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#$Date: 2022-09-15 03:04:42 +0300 (Thu, 15 Sep 2022) $
#$Revision: 277859 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/30/06/4300628.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4300628
_journal_name_full               'Inorganic Chemistry'
_journal_paper_doi               10.1021/ic0516818
_journal_year                    2006
_chemical_formula_moiety         '(C6 N6 Os), 3(C24 H20 P), 6(H2 O) '
_chemical_formula_sum            'C78 H72 N6 O6 Os P3'
_chemical_formula_weight         1472.53
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                91.4040(10)
_cell_angle_beta                 109.3600(10)
_cell_angle_gamma                102.3970(10)
_cell_formula_units_Z            2
_cell_length_a                   13.7609(11)
_cell_length_b                   16.2275(13)
_cell_length_c                   17.0895(14)
_cell_measurement_temperature    298(2)
_cell_volume                     3497.4(5)
_diffrn_ambient_temperature      298(2)
_exptl_crystal_density_diffrn    1.398
_cod_database_code               4300628
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Os1 Os 0.0000 0.5000 0.0000 0.04069(8) Uani 1 2 d S . .
Os2 Os 0.5000 1.0000 0.5000 0.04571(9) Uani 1 2 d S . .
C11 C 0.1221(4) 0.5597(3) -0.0383(3) 0.0462(11) Uani 1 1 d . . .
N11 N 0.1922(4) 0.5928(3) -0.0563(3) 0.0637(12) Uani 1 1 d . . .
C12 C 0.6420(4) 1.0325(3) 0.4800(3) 0.0558(13) Uani 1 1 d . . .
N12 N 0.7216(4) 1.0531(3) 0.4707(3) 0.0728(14) Uani 1 1 d . . .
C21 C 0.0449(4) 0.6012(3) 0.0907(3) 0.0441(11) Uani 1 1 d . . .
N21 N 0.0750(4) 0.6561(3) 0.1421(3) 0.0584(11) Uani 1 1 d . . .
C22 C 0.4440(4) 0.8933(3) 0.4152(4) 0.0581(13) Uani 1 1 d . . .
N22 N 0.4059(4) 0.8347(3) 0.3664(3) 0.0845(16) Uani 1 1 d . . .
C32 C 0.5689(4) 0.9353(3) 0.5961(4) 0.0593(14) Uani 1 1 d . . .
N32 N 0.6104(4) 0.9017(3) 0.6522(4) 0.0875(17) Uani 1 1 d . . .
C31 C 0.1052(4) 0.4437(3) 0.0835(3) 0.0445(11) Uani 1 1 d . . .
N31 N 0.1671(4) 0.4152(3) 0.1301(3) 0.0670(13) Uani 1 1 d . . .
P1A P 0.64768(10) 0.54835(8) 0.37793(8) 0.0458(3) Uani 1 1 d . . .
P1B P 0.24792(10) 0.14043(8) 0.90206(8) 0.0475(3) Uani 1 1 d . . .
P1C P 0.07728(9) 0.76736(8) 0.73758(7) 0.0424(3) Uani 1 1 d . . .
C12A C 0.5233(4) 0.5639(3) 0.3109(3) 0.0546(13) Uani 1 1 d . . .
C22A C 0.5042(5) 0.5741(4) 0.2274(3) 0.0744(17) Uani 1 1 d . . .
H22A H 0.5557 0.5717 0.2039 0.089 Uiso 1 1 calc R . .
C32A C 0.4079(7) 0.5880(4) 0.1797(5) 0.104(3) Uani 1 1 d . . .
H32A H 0.3937 0.5934 0.1232 0.125 Uiso 1 1 calc R . .
C42A C 0.3327(6) 0.5939(4) 0.2140(7) 0.110(3) Uani 1 1 d . . .
H42A H 0.2687 0.6048 0.1813 0.133 Uiso 1 1 calc R . .
C52A C 0.3517(6) 0.5840(5) 0.2957(7) 0.106(3) Uani 1 1 d . . .
H52A H 0.2997 0.5866 0.3186 0.127 Uiso 1 1 calc R . .
C62A C 0.4465(5) 0.5700(4) 0.3449(4) 0.0764(18) Uani 1 1 d . . .
H62A H 0.4594 0.5647 0.4013 0.092 Uiso 1 1 calc R . .
C11A C 0.7454(4) 0.5775(3) 0.3299(3) 0.0490(12) Uani 1 1 d . . .
C21A C 0.7418(5) 0.5257(3) 0.2631(3) 0.0638(15) Uani 1 1 d . . .
H21A H 0.6901 0.4752 0.2447 0.077 Uiso 1 1 calc R . .
C31A C 0.8145(6) 0.5488(5) 0.2239(4) 0.0804(19) Uani 1 1 d . . .
H31A H 0.8124 0.5139 0.1791 0.096 Uiso 1 1 calc R . .
C41A C 0.8899(6) 0.6231(5) 0.2508(5) 0.087(2) Uani 1 1 d . . .
H41A H 0.9381 0.6387 0.2233 0.105 Uiso 1 1 calc R . .
C51A C 0.8959(5) 0.6746(4) 0.3169(4) 0.0769(18) Uani 1 1 d . . .
H51A H 0.9485 0.7246 0.3350 0.092 Uiso 1 1 calc R . .
C61A C 0.8234(4) 0.6524(3) 0.3571(3) 0.0611(14) Uani 1 1 d . . .
H61A H 0.8269 0.6876 0.4022 0.073 Uiso 1 1 calc R . .
C13A C 0.6812(4) 0.6150(3) 0.4721(3) 0.0498(12) Uani 1 1 d . . .
C23A C 0.6735(4) 0.6984(3) 0.4669(4) 0.0664(15) Uani 1 1 d . . .
H23A H 0.6519 0.7189 0.4151 0.080 Uiso 1 1 calc R . .
C33A C 0.6978(5) 0.7512(4) 0.5384(4) 0.0790(18) Uani 1 1 d . . .
H33A H 0.6935 0.8075 0.5353 0.095 Uiso 1 1 calc R . .
C43A C 0.7283(4) 0.7199(5) 0.6142(4) 0.0762(18) Uani 1 1 d . . .
H43A H 0.7448 0.7557 0.6625 0.091 Uiso 1 1 calc R . .
C53A C 0.7351(4) 0.6378(5) 0.6204(4) 0.0783(18) Uani 1 1 d . . .
H53A H 0.7552 0.6176 0.6725 0.094 Uiso 1 1 calc R . .
C63A C 0.7122(4) 0.5850(4) 0.5497(3) 0.0566(13) Uani 1 1 d . . .
H63A H 0.7175 0.5289 0.5537 0.068 Uiso 1 1 calc R . .
C14A C 0.6410(4) 0.4404(3) 0.3992(3) 0.0478(11) Uani 1 1 d . . .
C24A C 0.5486(4) 0.3865(3) 0.3963(4) 0.0759(18) Uani 1 1 d . . .
H24A H 0.4856 0.4043 0.3792 0.091 Uiso 1 1 calc R . .
C34A C 0.5491(5) 0.3057(4) 0.4186(5) 0.099(2) Uani 1 1 d . . .
H34A H 0.4858 0.2690 0.4160 0.119 Uiso 1 1 calc R . .
C44A C 0.6393(5) 0.2788(4) 0.4441(4) 0.0797(18) Uani 1 1 d . . .
H44A H 0.6382 0.2246 0.4609 0.096 Uiso 1 1 calc R . .
C54A C 0.7326(5) 0.3306(4) 0.4456(4) 0.0751(17) Uani 1 1 d . . .
H54A H 0.7950 0.3118 0.4625 0.090 Uiso 1 1 calc R . .
C64A C 0.7326(4) 0.4115(3) 0.4215(3) 0.0661(15) Uani 1 1 d . . .
H64A H 0.7951 0.4466 0.4204 0.079 Uiso 1 1 calc R . .
C11B C 0.2822(4) 0.1371(3) 0.8098(3) 0.0502(12) Uani 1 1 d . . .
C21B C 0.2183(4) 0.0793(3) 0.7422(3) 0.0605(14) Uani 1 1 d . . .
H21B H 0.1544 0.0461 0.7428 0.073 Uiso 1 1 calc R . .
C31B C 0.2488(5) 0.0705(4) 0.6737(3) 0.0715(16) Uani 1 1 d . . .
H31B H 0.2056 0.0312 0.6285 0.086 Uiso 1 1 calc R . .
C41B C 0.3422(5) 0.1194(4) 0.6721(4) 0.0711(16) Uani 1 1 d . . .
H41B H 0.3628 0.1131 0.6261 0.085 Uiso 1 1 calc R . .
C51B C 0.4057(5) 0.1777(4) 0.7386(4) 0.0761(18) Uani 1 1 d . . .
H51B H 0.4689 0.2113 0.7371 0.091 Uiso 1 1 calc R . .
C61B C 0.3765(4) 0.1871(4) 0.8082(4) 0.0664(15) Uani 1 1 d . . .
H61B H 0.4198 0.2266 0.8531 0.080 Uiso 1 1 calc R . .
C12B C 0.2954(4) 0.2468(3) 0.9526(3) 0.0523(12) Uani 1 1 d . . .
C22B C 0.4032(5) 0.2771(3) 0.9903(3) 0.0630(14) Uani 1 1 d . . .
H22B H 0.4484 0.2408 0.9959 0.076 Uiso 1 1 calc R . .
C32B C 0.4439(6) 0.3620(4) 1.0199(4) 0.0832(19) Uani 1 1 d . . .
H32B H 0.5168 0.3831 1.0438 0.100 Uiso 1 1 calc R . .
C42B C 0.3782(8) 0.4144(4) 1.0140(4) 0.093(2) Uani 1 1 d . . .
H42B H 0.4063 0.4715 1.0338 0.112 Uiso 1 1 calc R . .
C52B C 0.2706(7) 0.3842(4) 0.9793(4) 0.086(2) Uani 1 1 d . . .
H52B H 0.2257 0.4202 0.9767 0.103 Uiso 1 1 calc R . .
C62B C 0.2294(5) 0.3002(3) 0.9483(3) 0.0636(15) Uani 1 1 d . . .
H62B H 0.1564 0.2796 0.9243 0.076 Uiso 1 1 calc R . .
C13B C 0.1066(4) 0.1053(3) 0.8710(3) 0.0513(12) Uani 1 1 d . . .
C23B C 0.0422(4) 0.1442(3) 0.8106(3) 0.0633(14) Uani 1 1 d . . .
H23B H 0.0727 0.1900 0.7881 0.076 Uiso 1 1 calc R . .
C33B C -0.0659(5) 0.1163(4) 0.7835(4) 0.0720(16) Uani 1 1 d . . .
H33B H -0.1085 0.1432 0.7433 0.086 Uiso 1 1 calc R . .
C43B C -0.1109(5) 0.0482(4) 0.8164(4) 0.0671(16) Uani 1 1 d . . .
H43B H -0.1842 0.0287 0.7979 0.080 Uiso 1 1 calc R . .
C53B C -0.0483(5) 0.0087(3) 0.8764(4) 0.0658(15) Uani 1 1 d . . .
H53B H -0.0796 -0.0370 0.8986 0.079 Uiso 1 1 calc R . .
C63B C 0.0604(4) 0.0363(3) 0.9039(3) 0.0536(12) Uani 1 1 d . . .
H63B H 0.1026 0.0090 0.9441 0.064 Uiso 1 1 calc R . .
C14B C 0.3090(4) 0.0710(3) 0.9713(3) 0.0484(11) Uani 1 1 d . . .
C24B C 0.3180(4) 0.0801(3) 1.0541(3) 0.0655(15) Uani 1 1 d . . .
H24B H 0.2959 0.1239 1.0741 0.079 Uiso 1 1 calc R . .
C34B C 0.3604(5) 0.0234(4) 1.1075(4) 0.0766(18) Uani 1 1 d . . .
H34B H 0.3656 0.0285 1.1631 0.092 Uiso 1 1 calc R . .
C44B C 0.3944(5) -0.0398(4) 1.0776(5) 0.081(2) Uani 1 1 d . . .
H44B H 0.4242 -0.0768 1.1137 0.097 Uiso 1 1 calc R . .
C54B C 0.3854(4) -0.0496(3) 0.9957(5) 0.0742(17) Uani 1 1 d . . .
H54B H 0.4079 -0.0935 0.9761 0.089 Uiso 1 1 calc R . .
C64B C 0.3427(4) 0.0059(3) 0.9420(4) 0.0634(14) Uani 1 1 d . . .
H64B H 0.3366 -0.0005 0.8862 0.076 Uiso 1 1 calc R . .
C11C C 0.2154(4) 0.7847(3) 0.7499(3) 0.0454(11) Uani 1 1 d . . .
C21C C 0.2673(4) 0.8533(4) 0.7224(3) 0.0658(15) Uani 1 1 d . . .
H21C H 0.2318 0.8938 0.6973 0.079 Uiso 1 1 calc R . .
C31C C 0.3732(5) 0.8617(4) 0.7323(4) 0.0849(19) Uani 1 1 d . . .
H31C H 0.4086 0.9082 0.7137 0.102 Uiso 1 1 calc R . .
C41C C 0.4258(5) 0.8036(5) 0.7685(4) 0.0808(19) Uani 1 1 d . . .
H41C H 0.4966 0.8097 0.7739 0.097 Uiso 1 1 calc R . .
C51C C 0.3756(5) 0.7367(4) 0.7969(4) 0.0767(18) Uani 1 1 d . . .
H51C H 0.4129 0.6976 0.8229 0.092 Uiso 1 1 calc R . .
C61C C 0.2695(4) 0.7249(4) 0.7884(3) 0.0609(14) Uani 1 1 d . . .
H61C H 0.2354 0.6783 0.8078 0.073 Uiso 1 1 calc R . .
C12C C 0.0612(4) 0.7848(3) 0.8363(3) 0.0420(10) Uani 1 1 d . . .
C22C C 0.1478(4) 0.8090(3) 0.9078(3) 0.0525(13) Uani 1 1 d . . .
H22C H 0.2159 0.8183 0.9056 0.063 Uiso 1 1 calc R . .
C32C C 0.1333(4) 0.8194(4) 0.9832(3) 0.0638(15) Uani 1 1 d . . .
H32C H 0.1919 0.8358 1.0318 0.077 Uiso 1 1 calc R . .
C42C C 0.0347(4) 0.8061(3) 0.9872(3) 0.0558(13) Uani 1 1 d . . .
H42C H 0.0259 0.8131 1.0384 0.067 Uiso 1 1 calc R . .
C52C C -0.0521(4) 0.7825(3) 0.9161(3) 0.0561(13) Uani 1 1 d . . .
H52C H -0.1198 0.7743 0.9189 0.067 Uiso 1 1 calc R . .
C62C C -0.0395(4) 0.7708(3) 0.8404(3) 0.0547(13) Uani 1 1 d . . .
H62C H -0.0985 0.7536 0.7922 0.066 Uiso 1 1 calc R . .
C13C C 0.0175(3) 0.6586(3) 0.6967(3) 0.0431(11) Uani 1 1 d . . .
C23C C -0.0152(4) 0.6000(3) 0.7458(3) 0.0559(13) Uani 1 1 d . . .
H23C H -0.0084 0.6173 0.8001 0.067 Uiso 1 1 calc R . .
C33C C -0.0578(4) 0.5161(3) 0.7144(4) 0.0700(16) Uani 1 1 d . . .
H33C H -0.0796 0.4773 0.7480 0.084 Uiso 1 1 calc R . .
C43C C -0.0686(5) 0.4892(4) 0.6369(4) 0.0735(17) Uani 1 1 d . . .
H43C H -0.0966 0.4323 0.6169 0.088 Uiso 1 1 calc R . .
C53C C -0.0375(5) 0.5471(4) 0.5866(4) 0.091(2) Uani 1 1 d . . .
H53C H -0.0459 0.5291 0.5322 0.109 Uiso 1 1 calc R . .
C63C C 0.0056(5) 0.6312(4) 0.6167(3) 0.0757(17) Uani 1 1 d . . .
H63C H 0.0267 0.6697 0.5826 0.091 Uiso 1 1 calc R . .
C14C C 0.0173(4) 0.8369(3) 0.6673(3) 0.0462(11) Uani 1 1 d . . .
C24C C -0.0376(4) 0.8896(3) 0.6893(3) 0.0552(13) Uani 1 1 d . . .
H24C H -0.0389 0.8925 0.7433 0.066 Uiso 1 1 calc R . .
C34C C -0.0907(5) 0.9384(3) 0.6328(4) 0.0682(15) Uani 1 1 d . . .
H34C H -0.1292 0.9724 0.6483 0.082 Uiso 1 1 calc R . .
C44C C -0.0864(5) 0.9362(4) 0.5542(4) 0.0696(16) Uani 1 1 d . . .
H44C H -0.1222 0.9688 0.5159 0.084 Uiso 1 1 calc R . .
C54C C -0.0305(6) 0.8870(4) 0.5315(4) 0.0807(19) Uani 1 1 d . . .
H54C H -0.0272 0.8864 0.4780 0.097 Uiso 1 1 calc R . .
C64C C 0.0221(5) 0.8374(4) 0.5879(3) 0.0723(17) Uani 1 1 d . . .
H64C H 0.0610 0.8042 0.5720 0.087 Uiso 1 1 calc R . .
O1W O 0.6612(4) 0.6559(3) 0.8016(3) 0.1044(15) Uani 1 1 d . . .
O2W O 0.7239(4) 0.8314(3) 0.7918(3) 0.1003(15) Uani 1 1 d . . .
O3W O 0.1156(3) 0.8003(3) 0.4396(3) 0.0987(15) Uani 1 1 d . . .
O4W O 0.3683(3) 0.7396(3) 0.0366(3) 0.0863(13) Uani 1 1 d . . .
O5W O 0.2963(4) 0.7928(3) 0.1755(3) 0.0945(14) Uani 1 1 d . . .
O6W O 0.1887(3) 0.7178(3) 0.3255(3) 0.0791(12) Uani 1 1 d . . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Os1 C31 2.056(5) 2_565 ?
Os1 C31 2.056(5) . ?
Os1 C11 2.063(5) . ?
Os1 C11 2.063(5) 2_565 ?
Os1 C21 2.070(5) 2_565 ?
Os1 C21 2.070(5) . ?
Os2 C32 2.044(6) . ?
Os2 C32 2.044(6) 2_676 ?
Os2 C12 2.054(5) 2_676 ?
Os2 C12 2.054(5) . ?
Os2 C22 2.063(5) . ?
Os2 C22 2.063(5) 2_676 ?
C11 N11 1.137(6) . ?
C12 N12 1.141(6) . ?
C21 N21 1.139(6) . ?
C22 N22 1.154(6) . ?
C32 N32 1.157(6) . ?
C31 N31 1.145(6) . ?
P1A C13A 1.783(5) . ?
P1A C14A 1.787(5) . ?
P1A C11A 1.784(5) . ?
P1A C12A 1.790(5) . ?
P1B C14B 1.786(5) . ?
P1B C13B 1.792(5) . ?
P1B C11B 1.792(5) . ?
P1B C12B 1.795(5) . ?
P1C C14C 1.790(5) . ?
P1C C13C 1.793(5) . ?
P1C C12C 1.796(4) . ?
P1C C11C 1.800(5) . ?
C12A C62A 1.384(7) . ?
C12A C22A 1.384(7) . ?
C22A C32A 1.376(8) . ?
C22A H22A 0.9300 . ?
C32A C42A 1.365(11) . ?
C32A H32A 0.9300 . ?
C42A C52A 1.353(11) . ?
C42A H42A 0.9300 . ?
C52A C62A 1.367(9) . ?
C52A H52A 0.9300 . ?
C62A H62A 0.9300 . ?
C11A C21A 1.382(7) . ?
C11A C61A 1.389(7) . ?
C21A C31A 1.374(8) . ?
C21A H21A 0.9300 . ?
C31A C41A 1.363(9) . ?
C31A H31A 0.9300 . ?
C41A C51A 1.359(9) . ?
C41A H41A 0.9300 . ?
C51A C61A 1.381(7) . ?
C51A H51A 0.9300 . ?
C61A H61A 0.9300 . ?
C13A C23A 1.383(7) . ?
C13A C63A 1.387(6) . ?
C23A C33A 1.376(7) . ?
C23A H23A 0.9300 . ?
C33A C43A 1.368(8) . ?
C33A H33A 0.9300 . ?
C43A C53A 1.361(8) . ?
C43A H43A 0.9300 . ?
C53A C63A 1.370(7) . ?
C53A H53A 0.9300 . ?
C63A H63A 0.9300 . ?
C14A C24A 1.364(6) . ?
C14A C64A 1.379(7) . ?
C24A C34A 1.375(8) . ?
C24A H24A 0.9300 . ?
C34A C44A 1.343(9) . ?
C34A H34A 0.9300 . ?
C44A C54A 1.368(8) . ?
C44A H44A 0.9300 . ?
C54A C64A 1.385(7) . ?
C54A H54A 0.9300 . ?
C64A H64A 0.9300 . ?
C11B C21B 1.381(7) . ?
C11B C61B 1.384(7) . ?
C21B C31B 1.382(7) . ?
C21B H21B 0.9300 . ?
C31B C41B 1.368(8) . ?
C31B H31B 0.9300 . ?
C41B C51B 1.373(8) . ?
C41B H41B 0.9300 . ?
C51B C61B 1.390(7) . ?
C51B H51B 0.9300 . ?
C61B H61B 0.9300 . ?
C12B C62B 1.371(7) . ?
C12B C22B 1.376(7) . ?
C22B C32B 1.383(8) . ?
C22B H22B 0.9300 . ?
C32B C42B 1.351(9) . ?
C32B H32B 0.9300 . ?
C42B C52B 1.370(9) . ?
C42B H42B 0.9300 . ?
C52B C62B 1.376(8) . ?
C52B H52B 0.9300 . ?
C62B H62B 0.9300 . ?
C13B C23B 1.385(7) . ?
C13B C63B 1.391(6) . ?
C23B C33B 1.370(7) . ?
C23B H23B 0.9300 . ?
C33B C43B 1.374(8) . ?
C33B H33B 0.9300 . ?
C43B C53B 1.374(8) . ?
C43B H43B 0.9300 . ?
C53B C63B 1.377(7) . ?
C53B H53B 0.9300 . ?
C63B H63B 0.9300 . ?
C14B C24B 1.379(7) . ?
C14B C64B 1.387(6) . ?
C24B C34B 1.392(7) . ?
C24B H24B 0.9300 . ?
C34B C44B 1.368(9) . ?
C34B H34B 0.9300 . ?
C44B C54B 1.367(8) . ?
C44B H44B 0.9300 . ?
C54B C64B 1.381(7) . ?
C54B H54B 0.9300 . ?
C64B H64B 0.9300 . ?
C11C C21C 1.370(6) . ?
C11C C61C 1.395(7) . ?
C21C C31C 1.386(7) . ?
C21C H21C 0.9300 . ?
C31C C41C 1.350(8) . ?
C31C H31C 0.9300 . ?
C41C C51C 1.348(8) . ?
C41C H41C 0.9300 . ?
C51C C61C 1.388(7) . ?
C51C H51C 0.9300 . ?
C61C H61C 0.9300 . ?
C12C C22C 1.371(6) . ?
C12C C62C 1.380(6) . ?
C22C C32C 1.379(7) . ?
C22C H22C 0.9300 . ?
C32C C42C 1.352(7) . ?
C32C H32C 0.9300 . ?
C42C C52C 1.367(7) . ?
C42C H42C 0.9300 . ?
C52C C62C 1.375(6) . ?
C52C H52C 0.9300 . ?
C62C H62C 0.9300 . ?
C13C C23C 1.384(6) . ?
C13C C63C 1.374(6) . ?
C23C C33C 1.379(7) . ?
C23C H23C 0.9300 . ?
C33C C43C 1.335(8) . ?
C33C H33C 0.9300 . ?
C43C C53C 1.383(9) . ?
C43C H43C 0.9300 . ?
C53C C63C 1.376(8) . ?
C53C H53C 0.9300 . ?
C63C H63C 0.9300 . ?
C14C C24C 1.375(6) . ?
C14C C64C 1.381(6) . ?
C24C C34C 1.383(7) . ?
C24C H24C 0.9300 . ?
C34C C44C 1.365(7) . ?
C34C H34C 0.9300 . ?
C44C C54C 1.352(8) . ?
C44C H44C 0.9300 . ?
C54C C64C 1.388(8) . ?
C54C H54C 0.9300 . ?
C64C H64C 0.9300 . ?
