#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:39:18 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179071 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/33/4303395.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4303395
loop_
_publ_author_name
'Jian Zhang'
'Fangrui Zheng'
'Hoi-Shan Chan'
'Zuowei Xie'
_publ_section_title
;
Reaction of a 14-Vertex Carborane with Nucleophiles: Formation
of nido-C2B12, nido-C2B11, and closo-CB11 Carborane Anions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9786
_journal_page_last               9791
_journal_paper_doi               10.1021/ic901335w
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C9 H30 B11 N O'
_chemical_formula_weight         287.25
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 109.850(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.706(3)
_cell_length_b                   12.298(3)
_cell_length_c                   13.143(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1779.7(8)
_computing_cell_refinement       'BRUKER SMART CCD DIFFRACTOMETER'
_computing_data_collection       'BRUKER SMART CCD DIFFRACTOMETER'
_computing_data_reduction        'BRUKER SMART CCD DIFFRACTOMETER'
_computing_molecular_graphics    'SIEMENS SHELXTL'
_computing_publication_material  'SIEMENS SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'BRUKER SMART CCD DIFFRACTOMETER'
_diffrn_measurement_method       'OMEGA SCAN'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0451
_diffrn_reflns_av_sigmaI/netI    0.0464
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            9414
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.02
_exptl_absorpt_coefficient_mu    0.056
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.705784
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.072
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             616
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.379
_refine_diff_density_min         -0.200
_refine_diff_density_rms         0.052
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     199
_refine_ls_number_reflns         3127
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.048
_refine_ls_R_factor_all          0.0955
_refine_ls_R_factor_gt           0.0681
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1100P)²+0.7494P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1772
_refine_ls_wR_factor_ref         0.2043
_reflns_number_gt                2180
_reflns_number_total             3127
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic901335w_si_001_1.cif
_cod_data_source_block           '[Me3NH][2b]'
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1779.6(6)
_cod_database_code               4303395
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.87648(18) 0.36820(13) 0.63469(14) 0.0513(6) Uani 1 1 d . . .
N1 N 0.8303(2) 0.15284(16) 0.58529(17) 0.0444(6) Uani 1 1 d . . .
B2 B 0.7057(2) 0.6312(2) 0.5062(2) 0.0304(6) Uani 1 1 d . . .
B3 B 0.7987(3) 0.7091(2) 0.4511(2) 0.0375(7) Uani 1 1 d . . .
H3 H 0.8983 0.7046 0.4859 0.045 Uiso 1 1 calc R . .
B4 B 0.7234(3) 0.7220(2) 0.3104(2) 0.0427(7) Uani 1 1 d . . .
H4 H 0.7743 0.7255 0.2538 0.051 Uiso 1 1 calc R . .
B5 B 0.5821(3) 0.6541(2) 0.2764(2) 0.0423(7) Uani 1 1 d . . .
H5 H 0.5410 0.6138 0.1977 0.051 Uiso 1 1 calc R . .
B6 B 0.5708(3) 0.5985(2) 0.3968(2) 0.0360(7) Uani 1 1 d . . .
H6 H 0.5217 0.5220 0.3959 0.043 Uiso 1 1 calc R . .
B7 B 0.7116(3) 0.7756(2) 0.5185(2) 0.0390(7) Uani 1 1 d . . .
H7 H 0.7537 0.8158 0.5971 0.047 Uiso 1 1 calc R . .
B8 B 0.7224(3) 0.8312(2) 0.3970(3) 0.0440(7) Uani 1 1 d . . .
H8 H 0.7716 0.9074 0.3967 0.053 Uiso 1 1 calc R . .
B9 B 0.5879(3) 0.7970(2) 0.2888(2) 0.0443(7) Uani 1 1 d . . .
H9 H 0.5498 0.8506 0.2183 0.053 Uiso 1 1 calc R . .
B10 B 0.4934(3) 0.7199(2) 0.3433(2) 0.0432(7) Uani 1 1 d . . .
H10 H 0.3937 0.7234 0.3084 0.052 Uiso 1 1 calc R . .
B11 B 0.5704(3) 0.7063(2) 0.4855(2) 0.0378(7) Uani 1 1 d . . .
H11 H 0.5207 0.7010 0.5429 0.045 Uiso 1 1 calc R . .
B12 B 0.5808(3) 0.8298(2) 0.4183(2) 0.0430(7) Uani 1 1 d . . .
H12 H 0.5377 0.9052 0.4322 0.052 Uiso 1 1 calc R . .
C1 C 0.7081(2) 0.60717(18) 0.37816(18) 0.0331(6) Uani 1 1 d . . .
C11 C 0.7697(3) 0.5022(2) 0.3620(2) 0.0445(7) Uani 1 1 d . . .
H11A H 0.7215 0.4702 0.2934 0.053 Uiso 1 1 calc R . .
H11B H 0.8485 0.5202 0.3576 0.053 Uiso 1 1 calc R . .
C12 C 0.7868(3) 0.4181(2) 0.4506(2) 0.0478(7) Uani 1 1 d . . .
H12A H 0.7082 0.3879 0.4444 0.057 Uiso 1 1 calc R . .
H12B H 0.8366 0.3593 0.4395 0.057 Uiso 1 1 calc R . .
C13 C 0.8454(2) 0.46243(19) 0.5636(2) 0.0416(6) Uani 1 1 d . . .
H13A H 0.9206 0.4999 0.5672 0.050 Uiso 1 1 calc R . .
C14 C 0.7650(2) 0.54172(19) 0.59649(18) 0.0363(6) Uani 1 1 d . . .
H14A H 0.8128 0.5778 0.6629 0.044 Uiso 1 1 calc R . .
H14B H 0.7008 0.5016 0.6109 0.044 Uiso 1 1 calc R . .
C15 C 0.9425(3) 0.3921(3) 0.7451(2) 0.0648(9) Uani 1 1 d . . .
H15A H 0.9592 0.3258 0.7861 0.097 Uiso 1 1 calc R . .
H15B H 0.8952 0.4395 0.7732 0.097 Uiso 1 1 calc R . .
H15C H 1.0176 0.4271 0.7504 0.097 Uiso 1 1 calc R . .
C16 C 0.8327(6) 0.1023(3) 0.6871(3) 0.1229(19) Uani 1 1 d U . .
H16A H 0.7671 0.1305 0.7076 0.184 Uiso 1 1 calc R . .
H16B H 0.9085 0.1184 0.7428 0.184 Uiso 1 1 calc R . .
H16C H 0.8239 0.0250 0.6777 0.184 Uiso 1 1 calc R . .
C17 C 0.7119(3) 0.1331(3) 0.5001(4) 0.0977(15) Uani 1 1 d . . .
H17A H 0.6479 0.1589 0.5242 0.147 Uiso 1 1 calc R . .
H17B H 0.7018 0.0566 0.4855 0.147 Uiso 1 1 calc R . .
H17C H 0.7090 0.1710 0.4355 0.147 Uiso 1 1 calc R . .
C18 C 0.9277(4) 0.1139(3) 0.5493(4) 0.0933(14) Uani 1 1 d . . .
H18A H 0.9223 0.1490 0.4826 0.140 Uiso 1 1 calc R . .
H18B H 0.9204 0.0367 0.5384 0.140 Uiso 1 1 calc R . .
H18C H 1.0047 0.1304 0.6032 0.140 Uiso 1 1 calc R . .
H1 H 0.8397 0.2263 0.5980 0.050 Uiso 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C15 O1 C13 114.9(2) . . ?
C18 N1 C16 112.5(3) . . ?
C18 N1 C17 109.7(3) . . ?
C16 N1 C17 110.1(3) . . ?
C14 B2 C1 117.57(18) . . ?
C14 B2 B11 127.91(19) . . ?
C1 B2 B11 104.48(18) . . ?
C14 B2 B3 120.2(2) . . ?
C1 B2 B3 58.52(14) . . ?
B11 B2 B3 107.16(18) . . ?
C14 B2 B7 128.8(2) . . ?
C1 B2 B7 104.27(18) . . ?
B11 B2 B7 59.98(15) . . ?
B3 B2 B7 59.31(15) . . ?
C14 B2 B6 119.2(2) . . ?
C1 B2 B6 58.44(14) . . ?
B11 B2 B6 59.53(15) . . ?
B3 B2 B6 106.87(18) . . ?
B7 B2 B6 107.07(19) . . ?
C1 B3 B7 105.54(19) . . ?
C1 B3 B4 58.97(15) . . ?
B7 B3 B4 108.5(2) . . ?
C1 B3 B8 105.4(2) . . ?
B7 B3 B8 60.54(16) . . ?
B4 B3 B8 59.88(16) . . ?
C1 B3 B2 58.99(14) . . ?
B7 B3 B2 60.49(15) . . ?
B4 B3 B2 108.6(2) . . ?
B8 B3 B2 109.0(2) . . ?
C1 B4 B8 105.53(19) . . ?
C1 B4 B3 58.90(15) . . ?
B8 B4 B3 60.16(16) . . ?
C1 B4 B5 59.20(15) . . ?
B8 B4 B5 108.1(2) . . ?
B3 B4 B5 108.2(2) . . ?
C1 B4 B9 105.5(2) . . ?
B8 B4 B9 60.33(17) . . ?
B3 B4 B9 108.4(2) . . ?
B5 B4 B9 59.74(17) . . ?
C1 B5 B9 105.5(2) . . ?
C1 B5 B10 105.10(19) . . ?
B9 B5 B10 60.61(17) . . ?
C1 B5 B4 58.71(16) . . ?
B9 B5 B4 60.22(17) . . ?
B10 B5 B4 108.4(2) . . ?
C1 B5 B6 58.66(15) . . ?
B9 B5 B6 108.3(2) . . ?
B10 B5 B6 59.81(16) . . ?
B4 B5 B6 107.7(2) . . ?
C1 B6 B10 105.69(19) . . ?
C1 B6 B11 105.14(19) . . ?
B10 B6 B11 60.80(16) . . ?
C1 B6 B5 59.20(15) . . ?
B10 B6 B5 60.03(16) . . ?
B11 B6 B5 108.5(2) . . ?
C1 B6 B2 58.88(14) . . ?
B10 B6 B2 109.00(19) . . ?
B11 B6 B2 59.95(15) . . ?
B5 B6 B2 108.6(2) . . ?
B3 B7 B12 107.6(2) . . ?
B3 B7 B11 107.66(19) . . ?
B12 B7 B11 60.21(16) . . ?
B3 B7 B8 59.92(16) . . ?
B12 B7 B8 59.81(17) . . ?
B11 B7 B8 108.0(2) . . ?
B3 B7 B2 60.20(15) . . ?
B12 B7 B2 108.1(2) . . ?
B11 B7 B2 59.73(15) . . ?
B8 B7 B2 108.31(19) . . ?
B4 B8 B3 59.96(16) . . ?
B4 B8 B12 107.8(2) . . ?
B3 B8 B12 107.4(2) . . ?
B4 B8 B9 60.08(17) . . ?
B3 B8 B9 108.0(2) . . ?
B12 B8 B9 60.17(17) . . ?
B4 B8 B7 107.72(19) . . ?
B3 B8 B7 59.54(16) . . ?
B12 B8 B7 59.96(17) . . ?
B9 B8 B7 108.3(2) . . ?
B5 B9 B4 60.04(17) . . ?
B5 B9 B8 107.8(2) . . ?
B4 B9 B8 59.59(17) . . ?
B5 B9 B12 107.5(2) . . ?
B4 B9 B12 107.1(2) . . ?
B8 B9 B12 59.78(17) . . ?
B5 B9 B10 59.80(17) . . ?
B4 B9 B10 107.6(2) . . ?
B8 B9 B10 107.8(2) . . ?
B12 B9 B10 59.91(17) . . ?
B6 B10 B5 60.16(16) . . ?
B6 B10 B12 107.5(2) . . ?
B5 B10 B12 107.4(2) . . ?
B6 B10 B9 107.8(2) . . ?
B5 B10 B9 59.59(17) . . ?
B12 B10 B9 59.96(17) . . ?
B6 B10 B11 59.65(15) . . ?
B5 B10 B11 107.7(2) . . ?
B12 B10 B11 59.99(16) . . ?
B9 B10 B11 108.0(2) . . ?
B6 B11 B2 60.52(15) . . ?
B6 B11 B7 108.08(19) . . ?
B2 B11 B7 60.29(15) . . ?
B6 B11 B12 107.29(19) . . ?
B2 B11 B12 108.2(2) . . ?
B7 B11 B12 59.83(16) . . ?
B6 B11 B10 59.55(16) . . ?
B2 B11 B10 108.46(19) . . ?
B7 B11 B10 107.9(2) . . ?
B12 B11 B10 59.79(16) . . ?
B8 B12 B7 60.23(17) . . ?
B8 B12 B10 108.2(2) . . ?
B7 B12 B10 108.3(2) . . ?
B8 B12 B9 60.04(18) . . ?
B7 B12 B9 108.4(2) . . ?
B10 B12 B9 60.12(17) . . ?
B8 B12 B11 108.2(2) . . ?
B7 B12 B11 59.97(16) . . ?
B10 B12 B11 60.22(16) . . ?
B9 B12 B11 108.3(2) . . ?
C11 C1 B3 117.7(2) . . ?
C11 C1 B6 118.6(2) . . ?
B3 C1 B6 113.52(18) . . ?
C11 C1 B4 119.12(19) . . ?
B3 C1 B4 62.13(16) . . ?
B6 C1 B4 113.32(19) . . ?
C11 C1 B2 116.55(18) . . ?
B3 C1 B2 62.49(15) . . ?
B6 C1 B2 62.69(15) . . ?
B4 C1 B2 114.06(18) . . ?
C11 C1 B5 119.7(2) . . ?
B3 C1 B5 113.25(19) . . ?
B6 C1 B5 62.14(16) . . ?
B4 C1 B5 62.09(17) . . ?
B2 C1 B5 114.14(19) . . ?
C12 C11 C1 114.46(19) . . ?
C13 C12 C11 113.9(2) . . ?
O1 C13 C12 105.96(19) . . ?
O1 C13 C14 111.9(2) . . ?
C12 C13 C14 113.2(2) . . ?
C13 C14 B2 112.76(19) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C15 1.424(3) . ?
O1 C13 1.455(3) . ?
N1 C18 1.456(4) . ?
N1 C16 1.467(4) . ?
N1 C17 1.477(4) . ?
B2 C14 1.594(3) . ?
B2 C1 1.718(3) . ?
B2 B11 1.773(4) . ?
B2 B3 1.778(4) . ?
B2 B7 1.783(4) . ?
B2 B6 1.783(4) . ?
B3 C1 1.710(4) . ?
B3 B7 1.762(4) . ?
B3 B4 1.765(4) . ?
B3 B8 1.769(4) . ?
B4 C1 1.711(3) . ?
B4 B8 1.764(4) . ?
B4 B5 1.770(4) . ?
B4 B9 1.773(4) . ?
B5 C1 1.720(4) . ?
B5 B9 1.764(4) . ?
B5 B10 1.768(4) . ?
B5 B6 1.770(4) . ?
B6 C1 1.710(4) . ?
B6 B10 1.764(4) . ?
B6 B11 1.766(4) . ?
B7 B12 1.775(4) . ?
B7 B11 1.778(4) . ?
B7 B8 1.780(4) . ?
B8 B12 1.772(4) . ?
B8 B9 1.777(4) . ?
B9 B12 1.779(4) . ?
B9 B10 1.782(4) . ?
B10 B12 1.778(4) . ?
B10 B11 1.786(4) . ?
B11 B12 1.782(4) . ?
C1 C11 1.528(3) . ?
C11 C12 1.520(3) . ?
C12 C13 1.510(4) . ?
C13 C14 1.517(3) . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
N1 H1 O1 0.92 1.82 2.737(3) 173.1 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C14 B2 B3 C1 105.8(2) . . . . ?
B11 B2 B3 C1 -96.77(19) . . . . ?
B7 B2 B3 C1 -134.4(2) . . . . ?
B6 B2 B3 C1 -34.21(17) . . . . ?
C14 B2 B3 B7 -119.9(2) . . . . ?
C1 B2 B3 B7 134.4(2) . . . . ?
B11 B2 B3 B7 37.62(18) . . . . ?
B6 B2 B3 B7 100.2(2) . . . . ?
C14 B2 B3 B4 139.0(2) . . . . ?
C1 B2 B3 B4 33.23(17) . . . . ?
B11 B2 B3 B4 -63.5(2) . . . . ?
B7 B2 B3 B4 -101.2(2) . . . . ?
B6 B2 B3 B4 -1.0(2) . . . . ?
C14 B2 B3 B8 -157.4(2) . . . . ?
C1 B2 B3 B8 96.9(2) . . . . ?
B11 B2 B3 B8 0.1(3) . . . . ?
B7 B2 B3 B8 -37.52(19) . . . . ?
B6 B2 B3 B8 62.7(2) . . . . ?
B7 B3 B4 C1 -97.4(2) . . . . ?
B8 B3 B4 C1 -134.9(2) . . . . ?
B2 B3 B4 C1 -33.23(17) . . . . ?
C1 B3 B4 B8 134.9(2) . . . . ?
B7 B3 B4 B8 37.54(19) . . . . ?
B2 B3 B4 B8 101.7(2) . . . . ?
C1 B3 B4 B5 34.05(18) . . . . ?
B7 B3 B4 B5 -63.4(2) . . . . ?
B8 B3 B4 B5 -100.9(2) . . . . ?
B2 B3 B4 B5 0.8(3) . . . . ?
C1 B3 B4 B9 97.3(2) . . . . ?
B7 B3 B4 B9 -0.1(3) . . . . ?
B8 B3 B4 B9 -37.6(2) . . . . ?
B2 B3 B4 B9 64.1(2) . . . . ?
B8 B4 B5 C1 -97.6(2) . . . . ?
B3 B4 B5 C1 -33.93(18) . . . . ?
B9 B4 B5 C1 -135.0(2) . . . . ?
C1 B4 B5 B9 135.0(2) . . . . ?
B8 B4 B5 B9 37.41(19) . . . . ?
B3 B4 B5 B9 101.1(2) . . . . ?
C1 B4 B5 B10 96.8(2) . . . . ?
B8 B4 B5 B10 -0.8(3) . . . . ?
B3 B4 B5 B10 62.9(2) . . . . ?
B9 B4 B5 B10 -38.18(19) . . . . ?
C1 B4 B5 B6 33.61(18) . . . . ?
B8 B4 B5 B6 -64.0(2) . . . . ?
B3 B4 B5 B6 -0.3(3) . . . . ?
B9 B4 B5 B6 -101.4(2) . . . . ?
B9 B5 B6 C1 -97.3(2) . . . . ?
B10 B5 B6 C1 -135.0(2) . . . . ?
B4 B5 B6 C1 -33.63(18) . . . . ?
C1 B5 B6 B10 135.0(2) . . . . ?
B9 B5 B6 B10 37.7(2) . . . . ?
B4 B5 B6 B10 101.4(2) . . . . ?
C1 B5 B6 B11 96.9(2) . . . . ?
B9 B5 B6 B11 -0.4(3) . . . . ?
B10 B5 B6 B11 -38.1(2) . . . . ?
B4 B5 B6 B11 63.3(3) . . . . ?
C1 B5 B6 B2 33.33(17) . . . . ?
B9 B5 B6 B2 -64.0(3) . . . . ?
B10 B5 B6 B2 -101.7(2) . . . . ?
B4 B5 B6 B2 -0.3(3) . . . . ?
C14 B2 B6 C1 -106.2(2) . . . . ?
B11 B2 B6 C1 134.57(19) . . . . ?
B3 B2 B6 C1 34.25(17) . . . . ?
B7 B2 B6 C1 96.55(19) . . . . ?
C14 B2 B6 B10 156.5(2) . . . . ?
C1 B2 B6 B10 -97.3(2) . . . . ?
B11 B2 B6 B10 37.32(19) . . . . ?
B3 B2 B6 B10 -63.0(2) . . . . ?
B7 B2 B6 B10 -0.7(3) . . . . ?
C14 B2 B6 B11 119.2(2) . . . . ?
C1 B2 B6 B11 -134.57(19) . . . . ?
B3 B2 B6 B11 -100.3(2) . . . . ?
B7 B2 B6 B11 -38.03(18) . . . . ?
C14 B2 B6 B5 -139.7(2) . . . . ?
C1 B2 B6 B5 -33.46(18) . . . . ?
B11 B2 B6 B5 101.1(2) . . . . ?
B3 B2 B6 B5 0.8(2) . . . . ?
B7 B2 B6 B5 63.1(2) . . . . ?
C1 B3 B7 B12 -61.7(2) . . . . ?
B4 B3 B7 B12 0.2(3) . . . . ?
B8 B3 B7 B12 37.5(2) . . . . ?
B2 B3 B7 B12 -101.1(2) . . . . ?
C1 B3 B7 B11 1.8(2) . . . . ?
B4 B3 B7 B11 63.7(2) . . . . ?
B8 B3 B7 B11 101.0(2) . . . . ?
B2 B3 B7 B11 -37.63(18) . . . . ?
C1 B3 B7 B8 -99.1(2) . . . . ?
B4 B3 B7 B8 -37.25(19) . . . . ?
B2 B3 B7 B8 -138.6(2) . . . . ?
C1 B3 B7 B2 39.47(17) . . . . ?
B4 B3 B7 B2 101.4(2) . . . . ?
B8 B3 B7 B2 138.6(2) . . . . ?
C14 B2 B7 B3 105.9(3) . . . . ?
C1 B2 B7 B3 -38.97(18) . . . . ?
B11 B2 B7 B3 -137.7(2) . . . . ?
B6 B2 B7 B3 -99.8(2) . . . . ?
C14 B2 B7 B12 -153.8(2) . . . . ?
C1 B2 B7 B12 61.4(2) . . . . ?
B11 B2 B7 B12 -37.29(19) . . . . ?
B3 B2 B7 B12 100.4(2) . . . . ?
B6 B2 B7 B12 0.5(3) . . . . ?
C14 B2 B7 B11 -116.5(3) . . . . ?
C1 B2 B7 B11 98.68(19) . . . . ?
B3 B2 B7 B11 137.7(2) . . . . ?
B6 B2 B7 B11 37.82(18) . . . . ?
C14 B2 B7 B8 142.9(2) . . . . ?
C1 B2 B7 B8 -1.9(3) . . . . ?
B11 B2 B7 B8 -100.6(2) . . . . ?
B3 B2 B7 B8 37.06(19) . . . . ?
B6 B2 B7 B8 -62.8(2) . . . . ?
C1 B4 B8 B3 38.98(19) . . . . ?
B5 B4 B8 B3 101.1(2) . . . . ?
B9 B4 B8 B3 138.2(2) . . . . ?
C1 B4 B8 B12 -61.2(3) . . . . ?
B3 B4 B8 B12 -100.2(2) . . . . ?
B5 B4 B8 B12 0.8(3) . . . . ?
B9 B4 B8 B12 38.0(2) . . . . ?
C1 B4 B8 B9 -99.2(2) . . . . ?
B3 B4 B8 B9 -138.2(2) . . . . ?
B5 B4 B8 B9 -37.15(19) . . . . ?
C1 B4 B8 B7 2.1(3) . . . . ?
B3 B4 B8 B7 -36.9(2) . . . . ?
B5 B4 B8 B7 64.1(3) . . . . ?
B9 B4 B8 B7 101.3(2) . . . . ?
C1 B3 B8 B4 -38.98(18) . . . . ?
B7 B3 B8 B4 -138.4(2) . . . . ?
B2 B3 B8 B4 -100.9(2) . . . . ?
C1 B3 B8 B12 61.9(2) . . . . ?
B7 B3 B8 B12 -37.5(2) . . . . ?
B4 B3 B8 B12 100.9(2) . . . . ?
B2 B3 B8 B12 0.0(3) . . . . ?
C1 B3 B8 B9 -1.6(3) . . . . ?
B7 B3 B8 B9 -101.0(2) . . . . ?
B4 B3 B8 B9 37.4(2) . . . . ?
B2 B3 B8 B9 -63.5(3) . . . . ?
C1 B3 B8 B7 99.4(2) . . . . ?
B4 B3 B8 B7 138.4(2) . . . . ?
B2 B3 B8 B7 37.50(19) . . . . ?
B3 B7 B8 B4 37.1(2) . . . . ?
B12 B7 B8 B4 -100.8(2) . . . . ?
B11 B7 B8 B4 -63.3(3) . . . . ?
B2 B7 B8 B4 -0.1(3) . . . . ?
B12 B7 B8 B3 -137.9(2) . . . . ?
B11 B7 B8 B3 -100.4(2) . . . . ?
B2 B7 B8 B3 -37.18(19) . . . . ?
B3 B7 B8 B12 137.9(2) . . . . ?
B11 B7 B8 B12 37.48(19) . . . . ?
B2 B7 B8 B12 100.7(2) . . . . ?
B3 B7 B8 B9 100.6(2) . . . . ?
B12 B7 B8 B9 -37.3(2) . . . . ?
B11 B7 B8 B9 0.2(3) . . . . ?
B2 B7 B8 B9 63.4(3) . . . . ?
C1 B5 B9 B4 38.80(18) . . . . ?
B10 B5 B9 B4 137.7(2) . . . . ?
B6 B5 B9 B4 100.3(2) . . . . ?
C1 B5 B9 B8 1.8(3) . . . . ?
B10 B5 B9 B8 100.7(2) . . . . ?
B4 B5 B9 B8 -37.0(2) . . . . ?
B6 B5 B9 B8 63.3(3) . . . . ?
C1 B5 B9 B12 -61.3(3) . . . . ?
B10 B5 B9 B12 37.6(2) . . . . ?
B4 B5 B9 B12 -100.1(2) . . . . ?
B6 B5 B9 B12 0.3(3) . . . . ?
C1 B5 B9 B10 -98.9(2) . . . . ?
B4 B5 B9 B10 -137.7(2) . . . . ?
B6 B5 B9 B10 -37.4(2) . . . . ?
C1 B4 B9 B5 -39.04(18) . . . . ?
B8 B4 B9 B5 -138.4(2) . . . . ?
B3 B4 B9 B5 -100.8(2) . . . . ?
C1 B4 B9 B8 99.3(2) . . . . ?
B3 B4 B9 B8 37.53(19) . . . . ?
B5 B4 B9 B8 138.4(2) . . . . ?
C1 B4 B9 B12 61.7(3) . . . . ?
B8 B4 B9 B12 -37.6(2) . . . . ?
B3 B4 B9 B12 -0.1(3) . . . . ?
B5 B4 B9 B12 100.7(2) . . . . ?
C1 B4 B9 B10 -1.4(3) . . . . ?
B8 B4 B9 B10 -100.7(2) . . . . ?
B3 B4 B9 B10 -63.2(3) . . . . ?
B5 B4 B9 B10 37.6(2) . . . . ?
B4 B8 B9 B5 37.2(2) . . . . ?
B3 B8 B9 B5 -0.1(3) . . . . ?
B12 B8 B9 B5 -100.3(2) . . . . ?
B7 B8 B9 B5 -63.2(3) . . . . ?
B3 B8 B9 B4 -37.35(19) . . . . ?
B12 B8 B9 B4 -137.5(2) . . . . ?
B7 B8 B9 B4 -100.4(2) . . . . ?
B4 B8 B9 B12 137.5(2) . . . . ?
B3 B8 B9 B12 100.2(2) . . . . ?
B7 B8 B9 B12 37.16(19) . . . . ?
B4 B8 B9 B10 100.3(2) . . . . ?
B3 B8 B9 B10 63.0(3) . . . . ?
B12 B8 B9 B10 -37.17(19) . . . . ?
B7 B8 B9 B10 0.0(3) . . . . ?
C1 B6 B10 B5 39.11(18) . . . . ?
B11 B6 B10 B5 138.0(2) . . . . ?
B2 B6 B10 B5 101.0(2) . . . . ?
C1 B6 B10 B12 -61.3(2) . . . . ?
B11 B6 B10 B12 37.56(19) . . . . ?
B5 B6 B10 B12 -100.4(2) . . . . ?
B2 B6 B10 B12 0.6(3) . . . . ?
C1 B6 B10 B9 2.0(3) . . . . ?
B11 B6 B10 B9 100.8(2) . . . . ?
B5 B6 B10 B9 -37.1(2) . . . . ?
B2 B6 B10 B9 63.9(2) . . . . ?
C1 B6 B10 B11 -98.8(2) . . . . ?
B5 B6 B10 B11 -138.0(2) . . . . ?
B2 B6 B10 B11 -36.95(19) . . . . ?
C1 B5 B10 B6 -38.71(18) . . . . ?
B9 B5 B10 B6 -138.2(2) . . . . ?
B4 B5 B10 B6 -100.2(2) . . . . ?
C1 B5 B10 B12 61.9(2) . . . . ?
B9 B5 B10 B12 -37.61(19) . . . . ?
B4 B5 B10 B12 0.4(3) . . . . ?
B6 B5 B10 B12 100.6(2) . . . . ?
C1 B5 B10 B9 99.5(2) . . . . ?
B4 B5 B10 B9 38.00(19) . . . . ?
B6 B5 B10 B9 138.2(2) . . . . ?
C1 B5 B10 B11 -1.4(3) . . . . ?
B9 B5 B10 B11 -100.9(2) . . . . ?
B4 B5 B10 B11 -62.9(2) . . . . ?
B6 B5 B10 B11 37.35(19) . . . . ?
B5 B9 B10 B6 37.38(19) . . . . ?
B4 B9 B10 B6 -0.3(3) . . . . ?
B8 B9 B10 B6 -63.2(3) . . . . ?
B12 B9 B10 B6 -100.3(2) . . . . ?
B4 B9 B10 B5 -37.7(2) . . . . ?
B8 B9 B10 B5 -100.6(2) . . . . ?
B12 B9 B10 B5 -137.7(2) . . . . ?
B5 B9 B10 B12 137.7(2) . . . . ?
B4 B9 B10 B12 100.0(2) . . . . ?
B8 B9 B10 B12 37.1(2) . . . . ?
B5 B9 B10 B11 100.4(2) . . . . ?
B4 B9 B10 B11 62.7(3) . . . . ?
B8 B9 B10 B11 -0.2(3) . . . . ?
B12 B9 B10 B11 -37.32(19) . . . . ?
C1 B6 B11 B2 -39.18(17) . . . . ?
B10 B6 B11 B2 -139.0(2) . . . . ?
B5 B6 B11 B2 -101.2(2) . . . . ?
C1 B6 B11 B7 -0.8(2) . . . . ?
B10 B6 B11 B7 -100.5(2) . . . . ?
B5 B6 B11 B7 -62.8(2) . . . . ?
B2 B6 B11 B7 38.42(18) . . . . ?
C1 B6 B11 B12 62.4(2) . . . . ?
B10 B6 B11 B12 -37.4(2) . . . . ?
B5 B6 B11 B12 0.3(3) . . . . ?
B2 B6 B11 B12 101.5(2) . . . . ?
C1 B6 B11 B10 99.8(2) . . . . ?
B5 B6 B11 B10 37.7(2) . . . . ?
B2 B6 B11 B10 139.0(2) . . . . ?
C14 B2 B11 B6 -105.0(3) . . . . ?
C1 B2 B11 B6 38.82(17) . . . . ?
B3 B2 B11 B6 99.8(2) . . . . ?
B7 B2 B11 B6 137.1(2) . . . . ?
C14 B2 B11 B7 117.9(3) . . . . ?
C1 B2 B11 B7 -98.33(19) . . . . ?
B3 B2 B11 B7 -37.32(18) . . . . ?
B6 B2 B11 B7 -137.1(2) . . . . ?
C14 B2 B11 B12 155.0(2) . . . . ?
C1 B2 B11 B12 -61.2(2) . . . . ?
B3 B2 B11 B12 -0.2(2) . . . . ?
B7 B2 B11 B12 37.16(19) . . . . ?
B6 B2 B11 B12 -100.0(2) . . . . ?
C14 B2 B11 B10 -141.6(2) . . . . ?
C1 B2 B11 B10 2.2(2) . . . . ?
B3 B2 B11 B10 63.2(2) . . . . ?
B7 B2 B11 B10 100.5(2) . . . . ?
B6 B2 B11 B10 -36.64(18) . . . . ?
B3 B7 B11 B6 -0.7(3) . . . . ?
B12 B7 B11 B6 99.9(2) . . . . ?
B8 B7 B11 B6 62.6(2) . . . . ?
B2 B7 B11 B6 -38.52(18) . . . . ?
B3 B7 B11 B2 37.84(18) . . . . ?
B12 B7 B11 B2 138.4(2) . . . . ?
B8 B7 B11 B2 101.1(2) . . . . ?
B3 B7 B11 B12 -100.6(2) . . . . ?
B8 B7 B11 B12 -37.30(18) . . . . ?
B2 B7 B11 B12 -138.4(2) . . . . ?
B3 B7 B11 B10 -63.6(2) . . . . ?
B12 B7 B11 B10 36.95(19) . . . . ?
B8 B7 B11 B10 -0.4(3) . . . . ?
B2 B7 B11 B10 -101.5(2) . . . . ?
B5 B10 B11 B6 -37.58(19) . . . . ?
B12 B10 B11 B6 -137.8(2) . . . . ?
B9 B10 B11 B6 -100.5(2) . . . . ?
B6 B10 B11 B2 37.06(19) . . . . ?
B5 B10 B11 B2 -0.5(3) . . . . ?
B12 B10 B11 B2 -100.8(2) . . . . ?
B9 B10 B11 B2 -63.5(2) . . . . ?
B6 B10 B11 B7 100.9(2) . . . . ?
B5 B10 B11 B7 63.3(2) . . . . ?
B12 B10 B11 B7 -36.96(19) . . . . ?
B9 B10 B11 B7 0.3(3) . . . . ?
B6 B10 B11 B12 137.8(2) . . . . ?
B5 B10 B11 B12 100.3(2) . . . . ?
B9 B10 B11 B12 37.31(19) . . . . ?
B4 B8 B12 B7 100.6(2) . . . . ?
B3 B8 B12 B7 37.31(19) . . . . ?
B9 B8 B12 B7 138.5(2) . . . . ?
B4 B8 B12 B10 -0.6(3) . . . . ?
B3 B8 B12 B10 -63.8(3) . . . . ?
B9 B8 B12 B10 37.35(19) . . . . ?
B7 B8 B12 B10 -101.1(2) . . . . ?
B4 B8 B12 B9 -37.9(2) . . . . ?
B3 B8 B12 B9 -101.2(2) . . . . ?
B7 B8 B12 B9 -138.5(2) . . . . ?
B4 B8 B12 B11 63.1(3) . . . . ?
B3 B8 B12 B11 -0.1(3) . . . . ?
B9 B8 B12 B11 101.1(2) . . . . ?
B7 B8 B12 B11 -37.41(19) . . . . ?
B3 B7 B12 B8 -37.52(19) . . . . ?
B11 B7 B12 B8 -138.2(2) . . . . ?
B2 B7 B12 B8 -101.1(2) . . . . ?
B3 B7 B12 B10 63.4(3) . . . . ?
B11 B7 B12 B10 -37.2(2) . . . . ?
B8 B7 B12 B10 100.9(2) . . . . ?
B2 B7 B12 B10 -0.2(3) . . . . ?
B3 B7 B12 B9 -0.3(3) . . . . ?
B11 B7 B12 B9 -101.0(2) . . . . ?
B8 B7 B12 B9 37.2(2) . . . . ?
B2 B7 B12 B9 -63.9(3) . . . . ?
B3 B7 B12 B11 100.7(2) . . . . ?
B8 B7 B12 B11 138.2(2) . . . . ?
B2 B7 B12 B11 37.08(18) . . . . ?
B6 B10 B12 B8 63.5(3) . . . . ?
B5 B10 B12 B8 0.1(3) . . . . ?
B9 B10 B12 B8 -37.3(2) . . . . ?
B11 B10 B12 B8 100.9(2) . . . . ?
B6 B10 B12 B7 -0.3(3) . . . . ?
B5 B10 B12 B7 -63.7(3) . . . . ?
B9 B10 B12 B7 -101.1(2) . . . . ?
B11 B10 B12 B7 37.14(19) . . . . ?
B6 B10 B12 B9 100.8(2) . . . . ?
B5 B10 B12 B9 37.44(19) . . . . ?
B11 B10 B12 B9 138.2(2) . . . . ?
B6 B10 B12 B11 -37.41(19) . . . . ?
B5 B10 B12 B11 -100.8(2) . . . . ?
B9 B10 B12 B11 -138.2(2) . . . . ?
B5 B9 B12 B8 100.8(2) . . . . ?
B4 B9 B12 B8 37.56(19) . . . . ?
B10 B9 B12 B8 138.3(2) . . . . ?
B5 B9 B12 B7 63.5(3) . . . . ?
B4 B9 B12 B7 0.3(3) . . . . ?
B8 B9 B12 B7 -37.3(2) . . . . ?
B10 B9 B12 B7 101.0(2) . . . . ?
B5 B9 B12 B10 -37.6(2) . . . . ?
B4 B9 B12 B10 -100.8(2) . . . . ?
B8 B9 B12 B10 -138.3(2) . . . . ?
B5 B9 B12 B11 -0.1(3) . . . . ?
B4 B9 B12 B11 -63.3(3) . . . . ?
B8 B9 B12 B11 -100.8(2) . . . . ?
B10 B9 B12 B11 37.5(2) . . . . ?
B6 B11 B12 B8 -63.7(3) . . . . ?
B2 B11 B12 B8 0.2(3) . . . . ?
B7 B11 B12 B8 37.5(2) . . . . ?
B10 B11 B12 B8 -101.0(2) . . . . ?
B6 B11 B12 B7 -101.2(2) . . . . ?
B2 B11 B12 B7 -37.36(18) . . . . ?
B10 B11 B12 B7 -138.6(2) . . . . ?
B6 B11 B12 B10 37.30(19) . . . . ?
B2 B11 B12 B10 101.2(2) . . . . ?
B7 B11 B12 B10 138.6(2) . . . . ?
B6 B11 B12 B9 -0.2(3) . . . . ?
B2 B11 B12 B9 63.7(3) . . . . ?
B7 B11 B12 B9 101.1(2) . . . . ?
B10 B11 B12 B9 -37.5(2) . . . . ?
B7 B3 C1 C11 -147.4(2) . . . . ?
B4 B3 C1 C11 110.1(2) . . . . ?
B8 B3 C1 C11 149.5(2) . . . . ?
B2 B3 C1 C11 -107.2(2) . . . . ?
B7 B3 C1 B6 -2.5(3) . . . . ?
B4 B3 C1 B6 -105.0(2) . . . . ?
B8 B3 C1 B6 -65.5(2) . . . . ?
B2 B3 C1 B6 37.73(18) . . . . ?
B7 B3 C1 B4 102.5(2) . . . . ?
B8 B3 C1 B4 39.42(19) . . . . ?
B2 B3 C1 B4 142.7(2) . . . . ?
B7 B3 C1 B2 -40.20(17) . . . . ?
B4 B3 C1 B2 -142.7(2) . . . . ?
B8 B3 C1 B2 -103.3(2) . . . . ?
B7 B3 C1 B5 65.9(2) . . . . ?
B4 B3 C1 B5 -36.5(2) . . . . ?
B8 B3 C1 B5 2.9(3) . . . . ?
B2 B3 C1 B5 106.1(2) . . . . ?
B10 B6 C1 C11 -150.0(2) . . . . ?
B11 B6 C1 C11 146.7(2) . . . . ?
B5 B6 C1 C11 -110.5(2) . . . . ?
B2 B6 C1 C11 107.0(2) . . . . ?
B10 B6 C1 B3 65.4(2) . . . . ?
B11 B6 C1 B3 2.0(2) . . . . ?
B5 B6 C1 B3 104.9(2) . . . . ?
B2 B6 C1 B3 -37.65(18) . . . . ?
B10 B6 C1 B4 -3.1(3) . . . . ?
B11 B6 C1 B4 -66.4(2) . . . . ?
B5 B6 C1 B4 36.4(2) . . . . ?
B2 B6 C1 B4 -106.1(2) . . . . ?
B10 B6 C1 B2 103.0(2) . . . . ?
B11 B6 C1 B2 39.70(17) . . . . ?
B5 B6 C1 B2 142.5(2) . . . . ?
B10 B6 C1 B5 -39.51(18) . . . . ?
B11 B6 C1 B5 -102.8(2) . . . . ?
B2 B6 C1 B5 -142.5(2) . . . . ?
B8 B4 C1 C11 -147.5(2) . . . . ?
B3 B4 C1 C11 -107.9(2) . . . . ?
B5 B4 C1 C11 110.3(2) . . . . ?
B9 B4 C1 C11 149.6(2) . . . . ?
B8 B4 C1 B3 -39.6(2) . . . . ?
B5 B4 C1 B3 -141.8(2) . . . . ?
B9 B4 C1 B3 -102.5(2) . . . . ?
B8 B4 C1 B6 65.7(3) . . . . ?
B3 B4 C1 B6 105.3(2) . . . . ?
B5 B4 C1 B6 -36.5(2) . . . . ?
B9 B4 C1 B6 2.8(3) . . . . ?
B8 B4 C1 B2 -3.5(3) . . . . ?
B3 B4 C1 B2 36.1(2) . . . . ?
B5 B4 C1 B2 -105.7(2) . . . . ?
B9 B4 C1 B2 -66.4(3) . . . . ?
B8 B4 C1 B5 102.2(2) . . . . ?
B3 B4 C1 B5 141.8(2) . . . . ?
B9 B4 C1 B5 39.30(19) . . . . ?
C14 B2 C1 C11 -1.2(3) . . . . ?
B11 B2 C1 C11 -149.5(2) . . . . ?
B3 B2 C1 C11 109.0(2) . . . . ?
B7 B2 C1 C11 148.4(2) . . . . ?
B6 B2 C1 C11 -110.1(2) . . . . ?
C14 B2 C1 B3 -110.2(2) . . . . ?
B11 B2 C1 B3 101.5(2) . . . . ?
B7 B2 C1 B3 39.35(18) . . . . ?
B6 B2 C1 B3 140.84(19) . . . . ?
C14 B2 C1 B6 108.9(2) . . . . ?
B11 B2 C1 B6 -39.36(17) . . . . ?
B3 B2 C1 B6 -140.84(19) . . . . ?
B7 B2 C1 B6 -101.5(2) . . . . ?
C14 B2 C1 B4 -146.2(2) . . . . ?
B11 B2 C1 B4 65.6(2) . . . . ?
B3 B2 C1 B4 -35.9(2) . . . . ?
B7 B2 C1 B4 3.4(3) . . . . ?
B6 B2 C1 B4 104.9(2) . . . . ?
C14 B2 C1 B5 145.0(2) . . . . ?
B11 B2 C1 B5 -3.2(3) . . . . ?
B3 B2 C1 B5 -104.7(2) . . . . ?
B7 B2 C1 B5 -65.4(2) . . . . ?
B6 B2 C1 B5 36.1(2) . . . . ?
B9 B5 C1 C11 -148.9(2) . . . . ?
B10 B5 C1 C11 148.0(2) . . . . ?
B4 B5 C1 C11 -109.4(2) . . . . ?
B6 B5 C1 C11 108.7(2) . . . . ?
B9 B5 C1 B3 -3.0(3) . . . . ?
B10 B5 C1 B3 -66.1(2) . . . . ?
B4 B5 C1 B3 36.6(2) . . . . ?
B6 B5 C1 B3 -105.3(2) . . . . ?
B9 B5 C1 B6 102.3(2) . . . . ?
B10 B5 C1 B6 39.27(19) . . . . ?
B4 B5 C1 B6 141.9(2) . . . . ?
B9 B5 C1 B4 -39.53(19) . . . . ?
B10 B5 C1 B4 -102.6(2) . . . . ?
B6 B5 C1 B4 -141.9(2) . . . . ?
B9 B5 C1 B2 66.0(3) . . . . ?
B10 B5 C1 B2 2.9(3) . . . . ?
B4 B5 C1 B2 105.6(2) . . . . ?
B6 B5 C1 B2 -36.32(19) . . . . ?
B3 C1 C11 C12 88.7(3) . . . . ?
B6 C1 C11 C12 -54.5(3) . . . . ?
B4 C1 C11 C12 160.5(2) . . . . ?
B2 C1 C11 C12 17.4(3) . . . . ?
B5 C1 C11 C12 -126.9(3) . . . . ?
C1 C11 C12 C13 -50.3(3) . . . . ?
C15 O1 C13 C12 175.0(2) . . . . ?
C15 O1 C13 C14 -61.2(3) . . . . ?
C11 C12 C13 O1 -168.8(2) . . . . ?
C11 C12 C13 C14 68.2(3) . . . . ?
O1 C13 C14 B2 -167.1(2) . . . . ?
C12 C13 C14 B2 -47.5(3) . . . . ?
C1 B2 C14 C13 15.7(3) . . . . ?
B11 B2 C14 C13 155.5(2) . . . . ?
B3 B2 C14 C13 -52.1(3) . . . . ?
B7 B2 C14 C13 -125.3(3) . . . . ?
B6 B2 C14 C13 83.0(3) . . . . ?
