#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:45:32 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179076 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/38/4303825.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4303825
loop_
_publ_author_name
'Daniel M. Wells'
'Geng Bang Jin'
'S. Skanthakumar'
'Richard G. Haire'
'L. Soderholm'
'James A. Ibers'
_publ_contact_author_address
;
Department of Chemistry
Northwestern University
Evanston, IL 60208-3113
;
_publ_contact_author_email       ibers@chem.northwestern.edu
_publ_contact_author_fax         '1 847 491 3976'
_publ_contact_author_name        'James A. Ibers'
_publ_contact_author_phone       '1 847 491 5449'
_publ_section_title
;
Quaternary Neptunium Compounds: Syntheses and Characterization of KCuNpS3,
RbCuNpS3, CsCuNpS3, KAgNpS3, and CsAgNpS3
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11513
_journal_page_last               11517
_journal_paper_doi               10.1021/ic901229d
_journal_volume                  48
_journal_year                    2009
_chemical_formula_moiety         'K Ag Np S3'
_chemical_formula_sum            'Ag K Np S3'
_chemical_formula_weight         480.15
_chemical_name_common            'potassium silver neptunium trisulfide'
_chemical_name_systematic        'neptunium potassium silver trisulfide'
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2009-04-05 # Formatted by publCIF
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   4.0575(17)
_cell_length_b                   13.989(6)
_cell_length_c                   10.422(4)
_cell_measurement_reflns_used    237
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      31.34
_cell_measurement_theta_min      3.91
_cell_volume                     591.6(4)
_computing_cell_refinement       'Bruker SAINT (Bruker, 2006)'
_computing_data_collection       'Bruker APEX2 (Bruker, 2006)'
_computing_data_reduction        'Bruker SAINT (Bruker, 2006)'
_computing_molecular_graphics    'CrystalMaker for Windows v2.0.6 (2008)'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.964
_diffrn_measured_fraction_theta_max 0.964
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0390
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            835
_diffrn_reflns_theta_full        33.89
_diffrn_reflns_theta_max         33.89
_diffrn_reflns_theta_min         3.51
_exptl_absorpt_coefficient_mu    22.386
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.7776
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'numerical (TWINABS; Sheldrick, 2008)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    5.391
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       plate
_exptl_crystal_F_000             828
_exptl_crystal_size_max          0.138
_exptl_crystal_size_mid          0.056
_exptl_crystal_size_min          0.043
_refine_diff_density_max         2.004
_refine_diff_density_min         -1.899
_refine_diff_density_rms         0.418
_refine_ls_extinction_coef       0.00029(12)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_matrix_type           full
_refine_ls_number_parameters     26
_refine_ls_number_reflns         896
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0447
_refine_ls_R_factor_gt           0.0292
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
; calc
 [1.00000+0.00000exp(0.00(sinθ/λ)²)]/
   [σ²(Fo²)+(0.0229Fo²)²]
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0504
_refine_ls_wR_factor_ref         0.0537
_reflns_number_gt                717
_reflns_number_total             896
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic901229d_si_001_5.cif
_cod_data_source_block           KAg
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4303825
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
K1 K 0.0000 0.74013(15) 0.2500 0.0247(4) Uani 1 4 d S . .
Ag1 Ag 0.0000 0.45370(6) 0.2500 0.01907(15) Uani 1 4 d S . .
Np1 Np 0.0000 0.0000 0.0000 0.01093(9) Uani 1 4 d S . .
S1 S 0.0000 0.06374(15) 0.2500 0.0134(4) Uani 1 4 d S . .
S2 S 0.0000 0.37303(11) 0.03885(13) 0.0145(3) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Np Np -11.4937 4.1493 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
S1 K1 S1 78.85(7) 5_455 5 ?
S1 K1 S2 68.93(4) 5_455 9_565 ?
S1 K1 S2 68.93(4) 5 9_565 ?
S1 K1 S2 68.93(4) 5_455 2_565 ?
S1 K1 S2 68.93(4) 5 2_565 ?
S2 K1 S2 124.53(8) 9_565 2_565 ?
S1 K1 S2 140.65(3) 5_455 14_556 ?
S1 K1 S2 92.40(4) 5 14_556 ?
S2 K1 S2 142.97(2) 9_565 14_556 ?
S2 K1 S2 72.11(4) 2_565 14_556 ?
S1 K1 S2 92.40(4) 5_455 5_455 ?
S1 K1 S2 140.65(3) 5 5_455 ?
S2 K1 S2 72.11(4) 9_565 5_455 ?
S2 K1 S2 142.97(2) 2_565 5_455 ?
S2 K1 S2 116.30(8) 14_556 5_455 ?
S1 K1 S2 92.40(4) 5_455 14_456 ?
S1 K1 S2 140.65(3) 5 14_456 ?
S2 K1 S2 142.97(2) 9_565 14_456 ?
S2 K1 S2 72.11(4) 2_565 14_456 ?
S2 K1 S2 70.31(5) 14_556 14_456 ?
S2 K1 S2 77.30(6) 5_455 14_456 ?
S1 K1 S2 140.65(3) 5_455 5 ?
S1 K1 S2 92.40(4) 5 5 ?
S2 K1 S2 72.11(4) 9_565 5 ?
S2 K1 S2 142.97(2) 2_565 5 ?
S2 K1 S2 77.30(6) 14_556 5 ?
S2 K1 S2 70.31(5) 5_455 5 ?
S2 K1 S2 116.30(8) 14_456 5 ?
S1 K1 Ag1 174.75(5) 5_455 5 ?
S1 K1 Ag1 106.40(4) 5 5 ?
S2 K1 Ag1 112.65(3) 9_565 5 ?
S2 K1 Ag1 112.65(3) 2_565 5 ?
S2 K1 Ag1 40.54(3) 14_556 5 ?
S2 K1 Ag1 83.51(5) 5_455 5 ?
S2 K1 Ag1 83.51(5) 14_456 5 ?
S2 K1 Ag1 40.54(3) 5 5 ?
S1 K1 Ag1 106.40(4) 5_455 5_455 ?
S1 K1 Ag1 174.75(5) 5 5_455 ?
S2 K1 Ag1 112.65(3) 9_565 5_455 ?
S2 K1 Ag1 112.65(3) 2_565 5_455 ?
S2 K1 Ag1 83.51(5) 14_556 5_455 ?
S2 K1 Ag1 40.54(3) 5_455 5_455 ?
S2 K1 Ag1 40.54(3) 14_456 5_455 ?
S2 K1 Ag1 83.51(5) 5 5_455 ?
Ag1 K1 Ag1 68.35(5) 5 5_455 ?
S1 K1 Ag1 39.43(4) 5_455 . ?
S1 K1 Ag1 39.43(4) 5 . ?
S2 K1 Ag1 62.26(4) 9_565 . ?
S2 K1 Ag1 62.26(4) 2_565 . ?
S2 K1 Ag1 121.85(4) 14_556 . ?
S2 K1 Ag1 121.85(4) 5_455 . ?
S2 K1 Ag1 121.85(4) 14_456 . ?
S2 K1 Ag1 121.85(4) 5 . ?
Ag1 K1 Ag1 145.82(2) 5 . ?
Ag1 K1 Ag1 145.82(3) 5_455 . ?
S1 K1 K1 50.57(4) 5_455 1_455 ?
S1 K1 K1 129.43(4) 5 1_455 ?
S2 K1 K1 90.0 9_565 1_455 ?
S2 K1 K1 90.0 2_565 1_455 ?
S2 K1 K1 125.15(2) 14_556 1_455 ?
S2 K1 K1 54.85(2) 5_455 1_455 ?
S2 K1 K1 54.85(2) 14_456 1_455 ?
S2 K1 K1 125.15(2) 5 1_455 ?
Ag1 K1 K1 124.18(3) 5 1_455 ?
Ag1 K1 K1 55.82(3) 5_455 1_455 ?
Ag1 K1 K1 90.0 . 1_455 ?
S2 Ag1 S2 125.70(8) . 10_556 y
S2 Ag1 S1 106.01(3) . 5 y
S2 Ag1 S1 106.01(3) 10_556 5 ?
S2 Ag1 S1 106.01(3) . 5_455 ?
S2 Ag1 S1 106.01(3) 10_556 5_455 ?
S1 Ag1 S1 105.62(9) 5 5_455 y
S2 Ag1 Np1 140.97(2) . 6 ?
S2 Ag1 Np1 53.05(3) 10_556 6 ?
S1 Ag1 Np1 53.371(19) 5 6 ?
S1 Ag1 Np1 111.34(3) 5_455 6 ?
S2 Ag1 Np1 53.05(3) . 5_455 ?
S2 Ag1 Np1 140.97(2) 10_556 5_455 ?
S1 Ag1 Np1 111.34(3) 5 5_455 ?
S1 Ag1 Np1 53.371(19) 5_455 5_455 ?
Np1 Ag1 Np1 157.80(3) 6 5_455 ?
S2 Ag1 Np1 140.97(2) . 6_455 ?
S2 Ag1 Np1 53.05(3) 10_556 6_455 ?
S1 Ag1 Np1 111.34(3) 5 6_455 ?
S1 Ag1 Np1 53.371(19) 5_455 6_455 ?
Np1 Ag1 Np1 74.15(3) 6 6_455 ?
Np1 Ag1 Np1 101.48(3) 5_455 6_455 ?
S2 Ag1 Np1 53.05(3) . 5 ?
S2 Ag1 Np1 140.97(2) 10_556 5 ?
S1 Ag1 Np1 53.371(19) 5 5 ?
S1 Ag1 Np1 111.34(3) 5_455 5 ?
Np1 Ag1 Np1 101.48(3) 6 5 ?
Np1 Ag1 Np1 74.15(3) 5_455 5 ?
Np1 Ag1 Np1 157.80(3) 6_455 5 ?
S2 Ag1 K1 67.82(3) . 5_445 ?
S2 Ag1 K1 67.82(3) 10_556 5_445 ?
S1 Ag1 K1 161.37(5) 5 5_445 ?
S1 Ag1 K1 93.01(5) 5_455 5_445 ?
Np1 Ag1 K1 119.86(2) 6 5_445 ?
Np1 Ag1 K1 79.66(2) 5_455 5_445 ?
Np1 Ag1 K1 79.66(2) 6_455 5_445 ?
Np1 Ag1 K1 119.86(2) 5 5_445 ?
S2 Ag1 K1 67.82(3) . 5_545 ?
S2 Ag1 K1 67.82(3) 10_556 5_545 ?
S1 Ag1 K1 93.01(5) 5 5_545 ?
S1 Ag1 K1 161.37(5) 5_455 5_545 ?
Np1 Ag1 K1 79.66(2) 6 5_545 ?
Np1 Ag1 K1 119.86(2) 5_455 5_545 ?
Np1 Ag1 K1 119.86(2) 6_455 5_545 ?
Np1 Ag1 K1 79.66(2) 5 5_545 ?
K1 Ag1 K1 68.35(5) 5_445 5_545 ?
S2 Ag1 K1 117.15(4) . . ?
S2 Ag1 K1 117.15(4) 10_556 . ?
S1 Ag1 K1 52.81(4) 5 . ?
S1 Ag1 K1 52.81(4) 5_455 . ?
Np1 Ag1 K1 78.902(14) 6 . ?
Np1 Ag1 K1 78.902(14) 5_455 . ?
Np1 Ag1 K1 78.902(14) 6_455 . ?
Np1 Ag1 K1 78.902(14) 5 . ?
K1 Ag1 K1 145.82(2) 5_445 . ?
K1 Ag1 K1 145.82(3) 5_545 . ?
S2 Np1 S2 180.00(8) 13 5_445 y
S2 Np1 S2 96.15(6) 13 13_455 ?
S2 Np1 S2 83.85(6) 5_445 13_455 ?
S2 Np1 S2 83.85(6) 13 5_545 ?
S2 Np1 S2 96.15(6) 5_445 5_545 ?
S2 Np1 S2 180.00(8) 13_455 5_545 ?
S2 Np1 S1 85.96(4) 13 . y
S2 Np1 S1 94.04(4) 5_445 . ?
S2 Np1 S1 85.96(4) 13_455 . ?
S2 Np1 S1 94.04(4) 5_545 . ?
S2 Np1 S1 94.04(4) 13 9 ?
S2 Np1 S1 85.96(4) 5_445 9 ?
S2 Np1 S1 94.04(4) 13_455 9 ?
S2 Np1 S1 85.96(4) 5_545 9 ?
S1 Np1 S1 180.0 . 9 y
S2 Np1 Ag1 77.98(4) 13 5_545 ?
S2 Np1 Ag1 102.02(4) 5_445 5_545 ?
S2 Np1 Ag1 133.54(3) 13_455 5_545 ?
S2 Np1 Ag1 46.46(3) 5_545 5_545 ?
S1 Np1 Ag1 47.92(3) . 5_545 ?
S1 Np1 Ag1 132.08(3) 9 5_545 ?
S2 Np1 Ag1 102.02(4) 13 13_455 ?
S2 Np1 Ag1 77.98(4) 5_445 13_455 ?
S2 Np1 Ag1 46.46(3) 13_455 13_455 ?
S2 Np1 Ag1 133.54(3) 5_545 13_455 ?
S1 Np1 Ag1 132.08(3) . 13_455 ?
S1 Np1 Ag1 47.92(3) 9 13_455 ?
Ag1 Np1 Ag1 180.00(3) 5_545 13_455 ?
S2 Np1 Ag1 46.46(3) 13 13 ?
S2 Np1 Ag1 133.54(3) 5_445 13 ?
S2 Np1 Ag1 102.02(4) 13_455 13 ?
S2 Np1 Ag1 77.98(4) 5_545 13 ?
S1 Np1 Ag1 132.08(3) . 13 ?
S1 Np1 Ag1 47.92(3) 9 13 ?
Ag1 Np1 Ag1 105.85(3) 5_545 13 ?
Ag1 Np1 Ag1 74.15(3) 13_455 13 ?
S2 Np1 Ag1 133.54(3) 13 5_445 ?
S2 Np1 Ag1 46.46(3) 5_445 5_445 ?
S2 Np1 Ag1 77.98(4) 13_455 5_445 ?
S2 Np1 Ag1 102.02(4) 5_545 5_445 ?
S1 Np1 Ag1 47.92(3) . 5_445 ?
S1 Np1 Ag1 132.08(3) 9 5_445 ?
Ag1 Np1 Ag1 74.15(3) 5_545 5_445 ?
Ag1 Np1 Ag1 105.85(3) 13_455 5_445 ?
Ag1 Np1 Ag1 180.00(3) 13 5_445 ?
S2 Np1 Np1 41.92(3) 13 1_655 ?
S2 Np1 Np1 138.08(3) 5_445 1_655 ?
S2 Np1 Np1 138.08(3) 13_455 1_655 ?
S2 Np1 Np1 41.92(3) 5_545 1_655 ?
S1 Np1 Np1 90.0 . 1_655 ?
S1 Np1 Np1 90.0 9 1_655 ?
Ag1 Np1 Np1 52.923(16) 5_545 1_655 ?
Ag1 Np1 Np1 127.077(16) 13_455 1_655 ?
Ag1 Np1 Np1 52.923(16) 13 1_655 ?
Ag1 Np1 Np1 127.077(16) 5_445 1_655 ?
S2 Np1 Np1 138.08(3) 13 1_455 ?
S2 Np1 Np1 41.92(3) 5_445 1_455 ?
S2 Np1 Np1 41.92(3) 13_455 1_455 ?
S2 Np1 Np1 138.08(3) 5_545 1_455 ?
S1 Np1 Np1 90.0 . 1_455 ?
S1 Np1 Np1 90.0 9 1_455 ?
Ag1 Np1 Np1 127.077(16) 5_545 1_455 ?
Ag1 Np1 Np1 52.923(16) 13_455 1_455 ?
Ag1 Np1 Np1 127.077(16) 13 1_455 ?
Ag1 Np1 Np1 52.923(16) 5_445 1_455 ?
Np1 Np1 Np1 180.0 1_655 1_455 ?
Ag1 S1 Ag1 105.62(9) 5_445 5_545 ?
Ag1 S1 Np1 78.71(4) 5_445 . ?
Ag1 S1 Np1 78.71(4) 5_545 . ?
Ag1 S1 Np1 78.71(4) 5_445 2 ?
Ag1 S1 Np1 78.71(4) 5_545 2 ?
Np1 S1 Np1 142.21(8) . 2 ?
Ag1 S1 K1 166.62(7) 5_445 5_545 ?
Ag1 S1 K1 87.77(5) 5_545 5_545 ?
Np1 S1 K1 104.48(3) . 5_545 ?
Np1 S1 K1 104.48(3) 2 5_545 ?
Ag1 S1 K1 87.77(5) 5_445 5_445 ?
Ag1 S1 K1 166.62(7) 5_545 5_445 ?
Np1 S1 K1 104.48(3) . 5_445 ?
Np1 S1 K1 104.48(3) 2 5_445 ?
K1 S1 K1 78.85(7) 5_545 5_445 ?
Ag1 S2 Np1 80.49(4) . 5 ?
Ag1 S2 Np1 80.49(4) . 5_455 ?
Np1 S2 Np1 96.15(6) 5 5_455 ?
Ag1 S2 K1 179.41(7) . 9_565 ?
Np1 S2 K1 99.89(4) 5 9_565 ?
Np1 S2 K1 99.89(4) 5_455 9_565 ?
Ag1 S2 K1 71.64(5) . 5_545 ?
Np1 S2 K1 90.46(4) 5 5_545 ?
Np1 S2 K1 149.87(5) 5_455 5_545 ?
K1 S2 K1 107.89(4) 9_565 5_545 ?
Ag1 S2 K1 71.64(5) . 5_445 ?
Np1 S2 K1 149.87(5) 5 5_445 ?
Np1 S2 K1 90.46(4) 5_455 5_445 ?
K1 S2 K1 107.89(4) 9_565 5_445 ?
K1 S2 K1 70.31(5) 5_545 5_445 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
K1 S1 3.194(2) 5_455 y
K1 S1 3.194(2) 5 ?
K1 S2 3.401(2) 9_565 y
K1 S2 3.401(2) 2_565 ?
K1 S2 3.5235(18) 14_556 y
K1 S2 3.5235(18) 5_455 ?
K1 S2 3.5235(18) 14_456 ?
K1 S2 3.5235(18) 5 ?
K1 Ag1 3.611(2) 5 ?
K1 Ag1 3.611(2) 5_455 ?
K1 Ag1 4.007(3) . ?
K1 K1 4.0575(17) 1_455 ?
Ag1 S2 2.4731(17) . y
Ag1 S2 2.4731(17) 10_556 ?
Ag1 S1 2.5467(16) 5 y
Ag1 S1 2.5467(16) 5_455 ?
Ag1 Np1 3.3650(10) 6 ?
Ag1 Np1 3.3650(10) 5_455 ?
Ag1 Np1 3.3650(10) 6_455 ?
Ag1 Np1 3.3650(10) 5 ?
Ag1 K1 3.611(2) 5_445 ?
Ag1 K1 3.611(2) 5_545 ?
Np1 S2 2.7267(13) 13 y
Np1 S2 2.7267(13) 5_445 ?
Np1 S2 2.7267(13) 13_455 ?
Np1 S2 2.7267(13) 5_545 ?
Np1 S1 2.7538(12) . y
Np1 S1 2.7538(12) 9 ?
Np1 Ag1 3.3650(10) 5_545 ?
Np1 Ag1 3.3650(10) 13_455 ?
Np1 Ag1 3.3650(10) 13 ?
Np1 Ag1 3.3650(10) 5_445 ?
Np1 Np1 4.0575(17) 1_655 ?
Np1 Np1 4.0575(17) 1_455 ?
S1 Ag1 2.5467(16) 5_445 ?
S1 Ag1 2.5467(16) 5_545 ?
S1 Np1 2.7538(12) 2 ?
S1 K1 3.194(2) 5_545 ?
S1 K1 3.194(2) 5_445 ?
S2 Np1 2.7267(13) 5 ?
S2 Np1 2.7267(13) 5_455 ?
S2 K1 3.401(2) 9_565 ?
S2 K1 3.5235(18) 5_545 ?
S2 K1 3.5235(18) 5_445 ?
