#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:06:12 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179093 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/55/4305530.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305530
loop_
_publ_author_name
'Yi Liu'
'Ling Chen'
'Long-Hua Li'
'Li-Ming Wu'
'Oksana Ya. Zelinska'
'Arthur Mar'
_publ_contact_author_address
; Department of Chemistry
  University of Alberta
  Edmonton, AB
  Canada  T6G 2G2
;
_publ_contact_author_email       arthur.mar@ualberta.ca
_publ_contact_author_fax         '(780) 492-8231'
_publ_contact_author_name        'Dr. Arthur Mar'
_publ_contact_author_phone       '(780) 492-5592'
_publ_section_title
;
Structures and Physical Properties of Rare-Earth Zinc Antimonides
Pr6Zn1+xSb14+yandRE6Zn1+xSb14 (RE= Sm, Gd-Ho)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11930
_journal_page_last               11941
_journal_paper_doi               10.1021/ic800524d
_journal_volume                  47
_journal_year                    2008
_chemical_formula_sum            'Dy12 Sb28 Zn2.68'
_chemical_formula_weight         5534.19
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           'by CrystalClear-SM 1.3.6 SP3 rc4'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            1
_cell_length_a                   4.1368(14)
_cell_length_b                   14.806(5)
_cell_length_c                   18.605(7)
_cell_measurement_reflns_used    1721
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.7513
_cell_volume                     1139.5(7)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0416
_diffrn_reflns_av_sigmaI/netI    0.0278
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            4419
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         2.19
_exptl_absorpt_coefficient_mu    37.020
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.5146
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            grey
_exptl_crystal_density_diffrn    8.064
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             2300
_exptl_crystal_size_max          0.0900
_exptl_crystal_size_mid          0.0300
_exptl_crystal_size_min          0.0300
_refine_diff_density_max         9.690
_refine_diff_density_min         -8.711
_refine_diff_density_rms         0.562
_refine_ls_extinction_coef       0.00175(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.099
_refine_ls_matrix_type           full
_refine_ls_number_parameters     43
_refine_ls_number_reflns         790
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.099
_refine_ls_R_factor_all          0.0394
_refine_ls_R_factor_gt           0.0352
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0180P)²+168.0180P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0751
_refine_ls_wR_factor_ref         0.0809
_reflns_number_gt                721
_reflns_number_total             790
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic800524d_si_001_4.cif
_cod_data_source_block           Dy
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        1139.6(7)
_cod_database_code               4305530
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.0000 0.0000 0.32321(6) 0.0094(3) Uani 1 4 d S . .
Dy2 Dy 0.0000 0.13852(5) 0.13648(4) 0.0074(2) Uani 1 2 d S . .
Zn1 Zn 0.0000 0.2615(3) 0.0000 0.0164(15) Uani 0.671(15) 4 d SP . .
Sb1 Sb 0.0000 0.0000 0.0000 0.076(2) Uani 1 8 d S . .
Sb2 Sb 0.5000 0.5000 0.0000 0.0228(6) Uani 1 8 d S . .
Sb3 Sb 0.0000 0.36816(9) 0.09982(7) 0.0200(3) Uani 1 2 d S . .
Sb4 Sb 0.0000 0.21110(7) 0.30271(5) 0.0077(3) Uani 1 2 d S . .
Sb5 Sb 0.0000 0.34555(10) 0.5000 0.0116(3) Uani 1 4 d S . .
Sb6 Sb 0.5000 0.0000 0.19803(7) 0.0069(3) Uani 1 4 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sb6 Dy1 Sb6 83.22(5) 1_455 . ?
Sb6 Dy1 Sb4 84.81(2) 1_455 . ?
Sb6 Dy1 Sb4 84.81(2) . . ?
Sb6 Dy1 Sb4 84.81(2) 1_455 2 ?
Sb6 Dy1 Sb4 84.81(2) . 2 ?
Sb4 Dy1 Sb4 166.09(5) . 2 ?
Sb6 Dy1 Sb3 140.14(3) 1_455 13 ?
Sb6 Dy1 Sb3 84.54(3) . 13 ?
Sb4 Dy1 Sb3 56.35(3) . 13 ?
Sb4 Dy1 Sb3 131.53(3) 2 13 ?
Sb6 Dy1 Sb3 84.54(3) 1_455 14_445 ?
Sb6 Dy1 Sb3 140.14(3) . 14_445 ?
Sb4 Dy1 Sb3 131.53(3) . 14_445 ?
Sb4 Dy1 Sb3 56.35(3) 2 14_445 ?
Sb3 Dy1 Sb3 126.55(6) 13 14_445 ?
Sb6 Dy1 Sb3 84.54(3) 1_455 13_455 ?
Sb6 Dy1 Sb3 140.14(3) . 13_455 ?
Sb4 Dy1 Sb3 56.35(3) . 13_455 ?
Sb4 Dy1 Sb3 131.53(3) 2 13_455 ?
Sb3 Dy1 Sb3 81.02(4) 13 13_455 ?
Sb3 Dy1 Sb3 75.62(5) 14_445 13_455 ?
Sb6 Dy1 Sb3 140.14(3) 1_455 14_545 ?
Sb6 Dy1 Sb3 84.54(3) . 14_545 ?
Sb4 Dy1 Sb3 131.53(3) . 14_545 ?
Sb4 Dy1 Sb3 56.35(3) 2 14_545 ?
Sb3 Dy1 Sb3 75.62(5) 13 14_545 ?
Sb3 Dy1 Sb3 81.02(4) 14_445 14_545 ?
Sb3 Dy1 Sb3 126.55(6) 13_455 14_545 ?
Sb6 Dy1 Sb2 138.39(3) 1_455 5_445 ?
Sb6 Dy1 Sb2 138.39(3) . 5_445 ?
Sb4 Dy1 Sb2 96.95(3) . 5_445 ?
Sb4 Dy1 Sb2 96.95(3) 2 5_445 ?
Sb3 Dy1 Sb2 63.27(3) 13 5_445 ?
Sb3 Dy1 Sb2 63.27(3) 14_445 5_445 ?
Sb3 Dy1 Sb2 63.27(3) 13_455 5_445 ?
Sb3 Dy1 Sb2 63.27(3) 14_545 5_445 ?
Zn1 Dy2 Sb6 132.78(4) . 1_455 ?
Zn1 Dy2 Sb6 132.78(4) . . ?
Sb6 Dy2 Sb6 82.73(3) 1_455 . ?
Zn1 Dy2 Sb4 83.31(6) . 13 ?
Sb6 Dy2 Sb4 138.06(4) 1_455 13 ?
Sb6 Dy2 Sb4 84.30(3) . 13 ?
Zn1 Dy2 Sb4 83.31(6) . 13_455 ?
Sb6 Dy2 Sb4 84.30(3) 1_455 13_455 ?
Sb6 Dy2 Sb4 138.06(4) . 13_455 ?
Sb4 Dy2 Sb4 79.26(4) 13 13_455 ?
Zn1 Dy2 Sb1 74.57(7) . . ?
Sb6 Dy2 Sb1 82.70(3) 1_455 . ?
Sb6 Dy2 Sb1 82.70(3) . . ?
Sb4 Dy2 Sb1 134.65(2) 13 . ?
Sb4 Dy2 Sb1 134.65(2) 13_455 . ?
Zn1 Dy2 Sb4 125.20(7) . . ?
Sb6 Dy2 Sb4 82.50(3) 1_455 . ?
Sb6 Dy2 Sb4 82.50(3) . . ?
Sb4 Dy2 Sb4 56.30(3) 13 . ?
Sb4 Dy2 Sb4 56.30(3) 13_455 . ?
Sb1 Dy2 Sb4 160.23(3) . . ?
Zn1 Dy2 Sb5 47.91(4) . 13_455 ?
Sb6 Dy2 Sb5 85.05(3) 1_455 13_455 ?
Sb6 Dy2 Sb5 138.27(4) . 13_455 ?
Sb4 Dy2 Sb5 128.48(4) 13 13_455 ?
Sb4 Dy2 Sb5 79.55(3) 13_455 13_455 ?
Sb1 Dy2 Sb5 56.19(3) . 13_455 ?
Sb4 Dy2 Sb5 134.99(3) . 13_455 ?
Zn1 Dy2 Sb5 47.91(4) . 13 ?
Sb6 Dy2 Sb5 138.27(4) 1_455 13 ?
Sb6 Dy2 Sb5 85.05(3) . 13 ?
Sb4 Dy2 Sb5 79.55(3) 13 13 ?
Sb4 Dy2 Sb5 128.48(4) 13_455 13 ?
Sb1 Dy2 Sb5 56.19(3) . 13 ?
Sb4 Dy2 Sb5 134.99(3) . 13 ?
Sb5 Dy2 Sb5 78.09(3) 13_455 13 ?
Zn1 Dy2 Sb3 43.02(7) . . ?
Sb6 Dy2 Sb3 135.598(18) 1_455 . ?
Sb6 Dy2 Sb3 135.598(18) . . ?
Sb4 Dy2 Sb3 52.80(3) 13 . ?
Sb4 Dy2 Sb3 52.80(3) 13_455 . ?
Sb1 Dy2 Sb3 117.59(4) . . ?
Sb4 Dy2 Sb3 82.18(4) . . ?
Sb5 Dy2 Sb3 77.14(3) 13_455 . ?
Sb5 Dy2 Sb3 77.14(3) 13 . ?
Sb3 Zn1 Sb3 99.24(16) . 10 ?
Sb3 Zn1 Sb5 113.20(2) . 13_455 ?
Sb3 Zn1 Sb5 113.20(2) 10 13_455 ?
Sb3 Zn1 Sb5 113.20(2) . 13 ?
Sb3 Zn1 Sb5 113.20(2) 10 13 ?
Sb5 Zn1 Sb5 105.09(16) 13_455 13 ?
Sb3 Zn1 Dy2 175.26(14) . 10 ?
Sb3 Zn1 Dy2 76.02(4) 10 10 ?
Sb5 Zn1 Dy2 69.25(7) 13_455 10 ?
Sb5 Zn1 Dy2 69.25(7) 13 10 ?
Sb3 Zn1 Dy2 76.02(4) . . ?
Sb3 Zn1 Dy2 175.26(14) 10 . ?
Sb5 Zn1 Dy2 69.25(7) 13_455 . ?
Sb5 Zn1 Dy2 69.25(7) 13 . ?
Dy2 Zn1 Dy2 108.73(13) 10 . ?
Sb5 Sb1 Sb5 180.00(4) 13 5_444 ?
Sb5 Sb1 Sb5 84.26(5) 13 13_455 ?
Sb5 Sb1 Sb5 95.74(5) 5_444 13_455 ?
Sb5 Sb1 Sb5 95.74(5) 13 5_544 ?
Sb5 Sb1 Sb5 84.26(5) 5_444 5_544 ?
Sb5 Sb1 Sb5 180.00(4) 13_455 5_544 ?
Sb5 Sb1 Dy2 62.225(18) 13 . ?
Sb5 Sb1 Dy2 117.775(18) 5_444 . ?
Sb5 Sb1 Dy2 62.225(18) 13_455 . ?
Sb5 Sb1 Dy2 117.775(18) 5_544 . ?
Sb5 Sb1 Dy2 117.775(18) 13 9 ?
Sb5 Sb1 Dy2 62.225(18) 5_444 9 ?
Sb5 Sb1 Dy2 117.775(18) 13_455 9 ?
Sb5 Sb1 Dy2 62.225(18) 5_544 9 ?
Dy2 Sb1 Dy2 180.000(16) . 9 ?
Sb5 Sb1 Dy2 117.775(18) 13 2 ?
Sb5 Sb1 Dy2 62.225(18) 5_444 2 ?
Sb5 Sb1 Dy2 117.775(18) 13_455 2 ?
Sb5 Sb1 Dy2 62.225(18) 5_544 2 ?
Dy2 Sb1 Dy2 77.86(4) . 2 ?
Dy2 Sb1 Dy2 102.14(4) 9 2 ?
Sb5 Sb1 Dy2 62.225(18) 13 10 ?
Sb5 Sb1 Dy2 117.775(18) 5_444 10 ?
Sb5 Sb1 Dy2 62.225(18) 13_455 10 ?
Sb5 Sb1 Dy2 117.775(18) 5_544 10 ?
Dy2 Sb1 Dy2 102.14(4) . 10 ?
Dy2 Sb1 Dy2 77.86(4) 9 10 ?
Dy2 Sb1 Dy2 180.00(2) 2 10 ?
Dy1 Sb2 Dy1 180.0 13 5_554 ?
Zn1 Sb3 Sb4 101.98(7) . 13 ?
Zn1 Sb3 Sb4 101.98(7) . 13_455 ?
Sb4 Sb3 Sb4 87.52(5) 13 13_455 ?
Zn1 Sb3 Dy1 137.71(3) . 13 ?
Sb4 Sb3 Dy1 61.22(3) 13 13 ?
Sb4 Sb3 Dy1 114.65(5) 13_455 13 ?
Zn1 Sb3 Dy1 137.71(3) . 13_455 ?
Sb4 Sb3 Dy1 114.65(5) 13 13_455 ?
Sb4 Sb3 Dy1 61.22(3) 13_455 13_455 ?
Dy1 Sb3 Dy1 81.02(4) 13 13_455 ?
Zn1 Sb3 Dy2 60.96(8) . . ?
Sb4 Sb3 Dy2 59.74(3) 13 . ?
Sb4 Sb3 Dy2 59.74(3) 13_455 . ?
Dy1 Sb3 Dy2 120.84(3) 13 . ?
Dy1 Sb3 Dy2 120.84(3) 13_455 . ?
Sb3 Sb4 Sb3 87.52(5) 13 13_455 ?
Sb3 Sb4 Sb4 177.66(6) 13 13_455 ?
Sb3 Sb4 Sb4 93.93(3) 13_455 13_455 ?
Sb3 Sb4 Sb4 93.93(3) 13 13 ?
Sb3 Sb4 Sb4 177.66(6) 13_455 13 ?
Sb4 Sb4 Sb4 84.56(5) 13_455 13 ?
Sb3 Sb4 Dy1 62.42(3) 13 . ?
Sb3 Sb4 Dy1 62.42(3) 13_455 . ?
Sb4 Sb4 Dy1 116.69(4) 13_455 . ?
Sb4 Sb4 Dy1 116.69(4) 13 . ?
Sb3 Sb4 Dy2 67.46(4) 13 13 ?
Sb3 Sb4 Dy2 119.94(5) 13_455 13 ?
Sb4 Sb4 Dy2 113.23(5) 13_455 13 ?
Sb4 Sb4 Dy2 62.37(3) 13 13 ?
Dy1 Sb4 Dy2 129.74(3) . 13 ?
Sb3 Sb4 Dy2 119.94(5) 13 13_455 ?
Sb3 Sb4 Dy2 67.46(4) 13_455 13_455 ?
Sb4 Sb4 Dy2 62.37(3) 13_455 13_455 ?
Sb4 Sb4 Dy2 113.23(5) 13 13_455 ?
Dy1 Sb4 Dy2 129.74(3) . 13_455 ?
Dy2 Sb4 Dy2 79.26(4) 13 13_455 ?
Sb3 Sb4 Dy2 116.36(4) 13 . ?
Sb3 Sb4 Dy2 116.36(4) 13_455 . ?
Sb4 Sb4 Dy2 61.33(4) 13_455 . ?
Sb4 Sb4 Dy2 61.33(4) 13 . ?
Dy1 Sb4 Dy2 77.80(3) . . ?
Dy2 Sb4 Dy2 123.70(3) 13 . ?
Dy2 Sb4 Dy2 123.70(3) 13_455 . ?
Zn1 Sb5 Zn1 105.09(16) 13_455 13 ?
Zn1 Sb5 Sb1 169.59(9) 13_455 5 ?
Zn1 Sb5 Sb1 85.33(8) 13 5 ?
Zn1 Sb5 Sb1 85.33(8) 13_455 5_455 ?
Zn1 Sb5 Sb1 169.59(9) 13 5_455 ?
Sb1 Sb5 Sb1 84.26(5) 5 5_455 ?
Zn1 Sb5 Dy2 62.85(4) 13_455 13_455 ?
Zn1 Sb5 Dy2 122.94(4) 13 13_455 ?
Sb1 Sb5 Dy2 111.67(4) 5 13_455 ?
Sb1 Sb5 Dy2 61.59(2) 5_455 13_455 ?
Zn1 Sb5 Dy2 122.94(4) 13_455 6 ?
Zn1 Sb5 Dy2 62.85(4) 13 6 ?
Sb1 Sb5 Dy2 61.59(2) 5 6 ?
Sb1 Sb5 Dy2 111.67(4) 5_455 6 ?
Dy2 Sb5 Dy2 171.76(6) 13_455 6 ?
Zn1 Sb5 Dy2 122.94(4) 13_455 13 ?
Zn1 Sb5 Dy2 62.85(4) 13 13 ?
Sb1 Sb5 Dy2 61.59(2) 5 13 ?
Sb1 Sb5 Dy2 111.67(4) 5_455 13 ?
Dy2 Sb5 Dy2 78.09(3) 13_455 13 ?
Dy2 Sb5 Dy2 101.31(3) 6 13 ?
Zn1 Sb5 Dy2 62.85(4) 13_455 6_455 ?
Zn1 Sb5 Dy2 122.94(4) 13 6_455 ?
Sb1 Sb5 Dy2 111.67(4) 5 6_455 ?
Sb1 Sb5 Dy2 61.59(2) 5_455 6_455 ?
Dy2 Sb5 Dy2 101.31(3) 13_455 6_455 ?
Dy2 Sb5 Dy2 78.09(3) 6 6_455 ?
Dy2 Sb5 Dy2 171.76(6) 13 6_455 ?
Dy1 Sb6 Dy1 83.22(5) 1_655 . ?
Dy1 Sb6 Dy2 135.43(3) 1_655 2 ?
Dy1 Sb6 Dy2 80.49(3) . 2 ?
Dy1 Sb6 Dy2 80.49(3) 1_655 1_655 ?
Dy1 Sb6 Dy2 135.43(3) . 1_655 ?
Dy2 Sb6 Dy2 137.08(6) 2 1_655 ?
Dy1 Sb6 Dy2 135.43(3) 1_655 . ?
Dy1 Sb6 Dy2 80.49(3) . . ?
Dy2 Sb6 Dy2 81.88(4) 2 . ?
Dy2 Sb6 Dy2 82.73(3) 1_655 . ?
Dy1 Sb6 Dy2 80.49(3) 1_655 2_655 ?
Dy1 Sb6 Dy2 135.43(3) . 2_655 ?
Dy2 Sb6 Dy2 82.73(3) 2 2_655 ?
Dy2 Sb6 Dy2 81.88(4) 1_655 2_655 ?
Dy2 Sb6 Dy2 137.08(6) . 2_655 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 Sb6 3.1149(15) 1_455 ?
Dy1 Sb6 3.1149(15) . ?
Dy1 Sb4 3.1487(14) . ?
Dy1 Sb4 3.1487(14) 2 ?
Dy1 Sb3 3.1843(13) 13 ?
Dy1 Sb3 3.1843(13) 14_445 ?
Dy1 Sb3 3.1843(13) 13_455 ?
Dy1 Sb3 3.1843(13) 14_545 ?
Dy1 Sb2 3.2893(16) 5_445 ?
Dy2 Zn1 3.124(3) . ?
Dy2 Sb6 3.1299(10) 1_455 ?
Dy2 Sb6 3.1299(10) . ?
Dy2 Sb4 3.2427(11) 13 ?
Dy2 Sb4 3.2427(11) 13_455 ?
Dy2 Sb1 3.2641(11) . ?
Dy2 Sb4 3.2742(16) . ?
Dy2 Sb5 3.2835(10) 13_455 ?
Dy2 Sb5 3.2835(10) 13 ?
Dy2 Sb3 3.4677(18) . ?
Zn1 Sb3 2.438(3) . ?
Zn1 Sb3 2.438(3) 10 ?
Zn1 Sb5 2.606(3) 13_455 ?
Zn1 Sb5 2.606(3) 13 ?
Zn1 Dy2 3.124(3) 10 ?
Sb1 Sb5 3.0834(13) 13 ?
Sb1 Sb5 3.0834(13) 5_444 ?
Sb1 Sb5 3.0834(13) 13_455 ?
Sb1 Sb5 3.0834(13) 5_544 ?
Sb1 Dy2 3.2641(11) 9 ?
Sb1 Dy2 3.2641(11) 2 ?
Sb1 Dy2 3.2641(11) 10 ?
Sb2 Dy1 3.2893(16) 13 ?
Sb2 Dy1 3.2893(16) 5_554 ?
Sb3 Sb4 2.9906(13) 13 ?
Sb3 Sb4 2.9906(13) 13_455 ?
Sb3 Dy1 3.1843(13) 13 ?
Sb3 Dy1 3.1843(13) 13_455 ?
Sb4 Sb3 2.9906(13) 13 ?
Sb4 Sb3 2.9906(13) 13_455 ?
Sb4 Sb4 3.0745(16) 13_455 ?
Sb4 Sb4 3.0745(16) 13 ?
Sb4 Dy2 3.2427(11) 13 ?
Sb4 Dy2 3.2427(11) 13_455 ?
Sb5 Zn1 2.606(3) 13_455 ?
Sb5 Zn1 2.606(3) 13 ?
Sb5 Sb1 3.0834(13) 5 ?
Sb5 Sb1 3.0834(13) 5_455 ?
Sb5 Dy2 3.2835(10) 13_455 ?
Sb5 Dy2 3.2835(10) 6 ?
Sb5 Dy2 3.2835(10) 13 ?
Sb5 Dy2 3.2835(10) 6_455 ?
Sb6 Dy1 3.1149(15) 1_655 ?
Sb6 Dy2 3.1299(10) 2 ?
Sb6 Dy2 3.1299(10) 1_655 ?
Sb6 Dy2 3.1299(10) 2_655 ?
