#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/48/4304867.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4304867
loop_
_publ_author_name
'Qiuwen Wang'
'Li Xiang'
'Haibin Song'
'Guofu Zi'
_publ_section_title
;
Synthesis of Amidolanthanides with New Chiral Biaryl-Based NNO Ligands and
Their Use as Catalysts for Enantioselective Hydroamination/Cyclization
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4319
_journal_page_last               4328
_journal_paper_doi               10.1021/ic702461f
_journal_volume                  47
_journal_year                    2008
_chemical_absolute_configuration rmad
_chemical_formula_moiety         'C116.50 H126 N9 O4 Si2 Y3'
_chemical_formula_sum            'C116.5 H126 N9 O4 Si2 Y3'
_chemical_formula_weight         2039.17
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 100.767(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.9688(12)
_cell_length_b                   22.379(2)
_cell_length_c                   31.488(3)
_cell_measurement_reflns_used    15512
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      25.0
_cell_measurement_theta_min      2.5
_cell_volume                     10362.4(16)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalClear
_computing_publication_material  'CrystalStructure 3.7.0'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean 7.31
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  confocal
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.1197
_diffrn_reflns_av_sigmaI/netI    0.1862
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            78828
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.64
_exptl_absorpt_coefficient_mu    1.746
_exptl_absorpt_correction_T_max  0.7921
_exptl_absorpt_correction_T_min  0.7215
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   crystalclear
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.307
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4260
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.14
_refine_diff_density_max         1.815
_refine_diff_density_min         -0.902
_refine_diff_density_rms         0.103
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.032(7)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2401
_refine_ls_number_reflns         35801
_refine_ls_number_restraints     68
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.1690
_refine_ls_R_factor_gt           0.1136
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1350P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2666
_refine_ls_wR_factor_ref         0.3146
_reflns_number_gt                21058
_reflns_number_total             35801
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic702461f-file003_5.cif
_cod_data_source_block           compound9
_cod_original_cell_volume        10362.7(15)
_cod_original_formula_sum        'C116.50 H126 N9 O4 Si2 Y3'
_cod_database_code               4304867
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Y1 Y -0.06458(8) 0.72941(6) 0.18186(4) 0.0510(3) Uani 1 1 d . . .
Y2 Y 0.21163(9) 0.69805(6) 0.05649(4) 0.0547(3) Uani 1 1 d . . .
Y3 Y 0.07464(9) 0.62562(6) 0.12805(4) 0.0541(3) Uani 1 1 d . . .
Y4 Y 0.74836(8) 0.63110(5) 0.67799(4) 0.0504(3) Uani 1 1 d . . .
Y5 Y 0.34774(8) 0.64541(6) 0.57379(4) 0.0545(3) Uani 1 1 d . . .
Y6 Y 0.54929(8) 0.72575(6) 0.63234(4) 0.0494(3) Uani 1 1 d . . .
Si1 Si 0.1641(3) 0.49981(19) 0.17986(14) 0.0666(11) Uani 1 1 d . . .
Si2 Si 0.0016(3) 0.48498(18) 0.10530(14) 0.0628(10) Uani 1 1 d . . .
Si3 Si 0.5135(3) 0.85625(17) 0.68266(14) 0.0585(10) Uani 1 1 d . . .
Si4 Si 0.5901(3) 0.86359(17) 0.59805(15) 0.0622(11) Uani 1 1 d . . .
N1 N 0.0587(8) 0.7700(5) 0.2371(3) 0.053(3) Uani 1 1 d . . .
N2 N -0.0529(8) 0.8324(5) 0.1696(4) 0.058(3) Uani 1 1 d . . .
N3 N -0.2233(7) 0.6989(5) 0.1591(4) 0.060(3) Uani 1 1 d . . .
N4 N -0.1511(8) 0.7586(5) 0.2350(4) 0.064(3) Uani 1 1 d . . .
N5 N 0.3712(7) 0.6776(5) 0.0875(4) 0.056(3) Uani 1 1 d . . .
N6 N 0.3000(7) 0.7033(6) 0.0008(4) 0.062(3) Uani 1 1 d . . .
N7 N 0.0859(7) 0.7172(6) -0.0043(4) 0.066(3) Uani 1 1 d . . .
N8 N 0.1961(8) 0.8022(6) 0.0474(4) 0.068(3) Uani 1 1 d . . .
N9 N 0.0813(7) 0.5272(5) 0.1395(4) 0.054(3) Uani 1 1 d . . .
N10 N 0.6993(7) 0.5921(5) 0.7425(4) 0.055(3) Uani 1 1 d . . .
N11 N 0.7308(6) 0.5272(5) 0.6686(4) 0.050(3) Uani 1 1 d . . .
N12 N 0.8730(7) 0.6638(5) 0.6445(4) 0.056(3) Uani 1 1 d . . .
N13 N 0.8909(7) 0.6099(5) 0.7239(4) 0.056(3) Uani 1 1 d . . .
N14 N 0.4026(7) 0.6245(5) 0.5064(3) 0.052(3) Uani 1 1 d . . .
N15 N 0.3617(8) 0.5420(6) 0.5679(4) 0.066(3) Uani 1 1 d . . .
N16 N 0.2258(8) 0.6702(5) 0.6135(3) 0.057(3) Uani 1 1 d . . .
N17 N 0.2047(8) 0.6388(6) 0.5266(4) 0.067(3) Uani 1 1 d . . .
N18 N 0.5495(6) 0.8241(5) 0.6390(3) 0.048(3) Uani 1 1 d . . .
O1 O 0.0388(5) 0.6489(4) 0.1905(3) 0.050(2) Uani 1 1 d . . .
O2 O -0.0453(5) 0.6891(4) 0.1155(3) 0.054(2) Uani 1 1 d . . .
O3 O 0.1930(6) 0.6876(4) 0.1281(3) 0.055(2) Uani 1 1 d . . .
O4 O 0.1097(6) 0.6199(4) 0.0619(3) 0.054(2) Uani 1 1 d . . .
O5 O 0.6495(5) 0.7061(4) 0.6931(2) 0.048(2) Uani 1 1 d . . .
O6 O 0.6588(5) 0.6664(4) 0.6145(3) 0.053(2) Uani 1 1 d . . .
O7 O 0.4470(5) 0.7243(4) 0.5700(2) 0.048(2) Uani 1 1 d . . .
O8 O 0.4407(5) 0.6590(4) 0.6414(3) 0.052(2) Uani 1 1 d . . .
C1 C 0.0127(8) 0.6516(5) 0.2669(4) 0.051(3) Uani 1 1 d . . .
C2 C -0.0083(8) 0.6294(6) 0.2219(4) 0.052(3) Uani 1 1 d . . .
C3 C -0.0874(9) 0.5947(5) 0.2110(4) 0.050(3) Uani 1 1 d . . .
H3 H -0.1035 0.5789 0.1826 0.060 Uiso 1 1 calc R . .
C4 C -0.1430(10) 0.5829(6) 0.2411(5) 0.061(4) Uani 1 1 d . . .
H4 H -0.1949 0.5581 0.2326 0.073 Uiso 1 1 calc R . .
C5 C -0.1261(9) 0.6054(6) 0.2821(4) 0.055(3) Uani 1 1 d . . .
C6 C -0.0458(9) 0.6414(6) 0.2951(5) 0.058(3) Uani 1 1 d . . .
C7 C -0.0265(9) 0.6696(7) 0.3399(4) 0.062(4) Uani 1 1 d . . .
H7A H 0.0262 0.6490 0.3575 0.074 Uiso 1 1 calc R . .
H7B H -0.0091 0.7119 0.3370 0.074 Uiso 1 1 calc R . .
C8 C -0.1054(12) 0.6675(7) 0.3639(5) 0.077(4) Uani 1 1 d . . .
H8A H -0.1516 0.6975 0.3515 0.092 Uiso 1 1 calc R . .
H8B H -0.0834 0.6778 0.3947 0.092 Uiso 1 1 calc R . .
C9 C -0.1487(13) 0.6060(9) 0.3609(5) 0.088(5) Uani 1 1 d . . .
H9A H -0.1961 0.6041 0.3790 0.106 Uiso 1 1 calc R . .
H9B H -0.1023 0.5751 0.3712 0.106 Uiso 1 1 calc R . .
C10 C -0.1917(10) 0.5952(7) 0.3124(5) 0.071(4) Uani 1 1 d . . .
H10A H -0.2146 0.5537 0.3089 0.085 Uiso 1 1 calc R . .
H10B H -0.2444 0.6223 0.3041 0.085 Uiso 1 1 calc R . .
C11 C 0.1009(8) 0.6801(6) 0.2816(4) 0.051(3) Uani 1 1 d . . .
C12 C 0.1232(8) 0.7391(5) 0.2684(4) 0.048(3) Uani 1 1 d . . .
C13 C 0.2094(9) 0.7654(6) 0.2862(4) 0.055(3) Uani 1 1 d . . .
H13 H 0.2263 0.8036 0.2771 0.066 Uiso 1 1 calc R . .
C14 C 0.2666(9) 0.7327(7) 0.3171(4) 0.065(4) Uani 1 1 d . . .
H14 H 0.3213 0.7512 0.3313 0.078 Uiso 1 1 calc R . .
C15 C 0.2494(9) 0.6745(6) 0.3289(5) 0.062(4) Uani 1 1 d . . .
C16 C 0.1673(10) 0.6481(6) 0.3103(5) 0.068(4) Uani 1 1 d . . .
C17 C 0.1540(10) 0.5826(6) 0.3195(4) 0.058(3) Uani 1 1 d . . .
H17A H 0.1033 0.5793 0.3356 0.069 Uiso 1 1 calc R . .
H17B H 0.1347 0.5619 0.2915 0.069 Uiso 1 1 calc R . .
C18 C 0.2295(19) 0.5514(12) 0.3431(14) 0.26(3) Uani 1 1 d . . .
H18A H 0.2046 0.5198 0.3595 0.311 Uiso 1 1 calc R . .
H18B H 0.2590 0.5308 0.3216 0.311 Uiso 1 1 calc R . .
C19 C 0.2960(16) 0.5781(9) 0.3709(7) 0.119(8) Uani 1 1 d . . .
H19A H 0.3512 0.5532 0.3728 0.143 Uiso 1 1 calc R . .
H19B H 0.2786 0.5771 0.3997 0.143 Uiso 1 1 calc R . .
C20 C 0.3219(11) 0.6406(7) 0.3630(5) 0.078(5) Uani 1 1 d . . .
H20A H 0.3806 0.6402 0.3528 0.094 Uiso 1 1 calc R . .
H20B H 0.3312 0.6628 0.3906 0.094 Uiso 1 1 calc R . .
C21 C 0.0575(9) 0.8294(7) 0.2364(5) 0.062(4) Uani 1 1 d . . .
H21 H 0.0956 0.8505 0.2590 0.075 Uiso 1 1 calc R . .
C22 C 0.0018(9) 0.8627(6) 0.2033(4) 0.053(3) Uani 1 1 d . . .
C23 C -0.0160(12) 0.9248(7) 0.2005(5) 0.076(4) Uani 1 1 d . . .
H23 H 0.0124 0.9552 0.2195 0.091 Uiso 1 1 calc R . .
C24 C -0.0852(11) 0.9322(8) 0.1635(5) 0.076(4) Uani 1 1 d . . .
H24 H -0.1135 0.9687 0.1529 0.091 Uiso 1 1 calc R . .
C25 C -0.1037(12) 0.8752(7) 0.1456(5) 0.076(5) Uani 1 1 d . . .
H25 H -0.1464 0.8673 0.1199 0.091 Uiso 1 1 calc R . .
C26 C -0.1876(9) 0.7270(6) 0.0731(4) 0.054(3) Uani 1 1 d . . .
C27 C -0.0939(8) 0.7266(6) 0.0843(4) 0.053(3) Uani 1 1 d . . .
C28 C -0.0423(10) 0.7733(6) 0.0667(5) 0.063(4) Uani 1 1 d . . .
H28 H 0.0223 0.7727 0.0719 0.075 Uiso 1 1 calc R . .
C29 C -0.0910(13) 0.8189(7) 0.0418(5) 0.081(5) Uani 1 1 d . . .
H29 H -0.0587 0.8496 0.0303 0.097 Uiso 1 1 calc R . .
C30 C -0.1841(15) 0.8199(7) 0.0338(6) 0.092(6) Uani 1 1 d . . .
C31 C -0.2356(10) 0.7748(6) 0.0508(5) 0.070(4) Uani 1 1 d . . .
C32 C -0.3421(11) 0.7762(9) 0.0453(9) 0.119(9) Uani 1 1 d . . .
H32A H -0.3692 0.7505 0.0207 0.143 Uiso 1 1 calc R . .
H32B H -0.3603 0.7603 0.0717 0.143 Uiso 1 1 calc R . .
C33 C -0.3782(16) 0.8412(11) 0.0371(9) 0.125(8) Uani 1 1 d . . .
H33A H -0.3573 0.8666 0.0628 0.150 Uiso 1 1 calc R . .
H33B H -0.4456 0.8416 0.0305 0.150 Uiso 1 1 calc R . .
C34 C -0.3376(17) 0.8647(11) -0.0033(9) 0.148(12) Uani 1 1 d . . .
H34A H -0.3517 0.8353 -0.0272 0.178 Uiso 1 1 calc R . .
H34B H -0.3675 0.9028 -0.0136 0.178 Uiso 1 1 calc R . .
C35 C -0.2319(14) 0.8746(8) 0.0078(7) 0.112(8) Uani 1 1 d . . .
H35A H -0.2183 0.9114 0.0252 0.135 Uiso 1 1 calc R . .
H35B H -0.2079 0.8796 -0.0192 0.135 Uiso 1 1 calc R . .
C36 C -0.2416(9) 0.6704(6) 0.0837(5) 0.065(4) Uani 1 1 d . . .
C37 C -0.2585(9) 0.6584(6) 0.1251(5) 0.060(4) Uani 1 1 d . . .
C38 C -0.3019(10) 0.6074(6) 0.1339(5) 0.062(4) Uani 1 1 d . . .
H38 H -0.3089 0.5986 0.1626 0.075 Uiso 1 1 calc R . .
C39 C -0.3366(9) 0.5673(7) 0.0994(7) 0.078(5) Uani 1 1 d . . .
H39 H -0.3682 0.5324 0.1053 0.093 Uiso 1 1 calc R . .
C40 C -0.3246(10) 0.5789(6) 0.0570(6) 0.065(4) Uani 1 1 d . . .
C41 C -0.2750(9) 0.6312(7) 0.0502(5) 0.064(4) Uani 1 1 d . . .
C42 C -0.2586(11) 0.6423(7) 0.0042(6) 0.090(6) Uani 1 1 d . . .
H42A H -0.2814 0.6827 -0.0050 0.108 Uiso 1 1 calc R . .
H42B H -0.1922 0.6421 0.0048 0.108 Uiso 1 1 calc R . .
C43 C -0.303(3) 0.5978(15) -0.0292(8) 0.198(18) Uani 1 1 d . . .
H43A H -0.3326 0.6213 -0.0545 0.237 Uiso 1 1 calc R . .
H43B H -0.2527 0.5753 -0.0384 0.237 Uiso 1 1 calc R . .
C44 C -0.367(2) 0.5550(11) -0.0209(7) 0.149(11) Uani 1 1 d . . .
H44A H -0.3590 0.5190 -0.0382 0.179 Uiso 1 1 calc R . .
H44B H -0.4280 0.5712 -0.0327 0.179 Uiso 1 1 calc R . .
C45 C -0.3675(13) 0.5352(8) 0.0228(6) 0.087(5) Uani 1 1 d . . .
H45A H -0.3348 0.4967 0.0276 0.104 Uiso 1 1 calc R . .
H45B H -0.4312 0.5282 0.0259 0.104 Uiso 1 1 calc R . .
C46 C -0.2741(9) 0.7118(6) 0.1871(5) 0.064(4) Uani 1 1 d . . .
H46 H -0.3361 0.7000 0.1804 0.076 Uiso 1 1 calc R . .
C47 C -0.2451(9) 0.7413(7) 0.2260(5) 0.058(4) Uani 1 1 d . . .
C48 C -0.2897(11) 0.7621(7) 0.2595(6) 0.074(4) Uani 1 1 d . . .
H48 H -0.3517 0.7564 0.2615 0.089 Uiso 1 1 calc R . .
C49 C -0.2221(11) 0.7930(8) 0.2895(6) 0.086(5) Uani 1 1 d . . .
H49 H -0.2302 0.8136 0.3149 0.103 Uiso 1 1 calc R . .
C50 C -0.1389(11) 0.7864(8) 0.2729(5) 0.077(5) Uani 1 1 d . . .
H50 H -0.0815 0.8004 0.2876 0.092 Uiso 1 1 calc R . .
C51 C 0.3333(10) 0.7394(6) 0.1648(4) 0.062(4) Uani 1 1 d . . .
C52 C 0.2370(10) 0.7390(8) 0.1489(5) 0.072(4) Uani 1 1 d . . .
C53 C 0.1866(11) 0.7895(7) 0.1552(4) 0.065(4) Uani 1 1 d . . .
H53 H 0.1220 0.7876 0.1494 0.079 Uiso 1 1 calc R . .
C54 C 0.2287(13) 0.8414(9) 0.1696(6) 0.095(6) Uani 1 1 d . . .
H54 H 0.1931 0.8751 0.1742 0.114 Uiso 1 1 calc R . .
C55 C 0.3275(13) 0.8462(7) 0.1783(6) 0.097(6) Uani 1 1 d D . .
C56 C 0.3790(9) 0.7936(8) 0.1756(7) 0.094(6) Uani 1 1 d D . .
C57 C 0.4827(10) 0.8032(9) 0.1861(7) 0.106(6) Uani 1 1 d DU . .
H57A H 0.5135 0.7665 0.1787 0.127 Uiso 1 1 calc R . .
H57B H 0.5019 0.8103 0.2175 0.127 Uiso 1 1 calc R . .
C58 C 0.512(2) 0.8570(10) 0.1607(10) 0.173(12) Uani 1 1 d DU . .
H58A H 0.5769 0.8660 0.1729 0.208 Uiso 1 1 calc R . .
H58B H 0.5095 0.8444 0.1304 0.208 Uiso 1 1 calc R . .
C59 C 0.4578(17) 0.9155(11) 0.1604(8) 0.138(9) Uani 1 1 d DU . .
H59A H 0.4296 0.9264 0.1304 0.165 Uiso 1 1 calc R . .
H59B H 0.4984 0.9485 0.1729 0.165 Uiso 1 1 calc R . .
C60 C 0.3828(13) 0.9048(7) 0.1879(8) 0.136(10) Uani 1 1 d D . .
H60A H 0.4121 0.9048 0.2189 0.164 Uiso 1 1 calc R . .
H60B H 0.3399 0.9388 0.1833 0.164 Uiso 1 1 calc R . .
C61 C 0.3896(9) 0.6798(7) 0.1654(5) 0.062(4) Uani 1 1 d . . .
C62 C 0.4047(9) 0.6526(6) 0.1287(4) 0.060(4) Uani 1 1 d . . .
C63 C 0.4559(9) 0.5998(6) 0.1320(5) 0.060(4) Uani 1 1 d . . .
H63 H 0.4644 0.5798 0.1064 0.072 Uiso 1 1 calc R . .
C64 C 0.4942(9) 0.5762(7) 0.1718(5) 0.062(4) Uani 1 1 d . . .
H64 H 0.5281 0.5401 0.1732 0.074 Uiso 1 1 calc R . .
C65 C 0.4840(11) 0.6042(8) 0.2093(6) 0.083(6) Uani 1 1 d . . .
C66 C 0.4293(10) 0.6576(7) 0.2068(5) 0.072(4) Uani 1 1 d . . .
C67 C 0.4109(13) 0.6863(9) 0.2481(5) 0.099(6) Uani 1 1 d . . .
H67A H 0.3512 0.6726 0.2535 0.119 Uiso 1 1 calc R . .
H67B H 0.4079 0.7303 0.2443 0.119 Uiso 1 1 calc R . .
C68 C 0.4858(14) 0.6706(9) 0.2877(6) 0.100(6) Uani 1 1 d . . .
H68A H 0.5440 0.6898 0.2848 0.120 Uiso 1 1 calc R . .
H68B H 0.4681 0.6853 0.3146 0.120 Uiso 1 1 calc R . .
C69 C 0.4968(13) 0.6033(9) 0.2894(6) 0.093(6) Uani 1 1 d . . .
H69A H 0.5401 0.5926 0.3161 0.111 Uiso 1 1 calc R . .
H69B H 0.4374 0.5850 0.2913 0.111 Uiso 1 1 calc R . .
C70 C 0.5296(11) 0.5773(8) 0.2520(5) 0.073(4) Uani 1 1 d . . .
H70A H 0.5184 0.5337 0.2513 0.087 Uiso 1 1 calc R . .
H70B H 0.5961 0.5836 0.2557 0.087 Uiso 1 1 calc R . .
C71 C 0.4244(10) 0.6799(6) 0.0588(6) 0.069(4) Uani 1 1 d . . .
H71 H 0.4871 0.6711 0.0682 0.083 Uiso 1 1 calc R . .
C72 C 0.3944(9) 0.6946(6) 0.0147(4) 0.052(3) Uani 1 1 d . . .
C73 C 0.4391(11) 0.7042(8) -0.0191(5) 0.080(5) Uani 1 1 d . . .
H73 H 0.5027 0.7008 -0.0181 0.096 Uiso 1 1 calc R . .
C74 C 0.3726(10) 0.7204(8) -0.0561(5) 0.072(4) Uani 1 1 d . . .
H74 H 0.3810 0.7289 -0.0846 0.086 Uiso 1 1 calc R . .
C75 C 0.2922(9) 0.7204(8) -0.0397(5) 0.072(4) Uani 1 1 d . . .
H75 H 0.2355 0.7319 -0.0566 0.086 Uiso 1 1 calc R . .
C76 C 0.1329(10) 0.5923(6) -0.0098(4) 0.058(3) Uani 1 1 d . . .
C77 C 0.1569(10) 0.5883(7) 0.0339(6) 0.069(4) Uani 1 1 d . . .
C78 C 0.2389(9) 0.5630(6) 0.0531(4) 0.052(3) Uani 1 1 d . . .
H78 H 0.2562 0.5607 0.0837 0.063 Uiso 1 1 calc R . .
C79 C 0.2959(11) 0.5408(6) 0.0261(6) 0.070(4) Uani 1 1 d . . .
H79 H 0.3499 0.5204 0.0390 0.085 Uiso 1 1 calc R . .
C80 C 0.2774(9) 0.5471(6) -0.0187(5) 0.058(3) Uani 1 1 d . . .
C81 C 0.1937(10) 0.5727(6) -0.0380(6) 0.067(4) Uani 1 1 d . . .
C82 C 0.1710(11) 0.5825(9) -0.0858(5) 0.083(5) Uani 1 1 d . . .
H82A H 0.1521 0.6247 -0.0911 0.099 Uiso 1 1 calc R . .
H82B H 0.1178 0.5572 -0.0977 0.099 Uiso 1 1 calc R . .
C83 C 0.2458(12) 0.5694(9) -0.1111(6) 0.089(5) Uani 1 1 d . . .
H83A H 0.2176 0.5571 -0.1408 0.107 Uiso 1 1 calc R . .
H83B H 0.2805 0.6066 -0.1133 0.107 Uiso 1 1 calc R . .
C84 C 0.3086(18) 0.5231(14) -0.0921(8) 0.150(11) Uani 1 1 d . . .
H84A H 0.3598 0.5220 -0.1079 0.180 Uiso 1 1 calc R . .
H84B H 0.2770 0.4842 -0.0967 0.180 Uiso 1 1 calc R . .
C85 C 0.3474(9) 0.5294(8) -0.0446(6) 0.079(5) Uani 1 1 d . . .
H85A H 0.3750 0.4909 -0.0335 0.095 Uiso 1 1 calc R . .
H85B H 0.3963 0.5599 -0.0407 0.095 Uiso 1 1 calc R . .
C86 C 0.0397(8) 0.6164(7) -0.0302(4) 0.062(4) Uani 1 1 d . . .
C87 C 0.0188(8) 0.6798(6) -0.0280(4) 0.058(4) Uani 1 1 d . . .
C88 C -0.0677(10) 0.6986(7) -0.0469(4) 0.062(4) Uani 1 1 d . . .
H88 H -0.0863 0.7383 -0.0425 0.074 Uiso 1 1 calc R . .
C89 C -0.1269(9) 0.6599(8) -0.0723(5) 0.066(4) Uani 1 1 d . . .
H89 H -0.1836 0.6748 -0.0871 0.079 Uiso 1 1 calc R . .
C90 C -0.1066(10) 0.6007(8) -0.0767(4) 0.064(4) Uani 1 1 d . . .
C91 C -0.0267(10) 0.5779(7) -0.0544(5) 0.072(4) Uani 1 1 d . . .
C92 C -0.0104(12) 0.5087(8) -0.0537(6) 0.084(5) Uani 1 1 d . . .
H92A H 0.0530 0.5014 -0.0574 0.101 Uiso 1 1 calc R . .
H92B H -0.0161 0.4935 -0.0248 0.101 Uiso 1 1 calc R . .
C93 C -0.0717(15) 0.4734(9) -0.0867(8) 0.121(8) Uani 1 1 d . . .
H93A H -0.0334 0.4515 -0.1040 0.145 Uiso 1 1 calc R . .
H93B H -0.1020 0.4431 -0.0714 0.145 Uiso 1 1 calc R . .
C94 C -0.137(2) 0.5024(10) -0.1146(10) 0.187(16) Uani 1 1 d . . .
H94A H -0.1900 0.4752 -0.1197 0.225 Uiso 1 1 calc R . .
H94B H -0.1146 0.5046 -0.1422 0.225 Uiso 1 1 calc R . .
C95 C -0.1721(10) 0.5595(7) -0.1085(5) 0.072(4) Uani 1 1 d . . .
H95A H -0.2294 0.5547 -0.0974 0.086 Uiso 1 1 calc R . .
H95B H -0.1872 0.5797 -0.1369 0.086 Uiso 1 1 calc R . .
C96 C 0.0875(9) 0.7746(6) -0.0189(5) 0.058(3) Uani 1 1 d . . .
H96 H 0.0488 0.7864 -0.0450 0.070 Uiso 1 1 calc R . .
C97 C 0.1490(9) 0.8169(7) 0.0058(5) 0.064(4) Uani 1 1 d . . .
C98 C 0.1767(12) 0.8728(8) -0.0072(6) 0.090(6) Uani 1 1 d . . .
H98 H 0.1531 0.8936 -0.0331 0.108 Uiso 1 1 calc R . .
C99 C 0.2487(14) 0.8922(8) 0.0271(6) 0.095(6) Uani 1 1 d . . .
H99 H 0.2850 0.9271 0.0274 0.114 Uiso 1 1 calc R . .
C100 C 0.2547(13) 0.8485(8) 0.0607(7) 0.090(5) Uani 1 1 d . . .
H100 H 0.2937 0.8511 0.0881 0.108 Uiso 1 1 calc R . .
C101 C 0.2452(16) 0.4446(10) 0.1597(6) 0.115(8) Uani 1 1 d . . .
H10C H 0.2128 0.4072 0.1508 0.173 Uiso 1 1 calc R . .
H10D H 0.2970 0.4364 0.1830 0.173 Uiso 1 1 calc R . .
H10E H 0.2671 0.4619 0.1349 0.173 Uiso 1 1 calc R . .
C102 C 0.1219(13) 0.4599(8) 0.2240(5) 0.091(6) Uani 1 1 d . . .
H10F H 0.0813 0.4863 0.2365 0.136 Uiso 1 1 calc R . .
H10G H 0.1735 0.4484 0.2464 0.136 Uiso 1 1 calc R . .
H10H H 0.0885 0.4241 0.2123 0.136 Uiso 1 1 calc R . .
C103 C 0.2345(11) 0.5665(8) 0.2050(5) 0.076(4) Uani 1 1 d . . .
H10I H 0.2848 0.5734 0.1897 0.114 Uiso 1 1 calc R . .
H10J H 0.2589 0.5582 0.2355 0.114 Uiso 1 1 calc R . .
H10K H 0.1958 0.6022 0.2027 0.114 Uiso 1 1 calc R . .
C104 C 0.0529(11) 0.4322(6) 0.0700(5) 0.070(4) Uani 1 1 d . . .
H10L H 0.0780 0.4551 0.0484 0.105 Uiso 1 1 calc R . .
H10M H 0.0059 0.4049 0.0553 0.105 Uiso 1 1 calc R . .
H10N H 0.1016 0.4092 0.0879 0.105 Uiso 1 1 calc R . .
C105 C -0.0769(12) 0.4406(8) 0.1327(5) 0.082(5) Uani 1 1 d . . .
H10O H -0.0424 0.4095 0.1506 0.122 Uiso 1 1 calc R . .
H10P H -0.1240 0.4221 0.1109 0.122 Uiso 1 1 calc R . .
H10Q H -0.1055 0.4671 0.1511 0.122 Uiso 1 1 calc R . .
C106 C -0.0761(10) 0.5378(7) 0.0679(6) 0.077(5) Uani 1 1 d . . .
H10R H -0.1106 0.5624 0.0850 0.115 Uiso 1 1 calc R . .
H10S H -0.1184 0.5145 0.0467 0.115 Uiso 1 1 calc R . .
H10T H -0.0394 0.5637 0.0529 0.115 Uiso 1 1 calc R . .
C107 C 0.7532(8) 0.7151(5) 0.7621(4) 0.041(3) Uani 1 1 d . . .
C108 C 0.7261(8) 0.7317(6) 0.7187(4) 0.052(3) Uani 1 1 d . . .
C109 C 0.7793(9) 0.7687(6) 0.6983(5) 0.057(3) Uani 1 1 d . . .
H109 H 0.7577 0.7807 0.6692 0.068 Uiso 1 1 calc R . .
C110 C 0.8642(9) 0.7886(6) 0.7199(4) 0.053(3) Uani 1 1 d . . .
H110 H 0.8985 0.8154 0.7058 0.064 Uiso 1 1 calc R . .
C111 C 0.8995(8) 0.7692(5) 0.7624(4) 0.049(3) Uani 1 1 d . . .
C112 C 0.8443(8) 0.7338(6) 0.7844(4) 0.048(3) Uani 1 1 d . . .
C113 C 0.8798(9) 0.7111(7) 0.8307(4) 0.061(4) Uani 1 1 d . . .
H11A H 0.8621 0.6687 0.8327 0.073 Uiso 1 1 calc R . .
H11B H 0.8508 0.7344 0.8512 0.073 Uiso 1 1 calc R . .
C114 C 0.9850(10) 0.7167(8) 0.8438(5) 0.074(4) Uani 1 1 d . . .
H11C H 1.0037 0.7101 0.8753 0.089 Uiso 1 1 calc R . .
H11D H 1.0146 0.6859 0.8286 0.089 Uiso 1 1 calc R . .
C115 C 1.0152(10) 0.7787(8) 0.8321(5) 0.077(5) Uani 1 1 d . . .
H11E H 1.0811 0.7833 0.8434 0.092 Uiso 1 1 calc R . .
H11F H 0.9828 0.8092 0.8462 0.092 Uiso 1 1 calc R . .
C116 C 0.9959(9) 0.7894(6) 0.7827(5) 0.064(4) Uani 1 1 d . . .
H11G H 1.0029 0.8324 0.7768 0.077 Uiso 1 1 calc R . .
H11H H 1.0407 0.7670 0.7694 0.077 Uiso 1 1 calc R . .
C117 C 0.6917(9) 0.6831(7) 0.7870(5) 0.059(4) Uani 1 1 d . . .
C118 C 0.6682(7) 0.6207(5) 0.7773(4) 0.049(3) Uani 1 1 d . . .
C119 C 0.6085(9) 0.5916(6) 0.7993(4) 0.054(3) Uani 1 1 d . . .
H119 H 0.5850 0.5532 0.7905 0.065 Uiso 1 1 calc R . .
C120 C 0.5837(9) 0.6212(7) 0.8352(5) 0.066(4) Uani 1 1 d . . .
H120 H 0.5505 0.5999 0.8532 0.080 Uiso 1 1 calc R . .
C121 C 0.6065(10) 0.6794(7) 0.8444(5) 0.063(4) Uani 1 1 d . . .
C122 C 0.6589(9) 0.7114(6) 0.8189(5) 0.055(3) Uani 1 1 d . . .
C123 C 0.6722(10) 0.7771(7) 0.8273(5) 0.063(4) Uani 1 1 d . . .
H12A H 0.7351 0.7874 0.8244 0.075 Uiso 1 1 calc R . .
H12B H 0.6305 0.7989 0.8044 0.075 Uiso 1 1 calc R . .
C124 C 0.658(2) 0.7994(10) 0.8692(11) 0.192(17) Uani 1 1 d . . .
H12C H 0.6519 0.8434 0.8677 0.230 Uiso 1 1 calc R . .
H12D H 0.7119 0.7898 0.8914 0.230 Uiso 1 1 calc R . .
C125 C 0.5730(18) 0.7734(10) 0.8838(8) 0.128(9) Uani 1 1 d . . .
H12E H 0.5699 0.7884 0.9131 0.154 Uiso 1 1 calc R . .
H12F H 0.5176 0.7868 0.8638 0.154 Uiso 1 1 calc R . .
C126 C 0.5767(13) 0.7086(9) 0.8844(7) 0.099(7) Uani 1 1 d . . .
H12G H 0.5158 0.6932 0.8866 0.119 Uiso 1 1 calc R . .
H12H H 0.6196 0.6958 0.9107 0.119 Uiso 1 1 calc R . .
C127 C 0.7039(9) 0.5327(6) 0.7423(4) 0.057(3) Uani 1 1 d . . .
H127 H 0.6956 0.5117 0.7675 0.069 Uiso 1 1 calc R . .
C128 C 0.7205(10) 0.4993(6) 0.7065(5) 0.062(4) Uani 1 1 d . . .
C129 C 0.7299(13) 0.4343(7) 0.7032(7) 0.086(5) Uani 1 1 d . . .
H129 H 0.7241 0.4048 0.7242 0.104 Uiso 1 1 calc R . .
C130 C 0.7491(12) 0.4261(7) 0.6626(7) 0.091(6) Uani 1 1 d . . .
H130 H 0.7603 0.3890 0.6499 0.110 Uiso 1 1 calc R . .
C131 C 0.7493(10) 0.4822(8) 0.6434(5) 0.075(5) Uani 1 1 d . . .
H131 H 0.7614 0.4880 0.6151 0.089 Uiso 1 1 calc R . .
C132 C 0.7468(8) 0.6258(6) 0.5622(4) 0.052(3) Uani 1 1 d . . .
C133 C 0.6698(8) 0.6245(5) 0.5829(4) 0.046(3) Uani 1 1 d . . .
C134 C 0.6022(9) 0.5777(6) 0.5718(5) 0.057(4) Uani 1 1 d . . .
H134 H 0.5482 0.5776 0.5835 0.068 Uiso 1 1 calc R . .
C135 C 0.6184(8) 0.5333(6) 0.5437(4) 0.054(3) Uani 1 1 d . . .
H135 H 0.5733 0.5036 0.5352 0.065 Uiso 1 1 calc R . .
C136 C 0.6974(12) 0.5307(7) 0.5277(5) 0.075(4) Uani 1 1 d . . .
C137 C 0.7638(9) 0.5754(6) 0.5384(5) 0.060(4) Uani 1 1 d . . .
C138 C 0.8505(10) 0.5757(6) 0.5193(5) 0.067(4) Uani 1 1 d . . .
H13A H 0.9022 0.5894 0.5415 0.081 Uiso 1 1 calc R . .
H13B H 0.8432 0.6042 0.4948 0.081 Uiso 1 1 calc R . .
C139 C 0.8723(11) 0.5114(8) 0.5028(7) 0.095(6) Uani 1 1 d . . .
H13C H 0.9199 0.5146 0.4850 0.114 Uiso 1 1 calc R . .
H13D H 0.8958 0.4856 0.5279 0.114 Uiso 1 1 calc R . .
C140 C 0.7892(12) 0.4840(10) 0.4768(7) 0.101(7) Uani 1 1 d . . .
H14A H 0.8047 0.4444 0.4663 0.121 Uiso 1 1 calc R . .
H14B H 0.7668 0.5095 0.4514 0.121 Uiso 1 1 calc R . .
C141 C 0.7159(10) 0.4769(8) 0.5025(6) 0.079(5) Uani 1 1 d . . .
H14C H 0.7321 0.4432 0.5228 0.094 Uiso 1 1 calc R . .
H14D H 0.6590 0.4658 0.4825 0.094 Uiso 1 1 calc R . .
C142 C 0.8066(8) 0.6812(5) 0.5678(4) 0.047(3) Uani 1 1 d . . .
C143 C 0.8650(7) 0.6996(5) 0.6051(4) 0.046(3) Uani 1 1 d . . .
C144 C 0.9155(9) 0.7529(7) 0.6065(5) 0.067(4) Uani 1 1 d . . .
H144 H 0.9529 0.7658 0.6327 0.080 Uiso 1 1 calc R . .
C145 C 0.9095(9) 0.7865(6) 0.5684(5) 0.054(3) Uani 1 1 d . . .
H145 H 0.9461 0.8213 0.5690 0.065 Uiso 1 1 calc R . .
C146 C 0.8530(10) 0.7712(7) 0.5304(5) 0.060(4) Uani 1 1 d . . .
C147 C 0.7999(8) 0.7192(6) 0.5297(4) 0.053(3) Uani 1 1 d . . .
C148 C 0.7344(9) 0.7066(7) 0.4874(4) 0.057(3) Uani 1 1 d . . .
H14E H 0.6816 0.7340 0.4845 0.068 Uiso 1 1 calc R . .
H14F H 0.7116 0.6651 0.4874 0.068 Uiso 1 1 calc R . .
C149 C 0.7836(11) 0.7156(8) 0.4491(5) 0.075(4) Uani 1 1 d . . .
H14G H 0.8291 0.6834 0.4494 0.090 Uiso 1 1 calc R . .
H14H H 0.7389 0.7122 0.4217 0.090 Uiso 1 1 calc R . .
C150 C 0.8308(16) 0.7753(9) 0.4504(5) 0.107(7) Uani 1 1 d . . .
H15A H 0.8938 0.7683 0.4460 0.128 Uiso 1 1 calc R . .
H15B H 0.7996 0.7993 0.4256 0.128 Uiso 1 1 calc R . .
C151 C 0.8350(11) 0.8107(7) 0.4895(5) 0.071(4) Uani 1 1 d . . .
H15C H 0.7769 0.8324 0.4881 0.085 Uiso 1 1 calc R . .
H15D H 0.8842 0.8407 0.4912 0.085 Uiso 1 1 calc R . .
C152 C 0.9522(8) 0.6613(6) 0.6704(5) 0.057(4) Uani 1 1 d . . .
H152 H 1.0032 0.6782 0.6608 0.068 Uiso 1 1 calc R . .
C153 C 0.9656(8) 0.6354(7) 0.7107(4) 0.056(3) Uani 1 1 d . . .
C154 C 1.0457(9) 0.6238(7) 0.7415(5) 0.068(4) Uani 1 1 d . . .
H154 H 1.1061 0.6346 0.7394 0.082 Uiso 1 1 calc R . .
C155 C 1.0178(10) 0.5932(7) 0.7756(5) 0.062(4) Uani 1 1 d . . .
H155 H 1.0553 0.5804 0.8017 0.074 Uiso 1 1 calc R . .
C156 C 0.9238(9) 0.5851(6) 0.7636(5) 0.066(4) Uani 1 1 d . . .
H156 H 0.8874 0.5650 0.7807 0.079 Uiso 1 1 calc R . .
C157 C 0.3514(10) 0.7495(6) 0.5016(5) 0.063(4) Uani 1 1 d . . .
C158 C 0.3736(9) 0.7540(7) 0.5456(5) 0.060(4) Uani 1 1 d . . .
C159 C 0.3157(11) 0.7855(7) 0.5692(5) 0.070(4) Uani 1 1 d . . .
H159 H 0.3333 0.7928 0.5993 0.084 Uiso 1 1 calc R . .
C160 C 0.2317(10) 0.8051(6) 0.5460(5) 0.066(4) Uani 1 1 d . . .
H160 H 0.1903 0.8229 0.5616 0.079 Uiso 1 1 calc R . .
C161 C 0.2054(10) 0.8001(7) 0.5019(5) 0.062(4) Uani 1 1 d . . .
C162 C 0.2641(11) 0.7715(7) 0.4784(5) 0.071(4) Uani 1 1 d . . .
C163 C 0.2355(11) 0.7586(9) 0.4289(5) 0.085(5) Uani 1 1 d . . .
H16A H 0.2844 0.7718 0.4137 0.102 Uiso 1 1 calc R . .
H16B H 0.2265 0.7151 0.4241 0.102 Uiso 1 1 calc R . .
C164 C 0.1488(11) 0.7912(8) 0.4107(5) 0.079(5) Uani 1 1 d . . .
H16C H 0.1659 0.8322 0.4035 0.094 Uiso 1 1 calc R . .
H16D H 0.1221 0.7715 0.3831 0.094 Uiso 1 1 calc R . .
C165 C 0.0799(17) 0.7966(17) 0.4345(7) 0.189(17) Uani 1 1 d . . .
H16E H 0.0518 0.7569 0.4363 0.227 Uiso 1 1 calc R . .
H16F H 0.0325 0.8235 0.4188 0.227 Uiso 1 1 calc R . .
C166 C 0.1094(11) 0.8198(8) 0.4789(5) 0.075(5) Uani 1 1 d . . .
H16G H 0.0648 0.8069 0.4966 0.090 Uiso 1 1 calc R . .
H16H H 0.1078 0.8641 0.4777 0.090 Uiso 1 1 calc R . .
C167 C 0.4182(10) 0.7240(8) 0.4749(4) 0.066(4) Uani 1 1 d . . .
C168 C 0.4394(9) 0.6625(6) 0.4771(4) 0.051(3) Uani 1 1 d . . .
C169 C 0.5006(8) 0.6387(7) 0.4519(4) 0.057(3) Uani 1 1 d . . .
H169 H 0.5173 0.5977 0.4539 0.069 Uiso 1 1 calc R . .
C170 C 0.5343(10) 0.6760(9) 0.4252(5) 0.079(5) Uani 1 1 d . . .
H170 H 0.5733 0.6597 0.4076 0.095 Uiso 1 1 calc R . .
C171 C 0.5146(9) 0.7395(7) 0.4217(5) 0.063(4) Uani 1 1 d . . .
C172 C 0.4602(10) 0.7616(7) 0.4485(5) 0.066(4) Uani 1 1 d . . .
C173 C 0.4452(15) 0.8318(8) 0.4486(5) 0.093(6) Uani 1 1 d . . .
H17C H 0.3800 0.8392 0.4488 0.111 Uiso 1 1 calc R . .
H17D H 0.4800 0.8476 0.4761 0.111 Uiso 1 1 calc R . .
C174 C 0.469(2) 0.8652(10) 0.4153(10) 0.164(14) Uani 1 1 d . . .
H17E H 0.5139 0.8952 0.4286 0.197 Uiso 1 1 calc R . .
H17F H 0.4137 0.8876 0.4016 0.197 Uiso 1 1 calc R . .
C175 C 0.5055(13) 0.8359(10) 0.3803(6) 0.096(6) Uani 1 1 d . . .
H17G H 0.5467 0.8644 0.3694 0.115 Uiso 1 1 calc R . .
H17H H 0.4545 0.8274 0.3561 0.115 Uiso 1 1 calc R . .
C176 C 0.5560(13) 0.7796(7) 0.3924(6) 0.087(5) Uani 1 1 d . . .
H17I H 0.6187 0.7896 0.4068 0.105 Uiso 1 1 calc R . .
H17J H 0.5600 0.7573 0.3657 0.105 Uiso 1 1 calc R . .
C177 C 0.3913(8) 0.5675(6) 0.4971(4) 0.053(3) Uani 1 1 d . . .
H177 H 0.4035 0.5539 0.4702 0.064 Uiso 1 1 calc R . .
C178 C 0.3622(9) 0.5257(7) 0.5245(5) 0.068(4) Uani 1 1 d . . .
C179 C 0.3394(12) 0.4624(8) 0.5194(7) 0.095(6) Uani 1 1 d . . .
H179 H 0.3385 0.4390 0.4941 0.114 Uiso 1 1 calc R . .
C180 C 0.3191(13) 0.4426(8) 0.5586(5) 0.081(5) Uani 1 1 d . . .
H180 H 0.3010 0.4034 0.5650 0.098 Uiso 1 1 calc R . .
C181 C 0.3305(10) 0.4924(8) 0.5872(5) 0.077(5) Uani 1 1 d . . .
H181 H 0.3184 0.4917 0.6157 0.092 Uiso 1 1 calc R . .
C182 C 0.3484(8) 0.6066(6) 0.6856(4) 0.049(3) Uani 1 1 d . . .
C183 C 0.4242(10) 0.6112(6) 0.6671(5) 0.057(3) Uani 1 1 d . . .
C184 C 0.4862(8) 0.5620(6) 0.6708(4) 0.055(3) Uani 1 1 d . . .
H184 H 0.5406 0.5650 0.6595 0.066 Uiso 1 1 calc R . .
C185 C 0.4658(9) 0.5090(6) 0.6912(5) 0.054(3) Uani 1 1 d . . .
H185 H 0.5077 0.4767 0.6944 0.065 Uiso 1 1 calc R . .
C186 C 0.3841(10) 0.5036(6) 0.7068(5) 0.064(4) Uani 1 1 d . . .
C187 C 0.3239(10) 0.5526(6) 0.7038(5) 0.067(4) Uani 1 1 d . . .
C188 C 0.2347(9) 0.5484(7) 0.7198(5) 0.068(4) Uani 1 1 d . . .
H18C H 0.1847 0.5620 0.6966 0.082 Uiso 1 1 calc R . .
H18D H 0.2368 0.5754 0.7448 0.082 Uiso 1 1 calc R . .
C189 C 0.2143(11) 0.4846(10) 0.7332(7) 0.108(8) Uani 1 1 d . . .
H18E H 0.1747 0.4877 0.7550 0.130 Uiso 1 1 calc R . .
H18F H 0.1782 0.4647 0.7075 0.130 Uiso 1 1 calc R . .
C190 C 0.2856(17) 0.4466(8) 0.7499(11) 0.161(14) Uani 1 1 d . . .
H19C H 0.2607 0.4058 0.7512 0.194 Uiso 1 1 calc R . .
H19D H 0.3103 0.4592 0.7799 0.194 Uiso 1 1 calc R . .
C191 C 0.3608(12) 0.4436(6) 0.7264(5) 0.071(4) Uani 1 1 d . . .
H19E H 0.3454 0.4140 0.7028 0.086 Uiso 1 1 calc R . .
H19F H 0.4155 0.4289 0.7463 0.086 Uiso 1 1 calc R . .
C192 C 0.2946(8) 0.6653(6) 0.6914(5) 0.057(4) Uani 1 1 d . . .
C193 C 0.2362(8) 0.6925(6) 0.6550(5) 0.056(3) Uani 1 1 d . . .
C194 C 0.1883(9) 0.7452(6) 0.6646(5) 0.064(4) Uani 1 1 d . . .
H194 H 0.1505 0.7657 0.6416 0.077 Uiso 1 1 calc R . .
C195 C 0.1955(8) 0.7667(6) 0.7062(4) 0.048(3) Uani 1 1 d . . .
H195 H 0.1618 0.8012 0.7111 0.058 Uiso 1 1 calc R . .
C196 C 0.2517(9) 0.7388(6) 0.7413(5) 0.060(4) Uani 1 1 d . . .
C197 C 0.3031(9) 0.6901(7) 0.7337(5) 0.065(4) Uani 1 1 d . . .
C198 C 0.3705(8) 0.6645(6) 0.7713(4) 0.056(3) Uani 1 1 d . . .
H19G H 0.3822 0.6222 0.7649 0.068 Uiso 1 1 calc R . .
H19H H 0.4288 0.6863 0.7737 0.068 Uiso 1 1 calc R . .
C199 C 0.3420(16) 0.6673(13) 0.8117(6) 0.138(10) Uani 1 1 d . . .
H19I H 0.3957 0.6784 0.8337 0.166 Uiso 1 1 calc R . .
H19J H 0.3244 0.6264 0.8188 0.166 Uiso 1 1 calc R . .
C200 C 0.2648(15) 0.7088(11) 0.8173(6) 0.113(7) Uani 1 1 d . . .
H20C H 0.2747 0.7238 0.8474 0.135 Uiso 1 1 calc R . .
H20D H 0.2065 0.6868 0.8115 0.135 Uiso 1 1 calc R . .
C201 C 0.2609(10) 0.7626(7) 0.7853(5) 0.069(4) Uani 1 1 d . . .
H20E H 0.2085 0.7886 0.7875 0.083 Uiso 1 1 calc R . .
H20F H 0.3172 0.7867 0.7926 0.083 Uiso 1 1 calc R . .
C202 C 0.1455(8) 0.6768(6) 0.5870(5) 0.064(4) Uani 1 1 d . . .
H202 H 0.0970 0.6945 0.5981 0.077 Uiso 1 1 calc R . .
C203 C 0.1295(9) 0.6591(6) 0.5437(4) 0.054(3) Uani 1 1 d . . .
C204 C 0.0502(9) 0.6594(7) 0.5131(5) 0.067(4) Uani 1 1 d . . .
H204 H -0.0077 0.6735 0.5168 0.080 Uiso 1 1 calc R . .
C205 C 0.0727(9) 0.6345(8) 0.4757(5) 0.073(4) Uani 1 1 d . . .
H205 H 0.0321 0.6253 0.4495 0.088 Uiso 1 1 calc R . .
C206 C 0.1667(10) 0.6261(8) 0.4845(5) 0.075(4) Uani 1 1 d . . .
H206 H 0.2006 0.6129 0.4636 0.090 Uiso 1 1 calc R . .
C207 C 0.6040(11) 0.8948(7) 0.7220(5) 0.079(5) Uani 1 1 d . . .
H20G H 0.6539 0.8669 0.7320 0.119 Uiso 1 1 calc R . .
H20H H 0.5785 0.9088 0.7468 0.119 Uiso 1 1 calc R . .
H20I H 0.6270 0.9290 0.7079 0.119 Uiso 1 1 calc R . .
C208 C 0.4174(12) 0.9112(8) 0.6669(6) 0.086(5) Uani 1 1 d . . .
H20J H 0.4367 0.9432 0.6494 0.128 Uiso 1 1 calc R . .
H20K H 0.4009 0.9283 0.6930 0.128 Uiso 1 1 calc R . .
H20L H 0.3646 0.8906 0.6501 0.128 Uiso 1 1 calc R . .
C209 C 0.4693(11) 0.7926(7) 0.7126(6) 0.079(5) Uani 1 1 d . . .
H20M H 0.4318 0.7660 0.6917 0.118 Uiso 1 1 calc R . .
H20N H 0.4325 0.8087 0.7326 0.118 Uiso 1 1 calc R . .
H20O H 0.5206 0.7701 0.7288 0.118 Uiso 1 1 calc R . .
C210 C 0.6964(15) 0.9100(9) 0.6204(6) 0.106(7) Uani 1 1 d . . .
H21A H 0.6809 0.9407 0.6400 0.159 Uiso 1 1 calc R . .
H21B H 0.7188 0.9291 0.5965 0.159 Uiso 1 1 calc R . .
H21C H 0.7437 0.8838 0.6362 0.159 Uiso 1 1 calc R . .
C211 C 0.4991(13) 0.9128(8) 0.5662(5) 0.084(5) Uani 1 1 d . . .
H21D H 0.4530 0.8878 0.5483 0.126 Uiso 1 1 calc R . .
H21E H 0.5264 0.9396 0.5476 0.126 Uiso 1 1 calc R . .
H21F H 0.4705 0.9365 0.5862 0.126 Uiso 1 1 calc R . .
C212 C 0.6261(11) 0.8080(6) 0.5591(5) 0.064(4) Uani 1 1 d . . .
H21G H 0.6683 0.7790 0.5753 0.096 Uiso 1 1 calc R . .
H21H H 0.6562 0.8292 0.5385 0.096 Uiso 1 1 calc R . .
H21I H 0.5724 0.7871 0.5435 0.096 Uiso 1 1 calc R . .
C213 C -0.0163(18) 0.4157(8) 0.6818(7) 0.152(10) Uani 1 1 d DU . .
H21J H 0.0270 0.4199 0.7091 0.227 Uiso 1 1 calc R . .
H21K H -0.0236 0.3732 0.6741 0.227 Uiso 1 1 calc R . .
H21L H -0.0752 0.4323 0.6850 0.227 Uiso 1 1 calc R . .
C214 C 0.0182(8) 0.4482(5) 0.6472(4) 0.098(6) Uani 1 1 d GDU . .
C215 C 0.0014(8) 0.5090(5) 0.6414(4) 0.085(5) Uani 1 1 d GDU . .
H215 H -0.0321 0.5296 0.6597 0.102 Uiso 1 1 calc R . .
C216 C 0.0337(9) 0.5397(5) 0.6090(4) 0.103(6) Uani 1 1 d GU . .
H216 H 0.0222 0.5812 0.6050 0.124 Uiso 1 1 calc R . .
C217 C 0.0827(10) 0.5095(7) 0.5823(4) 0.116(7) Uani 1 1 d GU . .
H217 H 0.1048 0.5304 0.5601 0.139 Uiso 1 1 calc R . .
C218 C 0.0995(9) 0.4486(7) 0.5880(4) 0.158(11) Uani 1 1 d GU . .
H218 H 0.1330 0.4280 0.5698 0.190 Uiso 1 1 calc R . .
C219 C 0.0672(9) 0.4180(5) 0.6205(5) 0.110(6) Uani 1 1 d GDU . .
H219 H 0.0786 0.3764 0.6244 0.132 Uiso 1 1 calc R . .
C220 C 0.349(2) 0.9228(12) 0.7859(8) 0.144(10) Uani 1 1 d . . .
H22A H 0.3228 0.8862 0.7718 0.216 Uiso 1 1 calc R . .
H22B H 0.4028 0.9341 0.7740 0.216 Uiso 1 1 calc R . .
H22C H 0.3041 0.9551 0.7806 0.216 Uiso 1 1 calc R . .
C221 C 0.3768(11) 0.9122(5) 0.8342(4) 0.101(7) Uani 1 1 d G . .
C222 C 0.3148(7) 0.8933(6) 0.8592(5) 0.089(5) Uani 1 1 d G . .
H222 H 0.2534 0.8857 0.8461 0.107 Uiso 1 1 calc R . .
C223 C 0.3426(12) 0.8856(6) 0.9035(5) 0.099(6) Uani 1 1 d G . .
H223 H 0.3002 0.8727 0.9206 0.118 Uiso 1 1 calc R . .
C224 C 0.4323(13) 0.8968(6) 0.9228(4) 0.119(8) Uani 1 1 d G . .
H224 H 0.4513 0.8915 0.9531 0.142 Uiso 1 1 calc R . .
C225 C 0.4943(8) 0.9157(6) 0.8978(7) 0.130(9) Uani 1 1 d G . .
H225 H 0.5557 0.9233 0.9110 0.156 Uiso 1 1 calc R . .
C226 C 0.4665(9) 0.9234(6) 0.8535(6) 0.127(9) Uani 1 1 d G . .
H226 H 0.5089 0.9363 0.8364 0.153 Uiso 1 1 calc R . .
C227 C -0.0940(18) 0.9621(12) 0.5745(9) 0.149(10) Uani 1 1 d . . .
H22D H -0.0795 1.0002 0.5620 0.223 Uiso 1 1 calc R . .
H22E H -0.1524 0.9655 0.5841 0.223 Uiso 1 1 calc R . .
H22F H -0.0977 0.9306 0.5527 0.223 Uiso 1 1 calc R . .
C228 C -0.0171(8) 0.9461(6) 0.6144(6) 0.106(7) Uani 1 1 d G . .
C229 C 0.0671(11) 0.9369(6) 0.6029(5) 0.104(7) Uani 1 1 d G . .
H229 H 0.0727 0.9379 0.5734 0.125 Uiso 1 1 calc R . .
C230 C 0.1432(8) 0.9261(6) 0.6347(7) 0.146(12) Uani 1 1 d G . .
H230 H 0.2008 0.9197 0.6269 0.175 Uiso 1 1 calc R . .
C231 C 0.1351(14) 0.9245(6) 0.6780(6) 0.129(10) Uani 1 1 d G . .
H231 H 0.1871 0.9172 0.6997 0.155 Uiso 1 1 calc R . .
C232 C 0.0509(19) 0.9338(6) 0.6894(5) 0.134(10) Uani 1 1 d G . .
H232 H 0.0454 0.9328 0.7190 0.160 Uiso 1 1 calc R . .
C233 C -0.0252(12) 0.9446(6) 0.6576(7) 0.135(11) Uani 1 1 d G . .
H233 H -0.0828 0.9509 0.6655 0.162 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Y1 N2 101.9(3) . . ?
O2 Y1 O1 67.8(3) . . ?
N2 Y1 O1 134.6(3) . . ?
O2 Y1 N4 154.5(4) . . ?
N2 Y1 N4 85.0(4) . . ?
O1 Y1 N4 123.9(3) . . ?
O2 Y1 N3 84.6(4) . . ?
N2 Y1 N3 108.9(4) . . ?
O1 Y1 N3 113.7(3) . . ?
N4 Y1 N3 69.9(4) . . ?
O2 Y1 N1 124.9(3) . . ?
N2 Y1 N1 71.6(4) . . ?
O1 Y1 N1 79.1(3) . . ?
N4 Y1 N1 80.6(4) . . ?
N3 Y1 N1 150.3(4) . . ?
O2 Y1 C2 91.0(4) . . ?
N2 Y1 C2 152.5(4) . . ?
O1 Y1 C2 31.7(3) . . ?
N4 Y1 C2 93.7(4) . . ?
N3 Y1 C2 96.3(4) . . ?
N1 Y1 C2 81.1(4) . . ?
O2 Y1 C27 26.4(3) . . ?
N2 Y1 C27 81.7(4) . . ?
O1 Y1 C27 94.0(3) . . ?
N4 Y1 C27 136.3(4) . . ?
N3 Y1 C27 75.4(4) . . ?
N1 Y1 C27 132.3(4) . . ?
C2 Y1 C27 116.2(4) . . ?
O2 Y1 Y3 35.23(19) . . ?
N2 Y1 Y3 118.1(3) . . ?
O1 Y1 Y3 33.6(2) . . ?
N4 Y1 Y3 155.4(3) . . ?
N3 Y1 Y3 106.7(3) . . ?
N1 Y1 Y3 98.2(2) . . ?
C2 Y1 Y3 62.1(3) . . ?
C27 Y1 Y3 60.8(2) . . ?
O3 Y2 O4 70.0(3) . . ?
O3 Y2 N8 100.9(4) . . ?
O4 Y2 N8 134.1(4) . . ?
O3 Y2 N6 153.7(3) . . ?
O4 Y2 N6 123.1(4) . . ?
N8 Y2 N6 85.3(4) . . ?
O3 Y2 N5 83.1(3) . . ?
O4 Y2 N5 115.5(3) . . ?
N8 Y2 N5 107.5(4) . . ?
N6 Y2 N5 70.7(4) . . ?
O3 Y2 N7 123.8(3) . . ?
O4 Y2 N7 76.9(3) . . ?
N8 Y2 N7 71.9(4) . . ?
N6 Y2 N7 82.5(4) . . ?
N5 Y2 N7 153.0(4) . . ?
O3 Y2 C77 94.6(4) . . ?
O4 Y2 C77 32.3(4) . . ?
N8 Y2 C77 150.2(5) . . ?
N6 Y2 C77 92.0(5) . . ?
N5 Y2 C77 99.4(4) . . ?
N7 Y2 C77 78.4(5) . . ?
O3 Y2 C52 27.4(4) . . ?
O4 Y2 C52 97.1(4) . . ?
N8 Y2 C52 78.9(4) . . ?
N6 Y2 C52 135.1(4) . . ?
N5 Y2 C52 74.6(4) . . ?
N7 Y2 C52 129.8(4) . . ?
C77 Y2 C52 121.4(5) . . ?
O3 Y2 Y3 35.6(2) . . ?
O4 Y2 Y3 35.5(2) . . ?
N8 Y2 Y3 117.1(3) . . ?
N6 Y2 Y3 156.4(3) . . ?
N5 Y2 Y3 106.6(3) . . ?
N7 Y2 Y3 96.9(3) . . ?
C77 Y2 Y3 65.0(4) . . ?
C52 Y2 Y3 61.8(3) . . ?
O1 Y3 N9 95.8(4) . . ?
O1 Y3 O4 169.5(3) . . ?
N9 Y3 O4 94.7(4) . . ?
O1 Y3 O3 100.2(3) . . ?
N9 Y3 O3 126.7(4) . . ?
O4 Y3 O3 73.4(3) . . ?
O1 Y3 O2 71.9(3) . . ?
N9 Y3 O2 131.1(4) . . ?
O4 Y3 O2 100.9(3) . . ?
O3 Y3 O2 102.2(3) . . ?
O1 Y3 Si2 106.8(2) . . ?
N9 Y3 Si2 27.6(3) . . ?
O4 Y3 Si2 82.7(3) . . ?
O3 Y3 Si2 143.3(2) . . ?
O2 Y3 Si2 109.5(2) . . ?
O1 Y3 Si1 84.6(2) . . ?
N9 Y3 Si1 26.3(3) . . ?
O4 Y3 Si1 105.0(2) . . ?
O3 Y3 Si1 105.7(2) . . ?
O2 Y3 Si1 146.2(2) . . ?
Si2 Y3 Si1 53.91(11) . . ?
O1 Y3 Y2 134.3(2) . . ?
N9 Y3 Y2 121.2(3) . . ?
O4 Y3 Y2 37.4(2) . . ?
O3 Y3 Y2 37.1(2) . . ?
O2 Y3 Y2 97.5(2) . . ?
Si2 Y3 Y2 118.44(9) . . ?
Si1 Y3 Y2 116.25(9) . . ?
O1 Y3 Y1 36.4(2) . . ?
N9 Y3 Y1 123.6(3) . . ?
O4 Y3 Y1 134.8(2) . . ?
O3 Y3 Y1 97.0(2) . . ?
O2 Y3 Y1 36.7(2) . . ?
Si2 Y3 Y1 119.46(8) . . ?
Si1 Y3 Y1 120.05(8) . . ?
Y2 Y3 Y1 115.13(5) . . ?
O6 Y4 O5 69.3(3) . . ?
O6 Y4 N11 101.2(3) . . ?
O5 Y4 N11 132.3(3) . . ?
O6 Y4 N13 153.2(4) . . ?
O5 Y4 N13 123.0(3) . . ?
N11 Y4 N13 86.9(4) . . ?
O6 Y4 N12 83.7(3) . . ?
O5 Y4 N12 116.0(3) . . ?
N11 Y4 N12 108.7(3) . . ?
N13 Y4 N12 69.5(4) . . ?
O6 Y4 N10 128.4(3) . . ?
O5 Y4 N10 77.8(3) . . ?
N11 Y4 N10 73.0(4) . . ?
N13 Y4 N10 78.4(4) . . ?
N12 Y4 N10 147.6(4) . . ?
O6 Y4 C108 91.3(4) . . ?
O5 Y4 C108 31.8(3) . . ?
N11 Y4 C108 151.9(4) . . ?
N13 Y4 C108 93.2(4) . . ?
N12 Y4 C108 97.5(4) . . ?
N10 Y4 C108 79.4(4) . . ?
O6 Y4 C133 26.7(3) . . ?
O5 Y4 C133 95.3(3) . . ?
N11 Y4 C133 79.2(4) . . ?
N13 Y4 C133 136.9(4) . . ?
N12 Y4 C133 76.8(4) . . ?
N10 Y4 C133 133.4(3) . . ?
C108 Y4 C133 117.6(4) . . ?
O6 Y4 Y6 35.3(2) . . ?
O5 Y4 Y6 34.93(18) . . ?
N11 Y4 Y6 116.9(2) . . ?
N13 Y4 Y6 155.1(3) . . ?
N12 Y4 Y6 106.6(3) . . ?
N10 Y4 Y6 100.4(2) . . ?
C108 Y4 Y6 62.5(3) . . ?
C133 Y4 Y6 60.5(2) . . ?
O7 Y5 O8 70.8(3) . . ?
O7 Y5 N15 133.0(4) . . ?
O8 Y5 N15 98.9(4) . . ?
O7 Y5 N17 121.7(4) . . ?
O8 Y5 N17 153.3(4) . . ?
N15 Y5 N17 88.4(4) . . ?
O7 Y5 N14 77.3(3) . . ?
O8 Y5 N14 125.0(3) . . ?
N15 Y5 N14 72.2(4) . . ?
N17 Y5 N14 81.7(4) . . ?
O7 Y5 N16 113.4(3) . . ?
O8 Y5 N16 83.1(3) . . ?
N15 Y5 N16 110.4(4) . . ?
N17 Y5 N16 70.3(4) . . ?
N14 Y5 N16 151.7(3) . . ?
O7 Y5 C158 31.6(3) . . ?
O8 Y5 C158 95.0(4) . . ?
N15 Y5 C158 149.9(5) . . ?
N17 Y5 C158 91.0(4) . . ?
N14 Y5 C158 78.0(4) . . ?
N16 Y5 C158 97.6(4) . . ?
O7 Y5 C183 96.4(3) . . ?
O8 Y5 C183 25.9(3) . . ?
N15 Y5 C183 78.7(4) . . ?
N17 Y5 C183 136.2(4) . . ?
N14 Y5 C183 131.2(3) . . ?
N16 Y5 C183 75.4(4) . . ?
C158 Y5 C183 120.2(4) . . ?
O7 Y5 Y6 35.56(19) . . ?
O8 Y5 Y6 35.9(2) . . ?
N15 Y5 Y6 116.4(3) . . ?
N17 Y5 Y6 154.2(3) . . ?
N14 Y5 Y6 98.6(2) . . ?
N16 Y5 Y6 104.6(2) . . ?
C158 Y5 Y6 64.1(3) . . ?
C183 Y5 Y6 61.1(3) . . ?
N18 Y6 O5 97.2(3) . . ?
N18 Y6 O7 94.9(3) . . ?
O5 Y6 O7 167.9(3) . . ?
N18 Y6 O6 128.3(3) . . ?
O5 Y6 O6 72.3(3) . . ?
O7 Y6 O6 100.4(3) . . ?
N18 Y6 O8 129.3(3) . . ?
O5 Y6 O8 98.3(3) . . ?
O7 Y6 O8 73.3(3) . . ?
O6 Y6 O8 102.4(3) . . ?
N18 Y6 Si4 28.3(3) . . ?
O5 Y6 Si4 108.7(2) . . ?
O7 Y6 Si4 82.4(2) . . ?
O6 Y6 Si4 106.0(2) . . ?
O8 Y6 Si4 145.4(2) . . ?
N18 Y6 Si3 26.0(3) . . ?
O5 Y6 Si3 84.9(2) . . ?
O7 Y6 Si3 106.0(2) . . ?
O6 Y6 Si3 143.4(2) . . ?
O8 Y6 Si3 109.1(2) . . ?
Si4 Y6 Si3 54.38(11) . . ?
N18 Y6 Y5 121.2(2) . . ?
O5 Y6 Y5 133.1(2) . . ?
O7 Y6 Y5 36.9(2) . . ?
O6 Y6 Y5 98.8(2) . . ?
O8 Y6 Y5 37.2(2) . . ?
Si4 Y6 Y5 117.82(8) . . ?
Si3 Y6 Y5 117.62(8) . . ?
N18 Y6 Y4 122.9(2) . . ?
O5 Y6 Y4 36.7(2) . . ?
O7 Y6 Y4 133.9(2) . . ?
O6 Y6 Y4 36.5(2) . . ?
O8 Y6 Y4 96.8(2) . . ?
Si4 Y6 Y4 117.78(8) . . ?
Si3 Y6 Y4 119.47(8) . . ?
Y5 Y6 Y4 115.86(4) . . ?
N9 Si1 C102 115.2(7) . . ?
N9 Si1 C103 107.1(6) . . ?
C102 Si1 C103 107.7(8) . . ?
N9 Si1 C101 113.4(7) . . ?
C102 Si1 C101 105.2(10) . . ?
C103 Si1 C101 107.9(9) . . ?
N9 Si1 Y3 35.2(4) . . ?
C102 Si1 Y3 126.7(6) . . ?
C103 Si1 Y3 71.9(5) . . ?
C101 Si1 Y3 126.2(7) . . ?
N9 Si2 C105 115.0(7) . . ?
N9 Si2 C104 113.5(7) . . ?
C105 Si2 C104 107.6(8) . . ?
N9 Si2 C106 108.4(6) . . ?
C105 Si2 C106 104.5(8) . . ?
C104 Si2 C106 107.1(7) . . ?
N9 Si2 Y3 36.7(3) . . ?
C105 Si2 Y3 127.3(6) . . ?
C104 Si2 Y3 124.1(6) . . ?
C106 Si2 Y3 71.8(5) . . ?
N18 Si3 C207 115.2(7) . . ?
N18 Si3 C208 113.5(7) . . ?
C207 Si3 C208 107.2(8) . . ?
N18 Si3 C209 105.8(7) . . ?
C207 Si3 C209 107.2(8) . . ?
C208 Si3 C209 107.5(8) . . ?
N18 Si3 Y6 34.2(4) . . ?
C207 Si3 Y6 123.1(6) . . ?
C208 Si3 Y6 127.9(6) . . ?
C209 Si3 Y6 71.7(5) . . ?
N18 Si4 C212 108.8(6) . . ?
N18 Si4 C211 111.6(7) . . ?
C212 Si4 C211 107.7(7) . . ?
N18 Si4 C210 112.2(7) . . ?
C212 Si4 C210 106.1(9) . . ?
C211 Si4 C210 110.2(9) . . ?
N18 Si4 Y6 36.5(4) . . ?
C212 Si4 Y6 72.3(4) . . ?
C211 Si4 Y6 123.3(6) . . ?
C210 Si4 Y6 124.5(6) . . ?
C21 N1 C12 120.2(12) . . ?
C21 N1 Y1 110.6(9) . . ?
C12 N1 Y1 129.2(8) . . ?
C25 N2 C22 105.6(12) . . ?
C25 N2 Y1 136.9(11) . . ?
C22 N2 Y1 113.9(8) . . ?
C46 N3 C37 118.0(12) . . ?
C46 N3 Y1 113.5(10) . . ?
C37 N3 Y1 126.8(9) . . ?
C50 N4 C47 105.6(13) . . ?
C50 N4 Y1 139.1(10) . . ?
C47 N4 Y1 115.3(9) . . ?
C71 N5 C62 119.3(13) . . ?
C71 N5 Y2 113.0(10) . . ?
C62 N5 Y2 126.2(9) . . ?
C75 N6 C72 104.1(11) . . ?
C75 N6 Y2 139.9(9) . . ?
C72 N6 Y2 115.1(8) . . ?
C96 N7 C87 115.7(12) . . ?
C96 N7 Y2 111.6(9) . . ?
C87 N7 Y2 132.5(9) . . ?
C100 N8 C97 106.7(14) . . ?
C100 N8 Y2 131.9(12) . . ?
C97 N8 Y2 111.4(9) . . ?
Si1 N9 Si2 125.8(6) . . ?
Si1 N9 Y3 118.5(6) . . ?
Si2 N9 Y3 115.7(5) . . ?
C127 N10 C118 118.6(12) . . ?
C127 N10 Y4 109.2(9) . . ?
C118 N10 Y4 132.2(8) . . ?
C131 N11 C128 104.0(12) . . ?
C131 N11 Y4 141.7(11) . . ?
C128 N11 Y4 111.4(8) . . ?
C152 N12 C143 118.2(11) . . ?
C152 N12 Y4 113.5(10) . . ?
C143 N12 Y4 126.0(7) . . ?
C156 N13 C153 105.4(11) . . ?
C156 N13 Y4 139.4(9) . . ?
C153 N13 Y4 114.6(8) . . ?
C177 N14 C168 118.7(11) . . ?
C177 N14 Y5 109.1(9) . . ?
C168 N14 Y5 132.2(8) . . ?
C181 N15 C178 106.2(12) . . ?
C181 N15 Y5 135.8(10) . . ?
C178 N15 Y5 110.4(10) . . ?
C202 N16 C193 118.7(12) . . ?
C202 N16 Y5 112.0(9) . . ?
C193 N16 Y5 126.8(8) . . ?
C206 N17 C203 102.6(11) . . ?
C206 N17 Y5 141.4(10) . . ?
C203 N17 Y5 115.7(9) . . ?
Si3 N18 Si4 125.1(6) . . ?
Si3 N18 Y6 119.7(6) . . ?
Si4 N18 Y6 115.1(5) . . ?
C2 O1 Y3 143.6(7) . . ?
C2 O1 Y1 85.0(6) . . ?
Y3 O1 Y1 110.0(4) . . ?
C27 O2 Y3 142.7(8) . . ?
C27 O2 Y1 105.2(7) . . ?
Y3 O2 Y1 108.1(3) . . ?
C52 O3 Y3 142.7(8) . . ?
C52 O3 Y2 103.6(8) . . ?
Y3 O3 Y2 107.3(4) . . ?
C77 O4 Y3 146.8(9) . . ?
C77 O4 Y2 85.4(7) . . ?
Y3 O4 Y2 107.0(3) . . ?
C108 O5 Y6 139.3(8) . . ?
C108 O5 Y4 86.0(6) . . ?
Y6 O5 Y4 108.3(3) . . ?
C133 O6 Y6 139.3(7) . . ?
C133 O6 Y4 104.9(6) . . ?
Y6 O6 Y4 108.3(4) . . ?
C158 O7 Y6 144.6(8) . . ?
C158 O7 Y5 86.8(6) . . ?
Y6 O7 Y5 107.6(4) . . ?
C183 O8 Y6 142.1(8) . . ?
C183 O8 Y5 106.9(7) . . ?
Y6 O8 Y5 106.9(3) . . ?
C6 C1 C11 120.9(12) . . ?
C6 C1 C2 121.0(11) . . ?
C11 C1 C2 117.9(12) . . ?
O1 C2 C3 121.3(11) . . ?
O1 C2 C1 122.0(11) . . ?
C3 C2 C1 116.0(12) . . ?
O1 C2 Y1 63.3(6) . . ?
C3 C2 Y1 100.0(8) . . ?
C1 C2 Y1 99.4(7) . . ?
C4 C3 C2 121.4(12) . . ?
C4 C3 H3 119.3 . . ?
C2 C3 H3 119.3 . . ?
C5 C4 C3 122.8(13) . . ?
C5 C4 H4 118.6 . . ?
C3 C4 H4 118.6 . . ?
C4 C5 C6 118.2(13) . . ?
C4 C5 C10 121.0(13) . . ?
C6 C5 C10 120.7(13) . . ?
C1 C6 C5 120.4(12) . . ?
C1 C6 C7 119.7(12) . . ?
C5 C6 C7 119.9(12) . . ?
C8 C7 C6 114.7(13) . . ?
C8 C7 H7A 108.6 . . ?
C6 C7 H7A 108.6 . . ?
C8 C7 H7B 108.6 . . ?
C6 C7 H7B 108.6 . . ?
H7A C7 H7B 107.6 . . ?
C7 C8 C9 111.2(14) . . ?
C7 C8 H8A 109.4 . . ?
C9 C8 H8A 109.4 . . ?
C7 C8 H8B 109.4 . . ?
C9 C8 H8B 109.4 . . ?
H8A C8 H8B 108.0 . . ?
C8 C9 C10 107.1(14) . . ?
C8 C9 H9A 110.3 . . ?
C10 C9 H9A 110.3 . . ?
C8 C9 H9B 110.3 . . ?
C10 C9 H9B 110.3 . . ?
H9A C9 H9B 108.5 . . ?
C5 C10 C9 113.4(13) . . ?
C5 C10 H10A 108.9 . . ?
C9 C10 H10A 108.9 . . ?
C5 C10 H10B 108.9 . . ?
C9 C10 H10B 108.9 . . ?
H10A C10 H10B 107.7 . . ?
C16 C11 C12 118.5(11) . . ?
C16 C11 C1 117.9(12) . . ?
C12 C11 C1 123.6(10) . . ?
N1 C12 C13 121.0(11) . . ?
N1 C12 C11 118.7(10) . . ?
C13 C12 C11 120.2(11) . . ?
C14 C13 C12 117.0(13) . . ?
C14 C13 H13 121.5 . . ?
C12 C13 H13 121.5 . . ?
C13 C14 C15 124.2(12) . . ?
C13 C14 H14 117.9 . . ?
C15 C14 H14 117.9 . . ?
C16 C15 C14 118.6(13) . . ?
C16 C15 C20 121.7(14) . . ?
C14 C15 C20 119.7(12) . . ?
C15 C16 C11 121.1(13) . . ?
C15 C16 C17 117.9(14) . . ?
C11 C16 C17 120.9(13) . . ?
C18 C17 C16 117.2(15) . . ?
C18 C17 H17A 108.0 . . ?
C16 C17 H17A 108.0 . . ?
C18 C17 H17B 108.0 . . ?
C16 C17 H17B 108.0 . . ?
H17A C17 H17B 107.3 . . ?
C19 C18 C17 123(3) . . ?
C19 C18 H18A 106.5 . . ?
C17 C18 H18A 106.5 . . ?
C19 C18 H18B 106.5 . . ?
C17 C18 H18B 106.5 . . ?
H18A C18 H18B 106.5 . . ?
C18 C19 C20 119.8(18) . . ?
C18 C19 H19A 107.4 . . ?
C20 C19 H19A 107.4 . . ?
C18 C19 H19B 107.4 . . ?
C20 C19 H19B 107.4 . . ?
H19A C19 H19B 106.9 . . ?
C19 C20 C15 113.6(13) . . ?
C19 C20 H20A 108.8 . . ?
C15 C20 H20A 108.8 . . ?
C19 C20 H20B 108.8 . . ?
C15 C20 H20B 108.8 . . ?
H20A C20 H20B 107.7 . . ?
N1 C21 C22 122.8(13) . . ?
N1 C21 H21 118.6 . . ?
C22 C21 H21 118.6 . . ?
N2 C22 C21 119.1(12) . . ?
N2 C22 C23 110.8(12) . . ?
C21 C22 C23 129.7(13) . . ?
C22 C23 C24 105.4(13) . . ?
C22 C23 H23 127.3 . . ?
C24 C23 H23 127.3 . . ?
C25 C24 C23 106.4(14) . . ?
C25 C24 H24 126.8 . . ?
C23 C24 H24 126.8 . . ?
N2 C25 C24 111.8(16) . . ?
N2 C25 H25 124.1 . . ?
C24 C25 H25 124.1 . . ?
C27 C26 C31 122.3(13) . . ?
C27 C26 C36 118.6(11) . . ?
C31 C26 C36 119.0(11) . . ?
C26 C27 O2 123.8(12) . . ?
C26 C27 C28 118.7(12) . . ?
O2 C27 C28 117.0(11) . . ?
C26 C27 Y1 101.9(8) . . ?
O2 C27 Y1 48.5(6) . . ?
C28 C27 Y1 112.5(9) . . ?
C29 C28 C27 118.2(14) . . ?
C29 C28 H28 120.9 . . ?
C27 C28 H28 120.9 . . ?
C30 C29 C28 121.3(15) . . ?
C30 C29 H29 119.3 . . ?
C28 C29 H29 119.3 . . ?
C29 C30 C31 121.3(15) . . ?
C29 C30 C35 117.3(16) . . ?
C31 C30 C35 121.3(18) . . ?
C26 C31 C30 117.6(14) . . ?
C26 C31 C32 119.0(14) . . ?
C30 C31 C32 123.4(14) . . ?
C33 C32 C31 110.6(15) . . ?
C33 C32 H32A 109.5 . . ?
C31 C32 H32A 109.5 . . ?
C33 C32 H32B 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 108.1 . . ?
C32 C33 C34 105.4(17) . . ?
C32 C33 H33A 110.7 . . ?
C34 C33 H33A 110.7 . . ?
C32 C33 H33B 110.7 . . ?
C34 C33 H33B 110.7 . . ?
H33A C33 H33B 108.8 . . ?
C35 C34 C33 112.7(19) . . ?
C35 C34 H34A 109.1 . . ?
C33 C34 H34A 109.1 . . ?
C35 C34 H34B 109.1 . . ?
C33 C34 H34B 109.1 . . ?
H34A C34 H34B 107.8 . . ?
C34 C35 C30 110.4(18) . . ?
C34 C35 H35A 109.6 . . ?
C30 C35 H35A 109.6 . . ?
C34 C35 H35B 109.6 . . ?
C30 C35 H35B 109.6 . . ?
H35A C35 H35B 108.1 . . ?
C41 C36 C37 118.8(14) . . ?
C41 C36 C26 118.3(14) . . ?
C37 C36 C26 122.9(13) . . ?
C38 C37 C36 121.7(15) . . ?
C38 C37 N3 120.1(14) . . ?
C36 C37 N3 118.1(13) . . ?
C37 C38 C39 119.3(15) . . ?
C37 C38 H38 120.4 . . ?
C39 C38 H38 120.4 . . ?
C40 C39 C38 120.9(15) . . ?
C40 C39 H39 119.6 . . ?
C38 C39 H39 119.6 . . ?
C39 C40 C41 117.3(14) . . ?
C39 C40 C45 116.6(15) . . ?
C41 C40 C45 126.1(16) . . ?
C36 C41 C40 121.9(15) . . ?
C36 C41 C42 121.0(14) . . ?
C40 C41 C42 117.1(14) . . ?
C43 C42 C41 115.1(17) . . ?
C43 C42 H42A 108.5 . . ?
C41 C42 H42A 108.5 . . ?
C43 C42 H42B 108.5 . . ?
C41 C42 H42B 108.5 . . ?
H42A C42 H42B 107.5 . . ?
C44 C43 C42 123(2) . . ?
C44 C43 H43A 106.6 . . ?
C42 C43 H43A 106.6 . . ?
C44 C43 H43B 106.6 . . ?
C42 C43 H43B 106.6 . . ?
H43A C43 H43B 106.6 . . ?
C43 C44 C45 120.4(19) . . ?
C43 C44 H44A 107.2 . . ?
C45 C44 H44A 107.2 . . ?
C43 C44 H44B 107.2 . . ?
C45 C44 H44B 107.2 . . ?
H44A C44 H44B 106.9 . . ?
C44 C45 C40 113.9(17) . . ?
C44 C45 H45A 108.8 . . ?
C40 C45 H45A 108.8 . . ?
C44 C45 H45B 108.8 . . ?
C40 C45 H45B 108.8 . . ?
H45A C45 H45B 107.7 . . ?
N3 C46 C47 125.3(13) . . ?
N3 C46 H46 117.4 . . ?
C47 C46 H46 117.4 . . ?
C46 C47 C48 134.0(13) . . ?
C46 C47 N4 115.9(12) . . ?
C48 C47 N4 110.0(13) . . ?
C49 C48 C47 106.0(14) . . ?
C49 C48 H48 127.0 . . ?
C47 C48 H48 127.0 . . ?
C48 C49 C50 105.2(17) . . ?
C48 C49 H49 127.4 . . ?
C50 C49 H49 127.4 . . ?
N4 C50 C49 113.0(16) . . ?
N4 C50 H50 123.5 . . ?
C49 C50 H50 123.5 . . ?
C56 C51 C52 120.2(13) . . ?
C56 C51 C61 119.6(12) . . ?
C52 C51 C61 119.9(12) . . ?
C53 C52 O3 120.3(13) . . ?
C53 C52 C51 118.7(14) . . ?
O3 C52 C51 120.9(12) . . ?
C53 C52 Y2 114.3(10) . . ?
O3 C52 Y2 49.0(6) . . ?
C51 C52 Y2 106.1(9) . . ?
C54 C53 C52 120.7(16) . . ?
C54 C53 H53 119.7 . . ?
C52 C53 H53 119.7 . . ?
C53 C54 C55 121.2(15) . . ?
C53 C54 H54 119.4 . . ?
C55 C54 H54 119.4 . . ?
C56 C55 C54 118.1(14) . . ?
C56 C55 C60 116.0(16) . . ?
C54 C55 C60 125.8(16) . . ?
C55 C56 C51 119.1(13) . . ?
C55 C56 C57 114.1(15) . . ?
C51 C56 C57 126.8(16) . . ?
C56 C57 C58 111.8(18) . . ?
C56 C57 H57A 109.3 . . ?
C58 C57 H57A 109.3 . . ?
C56 C57 H57B 109.3 . . ?
C58 C57 H57B 109.3 . . ?
H57A C57 H57B 107.9 . . ?
C59 C58 C57 117(2) . . ?
C59 C58 H58A 108.0 . . ?
C57 C58 H58A 108.0 . . ?
C59 C58 H58B 108.0 . . ?
C57 C58 H58B 108.0 . . ?
H58A C58 H58B 107.2 . . ?
C58 C59 C60 107.6(19) . . ?
C58 C59 H59A 110.2 . . ?
C60 C59 H59A 110.2 . . ?
C58 C59 H59B 110.2 . . ?
C60 C59 H59B 110.2 . . ?
H59A C59 H59B 108.5 . . ?
C55 C60 C59 115.7(18) . . ?
C55 C60 H60A 108.3 . . ?
C59 C60 H60A 108.3 . . ?
C55 C60 H60B 108.3 . . ?
C59 C60 H60B 108.3 . . ?
H60A C60 H60B 107.4 . . ?
C62 C61 C66 121.0(13) . . ?
C62 C61 C51 122.8(13) . . ?
C66 C61 C51 116.0(12) . . ?
C61 C62 C63 119.3(13) . . ?
C61 C62 N5 121.0(13) . . ?
C63 C62 N5 119.7(13) . . ?
C64 C63 C62 121.1(13) . . ?
C64 C63 H63 119.4 . . ?
C62 C63 H63 119.4 . . ?
C65 C64 C63 120.9(14) . . ?
C65 C64 H64 119.5 . . ?
C63 C64 H64 119.5 . . ?
C64 C65 C66 119.0(13) . . ?
C64 C65 C70 118.7(16) . . ?
C66 C65 C70 122.4(17) . . ?
C61 C66 C65 118.5(14) . . ?
C61 C66 C67 121.7(13) . . ?
C65 C66 C67 119.6(15) . . ?
C66 C67 C68 111.8(15) . . ?
C66 C67 H67A 109.2 . . ?
C68 C67 H67A 109.2 . . ?
C66 C67 H67B 109.2 . . ?
C68 C67 H67B 109.2 . . ?
H67A C67 H67B 107.9 . . ?
C69 C68 C67 108.1(15) . . ?
C69 C68 H68A 110.1 . . ?
C67 C68 H68A 110.1 . . ?
C69 C68 H68B 110.1 . . ?
C67 C68 H68B 110.1 . . ?
H68A C68 H68B 108.4 . . ?
C70 C69 C68 114.3(16) . . ?
C70 C69 H69A 108.7 . . ?
C68 C69 H69A 108.7 . . ?
C70 C69 H69B 108.7 . . ?
C68 C69 H69B 108.7 . . ?
H69A C69 H69B 107.6 . . ?
C69 C70 C65 113.0(15) . . ?
C69 C70 H70A 109.0 . . ?
C65 C70 H70A 109.0 . . ?
C69 C70 H70B 109.0 . . ?
C65 C70 H70B 109.0 . . ?
H70A C70 H70B 107.8 . . ?
N5 C71 C72 124.2(14) . . ?
N5 C71 H71 117.9 . . ?
C72 C71 H71 117.9 . . ?
C73 C72 C71 133.2(14) . . ?
C73 C72 N6 109.9(12) . . ?
C71 C72 N6 116.9(12) . . ?
C72 C73 C74 107.7(14) . . ?
C72 C73 H73 126.1 . . ?
C74 C73 H73 126.1 . . ?
C75 C74 C73 102.5(13) . . ?
C75 C74 H74 128.8 . . ?
C73 C74 H74 128.8 . . ?
N6 C75 C74 115.6(14) . . ?
N6 C75 H75 122.2 . . ?
C74 C75 H75 122.2 . . ?
C77 C76 C81 121.5(13) . . ?
C77 C76 C86 119.9(13) . . ?
C81 C76 C86 118.6(12) . . ?
C76 C77 C78 120.9(14) . . ?
C76 C77 O4 122.0(13) . . ?
C78 C77 O4 115.9(14) . . ?
C76 C77 Y2 102.8(10) . . ?
C78 C77 Y2 93.3(9) . . ?
O4 C77 Y2 62.3(7) . . ?
C77 C78 C79 118.0(13) . . ?
C77 C78 H78 121.0 . . ?
C79 C78 H78 121.0 . . ?
C80 C79 C78 123.3(14) . . ?
C80 C79 H79 118.3 . . ?
C78 C79 H79 118.3 . . ?
C79 C80 C81 118.1(14) . . ?
C79 C80 C85 119.8(14) . . ?
C81 C80 C85 122.0(14) . . ?
C80 C81 C76 117.9(14) . . ?
C80 C81 C82 120.7(15) . . ?
C76 C81 C82 121.3(13) . . ?
C81 C82 C83 116.6(15) . . ?
C81 C82 H82A 108.1 . . ?
C83 C82 H82A 108.1 . . ?
C81 C82 H82B 108.1 . . ?
C83 C82 H82B 108.1 . . ?
H82A C82 H82B 107.3 . . ?
C84 C83 C82 114.0(17) . . ?
C84 C83 H83A 108.8 . . ?
C82 C83 H83A 108.8 . . ?
C84 C83 H83B 108.8 . . ?
C82 C83 H83B 108.8 . . ?
H83A C83 H83B 107.7 . . ?
C83 C84 C85 116(2) . . ?
C83 C84 H84A 108.2 . . ?
C85 C84 H84A 108.2 . . ?
C83 C84 H84B 108.2 . . ?
C85 C84 H84B 108.2 . . ?
H84A C84 H84B 107.3 . . ?
C80 C85 C84 112.7(14) . . ?
C80 C85 H85A 109.0 . . ?
C84 C85 H85A 109.0 . . ?
C80 C85 H85B 109.0 . . ?
C84 C85 H85B 109.0 . . ?
H85A C85 H85B 107.8 . . ?
C91 C86 C87 118.7(12) . . ?
C91 C86 C76 120.3(14) . . ?
C87 C86 C76 120.9(12) . . ?
C88 C87 N7 124.3(13) . . ?
C88 C87 C86 117.8(13) . . ?
N7 C87 C86 117.7(10) . . ?
C89 C88 C87 120.4(14) . . ?
C89 C88 H88 119.8 . . ?
C87 C88 H88 119.8 . . ?
C90 C89 C88 122.3(14) . . ?
C90 C89 H89 118.9 . . ?
C88 C89 H89 118.9 . . ?
C91 C90 C89 119.8(14) . . ?
C91 C90 C95 119.4(15) . . ?
C89 C90 C95 120.7(14) . . ?
C90 C91 C86 120.3(15) . . ?
C90 C91 C92 119.7(14) . . ?
C86 C91 C92 120.0(13) . . ?
C93 C92 C91 116.3(14) . . ?
C93 C92 H92A 108.2 . . ?
C91 C92 H92A 108.2 . . ?
C93 C92 H92B 108.2 . . ?
C91 C92 H92B 108.2 . . ?
H92A C92 H92B 107.4 . . ?
C94 C93 C92 118.6(18) . . ?
C94 C93 H93A 107.7 . . ?
C92 C93 H93A 107.7 . . ?
C94 C93 H93B 107.7 . . ?
C92 C93 H93B 107.7 . . ?
H93A C93 H93B 107.1 . . ?
C93 C94 C95 126(2) . . ?
C93 C94 H94A 105.8 . . ?
C95 C94 H94A 105.8 . . ?
C93 C94 H94B 105.8 . . ?
C95 C94 H94B 105.8 . . ?
H94A C94 H94B 106.2 . . ?
C94 C95 C90 114.6(15) . . ?
C94 C95 H95A 108.6 . . ?
C90 C95 H95A 108.6 . . ?
C94 C95 H95B 108.6 . . ?
C90 C95 H95B 108.6 . . ?
H95A C95 H95B 107.6 . . ?
N7 C96 C97 118.9(12) . . ?
N7 C96 H96 120.5 . . ?
C97 C96 H96 120.5 . . ?
N8 C97 C98 110.8(13) . . ?
N8 C97 C96 120.6(13) . . ?
C98 C97 C96 128.4(14) . . ?
C97 C98 C99 105.7(15) . . ?
C97 C98 H98 127.2 . . ?
C99 C98 H98 127.2 . . ?
C100 C99 C98 106.4(15) . . ?
C100 C99 H99 126.8 . . ?
C98 C99 H99 126.8 . . ?
N8 C100 C99 110.2(17) . . ?
N8 C100 H100 124.9 . . ?
C99 C100 H100 124.9 . . ?
Si1 C101 H10C 109.5 . . ?
Si1 C101 H10D 109.5 . . ?
H10C C101 H10D 109.5 . . ?
Si1 C101 H10E 109.5 . . ?
H10C C101 H10E 109.5 . . ?
H10D C101 H10E 109.5 . . ?
Si1 C102 H10F 109.5 . . ?
Si1 C102 H10G 109.5 . . ?
H10F C102 H10G 109.5 . . ?
Si1 C102 H10H 109.5 . . ?
H10F C102 H10H 109.5 . . ?
H10G C102 H10H 109.5 . . ?
Si1 C103 H10I 109.5 . . ?
Si1 C103 H10J 109.5 . . ?
H10I C103 H10J 109.5 . . ?
Si1 C103 H10K 109.5 . . ?
H10I C103 H10K 109.5 . . ?
H10J C103 H10K 109.5 . . ?
Si2 C104 H10L 109.5 . . ?
Si2 C104 H10M 109.5 . . ?
H10L C104 H10M 109.5 . . ?
Si2 C104 H10N 109.5 . . ?
H10L C104 H10N 109.5 . . ?
H10M C104 H10N 109.5 . . ?
Si2 C105 H10O 109.5 . . ?
Si2 C105 H10P 109.5 . . ?
H10O C105 H10P 109.5 . . ?
Si2 C105 H10Q 109.5 . . ?
H10O C105 H10Q 109.5 . . ?
H10P C105 H10Q 109.5 . . ?
Si2 C106 H10R 109.5 . . ?
Si2 C106 H10S 109.5 . . ?
H10R C106 H10S 109.5 . . ?
Si2 C106 H10T 109.5 . . ?
H10R C106 H10T 109.5 . . ?
H10S C106 H10T 109.5 . . ?
C108 C107 C112 117.5(11) . . ?
C108 C107 C117 122.9(11) . . ?
C112 C107 C117 119.5(11) . . ?
C109 C108 O5 117.3(12) . . ?
C109 C108 C107 121.5(12) . . ?
O5 C108 C107 120.8(11) . . ?
C109 C108 Y4 98.6(8) . . ?
O5 C108 Y4 62.2(6) . . ?
C107 C108 Y4 102.0(8) . . ?
C108 C109 C110 120.9(13) . . ?
C108 C109 H109 119.5 . . ?
C110 C109 H109 119.5 . . ?
C109 C110 C111 120.4(12) . . ?
C109 C110 H110 119.8 . . ?
C111 C110 H110 119.8 . . ?
C110 C111 C112 119.2(11) . . ?
C110 C111 C116 117.3(12) . . ?
C112 C111 C116 123.5(12) . . ?
C111 C112 C107 120.0(11) . . ?
C111 C112 C113 121.2(11) . . ?
C107 C112 C113 118.7(11) . . ?
C112 C113 C114 112.2(11) . . ?
C112 C113 H11A 109.2 . . ?
C114 C113 H11A 109.2 . . ?
C112 C113 H11B 109.2 . . ?
C114 C113 H11B 109.2 . . ?
H11A C113 H11B 107.9 . . ?
C115 C114 C113 109.8(13) . . ?
C115 C114 H11C 109.7 . . ?
C113 C114 H11C 109.7 . . ?
C115 C114 H11D 109.7 . . ?
C113 C114 H11D 109.7 . . ?
H11C C114 H11D 108.2 . . ?
C114 C115 C116 112.1(12) . . ?
C114 C115 H11E 109.2 . . ?
C116 C115 H11E 109.2 . . ?
C114 C115 H11F 109.2 . . ?
C116 C115 H11F 109.2 . . ?
H11E C115 H11F 107.9 . . ?
C111 C116 C115 110.9(12) . . ?
C111 C116 H11G 109.5 . . ?
C115 C116 H11G 109.5 . . ?
C111 C116 H11H 109.5 . . ?
C115 C116 H11H 109.5 . . ?
H11G C116 H11H 108.1 . . ?
C122 C117 C118 119.7(12) . . ?
C122 C117 C107 120.6(13) . . ?
C118 C117 C107 119.7(11) . . ?
C119 C118 N10 120.4(12) . . ?
C119 C118 C117 119.7(12) . . ?
N10 C118 C117 119.5(11) . . ?
C118 C119 C120 117.8(13) . . ?
C118 C119 H119 121.1 . . ?
C120 C119 H119 121.1 . . ?
C121 C120 C119 121.6(14) . . ?
C121 C120 H120 119.2 . . ?
C119 C120 H120 119.2 . . ?
C120 C121 C122 120.2(14) . . ?
C120 C121 C126 118.5(14) . . ?
C122 C121 C126 121.2(13) . . ?
C117 C122 C121 120.1(12) . . ?
C117 C122 C123 122.2(12) . . ?
C121 C122 C123 117.7(11) . . ?
C124 C123 C122 117.1(14) . . ?
C124 C123 H12A 108.0 . . ?
C122 C123 H12A 108.0 . . ?
C124 C123 H12B 108.0 . . ?
C122 C123 H12B 108.0 . . ?
H12A C123 H12B 107.3 . . ?
C123 C124 C125 114(2) . . ?
C123 C124 H12C 108.7 . . ?
C125 C124 H12C 108.7 . . ?
C123 C124 H12D 108.7 . . ?
C125 C124 H12D 108.7 . . ?
H12C C124 H12D 107.6 . . ?
C126 C125 C124 110.4(19) . . ?
C126 C125 H12E 109.6 . . ?
C124 C125 H12E 109.6 . . ?
C126 C125 H12F 109.6 . . ?
C124 C125 H12F 109.6 . . ?
H12E C125 H12F 108.1 . . ?
C125 C126 C121 115.2(16) . . ?
C125 C126 H12G 108.5 . . ?
C121 C126 H12G 108.5 . . ?
C125 C126 H12H 108.5 . . ?
C121 C126 H12H 108.5 . . ?
H12G C126 H12H 107.5 . . ?
N10 C127 C128 123.3(13) . . ?
N10 C127 H127 118.4 . . ?
C128 C127 H127 118.4 . . ?
N11 C128 C127 121.0(13) . . ?
N11 C128 C129 111.0(13) . . ?
C127 C128 C129 128.0(15) . . ?
C130 C129 C128 103.8(15) . . ?
C130 C129 H129 128.1 . . ?
C128 C129 H129 128.1 . . ?
C129 C130 C131 107.6(14) . . ?
C129 C130 H130 126.2 . . ?
C131 C130 H130 126.2 . . ?
N11 C131 C130 113.6(16) . . ?
N11 C131 H131 123.2 . . ?
C130 C131 H131 123.2 . . ?
C137 C132 C133 118.0(12) . . ?
C137 C132 C142 123.8(12) . . ?
C133 C132 C142 118.2(11) . . ?
O6 C133 C132 121.6(11) . . ?
O6 C133 C134 119.0(11) . . ?
C132 C133 C134 119.4(12) . . ?
O6 C133 Y4 48.4(5) . . ?
C132 C133 Y4 104.7(7) . . ?
C134 C133 Y4 113.6(8) . . ?
C135 C134 C133 118.3(13) . . ?
C135 C134 H134 120.8 . . ?
C133 C134 H134 120.8 . . ?
C136 C135 C134 122.2(13) . . ?
C136 C135 H135 118.9 . . ?
C134 C135 H135 118.9 . . ?
C135 C136 C137 120.2(14) . . ?
C135 C136 C141 119.1(13) . . ?
C137 C136 C141 120.4(15) . . ?
C136 C137 C132 120.6(13) . . ?
C136 C137 C138 121.5(13) . . ?
C132 C137 C138 117.3(12) . . ?
C137 C138 C139 111.5(13) . . ?
C137 C138 H13A 109.3 . . ?
C139 C138 H13A 109.3 . . ?
C137 C138 H13B 109.3 . . ?
C139 C138 H13B 109.3 . . ?
H13A C138 H13B 108.0 . . ?
C140 C139 C138 110.6(14) . . ?
C140 C139 H13C 109.5 . . ?
C138 C139 H13C 109.5 . . ?
C140 C139 H13D 109.5 . . ?
C138 C139 H13D 109.5 . . ?
H13C C139 H13D 108.1 . . ?
C139 C140 C141 111.9(16) . . ?
C139 C140 H14A 109.2 . . ?
C141 C140 H14A 109.2 . . ?
C139 C140 H14B 109.2 . . ?
C141 C140 H14B 109.2 . . ?
H14A C140 H14B 107.9 . . ?
C140 C141 C136 115.4(15) . . ?
C140 C141 H14C 108.4 . . ?
C136 C141 H14C 108.4 . . ?
C140 C141 H14D 108.4 . . ?
C136 C141 H14D 108.4 . . ?
H14C C141 H14D 107.5 . . ?
C143 C142 C147 117.3(11) . . ?
C143 C142 C132 127.1(11) . . ?
C147 C142 C132 115.6(11) . . ?
C142 C143 C144 121.7(12) . . ?
C142 C143 N12 119.7(11) . . ?
C144 C143 N12 118.6(12) . . ?
C145 C144 C143 118.7(13) . . ?
C145 C144 H144 120.7 . . ?
C143 C144 H144 120.7 . . ?
C146 C145 C144 122.7(13) . . ?
C146 C145 H145 118.6 . . ?
C144 C145 H145 118.6 . . ?
C145 C146 C147 118.3(13) . . ?
C145 C146 C151 124.6(14) . . ?
C147 C146 C151 116.7(13) . . ?
C146 C147 C142 121.1(11) . . ?
C146 C147 C148 115.8(12) . . ?
C142 C147 C148 123.0(12) . . ?
C147 C148 C149 109.6(11) . . ?
C147 C148 H14E 109.7 . . ?
C149 C148 H14E 109.7 . . ?
C147 C148 H14F 109.7 . . ?
C149 C148 H14F 109.7 . . ?
H14E C148 H14F 108.2 . . ?
C150 C149 C148 112.6(13) . . ?
C150 C149 H14G 109.1 . . ?
C148 C149 H14G 109.1 . . ?
C150 C149 H14H 109.1 . . ?
C148 C149 H14H 109.1 . . ?
H14G C149 H14H 107.8 . . ?
C151 C150 C149 116.9(14) . . ?
C151 C150 H15A 108.1 . . ?
C149 C150 H15A 108.1 . . ?
C151 C150 H15B 108.1 . . ?
C149 C150 H15B 108.1 . . ?
H15A C150 H15B 107.3 . . ?
C150 C151 C146 111.6(14) . . ?
C150 C151 H15C 109.3 . . ?
C146 C151 H15C 109.3 . . ?
C150 C151 H15D 109.3 . . ?
C146 C151 H15D 109.3 . . ?
H15C C151 H15D 108.0 . . ?
N12 C152 C153 123.5(13) . . ?
N12 C152 H152 118.3 . . ?
C153 C152 H152 118.3 . . ?
C152 C153 N13 117.6(11) . . ?
C152 C153 C154 131.8(13) . . ?
N13 C153 C154 110.3(12) . . ?
C155 C154 C153 106.2(13) . . ?
C155 C154 H154 126.9 . . ?
C153 C154 H154 126.9 . . ?
C154 C155 C156 106.6(13) . . ?
C154 C155 H155 126.7 . . ?
C156 C155 H155 126.7 . . ?
N13 C156 C155 111.5(14) . . ?
N13 C156 H156 124.3 . . ?
C155 C156 H156 124.3 . . ?
C158 C157 C162 120.5(14) . . ?
C158 C157 C167 121.6(13) . . ?
C162 C157 C167 117.8(13) . . ?
C157 C158 O7 122.9(13) . . ?
C157 C158 C159 120.6(14) . . ?
O7 C158 C159 116.3(13) . . ?
C157 C158 Y5 104.5(10) . . ?
O7 C158 Y5 61.5(6) . . ?
C159 C158 Y5 97.9(9) . . ?
C160 C159 C158 117.0(14) . . ?
C160 C159 H159 121.5 . . ?
C158 C159 H159 121.5 . . ?
C161 C160 C159 124.2(14) . . ?
C161 C160 H160 117.9 . . ?
C159 C160 H160 117.9 . . ?
C160 C161 C162 118.7(14) . . ?
C160 C161 C166 121.0(13) . . ?
C162 C161 C166 120.0(14) . . ?
C161 C162 C157 118.6(14) . . ?
C161 C162 C163 121.9(14) . . ?
C157 C162 C163 119.3(13) . . ?
C164 C163 C162 110.1(14) . . ?
C164 C163 H16A 109.6 . . ?
C162 C163 H16A 109.6 . . ?
C164 C163 H16B 109.6 . . ?
C162 C163 H16B 109.6 . . ?
H16A C163 H16B 108.1 . . ?
C165 C164 C163 120.8(16) . . ?
C165 C164 H16C 107.1 . . ?
C163 C164 H16C 107.1 . . ?
C165 C164 H16D 107.1 . . ?
C163 C164 H16D 107.1 . . ?
H16C C164 H16D 106.8 . . ?
C164 C165 C166 115(2) . . ?
C164 C165 H16E 108.6 . . ?
C166 C165 H16E 108.6 . . ?
C164 C165 H16F 108.6 . . ?
C166 C165 H16F 108.6 . . ?
H16E C165 H16F 107.5 . . ?
C165 C166 C161 115.4(14) . . ?
C165 C166 H16G 108.4 . . ?
C161 C166 H16G 108.4 . . ?
C165 C166 H16H 108.4 . . ?
C161 C166 H16H 108.4 . . ?
H16G C166 H16H 107.5 . . ?
C172 C167 C168 119.3(14) . . ?
C172 C167 C157 120.6(14) . . ?
C168 C167 C157 120.1(14) . . ?
C167 C168 C169 120.1(13) . . ?
C167 C168 N14 119.8(12) . . ?
C169 C168 N14 120.0(12) . . ?
C170 C169 C168 118.1(15) . . ?
C170 C169 H169 121.0 . . ?
C168 C169 H169 121.0 . . ?
C169 C170 C171 124.0(15) . . ?
C169 C170 H170 118.0 . . ?
C171 C170 H170 118.0 . . ?
C172 C171 C170 116.3(14) . . ?
C172 C171 C176 121.5(15) . . ?
C170 C171 C176 122.1(14) . . ?
C171 C172 C167 121.9(14) . . ?
C171 C172 C173 117.3(15) . . ?
C167 C172 C173 120.8(15) . . ?
C174 C173 C172 118.5(17) . . ?
C174 C173 H17C 107.7 . . ?
C172 C173 H17C 107.7 . . ?
C174 C173 H17D 107.7 . . ?
C172 C173 H17D 107.7 . . ?
H17C C173 H17D 107.1 . . ?
C173 C174 C175 120.6(19) . . ?
C173 C174 H17E 107.2 . . ?
C175 C174 H17E 107.2 . . ?
C173 C174 H17F 107.2 . . ?
C175 C174 H17F 107.2 . . ?
H17E C174 H17F 106.8 . . ?
C174 C175 C176 115.4(17) . . ?
C174 C175 H17G 108.4 . . ?
C176 C175 H17G 108.4 . . ?
C174 C175 H17H 108.4 . . ?
C176 C175 H17H 108.4 . . ?
H17G C175 H17H 107.5 . . ?
C175 C176 C171 114.7(14) . . ?
C175 C176 H17I 108.6 . . ?
C171 C176 H17I 108.6 . . ?
C175 C176 H17J 108.6 . . ?
C171 C176 H17J 108.6 . . ?
H17I C176 H17J 107.6 . . ?
N14 C177 C178 123.8(12) . . ?
N14 C177 H177 118.1 . . ?
C178 C177 H177 118.1 . . ?
C177 C178 N15 118.9(13) . . ?
C177 C178 C179 132.5(15) . . ?
N15 C178 C179 108.3(16) . . ?
C180 C179 C178 107.2(16) . . ?
C180 C179 H179 126.4 . . ?
C178 C179 H179 126.4 . . ?
C179 C180 C181 106.8(16) . . ?
C179 C180 H180 126.6 . . ?
C181 C180 H180 126.6 . . ?
N15 C181 C180 111.3(14) . . ?
N15 C181 H181 124.4 . . ?
C180 C181 H181 124.4 . . ?
C183 C182 C187 122.2(12) . . ?
C183 C182 C192 118.0(12) . . ?
C187 C182 C192 119.3(12) . . ?
C182 C183 O8 123.7(12) . . ?
C182 C183 C184 118.9(13) . . ?
O8 C183 C184 117.1(12) . . ?
C182 C183 Y5 103.7(8) . . ?
O8 C183 Y5 47.1(6) . . ?
C184 C183 Y5 113.1(9) . . ?
C185 C184 C183 119.5(12) . . ?
C185 C184 H184 120.2 . . ?
C183 C184 H184 120.2 . . ?
C184 C185 C186 120.6(12) . . ?
C184 C185 H185 119.7 . . ?
C186 C185 H185 119.7 . . ?
C185 C186 C187 119.6(13) . . ?
C185 C186 C191 119.5(13) . . ?
C187 C186 C191 120.9(13) . . ?
C186 C187 C182 118.8(13) . . ?
C186 C187 C188 121.3(13) . . ?
C182 C187 C188 119.9(13) . . ?
C187 C188 C189 112.4(13) . . ?
C187 C188 H18C 109.1 . . ?
C189 C188 H18C 109.1 . . ?
C187 C188 H18D 109.1 . . ?
C189 C188 H18D 109.1 . . ?
H18C C188 H18D 107.9 . . ?
C190 C189 C188 119.7(16) . . ?
C190 C189 H18E 107.4 . . ?
C188 C189 H18E 107.4 . . ?
C190 C189 H18F 107.4 . . ?
C188 C189 H18F 107.4 . . ?
H18E C189 H18F 106.9 . . ?
C189 C190 C191 117(2) . . ?
C189 C190 H19C 108.2 . . ?
C191 C190 H19C 108.2 . . ?
C189 C190 H19D 108.2 . . ?
C191 C190 H19D 108.2 . . ?
H19C C190 H19D 107.3 . . ?
C190 C191 C186 114.6(13) . . ?
C190 C191 H19E 108.6 . . ?
C186 C191 H19E 108.6 . . ?
C190 C191 H19F 108.6 . . ?
C186 C191 H19F 108.6 . . ?
H19E C191 H19F 107.6 . . ?
C197 C192 C193 120.9(12) . . ?
C197 C192 C182 118.5(12) . . ?
C193 C192 C182 120.5(12) . . ?
N16 C193 C192 123.1(13) . . ?
N16 C193 C194 121.4(13) . . ?
C192 C193 C194 115.5(13) . . ?
C195 C194 C193 122.1(14) . . ?
C195 C194 H194 119.0 . . ?
C193 C194 H194 119.0 . . ?
C194 C195 C196 121.3(12) . . ?
C194 C195 H195 119.3 . . ?
C196 C195 H195 119.3 . . ?
C197 C196 C195 119.0(13) . . ?
C197 C196 C201 119.6(13) . . ?
C195 C196 C201 121.2(13) . . ?
C196 C197 C192 121.0(12) . . ?
C196 C197 C198 118.3(13) . . ?
C192 C197 C198 120.7(13) . . ?
C199 C198 C197 114.6(13) . . ?
C199 C198 H19G 108.6 . . ?
C197 C198 H19G 108.6 . . ?
C199 C198 H19H 108.6 . . ?
C197 C198 H19H 108.6 . . ?
H19G C198 H19H 107.6 . . ?
C198 C199 C200 119.7(17) . . ?
C198 C199 H19I 107.4 . . ?
C200 C199 H19I 107.4 . . ?
C198 C199 H19J 107.4 . . ?
C200 C199 H19J 107.4 . . ?
H19I C199 H19J 106.9 . . ?
C199 C200 C201 109.5(17) . . ?
C199 C200 H20C 109.8 . . ?
C201 C200 H20C 109.8 . . ?
C199 C200 H20D 109.8 . . ?
C201 C200 H20D 109.8 . . ?
H20C C200 H20D 108.2 . . ?
C196 C201 C200 108.3(14) . . ?
C196 C201 H20E 110.0 . . ?
C200 C201 H20E 110.0 . . ?
C196 C201 H20F 110.0 . . ?
C200 C201 H20F 110.0 . . ?
H20E C201 H20F 108.4 . . ?
N16 C202 C203 123.2(13) . . ?
N16 C202 H202 118.4 . . ?
C203 C202 H202 118.4 . . ?
C204 C203 C202 130.3(13) . . ?
C204 C203 N17 112.4(12) . . ?
C202 C203 N17 117.4(12) . . ?
C203 C204 C205 105.9(12) . . ?
C203 C204 H204 127.0 . . ?
C205 C204 H204 127.0 . . ?
C206 C205 C204 106.2(13) . . ?
C206 C205 H205 126.9 . . ?
C204 C205 H205 126.9 . . ?
N17 C206 C205 112.6(14) . . ?
N17 C206 H206 123.7 . . ?
C205 C206 H206 123.7 . . ?
Si3 C207 H20G 109.5 . . ?
Si3 C207 H20H 109.5 . . ?
H20G C207 H20H 109.5 . . ?
Si3 C207 H20I 109.5 . . ?
H20G C207 H20I 109.5 . . ?
H20H C207 H20I 109.5 . . ?
Si3 C208 H20J 109.5 . . ?
Si3 C208 H20K 109.5 . . ?
H20J C208 H20K 109.5 . . ?
Si3 C208 H20L 109.5 . . ?
H20J C208 H20L 109.5 . . ?
H20K C208 H20L 109.5 . . ?
Si3 C209 H20M 109.5 . . ?
Si3 C209 H20N 109.5 . . ?
H20M C209 H20N 109.5 . . ?
Si3 C209 H20O 109.5 . . ?
H20M C209 H20O 109.5 . . ?
H20N C209 H20O 109.5 . . ?
Si4 C210 H21A 109.5 . . ?
Si4 C210 H21B 109.5 . . ?
H21A C210 H21B 109.5 . . ?
Si4 C210 H21C 109.5 . . ?
H21A C210 H21C 109.5 . . ?
H21B C210 H21C 109.5 . . ?
Si4 C211 H21D 109.5 . . ?
Si4 C211 H21E 109.5 . . ?
H21D C211 H21E 109.5 . . ?
Si4 C211 H21F 109.5 . . ?
H21D C211 H21F 109.5 . . ?
H21E C211 H21F 109.5 . . ?
Si4 C212 H21G 109.5 . . ?
Si4 C212 H21H 109.5 . . ?
H21G C212 H21H 109.5 . . ?
Si4 C212 H21I 109.5 . . ?
H21G C212 H21I 109.5 . . ?
H21H C212 H21I 109.5 . . ?
C214 C213 H21J 109.5 . . ?
C214 C213 H21K 109.5 . . ?
H21J C213 H21K 109.5 . . ?
C214 C213 H21L 109.5 . . ?
H21J C213 H21L 109.5 . . ?
H21K C213 H21L 109.5 . . ?
C215 C214 C219 120.0 . . ?
C215 C214 C213 119.9(4) . . ?
C219 C214 C213 120.1(4) . . ?
C214 C215 C216 120.0 . . ?
C214 C215 H215 120.0 . . ?
C216 C215 H215 120.0 . . ?
C217 C216 C215 120.0 . . ?
C217 C216 H216 120.0 . . ?
C215 C216 H216 120.0 . . ?
C216 C217 C218 120.0 . . ?
C216 C217 H217 120.0 . . ?
C218 C217 H217 120.0 . . ?
C219 C218 C217 120.0 . . ?
C219 C218 H218 120.0 . . ?
C217 C218 H218 120.0 . . ?
C218 C219 C214 120.0 . . ?
C218 C219 H219 120.0 . . ?
C214 C219 H219 120.0 . . ?
C221 C220 H22A 109.5 . . ?
C221 C220 H22B 109.5 . . ?
H22A C220 H22B 109.5 . . ?
C221 C220 H22C 109.5 . . ?
H22A C220 H22C 109.5 . . ?
H22B C220 H22C 109.5 . . ?
C222 C221 C226 120.0 . . ?
C222 C221 C220 122.0(16) . . ?
C226 C221 C220 118.0(16) . . ?
C223 C222 C221 120.0 . . ?
C223 C222 H222 120.0 . . ?
C221 C222 H222 120.0 . . ?
C222 C223 C224 120.0 . . ?
C222 C223 H223 120.0 . . ?
C224 C223 H223 120.0 . . ?
C223 C224 C225 120.0 . . ?
C223 C224 H224 120.0 . . ?
C225 C224 H224 120.0 . . ?
C226 C225 C224 120.0 . . ?
C226 C225 H225 120.0 . . ?
C224 C225 H225 120.0 . . ?
C225 C226 C221 120.0 . . ?
C225 C226 H226 120.0 . . ?
C221 C226 H226 120.0 . . ?
C228 C227 H22D 109.5 . . ?
C228 C227 H22E 109.5 . . ?
H22D C227 H22E 109.5 . . ?
C228 C227 H22F 109.5 . . ?
H22D C227 H22F 109.5 . . ?
H22E C227 H22F 109.5 . . ?
C229 C228 C233 120.0 . . ?
C229 C228 C227 112.9(17) . . ?
C233 C228 C227 127.0(17) . . ?
C230 C229 C228 120.0 . . ?
C230 C229 H229 120.0 . . ?
C228 C229 H229 120.0 . . ?
C229 C230 C231 120.0 . . ?
C229 C230 H230 120.0 . . ?
C231 C230 H230 120.0 . . ?
C232 C231 C230 120.0 . . ?
C232 C231 H231 120.0 . . ?
C230 C231 H231 120.0 . . ?
C233 C232 C231 120.0 . . ?
C233 C232 H232 120.0 . . ?
C231 C232 H232 120.0 . . ?
C232 C233 C228 120.0 . . ?
C232 C233 H233 120.0 . . ?
C228 C233 H233 120.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y1 O2 2.344(9) . ?
Y1 N2 2.348(11) . ?
Y1 O1 2.357(8) . ?
Y1 N4 2.391(13) . ?
Y1 N3 2.447(11) . ?
Y1 N1 2.460(12) . ?
Y1 C2 2.629(13) . ?
Y1 C27 3.022(13) . ?
Y1 Y3 3.7320(18) . ?
Y2 O3 2.334(9) . ?
Y2 O4 2.348(9) . ?
Y2 N8 2.355(14) . ?
Y2 N6 2.388(11) . ?
Y2 N5 2.449(11) . ?
Y2 N7 2.457(12) . ?
Y2 C77 2.644(16) . ?
Y2 C52 3.007(15) . ?
Y2 Y3 3.6927(19) . ?
Y3 O1 2.197(9) . ?
Y3 N9 2.231(10) . ?
Y3 O4 2.244(8) . ?
Y3 O3 2.249(9) . ?
Y3 O2 2.265(8) . ?
Y3 Si2 3.365(4) . ?
Y3 Si1 3.401(4) . ?
Y4 O6 2.329(9) . ?
Y4 O5 2.343(8) . ?
Y4 N11 2.353(11) . ?
Y4 N13 2.390(11) . ?
Y4 N12 2.421(11) . ?
Y4 N10 2.447(12) . ?
Y4 C108 2.641(13) . ?
Y4 C133 3.010(11) . ?
Y4 Y6 3.7191(17) . ?
Y5 O7 2.326(9) . ?
Y5 O8 2.334(8) . ?
Y5 N15 2.334(13) . ?
Y5 N17 2.372(12) . ?
Y5 N14 2.459(10) . ?
Y5 N16 2.460(12) . ?
Y5 C158 2.641(14) . ?
Y5 C183 3.046(15) . ?
Y5 Y6 3.6953(17) . ?
Y6 N18 2.210(10) . ?
Y6 O5 2.243(7) . ?
Y6 O7 2.254(7) . ?
Y6 O6 2.260(8) . ?
Y6 O8 2.264(8) . ?
Y6 Si4 3.362(4) . ?
Y6 Si3 3.412(4) . ?
Si1 N9 1.715(11) . ?
Si1 C102 1.858(17) . ?
Si1 C103 1.912(17) . ?
Si1 C101 1.922(16) . ?
Si2 N9 1.731(12) . ?
Si2 C105 1.868(16) . ?
Si2 C104 1.881(14) . ?
Si2 C106 1.903(17) . ?
Si3 N18 1.725(11) . ?
Si3 C207 1.868(14) . ?
Si3 C208 1.886(15) . ?
Si3 C209 1.894(16) . ?
Si4 N18 1.763(12) . ?
Si4 C212 1.894(14) . ?
Si4 C211 1.888(16) . ?
Si4 C210 1.919(19) . ?
N1 C21 1.330(17) . ?
N1 C12 1.425(16) . ?
N2 C25 1.361(17) . ?
N2 C22 1.389(17) . ?
N3 C46 1.298(18) . ?
N3 C37 1.428(19) . ?
N4 C50 1.33(2) . ?
N4 C47 1.434(17) . ?
N5 C71 1.312(18) . ?
N5 C62 1.415(17) . ?
N6 C75 1.315(18) . ?
N6 C72 1.414(17) . ?
N7 C96 1.366(18) . ?
N7 C87 1.411(17) . ?
N8 C100 1.37(2) . ?
N8 C97 1.405(18) . ?
N10 C127 1.330(17) . ?
N10 C118 1.421(17) . ?
N11 C131 1.342(18) . ?
N11 C128 1.382(18) . ?
N12 C152 1.308(16) . ?
N12 C143 1.462(17) . ?
N13 C156 1.372(19) . ?
N13 C153 1.387(17) . ?
N14 C177 1.313(17) . ?
N14 C168 1.439(17) . ?
N15 C181 1.39(2) . ?
N15 C178 1.416(19) . ?
N16 C202 1.337(17) . ?
N16 C193 1.381(17) . ?
N17 C206 1.372(17) . ?
N17 C203 1.408(17) . ?
O1 C2 1.386(16) . ?
O2 C27 1.390(15) . ?
O3 C52 1.424(18) . ?
O4 C77 1.417(17) . ?
O5 C108 1.395(14) . ?
O6 C133 1.400(15) . ?
O7 C158 1.387(16) . ?
O8 C183 1.392(16) . ?
C1 C6 1.377(19) . ?
C1 C11 1.461(17) . ?
C1 C2 1.480(18) . ?
C2 C3 1.403(18) . ?
C3 C4 1.398(19) . ?
C3 H3 0.9500 . ?
C4 C5 1.364(19) . ?
C4 H4 0.9500 . ?
C5 C6 1.442(19) . ?
C5 C10 1.51(2) . ?
C6 C7 1.524(19) . ?
C7 C8 1.52(2) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C8 C9 1.52(2) . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C9 C10 1.56(2) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C10 H10A 0.9900 . ?
C10 H10B 0.9900 . ?
C11 C16 1.410(19) . ?
C11 C12 1.441(18) . ?
C12 C13 1.433(17) . ?
C13 C14 1.380(19) . ?
C13 H13 0.9500 . ?
C14 C15 1.39(2) . ?
C14 H14 0.9500 . ?
C15 C16 1.389(19) . ?
C15 C20 1.572(19) . ?
C16 C17 1.52(2) . ?
C17 C18 1.41(2) . ?
C17 H17A 0.9900 . ?
C17 H17B 0.9900 . ?
C18 C19 1.34(3) . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C19 C20 1.48(3) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C20 H20A 0.9900 . ?
C20 H20B 0.9900 . ?
C21 C22 1.416(19) . ?
C21 H21 0.9500 . ?
C22 C23 1.42(2) . ?
C23 C24 1.42(2) . ?
C23 H23 0.9500 . ?
C24 C25 1.40(2) . ?
C24 H24 0.9500 . ?
C25 H25 0.9500 . ?
C26 C27 1.380(17) . ?
C26 C31 1.403(18) . ?
C26 C36 1.57(2) . ?
C27 C28 1.469(19) . ?
C28 C29 1.40(2) . ?
C28 H28 0.9500 . ?
C29 C30 1.37(3) . ?
C29 H29 0.9500 . ?
C30 C31 1.43(2) . ?
C30 C35 1.57(2) . ?
C31 C32 1.57(2) . ?
C32 C33 1.56(3) . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C33 C34 1.60(4) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 C35 1.57(3) . ?
C34 H34A 0.9900 . ?
C34 H34B 0.9900 . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 C41 1.39(2) . ?
C36 C37 1.40(2) . ?
C37 C38 1.368(19) . ?
C38 C39 1.43(2) . ?
C38 H38 0.9500 . ?
C39 C40 1.40(2) . ?
C39 H39 0.9500 . ?
C40 C41 1.42(2) . ?
C40 C45 1.51(2) . ?
C41 C42 1.54(2) . ?
C42 C43 1.51(3) . ?
C42 H42A 0.9900 . ?
C42 H42B 0.9900 . ?
C43 C44 1.42(3) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 C45 1.45(3) . ?
C44 H44A 0.9900 . ?
C44 H44B 0.9900 . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 C47 1.39(2) . ?
C46 H46 0.9500 . ?
C47 C48 1.43(2) . ?
C48 C49 1.43(2) . ?
C48 H48 0.9500 . ?
C49 C50 1.45(2) . ?
C49 H49 0.9500 . ?
C50 H50 0.9500 . ?
C51 C56 1.40(2) . ?
C51 C52 1.43(2) . ?
C51 C61 1.576(19) . ?
C52 C53 1.39(2) . ?
C53 C54 1.36(2) . ?
C53 H53 0.9500 . ?
C54 C55 1.46(3) . ?
C54 H54 0.9500 . ?
C55 C56 1.42(2) . ?
C55 C60 1.550(10) . ?
C56 C57 1.541(10) . ?
C57 C58 1.557(10) . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C58 C59 1.542(10) . ?
C58 H58A 0.9900 . ?
C58 H58B 0.9900 . ?
C59 C60 1.560(10) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C60 H60A 0.9900 . ?
C60 H60B 0.9900 . ?
C61 C62 1.36(2) . ?
C61 C66 1.42(2) . ?
C62 C63 1.403(19) . ?
C63 C64 1.38(2) . ?
C63 H63 0.9500 . ?
C64 C65 1.37(2) . ?
C64 H64 0.9500 . ?
C65 C66 1.44(2) . ?
C65 C70 1.51(2) . ?
C66 C67 1.52(2) . ?
C67 C68 1.55(2) . ?
C67 H67A 0.9900 . ?
C67 H67B 0.9900 . ?
C68 C69 1.52(3) . ?
C68 H68A 0.9900 . ?
C68 H68B 0.9900 . ?
C69 C70 1.48(2) . ?
C69 H69A 0.9900 . ?
C69 H69B 0.9900 . ?
C70 H70A 0.9900 . ?
C70 H70B 0.9900 . ?
C71 C72 1.41(2) . ?
C71 H71 0.9500 . ?
C72 C73 1.377(19) . ?
C73 C74 1.43(2) . ?
C73 H73 0.9500 . ?
C74 C75 1.40(2) . ?
C74 H74 0.9500 . ?
C75 H75 0.9500 . ?
C76 C77 1.36(2) . ?
C76 C81 1.45(2) . ?
C76 C86 1.522(19) . ?
C77 C78 1.386(19) . ?
C78 C79 1.40(2) . ?
C78 H78 0.9500 . ?
C79 C80 1.39(2) . ?
C79 H79 0.9500 . ?
C80 C81 1.41(2) . ?
C80 C85 1.50(2) . ?
C81 C82 1.50(2) . ?
C82 C83 1.52(2) . ?
C82 H82A 0.9900 . ?
C82 H82B 0.9900 . ?
C83 C84 1.45(3) . ?
C83 H83A 0.9900 . ?
C83 H83B 0.9900 . ?
C84 C85 1.51(3) . ?
C84 H84A 0.9900 . ?
C84 H84B 0.9900 . ?
C85 H85A 0.9900 . ?
C85 H85B 0.9900 . ?
C86 C91 1.42(2) . ?
C86 C87 1.46(2) . ?
C87 C88 1.385(17) . ?
C88 C89 1.38(2) . ?
C88 H88 0.9500 . ?
C89 C90 1.37(2) . ?
C89 H89 0.9500 . ?
C90 C91 1.37(2) . ?
C90 C95 1.56(2) . ?
C91 C92 1.57(2) . ?
C92 C93 1.48(2) . ?
C92 H92A 0.9900 . ?
C92 H92B 0.9900 . ?
C93 C94 1.35(3) . ?
C93 H93A 0.9900 . ?
C93 H93B 0.9900 . ?
C94 C95 1.41(3) . ?
C94 H94A 0.9900 . ?
C94 H94B 0.9900 . ?
C95 H95A 0.9900 . ?
C95 H95B 0.9900 . ?
C96 C97 1.44(2) . ?
C96 H96 0.9500 . ?
C97 C98 1.40(2) . ?
C98 C99 1.44(2) . ?
C98 H98 0.9500 . ?
C99 C100 1.43(3) . ?
C99 H99 0.9500 . ?
C100 H100 0.9500 . ?
C101 H10C 0.9800 . ?
C101 H10D 0.9800 . ?
C101 H10E 0.9800 . ?
C102 H10F 0.9800 . ?
C102 H10G 0.9800 . ?
C102 H10H 0.9800 . ?
C103 H10I 0.9800 . ?
C103 H10J 0.9800 . ?
C103 H10K 0.9800 . ?
C104 H10L 0.9800 . ?
C104 H10M 0.9800 . ?
C104 H10N 0.9800 . ?
C105 H10O 0.9800 . ?
C105 H10P 0.9800 . ?
C105 H10Q 0.9800 . ?
C106 H10R 0.9800 . ?
C106 H10S 0.9800 . ?
C106 H10T 0.9800 . ?
C107 C108 1.403(17) . ?
C107 C112 1.473(16) . ?
C107 C117 1.497(18) . ?
C108 C109 1.388(18) . ?
C109 C110 1.398(18) . ?
C109 H109 0.9500 . ?
C110 C111 1.415(19) . ?
C110 H110 0.9500 . ?
C111 C112 1.414(18) . ?
C111 C116 1.534(18) . ?
C112 C113 1.541(18) . ?
C113 C114 1.558(19) . ?
C113 H11A 0.9900 . ?
C113 H11B 0.9900 . ?
C114 C115 1.52(2) . ?
C114 H11C 0.9900 . ?
C114 H11D 0.9900 . ?
C115 C116 1.55(2) . ?
C115 H11E 0.9900 . ?
C115 H11F 0.9900 . ?
C116 H11G 0.9900 . ?
C116 H11H 0.9900 . ?
C117 C122 1.355(18) . ?
C117 C118 1.459(19) . ?
C118 C119 1.390(18) . ?
C119 C120 1.42(2) . ?
C119 H119 0.9500 . ?
C120 C121 1.37(2) . ?
C120 H120 0.9500 . ?
C121 C122 1.417(19) . ?
C121 C126 1.55(2) . ?
C122 C123 1.50(2) . ?
C123 C124 1.46(3) . ?
C123 H12A 0.9900 . ?
C123 H12B 0.9900 . ?
C124 C125 1.54(3) . ?
C124 H12C 0.9900 . ?
C124 H12D 0.9900 . ?
C125 C126 1.45(3) . ?
C125 H12E 0.9900 . ?
C125 H12F 0.9900 . ?
C126 H12G 0.9900 . ?
C126 H12H 0.9900 . ?
C127 C128 1.413(19) . ?
C127 H127 0.9500 . ?
C128 C129 1.47(2) . ?
C129 C130 1.37(3) . ?
C129 H129 0.9500 . ?
C130 C131 1.39(2) . ?
C130 H130 0.9500 . ?
C131 H131 0.9500 . ?
C132 C137 1.402(19) . ?
C132 C133 1.427(17) . ?
C132 C142 1.521(18) . ?
C133 C134 1.453(17) . ?
C134 C135 1.380(19) . ?
C134 H134 0.9500 . ?
C135 C136 1.37(2) . ?
C135 H135 0.9500 . ?
C136 C137 1.41(2) . ?
C136 C141 1.50(2) . ?
C137 C138 1.53(2) . ?
C138 C139 1.582(19) . ?
C138 H13A 0.9900 . ?
C138 H13B 0.9900 . ?
C139 C140 1.49(2) . ?
C139 H13C 0.9900 . ?
C139 H13D 0.9900 . ?
C140 C141 1.49(2) . ?
C140 H14A 0.9900 . ?
C140 H14B 0.9900 . ?
C141 H14C 0.9900 . ?
C141 H14D 0.9900 . ?
C142 C143 1.390(17) . ?
C142 C147 1.458(18) . ?
C143 C144 1.409(18) . ?
C144 C145 1.40(2) . ?
C144 H144 0.9500 . ?
C145 C146 1.375(19) . ?
C145 H145 0.9500 . ?
C146 C147 1.41(2) . ?
C146 C151 1.54(2) . ?
C147 C148 1.525(17) . ?
C148 C149 1.54(2) . ?
C148 H14E 0.9900 . ?
C148 H14F 0.9900 . ?
C149 C150 1.51(2) . ?
C149 H14G 0.9900 . ?
C149 H14H 0.9900 . ?
C150 C151 1.46(2) . ?
C150 H15A 0.9900 . ?
C150 H15B 0.9900 . ?
C151 H15C 0.9900 . ?
C151 H15D 0.9900 . ?
C152 C153 1.376(19) . ?
C152 H152 0.9500 . ?
C153 C154 1.417(18) . ?
C154 C155 1.40(2) . ?
C154 H154 0.9500 . ?
C155 C156 1.398(19) . ?
C155 H155 0.9500 . ?
C156 H156 0.9500 . ?
C157 C158 1.37(2) . ?
C157 C162 1.46(2) . ?
C157 C167 1.53(2) . ?
C158 C159 1.43(2) . ?
C159 C160 1.40(2) . ?
C159 H159 0.9500 . ?
C160 C161 1.37(2) . ?
C160 H160 0.9500 . ?
C161 C162 1.40(2) . ?
C161 C166 1.55(2) . ?
C162 C163 1.56(2) . ?
C163 C164 1.51(2) . ?
C163 H16A 0.9900 . ?
C163 H16B 0.9900 . ?
C164 C165 1.39(3) . ?
C164 H16C 0.9900 . ?
C164 H16D 0.9900 . ?
C165 C166 1.48(3) . ?
C165 H16E 0.9900 . ?
C165 H16F 0.9900 . ?
C166 H16G 0.9900 . ?
C166 H16H 0.9900 . ?
C167 C172 1.41(2) . ?
C167 C168 1.41(2) . ?
C168 C169 1.421(18) . ?
C169 C170 1.35(2) . ?
C169 H169 0.9500 . ?
C170 C171 1.45(2) . ?
C170 H170 0.9500 . ?
C171 C172 1.37(2) . ?
C171 C176 1.50(2) . ?
C172 C173 1.59(2) . ?
C173 C174 1.39(3) . ?
C173 H17C 0.9900 . ?
C173 H17D 0.9900 . ?
C174 C175 1.48(3) . ?
C174 H17E 0.9900 . ?
C174 H17F 0.9900 . ?
C175 C176 1.48(3) . ?
C175 H17G 0.9900 . ?
C175 H17H 0.9900 . ?
C176 H17I 0.9900 . ?
C176 H17J 0.9900 . ?
C177 C178 1.40(2) . ?
C177 H177 0.9500 . ?
C178 C179 1.46(2) . ?
C179 C180 1.40(3) . ?
C179 H179 0.9500 . ?
C180 C181 1.42(2) . ?
C180 H180 0.9500 . ?
C181 H181 0.9500 . ?
C182 C183 1.372(19) . ?
C182 C187 1.414(19) . ?
C182 C192 1.569(18) . ?
C183 C184 1.431(18) . ?
C184 C185 1.409(19) . ?
C184 H184 0.9500 . ?
C185 C186 1.41(2) . ?
C185 H185 0.9500 . ?
C186 C187 1.41(2) . ?
C186 C191 1.54(2) . ?
C187 C188 1.52(2) . ?
C188 C189 1.54(2) . ?
C188 H18C 0.9900 . ?
C188 H18D 0.9900 . ?
C189 C190 1.39(3) . ?
C189 H18E 0.9900 . ?
C189 H18F 0.9900 . ?
C190 C191 1.46(2) . ?
C190 H19C 0.9900 . ?
C190 H19D 0.9900 . ?
C191 H19E 0.9900 . ?
C191 H19F 0.9900 . ?
C192 C197 1.43(2) . ?
C192 C193 1.441(19) . ?
C193 C194 1.442(19) . ?
C194 C195 1.381(19) . ?
C194 H194 0.9500 . ?
C195 C196 1.406(19) . ?
C195 H195 0.9500 . ?
C196 C197 1.38(2) . ?
C196 C201 1.47(2) . ?
C197 C198 1.518(18) . ?
C198 C199 1.42(2) . ?
C198 H19G 0.9900 . ?
C198 H19H 0.9900 . ?
C199 C200 1.52(3) . ?
C199 H19I 0.9900 . ?
C199 H19J 0.9900 . ?
C200 C201 1.56(3) . ?
C200 H20C 0.9900 . ?
C200 H20D 0.9900 . ?
C201 H20E 0.9900 . ?
C201 H20F 0.9900 . ?
C202 C203 1.40(2) . ?
C202 H202 0.9500 . ?
C203 C204 1.381(19) . ?
C204 C205 1.40(2) . ?
C204 H204 0.9500 . ?
C205 C206 1.39(2) . ?
C205 H205 0.9500 . ?
C206 H206 0.9500 . ?
C207 H20G 0.9800 . ?
C207 H20H 0.9800 . ?
C207 H20I 0.9800 . ?
C208 H20J 0.9800 . ?
C208 H20K 0.9800 . ?
C208 H20L 0.9800 . ?
C209 H20M 0.9800 . ?
C209 H20N 0.9800 . ?
C209 H20O 0.9800 . ?
C210 H21A 0.9800 . ?
C210 H21B 0.9800 . ?
C210 H21C 0.9800 . ?
C211 H21D 0.9800 . ?
C211 H21E 0.9800 . ?
C211 H21F 0.9800 . ?
C212 H21G 0.9800 . ?
C212 H21H 0.9800 . ?
C212 H21I 0.9800 . ?
C213 C214 1.481(10) . ?
C213 H21J 0.9800 . ?
C213 H21K 0.9800 . ?
C213 H21L 0.9800 . ?
C214 C215 1.3900 . ?
C214 C219 1.3900 . ?
C215 C216 1.3900 . ?
C215 H215 0.9500 . ?
C216 C217 1.3900 . ?
C216 H216 0.9500 . ?
C217 C218 1.3900 . ?
C217 H217 0.9500 . ?
C218 C219 1.3900 . ?
C218 H218 0.9500 . ?
C219 H219 0.9500 . ?
C220 C221 1.52(3) . ?
C220 H22A 0.9800 . ?
C220 H22B 0.9800 . ?
C220 H22C 0.9800 . ?
C221 C222 1.3900 . ?
C221 C226 1.3900 . ?
C222 C223 1.3900 . ?
C222 H222 0.9500 . ?
C223 C224 1.3900 . ?
C223 H223 0.9500 . ?
C224 C225 1.3900 . ?
C224 H224 0.9500 . ?
C225 C226 1.3900 . ?
C225 H225 0.9500 . ?
C226 H226 0.9500 . ?
C227 C228 1.58(3) . ?
C227 H22D 0.9800 . ?
C227 H22E 0.9800 . ?
C227 H22F 0.9800 . ?
C228 C229 1.3900 . ?
C228 C233 1.3900 . ?
C229 C230 1.3900 . ?
C229 H229 0.9500 . ?
C230 C231 1.3900 . ?
C230 H230 0.9500 . ?
C231 C232 1.3900 . ?
C231 H231 0.9500 . ?
C232 C233 1.3900 . ?
C232 H232 0.9500 . ?
C233 H233 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O3 Y2 Y3 O1 28.4(5) . . . . ?
O4 Y2 Y3 O1 -170.2(5) . . . . ?
N8 Y2 Y3 O1 -41.2(5) . . . . ?
N6 Y2 Y3 O1 158.8(8) . . . . ?
N5 Y2 Y3 O1 79.1(4) . . . . ?
N7 Y2 Y3 O1 -114.3(4) . . . . ?
C77 Y2 Y3 O1 171.9(5) . . . . ?
C52 Y2 Y3 O1 17.5(4) . . . . ?
O3 Y2 Y3 N9 -110.9(5) . . . . ?
O4 Y2 Y3 N9 50.6(5) . . . . ?
N8 Y2 Y3 N9 179.6(5) . . . . ?
N6 Y2 Y3 N9 19.6(8) . . . . ?
N5 Y2 Y3 N9 -60.1(4) . . . . ?
N7 Y2 Y3 N9 106.5(4) . . . . ?
C77 Y2 Y3 N9 32.7(5) . . . . ?
C52 Y2 Y3 N9 -121.7(5) . . . . ?
O3 Y2 Y3 O4 -161.5(5) . . . . ?
N8 Y2 Y3 O4 128.9(5) . . . . ?
N6 Y2 Y3 O4 -31.1(8) . . . . ?
N5 Y2 Y3 O4 -110.7(4) . . . . ?
N7 Y2 Y3 O4 55.8(5) . . . . ?
C77 Y2 Y3 O4 -17.9(5) . . . . ?
C52 Y2 Y3 O4 -172.4(5) . . . . ?
O4 Y2 Y3 O3 161.5(5) . . . . ?
N8 Y2 Y3 O3 -69.6(5) . . . . ?
N6 Y2 Y3 O3 130.4(8) . . . . ?
N5 Y2 Y3 O3 50.7(4) . . . . ?
N7 Y2 Y3 O3 -142.7(5) . . . . ?
C77 Y2 Y3 O3 143.6(5) . . . . ?
C52 Y2 Y3 O3 -10.9(5) . . . . ?
O3 Y2 Y3 O2 100.4(4) . . . . ?
O4 Y2 Y3 O2 -98.1(4) . . . . ?
N8 Y2 Y3 O2 30.8(4) . . . . ?
N6 Y2 Y3 O2 -129.2(7) . . . . ?
N5 Y2 Y3 O2 151.1(3) . . . . ?
N7 Y2 Y3 O2 -42.3(4) . . . . ?
C77 Y2 Y3 O2 -116.1(4) . . . . ?
C52 Y2 Y3 O2 89.5(4) . . . . ?
O3 Y2 Y3 Si2 -142.6(4) . . . . ?
O4 Y2 Y3 Si2 18.9(4) . . . . ?
N8 Y2 Y3 Si2 147.8(3) . . . . ?
N6 Y2 Y3 Si2 -12.2(7) . . . . ?
N5 Y2 Y3 Si2 -91.9(3) . . . . ?
N7 Y2 Y3 Si2 74.7(3) . . . . ?
C77 Y2 Y3 Si2 0.9(4) . . . . ?
C52 Y2 Y3 Si2 -153.5(3) . . . . ?
O3 Y2 Y3 Si1 -81.3(4) . . . . ?
O4 Y2 Y3 Si1 80.2(4) . . . . ?
N8 Y2 Y3 Si1 -150.9(3) . . . . ?
N6 Y2 Y3 Si1 49.1(7) . . . . ?
N5 Y2 Y3 Si1 -30.6(3) . . . . ?
N7 Y2 Y3 Si1 136.0(3) . . . . ?
C77 Y2 Y3 Si1 62.3(4) . . . . ?
C52 Y2 Y3 Si1 -92.2(3) . . . . ?
O3 Y2 Y3 Y1 66.7(4) . . . . ?
O4 Y2 Y3 Y1 -131.8(4) . . . . ?
N8 Y2 Y3 Y1 -2.9(3) . . . . ?
N6 Y2 Y3 Y1 -162.9(7) . . . . ?
N5 Y2 Y3 Y1 117.4(3) . . . . ?
N7 Y2 Y3 Y1 -76.0(3) . . . . ?
C77 Y2 Y3 Y1 -149.7(4) . . . . ?
C52 Y2 Y3 Y1 55.8(3) . . . . ?
O2 Y1 Y3 O1 -161.2(5) . . . . ?
N2 Y1 Y3 O1 129.3(5) . . . . ?
N4 Y1 Y3 O1 -29.5(8) . . . . ?
N3 Y1 Y3 O1 -107.8(4) . . . . ?
N1 Y1 Y3 O1 55.9(4) . . . . ?
C2 Y1 Y3 O1 -19.5(4) . . . . ?
C27 Y1 Y3 O1 -169.8(4) . . . . ?
O2 Y1 Y3 N9 -115.4(5) . . . . ?
N2 Y1 Y3 N9 175.1(5) . . . . ?
O1 Y1 Y3 N9 45.8(5) . . . . ?
N4 Y1 Y3 N9 16.3(8) . . . . ?
N3 Y1 Y3 N9 -61.9(4) . . . . ?
N1 Y1 Y3 N9 101.7(4) . . . . ?
C2 Y1 Y3 N9 26.3(5) . . . . ?
C27 Y1 Y3 N9 -124.0(4) . . . . ?
O2 Y1 Y3 O4 27.5(5) . . . . ?
N2 Y1 Y3 O4 -42.0(5) . . . . ?
O1 Y1 Y3 O4 -171.3(5) . . . . ?
N4 Y1 Y3 O4 159.2(8) . . . . ?
N3 Y1 Y3 O4 80.9(4) . . . . ?
N1 Y1 Y3 O4 -115.4(4) . . . . ?
C2 Y1 Y3 O4 169.2(4) . . . . ?
C27 Y1 Y3 O4 18.9(4) . . . . ?
O2 Y1 Y3 O3 101.1(4) . . . . ?
N2 Y1 Y3 O3 31.6(4) . . . . ?
O1 Y1 Y3 O3 -97.7(4) . . . . ?
N4 Y1 Y3 O3 -127.2(8) . . . . ?
N3 Y1 Y3 O3 154.5(4) . . . . ?
N1 Y1 Y3 O3 -41.8(3) . . . . ?
C2 Y1 Y3 O3 -117.2(4) . . . . ?
C27 Y1 Y3 O3 92.5(4) . . . . ?
N2 Y1 Y3 O2 -69.5(5) . . . . ?
O1 Y1 Y3 O2 161.2(5) . . . . ?
N4 Y1 Y3 O2 131.7(8) . . . . ?
N3 Y1 Y3 O2 53.5(4) . . . . ?
N1 Y1 Y3 O2 -142.9(4) . . . . ?
C2 Y1 Y3 O2 141.7(5) . . . . ?
C27 Y1 Y3 O2 -8.6(5) . . . . ?
O2 Y1 Y3 Si2 -83.2(4) . . . . ?
N2 Y1 Y3 Si2 -152.7(3) . . . . ?
O1 Y1 Y3 Si2 78.0(4) . . . . ?
N4 Y1 Y3 Si2 48.5(7) . . . . ?
N3 Y1 Y3 Si2 -29.8(3) . . . . ?
N1 Y1 Y3 Si2 133.9(3) . . . . ?
C2 Y1 Y3 Si2 58.5(3) . . . . ?
C27 Y1 Y3 Si2 -91.8(3) . . . . ?
O2 Y1 Y3 Si1 -146.2(4) . . . . ?
N2 Y1 Y3 Si1 144.3(3) . . . . ?
O1 Y1 Y3 Si1 15.0(4) . . . . ?
N4 Y1 Y3 Si1 -14.5(7) . . . . ?
N3 Y1 Y3 Si1 -92.7(3) . . . . ?
N1 Y1 Y3 Si1 70.9(3) . . . . ?
C2 Y1 Y3 Si1 -4.5(3) . . . . ?
C27 Y1 Y3 Si1 -154.8(3) . . . . ?
O2 Y1 Y3 Y2 67.1(4) . . . . ?
N2 Y1 Y3 Y2 -2.3(3) . . . . ?
O1 Y1 Y3 Y2 -131.7(3) . . . . ?
N4 Y1 Y3 Y2 -161.2(7) . . . . ?
N3 Y1 Y3 Y2 120.6(3) . . . . ?
N1 Y1 Y3 Y2 -75.8(2) . . . . ?
C2 Y1 Y3 Y2 -151.1(3) . . . . ?
C27 Y1 Y3 Y2 58.5(3) . . . . ?
O7 Y5 Y6 N18 50.1(5) . . . . ?
O8 Y5 Y6 N18 -115.2(5) . . . . ?
N15 Y5 Y6 N18 177.9(5) . . . . ?
N17 Y5 Y6 N18 14.8(7) . . . . ?
N14 Y5 Y6 N18 103.6(4) . . . . ?
N16 Y5 Y6 N18 -59.9(4) . . . . ?
C158 Y5 Y6 N18 31.5(5) . . . . ?
C183 Y5 Y6 N18 -123.7(4) . . . . ?
O7 Y5 Y6 O5 -169.7(4) . . . . ?
O8 Y5 Y6 O5 25.0(5) . . . . ?
N15 Y5 Y6 O5 -41.8(5) . . . . ?
N17 Y5 Y6 O5 155.1(7) . . . . ?
N14 Y5 Y6 O5 -116.1(4) . . . . ?
N16 Y5 Y6 O5 80.3(4) . . . . ?
C158 Y5 Y6 O5 171.8(5) . . . . ?
C183 Y5 Y6 O5 16.5(4) . . . . ?
O8 Y5 Y6 O7 -165.3(5) . . . . ?
N15 Y5 Y6 O7 127.8(5) . . . . ?
N17 Y5 Y6 O7 -35.3(7) . . . . ?
N14 Y5 Y6 O7 53.5(4) . . . . ?
N16 Y5 Y6 O7 -110.0(4) . . . . ?
C158 Y5 Y6 O7 -18.5(5) . . . . ?
C183 Y5 Y6 O7 -173.8(4) . . . . ?
O7 Y5 Y6 O6 -95.7(4) . . . . ?
O8 Y5 Y6 O6 99.0(4) . . . . ?
N15 Y5 Y6 O6 32.1(4) . . . . ?
N17 Y5 Y6 O6 -131.0(7) . . . . ?
N14 Y5 Y6 O6 -42.2(3) . . . . ?
N16 Y5 Y6 O6 154.3(4) . . . . ?
C158 Y5 Y6 O6 -114.2(4) . . . . ?
C183 Y5 Y6 O6 90.5(4) . . . . ?
O7 Y5 Y6 O8 165.3(5) . . . . ?
N15 Y5 Y6 O8 -66.9(5) . . . . ?
N17 Y5 Y6 O8 130.0(8) . . . . ?
N14 Y5 Y6 O8 -141.2(4) . . . . ?
N16 Y5 Y6 O8 55.3(5) . . . . ?
C158 Y5 Y6 O8 146.8(5) . . . . ?
C183 Y5 Y6 O8 -8.5(5) . . . . ?
O7 Y5 Y6 Si4 17.6(3) . . . . ?
O8 Y5 Y6 Si4 -147.7(4) . . . . ?
N15 Y5 Y6 Si4 145.5(4) . . . . ?
N17 Y5 Y6 Si4 -17.7(7) . . . . ?
N14 Y5 Y6 Si4 71.1(3) . . . . ?
N16 Y5 Y6 Si4 -92.4(3) . . . . ?
C158 Y5 Y6 Si4 -0.9(4) . . . . ?
C183 Y5 Y6 Si4 -156.2(3) . . . . ?
O7 Y5 Y6 Si3 79.8(3) . . . . ?
O8 Y5 Y6 Si3 -85.5(4) . . . . ?
N15 Y5 Y6 Si3 -152.4(4) . . . . ?
N17 Y5 Y6 Si3 44.5(7) . . . . ?
N14 Y5 Y6 Si3 133.3(3) . . . . ?
N16 Y5 Y6 Si3 -30.3(3) . . . . ?
C158 Y5 Y6 Si3 61.2(4) . . . . ?
C183 Y5 Y6 Si3 -94.0(3) . . . . ?
O7 Y5 Y6 Y4 -129.7(3) . . . . ?
O8 Y5 Y6 Y4 65.0(4) . . . . ?
N15 Y5 Y6 Y4 -1.8(4) . . . . ?
N17 Y5 Y6 Y4 -165.0(7) . . . . ?
N14 Y5 Y6 Y4 -76.2(3) . . . . ?
N16 Y5 Y6 Y4 120.3(3) . . . . ?
C158 Y5 Y6 Y4 -148.2(4) . . . . ?
C183 Y5 Y6 Y4 56.5(3) . . . . ?
O6 Y4 Y6 N18 -111.5(5) . . . . ?
O5 Y4 Y6 N18 51.9(5) . . . . ?
N11 Y4 Y6 N18 178.3(4) . . . . ?
N13 Y4 Y6 N18 17.2(8) . . . . ?
N12 Y4 Y6 N18 -59.9(4) . . . . ?
N10 Y4 Y6 N18 102.1(4) . . . . ?
C108 Y4 Y6 N18 30.0(5) . . . . ?
C133 Y4 Y6 N18 -123.6(4) . . . . ?
O6 Y4 Y6 O5 -163.4(5) . . . . ?
N11 Y4 Y6 O5 126.4(5) . . . . ?
N13 Y4 Y6 O5 -34.7(8) . . . . ?
N12 Y4 Y6 O5 -111.8(4) . . . . ?
N10 Y4 Y6 O5 50.2(4) . . . . ?
C108 Y4 Y6 O5 -21.9(5) . . . . ?
C133 Y4 Y6 O5 -175.5(4) . . . . ?
O6 Y4 Y6 O7 28.3(5) . . . . ?
O5 Y4 Y6 O7 -168.2(5) . . . . ?
N11 Y4 Y6 O7 -41.9(4) . . . . ?
N13 Y4 Y6 O7 157.0(7) . . . . ?
N12 Y4 Y6 O7 80.0(4) . . . . ?
N10 Y4 Y6 O7 -118.0(4) . . . . ?
C108 Y4 Y6 O7 169.8(4) . . . . ?
C133 Y4 Y6 O7 16.3(4) . . . . ?
O5 Y4 Y6 O6 163.4(5) . . . . ?
N11 Y4 Y6 O6 -70.2(5) . . . . ?
N13 Y4 Y6 O6 128.7(8) . . . . ?
N12 Y4 Y6 O6 51.6(4) . . . . ?
N10 Y4 Y6 O6 -146.4(4) . . . . ?
C108 Y4 Y6 O6 141.5(5) . . . . ?
C133 Y4 Y6 O6 -12.1(4) . . . . ?
O6 Y4 Y6 O8 101.7(4) . . . . ?
O5 Y4 Y6 O8 -94.9(4) . . . . ?
N11 Y4 Y6 O8 31.5(4) . . . . ?
N13 Y4 Y6 O8 -129.6(7) . . . . ?
N12 Y4 Y6 O8 153.3(3) . . . . ?
N10 Y4 Y6 O8 -44.7(3) . . . . ?
C108 Y4 Y6 O8 -116.8(4) . . . . ?
C133 Y4 Y6 O8 89.6(4) . . . . ?
O6 Y4 Y6 Si4 -79.1(4) . . . . ?
O5 Y4 Y6 Si4 84.3(4) . . . . ?
N11 Y4 Y6 Si4 -149.3(3) . . . . ?
N13 Y4 Y6 Si4 49.6(7) . . . . ?
N12 Y4 Y6 Si4 -27.5(3) . . . . ?
N10 Y4 Y6 Si4 134.6(3) . . . . ?
C108 Y4 Y6 Si4 62.4(3) . . . . ?
C133 Y4 Y6 Si4 -91.2(3) . . . . ?
O6 Y4 Y6 Si3 -141.8(4) . . . . ?
O5 Y4 Y6 Si3 21.6(4) . . . . ?
N11 Y4 Y6 Si3 148.0(3) . . . . ?
N13 Y4 Y6 Si3 -13.1(7) . . . . ?
N12 Y4 Y6 Si3 -90.2(3) . . . . ?
N10 Y4 Y6 Si3 71.8(3) . . . . ?
C108 Y4 Y6 Si3 -0.3(3) . . . . ?
C133 Y4 Y6 Si3 -153.9(3) . . . . ?
O6 Y4 Y6 Y5 68.2(3) . . . . ?
O5 Y4 Y6 Y5 -128.3(4) . . . . ?
N11 Y4 Y6 Y5 -2.0(3) . . . . ?
N13 Y4 Y6 Y5 -163.1(7) . . . . ?
N12 Y4 Y6 Y5 119.8(3) . . . . ?
N10 Y4 Y6 Y5 -78.1(2) . . . . ?
C108 Y4 Y6 Y5 -150.3(3) . . . . ?
C133 Y4 Y6 Y5 56.1(3) . . . . ?
O1 Y3 Si1 N9 114.7(7) . . . . ?
O4 Y3 Si1 N9 -69.5(7) . . . . ?
O3 Y3 Si1 N9 -146.1(7) . . . . ?
O2 Y3 Si1 N9 69.2(8) . . . . ?
Si2 Y3 Si1 N9 -0.5(6) . . . . ?
Y2 Y3 Si1 N9 -107.8(6) . . . . ?
Y1 Y3 Si1 N9 105.8(6) . . . . ?
O1 Y3 Si1 C102 32.4(8) . . . . ?
N9 Y3 Si1 C102 -82.3(10) . . . . ?
O4 Y3 Si1 C102 -151.8(8) . . . . ?
O3 Y3 Si1 C102 131.5(8) . . . . ?
O2 Y3 Si1 C102 -13.2(9) . . . . ?
Si2 Y3 Si1 C102 -82.9(8) . . . . ?
Y2 Y3 Si1 C102 169.8(8) . . . . ?
Y1 Y3 Si1 C102 23.5(8) . . . . ?
O1 Y3 Si1 C103 -66.5(6) . . . . ?
N9 Y3 Si1 C103 178.8(9) . . . . ?
O4 Y3 Si1 C103 109.3(6) . . . . ?
O3 Y3 Si1 C103 32.6(6) . . . . ?
O2 Y3 Si1 C103 -112.1(7) . . . . ?
Si2 Y3 Si1 C103 178.3(5) . . . . ?
Y2 Y3 Si1 C103 70.9(5) . . . . ?
Y1 Y3 Si1 C103 -75.4(5) . . . . ?
O1 Y3 Si1 C101 -165.7(10) . . . . ?
N9 Y3 Si1 C101 79.5(11) . . . . ?
O4 Y3 Si1 C101 10.0(10) . . . . ?
O3 Y3 Si1 C101 -66.6(10) . . . . ?
O2 Y3 Si1 C101 148.7(10) . . . . ?
Si2 Y3 Si1 C101 79.0(10) . . . . ?
Y2 Y3 Si1 C101 -28.3(10) . . . . ?
Y1 Y3 Si1 C101 -174.6(9) . . . . ?
O1 Y3 Si2 N9 -69.6(7) . . . . ?
O4 Y3 Si2 N9 115.1(7) . . . . ?
O3 Y3 Si2 N9 65.9(7) . . . . ?
O2 Y3 Si2 N9 -145.9(7) . . . . ?
Si1 Y3 Si2 N9 0.5(6) . . . . ?
Y2 Y3 Si2 N9 103.7(6) . . . . ?
Y1 Y3 Si2 N9 -106.9(6) . . . . ?
O1 Y3 Si2 C105 12.8(8) . . . . ?
N9 Y3 Si2 C105 82.4(9) . . . . ?
O4 Y3 Si2 C105 -162.5(8) . . . . ?
O3 Y3 Si2 C105 148.3(8) . . . . ?
O2 Y3 Si2 C105 -63.5(8) . . . . ?
Si1 Y3 Si2 C105 82.9(7) . . . . ?
Y2 Y3 Si2 C105 -173.9(7) . . . . ?
Y1 Y3 Si2 C105 -24.5(7) . . . . ?
O1 Y3 Si2 C104 -153.8(7) . . . . ?
N9 Y3 Si2 C104 -84.2(9) . . . . ?
O4 Y3 Si2 C104 30.9(7) . . . . ?
O3 Y3 Si2 C104 -18.3(8) . . . . ?
O2 Y3 Si2 C104 129.9(7) . . . . ?
Si1 Y3 Si2 C104 -83.7(6) . . . . ?
Y2 Y3 Si2 C104 19.5(6) . . . . ?
Y1 Y3 Si2 C104 168.9(6) . . . . ?
O1 Y3 Si2 C106 107.5(6) . . . . ?
N9 Y3 Si2 C106 177.1(9) . . . . ?
O4 Y3 Si2 C106 -67.8(6) . . . . ?
O3 Y3 Si2 C106 -117.0(7) . . . . ?
O2 Y3 Si2 C106 31.2(6) . . . . ?
Si1 Y3 Si2 C106 177.6(6) . . . . ?
Y2 Y3 Si2 C106 -79.2(5) . . . . ?
Y1 Y3 Si2 C106 70.2(6) . . . . ?
O5 Y6 Si3 N18 118.2(6) . . . . ?
O7 Y6 Si3 N18 -67.3(6) . . . . ?
O6 Y6 Si3 N18 67.3(7) . . . . ?
O8 Y6 Si3 N18 -144.8(6) . . . . ?
Si4 Y6 Si3 N18 0.7(5) . . . . ?
Y5 Y6 Si3 N18 -105.2(5) . . . . ?
Y4 Y6 Si3 N18 105.4(5) . . . . ?
N18 Y6 Si3 C207 -86.8(9) . . . . ?
O5 Y6 Si3 C207 31.3(7) . . . . ?
O7 Y6 Si3 C207 -154.1(7) . . . . ?
O6 Y6 Si3 C207 -19.5(8) . . . . ?
O8 Y6 Si3 C207 128.4(7) . . . . ?
Si4 Y6 Si3 C207 -86.2(7) . . . . ?
Y5 Y6 Si3 C207 168.0(7) . . . . ?
Y4 Y6 Si3 C207 18.5(7) . . . . ?
N18 Y6 Si3 C208 75.9(9) . . . . ?
O5 Y6 Si3 C208 -166.0(8) . . . . ?
O7 Y6 Si3 C208 8.6(8) . . . . ?
O6 Y6 Si3 C208 143.2(9) . . . . ?
O8 Y6 Si3 C208 -68.9(8) . . . . ?
Si4 Y6 Si3 C208 76.5(8) . . . . ?
Y5 Y6 Si3 C208 -29.3(8) . . . . ?
Y4 Y6 Si3 C208 -178.8(8) . . . . ?
N18 Y6 Si3 C209 174.2(8) . . . . ?
O5 Y6 Si3 C209 -67.7(6) . . . . ?
O7 Y6 Si3 C209 106.9(6) . . . . ?
O6 Y6 Si3 C209 -118.5(7) . . . . ?
O8 Y6 Si3 C209 29.4(6) . . . . ?
Si4 Y6 Si3 C209 174.9(6) . . . . ?
Y5 Y6 Si3 C209 69.0(6) . . . . ?
Y4 Y6 Si3 C209 -80.4(6) . . . . ?
O5 Y6 Si4 N18 -69.5(6) . . . . ?
O7 Y6 Si4 N18 115.4(5) . . . . ?
O6 Y6 Si4 N18 -145.9(6) . . . . ?
O8 Y6 Si4 N18 70.1(7) . . . . ?
Si3 Y6 Si4 N18 -0.6(5) . . . . ?
Y5 Y6 Si4 N18 104.9(5) . . . . ?
Y4 Y6 Si4 N18 -108.5(5) . . . . ?
N18 Y6 Si4 C212 178.6(7) . . . . ?
O5 Y6 Si4 C212 109.1(6) . . . . ?
O7 Y6 Si4 C212 -66.0(6) . . . . ?
O6 Y6 Si4 C212 32.7(6) . . . . ?
O8 Y6 Si4 C212 -111.2(7) . . . . ?
Si3 Y6 Si4 C212 178.0(6) . . . . ?
Y5 Y6 Si4 C212 -76.5(5) . . . . ?
Y4 Y6 Si4 C212 70.1(5) . . . . ?
N18 Y6 Si4 C211 -81.5(8) . . . . ?
O5 Y6 Si4 C211 -151.0(7) . . . . ?
O7 Y6 Si4 C211 33.9(7) . . . . ?
O6 Y6 Si4 C211 132.6(7) . . . . ?
O8 Y6 Si4 C211 -11.4(8) . . . . ?
Si3 Y6 Si4 C211 -82.1(6) . . . . ?
Y5 Y6 Si4 C211 23.4(7) . . . . ?
Y4 Y6 Si4 C211 170.0(6) . . . . ?
N18 Y6 Si4 C210 81.0(10) . . . . ?
O5 Y6 Si4 C210 11.4(9) . . . . ?
O7 Y6 Si4 C210 -163.6(9) . . . . ?
O6 Y6 Si4 C210 -64.9(9) . . . . ?
O8 Y6 Si4 C210 151.1(9) . . . . ?
Si3 Y6 Si4 C210 80.3(9) . . . . ?
Y5 Y6 Si4 C210 -174.2(9) . . . . ?
Y4 Y6 Si4 C210 -27.5(9) . . . . ?
O2 Y1 N1 C21 103.0(9) . . . . ?
N2 Y1 N1 C21 11.1(8) . . . . ?
O1 Y1 N1 C21 155.9(9) . . . . ?
N4 Y1 N1 C21 -76.8(9) . . . . ?
N3 Y1 N1 C21 -84.9(11) . . . . ?
C2 Y1 N1 C21 -172.0(9) . . . . ?
C27 Y1 N1 C21 70.4(10) . . . . ?
Y3 Y1 N1 C21 128.1(8) . . . . ?
O2 Y1 N1 C12 -79.9(11) . . . . ?
N2 Y1 N1 C12 -171.8(11) . . . . ?
O1 Y1 N1 C12 -27.0(10) . . . . ?
N4 Y1 N1 C12 100.3(10) . . . . ?
N3 Y1 N1 C12 92.2(12) . . . . ?
C2 Y1 N1 C12 5.1(10) . . . . ?
C27 Y1 N1 C12 -112.5(10) . . . . ?
Y3 Y1 N1 C12 -54.8(10) . . . . ?
O2 Y1 N2 C25 70.2(14) . . . . ?
O1 Y1 N2 C25 140.7(13) . . . . ?
N4 Y1 N2 C25 -84.9(14) . . . . ?
N3 Y1 N2 C25 -18.1(15) . . . . ?
N1 Y1 N2 C25 -166.7(15) . . . . ?
C2 Y1 N2 C25 -173.4(13) . . . . ?
C27 Y1 N2 C25 53.3(14) . . . . ?
Y3 Y1 N2 C25 103.7(14) . . . . ?
O2 Y1 N2 C22 -135.0(9) . . . . ?
O1 Y1 N2 C22 -64.6(10) . . . . ?
N4 Y1 N2 C22 69.8(9) . . . . ?
N3 Y1 N2 C22 136.7(9) . . . . ?
N1 Y1 N2 C22 -11.9(9) . . . . ?
C2 Y1 N2 C22 -18.6(14) . . . . ?
C27 Y1 N2 C22 -152.0(9) . . . . ?
Y3 Y1 N2 C22 -101.5(9) . . . . ?
O2 Y1 N3 C46 -179.8(9) . . . . ?
N2 Y1 N3 C46 -79.1(9) . . . . ?
O1 Y1 N3 C46 117.3(9) . . . . ?
N4 Y1 N3 C46 -1.9(9) . . . . ?
N1 Y1 N3 C46 6.7(13) . . . . ?
C2 Y1 N3 C46 89.7(9) . . . . ?
C27 Y1 N3 C46 -154.7(10) . . . . ?
Y3 Y1 N3 C46 152.4(8) . . . . ?
O2 Y1 N3 C37 15.4(10) . . . . ?
N2 Y1 N3 C37 116.2(10) . . . . ?
O1 Y1 N3 C37 -47.4(11) . . . . ?
N4 Y1 N3 C37 -166.6(11) . . . . ?
N1 Y1 N3 C37 -158.0(9) . . . . ?
C2 Y1 N3 C37 -75.0(11) . . . . ?
C27 Y1 N3 C37 40.5(10) . . . . ?
Y3 Y1 N3 C37 -12.3(11) . . . . ?
O2 Y1 N4 C50 -175.0(13) . . . . ?
N2 Y1 N4 C50 -67.5(15) . . . . ?
O1 Y1 N4 C50 74.6(16) . . . . ?
N3 Y1 N4 C50 -179.7(16) . . . . ?
N1 Y1 N4 C50 4.6(15) . . . . ?
C2 Y1 N4 C50 84.9(15) . . . . ?
C27 Y1 N4 C50 -140.0(14) . . . . ?
Y3 Y1 N4 C50 93.8(16) . . . . ?
O2 Y1 N4 C47 6.8(14) . . . . ?
N2 Y1 N4 C47 114.2(9) . . . . ?
O1 Y1 N4 C47 -103.6(9) . . . . ?
N3 Y1 N4 C47 2.0(9) . . . . ?
N1 Y1 N4 C47 -173.7(9) . . . . ?
C2 Y1 N4 C47 -93.3(9) . . . . ?
C27 Y1 N4 C47 41.7(11) . . . . ?
Y3 Y1 N4 C47 -84.5(11) . . . . ?
O3 Y2 N5 C71 -177.5(10) . . . . ?
O4 Y2 N5 C71 118.5(9) . . . . ?
N8 Y2 N5 C71 -78.2(10) . . . . ?
N6 Y2 N5 C71 0.2(9) . . . . ?
N7 Y2 N5 C71 6.0(15) . . . . ?
C77 Y2 N5 C71 89.0(10) . . . . ?
C52 Y2 N5 C71 -150.9(10) . . . . ?
Y3 Y2 N5 C71 155.5(9) . . . . ?
O3 Y2 N5 C62 16.5(10) . . . . ?
O4 Y2 N5 C62 -47.5(11) . . . . ?
N8 Y2 N5 C62 115.8(10) . . . . ?
N6 Y2 N5 C62 -165.8(11) . . . . ?
N7 Y2 N5 C62 -160.0(10) . . . . ?
C77 Y2 N5 C62 -77.0(11) . . . . ?
C52 Y2 N5 C62 43.1(10) . . . . ?
Y3 Y2 N5 C62 -10.5(11) . . . . ?
O3 Y2 N6 C75 -164.1(14) . . . . ?
O4 Y2 N6 C75 82.3(17) . . . . ?
N8 Y2 N6 C75 -58.9(17) . . . . ?
N5 Y2 N6 C75 -169.3(17) . . . . ?
N7 Y2 N6 C75 13.3(16) . . . . ?
C77 Y2 N6 C75 91.4(17) . . . . ?
C52 Y2 N6 C75 -128.0(16) . . . . ?
Y3 Y2 N6 C75 103.3(17) . . . . ?
O3 Y2 N6 C72 2.9(16) . . . . ?
O4 Y2 N6 C72 -110.7(9) . . . . ?
N8 Y2 N6 C72 108.1(10) . . . . ?
N5 Y2 N6 C72 -2.3(9) . . . . ?
N7 Y2 N6 C72 -179.6(10) . . . . ?
C77 Y2 N6 C72 -101.6(10) . . . . ?
C52 Y2 N6 C72 39.0(13) . . . . ?
Y3 Y2 N6 C72 -89.7(11) . . . . ?
O3 Y2 N7 C96 107.2(9) . . . . ?
O4 Y2 N7 C96 161.9(10) . . . . ?
N8 Y2 N7 C96 16.0(9) . . . . ?
N6 Y2 N7 C96 -71.5(10) . . . . ?
N5 Y2 N7 C96 -77.0(13) . . . . ?
C77 Y2 N7 C96 -165.1(10) . . . . ?
C52 Y2 N7 C96 73.6(11) . . . . ?
Y3 Y2 N7 C96 132.3(9) . . . . ?
O3 Y2 N7 C87 -78.2(13) . . . . ?
O4 Y2 N7 C87 -23.5(12) . . . . ?
N8 Y2 N7 C87 -169.4(13) . . . . ?
N6 Y2 N7 C87 103.1(13) . . . . ?
N5 Y2 N7 C87 97.6(14) . . . . ?
C77 Y2 N7 C87 9.5(12) . . . . ?
C52 Y2 N7 C87 -111.9(12) . . . . ?
Y3 Y2 N7 C87 -53.1(12) . . . . ?
O3 Y2 N8 C100 77.5(15) . . . . ?
O4 Y2 N8 C100 150.1(14) . . . . ?
N6 Y2 N8 C100 -76.7(15) . . . . ?
N5 Y2 N8 C100 -8.7(16) . . . . ?
N7 Y2 N8 C100 -160.3(16) . . . . ?
C77 Y2 N8 C100 -162.5(14) . . . . ?
C52 Y2 N8 C100 61.1(15) . . . . ?
Y3 Y2 N8 C100 111.2(14) . . . . ?
O3 Y2 N8 C97 -142.4(9) . . . . ?
O4 Y2 N8 C97 -69.8(10) . . . . ?
N6 Y2 N8 C97 63.4(9) . . . . ?
N5 Y2 N8 C97 131.4(9) . . . . ?
N7 Y2 N8 C97 -20.2(9) . . . . ?
C77 Y2 N8 C97 -22.4(14) . . . . ?
C52 Y2 N8 C97 -158.8(10) . . . . ?
Y3 Y2 N8 C97 -108.7(9) . . . . ?
C102 Si1 N9 Si2 -62.5(11) . . . . ?
C103 Si1 N9 Si2 177.8(8) . . . . ?
C101 Si1 N9 Si2 58.9(13) . . . . ?
Y3 Si1 N9 Si2 179.0(12) . . . . ?
C102 Si1 N9 Y3 118.5(9) . . . . ?
C103 Si1 N9 Y3 -1.2(8) . . . . ?
C101 Si1 N9 Y3 -120.1(10) . . . . ?
C105 Si2 N9 Si1 61.5(11) . . . . ?
C104 Si2 N9 Si1 -63.0(10) . . . . ?
C106 Si2 N9 Si1 178.1(8) . . . . ?
Y3 Si2 N9 Si1 -179.0(12) . . . . ?
C105 Si2 N9 Y3 -119.5(8) . . . . ?
C104 Si2 N9 Y3 116.0(7) . . . . ?
C106 Si2 N9 Y3 -2.9(9) . . . . ?
O1 Y3 N9 Si1 -65.4(6) . . . . ?
O4 Y3 N9 Si1 114.8(6) . . . . ?
O3 Y3 N9 Si1 42.0(8) . . . . ?
O2 Y3 N9 Si1 -136.4(5) . . . . ?
Si2 Y3 N9 Si1 179.1(11) . . . . ?
Y2 Y3 N9 Si1 86.6(6) . . . . ?
Y1 Y3 N9 Si1 -90.7(6) . . . . ?
O1 Y3 N9 Si2 115.5(6) . . . . ?
O4 Y3 N9 Si2 -64.3(6) . . . . ?
O3 Y3 N9 Si2 -137.1(5) . . . . ?
O2 Y3 N9 Si2 44.5(8) . . . . ?
Si1 Y3 N9 Si2 -179.1(11) . . . . ?
Y2 Y3 N9 Si2 -92.5(6) . . . . ?
Y1 Y3 N9 Si2 90.2(6) . . . . ?
O6 Y4 N10 C127 101.9(8) . . . . ?
O5 Y4 N10 C127 152.7(8) . . . . ?
N11 Y4 N10 C127 10.9(8) . . . . ?
N13 Y4 N10 C127 -79.4(8) . . . . ?
N12 Y4 N10 C127 -87.5(10) . . . . ?
C108 Y4 N10 C127 -174.9(9) . . . . ?
C133 Y4 N10 C127 67.0(9) . . . . ?
Y6 Y4 N10 C127 126.0(8) . . . . ?
O6 Y4 N10 C118 -77.4(10) . . . . ?
O5 Y4 N10 C118 -26.6(9) . . . . ?
N11 Y4 N10 C118 -168.4(10) . . . . ?
N13 Y4 N10 C118 101.3(10) . . . . ?
N12 Y4 N10 C118 93.2(11) . . . . ?
C108 Y4 N10 C118 5.8(10) . . . . ?
C133 Y4 N10 C118 -112.4(10) . . . . ?
Y6 Y4 N10 C118 -53.3(10) . . . . ?
O6 Y4 N11 C131 65.0(15) . . . . ?
O5 Y4 N11 C131 137.2(13) . . . . ?
N13 Y4 N11 C131 -89.2(15) . . . . ?
N12 Y4 N11 C131 -22.1(15) . . . . ?
N10 Y4 N11 C131 -168.1(15) . . . . ?
C108 Y4 N11 C131 179.9(13) . . . . ?
C133 Y4 N11 C131 49.8(14) . . . . ?
Y6 Y4 N11 C131 98.6(14) . . . . ?
O6 Y4 N11 C128 -138.7(8) . . . . ?
O5 Y4 N11 C128 -66.5(9) . . . . ?
N13 Y4 N11 C128 67.1(9) . . . . ?
N12 Y4 N11 C128 134.2(8) . . . . ?
N10 Y4 N11 C128 -11.7(8) . . . . ?
C108 Y4 N11 C128 -23.8(13) . . . . ?
C133 Y4 N11 C128 -153.8(9) . . . . ?
Y6 Y4 N11 C128 -105.1(8) . . . . ?
O6 Y4 N12 C152 172.0(9) . . . . ?
O5 Y4 N12 C152 108.6(9) . . . . ?
N11 Y4 N12 C152 -88.3(9) . . . . ?
N13 Y4 N12 C152 -9.1(8) . . . . ?
N10 Y4 N12 C152 -0.6(12) . . . . ?
C108 Y4 N12 C152 81.5(9) . . . . ?
C133 Y4 N12 C152 -161.8(9) . . . . ?
Y6 Y4 N12 C152 144.9(8) . . . . ?
O6 Y4 N12 C143 9.7(9) . . . . ?
O5 Y4 N12 C143 -53.6(10) . . . . ?
N11 Y4 N12 C143 109.5(9) . . . . ?
N13 Y4 N12 C143 -171.4(10) . . . . ?
N10 Y4 N12 C143 -162.9(8) . . . . ?
C108 Y4 N12 C143 -80.8(10) . . . . ?
C133 Y4 N12 C143 35.9(9) . . . . ?
Y6 Y4 N12 C143 -17.4(10) . . . . ?
O6 Y4 N13 C156 -178.1(11) . . . . ?
O5 Y4 N13 C156 71.1(14) . . . . ?
N11 Y4 N13 C156 -69.1(14) . . . . ?
N12 Y4 N13 C156 179.5(14) . . . . ?
N10 Y4 N13 C156 4.2(13) . . . . ?
C108 Y4 N13 C156 82.7(14) . . . . ?
C133 Y4 N13 C156 -139.7(13) . . . . ?
Y6 Y4 N13 C156 94.0(14) . . . . ?
O6 Y4 N13 C153 12.1(14) . . . . ?
O5 Y4 N13 C153 -98.6(9) . . . . ?
N11 Y4 N13 C153 121.1(9) . . . . ?
N12 Y4 N13 C153 9.7(9) . . . . ?
N10 Y4 N13 C153 -165.6(9) . . . . ?
C108 Y4 N13 C153 -87.1(9) . . . . ?
C133 Y4 N13 C153 50.5(11) . . . . ?
Y6 Y4 N13 C153 -75.7(12) . . . . ?
O7 Y5 N14 C177 158.2(8) . . . . ?
O8 Y5 N14 C177 102.9(8) . . . . ?
N15 Y5 N14 C177 14.4(8) . . . . ?
N17 Y5 N14 C177 -76.6(9) . . . . ?
N16 Y5 N14 C177 -85.8(11) . . . . ?
C158 Y5 N14 C177 -169.5(9) . . . . ?
C183 Y5 N14 C177 70.7(9) . . . . ?
Y6 Y5 N14 C177 129.5(8) . . . . ?
O7 Y5 N14 C168 -24.2(10) . . . . ?
O8 Y5 N14 C168 -79.5(11) . . . . ?
N15 Y5 N14 C168 -167.9(11) . . . . ?
N17 Y5 N14 C168 101.0(11) . . . . ?
N16 Y5 N14 C168 91.9(12) . . . . ?
C158 Y5 N14 C168 8.2(10) . . . . ?
C183 Y5 N14 C168 -111.6(10) . . . . ?
Y6 Y5 N14 C168 -52.8(10) . . . . ?
O7 Y5 N15 C181 143.9(13) . . . . ?
O8 Y5 N15 C181 72.0(14) . . . . ?
N17 Y5 N15 C181 -82.2(14) . . . . ?
N14 Y5 N15 C181 -164.0(15) . . . . ?
N16 Y5 N15 C181 -13.9(15) . . . . ?
C158 Y5 N15 C181 -171.6(13) . . . . ?
C183 Y5 N15 C181 55.6(14) . . . . ?
Y6 Y5 N15 C181 105.1(14) . . . . ?
O7 Y5 N15 C178 -72.1(9) . . . . ?
O8 Y5 N15 C178 -144.0(8) . . . . ?
N17 Y5 N15 C178 61.8(9) . . . . ?
N14 Y5 N15 C178 -20.0(8) . . . . ?
N16 Y5 N15 C178 130.1(8) . . . . ?
C158 Y5 N15 C178 -27.6(13) . . . . ?
C183 Y5 N15 C178 -160.4(9) . . . . ?
Y6 Y5 N15 C178 -111.0(8) . . . . ?
O7 Y5 N16 C202 106.6(9) . . . . ?
O8 Y5 N16 C202 172.1(9) . . . . ?
N15 Y5 N16 C202 -90.9(9) . . . . ?
N17 Y5 N16 C202 -10.4(9) . . . . ?
N14 Y5 N16 C202 -0.7(14) . . . . ?
C158 Y5 N16 C202 78.0(9) . . . . ?
C183 Y5 N16 C202 -162.7(9) . . . . ?
Y6 Y5 N16 C202 143.1(8) . . . . ?
O7 Y5 N16 C193 -54.8(11) . . . . ?
O8 Y5 N16 C193 10.7(10) . . . . ?
N15 Y5 N16 C193 107.7(11) . . . . ?
N17 Y5 N16 C193 -171.8(12) . . . . ?
N14 Y5 N16 C193 -162.1(10) . . . . ?
C158 Y5 N16 C193 -83.4(11) . . . . ?
C183 Y5 N16 C193 35.9(10) . . . . ?
Y6 Y5 N16 C193 -18.3(11) . . . . ?
O7 Y5 N17 C206 73.8(18) . . . . ?
O8 Y5 N17 C206 -174.7(15) . . . . ?
N15 Y5 N17 C206 -67.9(18) . . . . ?
N14 Y5 N17 C206 4.3(17) . . . . ?
N16 Y5 N17 C206 179.7(18) . . . . ?
C158 Y5 N17 C206 82.0(18) . . . . ?
C183 Y5 N17 C206 -139.8(16) . . . . ?
Y6 Y5 N17 C206 97.0(19) . . . . ?
O7 Y5 N17 C203 -98.3(10) . . . . ?
O8 Y5 N17 C203 13.2(16) . . . . ?
N15 Y5 N17 C203 120.0(10) . . . . ?
N14 Y5 N17 C203 -167.8(10) . . . . ?
N16 Y5 N17 C203 7.6(9) . . . . ?
C158 Y5 N17 C203 -90.1(10) . . . . ?
C183 Y5 N17 C203 48.1(12) . . . . ?
Y6 Y5 N17 C203 -75.1(12) . . . . ?
C207 Si3 N18 Si4 -66.3(9) . . . . ?
C208 Si3 N18 Si4 57.9(10) . . . . ?
C209 Si3 N18 Si4 175.5(7) . . . . ?
Y6 Si3 N18 Si4 -178.7(10) . . . . ?
C207 Si3 N18 Y6 112.4(7) . . . . ?
C208 Si3 N18 Y6 -123.4(8) . . . . ?
C209 Si3 N18 Y6 -5.7(8) . . . . ?
C212 Si4 N18 Si3 177.4(7) . . . . ?
C211 Si4 N18 Si3 -64.0(9) . . . . ?
C210 Si4 N18 Si3 60.3(11) . . . . ?
Y6 Si4 N18 Si3 178.8(10) . . . . ?
C212 Si4 N18 Y6 -1.4(8) . . . . ?
C211 Si4 N18 Y6 117.3(7) . . . . ?
C210 Si4 N18 Y6 -118.5(9) . . . . ?
O5 Y6 N18 Si3 -62.3(5) . . . . ?
O7 Y6 N18 Si3 117.2(5) . . . . ?
O6 Y6 N18 Si3 -135.4(5) . . . . ?
O8 Y6 N18 Si3 44.7(7) . . . . ?
Si4 Y6 N18 Si3 -178.8(9) . . . . ?
Y5 Y6 N18 Si3 89.7(5) . . . . ?
Y4 Y6 N18 Si3 -90.6(5) . . . . ?
O5 Y6 N18 Si4 116.6(5) . . . . ?
O7 Y6 N18 Si4 -64.0(5) . . . . ?
O6 Y6 N18 Si4 43.4(7) . . . . ?
O8 Y6 N18 Si4 -136.4(4) . . . . ?
Si3 Y6 N18 Si4 178.8(9) . . . . ?
Y5 Y6 N18 Si4 -91.5(5) . . . . ?
Y4 Y6 N18 Si4 88.3(5) . . . . ?
N9 Y3 O1 C2 -33.4(12) . . . . ?
O4 Y3 O1 C2 145.9(16) . . . . ?
O3 Y3 O1 C2 -162.3(12) . . . . ?
O2 Y3 O1 C2 98.1(12) . . . . ?
Si2 Y3 O1 C2 -7.5(12) . . . . ?
Si1 Y3 O1 C2 -57.2(12) . . . . ?
Y2 Y3 O1 C2 -179.2(10) . . . . ?
Y1 Y3 O1 C2 109.7(12) . . . . ?
N9 Y3 O1 Y1 -143.1(4) . . . . ?
O4 Y3 O1 Y1 36.2(17) . . . . ?
O3 Y3 O1 Y1 88.0(4) . . . . ?
O2 Y3 O1 Y1 -11.7(3) . . . . ?
Si2 Y3 O1 Y1 -117.2(3) . . . . ?
Si1 Y3 O1 Y1 -167.0(3) . . . . ?
Y2 Y3 O1 Y1 71.1(4) . . . . ?
O2 Y1 O1 C2 -134.3(7) . . . . ?
N2 Y1 O1 C2 140.8(7) . . . . ?
N4 Y1 O1 C2 19.9(8) . . . . ?
N3 Y1 O1 C2 -61.1(7) . . . . ?
N1 Y1 O1 C2 90.7(6) . . . . ?
C27 Y1 O1 C2 -136.9(6) . . . . ?
Y3 Y1 O1 C2 -145.9(8) . . . . ?
O2 Y1 O1 Y3 11.6(3) . . . . ?
N2 Y1 O1 Y3 -73.3(5) . . . . ?
N4 Y1 O1 Y3 165.7(4) . . . . ?
N3 Y1 O1 Y3 84.7(5) . . . . ?
N1 Y1 O1 Y3 -123.5(4) . . . . ?
C2 Y1 O1 Y3 145.9(8) . . . . ?
C27 Y1 O1 Y3 8.9(4) . . . . ?
O1 Y3 O2 C27 163.8(13) . . . . ?
N9 Y3 O2 C27 -114.5(13) . . . . ?
O4 Y3 O2 C27 -8.3(13) . . . . ?
O3 Y3 O2 C27 66.9(13) . . . . ?
Si2 Y3 O2 C27 -94.3(12) . . . . ?
Si1 Y3 O2 C27 -147.8(11) . . . . ?
Y2 Y3 O2 C27 29.5(13) . . . . ?
Y1 Y3 O2 C27 152.2(14) . . . . ?
O1 Y3 O2 Y1 11.6(3) . . . . ?
N9 Y3 O2 Y1 93.3(5) . . . . ?
O4 Y3 O2 Y1 -160.5(3) . . . . ?
O3 Y3 O2 Y1 -85.3(4) . . . . ?
Si2 Y3 O2 Y1 113.5(3) . . . . ?
Si1 Y3 O2 Y1 60.0(6) . . . . ?
Y2 Y3 O2 Y1 -122.7(3) . . . . ?
N2 Y1 O2 C27 -40.5(8) . . . . ?
O1 Y1 O2 C27 -174.1(8) . . . . ?
N4 Y1 O2 C27 63.2(11) . . . . ?
N3 Y1 O2 C27 67.7(7) . . . . ?
N1 Y1 O2 C27 -116.3(7) . . . . ?
C2 Y1 O2 C27 163.9(7) . . . . ?
Y3 Y1 O2 C27 -163.0(9) . . . . ?
N2 Y1 O2 Y3 122.4(4) . . . . ?
O1 Y1 O2 Y3 -11.1(3) . . . . ?
N4 Y1 O2 Y3 -133.9(7) . . . . ?
N3 Y1 O2 Y3 -129.4(4) . . . . ?
N1 Y1 O2 Y3 46.7(5) . . . . ?
C2 Y1 O2 Y3 -33.2(4) . . . . ?
C27 Y1 O2 Y3 163.0(9) . . . . ?
O1 Y3 O3 C52 -15.2(14) . . . . ?
N9 Y3 O3 C52 -120.4(14) . . . . ?
O4 Y3 O3 C52 156.2(14) . . . . ?
O2 Y3 O3 C52 58.3(14) . . . . ?
Si2 Y3 O3 C52 -152.2(12) . . . . ?
Si1 Y3 O3 C52 -102.5(14) . . . . ?
Y2 Y3 O3 C52 144.6(15) . . . . ?
Y1 Y3 O3 C52 21.5(14) . . . . ?
O1 Y3 O3 Y2 -159.8(3) . . . . ?
N9 Y3 O3 Y2 95.0(5) . . . . ?
O4 Y3 O3 Y2 11.6(3) . . . . ?
O2 Y3 O3 Y2 -86.3(4) . . . . ?
Si2 Y3 O3 Y2 63.2(5) . . . . ?
Si1 Y3 O3 Y2 112.9(3) . . . . ?
Y1 Y3 O3 Y2 -123.1(3) . . . . ?
O4 Y2 O3 C52 -170.1(8) . . . . ?
N8 Y2 O3 C52 -37.0(8) . . . . ?
N6 Y2 O3 C52 64.6(12) . . . . ?
N5 Y2 O3 C52 69.5(8) . . . . ?
N7 Y2 O3 C52 -112.4(8) . . . . ?
C77 Y2 O3 C52 168.5(8) . . . . ?
Y3 Y2 O3 C52 -158.8(9) . . . . ?
O4 Y2 O3 Y3 -11.3(3) . . . . ?
N8 Y2 O3 Y3 121.8(4) . . . . ?
N6 Y2 O3 Y3 -136.6(8) . . . . ?
N5 Y2 O3 Y3 -131.7(4) . . . . ?
N7 Y2 O3 Y3 46.4(5) . . . . ?
C77 Y2 O3 Y3 -32.7(4) . . . . ?
C52 Y2 O3 Y3 158.8(9) . . . . ?
O1 Y3 O4 C77 150.7(17) . . . . ?
N9 Y3 O4 C77 -30.1(15) . . . . ?
O3 Y3 O4 C77 96.9(15) . . . . ?
O2 Y3 O4 C77 -163.5(15) . . . . ?
Si2 Y3 O4 C77 -55.0(15) . . . . ?
Si1 Y3 O4 C77 -5.4(15) . . . . ?
Y2 Y3 O4 C77 108.4(16) . . . . ?
Y1 Y3 O4 C77 -179.8(14) . . . . ?
O1 Y3 O4 Y2 42.3(17) . . . . ?
N9 Y3 O4 Y2 -138.4(4) . . . . ?
O3 Y3 O4 Y2 -11.5(3) . . . . ?
O2 Y3 O4 Y2 88.1(4) . . . . ?
Si2 Y3 O4 Y2 -163.4(3) . . . . ?
Si1 Y3 O4 Y2 -113.8(3) . . . . ?
Y1 Y3 O4 Y2 71.8(4) . . . . ?
O3 Y2 O4 C77 -137.2(8) . . . . ?
N8 Y2 O4 C77 136.9(8) . . . . ?
N6 Y2 O4 C77 17.2(9) . . . . ?
N5 Y2 O4 C77 -65.5(8) . . . . ?
N7 Y2 O4 C77 88.9(8) . . . . ?
C52 Y2 O4 C77 -141.8(8) . . . . ?
Y3 Y2 O4 C77 -148.5(9) . . . . ?
O3 Y2 O4 Y3 11.3(3) . . . . ?
N8 Y2 O4 Y3 -74.5(6) . . . . ?
N6 Y2 O4 Y3 165.7(4) . . . . ?
N5 Y2 O4 Y3 83.0(4) . . . . ?
N7 Y2 O4 Y3 -122.5(4) . . . . ?
C77 Y2 O4 Y3 148.5(9) . . . . ?
C52 Y2 O4 Y3 6.8(4) . . . . ?
N18 Y6 O5 C108 -32.5(12) . . . . ?
O7 Y6 O5 C108 150.2(13) . . . . ?
O6 Y6 O5 C108 95.5(11) . . . . ?
O8 Y6 O5 C108 -164.0(11) . . . . ?
Si4 Y6 O5 C108 -5.8(12) . . . . ?
Si3 Y6 O5 C108 -55.4(11) . . . . ?
Y5 Y6 O5 C108 -179.0(10) . . . . ?
Y4 Y6 O5 C108 105.8(12) . . . . ?
N18 Y6 O5 Y4 -138.2(4) . . . . ?
O7 Y6 O5 Y4 44.4(15) . . . . ?
O6 Y6 O5 Y4 -10.3(3) . . . . ?
O8 Y6 O5 Y4 90.2(4) . . . . ?
Si4 Y6 O5 Y4 -111.6(3) . . . . ?
Si3 Y6 O5 Y4 -161.2(3) . . . . ?
Y5 Y6 O5 Y4 75.2(4) . . . . ?
O6 Y4 O5 C108 -130.9(7) . . . . ?
N11 Y4 O5 C108 142.7(7) . . . . ?
N13 Y4 O5 C108 22.3(8) . . . . ?
N12 Y4 O5 C108 -59.2(7) . . . . ?
N10 Y4 O5 C108 89.6(7) . . . . ?
C133 Y4 O5 C108 -137.1(7) . . . . ?
Y6 Y4 O5 C108 -141.0(8) . . . . ?
O6 Y4 O5 Y6 10.1(3) . . . . ?
N11 Y4 O5 Y6 -76.3(5) . . . . ?
N13 Y4 O5 Y6 163.4(4) . . . . ?
N12 Y4 O5 Y6 81.8(4) . . . . ?
N10 Y4 O5 Y6 -129.4(4) . . . . ?
C108 Y4 O5 Y6 141.0(8) . . . . ?
C133 Y4 O5 Y6 3.9(4) . . . . ?
N18 Y6 O6 C133 -121.4(11) . . . . ?
O5 Y6 O6 C133 153.4(12) . . . . ?
O7 Y6 O6 C133 -16.6(12) . . . . ?
O8 Y6 O6 C133 58.5(12) . . . . ?
Si4 Y6 O6 C133 -101.6(11) . . . . ?
Si3 Y6 O6 C133 -152.5(10) . . . . ?
Y5 Y6 O6 C133 20.8(12) . . . . ?
Y4 Y6 O6 C133 143.1(13) . . . . ?
N18 Y6 O6 Y4 95.5(5) . . . . ?
O5 Y6 O6 Y4 10.3(3) . . . . ?
O7 Y6 O6 Y4 -159.7(3) . . . . ?
O8 Y6 O6 Y4 -84.6(3) . . . . ?
Si4 Y6 O6 Y4 115.4(3) . . . . ?
Si3 Y6 O6 Y4 64.4(5) . . . . ?
Y5 Y6 O6 Y4 -122.3(3) . . . . ?
O5 Y4 O6 C133 -166.1(7) . . . . ?
N11 Y4 O6 C133 -34.9(7) . . . . ?
N13 Y4 O6 C133 70.8(10) . . . . ?
N12 Y4 O6 C133 73.0(7) . . . . ?
N10 Y4 O6 C133 -112.0(7) . . . . ?
C108 Y4 O6 C133 170.4(7) . . . . ?
Y6 Y4 O6 C133 -156.1(9) . . . . ?
O5 Y4 O6 Y6 -10.1(3) . . . . ?
N11 Y4 O6 Y6 121.2(4) . . . . ?
N13 Y4 O6 Y6 -133.2(6) . . . . ?
N12 Y4 O6 Y6 -130.9(4) . . . . ?
N10 Y4 O6 Y6 44.0(5) . . . . ?
C108 Y4 O6 Y6 -33.5(4) . . . . ?
C133 Y4 O6 Y6 156.1(9) . . . . ?
N18 Y6 O7 C158 -28.7(13) . . . . ?
O5 Y6 O7 C158 148.7(15) . . . . ?
O6 Y6 O7 C158 -159.1(13) . . . . ?
O8 Y6 O7 C158 101.0(13) . . . . ?
Si4 Y6 O7 C158 -54.2(13) . . . . ?
Si3 Y6 O7 C158 -4.7(13) . . . . ?
Y5 Y6 O7 C158 110.2(13) . . . . ?
Y4 Y6 O7 C158 -175.8(11) . . . . ?
N18 Y6 O7 Y5 -138.8(4) . . . . ?
O5 Y6 O7 Y5 38.5(15) . . . . ?
O6 Y6 O7 Y5 90.7(3) . . . . ?
O8 Y6 O7 Y5 -9.2(3) . . . . ?
Si4 Y6 O7 Y5 -164.3(3) . . . . ?
Si3 Y6 O7 Y5 -114.9(3) . . . . ?
Y4 Y6 O7 Y5 74.1(4) . . . . ?
O8 Y5 O7 C158 -137.9(8) . . . . ?
N15 Y5 O7 C158 137.9(8) . . . . ?
N17 Y5 O7 C158 15.8(9) . . . . ?
N14 Y5 O7 C158 87.6(8) . . . . ?
N16 Y5 O7 C158 -64.7(8) . . . . ?
C183 Y5 O7 C158 -141.5(8) . . . . ?
Y6 Y5 O7 C158 -147.0(9) . . . . ?
O8 Y5 O7 Y6 9.1(3) . . . . ?
N15 Y5 O7 Y6 -75.1(6) . . . . ?
N17 Y5 O7 Y6 162.8(4) . . . . ?
N14 Y5 O7 Y6 -125.4(4) . . . . ?
N16 Y5 O7 Y6 82.3(4) . . . . ?
C158 Y5 O7 Y6 147.0(9) . . . . ?
C183 Y5 O7 Y6 5.5(4) . . . . ?
N18 Y6 O8 C183 -115.8(12) . . . . ?
O5 Y6 O8 C183 -9.3(13) . . . . ?
O7 Y6 O8 C183 161.7(13) . . . . ?
O6 Y6 O8 C183 64.4(13) . . . . ?
Si4 Y6 O8 C183 -151.0(11) . . . . ?
Si3 Y6 O8 C183 -96.7(12) . . . . ?
Y5 Y6 O8 C183 152.5(14) . . . . ?
Y4 Y6 O8 C183 27.8(13) . . . . ?
N18 Y6 O8 Y5 91.7(5) . . . . ?
O5 Y6 O8 Y5 -161.8(3) . . . . ?
O7 Y6 O8 Y5 9.1(3) . . . . ?
O6 Y6 O8 Y5 -88.2(4) . . . . ?
Si4 Y6 O8 Y5 56.5(6) . . . . ?
Si3 Y6 O8 Y5 110.8(3) . . . . ?
Y4 Y6 O8 Y5 -124.8(3) . . . . ?
O7 Y5 O8 C183 -171.8(8) . . . . ?
N15 Y5 O8 C183 -39.2(8) . . . . ?
N17 Y5 O8 C183 65.2(12) . . . . ?
N14 Y5 O8 C183 -113.6(8) . . . . ?
N16 Y5 O8 C183 70.5(8) . . . . ?
C158 Y5 O8 C183 167.6(8) . . . . ?
Y6 Y5 O8 C183 -162.8(9) . . . . ?
O7 Y5 O8 Y6 -9.0(3) . . . . ?
N15 Y5 O8 Y6 123.6(4) . . . . ?
N17 Y5 O8 Y6 -132.0(8) . . . . ?
N14 Y5 O8 Y6 49.1(5) . . . . ?
N16 Y5 O8 Y6 -126.7(4) . . . . ?
C158 Y5 O8 Y6 -29.7(4) . . . . ?
C183 Y5 O8 Y6 162.8(9) . . . . ?
Y3 O1 C2 C3 -31.9(18) . . . . ?
Y1 O1 C2 C3 85.5(11) . . . . ?
Y3 O1 C2 C1 158.2(9) . . . . ?
Y1 O1 C2 C1 -84.4(10) . . . . ?
Y3 O1 C2 Y1 -117.4(11) . . . . ?
C6 C1 C2 O1 166.6(11) . . . . ?
C11 C1 C2 O1 -18.6(16) . . . . ?
C6 C1 C2 C3 -3.8(17) . . . . ?
C11 C1 C2 C3 171.0(11) . . . . ?
C6 C1 C2 Y1 102.3(11) . . . . ?
C11 C1 C2 Y1 -82.9(10) . . . . ?
O2 Y1 C2 O1 41.5(6) . . . . ?
N2 Y1 C2 O1 -77.3(10) . . . . ?
N4 Y1 C2 O1 -163.6(6) . . . . ?
N3 Y1 C2 O1 126.2(6) . . . . ?
N1 Y1 C2 O1 -83.7(6) . . . . ?
C27 Y1 C2 O1 49.4(7) . . . . ?
Y3 Y1 C2 O1 20.6(5) . . . . ?
O2 Y1 C2 C3 -78.6(8) . . . . ?
N2 Y1 C2 C3 162.7(8) . . . . ?
O1 Y1 C2 C3 -120.1(11) . . . . ?
N4 Y1 C2 C3 76.3(9) . . . . ?
N3 Y1 C2 C3 6.1(9) . . . . ?
N1 Y1 C2 C3 156.3(9) . . . . ?
C27 Y1 C2 C3 -70.7(9) . . . . ?
Y3 Y1 C2 C3 -99.5(9) . . . . ?
O2 Y1 C2 C1 162.7(8) . . . . ?
N2 Y1 C2 C1 43.9(13) . . . . ?
O1 Y1 C2 C1 121.2(10) . . . . ?
N4 Y1 C2 C1 -42.4(8) . . . . ?
N3 Y1 C2 C1 -112.6(8) . . . . ?
N1 Y1 C2 C1 37.5(8) . . . . ?
C27 Y1 C2 C1 170.6(7) . . . . ?
Y3 Y1 C2 C1 141.7(8) . . . . ?
O1 C2 C3 C4 -169.7(11) . . . . ?
C1 C2 C3 C4 0.8(17) . . . . ?
Y1 C2 C3 C4 -104.9(12) . . . . ?
C2 C3 C4 C5 2(2) . . . . ?
C3 C4 C5 C6 -2(2) . . . . ?
C3 C4 C5 C10 175.4(13) . . . . ?
C11 C1 C6 C5 -170.6(12) . . . . ?
C2 C1 C6 C5 4.1(19) . . . . ?
C11 C1 C6 C7 10.9(19) . . . . ?
C2 C1 C6 C7 -174.5(11) . . . . ?
C4 C5 C6 C1 -1.2(19) . . . . ?
C10 C5 C6 C1 -178.5(13) . . . . ?
C4 C5 C6 C7 177.3(13) . . . . ?
C10 C5 C6 C7 0.1(19) . . . . ?
C1 C6 C7 C8 166.4(13) . . . . ?
C5 C6 C7 C8 -12.2(19) . . . . ?
C6 C7 C8 C9 45.9(18) . . . . ?
C7 C8 C9 C10 -65.3(17) . . . . ?
C4 C5 C10 C9 161.9(14) . . . . ?
C6 C5 C10 C9 -21(2) . . . . ?
C8 C9 C10 C5 52.4(18) . . . . ?
C6 C1 C11 C16 68.2(17) . . . . ?
C2 C1 C11 C16 -106.6(14) . . . . ?
C6 C1 C11 C12 -111.6(15) . . . . ?
C2 C1 C11 C12 73.6(16) . . . . ?
C21 N1 C12 C13 -27.8(18) . . . . ?
Y1 N1 C12 C13 155.4(9) . . . . ?
C21 N1 C12 C11 153.0(12) . . . . ?
Y1 N1 C12 C11 -23.9(17) . . . . ?
C16 C11 C12 N1 175.8(12) . . . . ?
C1 C11 C12 N1 -4.4(19) . . . . ?
C16 C11 C12 C13 -3.5(19) . . . . ?
C1 C11 C12 C13 176.3(12) . . . . ?
N1 C12 C13 C14 178.4(12) . . . . ?
C11 C12 C13 C14 -2.3(19) . . . . ?
C12 C13 C14 C15 6(2) . . . . ?
C13 C14 C15 C16 -4(2) . . . . ?
C13 C14 C15 C20 177.1(14) . . . . ?
C14 C15 C16 C11 -3(2) . . . . ?
C20 C15 C16 C11 176.5(14) . . . . ?
C14 C15 C16 C17 173.2(13) . . . . ?
C20 C15 C16 C17 -8(2) . . . . ?
C12 C11 C16 C15 6(2) . . . . ?
C1 C11 C16 C15 -173.7(14) . . . . ?
C12 C11 C16 C17 -169.7(12) . . . . ?
C1 C11 C16 C17 10(2) . . . . ?
C15 C16 C17 C18 -6(3) . . . . ?
C11 C16 C17 C18 170(3) . . . . ?
C16 C17 C18 C19 27(5) . . . . ?
C17 C18 C19 C20 -32(6) . . . . ?
C18 C19 C20 C15 16(4) . . . . ?
C16 C15 C20 C19 3(2) . . . . ?
C14 C15 C20 C19 -177.6(17) . . . . ?
C12 N1 C21 C22 173.0(12) . . . . ?
Y1 N1 C21 C22 -9.6(16) . . . . ?
C25 N2 C22 C21 174.6(13) . . . . ?
Y1 N2 C22 C21 12.2(16) . . . . ?
C25 N2 C22 C23 0.7(17) . . . . ?
Y1 N2 C22 C23 -161.7(10) . . . . ?
N1 C21 C22 N2 -1(2) . . . . ?
N1 C21 C22 C23 171.3(15) . . . . ?
N2 C22 C23 C24 0.4(18) . . . . ?
C21 C22 C23 C24 -172.6(15) . . . . ?
C22 C23 C24 C25 -1.3(18) . . . . ?
C22 N2 C25 C24 -1.6(18) . . . . ?
Y1 N2 C25 C24 154.5(12) . . . . ?
C23 C24 C25 N2 2(2) . . . . ?
C31 C26 C27 O2 162.5(14) . . . . ?
C36 C26 C27 O2 -21(2) . . . . ?
C31 C26 C27 C28 -9(2) . . . . ?
C36 C26 C27 C28 167.4(13) . . . . ?
C31 C26 C27 Y1 114.9(13) . . . . ?
C36 C26 C27 Y1 -68.5(13) . . . . ?
Y3 O2 C27 C26 132.5(12) . . . . ?
Y1 O2 C27 C26 -74.8(14) . . . . ?
Y3 O2 C27 C28 -55.6(18) . . . . ?
Y1 O2 C27 C28 97.0(11) . . . . ?
Y3 O2 C27 Y1 -152.6(14) . . . . ?
O2 Y1 C27 C26 125.0(13) . . . . ?
N2 Y1 C27 C26 -95.0(9) . . . . ?
O1 Y1 C27 C26 130.5(9) . . . . ?
N4 Y1 C27 C26 -21.3(11) . . . . ?
N3 Y1 C27 C26 17.1(9) . . . . ?
N1 Y1 C27 C26 -150.6(8) . . . . ?
C2 Y1 C27 C26 106.9(9) . . . . ?
Y3 Y1 C27 C26 136.1(9) . . . . ?
N2 Y1 C27 O2 140.0(8) . . . . ?
O1 Y1 C27 O2 5.5(7) . . . . ?
N4 Y1 C27 O2 -146.2(7) . . . . ?
N3 Y1 C27 O2 -107.9(7) . . . . ?
N1 Y1 C27 O2 84.4(8) . . . . ?
C2 Y1 C27 O2 -18.1(8) . . . . ?
Y3 Y1 C27 O2 11.2(6) . . . . ?
O2 Y1 C27 C28 -106.8(12) . . . . ?
N2 Y1 C27 C28 33.2(10) . . . . ?
O1 Y1 C27 C28 -101.3(9) . . . . ?
N4 Y1 C27 C28 106.9(10) . . . . ?
N3 Y1 C27 C28 145.3(10) . . . . ?
N1 Y1 C27 C28 -22.4(11) . . . . ?
C2 Y1 C27 C28 -124.9(9) . . . . ?
Y3 Y1 C27 C28 -95.7(9) . . . . ?
C26 C27 C28 C29 5(2) . . . . ?
O2 C27 C28 C29 -167.6(13) . . . . ?
Y1 C27 C28 C29 -114.1(13) . . . . ?
C27 C28 C29 C30 0(3) . . . . ?
C28 C29 C30 C31 1(3) . . . . ?
C28 C29 C30 C35 176.8(17) . . . . ?
C27 C26 C31 C30 9(2) . . . . ?
C36 C26 C31 C30 -167.4(14) . . . . ?
C27 C26 C31 C32 -171.1(16) . . . . ?
C36 C26 C31 C32 12(2) . . . . ?
C29 C30 C31 C26 -5(3) . . . . ?
C35 C30 C31 C26 179.2(16) . . . . ?
C29 C30 C31 C32 175.6(19) . . . . ?
C35 C30 C31 C32 0(3) . . . . ?
C26 C31 C32 C33 157.2(18) . . . . ?
C30 C31 C32 C33 -23(3) . . . . ?
C31 C32 C33 C34 54(2) . . . . ?
C32 C33 C34 C35 -69(2) . . . . ?
C33 C34 C35 C30 46(2) . . . . ?
C29 C30 C35 C34 173.0(19) . . . . ?
C31 C30 C35 C34 -11(3) . . . . ?
C27 C26 C36 C41 -102.4(14) . . . . ?
C31 C26 C36 C41 74.4(18) . . . . ?
C27 C26 C36 C37 78.6(17) . . . . ?
C31 C26 C36 C37 -104.6(16) . . . . ?
C41 C36 C37 C38 4.2(19) . . . . ?
C26 C36 C37 C38 -176.8(12) . . . . ?
C41 C36 C37 N3 179.7(11) . . . . ?
C26 C36 C37 N3 -1.3(18) . . . . ?
C46 N3 C37 C38 -44.2(17) . . . . ?
Y1 N3 C37 C38 119.9(12) . . . . ?
C46 N3 C37 C36 140.2(13) . . . . ?
Y1 N3 C37 C36 -55.6(15) . . . . ?
C36 C37 C38 C39 -5(2) . . . . ?
N3 C37 C38 C39 -179.9(12) . . . . ?
C37 C38 C39 C40 2(2) . . . . ?
C38 C39 C40 C41 1(2) . . . . ?
C38 C39 C40 C45 -177.3(13) . . . . ?
C37 C36 C41 C40 -1.0(19) . . . . ?
C26 C36 C41 C40 180.0(12) . . . . ?
C37 C36 C41 C42 179.8(12) . . . . ?
C26 C36 C41 C42 0.8(18) . . . . ?
C39 C40 C41 C36 -2(2) . . . . ?
C45 C40 C41 C36 176.8(14) . . . . ?
C39 C40 C41 C42 177.5(12) . . . . ?
C45 C40 C41 C42 -4(2) . . . . ?
C36 C41 C42 C43 -177(2) . . . . ?
C40 C41 C42 C43 4(3) . . . . ?
C41 C42 C43 C44 10(5) . . . . ?
C42 C43 C44 C45 -25(5) . . . . ?
C43 C44 C45 C40 23(4) . . . . ?
C39 C40 C45 C44 169.6(19) . . . . ?
C41 C40 C45 C44 -9(3) . . . . ?
C37 N3 C46 C47 167.9(13) . . . . ?
Y1 N3 C46 C47 1.7(17) . . . . ?
N3 C46 C47 C48 176.2(15) . . . . ?
N3 C46 C47 N4 0(2) . . . . ?
C50 N4 C47 C46 179.2(13) . . . . ?
Y1 N4 C47 C46 -2.0(15) . . . . ?
C50 N4 C47 C48 2.2(16) . . . . ?
Y1 N4 C47 C48 -179.0(9) . . . . ?
C46 C47 C48 C49 -175.8(16) . . . . ?
N4 C47 C48 C49 0.5(17) . . . . ?
C47 C48 C49 C50 -2.7(17) . . . . ?
C47 N4 C50 C49 -4.0(18) . . . . ?
Y1 N4 C50 C49 177.6(11) . . . . ?
C48 C49 C50 N4 4.4(19) . . . . ?
Y3 O3 C52 C53 -48(2) . . . . ?
Y2 O3 C52 C53 97.2(14) . . . . ?
Y3 O3 C52 C51 130.0(13) . . . . ?
Y2 O3 C52 C51 -84.6(15) . . . . ?
Y3 O3 C52 Y2 -145.3(14) . . . . ?
C56 C51 C52 C53 -17(2) . . . . ?
C61 C51 C52 C53 169.6(14) . . . . ?
C56 C51 C52 O3 164.6(16) . . . . ?
C61 C51 C52 O3 -9(2) . . . . ?
C56 C51 C52 Y2 113.1(15) . . . . ?
C61 C51 C52 Y2 -60.1(15) . . . . ?
O3 Y2 C52 C53 -109.9(14) . . . . ?
O4 Y2 C52 C53 -100.6(12) . . . . ?
N8 Y2 C52 C53 33.0(12) . . . . ?
N6 Y2 C52 C53 104.6(12) . . . . ?
N5 Y2 C52 C53 144.9(13) . . . . ?
N7 Y2 C52 C53 -21.8(15) . . . . ?
C77 Y2 C52 C53 -123.4(12) . . . . ?
Y3 Y2 C52 C53 -96.1(12) . . . . ?
O4 Y2 C52 O3 9.3(8) . . . . ?
N8 Y2 C52 O3 142.9(8) . . . . ?
N6 Y2 C52 O3 -145.5(7) . . . . ?
N5 Y2 C52 O3 -105.2(8) . . . . ?
N7 Y2 C52 O3 88.2(9) . . . . ?
C77 Y2 C52 O3 -13.4(9) . . . . ?
Y3 Y2 C52 O3 13.8(6) . . . . ?
O3 Y2 C52 C51 117.3(14) . . . . ?
O4 Y2 C52 C51 126.6(10) . . . . ?
N8 Y2 C52 C51 -99.8(11) . . . . ?
N6 Y2 C52 C51 -28.2(14) . . . . ?
N5 Y2 C52 C51 12.1(10) . . . . ?
N7 Y2 C52 C51 -154.6(9) . . . . ?
C77 Y2 C52 C51 103.8(11) . . . . ?
Y3 Y2 C52 C51 131.1(11) . . . . ?
O3 C52 C53 C54 -171.0(15) . . . . ?
C51 C52 C53 C54 11(2) . . . . ?
Y2 C52 C53 C54 -115.8(15) . . . . ?
C52 C53 C54 C55 1(3) . . . . ?
C53 C54 C55 C56 -6(3) . . . . ?
C53 C54 C55 C60 170(2) . . . . ?
C54 C55 C56 C51 0(3) . . . . ?
C60 C55 C56 C51 -176.9(19) . . . . ?
C54 C55 C56 C57 -178.9(18) . . . . ?
C60 C55 C56 C57 4(3) . . . . ?
C52 C51 C56 C55 12(3) . . . . ?
C61 C51 C56 C55 -175.1(16) . . . . ?
C52 C51 C56 C57 -169.6(18) . . . . ?
C61 C51 C56 C57 4(3) . . . . ?
C55 C56 C57 C58 -49(3) . . . . ?
C51 C56 C57 C58 132(2) . . . . ?
C56 C57 C58 C59 47(3) . . . . ?
C57 C58 C59 C60 1(4) . . . . ?
C56 C55 C60 C59 47(3) . . . . ?
C54 C55 C60 C59 -130(2) . . . . ?
C58 C59 C60 C55 -47(3) . . . . ?
C56 C51 C61 C62 -103.7(18) . . . . ?
C52 C51 C61 C62 70(2) . . . . ?
C56 C51 C61 C66 72(2) . . . . ?
C52 C51 C61 C66 -114.4(16) . . . . ?
C66 C61 C62 C63 4(2) . . . . ?
C51 C61 C62 C63 179.7(13) . . . . ?
C66 C61 C62 N5 -174.8(14) . . . . ?
C51 C61 C62 N5 1(2) . . . . ?
C71 N5 C62 C61 135.5(15) . . . . ?
Y2 N5 C62 C61 -59.2(17) . . . . ?
C71 N5 C62 C63 -43.1(18) . . . . ?
Y2 N5 C62 C63 122.2(12) . . . . ?
C61 C62 C63 C64 -3(2) . . . . ?
N5 C62 C63 C64 176.0(13) . . . . ?
C62 C63 C64 C65 -1(2) . . . . ?
C63 C64 C65 C66 3(2) . . . . ?
C63 C64 C65 C70 -178.3(14) . . . . ?
C62 C61 C66 C65 -2(2) . . . . ?
C51 C61 C66 C65 -178.0(13) . . . . ?
C62 C61 C66 C67 -178.2(16) . . . . ?
C51 C61 C66 C67 6(2) . . . . ?
C64 C65 C66 C61 -1(2) . . . . ?
C70 C65 C66 C61 179.6(15) . . . . ?
C64 C65 C66 C67 175.0(16) . . . . ?
C70 C65 C66 C67 -4(2) . . . . ?
C61 C66 C67 C68 -159.1(17) . . . . ?
C65 C66 C67 C68 25(2) . . . . ?
C66 C67 C68 C69 -52(2) . . . . ?
C67 C68 C69 C70 64(2) . . . . ?
C68 C69 C70 C65 -43(2) . . . . ?
C64 C65 C70 C69 -166.9(16) . . . . ?
C66 C65 C70 C69 12(2) . . . . ?
C62 N5 C71 C72 169.2(13) . . . . ?
Y2 N5 C71 C72 2.1(17) . . . . ?
N5 C71 C72 C73 173.6(16) . . . . ?
N5 C71 C72 N6 -4(2) . . . . ?
C75 N6 C72 C73 -2.8(17) . . . . ?
Y2 N6 C72 C73 -174.3(10) . . . . ?
C75 N6 C72 C71 175.6(13) . . . . ?
Y2 N6 C72 C71 4.2(16) . . . . ?
C71 C72 C73 C74 -177.4(15) . . . . ?
N6 C72 C73 C74 0.7(18) . . . . ?
C72 C73 C74 C75 1.7(18) . . . . ?
C72 N6 C75 C74 4.2(19) . . . . ?
Y2 N6 C75 C74 172.1(12) . . . . ?
C73 C74 C75 N6 -4(2) . . . . ?
C81 C76 C77 C78 -3(2) . . . . ?
C86 C76 C77 C78 175.8(13) . . . . ?
C81 C76 C77 O4 164.1(13) . . . . ?
C86 C76 C77 O4 -17(2) . . . . ?
C81 C76 C77 Y2 99.0(13) . . . . ?
C86 C76 C77 Y2 -82.3(14) . . . . ?
Y3 O4 C77 C76 157.4(11) . . . . ?
Y2 O4 C77 C76 -88.1(14) . . . . ?
Y3 O4 C77 C78 -35(2) . . . . ?
Y2 O4 C77 C78 79.5(12) . . . . ?
Y3 O4 C77 Y2 -114.5(14) . . . . ?
O3 Y2 C77 C76 159.5(9) . . . . ?
O4 Y2 C77 C76 119.7(13) . . . . ?
N8 Y2 C77 C76 38.0(15) . . . . ?
N6 Y2 C77 C76 -46.0(10) . . . . ?
N5 Y2 C77 C76 -116.8(10) . . . . ?
N7 Y2 C77 C76 35.9(9) . . . . ?
C52 Y2 C77 C76 165.6(9) . . . . ?
Y3 Y2 C77 C76 139.2(10) . . . . ?
O3 Y2 C77 C78 -77.8(10) . . . . ?
O4 Y2 C77 C78 -117.6(13) . . . . ?
N8 Y2 C77 C78 160.8(9) . . . . ?
N6 Y2 C77 C78 76.7(10) . . . . ?
N5 Y2 C77 C78 6.0(10) . . . . ?
N7 Y2 C77 C78 158.6(10) . . . . ?
C52 Y2 C77 C78 -71.6(10) . . . . ?
Y3 Y2 C77 C78 -98.1(10) . . . . ?
O3 Y2 C77 O4 39.8(7) . . . . ?
N8 Y2 C77 O4 -81.6(11) . . . . ?
N6 Y2 C77 O4 -165.7(7) . . . . ?
N5 Y2 C77 O4 123.6(7) . . . . ?
N7 Y2 C77 O4 -83.8(7) . . . . ?
C52 Y2 C77 O4 46.0(8) . . . . ?
Y3 Y2 C77 O4 19.6(6) . . . . ?
C76 C77 C78 C79 -1(2) . . . . ?
O4 C77 C78 C79 -168.6(12) . . . . ?
Y2 C77 C78 C79 -107.9(12) . . . . ?
C77 C78 C79 C80 5(2) . . . . ?
C78 C79 C80 C81 -5(2) . . . . ?
C78 C79 C80 C85 171.9(14) . . . . ?
C79 C80 C81 C76 1(2) . . . . ?
C85 C80 C81 C76 -175.7(14) . . . . ?
C79 C80 C81 C82 178.1(13) . . . . ?
C85 C80 C81 C82 1(2) . . . . ?
C77 C76 C81 C80 3(2) . . . . ?
C86 C76 C81 C80 -176.2(13) . . . . ?
C77 C76 C81 C82 -174.0(15) . . . . ?
C86 C76 C81 C82 7(2) . . . . ?
C80 C81 C82 C83 -6(2) . . . . ?
C76 C81 C82 C83 170.5(15) . . . . ?
C81 C82 C83 C84 30(3) . . . . ?
C82 C83 C84 C85 -49(3) . . . . ?
C79 C80 C85 C84 164.4(18) . . . . ?
C81 C80 C85 C84 -18(2) . . . . ?
C83 C84 C85 C80 43(3) . . . . ?
C77 C76 C86 C91 -111.7(17) . . . . ?
C81 C76 C86 C91 67.1(18) . . . . ?
C77 C76 C86 C87 72.6(19) . . . . ?
C81 C76 C86 C87 -108.6(16) . . . . ?
C96 N7 C87 C88 -36(2) . . . . ?
Y2 N7 C87 C88 149.6(11) . . . . ?
C96 N7 C87 C86 148.5(13) . . . . ?
Y2 N7 C87 C86 -26(2) . . . . ?
C91 C86 C87 C88 5(2) . . . . ?
C76 C86 C87 C88 -179.4(12) . . . . ?
C91 C86 C87 N7 -179.4(13) . . . . ?
C76 C86 C87 N7 -4(2) . . . . ?
N7 C87 C88 C89 175.4(14) . . . . ?
C86 C87 C88 C89 -9(2) . . . . ?
C87 C88 C89 C90 6(2) . . . . ?
C88 C89 C90 C91 2(2) . . . . ?
C88 C89 C90 C95 -175.2(14) . . . . ?
C89 C90 C91 C86 -7(2) . . . . ?
C95 C90 C91 C86 170.9(14) . . . . ?
C89 C90 C91 C92 170.5(15) . . . . ?
C95 C90 C91 C92 -12(2) . . . . ?
C87 C86 C91 C90 3(2) . . . . ?
C76 C86 C91 C90 -172.8(14) . . . . ?
C87 C86 C91 C92 -174.1(14) . . . . ?
C76 C86 C91 C92 10(2) . . . . ?
C90 C91 C92 C93 16(3) . . . . ?
C86 C91 C92 C93 -166.9(18) . . . . ?
C91 C92 C93 C94 0(4) . . . . ?
C92 C93 C94 C95 -21(5) . . . . ?
C93 C94 C95 C90 24(5) . . . . ?
C91 C90 C95 C94 -6(3) . . . . ?
C89 C90 C95 C94 171(2) . . . . ?
C87 N7 C96 C97 174.7(12) . . . . ?
Y2 N7 C96 C97 -9.7(16) . . . . ?
C100 N8 C97 C98 -0.8(19) . . . . ?
Y2 N8 C97 C98 -150.9(12) . . . . ?
C100 N8 C97 C96 174.3(14) . . . . ?
Y2 N8 C97 C96 24.2(16) . . . . ?
N7 C96 C97 N8 -10(2) . . . . ?
N7 C96 C97 C98 164.5(16) . . . . ?
N8 C97 C98 C99 4(2) . . . . ?
C96 C97 C98 C99 -171.1(16) . . . . ?
C97 C98 C99 C100 -5(2) . . . . ?
C97 N8 C100 C99 -2(2) . . . . ?
Y2 N8 C100 C99 139.1(14) . . . . ?
C98 C99 C100 N8 4(2) . . . . ?
Y6 O5 C108 C109 -28.4(18) . . . . ?
Y4 O5 C108 C109 85.3(11) . . . . ?
Y6 O5 C108 C107 158.6(9) . . . . ?
Y4 O5 C108 C107 -87.7(11) . . . . ?
Y6 O5 C108 Y4 -113.7(10) . . . . ?
C112 C107 C108 C109 -5.6(18) . . . . ?
C117 C107 C108 C109 170.4(12) . . . . ?
C112 C107 C108 O5 167.2(10) . . . . ?
C117 C107 C108 O5 -16.9(18) . . . . ?
C112 C107 C108 Y4 102.5(10) . . . . ?
C117 C107 C108 Y4 -81.6(12) . . . . ?
O6 Y4 C108 C109 -71.4(8) . . . . ?
O5 Y4 C108 C109 -116.4(12) . . . . ?
N11 Y4 C108 C109 171.5(8) . . . . ?
N13 Y4 C108 C109 82.2(9) . . . . ?
N12 Y4 C108 C109 12.5(9) . . . . ?
N10 Y4 C108 C109 159.8(9) . . . . ?
C133 Y4 C108 C109 -66.5(9) . . . . ?
Y6 Y4 C108 C109 -92.4(8) . . . . ?
O6 Y4 C108 O5 45.0(7) . . . . ?
N11 Y4 C108 O5 -72.1(11) . . . . ?
N13 Y4 C108 O5 -161.4(7) . . . . ?
N12 Y4 C108 O5 128.9(7) . . . . ?
N10 Y4 C108 O5 -83.8(7) . . . . ?
C133 Y4 C108 O5 49.9(7) . . . . ?
Y6 Y4 C108 O5 24.0(5) . . . . ?
O6 Y4 C108 C107 163.7(7) . . . . ?
O5 Y4 C108 C107 118.6(11) . . . . ?
N11 Y4 C108 C107 46.6(12) . . . . ?
N13 Y4 C108 C107 -42.8(8) . . . . ?
N12 Y4 C108 C107 -112.5(8) . . . . ?
N10 Y4 C108 C107 34.8(7) . . . . ?
C133 Y4 C108 C107 168.5(7) . . . . ?
Y6 Y4 C108 C107 142.6(8) . . . . ?
O5 C108 C109 C110 -169.9(12) . . . . ?
C107 C108 C109 C110 3(2) . . . . ?
Y4 C108 C109 C110 -106.8(12) . . . . ?
C108 C109 C110 C111 3(2) . . . . ?
C109 C110 C111 C112 -5.8(18) . . . . ?
C109 C110 C111 C116 175.7(12) . . . . ?
C110 C111 C112 C107 3.2(17) . . . . ?
C116 C111 C112 C107 -178.5(11) . . . . ?
C110 C111 C112 C113 179.6(11) . . . . ?
C116 C111 C112 C113 -2.1(18) . . . . ?
C108 C107 C112 C111 2.4(17) . . . . ?
C117 C107 C112 C111 -173.7(11) . . . . ?
C108 C107 C112 C113 -174.1(11) . . . . ?
C117 C107 C112 C113 9.8(17) . . . . ?
C111 C112 C113 C114 -15.3(17) . . . . ?
C107 C112 C113 C114 161.2(12) . . . . ?
C112 C113 C114 C115 47.3(16) . . . . ?
C113 C114 C115 C116 -64.8(16) . . . . ?
C110 C111 C116 C115 165.4(12) . . . . ?
C112 C111 C116 C115 -12.9(17) . . . . ?
C114 C115 C116 C111 46.1(16) . . . . ?
C108 C107 C117 C122 -109.8(15) . . . . ?
C112 C107 C117 C122 66.1(16) . . . . ?
C108 C107 C117 C118 71.3(16) . . . . ?
C112 C107 C117 C118 -112.9(13) . . . . ?
C127 N10 C118 C119 -27.9(16) . . . . ?
Y4 N10 C118 C119 151.3(9) . . . . ?
C127 N10 C118 C117 158.5(12) . . . . ?
Y4 N10 C118 C117 -22.3(16) . . . . ?
C122 C117 C118 C119 3.4(19) . . . . ?
C107 C117 C118 C119 -177.6(11) . . . . ?
C122 C117 C118 N10 177.1(12) . . . . ?
C107 C117 C118 N10 -4.0(17) . . . . ?
N10 C118 C119 C120 176.6(11) . . . . ?
C117 C118 C119 C120 -9.8(18) . . . . ?
C118 C119 C120 C121 9(2) . . . . ?
C119 C120 C121 C122 -2(2) . . . . ?
C119 C120 C121 C126 180.0(14) . . . . ?
C118 C117 C122 C121 4(2) . . . . ?
C107 C117 C122 C121 -175.2(12) . . . . ?
C118 C117 C122 C123 -173.3(12) . . . . ?
C107 C117 C122 C123 8(2) . . . . ?
C120 C121 C122 C117 -4(2) . . . . ?
C126 C121 C122 C117 173.3(15) . . . . ?
C120 C121 C122 C123 172.8(14) . . . . ?
C126 C121 C122 C123 -9(2) . . . . ?
C117 C122 C123 C124 -163(2) . . . . ?
C121 C122 C123 C124 20(2) . . . . ?
C122 C123 C124 C125 -43(3) . . . . ?
C123 C124 C125 C126 56(4) . . . . ?
C124 C125 C126 C121 -44(3) . . . . ?
C120 C121 C126 C125 -158.7(19) . . . . ?
C122 C121 C126 C125 24(3) . . . . ?
C118 N10 C127 C128 170.2(12) . . . . ?
Y4 N10 C127 C128 -9.3(16) . . . . ?
C131 N11 C128 C127 177.3(13) . . . . ?
Y4 N11 C128 C127 12.2(16) . . . . ?
C131 N11 C128 C129 -2.3(16) . . . . ?
Y4 N11 C128 C129 -167.4(10) . . . . ?
N10 C127 C128 N11 -2(2) . . . . ?
N10 C127 C128 C129 177.8(15) . . . . ?
N11 C128 C129 C130 2.1(19) . . . . ?
C127 C128 C129 C130 -177.5(16) . . . . ?
C128 C129 C130 C131 -1(2) . . . . ?
C128 N11 C131 C130 1.7(17) . . . . ?
Y4 N11 C131 C130 159.0(12) . . . . ?
C129 C130 C131 N11 0(2) . . . . ?
Y6 O6 C133 C132 134.6(10) . . . . ?
Y4 O6 C133 C132 -81.6(11) . . . . ?
Y6 O6 C133 C134 -47.0(16) . . . . ?
Y4 O6 C133 C134 96.8(9) . . . . ?
Y6 O6 C133 Y4 -143.8(12) . . . . ?
C137 C132 C133 O6 165.9(11) . . . . ?
C142 C132 C133 O6 -13.1(16) . . . . ?
C137 C132 C133 C134 -12.4(16) . . . . ?
C142 C132 C133 C134 168.5(11) . . . . ?
C137 C132 C133 Y4 116.1(10) . . . . ?
C142 C132 C133 Y4 -63.0(11) . . . . ?
O5 Y4 C133 O6 13.0(7) . . . . ?
N11 Y4 C133 O6 145.1(7) . . . . ?
N13 Y4 C133 O6 -141.4(7) . . . . ?
N12 Y4 C133 O6 -102.5(7) . . . . ?
N10 Y4 C133 O6 91.3(8) . . . . ?
C108 Y4 C133 O6 -10.8(8) . . . . ?
Y6 Y4 C133 O6 15.6(6) . . . . ?
O6 Y4 C133 C132 119.4(12) . . . . ?
O5 Y4 C133 C132 132.4(8) . . . . ?
N11 Y4 C133 C132 -95.5(9) . . . . ?
N13 Y4 C133 C132 -22.0(11) . . . . ?
N12 Y4 C133 C132 16.9(8) . . . . ?
N10 Y4 C133 C132 -149.4(8) . . . . ?
C108 Y4 C133 C132 108.6(8) . . . . ?
Y6 Y4 C133 C132 135.0(9) . . . . ?
O6 Y4 C133 C134 -108.7(12) . . . . ?
O5 Y4 C133 C134 -95.7(9) . . . . ?
N11 Y4 C133 C134 36.4(9) . . . . ?
N13 Y4 C133 C134 109.9(9) . . . . ?
N12 Y4 C133 C134 148.8(9) . . . . ?
N10 Y4 C133 C134 -17.4(11) . . . . ?
C108 Y4 C133 C134 -119.5(9) . . . . ?
Y6 Y4 C133 C134 -93.1(9) . . . . ?
O6 C133 C134 C135 -173.8(11) . . . . ?
C132 C133 C134 C135 4.6(17) . . . . ?
Y4 C133 C134 C135 -119.7(12) . . . . ?
C133 C134 C135 C136 3(2) . . . . ?
C134 C135 C136 C137 -2(2) . . . . ?
C134 C135 C136 C141 171.6(15) . . . . ?
C135 C136 C137 C132 -6(2) . . . . ?
C141 C136 C137 C132 -179.8(15) . . . . ?
C135 C136 C137 C138 -176.8(14) . . . . ?
C141 C136 C137 C138 9(2) . . . . ?
C133 C132 C137 C136 13(2) . . . . ?
C142 C132 C137 C136 -167.9(13) . . . . ?
C133 C132 C137 C138 -175.6(12) . . . . ?
C142 C132 C137 C138 3.4(19) . . . . ?
C136 C137 C138 C139 -22(2) . . . . ?
C132 C137 C138 C139 167.0(14) . . . . ?
C137 C138 C139 C140 47(2) . . . . ?
C138 C139 C140 C141 -60(2) . . . . ?
C139 C140 C141 C136 48(2) . . . . ?
C135 C136 C141 C140 164.7(16) . . . . ?
C137 C136 C141 C140 -21(3) . . . . ?
C137 C132 C142 C143 -108.1(16) . . . . ?
C133 C132 C142 C143 70.8(16) . . . . ?
C137 C132 C142 C147 73.0(16) . . . . ?
C133 C132 C142 C147 -108.0(13) . . . . ?
C147 C142 C143 C144 0.3(17) . . . . ?
C132 C142 C143 C144 -178.5(12) . . . . ?
C147 C142 C143 N12 178.7(10) . . . . ?
C132 C142 C143 N12 -0.1(18) . . . . ?
C152 N12 C143 C142 145.8(12) . . . . ?
Y4 N12 C143 C142 -52.7(14) . . . . ?
C152 N12 C143 C144 -35.8(16) . . . . ?
Y4 N12 C143 C144 125.7(10) . . . . ?
C142 C143 C144 C145 -3.1(19) . . . . ?
N12 C143 C144 C145 178.6(11) . . . . ?
C143 C144 C145 C146 3(2) . . . . ?
C144 C145 C146 C147 -1(2) . . . . ?
C144 C145 C146 C151 172.1(13) . . . . ?
C145 C146 C147 C142 -2.0(19) . . . . ?
C151 C146 C147 C142 -175.5(12) . . . . ?
C145 C146 C147 C148 176.5(12) . . . . ?
C151 C146 C147 C148 3.0(18) . . . . ?
C143 C142 C147 C146 2.3(18) . . . . ?
C132 C142 C147 C146 -178.8(12) . . . . ?
C143 C142 C147 C148 -176.1(11) . . . . ?
C132 C142 C147 C148 2.8(17) . . . . ?
C146 C147 C148 C149 45.7(16) . . . . ?
C142 C147 C148 C149 -135.9(13) . . . . ?
C147 C148 C149 C150 -51.8(19) . . . . ?
C148 C149 C150 C151 9(3) . . . . ?
C149 C150 C151 C146 39(2) . . . . ?
C145 C146 C151 C150 139.9(17) . . . . ?
C147 C146 C151 C150 -47.1(19) . . . . ?
C143 N12 C152 C153 171.7(12) . . . . ?
Y4 N12 C152 C153 8.0(16) . . . . ?
N12 C152 C153 N13 1(2) . . . . ?
N12 C152 C153 C154 173.9(14) . . . . ?
C156 N13 C153 C152 177.0(12) . . . . ?
Y4 N13 C153 C152 -9.9(15) . . . . ?
C156 N13 C153 C154 2.8(15) . . . . ?
Y4 N13 C153 C154 175.9(9) . . . . ?
C152 C153 C154 C155 -176.5(15) . . . . ?
N13 C153 C154 C155 -3.3(16) . . . . ?
C153 C154 C155 C156 2.5(16) . . . . ?
C153 N13 C156 C155 -1.1(16) . . . . ?
Y4 N13 C156 C155 -171.5(10) . . . . ?
C154 C155 C156 N13 -0.9(17) . . . . ?
C162 C157 C158 O7 167.5(12) . . . . ?
C167 C157 C158 O7 -15(2) . . . . ?
C162 C157 C158 C159 -6(2) . . . . ?
C167 C157 C158 C159 171.2(14) . . . . ?
C162 C157 C158 Y5 102.3(13) . . . . ?
C167 C157 C158 Y5 -80.3(14) . . . . ?
Y6 O7 C158 C157 154.3(11) . . . . ?
Y5 O7 C158 C157 -89.4(13) . . . . ?
Y6 O7 C158 C159 -31.7(19) . . . . ?
Y5 O7 C158 C159 84.6(11) . . . . ?
Y6 O7 C158 Y5 -116.3(12) . . . . ?
O7 Y5 C158 C157 119.8(13) . . . . ?
O8 Y5 C158 C157 159.3(9) . . . . ?
N15 Y5 C158 C157 41.9(14) . . . . ?
N17 Y5 C158 C157 -46.8(10) . . . . ?
N14 Y5 C158 C157 34.6(9) . . . . ?
N16 Y5 C158 C157 -117.0(9) . . . . ?
C183 Y5 C158 C157 165.5(9) . . . . ?
Y6 Y5 C158 C157 140.5(10) . . . . ?
O8 Y5 C158 O7 39.4(7) . . . . ?
N15 Y5 C158 O7 -77.9(11) . . . . ?
N17 Y5 C158 O7 -166.6(7) . . . . ?
N14 Y5 C158 O7 -85.3(7) . . . . ?
N16 Y5 C158 O7 123.2(7) . . . . ?
C183 Y5 C158 O7 45.7(8) . . . . ?
Y6 Y5 C158 O7 20.6(5) . . . . ?
O7 Y5 C158 C159 -115.7(13) . . . . ?
O8 Y5 C158 C159 -76.2(9) . . . . ?
N15 Y5 C158 C159 166.4(9) . . . . ?
N17 Y5 C158 C159 77.7(9) . . . . ?
N14 Y5 C158 C159 159.1(10) . . . . ?
N16 Y5 C158 C159 7.5(10) . . . . ?
C183 Y5 C158 C159 -70.0(10) . . . . ?
Y6 Y5 C158 C159 -95.0(9) . . . . ?
C157 C158 C159 C160 7(2) . . . . ?
O7 C158 C159 C160 -167.1(12) . . . . ?
Y5 C158 C159 C160 -105.0(13) . . . . ?
C158 C159 C160 C161 -5(2) . . . . ?
C159 C160 C161 C162 3(2) . . . . ?
C159 C160 C161 C166 176.8(15) . . . . ?
C160 C161 C162 C157 -1(2) . . . . ?
C166 C161 C162 C157 -175.6(14) . . . . ?
C160 C161 C162 C163 174.1(15) . . . . ?
C166 C161 C162 C163 0(2) . . . . ?
C158 C157 C162 C161 3(2) . . . . ?
C167 C157 C162 C161 -174.2(14) . . . . ?
C158 C157 C162 C163 -172.4(14) . . . . ?
C167 C157 C162 C163 10(2) . . . . ?
C161 C162 C163 C164 11(2) . . . . ?
C157 C162 C163 C164 -173.4(15) . . . . ?
C162 C163 C164 C165 -38(3) . . . . ?
C163 C164 C165 C166 51(4) . . . . ?
C164 C165 C166 C161 -35(3) . . . . ?
C160 C161 C166 C165 -163(2) . . . . ?
C162 C161 C166 C165 11(3) . . . . ?
C158 C157 C167 C172 -108.8(16) . . . . ?
C162 C157 C167 C172 68.6(18) . . . . ?
C158 C157 C167 C168 70.2(18) . . . . ?
C162 C157 C167 C168 -112.4(15) . . . . ?
C172 C167 C168 C169 -1.7(19) . . . . ?
C157 C167 C168 C169 179.3(11) . . . . ?
C172 C167 C168 N14 175.1(11) . . . . ?
C157 C167 C168 N14 -3.8(18) . . . . ?
C177 N14 C168 C167 153.2(12) . . . . ?
Y5 N14 C168 C167 -24.2(16) . . . . ?
C177 N14 C168 C169 -29.9(16) . . . . ?
Y5 N14 C168 C169 152.6(9) . . . . ?
C167 C168 C169 C170 -2.4(18) . . . . ?
N14 C168 C169 C170 -179.3(12) . . . . ?
C168 C169 C170 C171 2(2) . . . . ?
C169 C170 C171 C172 2(2) . . . . ?
C169 C170 C171 C176 178.1(15) . . . . ?
C170 C171 C172 C167 -6(2) . . . . ?
C176 C171 C172 C167 177.5(14) . . . . ?
C170 C171 C172 C173 174.3(14) . . . . ?
C176 C171 C172 C173 -2(2) . . . . ?
C168 C167 C172 C171 6(2) . . . . ?
C157 C167 C172 C171 -174.8(13) . . . . ?
C168 C167 C172 C173 -174.2(13) . . . . ?
C157 C167 C172 C173 5(2) . . . . ?
C171 C172 C173 C174 15(3) . . . . ?
C167 C172 C173 C174 -164(2) . . . . ?
C172 C173 C174 C175 1(4) . . . . ?
C173 C174 C175 C176 -28(4) . . . . ?
C174 C175 C176 C171 40(2) . . . . ?
C172 C171 C176 C175 -25(2) . . . . ?
C170 C171 C176 C175 158.6(15) . . . . ?
C168 N14 C177 C178 175.3(12) . . . . ?
Y5 N14 C177 C178 -6.6(15) . . . . ?
N14 C177 C178 N15 -13(2) . . . . ?
N14 C177 C178 C179 175.0(16) . . . . ?
C181 N15 C178 C177 -179.7(13) . . . . ?
Y5 N15 C178 C177 25.5(15) . . . . ?
C181 N15 C178 C179 -5.9(17) . . . . ?
Y5 N15 C178 C179 -160.6(10) . . . . ?
C177 C178 C179 C180 176.9(16) . . . . ?
N15 C178 C179 C180 4.2(19) . . . . ?
C178 C179 C180 C181 -1(2) . . . . ?
C178 N15 C181 C180 5.5(18) . . . . ?
Y5 N15 C181 C180 150.5(12) . . . . ?
C179 C180 C181 N15 -3(2) . . . . ?
C187 C182 C183 O8 166.3(12) . . . . ?
C192 C182 C183 O8 -21.1(19) . . . . ?
C187 C182 C183 C184 -7(2) . . . . ?
C192 C182 C183 C184 165.2(12) . . . . ?
C187 C182 C183 Y5 119.1(11) . . . . ?
C192 C182 C183 Y5 -68.3(11) . . . . ?
Y6 O8 C183 C182 130.9(12) . . . . ?
Y5 O8 C183 C182 -76.6(13) . . . . ?
Y6 O8 C183 C184 -55.3(18) . . . . ?
Y5 O8 C183 C184 97.2(11) . . . . ?
Y6 O8 C183 Y5 -152.5(14) . . . . ?
O7 Y5 C183 C182 131.5(9) . . . . ?
O8 Y5 C183 C182 123.7(12) . . . . ?
N15 Y5 C183 C182 -95.9(9) . . . . ?
N17 Y5 C183 C182 -20.3(11) . . . . ?
N14 Y5 C183 C182 -149.8(8) . . . . ?
N16 Y5 C183 C182 18.9(8) . . . . ?
C158 Y5 C183 C182 109.3(9) . . . . ?
Y6 Y5 C183 C182 135.1(9) . . . . ?
O7 Y5 C183 O8 7.8(7) . . . . ?
N15 Y5 C183 O8 140.4(8) . . . . ?
N17 Y5 C183 O8 -143.9(8) . . . . ?
N14 Y5 C183 O8 86.5(8) . . . . ?
N16 Y5 C183 O8 -104.7(8) . . . . ?
C158 Y5 C183 O8 -14.4(9) . . . . ?
Y6 Y5 C183 O8 11.4(6) . . . . ?
O7 Y5 C183 C184 -98.5(10) . . . . ?
O8 Y5 C183 C184 -106.3(13) . . . . ?
N15 Y5 C183 C184 34.1(9) . . . . ?
N17 Y5 C183 C184 109.8(10) . . . . ?
N14 Y5 C183 C184 -19.7(12) . . . . ?
N16 Y5 C183 C184 149.0(10) . . . . ?
C158 Y5 C183 C184 -120.7(9) . . . . ?
Y6 Y5 C183 C184 -94.8(10) . . . . ?
C182 C183 C184 C185 3(2) . . . . ?
O8 C183 C184 C185 -170.9(12) . . . . ?
Y5 C183 C184 C185 -118.7(12) . . . . ?
C183 C184 C185 C186 2(2) . . . . ?
C184 C185 C186 C187 -3(2) . . . . ?
C184 C185 C186 C191 176.1(13) . . . . ?
C185 C186 C187 C182 -1(2) . . . . ?
C191 C186 C187 C182 180.0(13) . . . . ?
C185 C186 C187 C188 179.3(13) . . . . ?
C191 C186 C187 C188 0(2) . . . . ?
C183 C182 C187 C186 6(2) . . . . ?
C192 C182 C187 C186 -166.1(13) . . . . ?
C183 C182 C187 C188 -174.0(13) . . . . ?
C192 C182 C187 C188 13.5(19) . . . . ?
C186 C187 C188 C189 -7(2) . . . . ?
C182 C187 C188 C189 173.0(15) . . . . ?
C187 C188 C189 C190 31(3) . . . . ?
C188 C189 C190 C191 -47(4) . . . . ?
C189 C190 C191 C186 37(3) . . . . ?
C185 C186 C191 C190 167(2) . . . . ?
C187 C186 C191 C190 -14(3) . . . . ?
C183 C182 C192 C197 -105.3(15) . . . . ?
C187 C182 C192 C197 67.5(16) . . . . ?
C183 C182 C192 C193 76.2(15) . . . . ?
C187 C182 C192 C193 -111.0(14) . . . . ?
C202 N16 C193 C192 147.9(13) . . . . ?
Y5 N16 C193 C192 -51.8(16) . . . . ?
C202 N16 C193 C194 -31.9(18) . . . . ?
Y5 N16 C193 C194 128.4(11) . . . . ?
C197 C192 C193 N16 179.9(12) . . . . ?
C182 C192 C193 N16 -1.6(18) . . . . ?
C197 C192 C193 C194 -0.2(18) . . . . ?
C182 C192 C193 C194 178.2(11) . . . . ?
N16 C193 C194 C195 177.6(12) . . . . ?
C192 C193 C194 C195 -2.2(18) . . . . ?
C193 C194 C195 C196 1(2) . . . . ?
C194 C195 C196 C197 2.5(19) . . . . ?
C194 C195 C196 C201 178.5(13) . . . . ?
C195 C196 C197 C192 -5(2) . . . . ?
C201 C196 C197 C192 179.0(13) . . . . ?
C195 C196 C197 C198 173.8(12) . . . . ?
C201 C196 C197 C198 -2(2) . . . . ?
C193 C192 C197 C196 4(2) . . . . ?
C182 C192 C197 C196 -174.6(12) . . . . ?
C193 C192 C197 C198 -174.9(12) . . . . ?
C182 C192 C197 C198 6.7(19) . . . . ?
C196 C197 C198 C199 35(2) . . . . ?
C192 C197 C198 C199 -146.7(19) . . . . ?
C197 C198 C199 C200 -17(3) . . . . ?
C198 C199 C200 C201 -27(3) . . . . ?
C197 C196 C201 C200 -42.9(19) . . . . ?
C195 C196 C201 C200 141.1(14) . . . . ?
C199 C200 C201 C196 56(2) . . . . ?
C193 N16 C202 C203 176.1(13) . . . . ?
Y5 N16 C202 C203 13.0(16) . . . . ?
N16 C202 C203 C204 175.5(15) . . . . ?
N16 C202 C203 N17 -6(2) . . . . ?
C206 N17 C203 C204 -0.9(17) . . . . ?
Y5 N17 C203 C204 174.1(10) . . . . ?
C206 N17 C203 C202 -179.3(13) . . . . ?
Y5 N17 C203 C202 -4.3(16) . . . . ?
C202 C203 C204 C205 -177.6(15) . . . . ?
N17 C203 C204 C205 4.2(18) . . . . ?
C203 C204 C205 C206 -5.7(18) . . . . ?
C203 N17 C206 C205 -3.0(18) . . . . ?
Y5 N17 C206 C205 -175.7(12) . . . . ?
C204 C205 C206 N17 6(2) . . . . ?
C219 C214 C215 C216 0.0 . . . . ?
C213 C214 C215 C216 180.0(16) . . . . ?
C214 C215 C216 C217 0.0 . . . . ?
C215 C216 C217 C218 0.0 . . . . ?
C216 C217 C218 C219 0.0 . . . . ?
C217 C218 C219 C214 0.0 . . . . ?
C215 C214 C219 C218 0.0 . . . . ?
C213 C214 C219 C218 -180.0(16) . . . . ?
C226 C221 C222 C223 0.0 . . . . ?
C220 C221 C222 C223 -178.4(15) . . . . ?
C221 C222 C223 C224 0.0 . . . . ?
C222 C223 C224 C225 0.0 . . . . ?
C223 C224 C225 C226 0.0 . . . . ?
C224 C225 C226 C221 0.0 . . . . ?
C222 C221 C226 C225 0.0 . . . . ?
C220 C221 C226 C225 178.4(14) . . . . ?
C233 C228 C229 C230 0.0 . . . . ?
C227 C228 C229 C230 176.0(14) . . . . ?
C228 C229 C230 C231 0.0 . . . . ?
C229 C230 C231 C232 0.0 . . . . ?
C230 C231 C232 C233 0.0 . . . . ?
C231 C232 C233 C228 0.0 . . . . ?
C229 C228 C233 C232 0.0 . . . . ?
C227 C228 C233 C232 -175.3(17) . . . . ?
