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#$Date: 2016-03-23 00:06:12 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179093 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/55/4305533.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305533
loop_
_publ_author_name
'Yi Liu'
'Ling Chen'
'Long-Hua Li'
'Li-Ming Wu'
'Oksana Ya. Zelinska'
'Arthur Mar'
_publ_contact_author_address
; Department of Chemistry
  University of Alberta
  Edmonton, AB
  Canada  T6G 2G2
;
_publ_contact_author_email       arthur.mar@ualberta.ca
_publ_contact_author_fax         '(780) 492-8231'
_publ_contact_author_name        'Dr. Arthur Mar'
_publ_contact_author_phone       '(780) 492-5592'
_publ_section_title
;
Structures and Physical Properties of Rare-Earth Zinc Antimonides
Pr6Zn1+xSb14+yandRE6Zn1+xSb14 (RE= Sm, Gd-Ho)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11930
_journal_page_last               11941
_journal_paper_doi               10.1021/ic800524d
_journal_volume                  47
_journal_year                    2008
_chemical_formula_structural     'Pr6 Zn1.22 Sb14.59'
_chemical_formula_sum            'Pr6 Sb14.59 Zn1.22'
_chemical_formula_weight         2700.61
_chemical_name_common            'praseodymium zinc antimonide (6/1/15)'
_chemical_name_systematic        'praseodymium zinc antimonide (6/1/15)'
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.2764(4)
_cell_length_b                   15.1483(14)
_cell_length_c                   19.1271(17)
_cell_measurement_reflns_used    1946
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      32.53
_cell_measurement_theta_min      4.26
_cell_volume                     1239.1(2)
_computing_cell_refinement       'Bruker SAINT 7.06 (Bruker, 2004)'
_computing_data_collection       'Bruker SMART 5.054 (Bruker, 1999)'
_computing_data_reduction        'Bruker SAINT 7.06'
_computing_molecular_graphics    'ATOMS 5.1 (Dowty, 1999)'
_computing_publication_material  'Bruker SHELXTL 6.12'
_computing_structure_refinement  'Bruker SHELXTL 6.12'
_computing_structure_solution    'Bruker SHELXTL 6.12'
_diffrn_ambient_temperature      295(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker Platform/SMART 1000 CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0799
_diffrn_reflns_av_sigmaI/netI    0.0498
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            8801
_diffrn_reflns_theta_full        33.13
_diffrn_reflns_theta_max         33.13
_diffrn_reflns_theta_min         1.71
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    28.259
_exptl_absorpt_correction_T_max  0.4835
_exptl_absorpt_correction_T_min  0.1010
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'Bruker SHELXTL 6.12 (Sheldrick, 2001)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    7.239
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2269
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.03
_refine_diff_density_max         9.604
_refine_diff_density_min         -6.027
_refine_diff_density_rms         0.640
_refine_ls_extinction_coef       0.00016(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_matrix_type           full
_refine_ls_number_parameters     48
_refine_ls_number_reflns         1386
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.027
_refine_ls_R_factor_all          0.0649
_refine_ls_R_factor_gt           0.0414
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0371P)²+58.7126P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0862
_refine_ls_wR_factor_ref         0.0953
_reflns_number_gt                1044
_reflns_number_total             1386
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ic800524d_si_003_2.cif
_cod_data_source_block           Pr6ZnSb15
_cod_database_code               4305533
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pr1 Pr 0.0000 0.13870(4) 0.36484(3) 0.00810(15) Uani 1 2 d S . .
Pr2 Pr 0.0000 0.0000 0.17447(5) 0.00938(19) Uani 1 4 d S . .
Zn1 Zn 0.5000 0.0000 0.4366(8) 0.009(4) Uiso 0.124(9) 4 d SP . .
Zn2 Zn 0.0000 0.2603(3) 0.5000 0.0144(13) Uani 0.482(10) 4 d SP . .
Sb1 Sb 0.0000 0.21353(5) 0.20025(4) 0.01038(17) Uani 1 2 d S . .
Sb2 Sb 0.0000 0.35989(6) 0.39501(5) 0.0183(2) Uani 1 2 d S . .
Sb3 Sb 0.5000 0.0000 0.30054(6) 0.0087(2) Uani 1 4 d S . .
Sb4 Sb 0.0000 0.34570(7) 0.0000 0.0110(2) Uani 1 4 d S . .
Sb5A Sb 0.5000 0.5000 0.0000 0.0100(6) Uiso 0.152(9) 8 d SP . .
Sb5B Sb 0.3879(9) 0.5000 0.0000 0.0100(6) Uiso 0.428(5) 4 d SP . .
Sb6A Sb 0.0000 0.0000 0.0000 0.0262(6) Uiso 0.350(5) 8 d SP . .
Sb6B Sb 0.0000 0.09232(17) 0.0000 0.0262(6) Uiso 0.614(5) 4 d SP . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pr Pr -0.2180 2.8214 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Zn2 Pr1 Sb3 133.27(3) . 1_455 ?
Zn2 Pr1 Sb3 133.27(3) . . ?
Sb3 Pr1 Sb3 82.58(2) 1_455 . ?
Zn2 Pr1 Zn1 91.8(2) . 1_455 ?
Sb3 Pr1 Zn1 46.9(3) 1_455 1_455 ?
Sb3 Pr1 Zn1 99.95(9) . 1_455 ?
Zn2 Pr1 Zn1 91.8(2) . . ?
Sb3 Pr1 Zn1 99.95(9) 1_455 . ?
Sb3 Pr1 Zn1 46.9(3) . . ?
Zn1 Pr1 Zn1 80.9(2) 1_455 . ?
Zn2 Pr1 Sb5A 74.58(7) . 5_445 ?
Sb3 Pr1 Sb5A 83.43(2) 1_455 5_445 ?
Sb3 Pr1 Sb5A 83.43(2) . 5_445 ?
Zn1 Pr1 Sb5A 43.53(19) 1_455 5_445 ?
Zn1 Pr1 Sb5A 43.53(19) . 5_445 ?
Zn2 Pr1 Sb1 85.10(5) . 13 ?
Sb3 Pr1 Sb1 135.75(3) 1_455 13 ?
Sb3 Pr1 Sb1 82.559(16) . 13 ?
Zn1 Pr1 Sb1 176.8(2) 1_455 13 ?
Zn1 Pr1 Sb1 99.63(9) . 13 ?
Sb5A Pr1 Sb1 135.455(16) 5_445 13 ?
Zn2 Pr1 Sb1 85.10(5) . 13_455 ?
Sb3 Pr1 Sb1 82.559(16) 1_455 13_455 ?
Sb3 Pr1 Sb1 135.75(3) . 13_455 ?
Zn1 Pr1 Sb1 99.63(9) 1_455 13_455 ?
Zn1 Pr1 Sb1 176.8(2) . 13_455 ?
Sb5A Pr1 Sb1 135.456(16) 5_445 13_455 ?
Sb1 Pr1 Sb1 79.71(2) 13 13_455 ?
Zn2 Pr1 Sb1 124.72(7) . . ?
Sb3 Pr1 Sb1 82.10(2) 1_455 . ?
Sb3 Pr1 Sb1 82.10(2) . . ?
Zn1 Pr1 Sb1 127.4(2) 1_455 . ?
Zn1 Pr1 Sb1 127.4(2) . . ?
Sb5A Pr1 Sb1 160.70(2) 5_445 . ?
Sb1 Pr1 Sb1 54.66(2) 13 . ?
Sb1 Pr1 Sb1 54.66(2) 13_455 . ?
Zn2 Pr1 Sb4 48.18(4) . 13 ?
Sb3 Pr1 Sb4 139.19(3) 1_455 13 ?
Sb3 Pr1 Sb4 85.28(2) . 13 ?
Zn1 Pr1 Sb4 97.9(2) 1_455 13 ?
Zn1 Pr1 Sb4 46.56(19) . 13 ?
Sb5A Pr1 Sb4 56.484(19) 5_445 13 ?
Sb1 Pr1 Sb4 80.34(2) 13 13 ?
Sb1 Pr1 Sb4 130.32(3) 13_455 13 ?
Sb1 Pr1 Sb4 134.378(17) . 13 ?
Zn2 Pr1 Sb4 48.18(4) . 13_455 ?
Sb3 Pr1 Sb4 85.28(2) 1_455 13_455 ?
Sb3 Pr1 Sb4 139.19(3) . 13_455 ?
Zn1 Pr1 Sb4 46.56(19) 1_455 13_455 ?
Zn1 Pr1 Sb4 97.9(2) . 13_455 ?
Sb5A Pr1 Sb4 56.484(19) 5_445 13_455 ?
Sb1 Pr1 Sb4 130.32(3) 13 13_455 ?
Sb1 Pr1 Sb4 80.34(2) 13_455 13_455 ?
Sb1 Pr1 Sb4 134.378(17) . 13_455 ?
Sb4 Pr1 Sb4 78.955(16) 13 13_455 ?
Zn2 Pr1 Sb5B 74.74(6) . 13 ?
Sb3 Pr1 Sb5B 88.90(5) 1_455 13 ?
Sb3 Pr1 Sb5B 78.04(5) . 13 ?
Zn1 Pr1 Sb5B 51.30(19) 1_455 13 ?
Zn1 Pr1 Sb5B 35.9(2) . 13 ?
Sb5A Pr1 Sb5B 8.19(7) 5_445 13 ?
Sb1 Pr1 Sb5B 127.89(7) 13 13 ?
Sb1 Pr1 Sb5B 142.82(6) 13_455 13 ?
Sb1 Pr1 Sb5B 159.10(3) . 13 ?
Sb4 Pr1 Sb5B 50.43(5) 13 13 ?
Sb4 Pr1 Sb5B 62.87(6) 13_455 13 ?
Zn2 Pr1 Sb5B 74.74(6) . 5_445 ?
Sb3 Pr1 Sb5B 78.04(5) 1_455 5_445 ?
Sb3 Pr1 Sb5B 88.90(5) . 5_445 ?
Zn1 Pr1 Sb5B 35.9(2) 1_455 5_445 ?
Zn1 Pr1 Sb5B 51.30(19) . 5_445 ?
Sb5A Pr1 Sb5B 8.19(7) 5_445 5_445 ?
Sb1 Pr1 Sb5B 142.82(6) 13 5_445 ?
Sb1 Pr1 Sb5B 127.89(7) 13_455 5_445 ?
Sb1 Pr1 Sb5B 159.10(4) . 5_445 ?
Sb4 Pr1 Sb5B 62.87(6) 13 5_445 ?
Sb4 Pr1 Sb5B 50.43(5) 13_455 5_445 ?
Sb5B Pr1 Sb5B 16.37(14) 13 5_445 ?
Zn2 Pr1 Sb2 44.76(7) . . ?
Sb3 Pr1 Sb2 134.703(13) 1_455 . ?
Sb3 Pr1 Sb2 134.703(13) . . ?
Zn1 Pr1 Sb2 123.87(14) 1_455 . ?
Zn1 Pr1 Sb2 123.87(14) . . ?
Sb5A Pr1 Sb2 119.33(3) 5_445 . ?
Sb1 Pr1 Sb2 53.285(18) 13 . ?
Sb1 Pr1 Sb2 53.285(18) 13_455 . ?
Sb1 Pr1 Sb2 79.97(3) . . ?
Sb4 Pr1 Sb2 78.48(3) 13 . ?
Sb4 Pr1 Sb2 78.48(3) 13_455 . ?
Sb5B Pr1 Sb2 119.00(3) 13 . ?
Sb5B Pr1 Sb2 119.00(3) 5_445 . ?
Zn2 Pr1 Pr1 125.47(6) . 2 ?
Sb3 Pr1 Pr1 49.577(12) 1_455 2 ?
Sb3 Pr1 Pr1 49.577(12) . 2 ?
Zn1 Pr1 Pr1 50.41(10) 1_455 2 ?
Zn1 Pr1 Pr1 50.41(10) . 2 ?
Sb5A Pr1 Pr1 50.898(11) 5_445 2 ?
Sb1 Pr1 Pr1 132.136(15) 13 2 ?
Sb1 Pr1 Pr1 132.136(15) 13_455 2 ?
Sb1 Pr1 Pr1 109.803(17) . 2 ?
Sb4 Pr1 Pr1 94.03(2) 13 2 ?
Sb4 Pr1 Pr1 94.03(2) 13_455 2 ?
Sb5B Pr1 Pr1 51.371(14) 13 2 ?
Sb5B Pr1 Pr1 51.371(14) 5_445 2 ?
Sb2 Pr1 Pr1 170.23(2) . 2 ?
Zn2 Pr1 Pr2 174.51(7) . . ?
Sb3 Pr1 Pr2 49.245(19) 1_455 . ?
Sb3 Pr1 Pr2 49.245(19) . . ?
Zn1 Pr1 Pr2 92.4(2) 1_455 . ?
Zn1 Pr1 Pr2 92.4(2) . . ?
Sb5A Pr1 Pr2 110.914(18) 5_445 . ?
Sb1 Pr1 Pr2 90.69(2) 13 . ?
Sb1 Pr1 Pr2 90.69(2) 13_455 . ?
Sb1 Pr1 Pr2 49.788(18) . . ?
Sb4 Pr1 Pr2 134.501(17) 13 . ?
Sb4 Pr1 Pr2 134.501(17) 13_455 . ?
Sb5B Pr1 Pr2 110.691(18) 13 . ?
Sb5B Pr1 Pr2 110.691(18) 5_445 . ?
Sb2 Pr1 Pr2 129.75(3) . . ?
Pr1 Pr1 Pr2 60.015(11) 2 . ?
Zn2 Pr1 Pr1 90.0 . 1_455 ?
Sb3 Pr1 Pr1 48.708(11) 1_455 1_455 ?
Sb3 Pr1 Pr1 131.292(11) . 1_455 ?
Zn1 Pr1 Pr1 49.57(10) 1_455 1_455 ?
Zn1 Pr1 Pr1 130.43(10) . 1_455 ?
Sb5A Pr1 Pr1 90.0 5_445 1_455 ?
Sb1 Pr1 Pr1 129.854(12) 13 1_455 ?
Sb1 Pr1 Pr1 50.146(12) 13_455 1_455 ?
Sb1 Pr1 Pr1 90.0 . 1_455 ?
Sb4 Pr1 Pr1 129.478(8) 13 1_455 ?
Sb4 Pr1 Pr1 50.522(8) 13_455 1_455 ?
Sb5B Pr1 Pr1 98.19(7) 13 1_455 ?
Sb5B Pr1 Pr1 81.81(7) 5_445 1_455 ?
Sb2 Pr1 Pr1 90.0 . 1_455 ?
Pr1 Pr1 Pr1 90.0 2 1_455 ?
Pr2 Pr1 Pr1 90.0 . 1_455 ?
Zn2 Pr1 Pr1 90.0 . 1_655 ?
Sb3 Pr1 Pr1 131.292(11) 1_455 1_655 ?
Sb3 Pr1 Pr1 48.708(11) . 1_655 ?
Zn1 Pr1 Pr1 130.43(10) 1_455 1_655 ?
Zn1 Pr1 Pr1 49.57(10) . 1_655 ?
Sb5A Pr1 Pr1 90.0 5_445 1_655 ?
Sb1 Pr1 Pr1 50.146(12) 13 1_655 ?
Sb1 Pr1 Pr1 129.854(12) 13_455 1_655 ?
Sb1 Pr1 Pr1 90.0 . 1_655 ?
Sb4 Pr1 Pr1 50.522(8) 13 1_655 ?
Sb4 Pr1 Pr1 129.478(8) 13_455 1_655 ?
Sb5B Pr1 Pr1 81.81(7) 13 1_655 ?
Sb5B Pr1 Pr1 98.19(7) 5_445 1_655 ?
Sb2 Pr1 Pr1 90.0 . 1_655 ?
Pr1 Pr1 Pr1 90.0 2 1_655 ?
Pr2 Pr1 Pr1 90.0 . 1_655 ?
Pr1 Pr1 Pr1 180.00(5) 1_455 1_655 ?
Sb3 Pr2 Sb3 83.13(3) . 1_455 ?
Sb3 Pr2 Sb1 83.526(17) . . ?
Sb3 Pr2 Sb1 83.526(17) 1_455 . ?
Sb3 Pr2 Sb1 83.526(17) . 2 ?
Sb3 Pr2 Sb1 83.526(17) 1_455 2 ?
Sb1 Pr2 Sb1 162.66(4) . 2 ?
Sb3 Pr2 Sb2 137.12(2) . 14_445 ?
Sb3 Pr2 Sb2 82.597(19) 1_455 14_445 ?
Sb1 Pr2 Sb2 134.268(17) . 14_445 ?
Sb1 Pr2 Sb2 54.804(18) 2 14_445 ?
Sb3 Pr2 Sb2 82.597(19) . 13 ?
Sb3 Pr2 Sb2 137.12(2) 1_455 13 ?
Sb1 Pr2 Sb2 54.804(18) . 13 ?
Sb1 Pr2 Sb2 134.268(17) 2 13 ?
Sb2 Pr2 Sb2 132.40(4) 14_445 13 ?
Sb3 Pr2 Sb2 82.597(19) . 14_545 ?
Sb3 Pr2 Sb2 137.12(2) 1_455 14_545 ?
Sb1 Pr2 Sb2 134.268(17) . 14_545 ?
Sb1 Pr2 Sb2 54.804(18) 2 14_545 ?
Sb2 Pr2 Sb2 80.99(3) 14_445 14_545 ?
Sb2 Pr2 Sb2 80.27(3) 13 14_545 ?
Sb3 Pr2 Sb2 137.12(2) . 13_455 ?
Sb3 Pr2 Sb2 82.597(19) 1_455 13_455 ?
Sb1 Pr2 Sb2 54.804(18) . 13_455 ?
Sb1 Pr2 Sb2 134.268(17) 2 13_455 ?
Sb2 Pr2 Sb2 80.26(3) 14_445 13_455 ?
Sb2 Pr2 Sb2 80.99(3) 13 13_455 ?
Sb2 Pr2 Sb2 132.40(4) 14_545 13_455 ?
Sb3 Pr2 Sb6A 138.437(17) . . ?
Sb3 Pr2 Sb6A 138.437(17) 1_455 . ?
Sb1 Pr2 Sb6A 98.67(2) . . ?
Sb1 Pr2 Sb6A 98.67(2) 2 . ?
Sb2 Pr2 Sb6A 66.20(2) 14_445 . ?
Sb2 Pr2 Sb6A 66.20(2) 13 . ?
Sb2 Pr2 Sb6A 66.20(2) 14_545 . ?
Sb2 Pr2 Sb6A 66.20(2) 13_455 . ?
Sb3 Pr2 Sb6B 133.64(2) . 9 ?
Sb3 Pr2 Sb6B 133.64(2) 1_455 9 ?
Sb1 Pr2 Sb6B 121.40(4) . 9 ?
Sb1 Pr2 Sb6B 75.93(4) 2 9 ?
Sb2 Pr2 Sb6B 51.59(3) 14_445 9 ?
Sb2 Pr2 Sb6B 82.93(4) 13 9 ?
Sb2 Pr2 Sb6B 51.59(3) 14_545 9 ?
Sb2 Pr2 Sb6B 82.93(4) 13_455 9 ?
Sb6A Pr2 Sb6B 22.74(4) . 9 ?
Sb3 Pr2 Sb6B 133.64(2) . . ?
Sb3 Pr2 Sb6B 133.64(2) 1_455 . ?
Sb1 Pr2 Sb6B 75.93(4) . . ?
Sb1 Pr2 Sb6B 121.40(4) 2 . ?
Sb2 Pr2 Sb6B 82.93(4) 14_445 . ?
Sb2 Pr2 Sb6B 51.59(3) 13 . ?
Sb2 Pr2 Sb6B 82.93(4) 14_545 . ?
Sb2 Pr2 Sb6B 51.59(3) 13_455 . ?
Sb6A Pr2 Sb6B 22.74(4) . . ?
Sb6B Pr2 Sb6B 45.47(7) 9 . ?
Sb3 Pr2 Pr1 49.603(16) . . ?
Sb3 Pr2 Pr1 49.603(16) 1_455 . ?
Sb1 Pr2 Pr1 51.348(19) . . ?
Sb1 Pr2 Pr1 111.32(3) 2 . ?
Sb2 Pr2 Pr1 132.20(2) 14_445 . ?
Sb2 Pr2 Pr1 91.57(2) 13 . ?
Sb2 Pr2 Pr1 132.20(2) 14_545 . ?
Sb2 Pr2 Pr1 91.57(2) 13_455 . ?
Sb6A Pr2 Pr1 150.015(11) . . ?
Sb6B Pr2 Pr1 172.75(4) 9 . ?
Sb6B Pr2 Pr1 127.28(4) . . ?
Sb3 Pr2 Pr1 49.603(16) . 2 ?
Sb3 Pr2 Pr1 49.603(16) 1_455 2 ?
Sb1 Pr2 Pr1 111.32(3) . 2 ?
Sb1 Pr2 Pr1 51.348(19) 2 2 ?
Sb2 Pr2 Pr1 91.57(2) 14_445 2 ?
Sb2 Pr2 Pr1 132.20(2) 13 2 ?
Sb2 Pr2 Pr1 91.57(2) 14_545 2 ?
Sb2 Pr2 Pr1 132.20(2) 13_455 2 ?
Sb6A Pr2 Pr1 150.015(11) . 2 ?
Sb6B Pr2 Pr1 127.28(4) 9 2 ?
Sb6B Pr2 Pr1 172.75(4) . 2 ?
Pr1 Pr2 Pr1 59.97(2) . 2 ?
Sb3 Pr2 Pr2 48.437(17) . 1_655 ?
Sb3 Pr2 Pr2 131.563(17) 1_455 1_655 ?
Sb1 Pr2 Pr2 90.0 . 1_655 ?
Sb1 Pr2 Pr2 90.0 2 1_655 ?
Sb2 Pr2 Pr2 130.493(13) 14_445 1_655 ?
Sb2 Pr2 Pr2 49.507(13) 13 1_655 ?
Sb2 Pr2 Pr2 49.507(13) 14_545 1_655 ?
Sb2 Pr2 Pr2 130.493(13) 13_455 1_655 ?
Sb6A Pr2 Pr2 90.0 . 1_655 ?
Sb6B Pr2 Pr2 90.0 9 1_655 ?
Sb6B Pr2 Pr2 90.0 . 1_655 ?
Pr1 Pr2 Pr2 90.0 . 1_655 ?
Pr1 Pr2 Pr2 90.0 2 1_655 ?
Sb3 Pr2 Pr2 131.563(17) . 1_455 ?
Sb3 Pr2 Pr2 48.437(17) 1_455 1_455 ?
Sb1 Pr2 Pr2 90.0 . 1_455 ?
Sb1 Pr2 Pr2 90.0 2 1_455 ?
Sb2 Pr2 Pr2 49.507(13) 14_445 1_455 ?
Sb2 Pr2 Pr2 130.493(13) 13 1_455 ?
Sb2 Pr2 Pr2 130.493(13) 14_545 1_455 ?
Sb2 Pr2 Pr2 49.507(13) 13_455 1_455 ?
Sb6A Pr2 Pr2 90.0 . 1_455 ?
Sb6B Pr2 Pr2 90.0 9 1_455 ?
Sb6B Pr2 Pr2 90.0 . 1_455 ?
Pr1 Pr2 Pr2 90.0 . 1_455 ?
Pr1 Pr2 Pr2 90.0 2 1_455 ?
Pr2 Pr2 Pr2 180.00(5) 1_655 1_455 ?
Sb5B Zn1 Sb5B 107.7(7) 5_545 13 ?
Sb5B Zn1 Zn1 53.8(4) 5_545 9_656 ?
Sb5B Zn1 Zn1 53.8(4) 13 9_656 ?
Sb5B Zn1 Sb5A 6.61(8) 5_545 5_545 ?
Sb5B Zn1 Sb5A 114.3(7) 13 5_545 ?
Zn1 Zn1 Sb5A 60.4(3) 9_656 5_545 ?
Sb5B Zn1 Sb5A 114.3(7) 5_545 5_445 ?
Sb5B Zn1 Sb5A 6.61(8) 13 5_445 ?
Zn1 Zn1 Sb5A 60.4(3) 9_656 5_445 ?
Sb5A Zn1 Sb5A 120.9(7) 5_545 5_445 ?
Sb5B Zn1 Sb3 126.2(4) 5_545 . ?
Sb5B Zn1 Sb3 126.2(4) 13 . ?
Zn1 Zn1 Sb3 180.000(1) 9_656 . ?
Sb5A Zn1 Sb3 119.6(3) 5_545 . ?
Sb5A Zn1 Sb3 119.6(3) 5_445 . ?
Sb5B Zn1 Sb4 74.2(3) 5_545 13 ?
Sb5B Zn1 Sb4 74.2(3) 13 13 ?
Zn1 Zn1 Sb4 62.6(3) 9_656 13 ?
Sb5A Zn1 Sb4 76.9(3) 5_545 13 ?
Sb5A Zn1 Sb4 76.9(3) 5_445 13 ?
Sb3 Zn1 Sb4 117.4(3) . 13 ?
Sb5B Zn1 Sb4 74.2(3) 5_545 5_545 ?
Sb5B Zn1 Sb4 74.2(3) 13 5_545 ?
Zn1 Zn1 Sb4 62.6(3) 9_656 5_545 ?
Sb5A Zn1 Sb4 76.9(3) 5_545 5_545 ?
Sb5A Zn1 Sb4 76.9(3) 5_445 5_545 ?
Sb3 Zn1 Sb4 117.4(3) . 5_545 ?
Sb4 Zn1 Sb4 125.2(6) 13 5_545 ?
Sb5B Zn1 Sb5B 11.31(13) 5_545 13_655 ?
Sb5B Zn1 Sb5B 119.0(7) 13 13_655 ?
Zn1 Zn1 Sb5B 65.1(3) 9_656 13_655 ?
Sb5A Zn1 Sb5B 4.70(5) 5_545 13_655 ?
Sb5A Zn1 Sb5B 125.6(6) 5_445 13_655 ?
Sb3 Zn1 Sb5B 114.9(3) . 13_655 ?
Sb4 Zn1 Sb5B 78.8(2) 13 13_655 ?
Sb4 Zn1 Sb5B 78.8(2) 5_545 13_655 ?
Sb5B Zn1 Sb5B 119.0(7) 5_545 5_445 ?
Sb5B Zn1 Sb5B 11.31(13) 13 5_445 ?
Zn1 Zn1 Sb5B 65.1(3) 9_656 5_445 ?
Sb5A Zn1 Sb5B 125.6(6) 5_545 5_445 ?
Sb5A Zn1 Sb5B 4.70(5) 5_445 5_445 ?
Sb3 Zn1 Sb5B 114.9(3) . 5_445 ?
Sb4 Zn1 Sb5B 78.8(2) 13 5_445 ?
Sb4 Zn1 Sb5B 78.8(2) 5_545 5_445 ?
Sb5B Zn1 Sb5B 130.3(6) 13_655 5_445 ?
Sb5B Zn1 Pr1 140.29(15) 5_545 2 ?
Sb5B Zn1 Pr1 73.86(8) 13 2 ?
Zn1 Zn1 Pr1 114.6(3) 9_656 2 ?
Sb5A Zn1 Pr1 140.31(6) 5_545 2 ?
Sb5A Zn1 Pr1 68.98(5) 5_445 2 ?
Sb3 Zn1 Pr1 65.4(3) . 2 ?
Sb4 Zn1 Pr1 139.23(3) 13 2 ?
Sb4 Zn1 Pr1 68.04(4) 5_545 2 ?
Sb5B Zn1 Pr1 139.769(11) 13_655 2 ?
Sb5B Zn1 Pr1 65.58(4) 5_445 2 ?
Sb5B Zn1 Pr1 73.86(8) 5_545 1_655 ?
Sb5B Zn1 Pr1 140.29(15) 13 1_655 ?
Zn1 Zn1 Pr1 114.6(3) 9_656 1_655 ?
Sb5A Zn1 Pr1 68.97(5) 5_545 1_655 ?
Sb5A Zn1 Pr1 140.31(6) 5_445 1_655 ?
Sb3 Zn1 Pr1 65.4(3) . 1_655 ?
Sb4 Zn1 Pr1 68.04(4) 13 1_655 ?
Sb4 Zn1 Pr1 139.23(3) 5_545 1_655 ?
Sb5B Zn1 Pr1 65.58(4) 13_655 1_655 ?
Sb5B Zn1 Pr1 139.769(12) 5_445 1_655 ?
Pr1 Zn1 Pr1 130.8(5) 2 1_655 ?
Sb5B Zn1 Pr1 73.86(8) 5_545 2_655 ?
Sb5B Zn1 Pr1 140.29(15) 13 2_655 ?
Zn1 Zn1 Pr1 114.6(3) 9_656 2_655 ?
Sb5A Zn1 Pr1 68.98(5) 5_545 2_655 ?
Sb5A Zn1 Pr1 140.31(6) 5_445 2_655 ?
Sb3 Zn1 Pr1 65.4(3) . 2_655 ?
Sb4 Zn1 Pr1 139.23(3) 13 2_655 ?
Sb4 Zn1 Pr1 68.04(4) 5_545 2_655 ?
Sb5B Zn1 Pr1 65.58(4) 13_655 2_655 ?
Sb5B Zn1 Pr1 139.769(12) 5_445 2_655 ?
Pr1 Zn1 Pr1 80.9(2) 2 2_655 ?
Pr1 Zn1 Pr1 79.17(19) 1_655 2_655 ?
Sb5B Zn1 Pr1 140.29(15) 5_545 . ?
Sb5B Zn1 Pr1 73.86(8) 13 . ?
Zn1 Zn1 Pr1 114.6(3) 9_656 . ?
Sb5A Zn1 Pr1 140.31(6) 5_545 . ?
Sb5A Zn1 Pr1 68.98(5) 5_445 . ?
Sb3 Zn1 Pr1 65.4(3) . . ?
Sb4 Zn1 Pr1 68.04(4) 13 . ?
Sb4 Zn1 Pr1 139.23(3) 5_545 . ?
Sb5B Zn1 Pr1 139.769(12) 13_655 . ?
Sb5B Zn1 Pr1 65.58(4) 5_445 . ?
Pr1 Zn1 Pr1 79.17(19) 2 . ?
Pr1 Zn1 Pr1 80.9(2) 1_655 . ?
Pr1 Zn1 Pr1 130.8(5) 2_655 . ?
Sb2 Zn2 Sb2 106.17(16) 10_556 . ?
Sb2 Zn2 Sb4 111.142(16) 10_556 13_455 ?
Sb2 Zn2 Sb4 111.142(16) . 13_455 ?
Sb2 Zn2 Sb4 111.142(16) 10_556 13 ?
Sb2 Zn2 Sb4 111.142(16) . 13 ?
Sb4 Zn2 Sb4 106.19(15) 13_455 13 ?
Sb2 Zn2 Sb6B 64.29(8) 10_556 13 ?
Sb2 Zn2 Sb6B 64.29(8) . 13 ?
Sb4 Zn2 Sb6B 170.67(13) 13_455 13 ?
Sb4 Zn2 Sb6B 83.14(4) 13 13 ?
Sb2 Zn2 Sb6B 64.29(8) 10_556 13_455 ?
Sb2 Zn2 Sb6B 64.29(8) . 13_455 ?
Sb4 Zn2 Sb6B 83.14(4) 13_455 13_455 ?
Sb4 Zn2 Sb6B 170.67(13) 13 13_455 ?
Sb6B Zn2 Sb6B 87.53(13) 13 13_455 ?
Sb2 Zn2 Pr1 178.56(14) 10_556 . ?
Sb2 Zn2 Pr1 72.39(3) . . ?
Sb4 Zn2 Pr1 69.60(7) 13_455 . ?
Sb4 Zn2 Pr1 69.60(7) 13 . ?
Sb6B Zn2 Pr1 114.78(2) 13 . ?
Sb6B Zn2 Pr1 114.78(2) 13_455 . ?
Sb2 Zn2 Pr1 72.39(3) 10_556 10_556 ?
Sb2 Zn2 Pr1 178.56(14) . 10_556 ?
Sb4 Zn2 Pr1 69.60(7) 13_455 10_556 ?
Sb4 Zn2 Pr1 69.60(7) 13 10_556 ?
Sb6B Zn2 Pr1 114.78(2) 13 10_556 ?
Sb6B Zn2 Pr1 114.78(2) 13_455 10_556 ?
Pr1 Zn2 Pr1 109.05(13) . 10_556 ?
Sb2 Sb1 Sb2 90.09(3) 13_455 13 ?
Sb2 Sb1 Sb1 178.75(4) 13_455 13 ?
Sb2 Sb1 Sb1 90.770(18) 13 13 ?
Sb2 Sb1 Sb1 90.770(18) 13_455 13_455 ?
Sb2 Sb1 Sb1 178.75(4) 13 13_455 ?
Sb1 Sb1 Sb1 88.35(4) 13 13_455 ?
Sb2 Sb1 Pr2 62.95(2) 13_455 . ?
Sb2 Sb1 Pr2 62.95(2) 13 . ?
Sb1 Sb1 Pr2 116.71(3) 13 . ?
Sb1 Sb1 Pr2 116.71(3) 13_455 . ?
Sb2 Sb1 Pr1 118.39(3) 13_455 13 ?
Sb2 Sb1 Pr1 64.43(2) 13 13 ?
Sb1 Sb1 Pr1 62.83(2) 13 13 ?
Sb1 Sb1 Pr1 115.88(4) 13_455 13 ?
Pr2 Sb1 Pr1 127.37(2) . 13 ?
Sb2 Sb1 Pr1 64.43(2) 13_455 13_455 ?
Sb2 Sb1 Pr1 118.39(3) 13 13_455 ?
Sb1 Sb1 Pr1 115.88(4) 13 13_455 ?
Sb1 Sb1 Pr1 62.83(2) 13_455 13_455 ?
Pr2 Sb1 Pr1 127.37(2) . 13_455 ?
Pr1 Sb1 Pr1 79.71(2) 13 13_455 ?
Sb2 Sb1 Pr1 116.27(3) 13_455 . ?
Sb2 Sb1 Pr1 116.27(3) 13 . ?
Sb1 Sb1 Pr1 62.51(3) 13 . ?
Sb1 Sb1 Pr1 62.51(3) 13_455 . ?
Pr2 Sb1 Pr1 78.86(3) . . ?
Pr1 Sb1 Pr1 125.34(2) 13 . ?
Pr1 Sb1 Pr1 125.34(2) 13_455 . ?
Zn2 Sb2 Sb6B 67.20(7) . 13 ?
Zn2 Sb2 Sb6B 67.20(6) . 13_455 ?
Sb6B Sb2 Sb6B 90.09(4) 13 13_455 ?
Zn2 Sb2 Sb1 105.13(6) . 13_455 ?
Sb6B Sb2 Sb1 171.83(6) 13 13_455 ?
Sb6B Sb2 Sb1 89.32(2) 13_455 13_455 ?
Zn2 Sb2 Sb1 105.13(6) . 13 ?
Sb6B Sb2 Sb1 89.32(2) 13 13 ?
Sb6B Sb2 Sb1 171.83(6) 13_455 13 ?
Sb1 Sb2 Sb1 90.09(3) 13_455 13 ?
Zn2 Sb2 Pr2 135.22(4) . 13 ?
Sb6B Sb2 Pr2 69.77(3) 13 13 ?
Sb6B Sb2 Pr2 124.98(6) 13_455 13 ?
Sb1 Sb2 Pr2 116.97(4) 13_455 13 ?
Sb1 Sb2 Pr2 62.25(2) 13 13 ?
Zn2 Sb2 Pr2 135.22(4) . 13_455 ?
Sb6B Sb2 Pr2 124.98(6) 13 13_455 ?
Sb6B Sb2 Pr2 69.77(3) 13_455 13_455 ?
Sb1 Sb2 Pr2 62.25(2) 13_455 13_455 ?
Sb1 Sb2 Pr2 116.97(4) 13 13_455 ?
Pr2 Sb2 Pr2 80.99(3) 13 13_455 ?
Zn2 Sb2 Pr1 62.86(8) . . ?
Sb6B Sb2 Pr1 110.42(5) 13 . ?
Sb6B Sb2 Pr1 110.42(5) 13_455 . ?
Sb1 Sb2 Pr1 62.28(2) 13_455 . ?
Sb1 Sb2 Pr1 62.28(2) 13 . ?
Pr2 Sb2 Pr1 124.52(2) 13 . ?
Pr2 Sb2 Pr1 124.52(2) 13_455 . ?
Zn2 Sb2 Sb6A 84.76(7) . 5 ?
Sb6B Sb2 Sb6A 22.02(5) 13 5 ?
Sb6B Sb2 Sb6A 84.77(4) 13_455 5 ?
Sb1 Sb2 Sb6A 165.51(3) 13_455 5 ?
Sb1 Sb2 Sb6A 97.605(14) 13 5 ?
Pr2 Sb2 Sb6A 57.489(19) 13 5 ?
Pr2 Sb2 Sb6A 103.27(3) 13_455 5 ?
Pr1 Sb2 Sb6A 132.21(2) . 5 ?
Zn2 Sb2 Sb6A 84.76(7) . 5_455 ?
Sb6B Sb2 Sb6A 84.77(4) 13 5_455 ?
Sb6B Sb2 Sb6A 22.02(5) 13_455 5_455 ?
Sb1 Sb2 Sb6A 97.605(14) 13_455 5_455 ?
Sb1 Sb2 Sb6A 165.51(3) 13 5_455 ?
Pr2 Sb2 Sb6A 103.27(3) 13 5_455 ?
Pr2 Sb2 Sb6A 57.489(19) 13_455 5_455 ?
Pr1 Sb2 Sb6A 132.21(2) . 5_455 ?
Sb6A Sb2 Sb6A 72.393(19) 5 5_455 ?
Zn2 Sb2 Sb2 36.91(8) . 10_556 ?
Sb6B Sb2 Sb2 48.344(18) 13 10_556 ?
Sb6B Sb2 Sb2 48.344(18) 13_455 10_556 ?
Sb1 Sb2 Sb2 127.09(2) 13_455 10_556 ?
Sb1 Sb2 Sb2 127.09(2) 13 10_556 ?
Pr2 Sb2 Sb2 113.80(2) 13 10_556 ?
Pr2 Sb2 Sb2 113.80(2) 13_455 10_556 ?
Pr1 Sb2 Sb2 99.77(2) . 10_556 ?
Sb6A Sb2 Sb2 56.314(14) 5 10_556 ?
Sb6A Sb2 Sb2 56.314(14) 5_455 10_556 ?
Zn1 Sb3 Pr2 138.437(17) . . ?
Zn1 Sb3 Pr2 138.437(17) . 1_655 ?
Pr2 Sb3 Pr2 83.13(3) . 1_655 ?
Zn1 Sb3 Pr1 67.69(2) . 1_655 ?
Pr2 Sb3 Pr1 136.20(2) . 1_655 ?
Pr2 Sb3 Pr1 81.153(15) 1_655 1_655 ?
Zn1 Sb3 Pr1 67.69(2) . 2 ?
Pr2 Sb3 Pr1 81.153(15) . 2 ?
Pr2 Sb3 Pr1 136.20(2) 1_655 2 ?
Pr1 Sb3 Pr1 135.39(4) 1_655 2 ?
Zn1 Sb3 Pr1 67.69(2) . . ?
Pr2 Sb3 Pr1 81.153(15) . . ?
Pr2 Sb3 Pr1 136.20(2) 1_655 . ?
Pr1 Sb3 Pr1 82.58(2) 1_655 . ?
Pr1 Sb3 Pr1 80.85(2) 2 . ?
Zn1 Sb3 Pr1 67.69(2) . 2_655 ?
Pr2 Sb3 Pr1 136.20(2) . 2_655 ?
Pr2 Sb3 Pr1 81.153(15) 1_655 2_655 ?
Pr1 Sb3 Pr1 80.85(2) 1_655 2_655 ?
Pr1 Sb3 Pr1 82.58(2) 2 2_655 ?
Pr1 Sb3 Pr1 135.39(4) . 2_655 ?
Zn1 Sb4 Zn1 54.8(6) 13 5_454 ?
Zn1 Sb4 Zn2 122.21(12) 13 13_455 ?
Zn1 Sb4 Zn2 122.21(12) 5_454 13_455 ?
Zn1 Sb4 Zn2 122.21(12) 13 13 ?
Zn1 Sb4 Zn2 122.21(12) 5_454 13 ?
Zn2 Sb4 Zn2 106.19(15) 13_455 13 ?
Zn1 Sb4 Sb5B 43.62(18) 13 . ?
Zn1 Sb4 Sb5B 43.62(18) 5_454 . ?
Zn2 Sb4 Sb5B 162.27(11) 13_455 . ?
Zn2 Sb4 Sb5B 91.54(10) 13 . ?
Zn1 Sb4 Sb5B 43.62(18) 13 9_565 ?
Zn1 Sb4 Sb5B 43.62(18) 5_454 9_565 ?
Zn2 Sb4 Sb5B 91.54(10) 13_455 9_565 ?
Zn2 Sb4 Sb5B 162.27(11) 13 9_565 ?
Sb5B Sb4 Sb5B 70.73(13) . 9_565 ?
Zn1 Sb4 Sb5A 49.08(14) 13 . ?
Zn1 Sb4 Sb5A 49.08(14) 5_454 . ?
Zn2 Sb4 Sb5A 169.36(8) 13_455 . ?
Zn2 Sb4 Sb5A 84.46(7) 13 . ?
Sb5B Sb4 Sb5A 7.09(7) . . ?
Sb5B Sb4 Sb5A 77.82(7) 9_565 . ?
Zn1 Sb4 Sb5A 49.08(14) 13 1_455 ?
Zn1 Sb4 Sb5A 49.08(14) 5_454 1_455 ?
Zn2 Sb4 Sb5A 84.46(7) 13_455 1_455 ?
Zn2 Sb4 Sb5A 169.36(8) 13 1_455 ?
Sb5B Sb4 Sb5A 77.82(7) . 1_455 ?
Sb5B Sb4 Sb5A 7.09(7) 9_565 1_455 ?
Sb5A Sb4 Sb5A 84.90(3) . 1_455 ?
Zn1 Sb4 Pr1 65.4(2) 13 13 ?
Zn1 Sb4 Pr1 107.0(2) 5_454 13 ?
Zn2 Sb4 Pr1 123.41(4) 13_455 13 ?
Zn2 Sb4 Pr1 62.21(4) 13 13 ?
Sb5B Sb4 Pr1 64.83(4) . 13 ?
Sb5B Sb4 Pr1 108.10(5) 9_565 13 ?
Sb5A Sb4 Pr1 61.250(14) . 13 ?
Sb5A Sb4 Pr1 112.16(3) 1_455 13 ?
Zn1 Sb4 Pr1 107.0(2) 13 6_454 ?
Zn1 Sb4 Pr1 65.4(2) 5_454 6_454 ?
Zn2 Sb4 Pr1 62.21(4) 13_455 6_454 ?
Zn2 Sb4 Pr1 123.41(4) 13 6_454 ?
Sb5B Sb4 Pr1 108.10(5) . 6_454 ?
Sb5B Sb4 Pr1 64.83(4) 9_565 6_454 ?
Sb5A Sb4 Pr1 112.16(3) . 6_454 ?
Sb5A Sb4 Pr1 61.250(13) 1_455 6_454 ?
Pr1 Sb4 Pr1 171.94(4) 13 6_454 ?
Zn1 Sb4 Pr1 107.0(2) 13 6_554 ?
Zn1 Sb4 Pr1 65.4(2) 5_454 6_554 ?
Zn2 Sb4 Pr1 123.41(4) 13_455 6_554 ?
Zn2 Sb4 Pr1 62.21(4) 13 6_554 ?
Sb5B Sb4 Pr1 64.83(4) . 6_554 ?
Sb5B Sb4 Pr1 108.10(5) 9_565 6_554 ?
Sb5A Sb4 Pr1 61.250(13) . 6_554 ?
Sb5A Sb4 Pr1 112.16(3) 1_455 6_554 ?
Pr1 Sb4 Pr1 100.469(16) 13 6_554 ?
Pr1 Sb4 Pr1 78.955(16) 6_454 6_554 ?
Zn1 Sb4 Pr1 65.4(2) 13 13_455 ?
Zn1 Sb4 Pr1 107.0(2) 5_454 13_455 ?
Zn2 Sb4 Pr1 62.21(4) 13_455 13_455 ?
Zn2 Sb4 Pr1 123.41(4) 13 13_455 ?
Sb5B Sb4 Pr1 108.10(5) . 13_455 ?
Sb5B Sb4 Pr1 64.83(4) 9_565 13_455 ?
Sb5A Sb4 Pr1 112.16(3) . 13_455 ?
Sb5A Sb4 Pr1 61.250(13) 1_455 13_455 ?
Pr1 Sb4 Pr1 78.955(16) 13 13_455 ?
Pr1 Sb4 Pr1 100.469(16) 6_454 13_455 ?
Pr1 Sb4 Pr1 171.94(4) 6_554 13_455 ?
Zn1 Sb4 Sb5B 53.75(13) 13 9_665 ?
Zn1 Sb4 Sb5B 53.75(13) 5_454 9_665 ?
Zn2 Sb4 Sb5B 175.14(9) 13_455 9_665 ?
Zn2 Sb4 Sb5B 78.67(9) 13 9_665 ?
Sb5B Sb4 Sb5B 12.87(11) . 9_665 ?
Sb5B Sb4 Sb5B 83.60(4) 9_565 9_665 ?
Sb5A Sb4 Sb5B 5.78(4) . 9_665 ?
Sb5A Sb4 Sb5B 90.69(5) 1_455 9_665 ?
Pr1 Sb4 Sb5B 58.60(2) 13 9_665 ?
Pr1 Sb4 Sb5B 115.30(3) 6_454 9_665 ?
Pr1 Sb4 Sb5B 58.60(2) 6_554 9_665 ?
Pr1 Sb4 Sb5B 115.30(3) 13_455 9_665 ?
Zn1 Sb4 Sb5B 53.75(13) 13 1_455 ?
Zn1 Sb4 Sb5B 53.75(13) 5_454 1_455 ?
Zn2 Sb4 Sb5B 78.67(9) 13_455 1_455 ?
Zn2 Sb4 Sb5B 175.14(9) 13 1_455 ?
Sb5B Sb4 Sb5B 83.60(4) . 1_455 ?
Sb5B Sb4 Sb5B 12.87(11) 9_565 1_455 ?
Sb5A Sb4 Sb5B 90.69(5) . 1_455 ?
Sb5A Sb4 Sb5B 5.78(4) 1_455 1_455 ?
Pr1 Sb4 Sb5B 115.30(3) 13 1_455 ?
Pr1 Sb4 Sb5B 58.60(2) 6_454 1_455 ?
Pr1 Sb4 Sb5B 115.30(3) 6_554 1_455 ?
Pr1 Sb4 Sb5B 58.60(2) 13_455 1_455 ?
Sb5B Sb4 Sb5B 96.47(9) 9_665 1_455 ?
Zn1 Sb4 Sb6B 152.6(3) 13 . ?
Zn1 Sb4 Sb6B 152.6(3) 5_454 . ?
Zn2 Sb4 Sb6B 53.09(8) 13_455 . ?
Zn2 Sb4 Sb6B 53.09(8) 13 . ?
Sb5B Sb4 Sb6B 144.64(7) . . ?
Sb5B Sb4 Sb6B 144.64(7) 9_565 . ?
Sb5A Sb4 Sb6B 137.549(14) . . ?
Sb5A Sb4 Sb6B 137.549(14) 1_455 . ?
Pr1 Sb4 Sb6B 94.03(2) 13 . ?
Pr1 Sb4 Sb6B 94.03(2) 6_454 . ?
Pr1 Sb4 Sb6B 94.03(2) 6_554 . ?
Pr1 Sb4 Sb6B 94.03(2) 13_455 . ?
Sb5B Sb4 Sb6B 131.76(5) 9_665 . ?
Sb5B Sb4 Sb6B 131.76(5) 1_455 . ?
Sb5B Sb5A Zn1 29.6(3) 9_665 13_655 ?
Sb5B Sb5A Zn1 150.4(3) 9_665 5_454 ?
Zn1 Sb5A Zn1 180.0 13_655 5_454 ?
Sb5B Sb5A Zn1 150.4(3) 9_665 13 ?
Zn1 Sb5A Zn1 120.9(7) 13_655 13 ?
Zn1 Sb5A Zn1 59.1(7) 5_454 13 ?
Sb5B Sb5A Zn1 29.6(3) 9_665 5_554 ?
Zn1 Sb5A Zn1 59.1(7) 13_655 5_554 ?
Zn1 Sb5A Zn1 120.9(7) 5_454 5_554 ?
Zn1 Sb5A Zn1 180.0(7) 13 5_554 ?
Sb5B Sb5A Sb4 132.451(14) 9_665 . ?
Zn1 Sb5A Sb4 125.95(13) 13_655 . ?
Zn1 Sb5A Sb4 54.05(13) 5_454 . ?
Zn1 Sb5A Sb4 54.05(13) 13 . ?
Zn1 Sb5A Sb4 125.95(13) 5_554 . ?
Sb5B Sb5A Sb4 47.549(14) 9_665 9_665 ?
Zn1 Sb5A Sb4 54.05(13) 13_655 9_665 ?
Zn1 Sb5A Sb4 125.95(13) 5_454 9_665 ?
Zn1 Sb5A Sb4 125.95(13) 13 9_665 ?
Zn1 Sb5A Sb4 54.05(13) 5_554 9_665 ?
Sb4 Sb5A Sb4 180.0 . 9_665 ?
Sb5B Sb5A Sb4 132.451(14) 9_665 9_565 ?
Zn1 Sb5A Sb4 125.95(13) 13_655 9_565 ?
Zn1 Sb5A Sb4 54.05(13) 5_454 9_565 ?
Zn1 Sb5A Sb4 54.05(13) 13 9_565 ?
Zn1 Sb5A Sb4 125.95(13) 5_554 9_565 ?
Sb4 Sb5A Sb4 95.10(3) . 9_565 ?
Sb4 Sb5A Sb4 84.90(3) 9_665 9_565 ?
Sb5B Sb5A Sb4 47.549(14) 9_665 1_655 ?
Zn1 Sb5A Sb4 54.05(13) 13_655 1_655 ?
Zn1 Sb5A Sb4 125.95(13) 5_454 1_655 ?
Zn1 Sb5A Sb4 125.95(13) 13 1_655 ?
Zn1 Sb5A Sb4 54.05(13) 5_554 1_655 ?
Sb4 Sb5A Sb4 84.90(3) . 1_655 ?
Sb4 Sb5A Sb4 95.10(3) 9_665 1_655 ?
Sb4 Sb5A Sb4 180.0 9_565 1_655 ?
Sb5B Sb5A Pr1 90.0 9_665 14 ?
Zn1 Sb5A Pr1 67.5(2) 13_655 14 ?
Zn1 Sb5A Pr1 112.5(2) 5_454 14 ?
Zn1 Sb5A Pr1 67.5(2) 13 14 ?
Zn1 Sb5A Pr1 112.5(2) 5_554 14 ?
Sb4 Sb5A Pr1 117.734(10) . 14 ?
Sb4 Sb5A Pr1 62.266(10) 9_665 14 ?
Sb4 Sb5A Pr1 62.266(10) 9_565 14 ?
Sb4 Sb5A Pr1 117.734(10) 1_655 14 ?
Sb5B Sb5A Pr1 90.0 9_665 6_554 ?
Zn1 Sb5A Pr1 112.5(2) 13_655 6_554 ?
Zn1 Sb5A Pr1 67.5(2) 5_454 6_554 ?
Zn1 Sb5A Pr1 112.5(2) 13 6_554 ?
Zn1 Sb5A Pr1 67.5(2) 5_554 6_554 ?
Sb4 Sb5A Pr1 62.266(10) . 6_554 ?
Sb4 Sb5A Pr1 117.734(10) 9_665 6_554 ?
Sb4 Sb5A Pr1 117.734(10) 9_565 6_554 ?
Sb4 Sb5A Pr1 62.266(10) 1_655 6_554 ?
Pr1 Sb5A Pr1 180.000(14) 14 6_554 ?
Sb5B Sb5A Pr1 90.0 9_665 13 ?
Zn1 Sb5A Pr1 67.5(2) 13_655 13 ?
Zn1 Sb5A Pr1 112.5(2) 5_454 13 ?
Zn1 Sb5A Pr1 67.5(2) 13 13 ?
Zn1 Sb5A Pr1 112.5(2) 5_554 13 ?
Sb4 Sb5A Pr1 62.266(10) . 13 ?
Sb4 Sb5A Pr1 117.734(10) 9_665 13 ?
Sb4 Sb5A Pr1 117.734(10) 9_565 13 ?
Sb4 Sb5A Pr1 62.266(10) 1_655 13 ?
Pr1 Sb5A Pr1 78.20(2) 14 13 ?
Pr1 Sb5A Pr1 101.80(2) 6_554 13 ?
Sb5B Sb5A Pr1 90.0 9_665 5_554 ?
Zn1 Sb5A Pr1 112.5(2) 13_655 5_554 ?
Zn1 Sb5A Pr1 67.5(2) 5_454 5_554 ?
Zn1 Sb5A Pr1 112.5(2) 13 5_554 ?
Zn1 Sb5A Pr1 67.5(2) 5_554 5_554 ?
Sb4 Sb5A Pr1 117.734(10) . 5_554 ?
Sb4 Sb5A Pr1 62.266(10) 9_665 5_554 ?
Sb4 Sb5A Pr1 62.266(10) 9_565 5_554 ?
Sb4 Sb5A Pr1 117.734(10) 1_655 5_554 ?
Pr1 Sb5A Pr1 101.80(2) 14 5_554 ?
Pr1 Sb5A Pr1 78.20(2) 6_554 5_554 ?
Pr1 Sb5A Pr1 180.00(2) 13 5_554 ?
Sb5B Sb5A Sb5B 0.0 9_665 1_655 ?
Zn1 Sb5A Sb5B 29.6(3) 13_655 1_655 ?
Zn1 Sb5A Sb5B 150.4(3) 5_454 1_655 ?
Zn1 Sb5A Sb5B 150.4(3) 13 1_655 ?
Zn1 Sb5A Sb5B 29.6(3) 5_554 1_655 ?
Sb4 Sb5A Sb5B 132.451(14) . 1_655 ?
Sb4 Sb5A Sb5B 47.549(14) 9_665 1_655 ?
Sb4 Sb5A Sb5B 132.451(14) 9_565 1_655 ?
Sb4 Sb5A Sb5B 47.549(14) 1_655 1_655 ?
Pr1 Sb5A Sb5B 90.0 14 1_655 ?
Pr1 Sb5A Sb5B 90.0 6_554 1_655 ?
Pr1 Sb5A Sb5B 90.0 13 1_655 ?
Pr1 Sb5A Sb5B 90.0 5_554 1_655 ?
Sb5B Sb5A Sb5B 180.0 9_665 9_565 ?
Zn1 Sb5A Sb5B 150.4(3) 13_655 9_565 ?
Zn1 Sb5A Sb5B 29.6(3) 5_454 9_565 ?
Zn1 Sb5A Sb5B 29.6(3) 13 9_565 ?
Zn1 Sb5A Sb5B 150.4(3) 5_554 9_565 ?
Sb4 Sb5A Sb5B 47.549(14) . 9_565 ?
Sb4 Sb5A Sb5B 132.451(14) 9_665 9_565 ?
Sb4 Sb5A Sb5B 47.549(14) 9_565 9_565 ?
Sb4 Sb5A Sb5B 132.451(14) 1_655 9_565 ?
Pr1 Sb5A Sb5B 90.0 14 9_565 ?
Pr1 Sb5A Sb5B 90.0 6_554 9_565 ?
Pr1 Sb5A Sb5B 90.0 13 9_565 ?
Pr1 Sb5A Sb5B 90.0 5_554 9_565 ?
Sb5B Sb5A Sb5B 180.0 1_655 9_565 ?
Sb5B Sb5B Zn1 143.8(4) 9_665 5_454 ?
Sb5B Sb5B Zn1 143.8(4) 9_665 13 ?
Zn1 Sb5B Zn1 72.3(7) 5_454 13 ?
Sb5B Sb5B Sb4 125.36(7) 9_665 . ?
Zn1 Sb5B Sb4 62.14(16) 5_454 . ?
Zn1 Sb5B Sb4 62.14(16) 13 . ?
Sb5B Sb5B Sb4 125.36(7) 9_665 9_565 ?
Zn1 Sb5B Sb4 62.14(16) 5_454 9_565 ?
Zn1 Sb5B Sb4 62.14(16) 13 9_565 ?
Sb4 Sb5B Sb4 109.27(13) . 9_565 ?
Sb5B Sb5B Zn1 24.9(3) 9_665 13_655 ?
Zn1 Sb5B Zn1 168.69(12) 5_454 13_655 ?
Zn1 Sb5B Zn1 119.0(7) 13 13_655 ?
Sb4 Sb5B Zn1 121.68(10) . 13_655 ?
Sb4 Sb5B Zn1 121.68(10) 9_565 13_655 ?
Sb5B Sb5B Zn1 24.9(3) 9_665 5_554 ?
Zn1 Sb5B Zn1 119.0(7) 5_454 5_554 ?
Zn1 Sb5B Zn1 168.69(12) 13 5_554 ?
Sb4 Sb5B Zn1 121.68(10) . 5_554 ?
Sb4 Sb5B Zn1 121.68(10) 9_565 5_554 ?
Zn1 Sb5B Zn1 49.7(6) 13_655 5_554 ?
Sb5B Sb5B Sb5B 180.0 9_665 9_565 ?
Zn1 Sb5B Sb5B 36.2(4) 5_454 9_565 ?
Zn1 Sb5B Sb5B 36.2(4) 13 9_565 ?
Sb4 Sb5B Sb5B 54.64(7) . 9_565 ?
Sb4 Sb5B Sb5B 54.64(7) 9_565 9_565 ?
Zn1 Sb5B Sb5B 155.1(3) 13_655 9_565 ?
Zn1 Sb5B Sb5B 155.1(3) 5_554 9_565 ?
Sb5B Sb5B Pr1 81.81(7) 9_665 14 ?
Zn1 Sb5B Pr1 124.6(3) 5_454 14 ?
Zn1 Sb5B Pr1 70.2(3) 13 14 ?
Sb4 Sb5B Pr1 126.26(6) . 14 ?
Sb4 Sb5B Pr1 64.744(18) 9_565 14 ?
Zn1 Sb5B Pr1 63.1(2) 13_655 14 ?
Zn1 Sb5B Pr1 101.2(2) 5_554 14 ?
Sb5B Sb5B Pr1 98.19(7) 9_565 14 ?
Sb5B Sb5B Pr1 81.81(7) 9_665 6_554 ?
Zn1 Sb5B Pr1 70.2(3) 5_454 6_554 ?
Zn1 Sb5B Pr1 124.6(3) 13 6_554 ?
Sb4 Sb5B Pr1 64.744(18) . 6_554 ?
Sb4 Sb5B Pr1 126.26(6) 9_565 6_554 ?
Zn1 Sb5B Pr1 101.2(2) 13_655 6_554 ?
Zn1 Sb5B Pr1 63.1(2) 5_554 6_554 ?
Sb5B Sb5B Pr1 98.19(7) 9_565 6_554 ?
Pr1 Sb5B Pr1 163.63(14) 14 6_554 ?
Sb5B Sb5B Pr1 81.81(7) 9_665 13 ?
Zn1 Sb5B Pr1 124.6(3) 5_454 13 ?
Zn1 Sb5B Pr1 70.2(3) 13 13 ?
Sb4 Sb5B Pr1 64.744(18) . 13 ?
Sb4 Sb5B Pr1 126.26(6) 9_565 13 ?
Zn1 Sb5B Pr1 63.1(2) 13_655 13 ?
Zn1 Sb5B Pr1 101.2(2) 5_554 13 ?
Sb5B Sb5B Pr1 98.19(7) 9_565 13 ?
Pr1 Sb5B Pr1 77.26(3) 14 13 ?
Pr1 Sb5B Pr1 100.37(3) 6_554 13 ?
Sb5B Sb5B Pr1 81.81(7) 9_665 5_554 ?
Zn1 Sb5B Pr1 70.2(3) 5_454 5_554 ?
Zn1 Sb5B Pr1 124.6(3) 13 5_554 ?
Sb4 Sb5B Pr1 126.26(6) . 5_554 ?
Sb4 Sb5B Pr1 64.744(18) 9_565 5_554 ?
Zn1 Sb5B Pr1 101.2(2) 13_655 5_554 ?
Zn1 Sb5B Pr1 63.1(2) 5_554 5_554 ?
Sb5B Sb5B Pr1 98.19(7) 9_565 5_554 ?
Pr1 Sb5B Pr1 100.37(3) 14 5_554 ?
Pr1 Sb5B Pr1 77.26(3) 6_554 5_554 ?
Pr1 Sb5B Pr1 163.63(14) 13 5_554 ?
Sb5B Sb5B Sb4 41.76(5) 9_665 9_665 ?
Zn1 Sb5B Sb4 127.0(2) 5_454 9_665 ?
Zn1 Sb5B Sb4 127.0(2) 13 9_665 ?
Sb4 Sb5B Sb4 167.13(11) . 9_665 ?
Sb4 Sb5B Sb4 83.60(4) 9_565 9_665 ?
Zn1 Sb5B Sb4 47.41(13) 13_655 9_665 ?
Zn1 Sb5B Sb4 47.41(13) 5_554 9_665 ?
Sb5B Sb5B Sb4 138.24(5) 9_565 9_665 ?
Pr1 Sb5B Sb4 58.53(4) 14 9_665 ?
Pr1 Sb5B Sb4 108.03(8) 6_554 9_665 ?
Pr1 Sb5B Sb4 108.03(8) 13 9_665 ?
Pr1 Sb5B Sb4 58.53(4) 5_554 9_665 ?
Sb5B Sb5B Sb4 41.76(5) 9_665 1_655 ?
Zn1 Sb5B Sb4 127.0(2) 5_454 1_655 ?
Zn1 Sb5B Sb4 127.0(2) 13 1_655 ?
Sb4 Sb5B Sb4 83.60(4) . 1_655 ?
Sb4 Sb5B Sb4 167.13(11) 9_565 1_655 ?
Zn1 Sb5B Sb4 47.41(13) 13_655 1_655 ?
Zn1 Sb5B Sb4 47.41(13) 5_554 1_655 ?
Sb5B Sb5B Sb4 138.24(5) 9_565 1_655 ?
Pr1 Sb5B Sb4 108.03(8) 14 1_655 ?
Pr1 Sb5B Sb4 58.53(4) 6_554 1_655 ?
Pr1 Sb5B Sb4 58.53(4) 13 1_655 ?
Pr1 Sb5B Sb4 108.03(8) 5_554 1_655 ?
Sb4 Sb5B Sb4 83.53(9) 9_665 1_655 ?
Sb5B Sb5B Sb5A 180.0 9_665 1_455 ?
Zn1 Sb5B Sb5A 36.2(4) 5_454 1_455 ?
Zn1 Sb5B Sb5A 36.2(4) 13 1_455 ?
Sb4 Sb5B Sb5A 54.64(7) . 1_455 ?
Sb4 Sb5B Sb5A 54.64(7) 9_565 1_455 ?
Zn1 Sb5B Sb5A 155.1(3) 13_655 1_455 ?
Zn1 Sb5B Sb5A 155.1(3) 5_554 1_455 ?
Sb5B Sb5B Sb5A 0.0 9_565 1_455 ?
Pr1 Sb5B Sb5A 98.19(7) 14 1_455 ?
Pr1 Sb5B Sb5A 98.19(7) 6_554 1_455 ?
Pr1 Sb5B Sb5A 98.19(7) 13 1_455 ?
Pr1 Sb5B Sb5A 98.19(7) 5_554 1_455 ?
Sb4 Sb5B Sb5A 138.24(5) 9_665 1_455 ?
Sb4 Sb5B Sb5A 138.24(5) 1_655 1_455 ?
Sb6B Sb6A Sb6B 180.0 9 . ?
Sb6B Sb6A Pr2 90.0 9 . ?
Sb6B Sb6A Pr2 90.0 . . ?
Sb6B Sb6A Pr2 90.0 9 9 ?
Sb6B Sb6A Pr2 90.0 . 9 ?
Pr2 Sb6A Pr2 180.0 . 9 ?
Sb6B Sb6A Sb2 54.113(14) 9 5_444 ?
Sb6B Sb6A Sb2 125.887(14) . 5_444 ?
Pr2 Sb6A Sb2 123.686(14) . 5_444 ?
Pr2 Sb6A Sb2 56.314(14) 9 5_444 ?
Sb6B Sb6A Sb2 125.887(14) 9 13 ?
Sb6B Sb6A Sb2 54.113(14) . 13 ?
Pr2 Sb6A Sb2 56.314(14) . 13 ?
Pr2 Sb6A Sb2 123.686(14) 9 13 ?
Sb2 Sb6A Sb2 180.00(4) 5_444 13 ?
Sb6B Sb6A Sb2 54.113(14) 9 14_445 ?
Sb6B Sb6A Sb2 125.887(14) . 14_445 ?
Pr2 Sb6A Sb2 56.314(14) . 14_445 ?
Pr2 Sb6A Sb2 123.686(14) 9 14_445 ?
Sb2 Sb6A Sb2 67.37(3) 5_444 14_445 ?
Sb2 Sb6A Sb2 112.63(3) 13 14_445 ?
Sb6B Sb6A Sb2 125.887(14) 9 6_554 ?
Sb6B Sb6A Sb2 54.113(14) . 6_554 ?
Pr2 Sb6A Sb2 123.686(14) . 6_554 ?
Pr2 Sb6A Sb2 56.314(14) 9 6_554 ?
Sb2 Sb6A Sb2 112.63(3) 5_444 6_554 ?
Sb2 Sb6A Sb2 67.37(3) 13 6_554 ?
Sb2 Sb6A Sb2 180.00(4) 14_445 6_554 ?
Sb6B Sb6A Sb2 54.113(14) 9 5_544 ?
Sb6B Sb6A Sb2 125.887(14) . 5_544 ?
Pr2 Sb6A Sb2 123.686(14) . 5_544 ?
Pr2 Sb6A Sb2 56.314(14) 9 5_544 ?
Sb2 Sb6A Sb2 72.393(19) 5_444 5_544 ?
Sb2 Sb6A Sb2 107.607(19) 13 5_544 ?
Sb2 Sb6A Sb2 108.23(3) 14_445 5_544 ?
Sb2 Sb6A Sb2 71.77(3) 6_554 5_544 ?
Sb6B Sb6A Sb2 125.887(14) 9 6_454 ?
Sb6B Sb6A Sb2 54.113(14) . 6_454 ?
Pr2 Sb6A Sb2 123.686(14) . 6_454 ?
Pr2 Sb6A Sb2 56.314(14) 9 6_454 ?
Sb2 Sb6A Sb2 71.77(3) 5_444 6_454 ?
Sb2 Sb6A Sb2 108.23(3) 13 6_454 ?
Sb2 Sb6A Sb2 107.607(19) 14_445 6_454 ?
Sb2 Sb6A Sb2 72.393(19) 6_554 6_454 ?
Sb2 Sb6A Sb2 112.63(3) 5_544 6_454 ?
Sb6B Sb6A Sb2 125.887(14) 9 13_455 ?
Sb6B Sb6A Sb2 54.113(14) . 13_455 ?
Pr2 Sb6A Sb2 56.314(14) . 13_455 ?
Pr2 Sb6A Sb2 123.686(14) 9 13_455 ?
Sb2 Sb6A Sb2 107.607(19) 5_444 13_455 ?
Sb2 Sb6A Sb2 72.393(19) 13 13_455 ?
Sb2 Sb6A Sb2 71.77(3) 14_445 13_455 ?
Sb2 Sb6A Sb2 108.23(3) 6_554 13_455 ?
Sb2 Sb6A Sb2 180.00(3) 5_544 13_455 ?
Sb2 Sb6A Sb2 67.37(3) 6_454 13_455 ?
Sb6B Sb6A Sb2 54.113(14) 9 14_545 ?
Sb6B Sb6A Sb2 125.887(14) . 14_545 ?
Pr2 Sb6A Sb2 56.314(14) . 14_545 ?
Pr2 Sb6A Sb2 123.686(14) 9 14_545 ?
Sb2 Sb6A Sb2 108.23(3) 5_444 14_545 ?
Sb2 Sb6A Sb2 71.77(3) 13 14_545 ?
Sb2 Sb6A Sb2 72.393(19) 14_445 14_545 ?
Sb2 Sb6A Sb2 107.607(19) 6_554 14_545 ?
Sb2 Sb6A Sb2 67.37(3) 5_544 14_545 ?
Sb2 Sb6A Sb2 180.00(4) 6_454 14_545 ?
Sb2 Sb6A Sb2 112.63(3) 13_455 14_545 ?
Sb6A Sb6B Sb6B 0.0 . 9 ?
Sb6A Sb6B Sb2 103.86(5) . 13 ?
Sb6B Sb6B Sb2 103.86(5) 9 13 ?
Sb6A Sb6B Sb2 103.86(5) . 6_454 ?
Sb6B Sb6B Sb2 103.86(5) 9 6_454 ?
Sb2 Sb6B Sb2 152.27(10) 13 6_454 ?
Sb6A Sb6B Sb2 103.86(5) . 6_554 ?
Sb6B Sb6B Sb2 103.86(5) 9 6_554 ?
Sb2 Sb6B Sb2 83.31(4) 13 6_554 ?
Sb2 Sb6B Sb2 90.09(4) 6_454 6_554 ?
Sb6A Sb6B Sb2 103.86(5) . 13_455 ?
Sb6B Sb6B Sb2 103.86(5) 9 13_455 ?
Sb2 Sb6B Sb2 90.09(4) 13 13_455 ?
Sb2 Sb6B Sb2 83.31(4) 6_454 13_455 ?
Sb2 Sb6B Sb2 152.27(10) 6_554 13_455 ?
Sb6A Sb6B Zn2 136.24(6) . 13 ?
Sb6B Sb6B Zn2 136.24(6) 9 13 ?
Sb2 Sb6B Zn2 48.51(4) 13 13 ?
Sb2 Sb6B Zn2 108.45(8) 6_454 13 ?
Sb2 Sb6B Zn2 48.51(4) 6_554 13 ?
Sb2 Sb6B Zn2 108.45(8) 13_455 13 ?
Sb6A Sb6B Zn2 136.24(6) . 13_455 ?
Sb6B Sb6B Zn2 136.24(6) 9 13_455 ?
Sb2 Sb6B Zn2 108.45(8) 13 13_455 ?
Sb2 Sb6B Zn2 48.51(4) 6_454 13_455 ?
Sb2 Sb6B Zn2 108.45(8) 6_554 13_455 ?
Sb2 Sb6B Zn2 48.51(4) 13_455 13_455 ?
Zn2 Sb6B Zn2 87.53(13) 13 13_455 ?
Sb6A Sb6B Pr2 67.26(4) . 9 ?
Sb6B Sb6B Pr2 67.26(4) 9 9 ?
Sb2 Sb6B Pr2 134.88(2) 13 9 ?
Sb2 Sb6B Pr2 58.641(19) 6_454 9 ?
Sb2 Sb6B Pr2 58.641(19) 6_554 9 ?
Sb2 Sb6B Pr2 134.88(2) 13_455 9 ?
Zn2 Sb6B Pr2 106.21(2) 13 9 ?
Zn2 Sb6B Pr2 106.21(2) 13_455 9 ?
Sb6A Sb6B Pr2 67.26(4) . . ?
Sb6B Sb6B Pr2 67.26(4) 9 . ?
Sb2 Sb6B Pr2 58.641(19) 13 . ?
Sb2 Sb6B Pr2 134.88(2) 6_454 . ?
Sb2 Sb6B Pr2 134.88(2) 6_554 . ?
Sb2 Sb6B Pr2 58.641(19) 13_455 . ?
Zn2 Sb6B Pr2 106.21(2) 13 . ?
Zn2 Sb6B Pr2 106.21(2) 13_455 . ?
Pr2 Sb6B Pr2 134.53(7) 9 . ?
Sb6A Sb6B Sb4 180.0 . . ?
Sb6B Sb6B Sb4 180.0 9 . ?
Sb2 Sb6B Sb4 76.14(5) 13 . ?
Sb2 Sb6B Sb4 76.14(5) 6_454 . ?
Sb2 Sb6B Sb4 76.14(5) 6_554 . ?
Sb2 Sb6B Sb4 76.14(5) 13_455 . ?
Zn2 Sb6B Sb4 43.76(6) 13 . ?
Zn2 Sb6B Sb4 43.76(6) 13_455 . ?
Pr2 Sb6B Sb4 112.74(4) 9 . ?
Pr2 Sb6B Sb4 112.74(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pr1 Zn2 3.174(3) . ?
Pr1 Sb3 3.2402(7) 1_455 ?
Pr1 Sb3 3.2402(7) . ?
Pr1 Zn1 3.297(7) 1_455 ?
Pr1 Zn1 3.297(7) . ?
Pr1 Sb5A 3.3312(7) 5_445 ?
Pr1 Sb1 3.3366(8) 13 ?
Pr1 Sb1 3.3366(8) 13_455 ?
Pr1 Sb1 3.3461(10) . ?
Pr1 Sb4 3.3631(6) 13 ?
Pr1 Sb4 3.3631(6) 13_455 ?
Pr1 Sb5B 3.3655(9) 13 ?
Pr1 Sb5B 3.3655(9) 5_445 ?
Pr1 Sb2 3.4001(12) . ?
Pr1 Pr1 4.2020(13) 2 ?
Pr1 Pr2 4.2040(11) . ?
Pr1 Pr1 4.2764(4) 1_455 ?
Pr1 Pr1 4.2764(4) 1_655 ?
Pr2 Sb3 3.2229(11) . ?
Pr2 Sb3 3.2229(11) 1_455 ?
Pr2 Sb1 3.2720(8) . ?
Pr2 Sb1 3.2720(8) 2 ?
Pr2 Sb2 3.2928(8) 14_445 ?
Pr2 Sb2 3.2928(8) 13 ?
Pr2 Sb2 3.2928(8) 14_545 ?
Pr2 Sb2 3.2928(8) 13_455 ?
Pr2 Sb6A 3.3371(10) . ?
Pr2 Sb6B 3.6183(13) 9 ?
Pr2 Sb6B 3.6183(13) . ?
Pr2 Pr1 4.2040(11) 2 ?
Pr2 Pr2 4.2764(4) 1_655 ?
Pr2 Pr2 4.2764(4) 1_455 ?
Zn1 Sb5B 2.055(10) 5_545 ?
Zn1 Sb5B 2.055(10) 13 ?
Zn1 Zn1 2.42(3) 9_656 ?
Zn1 Sb5A 2.458(8) 5_545 ?
Zn1 Sb5A 2.458(8) 5_445 ?
Zn1 Sb3 2.603(16) . ?
Zn1 Sb4 2.633(7) 13 ?
Zn1 Sb4 2.633(7) 5_545 ?
Zn1 Sb5B 2.885(8) 13_655 ?
Zn1 Sb5B 2.885(8) 5_445 ?
Zn1 Pr1 3.297(7) 2 ?
Zn1 Pr1 3.297(7) 1_655 ?
Zn1 Pr1 3.297(7) 2_655 ?
Zn2 Sb2 2.512(3) 10_556 ?
Zn2 Sb2 2.512(3) . ?
Zn2 Sb4 2.674(3) 13_455 ?
Zn2 Sb4 2.674(3) 13 ?
Zn2 Sb6B 3.091(4) 13 ?
Zn2 Sb6B 3.091(4) 13_455 ?
Zn2 Pr1 3.174(3) 10_556 ?
Sb1 Sb2 3.0214(9) 13_455 ?
Sb1 Sb2 3.0214(9) 13 ?
Sb1 Sb1 3.0683(12) 13 ?
Sb1 Sb1 3.0683(12) 13_455 ?
Sb1 Pr1 3.3366(8) 13 ?
Sb1 Pr1 3.3366(8) 13_455 ?
Sb2 Sb6B 3.0214(9) 13 ?
Sb2 Sb6B 3.0214(9) 13_455 ?
Sb2 Sb1 3.0214(9) 13_455 ?
Sb2 Sb1 3.0214(9) 13 ?
Sb2 Pr2 3.2928(8) 13 ?
Sb2 Pr2 3.2928(8) 13_455 ?
Sb2 Sb6A 3.6207(8) 5 ?
Sb2 Sb6A 3.6207(8) 5_455 ?
Sb2 Sb2 4.016(2) 10_556 ?
Sb3 Pr2 3.2229(11) 1_655 ?
Sb3 Pr1 3.2402(7) 1_655 ?
Sb3 Pr1 3.2402(7) 2 ?
Sb3 Pr1 3.2402(7) 2_655 ?
Sb4 Zn1 2.633(7) 13 ?
Sb4 Zn1 2.633(7) 5_454 ?
Sb4 Zn2 2.674(3) 13_455 ?
Sb4 Zn2 2.674(3) 13 ?
Sb4 Sb5B 2.866(3) . ?
Sb4 Sb5B 2.866(3) 9_565 ?
Sb4 Sb5A 3.1679(9) . ?
Sb4 Sb5A 3.1679(9) 1_455 ?
Sb4 Pr1 3.3631(6) 13 ?
Sb4 Pr1 3.3631(6) 6_454 ?
Sb4 Pr1 3.3631(6) 6_554 ?
Sb4 Pr1 3.3631(6) 13_455 ?
Sb4 Sb5B 3.509(3) 9_665 ?
Sb4 Sb5B 3.509(3) 1_455 ?
Sb4 Sb6B 3.838(3) . ?
Sb5A Sb5B 0.479(4) 9_665 ?
Sb5A Zn1 2.458(8) 13_655 ?
Sb5A Zn1 2.458(8) 5_454 ?
Sb5A Zn1 2.458(8) 13 ?
Sb5A Zn1 2.458(8) 5_554 ?
Sb5A Sb4 3.1679(9) 9_665 ?
Sb5A Sb4 3.1679(9) 9_565 ?
Sb5A Sb4 3.1679(9) 1_655 ?
Sb5A Pr1 3.3312(7) 14 ?
Sb5A Pr1 3.3312(7) 6_554 ?
Sb5A Pr1 3.3312(7) 13 ?
Sb5A Pr1 3.3312(7) 5_554 ?
Sb5A Sb5B 3.797(4) 1_655 ?
Sb5A Sb5B 3.797(4) 9_565 ?
Sb5B Sb5B 0.959(8) 9_665 ?
Sb5B Zn1 2.055(10) 5_454 ?
Sb5B Zn1 2.055(10) 13 ?
Sb5B Sb4 2.866(3) 9_565 ?
Sb5B Zn1 2.885(8) 13_655 ?
Sb5B Zn1 2.885(8) 5_554 ?
Sb5B Sb5B 3.318(8) 9_565 ?
Sb5B Pr1 3.3655(9) 14 ?
Sb5B Pr1 3.3655(9) 6_554 ?
Sb5B Pr1 3.3655(9) 13 ?
Sb5B Pr1 3.3655(9) 5_554 ?
Sb5B Sb4 3.509(3) 9_665 ?
Sb5B Sb4 3.509(3) 1_655 ?
Sb5B Sb5A 3.797(4) 1_455 ?
Sb6A Sb6B 1.398(3) 9 ?
Sb6A Sb6B 1.398(3) . ?
Sb6A Pr2 3.3371(10) 9 ?
Sb6A Sb2 3.6207(8) 5_444 ?
Sb6A Sb2 3.6207(8) 13 ?
Sb6A Sb2 3.6207(8) 14_445 ?
Sb6A Sb2 3.6207(8) 6_554 ?
Sb6A Sb2 3.6207(8) 5_544 ?
Sb6A Sb2 3.6207(8) 6_454 ?
Sb6A Sb2 3.6207(8) 13_455 ?
Sb6A Sb2 3.6207(8) 14_545 ?
Sb6B Sb6B 2.797(5) 9 ?
Sb6B Sb2 3.0214(9) 13 ?
Sb6B Sb2 3.0214(9) 6_454 ?
Sb6B Sb2 3.0214(9) 6_554 ?
Sb6B Sb2 3.0214(9) 13_455 ?
Sb6B Zn2 3.091(4) 13 ?
Sb6B Zn2 3.091(4) 13_455 ?
Sb6B Pr2 3.6183(13) 9 ?
