#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:13:32 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179051 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/13/4301369.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4301369
loop_
_publ_author_name
'Saovalak Sripothongnak'
'Anna M. Pischera'
'Matthew P. Espe'
'William S. Durfee'
'Christopher J. Ziegler'
_publ_section_title
;
Synthesis and Characterization of Lithium Hemiporphyrazines
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1293
_journal_page_last               1300
_journal_paper_doi               10.1021/ic800817x
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C36 H25 Li N10'
_chemical_formula_weight         604.60
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 101.078(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.593(3)
_cell_length_b                   10.444(2)
_cell_length_c                   19.979(5)
_cell_measurement_reflns_used    3167
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      25.05
_cell_measurement_theta_min      2.21
_cell_volume                     2988.2(11)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0586
_diffrn_reflns_av_sigmaI/netI    0.0625
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            24419
_diffrn_reflns_theta_full        27.00
_diffrn_reflns_theta_max         27.00
_diffrn_reflns_theta_min         1.92
_exptl_absorpt_coefficient_mu    0.084
_exptl_absorpt_correction_T_max  0.9916
_exptl_absorpt_correction_T_min  0.9672
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.344
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       block
_exptl_crystal_F_000             1256
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.264
_refine_diff_density_min         -0.214
_refine_diff_density_rms         0.046
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     428
_refine_ls_number_reflns         6519
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.049
_refine_ls_R_factor_all          0.0652
_refine_ls_R_factor_gt           0.0459
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0502P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1066
_refine_ls_wR_factor_ref         0.1136
_reflns_number_gt                4954
_reflns_number_total             6519
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic800817x_si_001_1.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        2988.2(12)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4301369
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.61719(10) 0.36594(13) 0.36472(7) 0.0161(3) Uani 1 1 d . . .
C2 C 0.60781(10) 0.38145(14) 0.43711(7) 0.0177(3) Uani 1 1 d . . .
C3 C 0.62609(10) 0.48318(14) 0.48252(7) 0.0196(3) Uani 1 1 d . . .
H3 H 0.6499 0.5621 0.4696 0.024 Uiso 1 1 calc R . .
C4 C 0.60806(10) 0.46478(15) 0.54772(7) 0.0217(3) Uani 1 1 d . . .
H4 H 0.6197 0.5326 0.5799 0.026 Uiso 1 1 calc R . .
C5 C 0.57325(10) 0.34912(14) 0.56677(7) 0.0212(3) Uani 1 1 d . . .
H5 H 0.5604 0.3401 0.6114 0.025 Uiso 1 1 calc R . .
C6 C 0.55689(10) 0.24623(14) 0.52154(7) 0.0201(3) Uani 1 1 d . . .
H6 H 0.5346 0.1664 0.5347 0.024 Uiso 1 1 calc R . .
C7 C 0.57460(10) 0.26563(13) 0.45636(7) 0.0171(3) Uani 1 1 d . . .
C8 C 0.56705(10) 0.18012(14) 0.39610(7) 0.0167(3) Uani 1 1 d . . .
C9 C 0.54645(10) -0.02510(14) 0.34626(7) 0.0174(3) Uani 1 1 d . . .
C10 C 0.58291(11) -0.14658(14) 0.36438(8) 0.0214(3) Uani 1 1 d . . .
H10 H 0.6090 -0.1652 0.4107 0.026 Uiso 1 1 calc R . .
C11 C 0.58106(11) -0.23940(14) 0.31525(8) 0.0236(4) Uani 1 1 d . . .
H11 H 0.6065 -0.3220 0.3270 0.028 Uiso 1 1 calc R . .
C12 C 0.54137(11) -0.20992(14) 0.24833(8) 0.0220(3) Uani 1 1 d . . .
H12 H 0.5381 -0.2719 0.2131 0.026 Uiso 1 1 calc R . .
C13 C 0.50671(10) -0.08757(14) 0.23435(7) 0.0177(3) Uani 1 1 d . . .
C14 C 0.46890(10) 0.04404(14) 0.12965(7) 0.0179(3) Uani 1 1 d . . .
C15 C 0.42348(10) 0.05538(14) 0.05686(8) 0.0203(3) Uani 1 1 d . . .
C16 C 0.37309(10) -0.02788(16) 0.00970(8) 0.0228(4) Uani 1 1 d . . .
H16 H 0.3596 -0.1127 0.0220 0.027 Uiso 1 1 calc R . .
C17 C 0.34286(11) 0.01752(16) -0.05652(8) 0.0247(4) Uani 1 1 d . . .
H17 H 0.3079 -0.0373 -0.0899 0.030 Uiso 1 1 calc R . .
C18 C 0.36294(11) 0.14141(16) -0.07454(8) 0.0262(4) Uani 1 1 d . . .
H18 H 0.3404 0.1705 -0.1198 0.031 Uiso 1 1 calc R . .
C19 C 0.41556(11) 0.22357(15) -0.02736(8) 0.0242(4) Uani 1 1 d . . .
H19 H 0.4307 0.3076 -0.0398 0.029 Uiso 1 1 calc R . .
C20 C 0.44513(10) 0.17825(15) 0.03848(7) 0.0207(3) Uani 1 1 d . . .
C21 C 0.50563(10) 0.23539(14) 0.09941(7) 0.0200(3) Uani 1 1 d . . .
C22 C 0.60674(10) 0.40206(14) 0.15101(7) 0.0190(3) Uani 1 1 d . . .
C23 C 0.67245(11) 0.48185(15) 0.13062(8) 0.0236(4) Uani 1 1 d . . .
H23 H 0.6747 0.4911 0.0837 0.028 Uiso 1 1 calc R . .
C24 C 0.73472(11) 0.54781(15) 0.17973(8) 0.0252(4) Uani 1 1 d . . .
H24 H 0.7819 0.6004 0.1673 0.030 Uiso 1 1 calc R . .
C25 C 0.72672(11) 0.53542(14) 0.24694(8) 0.0215(3) Uani 1 1 d . . .
H25 H 0.7675 0.5815 0.2814 0.026 Uiso 1 1 calc R . .
C26 C 0.65828(10) 0.45469(13) 0.26431(7) 0.0174(3) Uani 1 1 d . . .
C27 C 0.39639(12) 0.43286(16) 0.26444(8) 0.0288(4) Uani 1 1 d . . .
H27 H 0.4548 0.4620 0.2892 0.035 Uiso 1 1 calc R . .
C28 C 0.32024(11) 0.51286(16) 0.25997(8) 0.0287(4) Uani 1 1 d . . .
H28 H 0.3267 0.5947 0.2811 0.034 Uiso 1 1 calc R . .
C29 C 0.23475(11) 0.47261(16) 0.22455(8) 0.0255(4) Uani 1 1 d . . .
H29 H 0.1809 0.5250 0.2214 0.031 Uiso 1 1 calc R . .
C30 C 0.22960(11) 0.35447(16) 0.19383(8) 0.0290(4) Uani 1 1 d . . .
H30 H 0.1720 0.3239 0.1685 0.035 Uiso 1 1 calc R . .
C31 C 0.30968(11) 0.28040(15) 0.20034(8) 0.0261(4) Uani 1 1 d . . .
H31 H 0.3053 0.1994 0.1783 0.031 Uiso 1 1 calc R . .
C33 C 0.26363(12) 0.74410(16) 0.11072(9) 0.0315(4) Uani 1 1 d . . .
H33 H 0.2500 0.8228 0.1306 0.038 Uiso 1 1 calc R . .
C34 C 0.19025(14) 0.6697(2) 0.07908(10) 0.0468(5) Uani 1 1 d . . .
H34 H 0.1276 0.6971 0.0765 0.056 Uiso 1 1 calc R . .
C35 C 0.20953(18) 0.5549(2) 0.05129(10) 0.0547(7) Uani 1 1 d . . .
H35 H 0.1605 0.5021 0.0283 0.066 Uiso 1 1 calc R . .
C36 C 0.30099(18) 0.51797(18) 0.05734(9) 0.0485(6) Uani 1 1 d . . .
H36 H 0.3163 0.4379 0.0397 0.058 Uiso 1 1 calc R . .
C37 C 0.36995(14) 0.59849(16) 0.08923(9) 0.0354(4) Uani 1 1 d . . .
H37 H 0.4331 0.5722 0.0931 0.043 Uiso 1 1 calc R . .
H4N H 0.4333(13) -0.1333(17) 0.1423(9) 0.044(5) Uiso 1 1 d . . .
Li1 Li 0.52440(18) 0.2198(2) 0.24725(12) 0.0225(6) Uani 1 1 d . . .
N1 N 0.59085(8) 0.24540(11) 0.34230(6) 0.0165(3) Uani 1 1 d . . .
N2 N 0.54629(9) 0.05949(11) 0.40017(6) 0.0184(3) Uani 1 1 d . . .
N3 N 0.50921(8) 0.00615(11) 0.28074(6) 0.0174(3) Uani 1 1 d . . .
N4 N 0.46217(9) -0.06242(12) 0.16590(6) 0.0204(3) Uani 1 1 d . . .
N5 N 0.51623(8) 0.14757(11) 0.15373(6) 0.0189(3) Uani 1 1 d . . .
N6 N 0.54366(9) 0.34553(12) 0.09696(6) 0.0217(3) Uani 1 1 d . . .
N7 N 0.59963(8) 0.38525(11) 0.21711(6) 0.0173(3) Uani 1 1 d . . .
N8 N 0.64917(8) 0.45944(11) 0.33262(6) 0.0180(3) Uani 1 1 d . . .
N9 N 0.39277(9) 0.31658(12) 0.23592(6) 0.0220(3) Uani 1 1 d . . .
N10 N 0.35287(9) 0.71176(13) 0.11502(7) 0.0270(3) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N8 C1 N1 129.35(13) . . ?
N8 C1 C2 120.36(13) . . ?
N1 C1 C2 110.26(12) . . ?
C7 C2 C3 121.35(14) . . ?
C7 C2 C1 106.11(12) . . ?
C3 C2 C1 132.54(14) . . ?
C2 C3 C4 117.30(14) . . ?
C2 C3 H3 121.3 . . ?
C4 C3 H3 121.3 . . ?
C3 C4 C5 121.38(14) . . ?
C3 C4 H4 119.3 . . ?
C5 C4 H4 119.3 . . ?
C4 C5 C6 121.17(14) . . ?
C4 C5 H5 119.4 . . ?
C6 C5 H5 119.4 . . ?
C7 C6 C5 117.07(14) . . ?
C7 C6 H6 121.5 . . ?
C5 C6 H6 121.5 . . ?
C2 C7 C6 121.70(13) . . ?
C2 C7 C8 105.98(12) . . ?
C6 C7 C8 132.31(13) . . ?
N2 C8 N1 128.79(13) . . ?
N2 C8 C7 120.85(13) . . ?
N1 C8 C7 110.20(12) . . ?
N3 C9 N2 122.23(13) . . ?
N3 C9 C10 122.05(13) . . ?
N2 C9 C10 115.64(13) . . ?
C11 C10 C9 120.05(14) . . ?
C11 C10 H10 120.0 . . ?
C9 C10 H10 120.0 . . ?
C10 C11 C12 118.62(14) . . ?
C10 C11 H11 120.7 . . ?
C12 C11 H11 120.7 . . ?
C13 C12 C11 117.97(14) . . ?
C13 C12 H12 121.0 . . ?
C11 C12 H12 121.0 . . ?
N3 C13 C12 124.99(13) . . ?
N3 C13 N4 118.42(13) . . ?
C12 C13 N4 116.55(13) . . ?
N5 C14 N4 124.65(13) . . ?
N5 C14 C15 113.29(13) . . ?
N4 C14 C15 122.06(13) . . ?
C16 C15 C20 121.24(14) . . ?
C16 C15 C14 134.11(14) . . ?
C20 C15 C14 104.58(13) . . ?
C15 C16 C17 117.50(15) . . ?
C15 C16 H16 121.3 . . ?
C17 C16 H16 121.3 . . ?
C18 C17 C16 121.22(14) . . ?
C18 C17 H17 119.4 . . ?
C16 C17 H17 119.4 . . ?
C17 C18 C19 121.01(14) . . ?
C17 C18 H18 119.5 . . ?
C19 C18 H18 119.5 . . ?
C20 C19 C18 117.57(15) . . ?
C20 C19 H19 121.2 . . ?
C18 C19 H19 121.2 . . ?
C19 C20 C15 121.43(14) . . ?
C19 C20 C21 131.93(15) . . ?
C15 C20 C21 106.53(13) . . ?
N6 C21 N5 129.07(14) . . ?
N6 C21 C20 121.52(13) . . ?
N5 C21 C20 109.29(13) . . ?
N7 C22 C23 123.34(14) . . ?
N7 C22 N6 122.14(13) . . ?
C23 C22 N6 114.41(13) . . ?
C24 C23 C22 119.10(14) . . ?
C24 C23 H23 120.5 . . ?
C22 C23 H23 120.4 . . ?
C25 C24 C23 118.49(14) . . ?
C25 C24 H24 120.8 . . ?
C23 C24 H24 120.8 . . ?
C24 C25 C26 119.77(14) . . ?
C24 C25 H25 120.1 . . ?
C26 C25 H25 120.1 . . ?
N7 C26 N8 122.18(13) . . ?
N7 C26 C25 122.32(14) . . ?
N8 C26 C25 115.26(13) . . ?
N9 C27 C28 123.83(15) . . ?
N9 C27 H27 118.1 . . ?
C28 C27 H27 118.1 . . ?
C29 C28 C27 119.19(15) . . ?
C29 C28 H28 120.4 . . ?
C27 C28 H28 120.4 . . ?
C30 C29 C28 118.05(15) . . ?
C30 C29 H29 121.0 . . ?
C28 C29 H29 121.0 . . ?
C29 C30 C31 119.11(15) . . ?
C29 C30 H30 120.4 . . ?
C31 C30 H30 120.4 . . ?
N9 C31 C30 123.66(15) . . ?
N9 C31 H31 118.2 . . ?
C30 C31 H31 118.2 . . ?
N10 C33 C34 123.50(17) . . ?
N10 C33 H33 118.3 . . ?
C34 C33 H33 118.3 . . ?
C35 C34 C33 118.52(19) . . ?
C35 C34 H34 120.7 . . ?
C33 C34 H34 120.7 . . ?
C36 C35 C34 118.78(18) . . ?
C36 C35 H35 120.6 . . ?
C34 C35 H35 120.6 . . ?
C37 C36 C35 118.89(19) . . ?
C37 C36 H36 120.6 . . ?
C35 C36 H36 120.6 . . ?
N10 C37 C36 123.30(19) . . ?
N10 C37 H37 118.4 . . ?
C36 C37 H37 118.4 . . ?
N1 Li1 N5 151.59(15) . . ?
N1 Li1 N9 107.56(12) . . ?
N5 Li1 N9 100.84(12) . . ?
N1 Li1 N7 88.75(11) . . ?
N5 Li1 N7 89.07(11) . . ?
N9 Li1 N7 94.89(11) . . ?
N1 Li1 N3 84.88(10) . . ?
N5 Li1 N3 85.17(10) . . ?
N9 Li1 N3 110.23(12) . . ?
N7 Li1 N3 154.85(13) . . ?
C1 N1 C8 107.37(12) . . ?
C1 N1 Li1 119.63(12) . . ?
C8 N1 Li1 122.25(12) . . ?
C8 N2 C9 122.03(12) . . ?
C13 N3 C9 116.29(12) . . ?
C13 N3 Li1 119.10(11) . . ?
C9 N3 Li1 117.41(11) . . ?
C14 N4 C13 127.27(13) . . ?
C14 N4 H4N 117.2(11) . . ?
C13 N4 H4N 114.8(11) . . ?
C14 N5 C21 106.26(12) . . ?
C14 N5 Li1 125.61(12) . . ?
C21 N5 Li1 116.96(12) . . ?
C21 N6 C22 124.84(13) . . ?
C26 N7 C22 116.87(12) . . ?
C26 N7 Li1 120.87(11) . . ?
C22 N7 Li1 120.37(11) . . ?
C1 N8 C26 124.36(12) . . ?
C31 N9 C27 116.13(14) . . ?
C31 N9 Li1 128.73(13) . . ?
C27 N9 Li1 114.94(12) . . ?
C33 N10 C37 116.95(15) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 N8 1.3029(18) . ?
C1 N1 1.3663(17) . ?
C1 C2 1.488(2) . ?
C2 C7 1.385(2) . ?
C2 C3 1.389(2) . ?
C3 C4 1.391(2) . ?
C3 H3 0.9500 . ?
C4 C5 1.391(2) . ?
C4 H4 0.9500 . ?
C5 C6 1.395(2) . ?
C5 H5 0.9500 . ?
C6 C7 1.390(2) . ?
C6 H6 0.9500 . ?
C7 C8 1.4861(19) . ?
C8 N2 1.3020(18) . ?
C8 N1 1.3725(18) . ?
C9 N3 1.3571(18) . ?
C9 N2 1.3933(18) . ?
C9 C10 1.396(2) . ?
C10 C11 1.376(2) . ?
C10 H10 0.9500 . ?
C11 C12 1.386(2) . ?
C11 H11 0.9500 . ?
C12 C13 1.383(2) . ?
C12 H12 0.9500 . ?
C13 N3 1.3436(18) . ?
C13 N4 1.4213(19) . ?
C14 N5 1.3229(18) . ?
C14 N4 1.3407(19) . ?
C14 C15 1.482(2) . ?
C15 C16 1.385(2) . ?
C15 C20 1.388(2) . ?
C16 C17 1.395(2) . ?
C16 H16 0.9500 . ?
C17 C18 1.389(2) . ?
C17 H17 0.9500 . ?
C18 C19 1.392(2) . ?
C18 H18 0.9500 . ?
C19 C20 1.387(2) . ?
C19 H19 0.9500 . ?
C20 C21 1.485(2) . ?
C21 N6 1.2821(19) . ?
C21 N5 1.4066(18) . ?
C22 N7 1.3559(18) . ?
C22 C23 1.389(2) . ?
C22 N6 1.4071(19) . ?
C23 C24 1.386(2) . ?
C23 H23 0.9500 . ?
C24 C25 1.376(2) . ?
C24 H24 0.9500 . ?
C25 C26 1.401(2) . ?
C25 H25 0.9500 . ?
C26 N7 1.3555(18) . ?
C26 N8 1.3973(18) . ?
C27 N9 1.338(2) . ?
C27 C28 1.379(2) . ?
C27 H27 0.9500 . ?
C28 C29 1.376(2) . ?
C28 H28 0.9500 . ?
C29 C30 1.374(2) . ?
C29 H29 0.9500 . ?
C30 C31 1.387(2) . ?
C30 H30 0.9500 . ?
C31 N9 1.337(2) . ?
C31 H31 0.9500 . ?
C33 N10 1.332(2) . ?
C33 C34 1.375(2) . ?
C33 H33 0.9500 . ?
C34 C35 1.373(3) . ?
C34 H34 0.9500 . ?
C35 C36 1.372(3) . ?
C35 H35 0.9500 . ?
C36 C37 1.371(3) . ?
C36 H36 0.9500 . ?
C37 N10 1.333(2) . ?
C37 H37 0.9500 . ?
Li1 N1 1.978(3) . ?
Li1 N5 1.997(3) . ?
Li1 N9 2.144(3) . ?
Li1 N7 2.193(3) . ?
Li1 N3 2.352(3) . ?
N4 H4N 0.934(19) . ?
