#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:12:28 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179050 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/12/4301254.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4301254
loop_
_publ_author_name
'Richard D. Adams'
'Michael B. Hall'
'William C. Pearl'
'Xinzheng Yang'
_publ_section_title
;
Transformations and Reactions of Re2(CO)8(μ-SbPh2)(μ-H) Induced by the
Addition of a Platinum(tri-t-butylphosphine) Group
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              652
_journal_page_last               662
_journal_paper_doi               10.1021/ic801876s
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C58 H78 O10 P2 Pt2 Re2 Sb2'
_chemical_formula_weight         2003.22
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.2800(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.5394(10)
_cell_length_b                   14.4863(8)
_cell_length_c                   26.5084(15)
_cell_measurement_reflns_used    9536
_cell_measurement_temperature    453(2)
_cell_measurement_theta_max      24.07
_cell_measurement_theta_min      2.24
_cell_volume                     6555.2(6)
_computing_cell_refinement       'SAINT+  V6.45 (Bruker, 2003)'
_computing_data_collection       'SMART V5.632 (Bruker, 2005)'
_computing_data_reduction        'SAINT+  V6.45'
_computing_molecular_graphics    'SHELXTL V6.1 (Sheldrick, 2000)'
_computing_publication_material  'SHELXTL V6.1'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker SMART APEX CCD diffractometer'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0740
_diffrn_reflns_av_sigmaI/netI    0.0496
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            77119
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.58
_diffrn_standards_decay_%        <1
_exptl_absorpt_coefficient_mu    8.842
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.533
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS, Bruker, 1997)'
_exptl_crystal_colour            Brown
_exptl_crystal_density_diffrn    2.030
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Plate
_exptl_crystal_F_000             3776
_exptl_crystal_size_max          0.60
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.06
_refine_diff_density_max         2.559
_refine_diff_density_min         -1.485
_refine_diff_density_rms         0.218
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.045
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     637
_refine_ls_number_reflns         13413
_refine_ls_number_restraints     72
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.0594
_refine_ls_R_factor_gt           0.0421
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
; calc 
 [0.00000+1.00000exp(1.00(sinθ/λ)²)]/ 
   [σ²(Fo²)+0.0000+49.5427*P+(0.0619P)²+0.0000sinθ/λ] 
 where P = 0.33333Fo² + 0.66667Fc² 
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1020
_refine_ls_wR_factor_ref         0.1131
_reflns_number_gt                10603
_reflns_number_total             13413
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic801876s_si_001_5.cif
_cod_data_source_block           cisComp6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4301254
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.0769(7) 0.3657(9) 0.3876(6) 0.060(4) Uani 1 1 d D . .
C2 C 0.4035(7) 0.8747(8) 0.3348(5) 0.051(3) Uani 1 1 d D . .
C11 C 0.1803(6) 0.7077(6) 0.4500(4) 0.033(2) Uani 1 1 d . . .
C12 C 0.1287(6) 0.7927(7) 0.3482(4) 0.032(2) Uani 1 1 d . . .
C13 C 0.1612(5) 0.6143(7) 0.3080(4) 0.0287(19) Uani 1 1 d . . .
C14 C 0.0566(6) 0.6279(7) 0.3738(3) 0.032(2) Uani 1 1 d . . .
C15 C 0.2022(5) 0.4788(6) 0.4875(3) 0.0262(19) Uani 1 1 d . . .
C16 C 0.2523(6) 0.4259(9) 0.5252(4) 0.044(3) Uani 1 1 d . . .
H16 H 0.2996 0.4048 0.5193 0.053 Uiso 1 1 calc R . .
C17 C 0.2319(7) 0.4049(11) 0.5710(5) 0.065(4) Uani 1 1 d . . .
H17 H 0.2667 0.3721 0.5964 0.079 Uiso 1 1 calc R . .
C18 C 0.1602(8) 0.4319(11) 0.5798(5) 0.068(4) Uani 1 1 d . . .
H18 H 0.1463 0.4147 0.6103 0.082 Uiso 1 1 calc R . .
C19 C 0.1104(6) 0.4832(9) 0.5441(4) 0.043(3) Uani 1 1 d . . .
H19 H 0.0627 0.5023 0.5502 0.051 Uiso 1 1 calc R . .
C20 C 0.1310(6) 0.5074(7) 0.4981(3) 0.030(2) Uani 1 1 d . . .
H20 H 0.0968 0.5432 0.4739 0.036 Uiso 1 1 calc R . .
C21 C 0.3886(5) 0.5855(6) 0.4922(3) 0.0256(18) Uani 1 1 d . . .
C22 C 0.4913(5) 0.5757(6) 0.4216(3) 0.029(2) Uani 1 1 d . . .
C23 C 0.3655(5) 0.4968(6) 0.3489(4) 0.0279(19) Uani 1 1 d . . .
C24 C 0.4124(5) 0.4100(6) 0.4450(3) 0.0268(19) Uani 1 1 d . . .
C25 C 0.3594(6) 0.8061(6) 0.4435(3) 0.0264(19) Uani 1 1 d . A .
C26 C 0.4363(6) 0.8032(7) 0.4723(4) 0.038(2) Uani 1 1 d . . .
H26 H 0.4693 0.7558 0.4671 0.046 Uiso 1 1 calc R . .
C27 C 0.4639(7) 0.8708(8) 0.5089(4) 0.044(3) Uani 1 1 d . . .
H27 H 0.5161 0.8702 0.5269 0.053 Uiso 1 1 calc R . .
C28 C 0.4143(8) 0.9392(7) 0.5190(4) 0.049(3) Uani 1 1 d . . .
H28 H 0.4325 0.9828 0.5447 0.059 Uiso 1 1 calc R . .
C29 C 0.3380(7) 0.9426(7) 0.4907(4) 0.039(2) Uani 1 1 d . . .
H29 H 0.3049 0.9891 0.4972 0.047 Uiso 1 1 calc R . .
C30 C 0.3098(6) 0.8768(7) 0.4526(3) 0.035(2) Uani 1 1 d . . .
H30 H 0.2583 0.8798 0.4334 0.042 Uiso 1 1 calc R . .
C31 C 0.2410(7) 0.1454(8) 0.3483(5) 0.056(3) Uani 1 1 d D . .
C32 C 0.2522(10) 0.1532(11) 0.4067(6) 0.086(5) Uani 1 1 d D . .
H32A H 0.2985 0.1201 0.4235 0.129 Uiso 1 1 calc R . .
H32B H 0.2076 0.1275 0.4169 0.129 Uiso 1 1 calc R . .
H32C H 0.2577 0.2171 0.4167 0.129 Uiso 1 1 calc R . .
C33 C 0.3190(8) 0.1836(10) 0.3403(8) 0.109(8) Uani 1 1 d D . .
H33A H 0.3270 0.2448 0.3545 0.163 Uiso 1 1 calc R . .
H33B H 0.3177 0.1856 0.3039 0.163 Uiso 1 1 calc R . .
H33C H 0.3611 0.1444 0.3575 0.163 Uiso 1 1 calc R . .
C34 C 0.2362(8) 0.0442(8) 0.3292(6) 0.076(5) Uani 1 1 d D . .
H34A H 0.2814 0.0109 0.3475 0.114 Uiso 1 1 calc R . .
H34B H 0.2344 0.0431 0.2927 0.114 Uiso 1 1 calc R . .
H34C H 0.1897 0.0159 0.3354 0.114 Uiso 1 1 calc R . .
C35 C 0.1689(8) 0.2513(8) 0.2465(4) 0.063(4) Uani 1 1 d D . .
C36 C 0.2244(12) 0.3259(11) 0.2453(6) 0.115(8) Uani 1 1 d D . .
H36A H 0.2739 0.3112 0.2681 0.172 Uiso 1 1 calc R . .
H36B H 0.2046 0.3823 0.2565 0.172 Uiso 1 1 calc R . .
H36C H 0.2312 0.3332 0.2106 0.172 Uiso 1 1 calc R . .
C37 C 0.0858(9) 0.2918(10) 0.2154(5) 0.077(5) Uani 1 1 d D . .
H37A H 0.0772 0.3511 0.2293 0.116 Uiso 1 1 calc R . .
H37B H 0.0447 0.2504 0.2190 0.116 Uiso 1 1 calc R . .
H37C H 0.0861 0.2981 0.1794 0.116 Uiso 1 1 calc R . .
C38 C 0.1838(9) 0.1693(9) 0.2142(5) 0.070(4) Uani 1 1 d D . .
H38A H 0.1827 0.1894 0.1796 0.105 Uiso 1 1 calc R . .
H38B H 0.1439 0.1235 0.2134 0.105 Uiso 1 1 calc R . .
H38C H 0.2341 0.1431 0.2293 0.105 Uiso 1 1 calc R . .
C39 C 0.0605(6) 0.1592(7) 0.3085(5) 0.053(3) Uani 1 1 d D . .
C40 C 0.0612(9) 0.1188(10) 0.3646(5) 0.073(4) Uani 1 1 d D . .
H40A H 0.0710 0.1679 0.3896 0.110 Uiso 1 1 calc R . .
H40B H 0.1016 0.0730 0.3737 0.110 Uiso 1 1 calc R . .
H40C H 0.0113 0.0913 0.3643 0.110 Uiso 1 1 calc R . .
C41 C -0.0085(8) 0.2248(10) 0.2948(8) 0.096(6) Uani 1 1 d D . .
H41A H -0.0133 0.2474 0.2601 0.143 Uiso 1 1 calc R . .
H41B H -0.0003 0.2757 0.3186 0.143 Uiso 1 1 calc R . .
H41C H -0.0556 0.1927 0.2969 0.143 Uiso 1 1 calc R . .
C42 C 0.0475(7) 0.0774(7) 0.2701(4) 0.044(3) Uani 1 1 d D . .
H42A H -0.0026 0.0498 0.2690 0.066 Uiso 1 1 calc R . .
H42B H 0.0880 0.0323 0.2811 0.066 Uiso 1 1 calc R . .
H42C H 0.0490 0.0993 0.2361 0.066 Uiso 1 1 calc R . .
C43 C 0.2632(8) 0.7802(13) 0.1721(7) 0.068(7) Uiso 0.559(10) 1 d PD A 1
C44 C 0.2548(16) 0.8209(18) 0.1179(9) 0.072(7) Uiso 0.559(10) 1 d PD A 1
H44A H 0.2074 0.7984 0.0955 0.108 Uiso 0.559(10) 1 calc PR A 1
H44B H 0.2988 0.8029 0.1044 0.108 Uiso 0.559(10) 1 calc PR A 1
H44C H 0.2527 0.8870 0.1197 0.108 Uiso 0.559(10) 1 calc PR A 1
C45 C 0.2094(17) 0.8342(19) 0.1989(11) 0.085(9) Uiso 0.559(10) 1 d PD A 1
H45A H 0.2399 0.8764 0.2234 0.127 Uiso 0.559(10) 1 calc PR A 1
H45B H 0.1823 0.7922 0.2166 0.127 Uiso 0.559(10) 1 calc PR A 1
H45C H 0.1720 0.8681 0.1735 0.127 Uiso 0.559(10) 1 calc PR A 1
C46 C 0.2288(13) 0.6795(14) 0.1665(9) 0.047(7) Uiso 0.559(10) 1 d PD A 1
H46A H 0.2092 0.6645 0.1965 0.071 Uiso 0.559(10) 1 calc PR A 1
H46B H 0.2692 0.6365 0.1635 0.071 Uiso 0.559(10) 1 calc PR A 1
H46C H 0.1868 0.6759 0.1360 0.071 Uiso 0.559(10) 1 calc PR A 1
C47 C 0.4118(9) 0.9036(9) 0.2078(7) 0.043(5) Uiso 0.559(10) 1 d PD A 1
C48 C 0.4272(14) 0.9238(18) 0.1562(8) 0.068(7) Uiso 0.559(10) 1 d PD A 1
H48A H 0.4598 0.9776 0.1585 0.102 Uiso 0.559(10) 1 calc PR A 1
H48B H 0.3785 0.9347 0.1317 0.102 Uiso 0.559(10) 1 calc PR A 1
H48C H 0.4533 0.8721 0.1450 0.102 Uiso 0.559(10) 1 calc PR A 1
C49 C 0.3583(17) 0.987(2) 0.2197(12) 0.082(9) Uiso 0.559(10) 1 d PD A 1
H49A H 0.3880 1.0429 0.2238 0.122 Uiso 0.559(10) 1 calc PR A 1
H49B H 0.3416 0.9738 0.2510 0.122 Uiso 0.559(10) 1 calc PR A 1
H49C H 0.3133 0.9931 0.1914 0.122 Uiso 0.559(10) 1 calc PR A 1
C50 C 0.4886(12) 0.9183(17) 0.2486(8) 0.061(6) Uiso 0.559(10) 1 d PD A 1
H50A H 0.5318 0.9179 0.2319 0.092 Uiso 0.559(10) 1 calc PR A 1
H50B H 0.4952 0.8696 0.2737 0.092 Uiso 0.559(10) 1 calc PR A 1
H50C H 0.4869 0.9766 0.2655 0.092 Uiso 0.559(10) 1 calc PR A 1
C51 C 0.4333(11) 0.6959(12) 0.2004(9) 0.066(7) Uiso 0.559(10) 1 d PD A 1
C52 C 0.428(2) 0.690(3) 0.1402(10) 0.122(14) Uiso 0.559(10) 1 d PD A 1
H52A H 0.4380 0.7497 0.1275 0.183 Uiso 0.559(10) 1 calc PR A 1
H52B H 0.3760 0.6703 0.1229 0.183 Uiso 0.559(10) 1 calc PR A 1
H52C H 0.4655 0.6465 0.1337 0.183 Uiso 0.559(10) 1 calc PR A 1
C53 C 0.5168(17) 0.723(3) 0.2280(14) 0.123(15) Uiso 0.559(10) 1 d PD A 1
H53A H 0.5267 0.7038 0.2636 0.184 Uiso 0.559(10) 1 calc PR A 1
H53B H 0.5229 0.7884 0.2262 0.184 Uiso 0.559(10) 1 calc PR A 1
H53C H 0.5533 0.6928 0.2114 0.184 Uiso 0.559(10) 1 calc PR A 1
C54 C 0.419(2) 0.5981(19) 0.2199(13) 0.119(13) Uiso 0.559(10) 1 d PD A 1
H54A H 0.4655 0.5613 0.2222 0.178 Uiso 0.559(10) 1 calc PR A 1
H54B H 0.3761 0.5698 0.1960 0.178 Uiso 0.559(10) 1 calc PR A 1
H54C H 0.4076 0.6024 0.2534 0.178 Uiso 0.559(10) 1 calc PR A 1
C55 C 0.3114(14) 0.6781(12) 0.1714(9) 0.072(9) Uiso 0.441(10) 1 d PD A 2
C56 C 0.3222(16) 0.6662(18) 0.1150(9) 0.050(7) Uiso 0.441(10) 1 d PD A 2
H56A H 0.3767 0.6721 0.1149 0.075 Uiso 0.441(10) 1 calc PR A 2
H56B H 0.2928 0.7129 0.0932 0.075 Uiso 0.441(10) 1 calc PR A 2
H56C H 0.3038 0.6063 0.1022 0.075 Uiso 0.441(10) 1 calc PR A 2
C57 C 0.3355(16) 0.5818(16) 0.1940(10) 0.052(7) Uiso 0.441(10) 1 d PD A 2
H57A H 0.2986 0.5609 0.2132 0.078 Uiso 0.441(10) 1 calc PR A 2
H57B H 0.3868 0.5849 0.2166 0.078 Uiso 0.441(10) 1 calc PR A 2
H57C H 0.3362 0.5393 0.1663 0.078 Uiso 0.441(10) 1 calc PR A 2
C46A C 0.221(2) 0.683(5) 0.168(2) 0.18(4) Uiso 0.441(10) 1 d PD A 2
H46D H 0.1970 0.6262 0.1549 0.277 Uiso 0.441(10) 1 calc PR A 2
H46E H 0.1988 0.7329 0.1455 0.277 Uiso 0.441(10) 1 calc PR A 2
H46F H 0.2124 0.6942 0.2021 0.277 Uiso 0.441(10) 1 calc PR A 2
C58 C 0.3010(11) 0.8836(12) 0.1800(8) 0.060(8) Uiso 0.441(10) 1 d PD A 2
C59 C 0.2778(18) 0.883(2) 0.1229(9) 0.070(9) Uiso 0.441(10) 1 d PD A 2
H59A H 0.2941 0.9401 0.1099 0.104 Uiso 0.441(10) 1 calc PR A 2
H59B H 0.2219 0.8776 0.1120 0.104 Uiso 0.441(10) 1 calc PR A 2
H59C H 0.3022 0.8323 0.1098 0.104 Uiso 0.441(10) 1 calc PR A 2
C45A C 0.2234(13) 0.892(2) 0.2007(10) 0.052(7) Uiso 0.441(10) 1 d PD A 2
H45D H 0.1788 0.8938 0.1719 0.078 Uiso 0.441(10) 1 calc PR A 2
H45E H 0.2253 0.9470 0.2209 0.078 Uiso 0.441(10) 1 calc PR A 2
H45F H 0.2192 0.8390 0.2219 0.078 Uiso 0.441(10) 1 calc PR A 2
C49A C 0.3475(16) 0.9701(18) 0.2006(12) 0.053(8) Uiso 0.441(10) 1 d PD A 2
H49D H 0.3812 0.9863 0.1782 0.080 Uiso 0.441(10) 1 calc PR A 2
H49E H 0.3785 0.9583 0.2348 0.080 Uiso 0.441(10) 1 calc PR A 2
H49F H 0.3120 1.0200 0.2018 0.080 Uiso 0.441(10) 1 calc PR A 2
C53A C 0.4622(11) 0.7841(14) 0.2033(8) 0.049(7) Uiso 0.441(10) 1 d PD A 2
C62 C 0.5111(16) 0.8512(17) 0.2458(9) 0.051(7) Uiso 0.441(10) 1 d PD A 2
H62A H 0.4970 0.8408 0.2783 0.077 Uiso 0.441(10) 1 calc PR A 2
H62B H 0.4999 0.9141 0.2353 0.077 Uiso 0.441(10) 1 calc PR A 2
H62C H 0.5660 0.8394 0.2498 0.077 Uiso 0.441(10) 1 calc PR A 2
C60 C 0.4989(19) 0.6888(16) 0.2123(13) 0.061(8) Uiso 0.441(10) 1 d PD A 2
H60A H 0.4720 0.6474 0.1859 0.092 Uiso 0.441(10) 1 calc PR A 2
H60B H 0.4947 0.6665 0.2457 0.092 Uiso 0.441(10) 1 calc PR A 2
H60C H 0.5531 0.6923 0.2111 0.092 Uiso 0.441(10) 1 calc PR A 2
C61 C 0.4722(19) 0.817(2) 0.1497(9) 0.069(9) Uiso 0.441(10) 1 d PD A 2
H61A H 0.5267 0.8157 0.1490 0.103 Uiso 0.441(10) 1 calc PR A 2
H61B H 0.4526 0.8788 0.1434 0.103 Uiso 0.441(10) 1 calc PR A 2
H61C H 0.4435 0.7767 0.1232 0.103 Uiso 0.441(10) 1 calc PR A 2
C1S C -0.0048(10) 0.7663(15) 0.4929(7) 0.093(5) Uani 1 1 d . . .
H1S H -0.0305 0.7121 0.4978 0.112 Uiso 1 1 calc R . .
C2S C -0.0177(11) 0.8042(16) 0.4449(6) 0.093(6) Uani 1 1 d . . .
H2S H -0.0517 0.7750 0.4174 0.112 Uiso 1 1 calc R . .
C3S C 0.0174(14) 0.8826(15) 0.4360(9) 0.106(7) Uani 1 1 d . . .
H3S H 0.0070 0.9083 0.4030 0.127 Uiso 1 1 calc R . .
C4S C 0.0683(13) 0.9243(15) 0.4758(8) 0.099(6) Uani 1 1 d . . .
H4S H 0.0919 0.9792 0.4694 0.119 Uiso 1 1 calc R . .
C5S C 0.0860(11) 0.8892(12) 0.5242(8) 0.086(5) Uani 1 1 d . . .
H5S H 0.1230 0.9172 0.5505 0.103 Uiso 1 1 calc R . .
C6S C 0.0449(10) 0.8060(13) 0.5336(6) 0.081(5) Uani 1 1 d . . .
H6S H 0.0526 0.7810 0.5667 0.097 Uiso 1 1 calc R . .
C7S C 0.2453(11) 0.1735(13) 0.5382(7) 0.153(10) Uiso 1 1 d G . .
H7S H 0.2109 0.1938 0.5081 0.184 Uiso 1 1 calc R . .
C8S C 0.3226(11) 0.1964(11) 0.5475(7) 0.135(8) Uiso 1 1 d G . .
H8S H 0.3410 0.2325 0.5238 0.162 Uiso 1 1 calc R . .
C9S C 0.3729(9) 0.1666(12) 0.5915(7) 0.127(8) Uiso 1 1 d G . .
H9S H 0.4257 0.1823 0.5978 0.153 Uiso 1 1 calc R . .
C10S C 0.3460(11) 0.1138(12) 0.6262(6) 0.160(11) Uiso 1 1 d G . .
H10S H 0.3804 0.0934 0.6562 0.192 Uiso 1 1 calc R . .
C11S C 0.2688(12) 0.0908(12) 0.6169(7) 0.155(10) Uiso 1 1 d G . .
H11S H 0.2504 0.0548 0.6406 0.186 Uiso 1 1 calc R . .
C12S C 0.2184(10) 0.1207(12) 0.5729(8) 0.148(9) Uiso 1 1 d G . .
H12S H 0.1657 0.1050 0.5665 0.178 Uiso 1 1 calc R . .
O1 O 0.0219(7) 0.3769(8) 0.4043(5) 0.088(3) Uiso 1 1 d . . .
O2 O 0.4322(5) 0.9357(6) 0.3591(4) 0.068(3) Uani 1 1 d . . .
O11 O 0.1962(5) 0.7259(5) 0.4925(3) 0.0415(17) Uani 1 1 d . . .
O12 O 0.1096(5) 0.8640(5) 0.3319(3) 0.0483(19) Uani 1 1 d . . .
O13 O 0.1634(4) 0.5792(5) 0.2693(2) 0.0376(16) Uani 1 1 d . . .
O14 O -0.0065(4) 0.6000(6) 0.3721(3) 0.0439(18) Uani 1 1 d . . .
O21 O 0.3876(4) 0.6144(5) 0.5322(2) 0.0371(16) Uani 1 1 d . . .
O22 O 0.5540(4) 0.6002(6) 0.4218(3) 0.0432(18) Uani 1 1 d . . .
O23 O 0.3526(4) 0.4748(5) 0.3063(3) 0.0408(17) Uani 1 1 d . . .
O24 O 0.4256(4) 0.3356(5) 0.4576(3) 0.0394(17) Uani 1 1 d . . .
P1 P 0.15789(15) 0.22229(17) 0.31371(9) 0.0316(5) Uani 1 1 d . . .
P2 P 0.36259(19) 0.7837(2) 0.21391(11) 0.0521(8) Uani 1 1 d D . .
Pt1 Pt 0.16850(2) 0.35660(2) 0.363496(13) 0.02650(9) Uani 1 1 d D . .
H1 H 0.2518 0.3736 0.3386 0.032 Uiso 1 1 d RD . .
Pt2 Pt 0.35347(2) 0.76669(3) 0.300509(14) 0.03075(10) Uani 1 1 d D A .
H2 H 0.3349 0.6473 0.2935 0.037 Uiso 1 1 d RD . .
Re1 Re 0.16058(2) 0.67004(2) 0.375505(13) 0.02305(9) Uani 1 1 d . A .
Re2 Re 0.385797(19) 0.53599(2) 0.421740(12) 0.02078(9) Uani 1 1 d . A .
Sb1 Sb 0.22785(3) 0.50412(4) 0.41382(2) 0.02067(12) Uani 1 1 d . . .
Sb2 Sb 0.31908(3) 0.70378(4) 0.38426(2) 0.02157(12) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C1 Pt1 175.4(11) . . ?
O2 C2 Pt2 173.9(11) . . ?
O11 C11 Re1 175.3(9) . . ?
O12 C12 Re1 179.4(10) . . ?
O13 C13 Re1 177.5(8) . . ?
O14 C14 Re1 178.1(9) . . ?
C16 C15 C20 117.4(8) . . ?
C16 C15 Sb1 121.2(7) . . ?
C20 C15 Sb1 121.1(6) . . ?
C17 C16 C15 120.2(10) . . ?
C17 C16 H16 119.9 . . ?
C15 C16 H16 119.9 . . ?
C16 C17 C18 121.0(10) . . ?
C16 C17 H17 119.5 . . ?
C18 C17 H17 119.5 . . ?
C19 C18 C17 120.1(10) . . ?
C19 C18 H18 120.0 . . ?
C17 C18 H18 120.0 . . ?
C18 C19 C20 119.6(10) . . ?
C18 C19 H19 120.2 . . ?
C20 C19 H19 120.2 . . ?
C19 C20 C15 121.5(8) . . ?
C19 C20 H20 119.2 . . ?
C15 C20 H20 119.2 . . ?
O21 C21 Re2 177.8(8) . . ?
O22 C22 Re2 179.2(10) . . ?
O23 C23 Re2 178.9(9) . . ?
O24 C24 Re2 177.7(8) . . ?
C26 C25 C30 119.3(8) . . ?
C26 C25 Sb2 119.7(7) . . ?
C30 C25 Sb2 121.0(7) . . ?
C27 C26 C25 120.2(10) . . ?
C27 C26 H26 119.9 . . ?
C25 C26 H26 119.9 . . ?
C28 C27 C26 120.5(10) . . ?
C28 C27 H27 119.8 . . ?
C26 C27 H27 119.8 . . ?
C29 C28 C27 119.7(10) . . ?
C29 C28 H28 120.1 . . ?
C27 C28 H28 120.1 . . ?
C28 C29 C30 120.6(10) . . ?
C28 C29 H29 119.7 . . ?
C30 C29 H29 119.7 . . ?
C29 C30 C25 119.6(9) . . ?
C29 C30 H30 120.2 . . ?
C25 C30 H30 120.2 . . ?
C32 C31 C33 101.7(12) . . ?
C32 C31 C34 112.9(11) . . ?
C33 C31 C34 106.3(10) . . ?
C32 C31 P1 110.7(9) . . ?
C33 C31 P1 109.4(9) . . ?
C34 C31 P1 114.9(8) . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C31 C33 H33A 109.5 . . ?
C31 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
C31 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
C31 C34 H34A 109.5 . . ?
C31 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C31 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C36 C35 C38 111.3(12) . . ?
C36 C35 C37 104.3(12) . . ?
C38 C35 C37 104.4(10) . . ?
C36 C35 P1 113.6(8) . . ?
C38 C35 P1 115.3(9) . . ?
C37 C35 P1 106.8(9) . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C35 C37 H37A 109.5 . . ?
C35 C37 H37B 109.5 . . ?
H37A C37 H37B 109.5 . . ?
C35 C37 H37C 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C35 C38 H38A 109.5 . . ?
C35 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C35 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C41 C39 C42 109.5(9) . . ?
C41 C39 C40 106.7(12) . . ?
C42 C39 C40 107.6(9) . . ?
C41 C39 P1 111.6(9) . . ?
C42 C39 P1 114.1(8) . . ?
C40 C39 P1 107.0(7) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C45 C43 C44 107.7(16) . . ?
C45 C43 C46 104.7(16) . . ?
C44 C43 C46 108.5(15) . . ?
C45 C43 P2 108.0(16) . . ?
C44 C43 P2 115.5(15) . . ?
C46 C43 P2 111.9(13) . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C43 C45 H45A 109.5 . . ?
C43 C45 H45B 109.5 . . ?
H45A C45 H45B 109.5 . . ?
C43 C45 H45C 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
C43 C46 H46A 109.5 . . ?
C43 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C43 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C48 C47 C50 107.8(15) . . ?
C48 C47 C49 105.8(16) . . ?
C50 C47 C49 102.5(15) . . ?
C48 C47 P2 115.2(13) . . ?
C50 C47 P2 113.3(12) . . ?
C49 C47 P2 111.1(15) . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C47 C49 H49A 109.5 . . ?
C47 C49 H49B 109.5 . . ?
H49A C49 H49B 109.5 . . ?
C47 C49 H49C 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
C47 C50 H50A 109.5 . . ?
C47 C50 H50B 109.5 . . ?
H50A C50 H50B 109.5 . . ?
C47 C50 H50C 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C53 C51 C54 106.3(19) . . ?
C53 C51 C52 109.1(19) . . ?
C54 C51 C52 108.0(18) . . ?
C53 C51 P2 110.0(19) . . ?
C54 C51 P2 113.4(18) . . ?
C52 C51 P2 109.9(18) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C54 H54A 109.5 . . ?
C51 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C51 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C57 C55 C56 101.0(15) . . ?
C57 C55 C46A 104(2) . . ?
C56 C55 C46A 107(2) . . ?
C57 C55 P2 115.4(16) . . ?
C56 C55 P2 119.3(16) . . ?
C46A C55 P2 108(3) . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C55 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C55 C57 H57A 109.5 . . ?
C55 C57 H57B 109.5 . . ?
H57A C57 H57B 109.5 . . ?
C55 C57 H57C 109.5 . . ?
H57A C57 H57C 109.5 . . ?
H57B C57 H57C 109.5 . . ?
C55 C46A H46D 109.5 . . ?
C55 C46A H46E 109.5 . . ?
H46D C46A H46E 109.5 . . ?
C55 C46A H46F 109.5 . . ?
H46D C46A H46F 109.5 . . ?
H46E C46A H46F 109.5 . . ?
C59 C58 C49A 111.7(18) . . ?
C59 C58 C45A 107.4(17) . . ?
C49A C58 C45A 104.2(17) . . ?
C59 C58 P2 118.5(18) . . ?
C49A C58 P2 104.9(15) . . ?
C45A C58 P2 109.3(15) . . ?
C58 C59 H59A 109.5 . . ?
C58 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C58 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C58 C45A H45D 109.5 . . ?
C58 C45A H45E 109.5 . . ?
H45D C45A H45E 109.5 . . ?
C58 C45A H45F 109.5 . . ?
H45D C45A H45F 109.5 . . ?
H45E C45A H45F 109.5 . . ?
C58 C49A H49D 109.5 . . ?
C58 C49A H49E 109.5 . . ?
H49D C49A H49E 109.5 . . ?
C58 C49A H49F 109.5 . . ?
H49D C49A H49F 109.5 . . ?
H49E C49A H49F 109.5 . . ?
C60 C53A C61 106.9(18) . . ?
C60 C53A C62 107.8(18) . . ?
C61 C53A C62 108.0(17) . . ?
C60 C53A P2 110.9(17) . . ?
C61 C53A P2 117.1(17) . . ?
C62 C53A P2 105.8(15) . . ?
C53A C62 H62A 109.5 . . ?
C53A C62 H62B 109.5 . . ?
H62A C62 H62B 109.5 . . ?
C53A C62 H62C 109.5 . . ?
H62A C62 H62C 109.5 . . ?
H62B C62 H62C 109.5 . . ?
C53A C60 H60A 109.5 . . ?
C53A C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C53A C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C53A C61 H61A 109.5 . . ?
C53A C61 H61B 109.5 . . ?
H61A C61 H61B 109.5 . . ?
C53A C61 H61C 109.5 . . ?
H61A C61 H61C 109.5 . . ?
H61B C61 H61C 109.5 . . ?
C6S C1S C2S 121(2) . . ?
C6S C1S H1S 119.5 . . ?
C2S C1S H1S 119.5 . . ?
C3S C2S C1S 121.6(19) . . ?
C3S C2S H2S 119.2 . . ?
C1S C2S H2S 119.2 . . ?
C2S C3S C4S 119(2) . . ?
C2S C3S H3S 120.4 . . ?
C4S C3S H3S 120.4 . . ?
C5S C4S C3S 123(2) . . ?
C5S C4S H4S 118.7 . . ?
C3S C4S H4S 118.7 . . ?
C4S C5S C6S 117.4(19) . . ?
C4S C5S H5S 121.3 . . ?
C6S C5S H5S 121.3 . . ?
C1S C6S C5S 118.0(17) . . ?
C1S C6S H6S 121.0 . . ?
C5S C6S H6S 121.0 . . ?
C8S C7S C12S 120.0 . . ?
C8S C7S H7S 120.0 . . ?
C12S C7S H7S 120.0 . . ?
C7S C8S C9S 120.0 . . ?
C7S C8S H8S 120.0 . . ?
C9S C8S H8S 120.0 . . ?
C8S C9S C10S 120.0 . . ?
C8S C9S H9S 120.0 . . ?
C10S C9S H9S 120.0 . . ?
C11S C10S C9S 120.0 . . ?
C11S C10S H10S 120.0 . . ?
C9S C10S H10S 120.0 . . ?
C10S C11S C12S 120.0 . . ?
C10S C11S H11S 120.0 . . ?
C12S C11S H11S 120.0 . . ?
C11S C12S C7S 120.0 . . ?
C11S C12S H12S 120.0 . . ?
C7S C12S H12S 120.0 . . ?
C35 P1 C31 110.8(6) . . ?
C35 P1 C39 108.7(5) . . ?
C31 P1 C39 109.2(5) . . ?
C35 P1 Pt1 109.7(4) . . ?
C31 P1 Pt1 105.3(4) . . ?
C39 P1 Pt1 113.2(4) . . ?
C53A P2 C43 135.4(10) . . ?
C53A P2 C51 43.5(9) . . ?
C43 P2 C51 116.4(9) . . ?
C53A P2 C58 112.5(9) . . ?
C43 P2 C58 51.7(9) . . ?
C51 P2 C58 139.2(10) . . ?
C53A P2 C47 62.1(8) . . ?
C43 P2 C47 110.4(8) . . ?
C51 P2 C47 105.3(8) . . ?
C58 P2 C47 60.0(7) . . ?
C53A P2 C55 103.8(9) . . ?
C43 P2 C55 52.8(10) . . ?
C51 P2 C55 66.5(10) . . ?
C58 P2 C55 100.6(9) . . ?
C47 P2 C55 141.7(9) . . ?
C53A P2 Pt2 115.6(7) . . ?
C43 P2 Pt2 108.6(7) . . ?
C51 P2 Pt2 108.2(7) . . ?
C58 P2 Pt2 112.5(7) . . ?
C47 P2 Pt2 107.6(5) . . ?
C55 P2 Pt2 110.5(7) . . ?
C1 Pt1 P1 106.8(4) . . ?
C1 Pt1 Sb1 92.3(4) . . ?
P1 Pt1 Sb1 160.64(7) . . ?
C1 Pt1 H1 167.7 . . ?
P1 Pt1 H1 82.5 . . ?
Sb1 Pt1 H1 78.9 . . ?
C2 Pt2 P2 104.5(3) . . ?
C2 Pt2 Sb2 93.0(3) . . ?
P2 Pt2 Sb2 162.43(9) . . ?
C2 Pt2 H2 154.7 . . ?
P2 Pt2 H2 93.0 . . ?
Sb2 Pt2 H2 70.8 . . ?
C14 Re1 C12 95.3(4) . . ?
C14 Re1 C13 93.0(4) . . ?
C12 Re1 C13 95.6(4) . . ?
C14 Re1 C11 93.3(4) . . ?
C12 Re1 C11 95.0(4) . . ?
C13 Re1 C11 167.1(4) . . ?
C14 Re1 Sb1 93.2(3) . . ?
C12 Re1 Sb1 171.6(3) . . ?
C13 Re1 Sb1 83.5(3) . . ?
C11 Re1 Sb1 84.9(3) . . ?
C14 Re1 Sb2 170.9(3) . . ?
C12 Re1 Sb2 93.8(3) . . ?
C13 Re1 Sb2 86.2(3) . . ?
C11 Re1 Sb2 85.8(3) . . ?
Sb1 Re1 Sb2 77.763(19) . . ?
C22 Re2 C24 96.8(4) . . ?
C22 Re2 C23 92.3(4) . . ?
C24 Re2 C23 91.0(4) . . ?
C22 Re2 C21 94.4(4) . . ?
C24 Re2 C21 95.0(4) . . ?
C23 Re2 C21 170.3(4) . . ?
C22 Re2 Sb1 171.2(3) . . ?
C24 Re2 Sb1 91.7(3) . . ?
C23 Re2 Sb1 85.7(3) . . ?
C21 Re2 Sb1 86.6(2) . . ?
C22 Re2 Sb2 93.6(3) . . ?
C24 Re2 Sb2 169.3(3) . . ?
C23 Re2 Sb2 86.3(3) . . ?
C21 Re2 Sb2 86.4(3) . . ?
Sb1 Re2 Sb2 77.705(18) . . ?
C15 Sb1 Pt1 100.6(3) . . ?
C15 Sb1 Re1 108.9(2) . . ?
Pt1 Sb1 Re1 115.98(2) . . ?
C15 Sb1 Re2 112.1(2) . . ?
Pt1 Sb1 Re2 116.79(2) . . ?
Re1 Sb1 Re2 102.59(2) . . ?
C25 Sb2 Pt2 106.2(2) . . ?
C25 Sb2 Re1 109.6(3) . . ?
Pt2 Sb2 Re1 114.51(2) . . ?
C25 Sb2 Re2 107.5(2) . . ?
Pt2 Sb2 Re2 116.82(2) . . ?
Re1 Sb2 Re2 101.94(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O1 1.162(14) . ?
C1 Pt1 1.866(10) . ?
C2 O2 1.141(14) . ?
C2 Pt2 1.917(12) . ?
C11 O11 1.129(11) . ?
C11 Re1 2.000(10) . ?
C12 O12 1.140(11) . ?
C12 Re1 1.952(10) . ?
C13 O13 1.153(11) . ?
C13 Re1 1.966(10) . ?
C14 O14 1.169(12) . ?
C14 Re1 1.914(10) . ?
C15 C16 1.398(13) . ?
C15 C20 1.404(13) . ?
C15 Sb1 2.135(8) . ?
C16 C17 1.377(14) . ?
C16 H16 0.9300 . ?
C17 C18 1.387(17) . ?
C17 H17 0.9300 . ?
C18 C19 1.354(15) . ?
C18 H18 0.9300 . ?
C19 C20 1.392(12) . ?
C19 H19 0.9300 . ?
C20 H20 0.9300 . ?
C21 O21 1.142(10) . ?
C21 Re2 1.991(9) . ?
C22 O22 1.154(11) . ?
C22 Re2 1.938(9) . ?
C23 O23 1.144(11) . ?
C23 Re2 1.966(10) . ?
C24 O24 1.137(11) . ?
C24 Re2 1.948(9) . ?
C25 C26 1.390(13) . ?
C25 C30 1.401(13) . ?
C25 Sb2 2.156(8) . ?
C26 C27 1.385(14) . ?
C26 H26 0.9300 . ?
C27 C28 1.383(16) . ?
C27 H27 0.9300 . ?
C28 C29 1.376(16) . ?
C28 H28 0.9300 . ?
C29 C30 1.394(13) . ?
C29 H29 0.9300 . ?
C30 H30 0.9300 . ?
C31 C32 1.520(17) . ?
C31 C33 1.536(17) . ?
C31 C34 1.546(16) . ?
C31 P1 1.895(11) . ?
C32 H32A 0.9600 . ?
C32 H32B 0.9600 . ?
C32 H32C 0.9600 . ?
C33 H33A 0.9600 . ?
C33 H33B 0.9600 . ?
C33 H33C 0.9600 . ?
C34 H34A 0.9600 . ?
C34 H34B 0.9600 . ?
C34 H34C 0.9600 . ?
C35 C36 1.461(16) . ?
C35 C38 1.522(15) . ?
C35 C37 1.611(17) . ?
C35 P1 1.882(12) . ?
C36 H36A 0.9600 . ?
C36 H36B 0.9600 . ?
C36 H36C 0.9600 . ?
C37 H37A 0.9600 . ?
C37 H37B 0.9600 . ?
C37 H37C 0.9600 . ?
C38 H38A 0.9600 . ?
C38 H38B 0.9600 . ?
C38 H38C 0.9600 . ?
C39 C41 1.516(16) . ?
C39 C42 1.544(13) . ?
C39 C40 1.597(17) . ?
C39 P1 1.914(10) . ?
C40 H40A 0.9600 . ?
C40 H40B 0.9600 . ?
C40 H40C 0.9600 . ?
C41 H41A 0.9600 . ?
C41 H41B 0.9600 . ?
C41 H41C 0.9600 . ?
C42 H42A 0.9600 . ?
C42 H42B 0.9600 . ?
C42 H42C 0.9600 . ?
C43 C45 1.52(2) . ?
C43 C44 1.53(2) . ?
C43 C46 1.57(2) . ?
C43 P2 1.839(12) . ?
C44 H44A 0.9600 . ?
C44 H44B 0.9600 . ?
C44 H44C 0.9600 . ?
C45 H45A 0.9600 . ?
C45 H45B 0.9600 . ?
C45 H45C 0.9600 . ?
C46 H46A 0.9600 . ?
C46 H46B 0.9600 . ?
C46 H46C 0.9600 . ?
C47 C48 1.484(19) . ?
C47 C50 1.536(19) . ?
C47 C49 1.60(2) . ?
C47 P2 1.963(11) . ?
C48 H48A 0.9600 . ?
C48 H48B 0.9600 . ?
C48 H48C 0.9600 . ?
C49 H49A 0.9600 . ?
C49 H49B 0.9600 . ?
C49 H49C 0.9600 . ?
C50 H50A 0.9600 . ?
C50 H50B 0.9600 . ?
C50 H50C 0.9600 . ?
C51 C53 1.53(2) . ?
C51 C54 1.55(2) . ?
C51 C52 1.58(2) . ?
C51 P2 1.867(12) . ?
C52 H52A 0.9600 . ?
C52 H52B 0.9600 . ?
C52 H52C 0.9600 . ?
C53 H53A 0.9600 . ?
C53 H53B 0.9600 . ?
C53 H53C 0.9600 . ?
C54 H54A 0.9600 . ?
C54 H54B 0.9600 . ?
C54 H54C 0.9600 . ?
C55 C57 1.54(2) . ?
C55 C56 1.56(2) . ?
C55 C46A 1.57(2) . ?
C55 P2 1.987(13) . ?
C56 H56A 0.9600 . ?
C56 H56B 0.9600 . ?
C56 H56C 0.9600 . ?
C57 H57A 0.9600 . ?
C57 H57B 0.9600 . ?
C57 H57C 0.9600 . ?
C46A H46D 0.9600 . ?
C46A H46E 0.9600 . ?
C46A H46F 0.9600 . ?
C58 C59 1.47(2) . ?
C58 C49A 1.53(2) . ?
C58 C45A 1.59(2) . ?
C58 P2 1.904(13) . ?
C59 H59A 0.9600 . ?
C59 H59B 0.9600 . ?
C59 H59C 0.9600 . ?
C45A H45D 0.9600 . ?
C45A H45E 0.9600 . ?
C45A H45F 0.9600 . ?
C49A H49D 0.9600 . ?
C49A H49E 0.9600 . ?
C49A H49F 0.9600 . ?
C53A C60 1.52(2) . ?
C53A C61 1.55(2) . ?
C53A C62 1.58(2) . ?
C53A P2 1.83(2) . ?
C62 H62A 0.9600 . ?
C62 H62B 0.9600 . ?
C62 H62C 0.9600 . ?
C60 H60A 0.9600 . ?
C60 H60B 0.9600 . ?
C60 H60C 0.9600 . ?
C61 H61A 0.9600 . ?
C61 H61B 0.9600 . ?
C61 H61C 0.9600 . ?
C1S C6S 1.35(2) . ?
C1S C2S 1.36(2) . ?
C1S H1S 0.9300 . ?
C2S C3S 1.34(3) . ?
C2S H2S 0.9300 . ?
C3S C4S 1.36(3) . ?
C3S H3S 0.9300 . ?
C4S C5S 1.35(2) . ?
C4S H4S 0.9300 . ?
C5S C6S 1.45(2) . ?
C5S H5S 0.9300 . ?
C6S H6S 0.9300 . ?
C7S C8S 1.361(9) . ?
C7S C12S 1.362(9) . ?
C7S H7S 0.9300 . ?
C8S C9S 1.361(9) . ?
C8S H8S 0.9300 . ?
C9S C10S 1.362(9) . ?
C9S H9S 0.9300 . ?
C10S C11S 1.361(9) . ?
C10S H10S 0.9300 . ?
C11S C12S 1.362(9) . ?
C11S H11S 0.9300 . ?
C12S H12S 0.9300 . ?
P1 Pt1 2.334(2) . ?
P2 Pt2 2.351(3) . ?
Pt1 Sb1 2.6062(6) . ?
Pt1 H1 1.7540 . ?
Pt2 Sb2 2.5957(6) . ?
Pt2 H2 1.7615 . ?
Re1 Sb1 2.7660(6) . ?
Re1 Sb2 2.7794(7) . ?
Re2 Sb1 2.7685(7) . ?
Re2 Sb2 2.7804(7) . ?
