#------------------------------------------------------------------------------
#$Date: 2018-08-29 03:22:13 +0300 (Wed, 29 Aug 2018) $
#$Revision: 210211 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/30/10/4301067.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4301067
loop_
_publ_author_name
'Konu, Jari'
'Chivers, Tristram'
'Schatte, Gabriele'
'Parvez, Masood'
'Laitinen, Risto S.'
_publ_section_title
;
 Formation of N--I Charge-Transfer Bonds and Ion Pairs in Polyiodides with
 Imidotellurium Cations
;
_journal_coden_ASTM              INOCAJ
_journal_issue                   8
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2973
_journal_page_last               2982
_journal_paper_doi               10.1021/ic050058k
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C15 H33 I3 N4 O Te2'
_chemical_formula_weight         921.35
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 93.90(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.179(2)
_cell_length_b                   15.6740(11)
_cell_length_c                   14.360(3)
_cell_measurement_temperature    173(2)
_cell_volume                     2734.9(8)
_computing_cell_refinement       'DENZO-SMN (Otwinowski & Minor, 1997)'
_computing_data_collection       'KappaCCD Server Software (Nonius, 1997)'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'DIAMOND (Brandenburg & Berndt, 1999)'
_computing_publication_material  'WINGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker Nonius Kappaccd'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0320
_diffrn_reflns_av_sigmaI/netI    0.0327
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            19376
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         3.46
_exptl_absorpt_coefficient_mu    5.531
_exptl_absorpt_correction_T_max  0.6078
_exptl_absorpt_correction_T_min  0.4909
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.238
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1688
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.585
_refine_diff_density_min         -1.101
_refine_diff_density_rms         0.120
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     226
_refine_ls_number_reflns         5358
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.047
_refine_ls_R_factor_all          0.0358
_refine_ls_R_factor_gt           0.0254
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0310P)²+0.4178P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0579
_refine_ls_wR_factor_ref         0.0620
_reflns_number_gt                4418
_reflns_number_total             5358
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic050058ksi20050114_075231_5.cif
_cod_data_source_block           cmpd6.2MeCN
_cod_database_code               4301067
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
I1 I 0.14775(2) 0.222731(19) -0.036759(19) 0.04172(9) Uani 1 1 d . . .
I2 I 0.01454(2) 0.258662(17) 0.126537(18) 0.03395(8) Uani 1 1 d . . .
I3 I -0.11484(3) 0.29055(3) 0.28063(2) 0.06522(12) Uani 1 1 d . . .
Te1 Te 0.415921(19) 0.076050(15) 0.007245(16) 0.02489(7) Uani 1 1 d . . .
Te2 Te 0.270815(18) 0.113713(15) 0.174282(15) 0.02444(7) Uani 1 1 d . . .
O1 O 0.5583(2) 0.04208(16) 0.05753(18) 0.0306(6) Uani 1 1 d . . .
N1 N 0.3025(2) 0.02040(19) 0.0843(2) 0.0254(7) Uani 1 1 d . . .
N2 N 0.4086(2) 0.15170(19) 0.1265(2) 0.0265(7) Uani 1 1 d . . .
N3 N 0.3259(3) 0.0607(2) 0.2922(2) 0.0333(8) Uani 1 1 d . . .
N4 N 0.9354(5) -0.0226(4) 0.3030(5) 0.0995(19) Uani 1 1 d . . .
C10 C 0.2180(3) -0.0465(2) 0.0531(3) 0.0288(8) Uani 1 1 d . . .
C11 C 0.2667(4) -0.1337(3) 0.0801(3) 0.0431(10) Uani 1 1 d . . .
H11A H 0.2846 -0.1355 0.1477 0.052 Uiso 1 1 calc R . .
H11B H 0.3338 -0.1430 0.0475 0.052 Uiso 1 1 calc R . .
H11C H 0.2130 -0.1784 0.0626 0.052 Uiso 1 1 calc R . .
C12 C 0.1886(3) -0.0409(3) -0.0524(3) 0.0371(9) Uani 1 1 d . . .
H12A H 0.1575 0.0154 -0.0677 0.045 Uiso 1 1 calc R . .
H12B H 0.1344 -0.0851 -0.0708 0.045 Uiso 1 1 calc R . .
H12C H 0.2551 -0.0496 -0.0860 0.045 Uiso 1 1 calc R . .
C13 C 0.1138(3) -0.0318(3) 0.1051(3) 0.0372(10) Uani 1 1 d . . .
H13A H 0.0826 0.0241 0.0881 0.045 Uiso 1 1 calc R . .
H13B H 0.1325 -0.0337 0.1726 0.045 Uiso 1 1 calc R . .
H13C H 0.0599 -0.0765 0.0879 0.045 Uiso 1 1 calc R . .
C20 C 0.4630(3) 0.2360(2) 0.1449(3) 0.0280(8) Uani 1 1 d . . .
C21 C 0.5800(4) 0.2198(3) 0.1858(4) 0.0503(12) Uani 1 1 d . . .
H21A H 0.6209 0.1880 0.1407 0.060 Uiso 1 1 calc R . .
H21B H 0.5777 0.1867 0.2435 0.060 Uiso 1 1 calc R . .
H21C H 0.6167 0.2745 0.1995 0.060 Uiso 1 1 calc R . .
C22 C 0.4006(4) 0.2857(3) 0.2165(3) 0.0402(10) Uani 1 1 d . . .
H22A H 0.3251 0.2965 0.1911 0.048 Uiso 1 1 calc R . .
H22B H 0.4378 0.3402 0.2301 0.048 Uiso 1 1 calc R . .
H22C H 0.3989 0.2523 0.2740 0.048 Uiso 1 1 calc R . .
C23 C 0.4650(4) 0.2875(3) 0.0555(3) 0.0464(11) Uani 1 1 d . . .
H23A H 0.5051 0.2557 0.0098 0.056 Uiso 1 1 calc R . .
H23B H 0.5019 0.3421 0.0688 0.056 Uiso 1 1 calc R . .
H23C H 0.3895 0.2979 0.0302 0.056 Uiso 1 1 calc R . .
C30 C 0.2665(3) 0.0669(3) 0.3797(3) 0.0353(9) Uani 1 1 d . . .
C31 C 0.1646(4) 0.1233(3) 0.3621(3) 0.0481(12) Uani 1 1 d . . .
H31A H 0.1155 0.0979 0.3128 0.058 Uiso 1 1 calc R . .
H31B H 0.1871 0.1802 0.3426 0.058 Uiso 1 1 calc R . .
H31C H 0.1260 0.1278 0.4195 0.058 Uiso 1 1 calc R . .
C32 C 0.3426(4) 0.1064(3) 0.4565(3) 0.0575(13) Uani 1 1 d . . .
H32A H 0.3649 0.1635 0.4373 0.069 Uiso 1 1 calc R . .
H32B H 0.4080 0.0704 0.4677 0.069 Uiso 1 1 calc R . .
H32C H 0.3038 0.1107 0.5139 0.069 Uiso 1 1 calc R . .
C33 C 0.2303(5) -0.0221(3) 0.4077(3) 0.0548(13) Uani 1 1 d . . .
H33A H 0.1813 -0.0464 0.3576 0.066 Uiso 1 1 calc R . .
H33B H 0.1911 -0.0184 0.4650 0.066 Uiso 1 1 calc R . .
H33C H 0.2951 -0.0587 0.4186 0.066 Uiso 1 1 calc R . .
C41 C 0.4304(4) 0.0133(3) 0.2952(3) 0.0516(13) Uani 1 1 d . . .
H41A H 0.4600 0.0145 0.2334 0.062 Uiso 1 1 calc R . .
H41B H 0.4175 -0.0460 0.3133 0.062 Uiso 1 1 calc R . .
H41C H 0.4833 0.0398 0.3409 0.062 Uiso 1 1 calc R . .
C1 C 0.7433(5) 0.0419(5) 0.3078(4) 0.082(2) Uani 1 1 d . . .
H1A H 0.7144 0.0547 0.2440 0.098 Uiso 1 1 calc . . .
H1B H 0.7466 0.0944 0.3449 0.098 Uiso 1 1 calc . . .
H1C H 0.6949 0.0007 0.3360 0.098 Uiso 1 1 calc . . .
C2 C 0.8516(5) 0.0064(4) 0.3058(4) 0.0641(15) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
I3 I2 I1 178.979(14) . . ?
O1 Te1 N1 108.00(12) . . ?
O1 Te1 N2 86.37(11) . . ?
N1 Te1 N2 74.18(12) . . ?
O1 Te1 O1 76.27(11) . 3_655 ?
N1 Te1 O1 89.46(11) . 3_655 ?
N2 Te1 O1 151.28(11) . 3_655 ?
O1 Te1 Te2 107.97(8) . . ?
N1 Te1 Te2 38.82(8) . . ?
N2 Te1 Te2 37.55(8) . . ?
O1 Te1 Te2 127.83(7) 3_655 . ?
O1 Te1 Te1 40.35(7) . 3_655 ?
N1 Te1 Te1 100.40(9) . 3_655 ?
N2 Te1 Te1 123.11(8) . 3_655 ?
O1 Te1 Te1 35.93(7) 3_655 3_655 ?
Te2 Te1 Te1 126.516(16) . 3_655 ?
N2 Te2 N3 100.41(13) . . ?
N2 Te2 N1 77.79(12) . . ?
N3 Te2 N1 100.22(13) . . ?
N2 Te2 Te1 40.85(9) . . ?
N3 Te2 Te1 113.78(9) . . ?
N1 Te2 Te1 39.29(8) . . ?
Te1 O1 Te1 103.73(11) . 3_655 ?
C10 N1 Te2 122.6(2) . . ?
C10 N1 Te1 127.6(2) . . ?
Te2 N1 Te1 101.89(13) . . ?
C20 N2 Te2 126.2(2) . . ?
C20 N2 Te1 127.1(2) . . ?
Te2 N2 Te1 101.60(13) . . ?
C41 N3 C30 118.3(3) . . ?
C41 N3 Te2 118.9(3) . . ?
C30 N3 Te2 122.7(3) . . ?
N1 C10 C11 107.4(3) . . ?
N1 C10 C13 108.6(3) . . ?
C11 C10 C13 109.3(3) . . ?
N1 C10 C12 111.2(3) . . ?
C11 C10 C12 111.2(3) . . ?
C13 C10 C12 109.1(3) . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C10 C13 H13A 109.5 . . ?
C10 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C10 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
N2 C20 C23 110.7(3) . . ?
N2 C20 C21 108.2(3) . . ?
C23 C20 C21 110.2(4) . . ?
N2 C20 C22 109.5(3) . . ?
C23 C20 C22 109.5(3) . . ?
C21 C20 C22 108.7(3) . . ?
C20 C21 H21A 109.5 . . ?
C20 C21 H21B 109.5 . . ?
H21A C21 H21B 109.5 . . ?
C20 C21 H21C 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C20 C22 H22A 109.5 . . ?
C20 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C20 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C20 C23 H23A 109.5 . . ?
C20 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C20 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
N3 C30 C32 109.3(3) . . ?
N3 C30 C33 109.1(3) . . ?
C32 C30 C33 110.6(4) . . ?
N3 C30 C31 109.4(3) . . ?
C32 C30 C31 109.4(4) . . ?
C33 C30 C31 109.0(4) . . ?
C30 C31 H31A 109.5 . . ?
C30 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
C30 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C30 C32 H32A 109.5 . . ?
C30 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C30 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C30 C33 H33A 109.5 . . ?
C30 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
C30 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
N3 C41 H41A 109.5 . . ?
N3 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
N3 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C2 C1 H1A 109.5 . . ?
C2 C1 H1B 109.5 . . ?
H1A C1 H1B 109.5 . . ?
C2 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
N4 C2 C1 178.6(8) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
I1 I2 2.9943(9) . ?
I2 I3 2.8467(9) . ?
Te1 O1 1.908(3) . ?
Te1 N1 2.026(3) . ?
Te1 N2 2.090(3) . ?
Te1 O1 2.105(2) 3_655 ?
Te1 Te2 3.1309(9) . ?
Te1 Te1 3.1590(6) 3_655 ?
Te2 N2 1.948(3) . ?
Te2 N3 1.962(3) . ?
Te2 N1 2.006(3) . ?
O1 Te1 2.105(2) 3_655 ?
N1 C10 1.515(5) . ?
N2 C20 1.494(5) . ?
N3 C41 1.472(5) . ?
N3 C30 1.495(5) . ?
N4 C2 1.120(7) . ?
C10 C11 1.529(5) . ?
C10 C13 1.533(5) . ?
C10 C12 1.535(5) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
C20 C23 1.518(6) . ?
C20 C21 1.526(6) . ?
C20 C22 1.532(5) . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C30 C32 1.523(6) . ?
C30 C33 1.526(6) . ?
C30 C31 1.530(6) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 H33C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C1 C2 1.434(7) . ?
C1 H1A 0.9800 . ?
C1 H1B 0.9800 . ?
C1 H1C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Te1 Te2 N2 57.94(16) . . . . ?
N1 Te1 Te2 N2 154.56(19) . . . . ?
O1 Te1 Te2 N2 144.27(16) 3_655 . . . ?
Te1 Te1 Te2 N2 98.75(14) 3_655 . . . ?
O1 Te1 Te2 N3 -20.07(14) . . . . ?
N1 Te1 Te2 N3 76.56(17) . . . . ?
N2 Te1 Te2 N3 -78.00(17) . . . . ?
O1 Te1 Te2 N3 66.26(14) 3_655 . . . ?
Te1 Te1 Te2 N3 20.75(11) 3_655 . . . ?
O1 Te1 Te2 N1 -96.62(16) . . . . ?
N2 Te1 Te2 N1 -154.56(19) . . . . ?
O1 Te1 Te2 N1 -10.30(16) 3_655 . . . ?
Te1 Te1 Te2 N1 -55.81(13) 3_655 . . . ?
N1 Te1 O1 Te1 84.86(13) . . . 3_655 ?
N2 Te1 O1 Te1 156.94(13) . . . 3_655 ?
O1 Te1 O1 Te1 0.0 3_655 . . 3_655 ?
Te2 Te1 O1 Te1 125.77(8) . . . 3_655 ?
N2 Te2 N1 C10 -167.8(3) . . . . ?
N3 Te2 N1 C10 93.6(3) . . . . ?
Te1 Te2 N1 C10 -151.1(3) . . . . ?
N2 Te2 N1 Te1 -16.70(12) . . . . ?
N3 Te2 N1 Te1 -115.26(14) . . . . ?
O1 Te1 N1 C10 -114.4(3) . . . . ?
N2 Te1 N1 C10 164.9(3) . . . . ?
O1 Te1 N1 C10 -39.0(3) 3_655 . . . ?
Te2 Te1 N1 C10 149.1(3) . . . . ?
Te1 Te1 N1 C10 -73.4(3) 3_655 . . . ?
O1 Te1 N1 Te2 96.51(13) . . . . ?
N2 Te1 N1 Te2 15.79(12) . . . . ?
O1 Te1 N1 Te2 171.88(12) 3_655 . . . ?
Te1 Te1 N1 Te2 137.48(9) 3_655 . . . ?
N3 Te2 N2 C20 -89.5(3) . . . . ?
N1 Te2 N2 C20 172.1(3) . . . . ?
Te1 Te2 N2 C20 156.0(4) . . . . ?
N3 Te2 N2 Te1 114.48(14) . . . . ?
N1 Te2 N2 Te1 16.16(12) . . . . ?
O1 Te1 N2 C20 78.2(3) . . . . ?
N1 Te1 N2 C20 -171.9(3) . . . . ?
O1 Te1 N2 C20 130.6(3) 3_655 . . . ?
Te2 Te1 N2 C20 -155.7(4) . . . . ?
Te1 Te1 N2 C20 95.8(3) 3_655 . . . ?
O1 Te1 N2 Te2 -126.12(14) . . . . ?
N1 Te1 N2 Te2 -16.25(12) . . . . ?
O1 Te1 N2 Te2 -73.8(2) 3_655 . . . ?
Te1 Te1 N2 Te2 -108.50(10) 3_655 . . . ?
N2 Te2 N3 C41 -37.2(3) . . . . ?
N1 Te2 N3 C41 42.1(3) . . . . ?
Te1 Te2 N3 C41 3.4(4) . . . . ?
N2 Te2 N3 C30 142.4(3) . . . . ?
N1 Te2 N3 C30 -138.3(3) . . . . ?
Te1 Te2 N3 C30 -177.0(3) . . . . ?
Te2 N1 C10 C11 -121.1(3) . . . . ?
Te1 N1 C10 C11 95.6(3) . . . . ?
Te2 N1 C10 C13 -3.0(4) . . . . ?
Te1 N1 C10 C13 -146.3(3) . . . . ?
Te2 N1 C10 C12 117.0(3) . . . . ?
Te1 N1 C10 C12 -26.3(4) . . . . ?
Te2 N2 C20 C23 -114.7(3) . . . . ?
Te1 N2 C20 C23 35.3(4) . . . . ?
Te2 N2 C20 C21 124.5(3) . . . . ?
Te1 N2 C20 C21 -85.6(4) . . . . ?
Te2 N2 C20 C22 6.2(4) . . . . ?
Te1 N2 C20 C22 156.2(3) . . . . ?
C41 N3 C30 C32 56.8(5) . . . . ?
Te2 N3 C30 C32 -122.8(3) . . . . ?
C41 N3 C30 C33 -64.3(5) . . . . ?
Te2 N3 C30 C33 116.1(4) . . . . ?
C41 N3 C30 C31 176.5(4) . . . . ?
Te2 N3 C30 C31 -3.1(4) . . . . ?
