#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/55/4305531.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305531
loop_
_publ_author_name
'Yi Liu'
'Ling Chen'
'Long-Hua Li'
'Li-Ming Wu'
'Oksana Ya. Zelinska'
'Arthur Mar'
_publ_contact_author_address
; Department of Chemistry
  University of Alberta
  Edmonton, AB
  Canada  T6G 2G2
;
_publ_contact_author_email       arthur.mar@ualberta.ca
_publ_contact_author_fax         '(780) 492-8231'
_publ_contact_author_name        'Dr. Arthur Mar'
_publ_contact_author_phone       '(780) 492-5592'
_publ_section_title
;
Structures and Physical Properties of Rare-Earth Zinc Antimonides
Pr6Zn1+xSb14+yandRE6Zn1+xSb14 (RE= Sm, Gd-Ho)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11930
_journal_page_last               11941
_journal_paper_doi               10.1021/ic800524d
_journal_volume                  47
_journal_year                    2008
_chemical_formula_sum            'Ho12 Sb28 Zn2.6'
_chemical_formula_weight         5558.12
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           'by CrystalClear-SM 1.3.6 SP3 rc4'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            1
_cell_length_a                   4.1296(15)
_cell_length_b                   14.744(6)
_cell_length_c                   18.570(7)
_cell_measurement_reflns_used    1742
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.1933
_cell_volume                     1130.7(7)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0668
_diffrn_reflns_av_sigmaI/netI    0.0460
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -4
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            4211
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.19
_exptl_absorpt_coefficient_mu    38.435
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.3944
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Grey
_exptl_crystal_density_diffrn    8.162
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             2310
_exptl_crystal_size_max          0.1800
_exptl_crystal_size_mid          0.0400
_exptl_crystal_size_min          0.0200
_refine_diff_density_max         12.454
_refine_diff_density_min         -11.155
_refine_diff_density_rms         1.749
_refine_ls_extinction_coef       0.00187(16)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.198
_refine_ls_matrix_type           full
_refine_ls_number_parameters     43
_refine_ls_number_reflns         790
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.198
_refine_ls_R_factor_all          0.0593
_refine_ls_R_factor_gt           0.0537
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0668P)²+119.7991P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1307
_refine_ls_wR_factor_ref         0.1409
_reflns_number_gt                686
_reflns_number_total             790
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic800524d_si_001_5.cif
_cod_data_source_block           Ho
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_formula_sum        'Ho12 Sb28 Zn2.60'
_cod_database_code               4305531
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ho1 Ho 0.0000 0.0000 0.32311(8) 0.0105(4) Uani 1 4 d S . .
Ho2 Ho 0.0000 0.13857(7) 0.13656(5) 0.0084(4) Uani 1 2 d S . .
Zn1 Zn 0.0000 0.2616(5) 0.0000 0.018(2) Uani 0.651(19) 4 d SP . .
Sb1 Sb 0.0000 0.0000 0.0000 0.084(3) Uani 1 8 d S . .
Sb2 Sb 0.5000 0.5000 0.0000 0.0230(8) Uani 1 8 d S . .
Sb3 Sb 0.0000 0.36787(13) 0.09926(10) 0.0213(5) Uani 1 2 d S . .
Sb4 Sb 0.0000 0.21104(10) 0.30278(7) 0.0085(4) Uani 1 2 d S . .
Sb5 Sb 0.0000 0.34491(16) 0.5000 0.0130(5) Uani 1 4 d S . .
Sb6 Sb 0.5000 0.0000 0.19800(11) 0.0075(5) Uani 1 4 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ho Ho -0.2175 4.6783 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sb6 Ho1 Sb6 83.26(7) 1_455 . ?
Sb6 Ho1 Sb4 84.83(3) 1_455 2 ?
Sb6 Ho1 Sb4 84.83(3) . 2 ?
Sb6 Ho1 Sb4 84.83(3) 1_455 . ?
Sb6 Ho1 Sb4 84.83(3) . . ?
Sb4 Ho1 Sb4 166.16(7) 2 . ?
Sb6 Ho1 Sb3 140.29(4) 1_455 13 ?
Sb6 Ho1 Sb3 84.70(4) . 13 ?
Sb4 Ho1 Sb3 131.45(4) 2 13 ?
Sb4 Ho1 Sb3 56.44(4) . 13 ?
Sb6 Ho1 Sb3 84.70(4) 1_455 14_445 ?
Sb6 Ho1 Sb3 140.29(4) . 14_445 ?
Sb4 Ho1 Sb3 56.44(4) 2 14_445 ?
Sb4 Ho1 Sb3 131.45(4) . 14_445 ?
Sb3 Ho1 Sb3 126.15(8) 13 14_445 ?
Sb6 Ho1 Sb3 84.70(4) 1_455 13_455 ?
Sb6 Ho1 Sb3 140.29(4) . 13_455 ?
Sb4 Ho1 Sb3 131.45(4) 2 13_455 ?
Sb4 Ho1 Sb3 56.44(4) . 13_455 ?
Sb3 Ho1 Sb3 80.86(6) 13 13_455 ?
Sb3 Ho1 Sb3 75.45(7) 14_445 13_455 ?
Sb6 Ho1 Sb3 140.29(4) 1_455 14_545 ?
Sb6 Ho1 Sb3 84.70(4) . 14_545 ?
Sb4 Ho1 Sb3 56.44(4) 2 14_545 ?
Sb4 Ho1 Sb3 131.45(4) . 14_545 ?
Sb3 Ho1 Sb3 75.45(7) 13 14_545 ?
Sb3 Ho1 Sb3 80.86(6) 14_445 14_545 ?
Sb3 Ho1 Sb3 126.15(8) 13_455 14_545 ?
Sb6 Ho1 Sb2 138.37(3) 1_455 5_445 ?
Sb6 Ho1 Sb2 138.37(3) . 5_445 ?
Sb4 Ho1 Sb2 96.92(4) 2 5_445 ?
Sb4 Ho1 Sb2 96.92(4) . 5_445 ?
Sb3 Ho1 Sb2 63.08(4) 13 5_445 ?
Sb3 Ho1 Sb2 63.08(4) 14_445 5_445 ?
Sb3 Ho1 Sb2 63.08(4) 13_455 5_445 ?
Sb3 Ho1 Sb2 63.08(4) 14_545 5_445 ?
Zn1 Ho2 Sb6 132.71(6) . 1_455 ?
Zn1 Ho2 Sb6 132.71(6) . . ?
Sb6 Ho2 Sb6 82.85(4) 1_455 . ?
Zn1 Ho2 Sb4 83.36(9) . 13 ?
Sb6 Ho2 Sb4 138.10(6) 1_455 13 ?
Sb6 Ho2 Sb4 84.21(4) . 13 ?
Zn1 Ho2 Sb4 83.36(9) . 13_455 ?
Sb6 Ho2 Sb4 84.21(4) 1_455 13_455 ?
Sb6 Ho2 Sb4 138.10(6) . 13_455 ?
Sb4 Ho2 Sb4 79.40(5) 13 13_455 ?
Zn1 Ho2 Sb1 74.43(11) . . ?
Sb6 Ho2 Sb1 82.76(4) 1_455 . ?
Sb6 Ho2 Sb1 82.76(4) . . ?
Sb4 Ho2 Sb1 134.57(3) 13 . ?
Sb4 Ho2 Sb1 134.57(3) 13_455 . ?
Zn1 Ho2 Sb4 125.33(11) . . ?
Sb6 Ho2 Sb4 82.45(5) 1_455 . ?
Sb6 Ho2 Sb4 82.45(5) . . ?
Sb4 Ho2 Sb4 56.38(4) 13 . ?
Sb4 Ho2 Sb4 56.38(4) 13_455 . ?
Sb1 Ho2 Sb4 160.24(5) . . ?
Zn1 Ho2 Sb5 47.76(7) . 13_455 ?
Sb6 Ho2 Sb5 85.11(5) 1_455 13_455 ?
Sb6 Ho2 Sb5 138.41(6) . 13_455 ?
Sb4 Ho2 Sb5 128.37(6) 13 13_455 ?
Sb4 Ho2 Sb5 79.42(4) 13_455 13_455 ?
Sb1 Ho2 Sb5 56.25(4) . 13_455 ?
Sb4 Ho2 Sb5 134.95(4) . 13_455 ?
Zn1 Ho2 Sb5 47.76(7) . 13 ?
Sb6 Ho2 Sb5 138.41(6) 1_455 13 ?
Sb6 Ho2 Sb5 85.11(5) . 13 ?
Sb4 Ho2 Sb5 79.42(4) 13 13 ?
Sb4 Ho2 Sb5 128.37(6) 13_455 13 ?
Sb1 Ho2 Sb5 56.25(4) . 13 ?
Sb4 Ho2 Sb5 134.95(4) . 13 ?
Sb5 Ho2 Sb5 78.05(4) 13_455 13 ?
Zn1 Ho2 Sb3 42.85(11) . . ?
Sb6 Ho2 Sb3 135.62(2) 1_455 . ?
Sb6 Ho2 Sb3 135.62(2) . . ?
Sb4 Ho2 Sb3 52.98(4) 13 . ?
Sb4 Ho2 Sb3 52.98(4) 13_455 . ?
Sb1 Ho2 Sb3 117.28(5) . . ?
Sb4 Ho2 Sb3 82.48(5) . . ?
Sb5 Ho2 Sb3 76.82(5) 13_455 . ?
Sb5 Ho2 Sb3 76.82(5) 13 . ?
Sb3 Zn1 Sb3 99.3(3) . 10 ?
Sb3 Zn1 Sb5 113.09(3) . 13_455 ?
Sb3 Zn1 Sb5 113.09(3) 10 13_455 ?
Sb3 Zn1 Sb5 113.09(3) . 13 ?
Sb3 Zn1 Sb5 113.09(3) 10 13 ?
Sb5 Zn1 Sb5 105.5(3) 13_455 13 ?
Sb3 Zn1 Ho2 75.95(6) . . ?
Sb3 Zn1 Ho2 175.2(2) 10 . ?
Sb5 Zn1 Ho2 69.38(12) 13_455 . ?
Sb5 Zn1 Ho2 69.38(12) 13 . ?
Sb3 Zn1 Ho2 175.2(2) . 10 ?
Sb3 Zn1 Ho2 75.95(6) 10 10 ?
Sb5 Zn1 Ho2 69.38(12) 13_455 10 ?
Sb5 Zn1 Ho2 69.38(12) 13 10 ?
Ho2 Zn1 Ho2 108.8(2) . 10 ?
Sb5 Sb1 Sb5 180.00(6) 5_444 13 ?
Sb5 Sb1 Sb5 84.16(7) 5_444 5_544 ?
Sb5 Sb1 Sb5 95.84(7) 13 5_544 ?
Sb5 Sb1 Sb5 95.84(7) 5_444 13_455 ?
Sb5 Sb1 Sb5 84.16(7) 13 13_455 ?
Sb5 Sb1 Sb5 180.00(6) 5_544 13_455 ?
Sb5 Sb1 Ho2 117.75(2) 5_444 . ?
Sb5 Sb1 Ho2 62.25(2) 13 . ?
Sb5 Sb1 Ho2 117.75(2) 5_544 . ?
Sb5 Sb1 Ho2 62.25(2) 13_455 . ?
Sb5 Sb1 Ho2 62.25(2) 5_444 9 ?
Sb5 Sb1 Ho2 117.75(2) 13 9 ?
Sb5 Sb1 Ho2 62.25(2) 5_544 9 ?
Sb5 Sb1 Ho2 117.75(2) 13_455 9 ?
Ho2 Sb1 Ho2 180.00(4) . 9 ?
Sb5 Sb1 Ho2 117.75(2) 5_444 10 ?
Sb5 Sb1 Ho2 62.25(2) 13 10 ?
Sb5 Sb1 Ho2 117.75(2) 5_544 10 ?
Sb5 Sb1 Ho2 62.25(2) 13_455 10 ?
Ho2 Sb1 Ho2 102.28(5) . 10 ?
Ho2 Sb1 Ho2 77.72(5) 9 10 ?
Sb5 Sb1 Ho2 62.25(2) 5_444 2 ?
Sb5 Sb1 Ho2 117.75(2) 13 2 ?
Sb5 Sb1 Ho2 62.25(2) 5_544 2 ?
Sb5 Sb1 Ho2 117.75(2) 13_455 2 ?
Ho2 Sb1 Ho2 77.72(5) . 2 ?
Ho2 Sb1 Ho2 102.28(5) 9 2 ?
Ho2 Sb1 Ho2 180.00(4) 10 2 ?
Ho1 Sb2 Ho1 180.0 5_554 13 ?
Zn1 Sb3 Sb4 102.22(11) . 13 ?
Zn1 Sb3 Sb4 102.22(11) . 13_455 ?
Sb4 Sb3 Sb4 87.43(7) 13 13_455 ?
Zn1 Sb3 Ho1 137.84(5) . 13 ?
Sb4 Sb3 Ho1 60.95(4) 13 13 ?
Sb4 Sb3 Ho1 114.25(7) 13_455 13 ?
Zn1 Sb3 Ho1 137.84(5) . 13_455 ?
Sb4 Sb3 Ho1 114.25(7) 13 13_455 ?
Sb4 Sb3 Ho1 60.95(4) 13_455 13_455 ?
Ho1 Sb3 Ho1 80.86(6) 13 13_455 ?
Zn1 Sb3 Ho2 61.21(13) . . ?
Sb4 Sb3 Ho2 59.75(4) 13 . ?
Sb4 Sb3 Ho2 59.75(4) 13_455 . ?
Ho1 Sb3 Ho2 120.57(5) 13 . ?
Ho1 Sb3 Ho2 120.57(5) 13_455 . ?
Sb3 Sb4 Sb3 87.43(7) 13 13_455 ?
Sb3 Sb4 Sb4 177.82(8) 13 13_455 ?
Sb3 Sb4 Sb4 94.00(4) 13_455 13_455 ?
Sb3 Sb4 Sb4 94.00(4) 13 13 ?
Sb3 Sb4 Sb4 177.82(8) 13_455 13 ?
Sb4 Sb4 Sb4 84.53(8) 13_455 13 ?
Sb3 Sb4 Ho1 62.62(5) 13 . ?
Sb3 Sb4 Ho1 62.61(5) 13_455 . ?
Sb4 Sb4 Ho1 116.64(6) 13_455 . ?
Sb4 Sb4 Ho1 116.64(6) 13 . ?
Sb3 Sb4 Ho2 67.26(5) 13 13 ?
Sb3 Sb4 Ho2 119.76(6) 13_455 13 ?
Sb4 Sb4 Ho2 113.29(7) 13_455 13 ?
Sb4 Sb4 Ho2 62.37(5) 13 13 ?
Ho1 Sb4 Ho2 129.71(4) . 13 ?
Sb3 Sb4 Ho2 119.76(6) 13 13_455 ?
Sb3 Sb4 Ho2 67.26(5) 13_455 13_455 ?
Sb4 Sb4 Ho2 62.37(5) 13_455 13_455 ?
Sb4 Sb4 Ho2 113.29(7) 13 13_455 ?
Ho1 Sb4 Ho2 129.71(4) . 13_455 ?
Ho2 Sb4 Ho2 79.40(5) 13 13_455 ?
Sb3 Sb4 Ho2 116.62(6) 13 . ?
Sb3 Sb4 Ho2 116.61(6) 13_455 . ?
Sb4 Sb4 Ho2 61.25(5) 13_455 . ?
Sb4 Sb4 Ho2 61.25(5) 13 . ?
Ho1 Sb4 Ho2 77.82(5) . . ?
Ho2 Sb4 Ho2 123.62(4) 13 . ?
Ho2 Sb4 Ho2 123.62(4) 13_455 . ?
Zn1 Sb5 Zn1 105.5(3) 13_455 13 ?
Zn1 Sb5 Sb1 169.33(14) 13_455 5 ?
Zn1 Sb5 Sb1 85.17(13) 13 5 ?
Zn1 Sb5 Sb1 85.17(13) 13_455 5_455 ?
Zn1 Sb5 Sb1 169.33(14) 13 5_455 ?
Sb1 Sb5 Sb1 84.16(7) 5 5_455 ?
Zn1 Sb5 Ho2 123.10(7) 13_455 6 ?
Zn1 Sb5 Ho2 62.86(6) 13 6 ?
Sb1 Sb5 Ho2 61.50(3) 5 6 ?
Sb1 Sb5 Ho2 111.52(5) 5_455 6 ?
Zn1 Sb5 Ho2 62.86(6) 13_455 13_455 ?
Zn1 Sb5 Ho2 123.10(7) 13 13_455 ?
Sb1 Sb5 Ho2 111.52(5) 5 13_455 ?
Sb1 Sb5 Ho2 61.50(3) 5_455 13_455 ?
Ho2 Sb5 Ho2 171.48(9) 6 13_455 ?
Zn1 Sb5 Ho2 62.86(6) 13_455 6_455 ?
Zn1 Sb5 Ho2 123.10(7) 13 6_455 ?
Sb1 Sb5 Ho2 111.52(5) 5 6_455 ?
Sb1 Sb5 Ho2 61.50(3) 5_455 6_455 ?
Ho2 Sb5 Ho2 78.05(4) 6 6_455 ?
Ho2 Sb5 Ho2 101.31(4) 13_455 6_455 ?
Zn1 Sb5 Ho2 123.10(7) 13_455 13 ?
Zn1 Sb5 Ho2 62.86(6) 13 13 ?
Sb1 Sb5 Ho2 61.50(3) 5 13 ?
Sb1 Sb5 Ho2 111.52(5) 5_455 13 ?
Ho2 Sb5 Ho2 101.31(4) 6 13 ?
Ho2 Sb5 Ho2 78.05(4) 13_455 13 ?
Ho2 Sb5 Ho2 171.48(9) 6_455 13 ?
Ho1 Sb6 Ho1 83.26(7) 1_655 . ?
Ho1 Sb6 Ho2 135.46(4) 1_655 2 ?
Ho1 Sb6 Ho2 80.43(3) . 2 ?
Ho1 Sb6 Ho2 80.43(3) 1_655 1_655 ?
Ho1 Sb6 Ho2 135.46(4) . 1_655 ?
Ho2 Sb6 Ho2 137.11(8) 2 1_655 ?
Ho1 Sb6 Ho2 135.46(4) 1_655 . ?
Ho1 Sb6 Ho2 80.43(3) . . ?
Ho2 Sb6 Ho2 81.79(5) 2 . ?
Ho2 Sb6 Ho2 82.85(4) 1_655 . ?
Ho1 Sb6 Ho2 80.43(3) 1_655 2_655 ?
Ho1 Sb6 Ho2 135.46(4) . 2_655 ?
Ho2 Sb6 Ho2 82.85(4) 2 2_655 ?
Ho2 Sb6 Ho2 81.79(5) 1_655 2_655 ?
Ho2 Sb6 Ho2 137.11(8) . 2_655 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ho1 Sb6 3.108(2) 1_455 ?
Ho1 Sb6 3.108(2) . ?
Ho1 Sb4 3.1346(19) 2 ?
Ho1 Sb4 3.1346(19) . ?
Ho1 Sb3 3.1839(18) 13 ?
Ho1 Sb3 3.1839(18) 14_445 ?
Ho1 Sb3 3.1839(18) 13_455 ?
Ho1 Sb3 3.1839(18) 14_545 ?
Ho1 Sb2 3.2849(19) 5_445 ?
Ho2 Zn1 3.118(4) . ?
Ho2 Sb6 3.1209(13) 1_455 ?
Ho2 Sb6 3.1209(13) . ?
Ho2 Sb4 3.2325(15) 13 ?
Ho2 Sb4 3.2325(15) 13_455 ?
Ho2 Sb1 3.2566(13) . ?
Ho2 Sb4 3.266(2) . ?
Ho2 Sb5 3.2793(12) 13_455 ?
Ho2 Sb5 3.2793(12) 13 ?
Ho2 Sb3 3.451(3) . ?
Zn1 Sb3 2.419(5) . ?
Zn1 Sb3 2.419(5) 10 ?
Zn1 Sb5 2.594(4) 13_455 ?
Zn1 Sb5 2.594(4) 13 ?
Zn1 Ho2 3.118(4) 10 ?
Sb1 Sb5 3.0810(19) 5_444 ?
Sb1 Sb5 3.0810(19) 13 ?
Sb1 Sb5 3.0810(19) 5_544 ?
Sb1 Sb5 3.0810(19) 13_455 ?
Sb1 Ho2 3.2566(13) 9 ?
Sb1 Ho2 3.2566(13) 10 ?
Sb1 Ho2 3.2566(13) 2 ?
Sb2 Ho1 3.2849(19) 5_554 ?
Sb2 Ho1 3.2849(19) 13 ?
Sb3 Sb4 2.9879(18) 13 ?
Sb3 Sb4 2.9879(18) 13_455 ?
Sb3 Ho1 3.1839(18) 13 ?
Sb3 Ho1 3.1839(18) 13_455 ?
Sb4 Sb3 2.9879(18) 13 ?
Sb4 Sb3 2.9879(18) 13_455 ?
Sb4 Sb4 3.070(2) 13_455 ?
Sb4 Sb4 3.070(2) 13 ?
Sb4 Ho2 3.2325(15) 13 ?
Sb4 Ho2 3.2325(15) 13_455 ?
Sb5 Zn1 2.594(5) 13_455 ?
Sb5 Zn1 2.594(4) 13 ?
Sb5 Sb1 3.0810(19) 5 ?
Sb5 Sb1 3.0810(19) 5_455 ?
Sb5 Ho2 3.2793(12) 6 ?
Sb5 Ho2 3.2793(12) 13_455 ?
Sb5 Ho2 3.2793(12) 6_455 ?
Sb5 Ho2 3.2793(12) 13 ?
Sb6 Ho1 3.108(2) 1_655 ?
Sb6 Ho2 3.1209(13) 2 ?
Sb6 Ho2 3.1209(13) 1_655 ?
Sb6 Ho2 3.1209(13) 2_655 ?
