#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:58:59 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179087 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/49/4304944.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4304944
loop_
_publ_author_name
'Vito Gallo'
'Mario Latronico'
'Piero Mastrorilli'
'Cosimo F. Nobile'
'Flavia Polini'
'Nazzareno Re'
'Ulli Englert'
_publ_contact_author_address
;
      Institut fuer Anorganische Chemie
      RWTH Aachen
      Landoltweg 1
      52074 Aachen
      Germany
;
_publ_contact_author_email       ullrich.englert@ac.rwth-aachen.de
_publ_contact_author_fax         0049-241-8092288
_publ_contact_author_name        'Ulli Englert'
_publ_contact_author_phone       0049-241-8094666
_publ_section_title
;
Reactivity of a Phosphinito-Bridged PtI-PtI Complex with Nucleophiles:
Substitution versus Addition
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4785
_journal_page_last               4795
_journal_paper_doi               10.1021/ic800045u
_journal_volume                  47
_journal_year                    2008
_chemical_formula_moiety         'C48 H90 O P4 Pt2'
_chemical_formula_sum            'C48 H90 O P4 Pt2'
_chemical_formula_weight         1197.26
_chemical_name_common            'compound 1'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 125.31(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.548(10)
_cell_length_b                   19.811(14)
_cell_length_c                   21.225(12)
_cell_measurement_reflns_used    6357
_cell_measurement_temperature    130(2)
_cell_measurement_theta_max      26.83
_cell_measurement_theta_min      2.20
_cell_volume                     4992(6)
_computing_cell_refinement       SMART
_computing_data_collection       'SMART (Bruker, 2001)'
_computing_data_reduction        'SAINT (Bruker, 1999)'
_computing_molecular_graphics    'PLATON (Spek, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      130(2)
_diffrn_measured_fraction_theta_full .972
_diffrn_measured_fraction_theta_max .972
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0596
_diffrn_reflns_av_sigmaI/netI    0.0496
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            67284
_diffrn_reflns_theta_full        29.16
_diffrn_reflns_theta_max         29.16
_diffrn_reflns_theta_min         2.00
_exptl_absorpt_coefficient_mu    5.760
_exptl_absorpt_correction_T_max  0.44
_exptl_absorpt_correction_T_min  0.30
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (1996)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.593
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2408
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.17
_refine_diff_density_max         4.936
_refine_diff_density_min         -3.938
_refine_diff_density_rms         .169
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.027
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     541
_refine_ls_number_reflns         13077
_refine_ls_number_restraints     58
_refine_ls_restrained_S_all      1.026
_refine_ls_R_factor_all          0.0572
_refine_ls_R_factor_gt           0.0396
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0330P)²+19.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0855
_refine_ls_wR_factor_ref         0.0938
_reflns_number_gt                10406
_reflns_number_total             13077
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic800045u-file002_2.cif
_cod_data_source_block           comp1
_cod_database_code               4304944
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.241868(19) 0.278321(9) 0.267527(11) 0.03251(6) Uani 1 1 d . . .
Pt2 Pt 0.165885(15) 0.157045(8) 0.228675(9) 0.02119(5) Uani 1 1 d . . .
P1 P 0.03007(11) 0.23167(6) 0.14360(7) 0.0238(2) Uani 1 1 d . . .
P2 P 0.34665(12) 0.18764(7) 0.32515(7) 0.0305(3) Uani 1 1 d . A .
P3 P 0.11612(10) 0.04780(6) 0.21786(7) 0.0217(2) Uani 1 1 d . . .
H3 H 0.0330 0.0459 0.1777 0.026 Uiso 1 1 calc R . .
P4 P 0.32330(12) 0.37923(7) 0.31230(8) 0.0320(3) Uani 1 1 d . . .
H4 H 0.4041 0.3735 0.3320 0.038 Uiso 1 1 calc R . .
O1 O 0.0712(3) 0.30523(17) 0.1715(2) 0.0344(8) Uani 1 1 d . . .
C1 C -0.1079(5) 0.2270(2) 0.1272(3) 0.0305(11) Uani 1 1 d . . .
H1 H -0.1574 0.2621 0.0880 0.037 Uiso 1 1 calc R . .
C2 C -0.1656(5) 0.1591(3) 0.0965(4) 0.0410(13) Uani 1 1 d . . .
H2A H -0.1158 0.1231 0.1327 0.049 Uiso 1 1 calc R . .
H2B H -0.1786 0.1504 0.0460 0.049 Uiso 1 1 calc R . .
C3 C -0.2781(6) 0.1572(3) 0.0870(5) 0.060(2) Uani 1 1 d . . .
H3A H -0.3309 0.1894 0.0462 0.072 Uiso 1 1 calc R . .
H3B H -0.3110 0.1114 0.0704 0.072 Uiso 1 1 calc R . .
C4 C -0.2642(7) 0.1748(4) 0.1608(6) 0.073(2) Uani 1 1 d . . .
H4A H -0.2186 0.1396 0.1999 0.087 Uiso 1 1 calc R . .
H4B H -0.3391 0.1760 0.1516 0.087 Uiso 1 1 calc R . .
C5 C -0.2075(7) 0.2425(4) 0.1912(5) 0.062(2) Uani 1 1 d . . .
H5A H -0.1962 0.2516 0.2411 0.075 Uiso 1 1 calc R . .
H5B H -0.2570 0.2783 0.1545 0.075 Uiso 1 1 calc R . .
C6 C -0.0940(6) 0.2449(3) 0.2025(4) 0.0439(14) Uani 1 1 d . . .
H6A H -0.0415 0.2126 0.2434 0.053 Uiso 1 1 calc R . .
H6B H -0.0614 0.2907 0.2193 0.053 Uiso 1 1 calc R . .
C7 C -0.0038(4) 0.2274(2) 0.0458(3) 0.0291(11) Uani 1 1 d . . .
H7 H -0.0466 0.1847 0.0213 0.035 Uiso 1 1 calc R . .
C8 C 0.1037(5) 0.2239(3) 0.0500(3) 0.0383(13) Uani 1 1 d . . .
H8A H 0.1456 0.1825 0.0781 0.046 Uiso 1 1 calc R . .
H8B H 0.1517 0.2632 0.0795 0.046 Uiso 1 1 calc R . .
C9 C 0.0809(6) 0.2235(4) -0.0299(4) 0.0495(16) Uani 1 1 d . . .
H9A H 0.1534 0.2240 -0.0243 0.059 Uiso 1 1 calc R . .
H9B H 0.0404 0.1815 -0.0574 0.059 Uiso 1 1 calc R . .
C10 C 0.0123(9) 0.2829(4) -0.0763(5) 0.076(3) Uani 1 1 d . . .
H10A H -0.0025 0.2810 -0.1280 0.092 Uiso 1 1 calc R . .
H10B H 0.0546 0.3249 -0.0505 0.092 Uiso 1 1 calc R . .
C11 C -0.0984(8) 0.2837(5) -0.0846(4) 0.088(3) Uani 1 1 d . . .
H11A H -0.1422 0.2427 -0.1126 0.106 Uiso 1 1 calc R . .
H11B H -0.1430 0.3235 -0.1152 0.106 Uiso 1 1 calc R . .
C12 C -0.0776(8) 0.2861(4) -0.0048(4) 0.074(3) Uani 1 1 d . . .
H12A H -0.0404 0.3292 0.0209 0.088 Uiso 1 1 calc R . .
H12B H -0.1507 0.2842 -0.0114 0.088 Uiso 1 1 calc R . .
C13 C 0.4123(5) 0.1759(3) 0.4292(3) 0.0317(11) Uani 1 1 d . . .
H13 H 0.4689 0.2127 0.4579 0.038 Uiso 1 1 calc R . .
C14 C 0.4728(5) 0.1088(3) 0.4592(3) 0.0377(12) Uani 1 1 d . . .
H14A H 0.5347 0.1068 0.4525 0.045 Uiso 1 1 calc R . .
H14B H 0.4195 0.0718 0.4284 0.045 Uiso 1 1 calc R . .
C15 C 0.5214(5) 0.0980(4) 0.5445(3) 0.0504(16) Uani 1 1 d . . .
H15A H 0.5556 0.0525 0.5609 0.060 Uiso 1 1 calc R . .
H15B H 0.5810 0.1318 0.5763 0.060 Uiso 1 1 calc R . .
C16 C 0.4287(6) 0.1048(4) 0.5570(4) 0.062(2) Uani 1 1 d . . .
H16A H 0.3727 0.0684 0.5288 0.075 Uiso 1 1 calc R . .
H16B H 0.4616 0.0997 0.6127 0.075 Uiso 1 1 calc R . .
C17 C 0.3705(6) 0.1726(4) 0.5292(4) 0.0595(19) Uani 1 1 d . . .
H17A H 0.4252 0.2090 0.5603 0.071 Uiso 1 1 calc R . .
H17B H 0.3093 0.1750 0.5366 0.071 Uiso 1 1 calc R . .
C18 C 0.3215(5) 0.1834(3) 0.4440(3) 0.0388(13) Uani 1 1 d . . .
H18A H 0.2879 0.2290 0.4280 0.047 Uiso 1 1 calc R . .
H18B H 0.2610 0.1500 0.4124 0.047 Uiso 1 1 calc R . .
C19 C 0.4596(5) 0.1703(4) 0.3137(3) 0.058(2) Uani 1 1 d DU . .
H19 H 0.4834 0.1245 0.3306 0.070 Uiso 1 1 d R A .
C20A C 0.5845(6) 0.1981(5) 0.3640(6) 0.033(2) Uani 0.50 1 d PDU A 1
H20A H 0.6123 0.2037 0.4187 0.039 Uiso 0.50 1 calc PR A 1
H20B H 0.6360 0.1678 0.3612 0.039 Uiso 0.50 1 calc PR A 1
C21A C 0.5728(9) 0.2651(5) 0.3268(6) 0.037(2) Uani 0.50 1 d PDU A 1
H21A H 0.6465 0.2885 0.3562 0.044 Uiso 0.50 1 calc PR A 1
H21B H 0.5185 0.2935 0.3288 0.044 Uiso 0.50 1 calc PR A 1
C22A C 0.5328(9) 0.2575(6) 0.2437(7) 0.037(3) Uani 0.50 1 d PDU A 1
H22A H 0.5884 0.2306 0.2417 0.045 Uiso 0.50 1 calc PR A 1
H22B H 0.5275 0.3026 0.2218 0.045 Uiso 0.50 1 calc PR A 1
C23A C 0.4192(8) 0.2232(5) 0.1956(6) 0.031(2) Uani 0.50 1 d PDU A 1
H23A H 0.3966 0.2177 0.1420 0.038 Uiso 0.50 1 calc PR A 1
H23B H 0.3621 0.2518 0.1941 0.038 Uiso 0.50 1 calc PR A 1
C24A C 0.4231(9) 0.1545(5) 0.2287(4) 0.028(2) Uani 0.50 1 d PDU A 1
H24A H 0.4787 0.1248 0.2299 0.033 Uiso 0.50 1 calc PR A 1
H24B H 0.3482 0.1325 0.1979 0.033 Uiso 0.50 1 calc PR A 1
C20B C 0.5468(10) 0.2297(6) 0.3617(8) 0.052(4) Uani 0.50 1 d PDU A 2
H20C H 0.5061 0.2733 0.3475 0.062 Uiso 0.50 1 calc PR A 2
H20D H 0.5835 0.2222 0.4175 0.062 Uiso 0.50 1 calc PR A 2
C21B C 0.6353(10) 0.2326(7) 0.3457(8) 0.052(3) Uani 0.50 1 d PDU A 2
H21C H 0.6801 0.1904 0.3642 0.062 Uiso 0.50 1 calc PR A 2
H21D H 0.6870 0.2707 0.3746 0.062 Uiso 0.50 1 calc PR A 2
C22B C 0.5828(12) 0.2413(7) 0.2602(8) 0.054(4) Uani 0.50 1 d PDU A 2
H22C H 0.6423 0.2374 0.2513 0.065 Uiso 0.50 1 calc PR A 2
H22D H 0.5499 0.2871 0.2440 0.065 Uiso 0.50 1 calc PR A 2
C23B C 0.4917(10) 0.1892(6) 0.2112(7) 0.045(3) Uani 0.50 1 d PDU A 2
H23C H 0.4569 0.1983 0.1559 0.054 Uiso 0.50 1 calc PR A 2
H23D H 0.5257 0.1436 0.2233 0.054 Uiso 0.50 1 calc PR A 2
C24B C 0.4026(8) 0.1916(6) 0.2264(4) 0.032(2) Uani 0.50 1 d PDU A 2
H24C H 0.3406 0.1602 0.1914 0.038 Uiso 0.50 1 calc PR A 2
H24D H 0.3712 0.2378 0.2173 0.038 Uiso 0.50 1 calc PR A 2
C25 C 0.1792(4) -0.0145(2) 0.1895(3) 0.0253(10) Uani 1 1 d . . .
H25 H 0.1517 -0.0602 0.1915 0.030 Uiso 1 1 calc R . .
C26 C 0.1395(5) -0.0018(3) 0.1065(3) 0.0355(12) Uani 1 1 d . . .
H26A H 0.0561 -0.0034 0.0722 0.043 Uiso 1 1 calc R . .
H26B H 0.1636 0.0438 0.1026 0.043 Uiso 1 1 calc R . .
C27 C 0.1870(6) -0.0540(3) 0.0804(4) 0.0485(15) Uani 1 1 d . . .
H27A H 0.1639 -0.0427 0.0277 0.058 Uiso 1 1 calc R . .
H27B H 0.1554 -0.0989 0.0784 0.058 Uiso 1 1 calc R . .
C28 C 0.3147(6) -0.0572(4) 0.1343(4) 0.0523(17) Uani 1 1 d . . .
H28A H 0.3469 -0.0146 0.1307 0.063 Uiso 1 1 calc R . .
H28B H 0.3421 -0.0946 0.1182 0.063 Uiso 1 1 calc R . .
C29 C 0.3547(6) -0.0683(4) 0.2175(4) 0.0502(16) Uani 1 1 d . . .
H29A H 0.3308 -0.1137 0.2224 0.060 Uiso 1 1 calc R . .
H29B H 0.4380 -0.0667 0.2517 0.060 Uiso 1 1 calc R . .
C30 C 0.3074(5) -0.0153(3) 0.2431(3) 0.0364(12) Uani 1 1 d . . .
H30A H 0.3369 0.0296 0.2430 0.044 Uiso 1 1 calc R . .
H30B H 0.3319 -0.0252 0.2965 0.044 Uiso 1 1 calc R . .
C31 C 0.1400(4) 0.0165(2) 0.3081(3) 0.0251(10) Uani 1 1 d . . .
H31 H 0.2164 0.0325 0.3515 0.030 Uiso 1 1 calc R . .
C32 C 0.0544(5) 0.0509(3) 0.3173(3) 0.0336(12) Uani 1 1 d . . .
H32A H 0.0591 0.1005 0.3137 0.040 Uiso 1 1 calc R . .
H32B H -0.0226 0.0364 0.2751 0.040 Uiso 1 1 calc R . .
C33 C 0.0768(6) 0.0329(3) 0.3949(3) 0.0401(13) Uani 1 1 d . . .
H33A H 0.1498 0.0526 0.4370 0.048 Uiso 1 1 calc R . .
H33B H 0.0171 0.0529 0.3980 0.048 Uiso 1 1 calc R . .
C34 C 0.0795(5) -0.0431(3) 0.4061(3) 0.0380(13) Uani 1 1 d . . .
H34A H 0.1005 -0.0527 0.4587 0.046 Uiso 1 1 calc R . .
H34B H 0.0034 -0.0619 0.3685 0.046 Uiso 1 1 calc R . .
C35 C 0.1627(5) -0.0770(3) 0.3954(3) 0.0348(12) Uani 1 1 d . . .
H35A H 0.1590 -0.1265 0.3999 0.042 Uiso 1 1 calc R . .
H35B H 0.2400 -0.0620 0.4366 0.042 Uiso 1 1 calc R . .
C36 C 0.1375(5) -0.0600(2) 0.3168(3) 0.0302(11) Uani 1 1 d . . .
H36A H 0.0624 -0.0778 0.2755 0.036 Uiso 1 1 calc R . .
H36B H 0.1942 -0.0817 0.3117 0.036 Uiso 1 1 calc R . .
C37 C 0.3237(5) 0.4166(3) 0.3918(3) 0.0345(12) Uani 1 1 d . . .
H37 H 0.3414 0.4657 0.3948 0.041 Uiso 1 1 calc R . .
C38 C 0.2101(5) 0.4096(3) 0.3784(3) 0.0448(14) Uani 1 1 d . . .
H38A H 0.1529 0.4343 0.3308 0.054 Uiso 1 1 calc R . .
H38B H 0.1883 0.3614 0.3706 0.054 Uiso 1 1 calc R . .
C39 C 0.2114(7) 0.4368(4) 0.4452(5) 0.063(2) Uani 1 1 d . . .
H39A H 0.1372 0.4289 0.4358 0.076 Uiso 1 1 calc R . .
H39B H 0.2251 0.4860 0.4496 0.076 Uiso 1 1 calc R . .
C40 C 0.3022(8) 0.4028(4) 0.5194(4) 0.065(2) Uani 1 1 d . . .
H40A H 0.3033 0.4223 0.5628 0.078 Uiso 1 1 calc R . .
H40B H 0.2850 0.3541 0.5164 0.078 Uiso 1 1 calc R . .
C41 C 0.4146(8) 0.4114(4) 0.5345(4) 0.073(2) Uani 1 1 d . . .
H41A H 0.4719 0.3876 0.5828 0.087 Uiso 1 1 calc R . .
H41B H 0.4344 0.4599 0.5415 0.087 Uiso 1 1 calc R . .
C42 C 0.4160(6) 0.3835(4) 0.4681(3) 0.0541(17) Uani 1 1 d . . .
H42A H 0.4041 0.3341 0.4645 0.065 Uiso 1 1 calc R . .
H42B H 0.4904 0.3923 0.4782 0.065 Uiso 1 1 calc R . .
C43 C 0.2662(5) 0.4446(3) 0.2382(3) 0.0329(11) Uani 1 1 d . . .
H43 H 0.1862 0.4526 0.2193 0.039 Uiso 1 1 calc R . .
C44 C 0.3279(6) 0.5126(3) 0.2654(3) 0.0417(14) Uani 1 1 d . . .
H44A H 0.3250 0.5306 0.3077 0.050 Uiso 1 1 calc R . .
H44B H 0.4079 0.5061 0.2855 0.050 Uiso 1 1 calc R . .
C45 C 0.2744(6) 0.5615(3) 0.2002(4) 0.0497(16) Uani 1 1 d . . .
H45A H 0.3147 0.6052 0.2186 0.060 Uiso 1 1 calc R . .
H45B H 0.1954 0.5692 0.1818 0.060 Uiso 1 1 calc R . .
C46 C 0.2766(7) 0.5365(3) 0.1341(4) 0.0554(18) Uani 1 1 d . . .
H46A H 0.3556 0.5316 0.1511 0.067 Uiso 1 1 calc R . .
H46B H 0.2388 0.5696 0.0913 0.067 Uiso 1 1 calc R . .
C47 C 0.2161(7) 0.4682(3) 0.1059(4) 0.0565(18) Uani 1 1 d . . .
H47A H 0.1353 0.4745 0.0837 0.068 Uiso 1 1 calc R . .
H47B H 0.2219 0.4507 0.0647 0.068 Uiso 1 1 calc R . .
C48 C 0.2656(7) 0.4175(3) 0.1703(4) 0.0514(17) Uani 1 1 d . . .
H48A H 0.3437 0.4069 0.1882 0.062 Uiso 1 1 calc R . .
H48B H 0.2211 0.3753 0.1510 0.062 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C .0033 .0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H .0000 .0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O .0106 .0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P .1023 .0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Pt1 P2 139.83(10) . . ?
O1 Pt1 P4 102.47(10) . . ?
P2 Pt1 P4 117.68(7) . . ?
O1 Pt1 Pt2 83.26(9) . . ?
P2 Pt1 Pt2 56.63(6) . . ?
P4 Pt1 Pt2 174.15(4) . . ?
O1 Pt1 P1 33.42(10) . . ?
P2 Pt1 P1 106.43(6) . . ?
P4 Pt1 P1 135.77(5) . . ?
Pt2 Pt1 P1 50.02(2) . . ?
P3 Pt2 P1 117.45(6) . . ?
P3 Pt2 P2 118.73(5) . . ?
P1 Pt2 P2 123.80(6) . . ?
P3 Pt2 Pt1 169.59(3) . . ?
P1 Pt2 Pt1 70.39(6) . . ?
P2 Pt2 Pt1 53.71(4) . . ?
O1 P1 C1 104.9(2) . . ?
O1 P1 C7 105.4(2) . . ?
C1 P1 C7 103.6(2) . . ?
O1 P1 Pt2 109.77(16) . . ?
C1 P1 Pt2 118.01(17) . . ?
C7 P1 Pt2 114.02(17) . . ?
O1 P1 Pt1 50.47(15) . . ?
C1 P1 Pt1 133.07(18) . . ?
C7 P1 Pt1 120.36(18) . . ?
Pt2 P1 Pt1 59.60(5) . . ?
C19 P2 C13 104.6(3) . . ?
C19 P2 Pt1 117.7(3) . . ?
C13 P2 Pt1 118.59(19) . . ?
C19 P2 Pt2 119.17(16) . . ?
C13 P2 Pt2 124.69(18) . . ?
Pt1 P2 Pt2 69.67(6) . . ?
C25 P3 C31 106.6(2) . . ?
C25 P3 Pt2 119.17(17) . . ?
C31 P3 Pt2 111.13(16) . . ?
C25 P3 H3 106.4 . . ?
C31 P3 H3 106.4 . . ?
Pt2 P3 H3 106.4 . . ?
C43 P4 C37 105.3(3) . . ?
C43 P4 Pt1 113.74(17) . . ?
C37 P4 Pt1 118.01(18) . . ?
C43 P4 H4 106.3 . . ?
C37 P4 H4 106.3 . . ?
Pt1 P4 H4 106.3 . . ?
P1 O1 Pt1 96.11(18) . . ?
C2 C1 C6 111.1(5) . . ?
C2 C1 P1 113.5(3) . . ?
C6 C1 P1 108.7(4) . . ?
C2 C1 H1 107.8 . . ?
C6 C1 H1 107.8 . . ?
P1 C1 H1 107.8 . . ?
C1 C2 C3 111.3(5) . . ?
C1 C2 H2A 109.4 . . ?
C3 C2 H2A 109.4 . . ?
C1 C2 H2B 109.4 . . ?
C3 C2 H2B 109.4 . . ?
H2A C2 H2B 108.0 . . ?
C4 C3 C2 111.6(6) . . ?
C4 C3 H3A 109.3 . . ?
C2 C3 H3A 109.3 . . ?
C4 C3 H3B 109.3 . . ?
C2 C3 H3B 109.3 . . ?
H3A C3 H3B 108.0 . . ?
C3 C4 C5 111.3(6) . . ?
C3 C4 H4A 109.4 . . ?
C5 C4 H4A 109.4 . . ?
C3 C4 H4B 109.4 . . ?
C5 C4 H4B 109.4 . . ?
H4A C4 H4B 108.0 . . ?
C4 C5 C6 111.7(6) . . ?
C4 C5 H5A 109.3 . . ?
C6 C5 H5A 109.3 . . ?
C4 C5 H5B 109.3 . . ?
C6 C5 H5B 109.3 . . ?
H5A C5 H5B 107.9 . . ?
C5 C6 C1 110.5(6) . . ?
C5 C6 H6A 109.5 . . ?
C1 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
C1 C6 H6B 109.5 . . ?
H6A C6 H6B 108.1 . . ?
C8 C7 C12 111.0(5) . . ?
C8 C7 P1 110.0(4) . . ?
C12 C7 P1 112.3(4) . . ?
C8 C7 H7 107.8 . . ?
C12 C7 H7 107.8 . . ?
P1 C7 H7 107.8 . . ?
C7 C8 C9 112.3(5) . . ?
C7 C8 H8A 109.1 . . ?
C9 C8 H8A 109.1 . . ?
C7 C8 H8B 109.1 . . ?
C9 C8 H8B 109.1 . . ?
H8A C8 H8B 107.9 . . ?
C10 C9 C8 111.2(5) . . ?
C10 C9 H9A 109.4 . . ?
C8 C9 H9A 109.4 . . ?
C10 C9 H9B 109.4 . . ?
C8 C9 H9B 109.4 . . ?
H9A C9 H9B 108.0 . . ?
C9 C10 C11 110.3(6) . . ?
C9 C10 H10A 109.6 . . ?
C11 C10 H10A 109.6 . . ?
C9 C10 H10B 109.6 . . ?
C11 C10 H10B 109.6 . . ?
H10A C10 H10B 108.1 . . ?
C10 C11 C12 110.6(7) . . ?
C10 C11 H11A 109.5 . . ?
C12 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
C12 C11 H11B 109.5 . . ?
H11A C11 H11B 108.1 . . ?
C7 C12 C11 111.2(5) . . ?
C7 C12 H12A 109.4 . . ?
C11 C12 H12A 109.4 . . ?
C7 C12 H12B 109.4 . . ?
C11 C12 H12B 109.4 . . ?
H12A C12 H12B 108.0 . . ?
C14 C13 C18 111.0(5) . . ?
C14 C13 P2 112.7(4) . . ?
C18 C13 P2 108.7(4) . . ?
C14 C13 H13 108.1 . . ?
C18 C13 H13 108.1 . . ?
P2 C13 H13 108.1 . . ?
C13 C14 C15 112.2(5) . . ?
C13 C14 H14A 109.2 . . ?
C15 C14 H14A 109.2 . . ?
C13 C14 H14B 109.2 . . ?
C15 C14 H14B 109.2 . . ?
H14A C14 H14B 107.9 . . ?
C16 C15 C14 110.1(5) . . ?
C16 C15 H15A 109.6 . . ?
C14 C15 H15A 109.6 . . ?
C16 C15 H15B 109.6 . . ?
C14 C15 H15B 109.6 . . ?
H15A C15 H15B 108.2 . . ?
C17 C16 C15 111.3(6) . . ?
C17 C16 H16A 109.4 . . ?
C15 C16 H16A 109.4 . . ?
C17 C16 H16B 109.4 . . ?
C15 C16 H16B 109.4 . . ?
H16A C16 H16B 108.0 . . ?
C16 C17 C18 111.0(6) . . ?
C16 C17 H17A 109.4 . . ?
C18 C17 H17A 109.4 . . ?
C16 C17 H17B 109.4 . . ?
C18 C17 H17B 109.4 . . ?
H17A C17 H17B 108.0 . . ?
C17 C18 C13 111.2(5) . . ?
C17 C18 H18A 109.4 . . ?
C13 C18 H18A 109.4 . . ?
C17 C18 H18B 109.4 . . ?
C13 C18 H18B 109.4 . . ?
H18A C18 H18B 108.0 . . ?
C20A C19 C24B 108.5(7) . . ?
C20A C19 C24A 109.6(7) . . ?
C24B C19 C24A 28.5(5) . . ?
C20A C19 C20B 29.7(5) . . ?
C24B C19 C20B 103.7(8) . . ?
C24A C19 C20B 119.5(7) . . ?
C20A C19 P2 128.0(5) . . ?
C24B C19 P2 101.7(5) . . ?
C24A C19 P2 116.8(5) . . ?
C20B C19 P2 102.8(5) . . ?
C20A C19 H19 92.9 . . ?
C24B C19 H19 121.1 . . ?
C24A C19 H19 92.8 . . ?
C20B C19 H19 118.4 . . ?
P2 C19 H19 106.6 . . ?
C21A C20A C19 102.4(7) . . ?
C21A C20A H20A 111.3 . . ?
C19 C20A H20A 111.3 . . ?
C21A C20A H20B 111.3 . . ?
C19 C20A H20B 111.3 . . ?
H20A C20A H20B 109.2 . . ?
C20A C21A C22A 112.0(9) . . ?
C20A C21A H21A 109.2 . . ?
C22A C21A H21A 109.2 . . ?
C20A C21A H21B 109.2 . . ?
C22A C21A H21B 109.2 . . ?
H21A C21A H21B 107.9 . . ?
C21A C22A C23A 111.5(9) . . ?
C21A C22A H22A 109.3 . . ?
C23A C22A H22A 109.3 . . ?
C21A C22A H22B 109.3 . . ?
C23A C22A H22B 109.3 . . ?
H22A C22A H22B 108.0 . . ?
C22A C23A C24A 110.9(9) . . ?
C22A C23A H23A 109.5 . . ?
C24A C23A H23A 109.5 . . ?
C22A C23A H23B 109.5 . . ?
C24A C23A H23B 109.5 . . ?
H23A C23A H23B 108.1 . . ?
C23A C24A C19 104.4(7) . . ?
C23A C24A H24A 110.9 . . ?
C19 C24A H24A 110.9 . . ?
C23A C24A H24B 110.9 . . ?
C19 C24A H24B 110.9 . . ?
H24A C24A H24B 108.9 . . ?
C21B C20B C19 110.6(8) . . ?
C21B C20B H20C 109.5 . . ?
C19 C20B H20C 109.5 . . ?
C21B C20B H20D 109.5 . . ?
C19 C20B H20D 109.5 . . ?
H20C C20B H20D 108.1 . . ?
C20B C21B C22B 111.6(11) . . ?
C20B C21B H21C 109.3 . . ?
C22B C21B H21C 109.3 . . ?
C20B C21B H21D 109.3 . . ?
C22B C21B H21D 109.3 . . ?
H21C C21B H21D 108.0 . . ?
C21B C22B C23B 112.2(11) . . ?
C21B C22B H22C 109.2 . . ?
C23B C22B H22C 109.2 . . ?
C21B C22B H22D 109.2 . . ?
C23B C22B H22D 109.2 . . ?
H22C C22B H22D 107.9 . . ?
C24B C23B C22B 110.5(10) . . ?
C24B C23B H23C 109.5 . . ?
C22B C23B H23C 109.5 . . ?
C24B C23B H23D 109.5 . . ?
C22B C23B H23D 109.5 . . ?
H23C C23B H23D 108.1 . . ?
C23B C24B C19 108.0(7) . . ?
C23B C24B H24C 110.1 . . ?
C19 C24B H24C 110.1 . . ?
C23B C24B H24D 110.1 . . ?
C19 C24B H24D 110.1 . . ?
H24C C24B H24D 108.4 . . ?
C30 C25 C26 110.5(4) . . ?
C30 C25 P3 113.0(3) . . ?
C26 C25 P3 109.9(3) . . ?
C30 C25 H25 107.8 . . ?
C26 C25 H25 107.8 . . ?
P3 C25 H25 107.8 . . ?
C27 C26 C25 111.2(5) . . ?
C27 C26 H26A 109.4 . . ?
C25 C26 H26A 109.4 . . ?
C27 C26 H26B 109.4 . . ?
C25 C26 H26B 109.4 . . ?
H26A C26 H26B 108.0 . . ?
C26 C27 C28 111.8(5) . . ?
C26 C27 H27A 109.3 . . ?
C28 C27 H27A 109.3 . . ?
C26 C27 H27B 109.3 . . ?
C28 C27 H27B 109.3 . . ?
H27A C27 H27B 107.9 . . ?
C27 C28 C29 111.1(5) . . ?
C27 C28 H28A 109.4 . . ?
C29 C28 H28A 109.4 . . ?
C27 C28 H28B 109.4 . . ?
C29 C28 H28B 109.4 . . ?
H28A C28 H28B 108.0 . . ?
C30 C29 C28 111.6(5) . . ?
C30 C29 H29A 109.3 . . ?
C28 C29 H29A 109.3 . . ?
C30 C29 H29B 109.3 . . ?
C28 C29 H29B 109.3 . . ?
H29A C29 H29B 108.0 . . ?
C29 C30 C25 110.6(5) . . ?
C29 C30 H30A 109.5 . . ?
C25 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
C25 C30 H30B 109.5 . . ?
H30A C30 H30B 108.1 . . ?
C32 C31 C36 110.3(4) . . ?
C32 C31 P3 107.8(3) . . ?
C36 C31 P3 117.1(3) . . ?
C32 C31 H31 107.1 . . ?
C36 C31 H31 107.1 . . ?
P3 C31 H31 107.1 . . ?
C33 C32 C31 110.7(4) . . ?
C33 C32 H32A 109.5 . . ?
C31 C32 H32A 109.5 . . ?
C33 C32 H32B 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 108.1 . . ?
C34 C33 C32 111.7(5) . . ?
C34 C33 H33A 109.3 . . ?
C32 C33 H33A 109.3 . . ?
C34 C33 H33B 109.3 . . ?
C32 C33 H33B 109.3 . . ?
H33A C33 H33B 107.9 . . ?
C35 C34 C33 111.6(4) . . ?
C35 C34 H34A 109.3 . . ?
C33 C34 H34A 109.3 . . ?
C35 C34 H34B 109.3 . . ?
C33 C34 H34B 109.3 . . ?
H34A C34 H34B 108.0 . . ?
C34 C35 C36 111.0(4) . . ?
C34 C35 H35A 109.4 . . ?
C36 C35 H35A 109.4 . . ?
C34 C35 H35B 109.4 . . ?
C36 C35 H35B 109.4 . . ?
H35A C35 H35B 108.0 . . ?
C35 C36 C31 110.2(4) . . ?
C35 C36 H36A 109.6 . . ?
C31 C36 H36A 109.6 . . ?
C35 C36 H36B 109.6 . . ?
C31 C36 H36B 109.6 . . ?
H36A C36 H36B 108.1 . . ?
C38 C37 C42 110.8(5) . . ?
C38 C37 P4 111.5(4) . . ?
C42 C37 P4 109.6(4) . . ?
C38 C37 H37 108.3 . . ?
C42 C37 H37 108.3 . . ?
P4 C37 H37 108.3 . . ?
C39 C38 C37 111.8(6) . . ?
C39 C38 H38A 109.3 . . ?
C37 C38 H38A 109.3 . . ?
C39 C38 H38B 109.3 . . ?
C37 C38 H38B 109.3 . . ?
H38A C38 H38B 107.9 . . ?
C38 C39 C40 110.6(6) . . ?
C38 C39 H39A 109.5 . . ?
C40 C39 H39A 109.5 . . ?
C38 C39 H39B 109.5 . . ?
C40 C39 H39B 109.5 . . ?
H39A C39 H39B 108.1 . . ?
C41 C40 C39 111.4(6) . . ?
C41 C40 H40A 109.4 . . ?
C39 C40 H40A 109.4 . . ?
C41 C40 H40B 109.4 . . ?
C39 C40 H40B 109.4 . . ?
H40A C40 H40B 108.0 . . ?
C40 C41 C42 111.2(6) . . ?
C40 C41 H41A 109.4 . . ?
C42 C41 H41A 109.4 . . ?
C40 C41 H41B 109.4 . . ?
C42 C41 H41B 109.4 . . ?
H41A C41 H41B 108.0 . . ?
C41 C42 C37 110.6(6) . . ?
C41 C42 H42A 109.5 . . ?
C37 C42 H42A 109.5 . . ?
C41 C42 H42B 109.5 . . ?
C37 C42 H42B 109.5 . . ?
H42A C42 H42B 108.1 . . ?
C48 C43 C44 110.1(4) . . ?
C48 C43 P4 108.4(4) . . ?
C44 C43 P4 115.0(4) . . ?
C48 C43 H43 107.7 . . ?
C44 C43 H43 107.7 . . ?
P4 C43 H43 107.7 . . ?
C45 C44 C43 110.2(5) . . ?
C45 C44 H44A 109.6 . . ?
C43 C44 H44A 109.6 . . ?
C45 C44 H44B 109.6 . . ?
C43 C44 H44B 109.6 . . ?
H44A C44 H44B 108.1 . . ?
C44 C45 C46 111.8(6) . . ?
C44 C45 H45A 109.3 . . ?
C46 C45 H45A 109.3 . . ?
C44 C45 H45B 109.3 . . ?
C46 C45 H45B 109.3 . . ?
H45A C45 H45B 107.9 . . ?
C45 C46 C47 109.6(5) . . ?
C45 C46 H46A 109.7 . . ?
C47 C46 H46A 109.7 . . ?
C45 C46 H46B 109.7 . . ?
C47 C46 H46B 109.7 . . ?
H46A C46 H46B 108.2 . . ?
C48 C47 C46 111.7(6) . . ?
C48 C47 H47A 109.3 . . ?
C46 C47 H47A 109.3 . . ?
C48 C47 H47B 109.3 . . ?
C46 C47 H47B 109.3 . . ?
H47A C47 H47B 107.9 . . ?
C47 C48 C43 111.2(5) . . ?
C47 C48 H48A 109.4 . . ?
C43 C48 H48A 109.4 . . ?
C47 C48 H48B 109.4 . . ?
C43 C48 H48B 109.4 . . ?
H48A C48 H48B 108.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 O1 2.180(4) . ?
Pt1 P2 2.2117(19) . ?
Pt1 P4 2.2365(18) . ?
Pt1 Pt2 2.5731(16) . ?
Pt1 P1 2.810(2) . ?
Pt2 P3 2.2513(19) . ?
Pt2 P1 2.2860(17) . ?
Pt2 P2 2.292(2) . ?
P1 O1 1.556(4) . ?
P1 C1 1.831(6) . ?
P1 C7 1.838(5) . ?
P2 C19 1.827(7) . ?
P2 C13 1.846(5) . ?
P3 C25 1.836(5) . ?
P3 C31 1.844(5) . ?
P3 H3 1.0000 . ?
P4 C43 1.824(6) . ?
P4 C37 1.839(5) . ?
P4 H4 1.0000 . ?
C1 C2 1.518(7) . ?
C1 C6 1.532(7) . ?
C1 H1 1.0000 . ?
C2 C3 1.529(8) . ?
C2 H2A 0.9900 . ?
C2 H2B 0.9900 . ?
C3 C4 1.501(12) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 C5 1.509(11) . ?
C4 H4A 0.9900 . ?
C4 H4B 0.9900 . ?
C5 C6 1.526(9) . ?
C5 H5A 0.9900 . ?
C5 H5B 0.9900 . ?
C6 H6A 0.9900 . ?
C6 H6B 0.9900 . ?
C7 C8 1.515(8) . ?
C7 C12 1.525(7) . ?
C7 H7 1.0000 . ?
C8 C9 1.529(8) . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C9 C10 1.488(10) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C10 C11 1.515(13) . ?
C10 H10A 0.9900 . ?
C10 H10B 0.9900 . ?
C11 C12 1.540(9) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C13 C14 1.518(8) . ?
C13 C18 1.531(8) . ?
C13 H13 1.0000 . ?
C14 C15 1.531(7) . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C15 C16 1.524(9) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C16 C17 1.513(10) . ?
C16 H16A 0.9900 . ?
C16 H16B 0.9900 . ?
C17 C18 1.529(8) . ?
C17 H17A 0.9900 . ?
C17 H17B 0.9900 . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C19 C20A 1.581(7) . ?
C19 C24B 1.588(7) . ?
C19 C24A 1.589(7) . ?
C19 C20B 1.592(7) . ?
C19 H19 0.9634 . ?
C20A C21A 1.504(11) . ?
C20A H20A 0.9900 . ?
C20A H20B 0.9900 . ?
C21A C22A 1.511(12) . ?
C21A H21A 0.9900 . ?
C21A H21B 0.9900 . ?
C22A C23A 1.512(11) . ?
C22A H22A 0.9900 . ?
C22A H22B 0.9900 . ?
C23A C24A 1.517(10) . ?
C23A H23A 0.9900 . ?
C23A H23B 0.9900 . ?
C24A H24A 0.9900 . ?
C24A H24B 0.9900 . ?
C20B C21B 1.511(11) . ?
C20B H20C 0.9900 . ?
C20B H20D 0.9900 . ?
C21B C22B 1.517(13) . ?
C21B H21C 0.9900 . ?
C21B H21D 0.9900 . ?
C22B C23B 1.520(12) . ?
C22B H22C 0.9900 . ?
C22B H22D 0.9900 . ?
C23B C24B 1.506(11) . ?
C23B H23C 0.9900 . ?
C23B H23D 0.9900 . ?
C24B H24C 0.9900 . ?
C24B H24D 0.9900 . ?
C25 C30 1.523(7) . ?
C25 C26 1.523(7) . ?
C25 H25 1.0000 . ?
C26 C27 1.517(8) . ?
C26 H26A 0.9900 . ?
C26 H26B 0.9900 . ?
C27 C28 1.519(10) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C28 C29 1.522(8) . ?
C28 H28A 0.9900 . ?
C28 H28B 0.9900 . ?
C29 C30 1.518(8) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 H30A 0.9900 . ?
C30 H30B 0.9900 . ?
C31 C32 1.529(7) . ?
C31 C36 1.531(6) . ?
C31 H31 1.0000 . ?
C32 C33 1.525(7) . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C33 C34 1.521(8) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 C35 1.513(8) . ?
C34 H34A 0.9900 . ?
C34 H34B 0.9900 . ?
C35 C36 1.524(7) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 H36A 0.9900 . ?
C36 H36B 0.9900 . ?
C37 C38 1.513(8) . ?
C37 C42 1.530(8) . ?
C37 H37 1.0000 . ?
C38 C39 1.506(9) . ?
C38 H38A 0.9900 . ?
C38 H38B 0.9900 . ?
C39 C40 1.508(10) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 C41 1.484(12) . ?
C40 H40A 0.9900 . ?
C40 H40B 0.9900 . ?
C41 C42 1.524(10) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 H42A 0.9900 . ?
C42 H42B 0.9900 . ?
C43 C48 1.533(8) . ?
C43 C44 1.534(7) . ?
C43 H43 1.0000 . ?
C44 C45 1.489(8) . ?
C44 H44A 0.9900 . ?
C44 H44B 0.9900 . ?
C45 C46 1.506(9) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 C47 1.536(9) . ?
C46 H46A 0.9900 . ?
C46 H46B 0.9900 . ?
C47 C48 1.502(9) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C48 H48A 0.9900 . ?
C48 H48B 0.9900 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Pt1 Pt2 P3 -136.4(2) . . . . ?
P2 Pt1 Pt2 P3 45.81(19) . . . . ?
P4 Pt1 Pt2 P3 31.8(4) . . . . ?
P1 Pt1 Pt2 P3 -140.26(19) . . . . ?
O1 Pt1 Pt2 P1 3.84(10) . . . . ?
P2 Pt1 Pt2 P1 -173.93(5) . . . . ?
P4 Pt1 Pt2 P1 172.1(4) . . . . ?
O1 Pt1 Pt2 P2 177.78(11) . . . . ?
P4 Pt1 Pt2 P2 -14.0(4) . . . . ?
P1 Pt1 Pt2 P2 173.93(5) . . . . ?
P3 Pt2 P1 O1 166.84(16) . . . . ?
P2 Pt2 P1 O1 -11.57(17) . . . . ?
Pt1 Pt2 P1 O1 -5.68(15) . . . . ?
P3 Pt2 P1 C1 46.7(2) . . . . ?
P2 Pt2 P1 C1 -131.7(2) . . . . ?
Pt1 Pt2 P1 C1 -125.8(2) . . . . ?
P3 Pt2 P1 C7 -75.1(2) . . . . ?
P2 Pt2 P1 C7 106.5(2) . . . . ?
Pt1 Pt2 P1 C7 112.3(2) . . . . ?
P3 Pt2 P1 Pt1 172.52(4) . . . . ?
P2 Pt2 P1 Pt1 -5.88(5) . . . . ?
P2 Pt1 P1 O1 178.34(18) . . . . ?
P4 Pt1 P1 O1 -5.78(19) . . . . ?
Pt2 Pt1 P1 O1 173.06(19) . . . . ?
O1 Pt1 P1 C1 -71.7(3) . . . . ?
P2 Pt1 P1 C1 106.6(2) . . . . ?
P4 Pt1 P1 C1 -77.5(2) . . . . ?
Pt2 Pt1 P1 C1 101.4(2) . . . . ?
O1 Pt1 P1 C7 85.2(3) . . . . ?
P2 Pt1 P1 C7 -96.44(19) . . . . ?
P4 Pt1 P1 C7 79.4(2) . . . . ?
Pt2 Pt1 P1 C7 -101.72(19) . . . . ?
O1 Pt1 P1 Pt2 -173.06(19) . . . . ?
P2 Pt1 P1 Pt2 5.28(5) . . . . ?
P4 Pt1 P1 Pt2 -178.84(5) . . . . ?
O1 Pt1 P2 C19 109.7(2) . . . . ?
P4 Pt1 P2 C19 -68.5(2) . . . . ?
Pt2 Pt1 P2 C19 113.11(19) . . . . ?
P1 Pt1 P2 C19 108.27(19) . . . . ?
O1 Pt1 P2 C13 -122.7(2) . . . . ?
P4 Pt1 P2 C13 59.1(2) . . . . ?
Pt2 Pt1 P2 C13 -119.3(2) . . . . ?
P1 Pt1 P2 C13 -124.1(2) . . . . ?
O1 Pt1 P2 Pt2 -3.43(16) . . . . ?
P4 Pt1 P2 Pt2 178.40(4) . . . . ?
P1 Pt1 P2 Pt2 -4.84(4) . . . . ?
P3 Pt2 P2 C19 77.4(3) . . . . ?
P1 Pt2 P2 C19 -104.2(3) . . . . ?
Pt1 Pt2 P2 C19 -111.1(3) . . . . ?
P3 Pt2 P2 C13 -60.1(2) . . . . ?
P1 Pt2 P2 C13 118.2(2) . . . . ?
Pt1 Pt2 P2 C13 111.4(2) . . . . ?
P3 Pt2 P2 Pt1 -171.51(4) . . . . ?
P1 Pt2 P2 Pt1 6.88(6) . . . . ?
P1 Pt2 P3 C25 114.29(19) . . . . ?
P2 Pt2 P3 C25 -67.22(19) . . . . ?
Pt1 Pt2 P3 C25 -108.4(2) . . . . ?
P1 Pt2 P3 C31 -121.26(18) . . . . ?
P2 Pt2 P3 C31 57.23(19) . . . . ?
Pt1 Pt2 P3 C31 16.0(3) . . . . ?
O1 Pt1 P4 C43 -30.3(2) . . . . ?
P2 Pt1 P4 C43 148.5(2) . . . . ?
Pt2 Pt1 P4 C43 161.7(4) . . . . ?
P1 Pt1 P4 C43 -27.1(2) . . . . ?
O1 Pt1 P4 C37 93.7(2) . . . . ?
P2 Pt1 P4 C37 -87.5(2) . . . . ?
Pt2 Pt1 P4 C37 -74.3(5) . . . . ?
P1 Pt1 P4 C37 97.0(2) . . . . ?
C1 P1 O1 Pt1 134.1(2) . . . . ?
C7 P1 O1 Pt1 -116.9(2) . . . . ?
Pt2 P1 O1 Pt1 6.36(17) . . . . ?
P2 Pt1 O1 P1 -2.5(3) . . . . ?
P4 Pt1 O1 P1 175.87(14) . . . . ?
Pt2 Pt1 O1 P1 -5.35(14) . . . . ?
O1 P1 C1 C2 177.9(4) . . . . ?
C7 P1 C1 C2 67.6(4) . . . . ?
Pt2 P1 C1 C2 -59.5(4) . . . . ?
Pt1 P1 C1 C2 -132.8(4) . . . . ?
O1 P1 C1 C6 -57.9(4) . . . . ?
C7 P1 C1 C6 -168.3(4) . . . . ?
Pt2 P1 C1 C6 64.6(4) . . . . ?
Pt1 P1 C1 C6 -8.7(5) . . . . ?
C6 C1 C2 C3 54.9(7) . . . . ?
P1 C1 C2 C3 177.7(5) . . . . ?
C1 C2 C3 C4 -55.1(8) . . . . ?
C2 C3 C4 C5 55.4(8) . . . . ?
C3 C4 C5 C6 -56.1(9) . . . . ?
C4 C5 C6 C1 55.7(8) . . . . ?
C2 C1 C6 C5 -55.1(7) . . . . ?
P1 C1 C6 C5 179.3(4) . . . . ?
O1 P1 C7 C8 75.4(4) . . . . ?
C1 P1 C7 C8 -174.6(4) . . . . ?
Pt2 P1 C7 C8 -45.1(4) . . . . ?
Pt1 P1 C7 C8 22.5(4) . . . . ?
O1 P1 C7 C12 -48.8(6) . . . . ?
C1 P1 C7 C12 61.2(5) . . . . ?
Pt2 P1 C7 C12 -169.3(5) . . . . ?
Pt1 P1 C7 C12 -101.7(5) . . . . ?
C12 C7 C8 C9 -52.4(7) . . . . ?
P1 C7 C8 C9 -177.4(4) . . . . ?
C7 C8 C9 C10 55.6(8) . . . . ?
C8 C9 C10 C11 -58.2(9) . . . . ?
C9 C10 C11 C12 58.8(10) . . . . ?
C8 C7 C12 C11 52.8(9) . . . . ?
P1 C7 C12 C11 176.4(7) . . . . ?
C10 C11 C12 C7 -56.2(10) . . . . ?
C19 P2 C13 C14 -51.6(5) . . . . ?
Pt1 P2 C13 C14 174.9(3) . . . . ?
Pt2 P2 C13 C14 90.8(4) . . . . ?
C19 P2 C13 C18 -175.2(4) . . . . ?
Pt1 P2 C13 C18 51.3(4) . . . . ?
Pt2 P2 C13 C18 -32.7(5) . . . . ?
C18 C13 C14 C15 -54.6(6) . . . . ?
P2 C13 C14 C15 -176.9(4) . . . . ?
C13 C14 C15 C16 55.6(7) . . . . ?
C14 C15 C16 C17 -56.7(8) . . . . ?
C15 C16 C17 C18 57.3(8) . . . . ?
C16 C17 C18 C13 -55.8(8) . . . . ?
C14 C13 C18 C17 54.2(7) . . . . ?
P2 C13 C18 C17 178.7(5) . . . . ?
C13 P2 C19 C20A -47.2(8) . . . . ?
Pt1 P2 C19 C20A 86.8(7) . . . . ?
Pt2 P2 C19 C20A 167.8(6) . . . . ?
C13 P2 C19 C24B -172.1(6) . . . . ?
Pt1 P2 C19 C24B -38.1(6) . . . . ?
Pt2 P2 C19 C24B 42.9(6) . . . . ?
C13 P2 C19 C24A 162.2(6) . . . . ?
Pt1 P2 C19 C24A -63.8(6) . . . . ?
Pt2 P2 C19 C24A 17.2(7) . . . . ?
C13 P2 C19 C20B -65.0(7) . . . . ?
Pt1 P2 C19 C20B 69.0(7) . . . . ?
Pt2 P2 C19 C20B 150.0(6) . . . . ?
C24B C19 C20A C21A 37.0(10) . . . . ?
C24A C19 C20A C21A 67.2(10) . . . . ?
C20B C19 C20A C21A -48.3(12) . . . . ?
P2 C19 C20A C21A -85.1(10) . . . . ?
C19 C20A C21A C22A -62.3(11) . . . . ?
C20A C21A C22A C23A 59.9(12) . . . . ?
C21A C22A C23A C24A -57.4(13) . . . . ?
C22A C23A C24A C19 59.3(11) . . . . ?
C20A C19 C24A C23A -66.7(10) . . . . ?
C24B C19 C24A C23A 26.2(9) . . . . ?
C20B C19 C24A C23A -35.7(12) . . . . ?
P2 C19 C24A C23A 89.1(8) . . . . ?
C20A C19 C20B C21B 40.7(11) . . . . ?
C24B C19 C20B C21B -62.7(13) . . . . ?
C24A C19 C20B C21B -37.0(15) . . . . ?
P2 C19 C20B C21B -168.3(10) . . . . ?
C19 C20B C21B C22B 57.0(15) . . . . ?
C20B C21B C22B C23B -52.0(15) . . . . ?
C21B C22B C23B C24B 56.0(15) . . . . ?
C22B C23B C24B C19 -64.2(13) . . . . ?
C20A C19 C24B C23B 35.3(11) . . . . ?
C24A C19 C24B C23B -62.0(12) . . . . ?
C20B C19 C24B C23B 65.8(10) . . . . ?
P2 C19 C24B C23B 172.2(8) . . . . ?
C31 P3 C25 C30 -69.7(4) . . . . ?
Pt2 P3 C25 C30 56.9(4) . . . . ?
C31 P3 C25 C26 166.5(4) . . . . ?
Pt2 P3 C25 C26 -66.9(4) . . . . ?
C30 C25 C26 C27 56.7(6) . . . . ?
P3 C25 C26 C27 -178.0(4) . . . . ?
C25 C26 C27 C28 -55.2(7) . . . . ?
C26 C27 C28 C29 53.9(8) . . . . ?
C27 C28 C29 C30 -54.6(8) . . . . ?
C28 C29 C30 C25 56.5(7) . . . . ?
C26 C25 C30 C29 -57.2(6) . . . . ?
P3 C25 C30 C29 179.2(4) . . . . ?
C25 P3 C31 C32 -159.3(3) . . . . ?
Pt2 P3 C31 C32 69.3(4) . . . . ?
C25 P3 C31 C36 -34.4(4) . . . . ?
Pt2 P3 C31 C36 -165.7(3) . . . . ?
C36 C31 C32 C33 56.8(6) . . . . ?
P3 C31 C32 C33 -174.2(4) . . . . ?
C31 C32 C33 C34 -54.8(7) . . . . ?
C32 C33 C34 C35 54.3(7) . . . . ?
C33 C34 C35 C36 -55.6(6) . . . . ?
C34 C35 C36 C31 57.7(6) . . . . ?
C32 C31 C36 C35 -58.2(6) . . . . ?
P3 C31 C36 C35 178.1(4) . . . . ?
C43 P4 C37 C38 83.7(4) . . . . ?
Pt1 P4 C37 C38 -44.4(5) . . . . ?
C43 P4 C37 C42 -153.2(4) . . . . ?
Pt1 P4 C37 C42 78.6(4) . . . . ?
C42 C37 C38 C39 54.6(7) . . . . ?
P4 C37 C38 C39 177.0(4) . . . . ?
C37 C38 C39 C40 -55.8(8) . . . . ?
C38 C39 C40 C41 57.2(8) . . . . ?
C39 C40 C41 C42 -57.6(9) . . . . ?
C40 C41 C42 C37 55.9(8) . . . . ?
C38 C37 C42 C41 -54.0(7) . . . . ?
P4 C37 C42 C41 -177.4(5) . . . . ?
C37 P4 C43 C48 178.8(4) . . . . ?
Pt1 P4 C43 C48 -50.5(4) . . . . ?
C37 P4 C43 C44 55.0(5) . . . . ?
Pt1 P4 C43 C44 -174.3(4) . . . . ?
C48 C43 C44 C45 56.9(7) . . . . ?
P4 C43 C44 C45 179.6(4) . . . . ?
C43 C44 C45 C46 -59.4(7) . . . . ?
C44 C45 C46 C47 58.0(8) . . . . ?
C45 C46 C47 C48 -55.5(9) . . . . ?
C46 C47 C48 C43 54.9(8) . . . . ?
C44 C43 C48 C47 -55.1(7) . . . . ?
P4 C43 C48 C47 178.3(5) . . . . ?
