#------------------------------------------------------------------------------
#$Date: 2018-08-29 03:22:13 +0300 (Wed, 29 Aug 2018) $
#$Revision: 210211 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/30/10/4301066.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4301066
loop_
_publ_author_name
'Konu, Jari'
'Chivers, Tristram'
'Schatte, Gabriele'
'Parvez, Masood'
'Laitinen, Risto S.'
_publ_section_title
;
 Formation of N--I Charge-Transfer Bonds and Ion Pairs in Polyiodides with
 Imidotellurium Cations
;
_journal_coden_ASTM              INOCAJ
_journal_issue                   8
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2973
_journal_page_last               2982
_journal_paper_doi               10.1021/ic050058k
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C13 H30 I3 N3 O Te2'
_chemical_formula_weight         880.30
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                104.44(3)
_cell_angle_beta                 101.61(3)
_cell_angle_gamma                93.68(3)
_cell_formula_units_Z            2
_cell_length_a                   9.943(2)
_cell_length_b                   9.957(2)
_cell_length_c                   12.931(3)
_cell_measurement_temperature    173(2)
_cell_volume                     1205.5(5)
_computing_cell_refinement       'DENZO-SMN (Otwinowski & Minor, 1997)'
_computing_data_collection       'KappaCCD Server Software (Nonius, 1997)'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'DIAMOND (Brandenburg & Berndt, 1999)'
_computing_publication_material  'WINGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker Nonius Kappaccd'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0360
_diffrn_reflns_av_sigmaI/netI    0.0611
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            8477
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         2.81
_exptl_absorpt_coefficient_mu    6.266
_exptl_absorpt_correction_T_max  0.7447
_exptl_absorpt_correction_T_min  0.5730
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.425
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             800
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.728
_refine_diff_density_min         -0.990
_refine_diff_density_rms         0.169
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.978
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     199
_refine_ls_number_reflns         4709
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.978
_refine_ls_R_factor_all          0.0504
_refine_ls_R_factor_gt           0.0306
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0158P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0595
_refine_ls_wR_factor_ref         0.0659
_reflns_number_gt                3581
_reflns_number_total             4709
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic050058ksi20050114_075231_4.cif
_cod_data_source_block           cmpd6
_cod_original_cell_volume        1205.5(4)
_cod_database_code               4301066
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
I1 I 0.34936(4) 0.48719(5) 0.27830(3) 0.03922(12) Uani 1 1 d . . .
I2 I 0.34297(4) 0.74881(4) 0.20158(3) 0.02963(11) Uani 1 1 d . . .
I3 I 0.34847(5) 0.99900(4) 0.13186(3) 0.04070(12) Uani 1 1 d . . .
Te1 Te 0.15631(4) 0.46933(4) 0.51983(3) 0.02253(10) Uani 1 1 d . . .
Te2 Te 0.29568(3) 0.36359(4) 0.72339(3) 0.01966(10) Uani 1 1 d . . .
O1 O -0.0263(4) 0.3712(4) 0.4748(3) 0.0268(9) Uani 1 1 d . . .
N1 N 0.2089(4) 0.5260(4) 0.6846(3) 0.0218(10) Uani 1 1 d . . .
N2 N 0.2220(4) 0.2907(4) 0.5652(3) 0.0234(10) Uani 1 1 d . . .
N3 N 0.1461(4) 0.2812(5) 0.7758(3) 0.0250(10) Uani 1 1 d . . .
C10 C 0.2296(5) 0.6697(5) 0.7637(4) 0.0229(12) Uani 1 1 d . . .
C11 C 0.0925(6) 0.6985(6) 0.7962(5) 0.0304(14) Uani 1 1 d . . .
H11A H 0.0220 0.6978 0.7310 0.037 Uiso 1 1 calc R . .
H11B H 0.1046 0.7901 0.8495 0.037 Uiso 1 1 calc R . .
H11C H 0.0630 0.6260 0.8290 0.037 Uiso 1 1 calc R . .
C12 C 0.2805(6) 0.7786(6) 0.7098(5) 0.0346(15) Uani 1 1 d . . .
H12A H 0.3682 0.7562 0.6902 0.042 Uiso 1 1 calc R . .
H12B H 0.2943 0.8716 0.7613 0.042 Uiso 1 1 calc R . .
H12C H 0.2115 0.7772 0.6436 0.042 Uiso 1 1 calc R . .
C13 C 0.3393(6) 0.6703(6) 0.8649(5) 0.0349(14) Uani 1 1 d . . .
H13A H 0.4271 0.6520 0.8438 0.042 Uiso 1 1 calc R . .
H13B H 0.3099 0.5976 0.8974 0.042 Uiso 1 1 calc R . .
H13C H 0.3515 0.7617 0.9184 0.042 Uiso 1 1 calc R . .
C20 C 0.2636(6) 0.1644(6) 0.4948(4) 0.0246(12) Uani 1 1 d . . .
C21 C 0.1609(6) 0.1282(6) 0.3849(5) 0.0347(15) Uani 1 1 d . . .
H21A H 0.1672 0.2053 0.3510 0.042 Uiso 1 1 calc R . .
H21B H 0.0671 0.1127 0.3959 0.042 Uiso 1 1 calc R . .
H21C H 0.1823 0.0431 0.3370 0.042 Uiso 1 1 calc R . .
C22 C 0.2557(7) 0.0457(6) 0.5494(5) 0.0422(17) Uani 1 1 d . . .
H22A H 0.1619 0.0290 0.5600 0.051 Uiso 1 1 calc R . .
H22B H 0.3215 0.0713 0.6207 0.051 Uiso 1 1 calc R . .
H22C H 0.2789 -0.0393 0.5028 0.051 Uiso 1 1 calc R . .
C23 C 0.4095(6) 0.1917(6) 0.4778(5) 0.0331(14) Uani 1 1 d . . .
H23A H 0.4135 0.2681 0.4428 0.040 Uiso 1 1 calc R . .
H23B H 0.4329 0.1070 0.4308 0.040 Uiso 1 1 calc R . .
H23C H 0.4757 0.2174 0.5488 0.040 Uiso 1 1 calc R . .
C30 C 0.1666(5) 0.2549(6) 0.8865(4) 0.0225(12) Uani 1 1 d . . .
C31 C 0.3201(5) 0.2676(7) 0.9374(5) 0.0347(15) Uani 1 1 d . . .
H31A H 0.3637 0.1995 0.8901 0.042 Uiso 1 1 calc R . .
H31B H 0.3327 0.2494 1.0097 0.042 Uiso 1 1 calc R . .
H31C H 0.3630 0.3621 0.9455 0.042 Uiso 1 1 calc R . .
C32 C 0.0997(7) 0.1073(6) 0.8741(5) 0.0382(15) Uani 1 1 d . . .
H32A H 0.1429 0.0392 0.8263 0.046 Uiso 1 1 calc R . .
H32B H 0.0006 0.0992 0.8418 0.046 Uiso 1 1 calc R . .
H32C H 0.1130 0.0889 0.9463 0.046 Uiso 1 1 calc R . .
C33 C 0.1001(6) 0.3613(6) 0.9614(5) 0.0371(15) Uani 1 1 d . . .
H33A H 0.0009 0.3536 0.9294 0.045 Uiso 1 1 calc R . .
H33B H 0.1432 0.4557 0.9693 0.045 Uiso 1 1 calc R . .
H33C H 0.1136 0.3429 1.0335 0.045 Uiso 1 1 calc R . .
C41 C 0.0024(6) 0.2742(7) 0.7147(5) 0.0345(15) Uani 1 1 d . . .
H41A H 0.0027 0.2923 0.6436 0.041 Uiso 1 1 calc R . .
H41B H -0.0447 0.3445 0.7567 0.041 Uiso 1 1 calc R . .
H41C H -0.0463 0.1810 0.7030 0.041 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
I3 I2 I1 177.740(18) . . ?
O1 Te1 N1 108.20(17) . . ?
O1 Te1 O1 75.90(16) . 2_566 ?
N1 Te1 O1 89.25(16) . 2_566 ?
O1 Te1 N2 86.88(16) . . ?
N1 Te1 N2 74.34(16) . . ?
O1 Te1 N2 151.30(15) 2_566 . ?
O1 Te1 Te1 40.13(10) . 2_566 ?
N1 Te1 Te1 100.34(12) . 2_566 ?
O1 Te1 Te1 35.77(10) 2_566 2_566 ?
N2 Te1 Te1 123.37(12) . 2_566 ?
O1 Te1 Te2 103.77(11) . . ?
N1 Te1 Te2 37.78(12) . . ?
O1 Te1 Te2 125.35(10) 2_566 . ?
N2 Te1 Te2 37.10(12) . . ?
Te1 Te1 Te2 121.87(3) 2_566 . ?
N2 Te2 N3 99.21(18) . . ?
N2 Te2 N1 77.89(17) . . ?
N3 Te2 N1 99.96(18) . . ?
N2 Te2 Te1 40.52(12) . . ?
N3 Te2 Te1 107.49(13) . . ?
N1 Te2 Te1 37.93(12) . . ?
Te1 O1 Te1 104.10(16) . 2_566 ?
C10 N1 Te2 122.9(3) . . ?
C10 N1 Te1 129.6(3) . . ?
Te2 N1 Te1 104.29(19) . . ?
C20 N2 Te2 124.7(3) . . ?
C20 N2 Te1 127.6(3) . . ?
Te2 N2 Te1 102.38(19) . . ?
C41 N3 C30 117.2(4) . . ?
C41 N3 Te2 118.2(3) . . ?
C30 N3 Te2 123.1(3) . . ?
N1 C10 C13 108.3(4) . . ?
N1 C10 C11 108.2(4) . . ?
C13 C10 C11 109.6(4) . . ?
N1 C10 C12 109.6(4) . . ?
C13 C10 C12 108.9(5) . . ?
C11 C10 C12 112.1(5) . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C10 C13 H13A 109.5 . . ?
C10 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C10 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
N2 C20 C21 106.8(4) . . ?
N2 C20 C22 108.3(4) . . ?
C21 C20 C22 110.5(5) . . ?
N2 C20 C23 111.7(4) . . ?
C21 C20 C23 109.4(4) . . ?
C22 C20 C23 110.1(5) . . ?
C20 C21 H21A 109.5 . . ?
C20 C21 H21B 109.5 . . ?
H21A C21 H21B 109.5 . . ?
C20 C21 H21C 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C20 C22 H22A 109.5 . . ?
C20 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C20 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C20 C23 H23A 109.5 . . ?
C20 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C20 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
N3 C30 C31 109.9(4) . . ?
N3 C30 C33 110.1(4) . . ?
C31 C30 C33 108.8(5) . . ?
N3 C30 C32 108.9(4) . . ?
C31 C30 C32 109.4(5) . . ?
C33 C30 C32 109.6(5) . . ?
C30 C31 H31A 109.5 . . ?
C30 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
C30 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C30 C32 H32A 109.5 . . ?
C30 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C30 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C30 C33 H33A 109.5 . . ?
C30 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
C30 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
N3 C41 H41A 109.5 . . ?
N3 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
N3 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
I1 I2 3.0098(9) . ?
I2 I3 2.8538(9) . ?
Te1 O1 1.911(4) . ?
Te1 N1 2.012(4) . ?
Te1 O1 2.107(3) 2_566 ?
Te1 N2 2.110(4) . ?
Te1 Te1 3.1712(10) 2_566 ?
Te1 Te2 3.1716(10) . ?
Te2 N2 1.959(4) . ?
Te2 N3 1.967(4) . ?
Te2 N1 2.005(4) . ?
O1 Te1 2.107(3) 2_566 ?
N1 C10 1.511(7) . ?
N2 C20 1.493(6) . ?
N3 C41 1.476(7) . ?
N3 C30 1.495(6) . ?
C10 C13 1.524(7) . ?
C10 C11 1.529(7) . ?
C10 C12 1.538(7) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
C20 C21 1.518(8) . ?
C20 C22 1.525(7) . ?
C20 C23 1.529(7) . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C30 C31 1.520(7) . ?
C30 C33 1.527(7) . ?
C30 C32 1.530(8) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 H33C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Te1 Te2 N2 65.3(2) . . . . ?
N1 Te1 Te2 N2 167.4(3) . . . . ?
O1 Te1 Te2 N2 147.7(2) 2_566 . . . ?
Te1 Te1 Te2 N2 104.6(2) 2_566 . . . ?
O1 Te1 Te2 N3 -18.32(18) . . . . ?
N1 Te1 Te2 N3 83.7(2) . . . . ?
O1 Te1 Te2 N3 64.01(18) 2_566 . . . ?
N2 Te1 Te2 N3 -83.7(2) . . . . ?
Te1 Te1 Te2 N3 20.92(14) 2_566 . . . ?
O1 Te1 Te2 N1 -102.0(2) . . . . ?
O1 Te1 Te2 N1 -19.7(2) 2_566 . . . ?
N2 Te1 Te2 N1 -167.4(3) . . . . ?
Te1 Te1 Te2 N1 -62.8(2) 2_566 . . . ?
N1 Te1 O1 Te1 84.45(18) . . . 2_566 ?
O1 Te1 O1 Te1 0.0 2_566 . . 2_566 ?
N2 Te1 O1 Te1 156.85(18) . . . 2_566 ?
Te2 Te1 O1 Te1 123.55(12) . . . 2_566 ?
N2 Te2 N1 C10 -169.9(4) . . . . ?
N3 Te2 N1 C10 92.7(4) . . . . ?
Te1 Te2 N1 C10 -161.6(5) . . . . ?
N2 Te2 N1 Te1 -8.35(18) . . . . ?
N3 Te2 N1 Te1 -105.7(2) . . . . ?
O1 Te1 N1 C10 -111.0(4) . . . . ?
O1 Te1 N1 C10 -36.1(4) 2_566 . . . ?
N2 Te1 N1 C10 167.7(5) . . . . ?
Te1 Te1 N1 C10 -70.3(4) 2_566 . . . ?
Te2 Te1 N1 C10 159.8(5) . . . . ?
O1 Te1 N1 Te2 89.1(2) . . . . ?
O1 Te1 N1 Te2 164.03(18) 2_566 . . . ?
N2 Te1 N1 Te2 7.87(17) . . . . ?
Te1 Te1 N1 Te2 129.84(15) 2_566 . . . ?
N3 Te2 N2 C20 -98.0(4) . . . . ?
N1 Te2 N2 C20 163.7(4) . . . . ?
Te1 Te2 N2 C20 155.8(5) . . . . ?
N3 Te2 N2 Te1 106.2(2) . . . . ?
N1 Te2 N2 Te1 7.90(17) . . . . ?
O1 Te1 N2 C20 87.4(4) . . . . ?
N1 Te1 N2 C20 -162.8(5) . . . . ?
O1 Te1 N2 C20 139.9(4) 2_566 . . . ?
Te1 Te1 N2 C20 105.0(4) 2_566 . . . ?
Te2 Te1 N2 C20 -154.8(5) . . . . ?
O1 Te1 N2 Te2 -117.87(19) . . . . ?
N1 Te1 N2 Te2 -7.99(17) . . . . ?
O1 Te1 N2 Te2 -65.3(4) 2_566 . . . ?
Te1 Te1 N2 Te2 -100.21(17) 2_566 . . . ?
N2 Te2 N3 C41 -38.0(4) . . . . ?
N1 Te2 N3 C41 41.2(4) . . . . ?
Te1 Te2 N3 C41 2.8(4) . . . . ?
N2 Te2 N3 C30 156.1(4) . . . . ?
N1 Te2 N3 C30 -124.7(4) . . . . ?
Te1 Te2 N3 C30 -163.1(4) . . . . ?
Te2 N1 C10 C13 7.9(6) . . . . ?
Te1 N1 C10 C13 -148.6(4) . . . . ?
Te2 N1 C10 C11 -110.8(4) . . . . ?
Te1 N1 C10 C11 92.6(5) . . . . ?
Te2 N1 C10 C12 126.7(4) . . . . ?
Te1 N1 C10 C12 -29.9(6) . . . . ?
Te2 N2 C20 C21 168.2(4) . . . . ?
Te1 N2 C20 C21 -42.2(6) . . . . ?
Te2 N2 C20 C22 49.2(6) . . . . ?
Te1 N2 C20 C22 -161.3(4) . . . . ?
Te2 N2 C20 C23 -72.3(5) . . . . ?
Te1 N2 C20 C23 77.3(5) . . . . ?
C41 N3 C30 C31 -179.5(5) . . . . ?
Te2 N3 C30 C31 -13.5(6) . . . . ?
C41 N3 C30 C33 -59.6(6) . . . . ?
Te2 N3 C30 C33 106.5(4) . . . . ?
C41 N3 C30 C32 60.7(6) . . . . ?
Te2 N3 C30 C32 -133.3(4) . . . . ?
