900 . ?
C40A C45A 1.3900 . ?
C40A H40A 0.9900 . ?
C41A C42A 1.3900 . ?
C41A H41A 0.9900 . ?
C42A C43A 1.3900 . ?
C42A H42A 0.9900 . ?
C43A C44A 1.3900 . ?
C43A H43A 0.9900 . ?
C44A C45A 1.3899 . ?
C44A H44A 0.9900 . ?
C45A C46A 1.560(10) . ?
C46A H46A 0.9700 . ?
C46A H46B 0.9700 . ?
C46A H46C 0.9700 . ?
Rh1C C5C 2.145(12) . ?
Rh1C C4C 2.133(13) . ?
Rh1C C6C 2.169(12) . ?
Rh1C C3C 2.150(12) . ?
Rh1C C2C 2.172(11) . ?
Rh1C C44C 2.236(12) . ?
Rh1C C43C 2.252(12) . ?
Rh1C C45C 2.254(13) . ?
Rh1C C42C 2.284(12) . ?
Rh1C C40C 2.286(13) . ?
Rh1C C41C 2.301(12) . ?
C2C C6C 1.4200 . ?
C2C C3C 1.4200 . ?
C2C C7C 1.525(9) . ?
C3C C4C 1.4200 . ?
C3C C8C 1.562(9) . ?
C4C C5C 1.4200 . ?
C4C C9C 1.545(9) . ?
C5C C6C 1.4200 . ?
C5C C10C 1.551(9) . ?
C6C C11C 1.455(12) . ?
C7C H7CA 0.9700 . ?
C7C H7CB 0.9700 . ?
C7C H7CC 0.9700 . ?
C8C H8CA 0.9700 . ?
C8C H8CB 0.9700 . ?
C8C H8CC 0.9700 . ?
C9C H9CA 0.9700 . ?
C9C H9CB 0.9700 . ?
C9C H9CC 0.9700 . ?
C10C H10D 0.9700 . ?
C10C H10E 0.9700 . ?
C10C H10F 0.9700 . ?
C11C C12C 1.3900 . ?
C11C C16C 1.3900 . ?
C12C C13C 1.3900 . ?
C12C H12C 0.9400 . ?
C13C C14C 1.3900 . ?
C13C H13C 0.9400 . ?
C14C C15C 1.3900 . ?
C14C N17C 1.449(12) . ?
C15C C16C 1.3900 . ?
C15C H15C 0.9400 . ?
C16C H16C 0.9400 . ?
N17C C18C 1.362(13) . ?
N17C C30C 1.394(13) . ?
C18C C19C 1.3900 . ?
C18C C23C 1.3900 . ?
C19C C20C 1.3900 . ?
C19C H19C 0.9400 . ?
C20C C21C 1.3900 . ?
C20C H20C 0.9400 . ?
C21C C22C 1.3900 . ?
C21C H21C 0.9400 . ?
C22C C23C 1.3900 . ?
C22C H22C 0.9400 . ?
C23C C24C 1.433(19) . ?
C24C C25C 1.408(19) . ?
C24C C31C 1.486(18) . ?
C25C C26C 1.3900 . ?
C25C C30C 1.3900 . ?
C26C C27C 1.3900 . ?
C26C H26C 0.9400 . ?
C27C C28C 1.3900 . ?
C27C H27C 0.9400 . ?
C28C C29C 1.3900 . ?
C28C H28C 0.9400 . ?
C29C C30C 1.3900 . ?
C29C H29C 0.9400 . ?
C31C C32C 1.3900 . ?
C31C C36C 1.3900 . ?
C32C C33C 1.3900 . ?
C32C C37C 1.540(10) . ?
C33C C34C 1.3900 . ?
C33C H33C 0.9400 . ?
C34C C35C 1.3900 . ?
C34C C38C 1.552(10) . ?
C35C C36C 1.3900 . ?
C35C H35C 0.9400 . ?
C36C C39C 1.537(10) . ?
C37C H37D 0.9700 . ?
C37C H37E 0.9700 . ?
C37C H37F 0.9700 . ?
C38C H38D 0.9700 . ?
C38C H38E 0.9700 . ?
C38C H38F 0.9700 . ?
C39C H39D 0.9700 . ?
C39C H39E 0.9700 . ?
C39C H39F 0.9700 . ?
C40C C41C 1.3900 . ?
C40C C45C 1.3900 . ?
C40C H40C 0.9900 . ?
C41C C42C 1.3900 . ?
C41C H41C 0.9900 . ?
C42C C43C 1.3900 . ?
C42C H42C 0.9900 . ?
C43C C44C 1.3900 . ?
C43C H43C 0.9900 . ?
C44C C45C 1.3900 . ?
C44C H44C 0.9900 . ?
C45C C46C 1.549(10) . ?
C46C H46D 0.9700 . ?
C46C H46E 0.9700 . ?
C46C H46F 0.9700 . ?
Sb1E F7E 1.760(8) . ?
Sb1E F3E 1.780(8) . ?
Sb1E F5E 1.785(8) . ?
Sb1E F6E 1.804(8) . ?
Sb1E F4E 1.816(7) . ?
Sb1E F2E 1.810(6) . ?
Sb1F F7F 1.682(12) . ?
Sb1F F3F 1.761(12) . ?
Sb1F F4F 1.767(11) . ?
Sb1F F6F 1.815(10) . ?
Sb1F F2F 1.820(10) . ?
Sb1F F5F 1.819(11) . ?
Sb1G F7G 1.732(13) . ?
Sb1G F3G 1.759(12) . ?
Sb1G F4G 1.786(14) . ?
Sb1G F6G 1.784(12) . ?
Sb1G F2G 1.803(12) . ?
Sb1G F5G 1.814(12) . ?
Sb1H F7H 1.703(15) . ?
Sb1H F3H 1.755(15) . ?
Sb1H F5H 1.786(15) . ?
Sb1H F4H 1.798(14) . ?
Sb1H F2H 1.802(14) . ?
Sb1H F6H 1.834(15) . ?
Sb1I F7I 1.725(15) . ?
Sb1I F3I 1.750(14) . ?
Sb1I F4I 1.779(14) . ?
Sb1I F5I 1.791(14) . ?
Sb1I F6I 1.820(15) . ?
Sb1I F2I 1.814(14) . ?
Sb1J F6J 1.704(10) . ?
Sb1J F7J 1.702(10) . ?
Sb1J F3J 1.709(10) . ?
Sb1J F2J 1.703(10) . ?
Sb1J F5J 1.704(10) . ?
Sb1J F4J 1.712(10) . ?
F5J F7J 2.19(4) . ?
Sb8G F14G 1.718(15) . ?
Sb8G F11G 1.770(15) . ?
Sb8G F10G 1.771(15) . ?
Sb8G F12G 1.774(14) . ?
Sb8G F13G 1.807(15) . ?
Sb8G F9G 1.815(15) . ?
Sb8H F14H 1.745(14) . ?
Sb8H F10H 1.776(13) . ?
Sb8H F11H 1.782(13) . ?
Sb8H F12H 1.781(14) . ?
Sb8H F9H 1.793(13) . ?
Sb8H F13H 1.807(14) . ?
Sb8I F14I 1.721(15) . ?
Sb8I F12I 1.743(15) . ?
Sb8I F10I 1.798(15) . ?
Sb8I F11I 1.810(15) . ?
Sb8I F9I 1.799(15) . ?
Sb8I F13I 1.819(15) . ?
Sb8J F14J 1.690(14) . ?
Sb8J F12J 1.733(13) . ?
Sb8J F11J 1.817(14) . ?
Sb8J F10J 1.824(14) . ?
Sb8J F13J 1.807(14) . ?
Sb8J F9J 1.785(13) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6A C2A C3A C4A 0.0 . . . . ?
C7A C2A C3A C4A 170.2(14) . . . . ?
Rh1A C2A C3A C4A -59.9(5) . . . . ?
C6A C2A C3A C8A 174.5(16) . . . . ?
C7A C2A C3A C8A -15.3(19) . . . . ?
Rh1A C2A C3A C8A 114.5(14) . . . . ?
C6A C2A C3A Rh1A 59.9(5) . . . . ?
C7A C2A C3A Rh1A -129.8(13) . . . . ?
C2A C3A C4A C5A 0.0 . . . . ?
C8A C3A C4A C5A -175.0(14) . . . . ?
Rh1A C3A C4A C5A -60.6(5) . . . . ?
C2A C3A C4A C9A -176.1(16) . . . . ?
C8A C3A C4A C9A 8.9(18) . . . . ?
Rh1A C3A C4A C9A 123.3(15) . . . . ?
C2A C3A C4A Rh1A 60.6(5) . . . . ?
C8A C3A C4A Rh1A -114.5(12) . . . . ?
C3A C4A C5A C6A 0.0 . . . . ?
C9A C4A C5A C6A 176.1(16) . . . . ?
Rh1A C4A C5A C6A -62.9(5) . . . . ?
C3A C4A C5A C10A -176.0(13) . . . . ?
C9A C4A C5A C10A 0.1(19) . . . . ?
Rh1A C4A C5A C10A 121.1(12) . . . . ?
C3A C4A C5A Rh1A 62.9(5) . . . . ?
C9A C4A C5A Rh1A -121.0(15) . . . . ?
C4A C5A C6A C2A 0.0 . . . . ?
C10A C5A C6A C2A 175.8(14) . . . . ?
Rh1A C5A C6A C2A -63.7(5) . . . . ?
C4A C5A C6A C11A -173.0(13) . . . . ?
C10A C5A C6A C11A 2.7(17) . . . . ?
Rh1A C5A C6A C11A 123.2(11) . . . . ?
C4A C5A C6A Rh1A 63.7(5) . . . . ?
C10A C5A C6A Rh1A -120.5(13) . . . . ?
C3A C2A C6A C5A 0.0 . . . . ?
C7A C2A C6A C5A -168.3(17) . . . . ?
Rh1A C2A C6A C5A 61.9(5) . . . . ?
C3A C2A C6A C11A 173.0(13) . . . . ?
C7A C2A C6A C11A 4.7(19) . . . . ?
Rh1A C2A C6A C11A -125.1(12) . . . . ?
C3A C2A C6A Rh1A -61.9(5) . . . . ?
C7A C2A C6A Rh1A 129.8(16) . . . . ?
C5A C6A C11A C12A -127.7(10) . . . . ?
C2A C6A C11A C12A 60.5(13) . . . . ?
Rh1A C6A C11A C12A -35.9(16) . . . . ?
C5A C6A C11A C16A 54.3(13) . . . . ?
C2A C6A C11A C16A -117.5(10) . . . . ?
Rh1A C6A C11A C16A 146.1(9) . . . . ?
C16A C11A C12A C13A 0.0 . . . . ?
C6A C11A C12A C13A -177.9(12) . . . . ?
C11A C12A C13A C14A 0.0 . . . . ?
C12A C13A C14A C15A 0.0 . . . . ?
C12A C13A C14A N17A -176.9(12) . . . . ?
C13A C14A C15A C16A 0.0 . . . . ?
N17A C14A C15A C16A 176.9(12) . . . . ?
C14A C15A C16A C11A 0.0 . . . . ?
C12A C11A C16A C15A 0.0 . . . . ?
C6A C11A C16A C15A 178.0(11) . . . . ?
C15A C14A N17A C30A 105.7(13) . . . . ?
C13A C14A N17A C30A -77.4(14) . . . . ?
C15A C14A N17A C18A -76.4(14) . . . . ?
C13A C14A N17A C18A 100.5(13) . . . . ?
C30A N17A C18A C19A 176.3(11) . . . . ?
C14A N17A C18A C19A -1.5(16) . . . . ?
C30A N17A C18A C23A -5.8(18) . . . . ?
C14A N17A C18A C23A 176.5(9) . . . . ?
C23A C18A C19A C20A 0.0 . . . . ?
N17A C18A C19A C20A 177.9(12) . . . . ?
C18A C19A C20A C21A 0.0 . . . . ?
C19A C20A C21A C22A 0.0 . . . . ?
C20A C21A C22A C23A 0.0 . . . . ?
C21A C22A C23A C18A 0.0 . . . . ?
C21A C22A C23A C24A 175.3(13) . . . . ?
C19A C18A C23A C22A 0.0 . . . . ?
N17A C18A C23A C22A -178.0(12) . . . . ?
C19A C18A C23A C24A -175.4(13) . . . . ?
N17A C18A C23A C24A 6.5(13) . . . . ?
C22A C23A C24A C25A -177.3(10) . . . . ?
C18A C23A C24A C25A -1.9(19) . . . . ?
C22A C23A C24A C31A 1.9(19) . . . . ?
C18A C23A C24A C31A 177.3(11) . . . . ?
C23A C24A C25A C26A 179.4(11) . . . . ?
C31A C24A C25A C26A 0(2) . . . . ?
C23A C24A C25A C30A -4.2(19) . . . . ?
C31A C24A C25A C30A 176.7(12) . . . . ?
C24A C25A C26A C27A 176.5(13) . . . . ?
C30A C25A C26A C27A 0.0 . . . . ?
C25A C26A C27A C28A 0.0 . . . . ?
C26A C27A C28A C29A 0.0 . . . . ?
C27A C28A C29A C30A 0.0 . . . . ?
C18A N17A C30A C29A -178.5(11) . . . . ?
C14A N17A C30A C29A -0.8(17) . . . . ?
C18A N17A C30A C25A -0.3(19) . . . . ?
C14A N17A C30A C25A 177.4(9) . . . . ?
C28A C29A C30A N17A 178.1(12) . . . . ?
C28A C29A C30A C25A 0.0 . . . . ?
C24A C25A C30A N17A 5.3(14) . . . . ?
C26A C25A C30A N17A -178.2(12) . . . . ?
C24A C25A C30A C29A -176.5(13) . . . . ?
C26A C25A C30A C29A 0.0 . . . . ?
C25A C24A C31A C32A 86.2(18) . . . . ?
C23A C24A C31A C32A -93.0(16) . . . . ?
C25A C24A C31A C36A -82.4(18) . . . . ?
C23A C24A C31A C36A 98.4(15) . . . . ?
C36A C31A C32A C33A 0.0 . . . . ?
C24A C31A C32A C33A -168.4(14) . . . . ?
C36A C31A C32A C37A 177(2) . . . . ?
C24A C31A C32A C37A 9(2) . . . . ?
C31A C32A C33A C34A 0.0 . . . . ?
C37A C32A C33A C34A -177.4(17) . . . . ?
C32A C33A C34A C35A 0.0 . . . . ?
C32A C33A C34A C38A 179.5(19) . . . . ?
C33A C34A C35A C36A 0.0 . . . . ?
C38A C34A C35A C36A -179.5(19) . . . . ?
C34A C35A C36A C31A 0.0 . . . . ?
C34A C35A C36A C39A -175.4(16) . . . . ?
C32A C31A C36A C35A 0.0 . . . . ?
C24A C31A C36A C35A 168.6(14) . . . . ?
C32A C31A C36A C39A 175.1(17) . . . . ?
C24A C31A C36A C39A -16.3(18) . . . . ?
C45A C40A C41A C42A 0.0 . . . . ?
Rh1A C40A C41A C42A 54.2(4) . . . . ?
C45A C40A C41A Rh1A -54.2(4) . . . . ?
C40A C41A C42A C43A 0.0 . . . . ?
Rh1A C41A C42A C43A 53.8(4) . . . . ?
C40A C41A C42A Rh1A -53.8(4) . . . . ?
C41A C42A C43A C44A 0.0 . . . . ?
Rh1A C42A C43A C44A 55.4(4) . . . . ?
C41A C42A C43A Rh1A -55.4(4) . . . . ?
C42A C43A C44A C45A 0.0 . . . . ?
Rh1A C43A C44A C45A 57.5(4) . . . . ?
C42A C43A C44A Rh1A -57.5(4) . . . . ?
C43A C44A C45A C40A 0.0 . . . . ?
Rh1A C44A C45A C40A 58.0(4) . . . . ?
C43A C44A C45A C46A 178.3(18) . . . . ?
Rh1A C44A C45A C46A -123.7(17) . . . . ?
C43A C44A C45A Rh1A -58.0(4) . . . . ?
C41A C40A C45A C44A 0.0 . . . . ?
Rh1A C40A C45A C44A -56.3(4) . . . . ?
C41A C40A C45A C46A -178.4(17) . . . . ?
Rh1A C40A C45A C46A 125.3(16) . . . . ?
C41A C40A C45A Rh1A 56.3(4) . . . . ?
C6C C2C C3C C4C 0.0 . . . . ?
C7C C2C C3C C4C -175.5(14) . . . . ?
Rh1C C2C C3C C4C 60.9(5) . . . . ?
C6C C2C C3C C8C 178.5(16) . . . . ?
C7C C2C C3C C8C 2.9(19) . . . . ?
Rh1C C2C C3C C8C -120.6(15) . . . . ?
C6C C2C C3C Rh1C -60.9(5) . . . . ?
C7C C2C C3C Rh1C 123.6(13) . . . . ?
C2C C3C C4C C5C 0.0 . . . . ?
C8C C3C C4C C5C -178.6(15) . . . . ?
Rh1C C3C C4C C5C 62.0(5) . . . . ?
C2C C3C C4C C9C 177.9(18) . . . . ?
C8C C3C C4C C9C -1(2) . . . . ?
Rh1C C3C C4C C9C -120.2(16) . . . . ?
C2C C3C C4C Rh1C -62.0(5) . . . . ?
C8C C3C C4C Rh1C 119.5(13) . . . . ?
C3C C4C C5C C6C 0.0 . . . . ?
C9C C4C C5C C6C -178.1(16) . . . . ?
Rh1C C4C C5C C6C 62.1(5) . . . . ?
C3C C4C C5C C10C 179.5(15) . . . . ?
C9C C4C C5C C10C 1.4(19) . . . . ?
Rh1C C4C C5C C10C -118.4(13) . . . . ?
C3C C4C C5C Rh1C -62.1(5) . . . . ?
C9C C4C C5C Rh1C 119.8(15) . . . . ?
C3C C2C C6C C5C 0.0 . . . . ?
C7C C2C C6C C5C 175.3(15) . . . . ?
Rh1C C2C C6C C5C -60.4(5) . . . . ?
C3C C2C C6C C11C -173.5(14) . . . . ?
C7C C2C C6C C11C 1.8(18) . . . . ?
Rh1C C2C C6C C11C 126.1(12) . . . . ?
C3C C2C C6C Rh1C 60.4(5) . . . . ?
C7C C2C C6C Rh1C -124.3(14) . . . . ?
C4C C5C C6C C2C 0.0 . . . . ?
C10C C5C C6C C2C -179.5(14) . . . . ?
Rh1C C5C C6C C2C 61.1(5) . . . . ?
C4C C5C C6C C11C 173.9(13) . . . . ?
C10C C5C C6C C11C -5.7(17) . . . . ?
Rh1C C5C C6C C11C -125.0(11) . . . . ?
C4C C5C C6C Rh1C -61.1(5) . . . . ?
C10C C5C C6C Rh1C 119.4(13) . . . . ?
C2C C6C C11C C12C -61.0(14) . . . . ?
C5C C6C C11C C12C 126.5(9) . . . . ?
Rh1C C6C C11C C12C 35.6(15) . . . . ?
C2C C6C C11C C16C 112.3(11) . . . . ?
C5C C6C C11C C16C -60.3(12) . . . . ?
Rh1C C6C C11C C16C -151.1(8) . . . . ?
C16C C11C C12C C13C 0.0 . . . . ?
C6C C11C C12C C13C 173.1(11) . . . . ?
C11C C12C C13C C14C 0.0 . . . . ?
C12C C13C C14C C15C 0.0 . . . . ?
C12C C13C C14C N17C -171.7(12) . . . . ?
C13C C14C C15C C16C 0.0 . . . . ?
N17C C14C C15C C16C 171.9(12) . . . . ?
C14C C15C C16C C11C 0.0 . . . . ?
C12C C11C C16C C15C 0.0 . . . . ?
C6C C11C C16C C15C -173.4(11) . . . . ?
C15C C14C N17C C18C -98.9(14) . . . . ?
C13C C14C N17C C18C 73.0(15) . . . . ?
C15C C14C N17C C30C 85.2(14) . . . . ?
C13C C14C N17C C30C -102.9(13) . . . . ?
C30C N17C C18C C19C -178.9(11) . . . . ?
C14C N17C C18C C19C 5.4(18) . . . . ?
C30C N17C C18C C23C 1.0(18) . . . . ?
C14C N17C C18C C23C -174.7(11) . . . . ?
N17C C18C C19C C20C 179.9(12) . . . . ?
C23C C18C C19C C20C 0.0 . . . . ?
C18C C19C C20C C21C 0.0 . . . . ?
C19C C20C C21C C22C 0.0 . . . . ?
C20C C21C C22C C23C 0.0 . . . . ?
C21C C22C C23C C18C 0.0 . . . . ?
C21C C22C C23C C24C -179.7(13) . . . . ?
N17C C18C C23C C22C -179.9(13) . . . . ?
C19C C18C C23C C22C 0.0 . . . . ?
N17C C18C C23C C24C -0.2(14) . . . . ?
C19C C18C C23C C24C 179.7(13) . . . . ?
C22C C23C C24C C25C 174.9(12) . . . . ?
C18C C23C C24C C25C -5(2) . . . . ?
C22C C23C C24C C31C -1(2) . . . . ?
C18C C23C C24C C31C 179.8(11) . . . . ?
C23C C24C C25C C26C -170.6(12) . . . . ?
C31C C24C C25C C26C 5(2) . . . . ?
C23C C24C C25C C30C 9(2) . . . . ?
C31C C24C C25C C30C -175.8(12) . . . . ?
C30C C25C C26C C27C 0.0 . . . . ?
C24C C25C C26C C27C 179.6(16) . . . . ?
C25C C26C C27C C28C 0.0 . . . . ?
C26C C27C C28C C29C 0.0 . . . . ?
C27C C28C C29C C30C 0.0 . . . . ?
C28C C29C C30C C25C 0.0 . . . . ?
C28C C29C C30C N17C -171.3(14) . . . . ?
C26C C25C C30C C29C 0.0 . . . . ?
C24C C25C C30C C29C -179.6(15) . . . . ?
C26C C25C C30C N17C 171.3(15) . . . . ?
C24C C25C C30C N17C -8.3(16) . . . . ?
C18C N17C C30C C29C 174.7(12) . . . . ?
C14C N17C C30C C29C -9.4(18) . . . . ?
C18C N17C C30C C25C 3.3(19) . . . . ?
C14C N17C C30C C25C 179.2(10) . . . . ?
C25C C24C C31C C32C 79.6(18) . . . . ?
C23C C24C C31C C32C -105.1(15) . . . . ?
C25C C24C C31C C36C -104.6(17) . . . . ?
C23C C24C C31C C36C 70.7(18) . . . . ?
C36C C31C C32C C33C 0.0 . . . . ?
C24C C31C C32C C33C 176.0(13) . . . . ?
C36C C31C C32C C37C -176.2(16) . . . . ?
C24C C31C C32C C37C -0.3(17) . . . . ?
C31C C32C C33C C34C 0.0 . . . . ?
C37C C32C C33C C34C 176.6(15) . . . . ?
C32C C33C C34C C35C 0.0 . . . . ?
C32C C33C C34C C38C 176.0(17) . . . . ?
C33C C34C C35C C36C 0.0 . . . . ?
C38C C34C C35C C36C -175.5(19) . . . . ?
C34C C35C C36C C31C 0.0 . . . . ?
C34C C35C C36C C39C -176.9(15) . . . . ?
C32C C31C C36C C35C 0.0 . . . . ?
C24C C31C C36C C35C -175.6(14) . . . . ?
C32C C31C C36C C39C 176.7(16) . . . . ?
C24C C31C C36C C39C 1.1(18) . . . . ?
C45C C40C C41C C42C 0.0 . . . . ?
Rh1C C40C C41C C42C -55.1(4) . . . . ?
C45C C40C C41C Rh1C 55.1(4) . . . . ?
C40C C41C C42C C43C 0.0 . . . . ?
Rh1C C41C C42C C43C -55.1(4) . . . . ?
C40C C41C C42C Rh1C 55.1(4) . . . . ?
C41C C42C C43C C44C 0.0 . . . . ?
Rh1C C42C C43C C44C -56.2(4) . . . . ?
C41C C42C C43C Rh1C 56.2(4) . . . . ?
C42C C43C C44C C45C 0.0 . . . . ?
Rh1C C43C C44C C45C -57.2(4) . . . . ?
C42C C43C C44C Rh1C 57.2(4) . . . . ?
C43C C44C C45C C40C 0.0 . . . . ?
Rh1C C44C C45C C40C -57.1(4) . . . . ?
C43C C44C C45C C46C -174(3) . . . . ?
Rh1C C44C C45C C46C 129(3) . . . . ?
C43C C44C C45C Rh1C 57.1(4) . . . . ?
C41C C40C C45C C44C 0.0 . . . . ?
Rh1C C40C C45C C44C 56.1(4) . . . . ?
C41C C40C C45C C46C 173(3) . . . . ?
Rh1C C40C C45C C46C -131(3) . . . . ?
C41C C40C C45C Rh1C -56.1(4) . . . . ?
F6J Sb1J F5J F7J -166(4) . . . . ?
F3J Sb1J F5J F7J -52(8) . . . . ?
F2J Sb1J F5J F7J -107(4) . . . . ?
F4J Sb1J F5J F7J 79(2) . . . . ?
F6J Sb1J F7J F5J 73(13) . . . . ?
F3J Sb1J F7J F5J 164(4) . . . . ?
F2J Sb1J F7J F5J 82(2) . . . . ?
F4J Sb1J F7J F5J -114(4) . . . . ?
