#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:06:12 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179093 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/55/4305534.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305534
loop_
_publ_author_name
'Yi Liu'
'Ling Chen'
'Long-Hua Li'
'Li-Ming Wu'
'Oksana Ya. Zelinska'
'Arthur Mar'
_publ_contact_author_address
; Department of Chemistry
  University of Alberta
  Edmonton, AB
  Canada  T6G 2G2
;
_publ_contact_author_email       arthur.mar@ualberta.ca
_publ_contact_author_fax         '(780) 492-8231'
_publ_contact_author_name        'Dr. Arthur Mar'
_publ_contact_author_phone       '(780) 492-5592'
_publ_section_title
;
Structures and Physical Properties of Rare-Earth Zinc Antimonides
Pr6Zn1+xSb14+yandRE6Zn1+xSb14 (RE= Sm, Gd-Ho)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11930
_journal_page_last               11941
_journal_paper_doi               10.1021/ic800524d
_journal_volume                  47
_journal_year                    2008
_chemical_formula_structural     'Sm6 Zn1.52 Sb14'
_chemical_formula_sum            'Sb14 Sm6 Zn1.52'
_chemical_formula_weight         2705.96
_chemical_name_common            'samarium zinc antimonide (6/1/14)'
_chemical_name_systematic        'samarium zinc antimonide (6/1/14)'
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.1838(13)
_cell_length_b                   15.039(5)
_cell_length_c                   18.832(6)
_cell_measurement_reflns_used    1753
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.47
_cell_measurement_theta_min      3.47
_cell_volume                     1184.9(7)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Rigaku Mercury CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0290
_diffrn_reflns_av_sigmaI/netI    0.0196
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            4558
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.71
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    31.730
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.4015
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrystalClear (Rigaku/MSC Inc., 2005)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    7.584
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2263
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_refine_diff_density_max         10.326
_refine_diff_density_min         -6.860
_refine_diff_density_rms         0.544
_refine_ls_extinction_coef       0.00093(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.091
_refine_ls_matrix_type           full
_refine_ls_number_parameters     48
_refine_ls_number_reflns         826
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.093
_refine_ls_R_factor_all          0.0362
_refine_ls_R_factor_gt           0.0345
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0387P)²+90.9577P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0813
_refine_ls_wR_factor_ref         0.0824
_reflns_number_gt                780
_reflns_number_total             826
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ic800524d_si_003_3.cif
_cod_data_source_block           Sm6ZnSb14
_cod_original_cell_volume        1184.9(6)
_cod_database_code               4305534
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sm1 Sm 0.0000 0.13848(4) 0.36405(3) 0.0058(2) Uani 1 2 d S . .
Sm2 Sm 0.0000 0.0000 0.17577(5) 0.0079(2) Uani 1 4 d S . .
Zn1 Zn 0.5000 0.0000 0.4390(15) 0.018(10) Uiso 0.086(12) 4 d SP . .
Zn2 Zn 0.0000 0.2623(2) 0.5000 0.0105(11) Uani 0.674(11) 4 d SP . .
Sb1 Sb 0.0000 0.21183(5) 0.19784(4) 0.0074(2) Uani 1 2 d S . .
Sb2 Sb 0.0000 0.36688(7) 0.39839(6) 0.0182(3) Uani 1 2 d S . .
Sb3 Sb 0.5000 0.0000 0.30171(6) 0.0060(3) Uani 1 4 d S . .
Sb4 Sb 0.0000 0.34750(8) 0.0000 0.0090(3) Uani 1 4 d S . .
Sb5A Sb 0.5000 0.5000 0.0000 0.0071(7) Uiso 0.414(12) 8 d SP . .
Sb5B Sb 0.392(2) 0.5000 0.0000 0.0071(7) Uiso 0.292(6) 4 d SP . .
Sb6A Sb 0.0000 0.0000 0.0000 0.0237(7) Uiso 0.869(8) 8 d SP . .
Sb6B Sb 0.0000 0.0849(14) 0.0000 0.0237(7) Uiso 0.077(4) 4 d SP . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sm Sm -0.1638 3.4418 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Zn2 Sm1 Sb3 133.20(3) . 1_455 ?
Zn2 Sm1 Sb3 133.20(3) . . ?
Sb3 Sm1 Sb3 82.37(3) 1_455 . ?
Zn2 Sm1 Zn1 91.5(4) . 1_455 ?
Sb3 Sm1 Zn1 47.3(5) 1_455 1_455 ?
Sb3 Sm1 Zn1 99.39(16) . 1_455 ?
Zn2 Sm1 Zn1 91.5(4) . . ?
Sb3 Sm1 Zn1 99.39(16) 1_455 . ?
Sb3 Sm1 Zn1 47.3(5) . . ?
Zn1 Sm1 Zn1 79.5(4) 1_455 . ?
Zn2 Sm1 Sb1 83.33(4) . 13 ?
Sb3 Sm1 Sb1 137.48(3) 1_455 13 ?
Sb3 Sm1 Sb1 84.19(3) . 13 ?
Zn1 Sm1 Sb1 174.8(4) 1_455 13 ?
Zn1 Sm1 Sb1 100.49(15) . 13 ?
Zn2 Sm1 Sb1 83.33(4) . 13_455 ?
Sb3 Sm1 Sb1 84.19(3) 1_455 13_455 ?
Sb3 Sm1 Sb1 137.48(3) . 13_455 ?
Zn1 Sm1 Sb1 100.49(14) 1_455 13_455 ?
Zn1 Sm1 Sb1 174.8(4) . 13_455 ?
Sb1 Sm1 Sb1 79.06(3) 13 13_455 ?
Zn2 Sm1 Sb5A 75.16(5) . 5_445 ?
Sb3 Sm1 Sb5A 82.70(3) 1_455 5_445 ?
Sb3 Sm1 Sb5A 82.70(3) . 5_445 ?
Zn1 Sm1 Sb5A 42.6(3) 1_455 5_445 ?
Zn1 Sm1 Sb5A 42.6(3) . 5_445 ?
Sb1 Sm1 Sb5A 135.018(18) 13 5_445 ?
Sb1 Sm1 Sb5A 135.018(18) 13_455 5_445 ?
Zn2 Sm1 Sb4 48.52(3) . 13 ?
Sb3 Sm1 Sb4 138.00(3) 1_455 13 ?
Sb3 Sm1 Sb4 84.92(3) . 13 ?
Zn1 Sm1 Sb4 96.4(4) 1_455 13 ?
Zn1 Sm1 Sb4 45.8(3) . 13 ?
Sb1 Sm1 Sb4 80.13(3) 13 13 ?
Sb1 Sm1 Sb4 129.23(3) 13_455 13 ?
Sb5A Sm1 Sb4 55.99(2) 5_445 13 ?
Zn2 Sm1 Sb4 48.52(3) . 13_455 ?
Sb3 Sm1 Sb4 84.92(3) 1_455 13_455 ?
Sb3 Sm1 Sb4 138.00(3) . 13_455 ?
Zn1 Sm1 Sb4 45.8(3) 1_455 13_455 ?
Zn1 Sm1 Sb4 96.4(4) . 13_455 ?
Sb1 Sm1 Sb4 129.23(3) 13 13_455 ?
Sb1 Sm1 Sb4 80.13(3) 13_455 13_455 ?
Sb5A Sm1 Sb4 55.99(2) 5_445 13_455 ?
Sb4 Sm1 Sb4 78.32(3) 13 13_455 ?
Zn2 Sm1 Sb1 124.56(6) . . ?
Sb3 Sm1 Sb1 82.49(3) 1_455 . ?
Sb3 Sm1 Sb1 82.49(3) . . ?
Zn1 Sm1 Sb1 128.2(4) 1_455 . ?
Zn1 Sm1 Sb1 128.2(4) . . ?
Sb1 Sm1 Sb1 55.80(2) 13 . ?
Sb1 Sm1 Sb1 55.80(2) 13_455 . ?
Sb5A Sm1 Sb1 160.29(3) 5_445 . ?
Sb4 Sm1 Sb1 135.05(2) 13 . ?
Sb4 Sm1 Sb1 135.05(2) 13_455 . ?
Zn2 Sm1 Sb5B 75.30(5) . 13 ?
Sb3 Sm1 Sb5B 87.89(10) 1_455 13 ?
Sb3 Sm1 Sb5B 77.59(10) . 13 ?
Zn1 Sm1 Sb5B 50.0(4) 1_455 13 ?
Zn1 Sm1 Sb5B 35.3(4) . 13 ?
Sb1 Sm1 Sb5B 127.93(14) 13 13 ?
Sb1 Sm1 Sb5B 141.90(13) 13_455 13 ?
Sb5A Sm1 Sb5B 7.77(14) 5_445 13 ?
Sb4 Sm1 Sb5B 50.24(11) 13 13 ?
Sb4 Sm1 Sb5B 62.04(12) 13_455 13 ?
Sb1 Sm1 Sb5B 158.87(6) . 13 ?
Zn2 Sm1 Sb5B 75.30(5) . 5_445 ?
Sb3 Sm1 Sb5B 77.59(10) 1_455 5_445 ?
Sb3 Sm1 Sb5B 87.89(10) . 5_445 ?
Zn1 Sm1 Sb5B 35.3(4) 1_455 5_445 ?
Zn1 Sm1 Sb5B 50.0(4) . 5_445 ?
Sb1 Sm1 Sb5B 141.90(13) 13 5_445 ?
Sb1 Sm1 Sb5B 127.93(14) 13_455 5_445 ?
Sb5A Sm1 Sb5B 7.77(14) 5_445 5_445 ?
Sb4 Sm1 Sb5B 62.04(12) 13 5_445 ?
Sb4 Sm1 Sb5B 50.24(11) 13_455 5_445 ?
Sb1 Sm1 Sb5B 158.87(6) . 5_445 ?
Sb5B Sm1 Sb5B 15.5(3) 13 5_445 ?
Zn2 Sm1 Sb2 43.31(5) . . ?
Sb3 Sm1 Sb2 135.450(16) 1_455 . ?
Sb3 Sm1 Sb2 135.450(16) . . ?
Zn1 Sm1 Sb2 123.1(3) 1_455 . ?
Zn1 Sm1 Sb2 123.1(3) . . ?
Sb1 Sm1 Sb2 52.59(2) 13 . ?
Sb1 Sm1 Sb2 52.59(2) 13_455 . ?
Sb5A Sm1 Sb2 118.47(3) 5_445 . ?
Sb4 Sm1 Sb2 78.14(3) 13 . ?
Sb4 Sm1 Sb2 78.14(3) 13_455 . ?
Sb1 Sm1 Sb2 81.25(3) . . ?
Sb5B Sm1 Sb2 118.18(3) 13 . ?
Sb5B Sm1 Sb2 118.18(3) 5_445 . ?
Zn2 Sm1 Sm2 174.40(5) . . ?
Sb3 Sm1 Sm2 49.41(2) 1_455 . ?
Sb3 Sm1 Sm2 49.41(2) . . ?
Zn1 Sm1 Sm2 92.9(4) 1_455 . ?
Zn1 Sm1 Sm2 92.9(4) . . ?
Sb1 Sm1 Sm2 92.36(3) 13 . ?
Sb1 Sm1 Sm2 92.36(3) 13_455 . ?
Sb5A Sm1 Sm2 110.44(3) 5_445 . ?
Sb4 Sm1 Sm2 134.31(2) 13 . ?
Sb4 Sm1 Sm2 134.31(2) 13_455 . ?
Sb1 Sm1 Sm2 49.84(3) . . ?
Sb5B Sm1 Sm2 110.25(3) 13 . ?
Sb5B Sm1 Sm2 110.25(3) 5_445 . ?
Sb2 Sm1 Sm2 131.09(3) . . ?
Zn2 Sm1 Sm1 126.03(5) . 2 ?
Sb3 Sm1 Sm1 49.036(16) 1_455 2 ?
Sb3 Sm1 Sm1 49.036(16) . 2 ?
Zn1 Sm1 Sm1 50.47(18) 1_455 2 ?
Zn1 Sm1 Sm1 50.47(18) . 2 ?
Sb1 Sm1 Sm1 133.231(18) 13 2 ?
Sb1 Sm1 Sm1 133.231(18) 13_455 2 ?
Sb5A Sm1 Sm1 50.872(16) 5_445 2 ?
Sb4 Sm1 Sm1 93.65(2) 13 2 ?
Sb4 Sm1 Sm1 93.65(2) 13_455 2 ?
Sb1 Sm1 Sm1 109.42(2) . 2 ?
Sb5B Sm1 Sm1 51.30(2) 13 2 ?
Sb5B Sm1 Sm1 51.30(2) 5_445 2 ?
Sb2 Sm1 Sm1 169.34(2) . 2 ?
Sm2 Sm1 Sm1 59.571(15) . 2 ?
Zn2 Sm1 Sm1 90.0 . 1_655 ?
Sb3 Sm1 Sm1 131.185(15) 1_455 1_655 ?
Sb3 Sm1 Sm1 48.815(15) . 1_655 ?
Zn1 Sm1 Sm1 129.74(18) 1_455 1_655 ?
Zn1 Sm1 Sm1 50.26(18) . 1_655 ?
Sb1 Sm1 Sm1 50.471(16) 13 1_655 ?
Sb1 Sm1 Sm1 129.529(16) 13_455 1_655 ?
Sb5A Sm1 Sm1 90.0 5_445 1_655 ?
Sb4 Sm1 Sm1 50.842(14) 13 1_655 ?
Sb4 Sm1 Sm1 129.158(14) 13_455 1_655 ?
Sb1 Sm1 Sm1 90.0 . 1_655 ?
Sb5B Sm1 Sm1 82.23(15) 13 1_655 ?
Sb5B Sm1 Sm1 97.77(15) 5_445 1_655 ?
Sb2 Sm1 Sm1 90.0 . 1_655 ?
Sm2 Sm1 Sm1 90.0 . 1_655 ?
Sm1 Sm1 Sm1 90.0 2 1_655 ?
Zn2 Sm1 Sm1 90.0 . 1_455 ?
Sb3 Sm1 Sm1 48.815(15) 1_455 1_455 ?
Sb3 Sm1 Sm1 131.185(15) . 1_455 ?
Zn1 Sm1 Sm1 50.26(18) 1_455 1_455 ?
Zn1 Sm1 Sm1 129.74(18) . 1_455 ?
Sb1 Sm1 Sm1 129.529(16) 13 1_455 ?
Sb1 Sm1 Sm1 50.471(16) 13_455 1_455 ?
Sb5A Sm1 Sm1 90.0 5_445 1_455 ?
Sb4 Sm1 Sm1 129.158(14) 13 1_455 ?
Sb4 Sm1 Sm1 50.842(14) 13_455 1_455 ?
Sb1 Sm1 Sm1 90.0 . 1_455 ?
Sb5B Sm1 Sm1 97.77(15) 13 1_455 ?
Sb5B Sm1 Sm1 82.23(15) 5_445 1_455 ?
Sb2 Sm1 Sm1 90.0 . 1_455 ?
Sm2 Sm1 Sm1 90.0 . 1_455 ?
Sm1 Sm1 Sm1 90.0 2 1_455 ?
Sm1 Sm1 Sm1 180.00(3) 1_655 1_455 ?
Sb3 Sm2 Sb3 82.83(4) . 1_455 ?
Sb3 Sm2 Sb1 84.433(17) . . ?
Sb3 Sm2 Sb1 84.433(17) 1_455 . ?
Sb3 Sm2 Sb1 84.433(17) . 2 ?
Sb3 Sm2 Sb1 84.433(17) 1_455 2 ?
Sb1 Sm2 Sb1 165.13(4) . 2 ?
Sb3 Sm2 Sb2 139.13(2) . 14_445 ?
Sb3 Sm2 Sb2 83.99(3) 1_455 14_445 ?
Sb1 Sm2 Sb2 132.36(2) . 14_445 ?
Sb1 Sm2 Sb2 55.85(2) 2 14_445 ?
Sb3 Sm2 Sb2 83.99(3) . 13 ?
Sb3 Sm2 Sb2 139.13(2) 1_455 13 ?
Sb1 Sm2 Sb2 55.85(2) . 13 ?
Sb1 Sm2 Sb2 132.36(2) 2 13 ?
Sb2 Sm2 Sb2 128.50(5) 14_445 13 ?
Sb3 Sm2 Sb2 139.13(2) . 13_455 ?
Sb3 Sm2 Sb2 83.99(3) 1_455 13_455 ?
Sb1 Sm2 Sb2 55.85(2) . 13_455 ?
Sb1 Sm2 Sb2 132.36(2) 2 13_455 ?
Sb2 Sm2 Sb2 77.04(4) 14_445 13_455 ?
Sb2 Sm2 Sb2 81.19(4) 13 13_455 ?
Sb3 Sm2 Sb2 83.99(3) . 14_545 ?
Sb3 Sm2 Sb2 139.13(2) 1_455 14_545 ?
Sb1 Sm2 Sb2 132.36(2) . 14_545 ?
Sb1 Sm2 Sb2 55.85(2) 2 14_545 ?
Sb2 Sm2 Sb2 81.19(4) 14_445 14_545 ?
Sb2 Sm2 Sb2 77.04(4) 13 14_545 ?
Sb2 Sm2 Sb2 128.50(5) 13_455 14_545 ?
Sb3 Sm2 Sb6A 138.59(2) . . ?
Sb3 Sm2 Sb6A 138.59(2) 1_455 . ?
Sb1 Sm2 Sb6A 97.43(2) . . ?
Sb1 Sm2 Sb6A 97.43(2) 2 . ?
Sb2 Sm2 Sb6A 64.25(2) 14_445 . ?
Sb2 Sm2 Sb6A 64.25(2) 13 . ?
Sb2 Sm2 Sb6A 64.25(2) 13_455 . ?
Sb2 Sm2 Sb6A 64.25(2) 14_545 . ?
Sb3 Sm2 Sb6B 134.40(12) . 9 ?
Sb3 Sm2 Sb6B 134.40(12) 1_455 9 ?
Sb1 Sm2 Sb6B 118.5(3) . 9 ?
Sb1 Sm2 Sb6B 76.3(3) 2 9 ?
Sb2 Sm2 Sb6B 50.99(18) 14_445 9 ?
Sb2 Sm2 Sb6B 79.6(2) 13 9 ?
Sb2 Sm2 Sb6B 79.6(2) 13_455 9 ?
Sb2 Sm2 Sb6B 50.99(18) 14_545 9 ?
Sb6A Sm2 Sb6B 21.1(3) . 9 ?
Sb3 Sm2 Sb6B 134.40(12) . . ?
Sb3 Sm2 Sb6B 134.40(12) 1_455 . ?
Sb1 Sm2 Sb6B 76.3(3) . . ?
Sb1 Sm2 Sb6B 118.5(3) 2 . ?
Sb2 Sm2 Sb6B 79.6(2) 14_445 . ?
Sb2 Sm2 Sb6B 50.99(18) 13 . ?
Sb2 Sm2 Sb6B 50.99(18) 13_455 . ?
Sb2 Sm2 Sb6B 79.6(2) 14_545 . ?
Sb6A Sm2 Sb6B 21.1(3) . . ?
Sb6B Sm2 Sb6B 42.2(6) 9 . ?
Sb3 Sm2 Sm1 49.71(2) . . ?
Sb3 Sm2 Sm1 49.71(2) 1_455 . ?
Sb1 Sm2 Sm1 52.14(2) . . ?
Sb1 Sm2 Sm1 113.00(3) 2 . ?
Sb2 Sm2 Sm1 133.63(2) 14_445 . ?
Sb2 Sm2 Sm1 93.39(3) 13 . ?
Sb2 Sm2 Sm1 93.39(3) 13_455 . ?
Sb2 Sm2 Sm1 133.63(2) 14_545 . ?
Sb6A Sm2 Sm1 149.571(15) . . ?
Sb6B Sm2 Sm1 170.7(3) 9 . ?
Sb6B Sm2 Sm1 128.5(3) . . ?
Sb3 Sm2 Sm1 49.71(2) . 2 ?
Sb3 Sm2 Sm1 49.71(2) 1_455 2 ?
Sb1 Sm2 Sm1 113.00(3) . 2 ?
Sb1 Sm2 Sm1 52.14(2) 2 2 ?
Sb2 Sm2 Sm1 93.39(3) 14_445 2 ?
Sb2 Sm2 Sm1 133.63(2) 13 2 ?
Sb2 Sm2 Sm1 133.63(2) 13_455 2 ?
Sb2 Sm2 Sm1 93.39(3) 14_545 2 ?
Sb6A Sm2 Sm1 149.571(15) . 2 ?
Sb6B Sm2 Sm1 128.5(3) 9 2 ?
Sb6B Sm2 Sm1 170.7(3) . 2 ?
Sm1 Sm2 Sm1 60.86(3) . 2 ?
Sb3 Sm2 Sm2 131.41(2) . 1_455 ?
Sb3 Sm2 Sm2 48.59(2) 1_455 1_455 ?
Sb1 Sm2 Sm2 90.0 . 1_455 ?
Sb1 Sm2 Sm2 90.0 2 1_455 ?
Sb2 Sm2 Sm2 49.404(18) 14_445 1_455 ?
Sb2 Sm2 Sm2 130.596(18) 13 1_455 ?
Sb2 Sm2 Sm2 49.404(18) 13_455 1_455 ?
Sb2 Sm2 Sm2 130.596(18) 14_545 1_455 ?
Sb6A Sm2 Sm2 90.0 . 1_455 ?
Sb6B Sm2 Sm2 90.0 9 1_455 ?
Sb6B Sm2 Sm2 90.0 . 1_455 ?
Sm1 Sm2 Sm2 90.0 . 1_455 ?
Sm1 Sm2 Sm2 90.0 2 1_455 ?
Sb3 Sm2 Sm2 48.59(2) . 1_655 ?
Sb3 Sm2 Sm2 131.41(2) 1_455 1_655 ?
Sb1 Sm2 Sm2 90.0 . 1_655 ?
Sb1 Sm2 Sm2 90.0 2 1_655 ?
Sb2 Sm2 Sm2 130.596(18) 14_445 1_655 ?
Sb2 Sm2 Sm2 49.404(18) 13 1_655 ?
Sb2 Sm2 Sm2 130.596(18) 13_455 1_655 ?
Sb2 Sm2 Sm2 49.404(18) 14_545 1_655 ?
Sb6A Sm2 Sm2 90.0 . 1_655 ?
Sb6B Sm2 Sm2 90.0 9 1_655 ?
Sb6B Sm2 Sm2 90.0 . 1_655 ?
Sm1 Sm2 Sm2 90.0 . 1_655 ?
Sm1 Sm2 Sm2 90.0 2 1_655 ?
Sm2 Sm2 Sm2 180.00(5) 1_455 1_655 ?
Sb5B Zn1 Sb5B 110.1(14) 5_545 13 ?
Sb5B Zn1 Zn1 55.0(7) 5_545 9_656 ?
Sb5B Zn1 Zn1 55.0(7) 13 9_656 ?
Sb5B Zn1 Sb5A 6.21(16) 5_545 5_545 ?
Sb5B Zn1 Sb5A 116.3(13) 13 5_545 ?
Zn1 Zn1 Sb5A 61.2(6) 9_656 5_545 ?
Sb5B Zn1 Sb5A 116.3(13) 5_545 5_445 ?
Sb5B Zn1 Sb5A 6.21(16) 13 5_445 ?
Zn1 Zn1 Sb5A 61.2(6) 9_656 5_445 ?
Sb5A Zn1 Sb5A 122.5(12) 5_545 5_445 ?
Sb5B Zn1 Sb4 75.1(6) 5_545 13 ?
Sb5B Zn1 Sb4 75.1(6) 13 13 ?
Zn1 Zn1 Sb4 63.4(6) 9_656 13 ?
Sb5A Zn1 Sb4 77.6(5) 5_545 13 ?
Sb5A Zn1 Sb4 77.6(5) 5_445 13 ?
Sb5B Zn1 Sb4 75.1(6) 5_545 5_545 ?
Sb5B Zn1 Sb4 75.1(6) 13 5_545 ?
Zn1 Zn1 Sb4 63.4(6) 9_656 5_545 ?
Sb5A Zn1 Sb4 77.6(5) 5_545 5_545 ?
Sb5A Zn1 Sb4 77.6(5) 5_445 5_545 ?
Sb4 Zn1 Sb4 126.8(12) 13 5_545 ?
Sb5B Zn1 Sb3 125.0(7) 5_545 . ?
Sb5B Zn1 Sb3 125.0(7) 13 . ?
Zn1 Zn1 Sb3 180.000(2) 9_656 . ?
Sb5A Zn1 Sb3 118.8(6) 5_545 . ?
Sb5A Zn1 Sb3 118.8(6) 5_445 . ?
Sb4 Zn1 Sb3 116.6(6) 13 . ?
Sb4 Zn1 Sb3 116.6(6) 5_545 . ?
Sb5B Zn1 Sb5B 10.7(3) 5_545 13_655 ?
Sb5B Zn1 Sb5B 120.7(12) 13 13_655 ?
Zn1 Zn1 Sb5B 65.7(5) 9_656 13_655 ?
Sb5A Zn1 Sb5B 4.46(10) 5_545 13_655 ?
Sb5A Zn1 Sb5B 126.9(12) 5_445 13_655 ?
Sb4 Zn1 Sb5B 79.4(4) 13 13_655 ?
Sb4 Zn1 Sb5B 79.4(4) 5_545 13_655 ?
Sb3 Zn1 Sb5B 114.3(5) . 13_655 ?
Sb5B Zn1 Sb5B 120.7(12) 5_545 5_445 ?
Sb5B Zn1 Sb5B 10.7(3) 13 5_445 ?
Zn1 Zn1 Sb5B 65.7(5) 9_656 5_445 ?
Sb5A Zn1 Sb5B 126.9(12) 5_545 5_445 ?
Sb5A Zn1 Sb5B 4.46(10) 5_445 5_445 ?
Sb4 Zn1 Sb5B 79.4(4) 13 5_445 ?
Sb4 Zn1 Sb5B 79.4(4) 5_545 5_445 ?
Sb3 Zn1 Sb5B 114.3(5) . 5_445 ?
Sb5B Zn1 Sb5B 131.4(11) 13_655 5_445 ?
Sb5B Zn1 Sm1 140.5(2) 5_545 2 ?
Sb5B Zn1 Sm1 73.95(18) 13 2 ?
Zn1 Zn1 Sm1 115.6(5) 9_656 2 ?
Sb5A Zn1 Sm1 140.18(5) 5_545 2 ?
Sb5A Zn1 Sm1 69.34(11) 5_445 2 ?
Sb4 Zn1 Sm1 139.668(14) 13 2 ?
Sb4 Zn1 Sm1 67.92(9) 5_545 2 ?
Sb3 Zn1 Sm1 64.4(5) . 2 ?
Sb5B Zn1 Sm1 139.49(5) 13_655 2 ?
Sb5B Zn1 Sm1 66.11(9) 5_445 2 ?
Sb5B Zn1 Sm1 73.95(18) 5_545 1_655 ?
Sb5B Zn1 Sm1 140.5(2) 13 1_655 ?
Zn1 Zn1 Sm1 115.6(5) 9_656 1_655 ?
Sb5A Zn1 Sm1 69.34(11) 5_545 1_655 ?
Sb5A Zn1 Sm1 140.18(5) 5_445 1_655 ?
Sb4 Zn1 Sm1 67.92(9) 13 1_655 ?
Sb4 Zn1 Sm1 139.668(14) 5_545 1_655 ?
Sb3 Zn1 Sm1 64.4(5) . 1_655 ?
Sb5B Zn1 Sm1 66.11(9) 13_655 1_655 ?
Sb5B Zn1 Sm1 139.49(5) 5_445 1_655 ?
Sm1 Zn1 Sm1 128.9(9) 2 1_655 ?
Sb5B Zn1 Sm1 73.95(18) 5_545 2_655 ?
Sb5B Zn1 Sm1 140.5(2) 13 2_655 ?
Zn1 Zn1 Sm1 115.6(5) 9_656 2_655 ?
Sb5A Zn1 Sm1 69.34(11) 5_545 2_655 ?
Sb5A Zn1 Sm1 140.18(5) 5_445 2_655 ?
Sb4 Zn1 Sm1 139.668(14) 13 2_655 ?
Sb4 Zn1 Sm1 67.92(9) 5_545 2_655 ?
Sb3 Zn1 Sm1 64.4(5) . 2_655 ?
Sb5B Zn1 Sm1 66.11(9) 13_655 2_655 ?
Sb5B Zn1 Sm1 139.49(5) 5_445 2_655 ?
Sm1 Zn1 Sm1 79.5(4) 2 2_655 ?
Sm1 Zn1 Sm1 79.1(4) 1_655 2_655 ?
Sb5B Zn1 Sm1 140.5(2) 5_545 . ?
Sb5B Zn1 Sm1 73.95(18) 13 . ?
Zn1 Zn1 Sm1 115.6(5) 9_656 . ?
Sb5A Zn1 Sm1 140.18(5) 5_545 . ?
Sb5A Zn1 Sm1 69.34(11) 5_445 . ?
Sb4 Zn1 Sm1 67.92(9) 13 . ?
Sb4 Zn1 Sm1 139.668(14) 5_545 . ?
Sb3 Zn1 Sm1 64.4(5) . . ?
Sb5B Zn1 Sm1 139.49(5) 13_655 . ?
Sb5B Zn1 Sm1 66.11(9) 5_445 . ?
Sm1 Zn1 Sm1 79.1(4) 2 . ?
Sm1 Zn1 Sm1 79.5(4) 1_655 . ?
Sm1 Zn1 Sm1 128.9(9) 2_655 . ?
Sb2 Zn2 Sb2 101.15(12) 10_556 . ?
Sb2 Zn2 Sb4 113.17(2) 10_556 13_455 ?
Sb2 Zn2 Sb4 113.17(2) . 13_455 ?
Sb2 Zn2 Sb4 113.17(2) 10_556 13 ?
Sb2 Zn2 Sb4 113.17(2) . 13 ?
Sb4 Zn2 Sb4 103.43(12) 13_455 13 ?
Sb2 Zn2 Sb6B 61.99(14) 10_556 13 ?
Sb2 Zn2 Sb6B 61.99(14) . 13 ?
Sb4 Zn2 Sb6B 170.6(3) 13_455 13 ?
Sb4 Zn2 Sb6B 86.0(3) 13 13 ?
Sb2 Zn2 Sb6B 61.99(14) 10_556 13_455 ?
Sb2 Zn2 Sb6B 61.99(14) . 13_455 ?
Sb4 Zn2 Sb6B 86.0(3) 13_455 13_455 ?
Sb4 Zn2 Sb6B 170.6(3) 13 13_455 ?
Sb6B Zn2 Sb6B 84.6(5) 13 13_455 ?
Sb2 Zn2 Sm1 176.61(11) 10_556 . ?
Sb2 Zn2 Sm1 75.45(4) . . ?
Sb4 Zn2 Sm1 68.63(5) 13_455 . ?
Sb4 Zn2 Sm1 68.63(5) 13 . ?
Sb6B Zn2 Sm1 115.78(12) 13 . ?
Sb6B Zn2 Sm1 115.78(12) 13_455 . ?
Sb2 Zn2 Sm1 75.45(4) 10_556 10_556 ?
Sb2 Zn2 Sm1 176.61(11) . 10_556 ?
Sb4 Zn2 Sm1 68.63(5) 13_455 10_556 ?
Sb4 Zn2 Sm1 68.63(5) 13 10_556 ?
Sb6B Zn2 Sm1 115.78(12) 13 10_556 ?
Sb6B Zn2 Sm1 115.78(12) 13_455 10_556 ?
Sm1 Zn2 Sm1 107.94(10) . 10_556 ?
Sb2 Sb1 Sb2 88.04(4) 13_455 13 ?
Sb2 Sb1 Sb1 177.48(5) 13_455 13 ?
Sb2 Sb1 Sb1 93.35(3) 13 13 ?
Sb2 Sb1 Sb1 93.35(3) 13_455 13_455 ?
Sb2 Sb1 Sb1 177.48(5) 13 13_455 ?
Sb1 Sb1 Sb1 85.19(5) 13 13_455 ?
Sb2 Sb1 Sm2 62.11(3) 13_455 . ?
Sb2 Sb1 Sm2 62.11(3) 13 . ?
Sb1 Sb1 Sm2 116.78(3) 13 . ?
Sb1 Sb1 Sm2 116.78(3) 13_455 . ?
Sb2 Sb1 Sm1 119.88(4) 13_455 13 ?
Sb2 Sb1 Sm1 67.27(3) 13 13 ?
Sb1 Sb1 Sm1 62.63(3) 13 13 ?
Sb1 Sb1 Sm1 113.69(4) 13_455 13 ?
Sm2 Sb1 Sm1 129.29(2) . 13 ?
Sb2 Sb1 Sm1 67.27(3) 13_455 13_455 ?
Sb2 Sb1 Sm1 119.88(4) 13 13_455 ?
Sb1 Sb1 Sm1 113.69(4) 13 13_455 ?
Sb1 Sb1 Sm1 62.63(3) 13_455 13_455 ?
Sm2 Sb1 Sm1 129.29(2) . 13_455 ?
Sm1 Sb1 Sm1 79.06(3) 13 13_455 ?
Sb2 Sb1 Sm1 115.92(3) 13_455 . ?
Sb2 Sb1 Sm1 115.92(3) 13 . ?
Sb1 Sb1 Sm1 61.58(3) 13 . ?
Sb1 Sb1 Sm1 61.58(3) 13_455 . ?
Sm2 Sb1 Sm1 78.02(3) . . ?
Sm1 Sb1 Sm1 124.20(2) 13 . ?
Sm1 Sb1 Sm1 124.20(2) 13_455 . ?
Zn2 Sb2 Sb6B 69.6(3) . 13 ?
Zn2 Sb2 Sb6B 69.6(3) . 13_455 ?
Sb6B Sb2 Sb6B 91.3(2) 13 13_455 ?
Zn2 Sb2 Sb1 102.43(5) . 13_455 ?
Sb6B Sb2 Sb1 171.1(4) 13 13_455 ?
Sb6B Sb2 Sb1 89.67(17) 13_455 13_455 ?
Zn2 Sb2 Sb1 102.43(5) . 13 ?
Sb6B Sb2 Sb1 89.67(17) 13 13 ?
Sb6B Sb2 Sb1 171.1(4) 13_455 13 ?
Sb1 Sb2 Sb1 88.04(4) 13_455 13 ?
Zn2 Sb2 Sm2 136.98(3) . 13 ?
Sb6B Sb2 Sm2 70.4(2) 13 13 ?
Sb6B Sb2 Sm2 126.5(4) 13_455 13 ?
Sb1 Sb2 Sm2 115.82(4) 13_455 13 ?
Sb1 Sb2 Sm2 62.04(3) 13 13 ?
Zn2 Sb2 Sm2 136.98(3) . 13_455 ?
Sb6B Sb2 Sm2 126.5(4) 13 13_455 ?
Sb6B Sb2 Sm2 70.4(2) 13_455 13_455 ?
Sb1 Sb2 Sm2 62.04(3) 13_455 13_455 ?
Sb1 Sb2 Sm2 115.82(4) 13 13_455 ?
Sm2 Sb2 Sm2 81.19(4) 13 13_455 ?
Zn2 Sb2 Sb6A 86.59(6) . 5 ?
Sb6B Sb2 Sb6A 20.9(4) 13 5 ?
Sb6B Sb2 Sb6A 85.8(2) 13_455 5 ?
Sb1 Sb2 Sb6A 167.85(4) 13_455 5 ?
Sb1 Sb2 Sb6A 98.04(2) 13 5 ?
Sm2 Sb2 Sb6A 59.21(3) 13 5 ?
Sm2 Sb2 Sb6A 105.81(4) 13_455 5 ?
Zn2 Sb2 Sb6A 86.59(6) . 5_455 ?
Sb6B Sb2 Sb6A 85.8(2) 13 5_455 ?
Sb6B Sb2 Sb6A 20.9(4) 13_455 5_455 ?
Sb1 Sb2 Sb6A 98.04(2) 13_455 5_455 ?
Sb1 Sb2 Sb6A 167.85(4) 13 5_455 ?
Sm2 Sb2 Sb6A 105.81(4) 13 5_455 ?
Sm2 Sb2 Sb6A 59.21(3) 13_455 5_455 ?
Sb6A Sb2 Sb6A 74.13(3) 5 5_455 ?
Zn2 Sb2 Sm1 61.24(6) . . ?
Sb6B Sb2 Sm1 111.4(4) 13 . ?
Sb6B Sb2 Sm1 111.4(4) 13_455 . ?
Sb1 Sb2 Sm1 60.14(2) 13_455 . ?
Sb1 Sb2 Sm1 60.14(2) 13 . ?
Sm2 Sb2 Sm1 122.12(3) 13 . ?
Sm2 Sb2 Sm1 122.12(3) 13_455 . ?
Sb6A Sb2 Sm1 131.98(2) 5 . ?
Sb6A Sb2 Sm1 131.98(2) 5_455 . ?
Zn2 Sb2 Sb2 39.42(6) . 10_556 ?
Sb6B Sb2 Sb2 49.16(9) 13 10_556 ?
Sb6B Sb2 Sb2 49.16(9) 13_455 10_556 ?
Sb1 Sb2 Sb2 127.01(2) 13_455 10_556 ?
Sb1 Sb2 Sb2 127.01(2) 13 10_556 ?
Sm2 Sb2 Sb2 115.75(2) 13 10_556 ?
Sm2 Sb2 Sb2 115.75(2) 13_455 10_556 ?
Sb6A Sb2 Sb2 56.542(19) 5 10_556 ?
Sb6A Sb2 Sb2 56.542(19) 5_455 10_556 ?
Sm1 Sb2 Sb2 100.66(2) . 10_556 ?
Zn2 Sb2 Sb2 129.42(6) . 2_565 ?
Sb6B Sb2 Sb2 75.7(4) 13 2_565 ?
Sb6B Sb2 Sb2 75.7(4) 13_455 2_565 ?
Sb1 Sb2 Sb2 113.16(3) 13_455 2_565 ?
Sb1 Sb2 Sb2 113.16(3) 13 2_565 ?
Sm2 Sb2 Sb2 51.48(2) 13 2_565 ?
Sm2 Sb2 Sb2 51.48(2) 13_455 2_565 ?
Sb6A Sb2 Sb2 54.770(19) 5 2_565 ?
Sb6A Sb2 Sb2 54.770(19) 5_455 2_565 ?
Sm1 Sb2 Sb2 169.34(2) . 2_565 ?
Sb2 Sb2 Sb2 90.0 10_556 2_565 ?
Zn1 Sb3 Sm2 138.59(2) . . ?
Zn1 Sb3 Sm2 138.59(2) . 1_655 ?
Sm2 Sb3 Sm2 82.83(4) . 1_655 ?
Zn1 Sb3 Sm1 68.31(2) . 1_655 ?
Sm2 Sb3 Sm1 135.46(2) . 1_655 ?
Sm2 Sb3 Sm1 80.88(2) 1_655 1_655 ?
Zn1 Sb3 Sm1 68.31(2) . 2 ?
Sm2 Sb3 Sm1 80.88(2) . 2 ?
Sm2 Sb3 Sm1 135.46(2) 1_655 2 ?
Sm1 Sb3 Sm1 136.62(5) 1_655 2 ?
Zn1 Sb3 Sm1 68.31(2) . . ?
Sm2 Sb3 Sm1 80.88(2) . . ?
Sm2 Sb3 Sm1 135.46(2) 1_655 . ?
Sm1 Sb3 Sm1 82.37(3) 1_655 . ?
Sm1 Sb3 Sm1 81.93(3) 2 . ?
Zn1 Sb3 Sm1 68.31(2) . 2_655 ?
Sm2 Sb3 Sm1 135.46(2) . 2_655 ?
Sm2 Sb3 Sm1 80.88(2) 1_655 2_655 ?
Sm1 Sb3 Sm1 81.93(3) 1_655 2_655 ?
Sm1 Sb3 Sm1 82.37(3) 2 2_655 ?
Sm1 Sb3 Sm1 136.62(5) . 2_655 ?
Zn1 Sb3 Sb5B 23.73(11) . 5_545 ?
Sm2 Sb3 Sb5B 162.31(11) . 5_545 ?
Sm2 Sb3 Sb5B 114.86(11) 1_655 5_545 ?
Sm1 Sb3 Sb5B 52.89(7) 1_655 5_545 ?
Sm1 Sb3 Sb5B 85.79(9) 2 5_545 ?
Sm1 Sb3 Sb5B 85.79(9) . 5_545 ?
Sm1 Sb3 Sb5B 52.89(7) 2_655 5_545 ?
Zn1 Sb3 Sb5B 23.73(11) . 13 ?
Sm2 Sb3 Sb5B 114.86(11) . 13 ?
Sm2 Sb3 Sb5B 162.31(11) 1_655 13 ?
Sm1 Sb3 Sb5B 85.79(9) 1_655 13 ?
Sm1 Sb3 Sb5B 52.89(7) 2 13 ?
Sm1 Sb3 Sb5B 52.89(7) . 13 ?
Sm1 Sb3 Sb5B 85.79(9) 2_655 13 ?
Sb5B Sb3 Sb5B 47.5(2) 5_545 13 ?
Zn1 Sb4 Zn1 53.2(12) 13 5_454 ?
Zn1 Sb4 Zn2 123.6(2) 13 13_455 ?
Zn1 Sb4 Zn2 123.6(2) 5_454 13_455 ?
Zn1 Sb4 Zn2 123.6(2) 13 13 ?
Zn1 Sb4 Zn2 123.6(2) 5_454 13 ?
Zn2 Sb4 Zn2 103.43(12) 13_455 13 ?
Zn1 Sb4 Sb5B 43.3(3) 13 . ?
Zn1 Sb4 Sb5B 43.3(3) 5_454 . ?
Zn2 Sb4 Sb5B 163.88(16) 13_455 . ?
Zn2 Sb4 Sb5B 92.69(15) 13 . ?
Zn1 Sb4 Sb5B 43.3(3) 13 9_565 ?
Zn1 Sb4 Sb5B 43.3(3) 5_454 9_565 ?
Zn2 Sb4 Sb5B 92.69(15) 13_455 9_565 ?
Zn2 Sb4 Sb5B 163.88(16) 13 9_565 ?
Sb5B Sb4 Sb5B 71.2(3) . 9_565 ?
Zn1 Sb4 Sb5A 48.6(3) 13 . ?
Zn1 Sb4 Sb5A 48.6(3) 5_454 . ?
Zn2 Sb4 Sb5A 170.65(6) 13_455 . ?
Zn2 Sb4 Sb5A 85.92(6) 13 . ?
Sb5B Sb4 Sb5A 6.78(14) . . ?
Sb5B Sb4 Sb5A 77.96(15) 9_565 . ?
Zn1 Sb4 Sb5A 48.6(3) 13 1_455 ?
Zn1 Sb4 Sb5A 48.6(3) 5_454 1_455 ?
Zn2 Sb4 Sb5A 85.92(6) 13_455 1_455 ?
Zn2 Sb4 Sb5A 170.65(6) 13 1_455 ?
Sb5B Sb4 Sb5A 77.96(15) . 1_455 ?
Sb5B Sb4 Sb5A 6.78(14) 9_565 1_455 ?
Sb5A Sb4 Sb5A 84.74(4) . 1_455 ?
Zn1 Sb4 Sm1 66.2(4) 13 13 ?
Zn1 Sb4 Sm1 106.8(4) 5_454 13 ?
Zn2 Sb4 Sm1 122.35(4) 13_455 13 ?
Zn2 Sb4 Sm1 62.86(3) 13 13 ?
Sb5B Sb4 Sm1 65.21(8) . 13 ?
Sb5B Sb4 Sm1 108.41(9) 9_565 13 ?
Sb5A Sb4 Sm1 61.800(18) . 13 ?
Sb5A Sb4 Sm1 112.24(3) 1_455 13 ?
Zn1 Sb4 Sm1 106.8(4) 13 6_454 ?
Zn1 Sb4 Sm1 66.2(4) 5_454 6_454 ?
Zn2 Sb4 Sm1 62.86(3) 13_455 6_454 ?
Zn2 Sb4 Sm1 122.35(4) 13 6_454 ?
Sb5B Sb4 Sm1 108.41(9) . 6_454 ?
Sb5B Sb4 Sm1 65.21(8) 9_565 6_454 ?
Sb5A Sb4 Sm1 112.24(3) . 6_454 ?
Sb5A Sb4 Sm1 61.800(18) 1_455 6_454 ?
Sm1 Sb4 Sm1 172.70(5) 13 6_454 ?
Zn1 Sb4 Sm1 106.8(4) 13 6_554 ?
Zn1 Sb4 Sm1 66.2(4) 5_454 6_554 ?
Zn2 Sb4 Sm1 122.35(4) 13_455 6_554 ?
Zn2 Sb4 Sm1 62.86(3) 13 6_554 ?
Sb5B Sb4 Sm1 65.21(8) . 6_554 ?
Sb5B Sb4 Sm1 108.41(9) 9_565 6_554 ?
Sb5A Sb4 Sm1 61.800(18) . 6_554 ?
Sb5A Sb4 Sm1 112.24(3) 1_455 6_554 ?
Sm1 Sb4 Sm1 101.21(3) 13 6_554 ?
Sm1 Sb4 Sm1 78.32(3) 6_454 6_554 ?
Zn1 Sb4 Sm1 66.2(4) 13 13_455 ?
Zn1 Sb4 Sm1 106.8(4) 5_454 13_455 ?
Zn2 Sb4 Sm1 62.86(3) 13_455 13_455 ?
Zn2 Sb4 Sm1 122.35(4) 13 13_455 ?
Sb5B Sb4 Sm1 108.41(9) . 13_455 ?
Sb5B Sb4 Sm1 65.21(8) 9_565 13_455 ?
Sb5A Sb4 Sm1 112.24(3) . 13_455 ?
Sb5A Sb4 Sm1 61.800(18) 1_455 13_455 ?
Sm1 Sb4 Sm1 78.32(3) 13 13_455 ?
Sm1 Sb4 Sm1 101.21(3) 6_454 13_455 ?
Sm1 Sb4 Sm1 172.70(5) 6_554 13_455 ?
Zn1 Sb4 Sb5B 53.2(2) 13 9_665 ?
Zn1 Sb4 Sb5B 53.2(2) 5_454 9_665 ?
Zn2 Sb4 Sb5B 176.23(12) 13_455 9_665 ?
Zn2 Sb4 Sb5B 80.34(11) 13 9_665 ?
Sb5B Sb4 Sb5B 12.4(2) . 9_665 ?
Sb5B Sb4 Sb5B 83.54(6) 9_565 9_665 ?
Sb5A Sb4 Sb5B 5.58(9) . 9_665 ?
Sb5A Sb4 Sb5B 90.32(10) 1_455 9_665 ?
Sm1 Sb4 Sb5B 59.24(5) 13 9_665 ?
Sm1 Sb4 Sb5B 115.23(6) 6_454 9_665 ?
Sm1 Sb4 Sb5B 59.24(5) 6_554 9_665 ?
Sm1 Sb4 Sb5B 115.23(6) 13_455 9_665 ?
Zn1 Sb4 Sb5B 53.2(2) 13 1_455 ?
Zn1 Sb4 Sb5B 53.2(2) 5_454 1_455 ?
Zn2 Sb4 Sb5B 80.34(11) 13_455 1_455 ?
Zn2 Sb4 Sb5B 176.23(12) 13 1_455 ?
Sb5B Sb4 Sb5B 83.54(6) . 1_455 ?
Sb5B Sb4 Sb5B 12.4(2) 9_565 1_455 ?
Sb5A Sb4 Sb5B 90.32(10) . 1_455 ?
Sb5A Sb4 Sb5B 5.58(9) 1_455 1_455 ?
Sm1 Sb4 Sb5B 115.23(6) 13 1_455 ?
Sm1 Sb4 Sb5B 59.24(5) 6_454 1_455 ?
Sm1 Sb4 Sb5B 115.23(6) 6_554 1_455 ?
Sm1 Sb4 Sb5B 59.24(5) 13_455 1_455 ?
Sb5B Sb4 Sb5B 95.89(19) 9_665 1_455 ?
Zn1 Sb4 Sb6B 153.4(6) 13 . ?
Zn1 Sb4 Sb6B 153.4(6) 5_454 . ?
Zn2 Sb4 Sb6B 51.72(6) 13_455 . ?
Zn2 Sb4 Sb6B 51.72(6) 13 . ?
Sb5B Sb4 Sb6B 144.41(14) . . ?
Sb5B Sb4 Sb6B 144.41(14) 9_565 . ?
Sb5A Sb4 Sb6B 137.63(2) . . ?
Sb5A Sb4 Sb6B 137.63(2) 1_455 . ?
Sm1 Sb4 Sb6B 93.65(2) 13 . ?
Sm1 Sb4 Sb6B 93.65(2) 6_454 . ?
Sm1 Sb4 Sb6B 93.65(2) 6_554 . ?
Sm1 Sb4 Sb6B 93.65(2) 13_455 . ?
Sb5B Sb4 Sb6B 132.05(10) 9_665 . ?
Sb5B Sb4 Sb6B 132.05(10) 1_455 . ?
Sb5B Sb5A Zn1 28.8(6) 9_665 13_655 ?
Sb5B Sb5A Zn1 151.2(6) 9_665 5_454 ?
Zn1 Sb5A Zn1 180.000(1) 13_655 5_454 ?
Sb5B Sb5A Zn1 151.2(6) 9_665 13 ?
Zn1 Sb5A Zn1 122.5(12) 13_655 13 ?
Zn1 Sb5A Zn1 57.5(12) 5_454 13 ?
Sb5B Sb5A Zn1 28.8(6) 9_665 5_554 ?
Zn1 Sb5A Zn1 57.5(12) 13_655 5_554 ?
Zn1 Sb5A Zn1 122.5(12) 5_454 5_554 ?
Zn1 Sb5A Zn1 180.0(12) 13 5_554 ?
Sb5B Sb5A Sb4 132.37(2) 9_665 . ?
Zn1 Sb5A Sb4 126.2(2) 13_655 . ?
Zn1 Sb5A Sb4 53.8(2) 5_454 . ?
Zn1 Sb5A Sb4 53.8(2) 13 . ?
Zn1 Sb5A Sb4 126.2(2) 5_554 . ?
Sb5B Sb5A Sb4 47.63(2) 9_665 9_665 ?
Zn1 Sb5A Sb4 53.8(2) 13_655 9_665 ?
Zn1 Sb5A Sb4 126.2(2) 5_454 9_665 ?
Zn1 Sb5A Sb4 126.2(2) 13 9_665 ?
Zn1 Sb5A Sb4 53.8(2) 5_554 9_665 ?
Sb4 Sb5A Sb4 180.0 . 9_665 ?
Sb5B Sb5A Sb4 47.63(2) 9_665 1_655 ?
Zn1 Sb5A Sb4 53.8(2) 13_655 1_655 ?
Zn1 Sb5A Sb4 126.2(2) 5_454 1_655 ?
Zn1 Sb5A Sb4 126.2(2) 13 1_655 ?
Zn1 Sb5A Sb4 53.8(2) 5_554 1_655 ?
Sb4 Sb5A Sb4 84.74(4) . 1_655 ?
Sb4 Sb5A Sb4 95.26(4) 9_665 1_655 ?
Sb5B Sb5A Sb4 132.37(2) 9_665 9_565 ?
Zn1 Sb5A Sb4 126.2(2) 13_655 9_565 ?
Zn1 Sb5A Sb4 53.8(2) 5_454 9_565 ?
Zn1 Sb5A Sb4 53.8(2) 13 9_565 ?
Zn1 Sb5A Sb4 126.2(2) 5_554 9_565 ?
Sb4 Sb5A Sb4 95.26(4) . 9_565 ?
Sb4 Sb5A Sb4 84.74(4) 9_665 9_565 ?
Sb4 Sb5A Sb4 180.0 1_655 9_565 ?
Sb5B Sb5A Sm1 90.000(1) 9_665 14 ?
Zn1 Sb5A Sm1 68.1(4) 13_655 14 ?
Zn1 Sb5A Sm1 111.9(4) 5_454 14 ?
Zn1 Sb5A Sm1 68.1(4) 13 14 ?
Zn1 Sb5A Sm1 111.9(4) 5_554 14 ?
Sb4 Sb5A Sm1 117.791(16) . 14 ?
Sb4 Sb5A Sm1 62.209(16) 9_665 14 ?
Sb4 Sb5A Sm1 117.791(16) 1_655 14 ?
Sb4 Sb5A Sm1 62.209(16) 9_565 14 ?
Sb5B Sb5A Sm1 90.000(1) 9_665 6_554 ?
Zn1 Sb5A Sm1 111.9(4) 13_655 6_554 ?
Zn1 Sb5A Sm1 68.1(4) 5_454 6_554 ?
Zn1 Sb5A Sm1 111.9(4) 13 6_554 ?
Zn1 Sb5A Sm1 68.1(4) 5_554 6_554 ?
Sb4 Sb5A Sm1 62.209(16) . 6_554 ?
Sb4 Sb5A Sm1 117.791(16) 9_665 6_554 ?
Sb4 Sb5A Sm1 62.209(16) 1_655 6_554 ?
Sb4 Sb5A Sm1 117.791(16) 9_565 6_554 ?
Sm1 Sb5A Sm1 180.00(2) 14 6_554 ?
Sb5B Sb5A Sm1 90.0 9_665 13 ?
Zn1 Sb5A Sm1 68.1(4) 13_655 13 ?
Zn1 Sb5A Sm1 111.9(4) 5_454 13 ?
Zn1 Sb5A Sm1 68.1(4) 13 13 ?
Zn1 Sb5A Sm1 111.9(4) 5_554 13 ?
Sb4 Sb5A Sm1 62.209(16) . 13 ?
Sb4 Sb5A Sm1 117.791(16) 9_665 13 ?
Sb4 Sb5A Sm1 62.209(16) 1_655 13 ?
Sb4 Sb5A Sm1 117.791(16) 9_565 13 ?
Sm1 Sb5A Sm1 78.26(3) 14 13 ?
Sm1 Sb5A Sm1 101.74(3) 6_554 13 ?
Sb5B Sb5A Sm1 90.0 9_665 5_554 ?
Zn1 Sb5A Sm1 111.9(4) 13_655 5_554 ?
Zn1 Sb5A Sm1 68.1(4) 5_454 5_554 ?
Zn1 Sb5A Sm1 111.9(4) 13 5_554 ?
Zn1 Sb5A Sm1 68.1(4) 5_554 5_554 ?
Sb4 Sb5A Sm1 117.791(16) . 5_554 ?
Sb4 Sb5A Sm1 62.209(16) 9_665 5_554 ?
Sb4 Sb5A Sm1 117.791(16) 1_655 5_554 ?
Sb4 Sb5A Sm1 62.209(16) 9_565 5_554 ?
Sm1 Sb5A Sm1 101.74(3) 14 5_554 ?
Sm1 Sb5A Sm1 78.26(3) 6_554 5_554 ?
Sm1 Sb5A Sm1 180.00(2) 13 5_554 ?
Sb5B Sb5A Sb5B 0.0 9_665 1_655 ?
Zn1 Sb5A Sb5B 28.8(6) 13_655 1_655 ?
Zn1 Sb5A Sb5B 151.2(6) 5_454 1_655 ?
Zn1 Sb5A Sb5B 151.2(6) 13 1_655 ?
Zn1 Sb5A Sb5B 28.8(6) 5_554 1_655 ?
Sb4 Sb5A Sb5B 132.37(2) . 1_655 ?
Sb4 Sb5A Sb5B 47.63(2) 9_665 1_655 ?
Sb4 Sb5A Sb5B 47.63(2) 1_655 1_655 ?
Sb4 Sb5A Sb5B 132.37(2) 9_565 1_655 ?
Sm1 Sb5A Sb5B 90.000(1) 14 1_655 ?
Sm1 Sb5A Sb5B 90.000(1) 6_554 1_655 ?
Sm1 Sb5A Sb5B 90.000(1) 13 1_655 ?
Sm1 Sb5A Sb5B 90.000(1) 5_554 1_655 ?
Sb5B Sb5A Sb5B 180.0 9_665 9_565 ?
Zn1 Sb5A Sb5B 151.2(6) 13_655 9_565 ?
Zn1 Sb5A Sb5B 28.8(6) 5_454 9_565 ?
Zn1 Sb5A Sb5B 28.8(6) 13 9_565 ?
Zn1 Sb5A Sb5B 151.2(6) 5_554 9_565 ?
Sb4 Sb5A Sb5B 47.63(2) . 9_565 ?
Sb4 Sb5A Sb5B 132.37(2) 9_665 9_565 ?
Sb4 Sb5A Sb5B 132.37(2) 1_655 9_565 ?
Sb4 Sb5A Sb5B 47.63(2) 9_565 9_565 ?
Sm1 Sb5A Sb5B 90.000(1) 14 9_565 ?
Sm1 Sb5A Sb5B 90.000(1) 6_554 9_565 ?
Sm1 Sb5A Sb5B 90.000(1) 13 9_565 ?
Sm1 Sb5A Sb5B 90.000(1) 5_554 9_565 ?
Sb5B Sb5A Sb5B 180.0 1_655 9_565 ?
Sb5B Sb5B Zn1 145.0(7) 9_665 5_454 ?
Sb5B Sb5B Zn1 145.0(7) 9_665 13 ?
Zn1 Sb5B Zn1 69.9(14) 5_454 13 ?
Sb5B Sb5B Zn1 24.3(5) 9_665 13_655 ?
Zn1 Sb5B Zn1 169.3(2) 5_454 13_655 ?
Zn1 Sb5B Zn1 120.7(12) 13 13_655 ?
Sb5B Sb5B Zn1 24.3(5) 9_665 5_554 ?
Zn1 Sb5B Zn1 120.7(12) 5_454 5_554 ?
Zn1 Sb5B Zn1 169.3(2) 13 5_554 ?
Zn1 Sb5B Zn1 48.6(11) 13_655 5_554 ?
Sb5B Sb5B Sb4 125.59(14) 9_665 . ?
Zn1 Sb5B Sb4 61.5(3) 5_454 . ?
Zn1 Sb5B Sb4 61.5(3) 13 . ?
Zn1 Sb5B Sb4 122.03(18) 13_655 . ?
Zn1 Sb5B Sb4 122.03(18) 5_554 . ?
Sb5B Sb5B Sb4 125.59(14) 9_665 9_565 ?
Zn1 Sb5B Sb4 61.5(3) 5_454 9_565 ?
Zn1 Sb5B Sb4 61.5(3) 13 9_565 ?
Zn1 Sb5B Sb4 122.03(18) 13_655 9_565 ?
Zn1 Sb5B Sb4 122.03(18) 5_554 9_565 ?
Sb4 Sb5B Sb4 108.8(3) . 9_565 ?
Sb5B Sb5B Sb5B 180.0 9_665 9_565 ?
Zn1 Sb5B Sb5B 35.0(7) 5_454 9_565 ?
Zn1 Sb5B Sb5B 35.0(7) 13 9_565 ?
Zn1 Sb5B Sb5B 155.7(5) 13_655 9_565 ?
Zn1 Sb5B Sb5B 155.7(5) 5_554 9_565 ?
Sb4 Sb5B Sb5B 54.41(14) . 9_565 ?
Sb4 Sb5B Sb5B 54.41(14) 9_565 9_565 ?
Sb5B Sb5B Sm1 82.23(14) 9_665 14 ?
Zn1 Sb5B Sm1 123.5(5) 5_454 14 ?
Zn1 Sb5B Sm1 70.8(5) 13 14 ?
Zn1 Sb5B Sm1 63.9(4) 13_655 14 ?
Zn1 Sb5B Sm1 101.1(5) 5_554 14 ?
Sb4 Sb5B Sm1 125.96(14) . 14 ?
Sb4 Sb5B Sm1 64.55(3) 9_565 14 ?
Sb5B Sb5B Sm1 97.77(14) 9_565 14 ?
Sb5B Sb5B Sm1 82.23(14) 9_665 6_554 ?
Zn1 Sb5B Sm1 70.8(5) 5_454 6_554 ?
Zn1 Sb5B Sm1 123.5(5) 13 6_554 ?
Zn1 Sb5B Sm1 101.1(5) 13_655 6_554 ?
Zn1 Sb5B Sm1 63.9(4) 5_554 6_554 ?
Sb4 Sb5B Sm1 64.55(3) . 6_554 ?
Sb4 Sb5B Sm1 125.96(14) 9_565 6_554 ?
Sb5B Sb5B Sm1 97.77(14) 9_565 6_554 ?
Sm1 Sb5B Sm1 164.5(3) 14 6_554 ?
Sb5B Sb5B Sm1 82.23(14) 9_665 5_554 ?
Zn1 Sb5B Sm1 70.8(5) 5_454 5_554 ?
Zn1 Sb5B Sm1 123.5(5) 13 5_554 ?
Zn1 Sb5B Sm1 101.1(5) 13_655 5_554 ?
Zn1 Sb5B Sm1 63.9(4) 5_554 5_554 ?
Sb4 Sb5B Sm1 125.96(14) . 5_554 ?
Sb4 Sb5B Sm1 64.55(3) 9_565 5_554 ?
Sb5B Sb5B Sm1 97.77(14) 9_565 5_554 ?
Sm1 Sb5B Sm1 100.46(6) 14 5_554 ?
Sm1 Sb5B Sm1 77.40(4) 6_554 5_554 ?
Sb5B Sb5B Sm1 82.23(14) 9_665 13 ?
Zn1 Sb5B Sm1 123.5(5) 5_454 13 ?
Zn1 Sb5B Sm1 70.8(5) 13 13 ?
Zn1 Sb5B Sm1 63.9(4) 13_655 13 ?
Zn1 Sb5B Sm1 101.1(5) 5_554 13 ?
Sb4 Sb5B Sm1 64.55(3) . 13 ?
Sb4 Sb5B Sm1 125.96(14) 9_565 13 ?
Sb5B Sb5B Sm1 97.77(14) 9_565 13 ?
Sm1 Sb5B Sm1 77.40(4) 14 13 ?
Sm1 Sb5B Sm1 100.46(6) 6_554 13 ?
Sm1 Sb5B Sm1 164.5(3) 5_554 13 ?
Sb5B Sb5B Sb4 42.05(10) 9_665 9_665 ?
Zn1 Sb5B Sb4 127.5(4) 5_454 9_665 ?
Zn1 Sb5B Sb4 127.5(4) 13 9_665 ?
Zn1 Sb5B Sb4 47.4(3) 13_655 9_665 ?
Zn1 Sb5B Sb4 47.4(3) 5_554 9_665 ?
Sb4 Sb5B Sb4 167.6(2) . 9_665 ?
Sb4 Sb5B Sb4 83.54(6) 9_565 9_665 ?
Sb5B Sb5B Sb4 137.95(10) 9_565 9_665 ?
Sm1 Sb5B Sb4 58.72(7) 14 9_665 ?
Sm1 Sb5B Sb4 108.57(18) 6_554 9_665 ?
Sm1 Sb5B Sb4 58.72(7) 5_554 9_665 ?
Sm1 Sb5B Sb4 108.57(18) 13 9_665 ?
Sb5B Sb5B Sb4 42.05(10) 9_665 1_655 ?
Zn1 Sb5B Sb4 127.5(4) 5_454 1_655 ?
Zn1 Sb5B Sb4 127.5(4) 13 1_655 ?
Zn1 Sb5B Sb4 47.4(3) 13_655 1_655 ?
Zn1 Sb5B Sb4 47.4(3) 5_554 1_655 ?
Sb4 Sb5B Sb4 83.54(6) . 1_655 ?
Sb4 Sb5B Sb4 167.6(2) 9_565 1_655 ?
Sb5B Sb5B Sb4 137.95(10) 9_565 1_655 ?
Sm1 Sb5B Sb4 108.57(18) 14 1_655 ?
Sm1 Sb5B Sb4 58.72(7) 6_554 1_655 ?
Sm1 Sb5B Sb4 108.57(18) 5_554 1_655 ?
Sm1 Sb5B Sb4 58.72(7) 13 1_655 ?
Sb4 Sb5B Sb4 84.11(19) 9_665 1_655 ?
Sb5B Sb5B Sb5A 180.0 9_665 1_455 ?
Zn1 Sb5B Sb5A 35.0(7) 5_454 1_455 ?
Zn1 Sb5B Sb5A 35.0(7) 13 1_455 ?
Zn1 Sb5B Sb5A 155.7(5) 13_655 1_455 ?
Zn1 Sb5B Sb5A 155.7(5) 5_554 1_455 ?
Sb4 Sb5B Sb5A 54.41(14) . 1_455 ?
Sb4 Sb5B Sb5A 54.41(14) 9_565 1_455 ?
Sb5B Sb5B Sb5A 0.0 9_565 1_455 ?
Sm1 Sb5B Sb5A 97.77(14) 14 1_455 ?
Sm1 Sb5B Sb5A 97.77(14) 6_554 1_455 ?
Sm1 Sb5B Sb5A 97.77(14) 5_554 1_455 ?
Sm1 Sb5B Sb5A 97.77(14) 13 1_455 ?
Sb4 Sb5B Sb5A 137.95(10) 9_665 1_455 ?
Sb4 Sb5B Sb5A 137.95(10) 1_655 1_455 ?
Sb5B Sb5B Sb3 113.73(11) 9_665 5_454 ?
Zn1 Sb5B Sb3 31.3(7) 5_454 5_454 ?
Zn1 Sb5B Sb3 101.2(7) 13 5_454 ?
Zn1 Sb5B Sb3 138.0(6) 13_655 5_454 ?
Zn1 Sb5B Sb3 89.4(5) 5_554 5_454 ?
Sb4 Sb5B Sb3 76.46(11) . 5_454 ?
Sb4 Sb5B Sb3 76.46(11) 9_565 5_454 ?
Sb5B Sb5B Sb3 66.27(11) 9_565 5_454 ?
Sm1 Sb5B Sb3 139.29(10) 14 5_454 ?
Sm1 Sb5B Sb3 49.52(4) 6_554 5_454 ?
Sm1 Sb5B Sb3 49.52(4) 5_554 5_454 ?
Sm1 Sb5B Sb3 139.29(10) 13 5_454 ?
Sb4 Sb5B Sb3 107.39(5) 9_665 5_454 ?
Sb4 Sb5B Sb3 107.39(5) 1_655 5_454 ?
Sb5A Sb5B Sb3 66.27(11) 1_455 5_454 ?
Sb6B Sb6A Sb6B 180.0 9 . ?
Sb6B Sb6A Sm2 90.0 9 . ?
Sb6B Sb6A Sm2 90.0 . . ?
Sb6B Sb6A Sm2 90.0 9 9 ?
Sb6B Sb6A Sm2 90.0 . 9 ?
Sm2 Sb6A Sm2 180.0 . 9 ?
Sb6B Sb6A Sb2 54.770(19) 9 5_444 ?
Sb6B Sb6A Sb2 125.230(19) . 5_444 ?
Sm2 Sb6A Sb2 123.458(19) . 5_444 ?
Sm2 Sb6A Sb2 56.542(19) 9 5_444 ?
Sb6B Sb6A Sb2 125.230(19) 9 13 ?
Sb6B Sb6A Sb2 54.770(19) . 13 ?
Sm2 Sb6A Sb2 56.542(19) . 13 ?
Sm2 Sb6A Sb2 123.458(19) 9 13 ?
Sb2 Sb6A Sb2 180.00(4) 5_444 13 ?
Sb6B Sb6A Sb2 54.770(19) 9 14_545 ?
Sb6B Sb6A Sb2 125.230(19) . 14_545 ?
Sm2 Sb6A Sb2 56.542(19) . 14_545 ?
Sm2 Sb6A Sb2 123.458(19) 9 14_545 ?
Sb2 Sb6A Sb2 109.54(4) 5_444 14_545 ?
Sb2 Sb6A Sb2 70.46(4) 13 14_545 ?
Sb6B Sb6A Sb2 54.770(19) 9 14_445 ?
Sb6B Sb6A Sb2 125.230(19) . 14_445 ?
Sm2 Sb6A Sb2 56.542(19) . 14_445 ?
Sm2 Sb6A Sb2 123.458(19) 9 14_445 ?
Sb2 Sb6A Sb2 66.92(4) 5_444 14_445 ?
Sb2 Sb6A Sb2 113.08(4) 13 14_445 ?
Sb2 Sb6A Sb2 74.13(3) 14_545 14_445 ?
Sb6B Sb6A Sb2 125.230(19) 9 6_454 ?
Sb6B Sb6A Sb2 54.770(19) . 6_454 ?
Sm2 Sb6A Sb2 123.458(19) . 6_454 ?
Sm2 Sb6A Sb2 56.542(19) 9 6_454 ?
Sb2 Sb6A Sb2 70.46(4) 5_444 6_454 ?
Sb2 Sb6A Sb2 109.54(4) 13 6_454 ?
Sb2 Sb6A Sb2 180.00(4) 14_545 6_454 ?
Sb2 Sb6A Sb2 105.87(3) 14_445 6_454 ?
Sb6B Sb6A Sb2 125.230(19) 9 6_554 ?
Sb6B Sb6A Sb2 54.770(19) . 6_554 ?
Sm2 Sb6A Sb2 123.458(19) . 6_554 ?
Sm2 Sb6A Sb2 56.542(19) 9 6_554 ?
Sb2 Sb6A Sb2 113.08(4) 5_444 6_554 ?
Sb2 Sb6A Sb2 66.92(4) 13 6_554 ?
Sb2 Sb6A Sb2 105.87(3) 14_545 6_554 ?
Sb2 Sb6A Sb2 180.00(4) 14_445 6_554 ?
Sb2 Sb6A Sb2 74.13(3) 6_454 6_554 ?
Sb6B Sb6A Sb2 54.770(19) 9 5_544 ?
Sb6B Sb6A Sb2 125.230(19) . 5_544 ?
Sm2 Sb6A Sb2 123.458(19) . 5_544 ?
Sm2 Sb6A Sb2 56.542(19) 9 5_544 ?
Sb2 Sb6A Sb2 74.13(3) 5_444 5_544 ?
Sb2 Sb6A Sb2 105.87(3) 13 5_544 ?
Sb2 Sb6A Sb2 66.92(4) 14_545 5_544 ?
Sb2 Sb6A Sb2 109.54(4) 14_445 5_544 ?
Sb2 Sb6A Sb2 113.08(4) 6_454 5_544 ?
Sb2 Sb6A Sb2 70.46(4) 6_554 5_544 ?
Sb6B Sb6A Sb2 125.230(19) 9 13_455 ?
Sb6B Sb6A Sb2 54.770(19) . 13_455 ?
Sm2 Sb6A Sb2 56.542(19) . 13_455 ?
Sm2 Sb6A Sb2 123.458(19) 9 13_455 ?
Sb2 Sb6A Sb2 105.87(3) 5_444 13_455 ?
Sb2 Sb6A Sb2 74.13(3) 13 13_455 ?
Sb2 Sb6A Sb2 113.08(4) 14_545 13_455 ?
Sb2 Sb6A Sb2 70.46(4) 14_445 13_455 ?
Sb2 Sb6A Sb2 66.92(4) 6_454 13_455 ?
Sb2 Sb6A Sb2 109.54(4) 6_554 13_455 ?
Sb2 Sb6A Sb2 180.00(3) 5_544 13_455 ?
Sb6A Sb6B Sb6B 0.0 . 9 ?
Sb6A Sb6B Sb2 104.3(4) . 13 ?
Sb6B Sb6B Sb2 104.3(4) 9 13 ?
Sb6A Sb6B Sb2 104.3(4) . 6_454 ?
Sb6B Sb6B Sb2 104.3(4) 9 6_454 ?
Sb2 Sb6B Sb2 151.3(8) 13 6_454 ?
Sb6A Sb6B Sb2 104.3(4) . 6_554 ?
Sb6B Sb6B Sb2 104.3(4) 9 6_554 ?
Sb2 Sb6B Sb2 81.68(18) 13 6_554 ?
Sb2 Sb6B Sb2 91.3(2) 6_454 6_554 ?
Sb6A Sb6B Sb2 104.3(4) . 13_455 ?
Sb6B Sb6B Sb2 104.3(4) 9 13_455 ?
Sb2 Sb6B Sb2 91.3(2) 13 13_455 ?
Sb2 Sb6B Sb2 81.68(18) 6_454 13_455 ?
Sb2 Sb6B Sb2 151.3(8) 6_554 13_455 ?
Sb6A Sb6B Zn2 137.7(3) . 13 ?
Sb6B Sb6B Zn2 137.7(3) 9 13 ?
Sb2 Sb6B Zn2 48.4(2) 13 13 ?
Sb2 Sb6B Zn2 107.3(5) 6_454 13 ?
Sb2 Sb6B Zn2 48.4(2) 6_554 13 ?
Sb2 Sb6B Zn2 107.3(5) 13_455 13 ?
Sb6A Sb6B Zn2 137.7(3) . 13_455 ?
Sb6B Sb6B Zn2 137.7(3) 9 13_455 ?
Sb2 Sb6B Zn2 107.3(5) 13 13_455 ?
Sb2 Sb6B Zn2 48.4(2) 6_454 13_455 ?
Sb2 Sb6B Zn2 107.3(5) 6_554 13_455 ?
Sb2 Sb6B Zn2 48.4(2) 13_455 13_455 ?
Zn2 Sb6B Zn2 84.6(5) 13 13_455 ?
Sb6A Sb6B Sm2 68.9(3) . 9 ?
Sb6B Sb6B Sm2 68.9(3) 9 9 ?
Sb2 Sb6B Sm2 134.36(11) 13 9 ?
Sb2 Sb6B Sm2 58.61(7) 6_454 9 ?
Sb2 Sb6B Sm2 58.61(7) 6_554 9 ?
Sb2 Sb6B Sm2 134.36(11) 13_455 9 ?
Zn2 Sb6B Sm2 105.44(16) 13 9 ?
Zn2 Sb6B Sm2 105.44(16) 13_455 9 ?
Sb6A Sb6B Sm2 68.9(3) . . ?
Sb6B Sb6B Sm2 68.9(3) 9 . ?
Sb2 Sb6B Sm2 58.61(7) 13 . ?
Sb2 Sb6B Sm2 134.36(11) 6_454 . ?
Sb2 Sb6B Sm2 134.36(11) 6_554 . ?
Sb2 Sb6B Sm2 58.61(7) 13_455 . ?
Zn2 Sb6B Sm2 105.44(16) 13 . ?
Zn2 Sb6B Sm2 105.44(16) 13_455 . ?
Sm2 Sb6B Sm2 137.8(6) 9 . ?
Sb6A Sb6B Sb4 180.0 . . ?
Sb6B Sb6B Sb4 180.0 9 . ?
Sb2 Sb6B Sb4 75.7(4) 13 . ?
Sb2 Sb6B Sb4 75.7(4) 6_454 . ?
Sb2 Sb6B Sb4 75.7(4) 6_554 . ?
Sb2 Sb6B Sb4 75.7(4) 13_455 . ?
Zn2 Sb6B Sb4 42.3(3) 13 . ?
Zn2 Sb6B Sb4 42.3(3) 13_455 . ?
Sm2 Sb6B Sb4 111.1(3) 9 . ?
Sm2 Sb6B Sb4 111.1(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sm1 Zn2 3.166(2) . ?
Sm1 Sb3 3.1768(9) 1_455 ?
Sm1 Sb3 3.1768(9) . ?
Sm1 Zn1 3.272(13) 1_455 ?
Sm1 Zn1 3.272(13) . ?
Sm1 Sb1 3.2867(10) 13 ?
Sm1 Sb1 3.2867(10) 13_455 ?
Sm1 Sb5A 3.3002(10) 5_445 ?
Sm1 Sb4 3.3128(9) 13 ?
Sm1 Sb4 3.3128(9) 13_455 ?
Sm1 Sb1 3.3188(14) . ?
Sm1 Sb5B 3.3308(15) 13 ?
Sm1 Sb5B 3.3308(15) 5_445 ?
Sm1 Sb2 3.4953(16) . ?
Sm1 Sm2 4.1121(14) . ?
Sm1 Sm1 4.1653(18) 2 ?
Sm1 Sm1 4.1838(13) 1_655 ?
Sm1 Sm1 4.1838(13) 1_455 ?
Sm2 Sb3 3.1624(13) . ?
Sm2 Sb3 3.1624(13) 1_455 ?
Sm2 Sb1 3.2129(13) . ?
Sm2 Sb1 3.2129(13) 2 ?
Sm2 Sb2 3.2148(11) 14_445 ?
Sm2 Sb2 3.2148(11) 13 ?
Sm2 Sb2 3.2148(11) 13_455 ?
Sm2 Sb2 3.2148(11) 14_545 ?
Sm2 Sb6A 3.3100(14) . ?
Sm2 Sb6B 3.548(8) 9 ?
Sm2 Sb6B 3.548(8) . ?
Sm2 Sm1 4.1121(14) 2 ?
Sm2 Sm2 4.1838(13) 1_455 ?
Sm2 Sm2 4.1838(13) 1_655 ?
Zn1 Sb5B 2.003(18) 5_545 ?
Zn1 Sb5B 2.003(18) 13 ?
Zn1 Zn1 2.30(6) 9_656 ?
Zn1 Sb5A 2.386(14) 5_545 ?
Zn1 Sb5A 2.386(14) 5_445 ?
Zn1 Sb4 2.565(13) 13 ?
Zn1 Sb4 2.565(13) 5_545 ?
Zn1 Sb3 2.59(3) . ?
Zn1 Sb5B 2.790(14) 13_655 ?
Zn1 Sb5B 2.790(14) 5_445 ?
Zn1 Sm1 3.272(12) 2 ?
Zn1 Sm1 3.272(12) 1_655 ?
Zn1 Sm1 3.272(12) 2_655 ?
Zn2 Sb2 2.477(2) 10_556 ?
Zn2 Sb2 2.477(2) . ?
Zn2 Sb4 2.665(2) 13_455 ?
Zn2 Sb4 2.665(2) 13 ?
Zn2 Sb6B 3.107(16) 13 ?
Zn2 Sb6B 3.107(16) 13_455 ?
Zn2 Sm1 3.166(2) 10_556 ?
Sb1 Sb2 3.0102(11) 13_455 ?
Sb1 Sb2 3.0102(11) 13 ?
Sb1 Sb1 3.0908(13) 13 ?
Sb1 Sb1 3.0908(13) 13_455 ?
Sb1 Sm1 3.2867(10) 13 ?
Sb1 Sm1 3.2867(10) 13_455 ?
Sb2 Sb6B 2.926(5) 13 ?
Sb2 Sb6B 2.926(5) 13_455 ?
Sb2 Sb1 3.0102(11) 13_455 ?
Sb2 Sb1 3.0102(11) 13 ?
Sb2 Sm2 3.2148(11) 13 ?
Sb2 Sm2 3.2148(11) 13_455 ?
Sb2 Sb6A 3.4707(10) 5 ?
Sb2 Sb6A 3.4707(10) 5_455 ?
Sb2 Sb2 3.827(2) 10_556 ?
Sb2 Sb2 4.004(2) 2_565 ?
Sb3 Sm2 3.1624(13) 1_655 ?
Sb3 Sm1 3.1768(9) 1_655 ?
Sb3 Sm1 3.1768(9) 2 ?
Sb3 Sm1 3.1768(9) 2_655 ?
Sb3 Sb5B 4.079(4) 5_545 ?
Sb3 Sb5B 4.079(4) 13 ?
Sb4 Zn1 2.565(13) 13 ?
Sb4 Zn1 2.565(13) 5_454 ?
Sb4 Zn2 2.665(2) 13_455 ?
Sb4 Zn2 2.665(2) 13 ?
Sb4 Sb5B 2.820(5) . ?
Sb4 Sb5B 2.820(5) 9_565 ?
Sb4 Sb5A 3.1042(11) . ?
Sb4 Sb5A 3.1042(11) 1_455 ?
Sb4 Sm1 3.3128(9) 13 ?
Sb4 Sm1 3.3128(9) 6_454 ?
Sb4 Sm1 3.3128(9) 6_554 ?
Sb4 Sm1 3.3128(9) 13_455 ?
Sb4 Sb5B 3.424(6) 9_665 ?
Sb4 Sb5B 3.424(6) 1_455 ?
Sb4 Sb6B 3.95(2) . ?
Sb5A Sb5B 0.450(9) 9_665 ?
Sb5A Zn1 2.386(14) 13_655 ?
Sb5A Zn1 2.386(14) 5_454 ?
Sb5A Zn1 2.386(14) 13 ?
Sb5A Zn1 2.386(14) 5_554 ?
Sb5A Sb4 3.1042(11) 9_665 ?
Sb5A Sb4 3.1042(11) 1_655 ?
Sb5A Sb4 3.1042(11) 9_565 ?
Sb5A Sm1 3.3002(10) 14 ?
Sb5A Sm1 3.3002(10) 6_554 ?
Sb5A Sm1 3.3002(10) 13 ?
Sb5A Sm1 3.3002(10) 5_554 ?
Sb5A Sb5B 3.733(9) 1_655 ?
Sb5A Sb5B 3.733(9) 9_565 ?
Sb5B Sb5B 0.901(17) 9_665 ?
Sb5B Zn1 2.003(18) 5_454 ?
Sb5B Zn1 2.003(18) 13 ?
Sb5B Zn1 2.790(14) 13_655 ?
Sb5B Zn1 2.790(14) 5_554 ?
Sb5B Sb4 2.820(5) 9_565 ?
Sb5B Sb5B 3.283(17) 9_565 ?
Sb5B Sm1 3.3308(15) 14 ?
Sb5B Sm1 3.3308(15) 6_554 ?
Sb5B Sm1 3.3308(15) 5_554 ?
Sb5B Sm1 3.3308(15) 13 ?
Sb5B Sb4 3.424(6) 9_665 ?
Sb5B Sb4 3.424(6) 1_655 ?
Sb5B Sb5A 3.733(9) 1_455 ?
Sb5B Sb3 4.079(4) 5_454 ?
Sb6A Sb6B 1.28(2) 9 ?
Sb6A Sb6B 1.28(2) . ?
Sb6A Sm2 3.3100(14) 9 ?
Sb6A Sb2 3.4707(10) 5_444 ?
Sb6A Sb2 3.4707(10) 13 ?
Sb6A Sb2 3.4707(10) 14_545 ?
Sb6A Sb2 3.4707(10) 14_445 ?
Sb6A Sb2 3.4707(10) 6_454 ?
Sb6A Sb2 3.4707(10) 6_554 ?
Sb6A Sb2 3.4707(10) 5_544 ?
Sb6A Sb2 3.4707(10) 13_455 ?
Sb6B Sb6B 2.56(4) 9 ?
Sb6B Sb2 2.926(5) 13 ?
Sb6B Sb2 2.926(5) 6_454 ?
Sb6B Sb2 2.926(5) 6_554 ?
Sb6B Sb2 2.926(5) 13_455 ?
Sb6B Zn2 3.107(16) 13 ?
Sb6B Zn2 3.107(16) 13_455 ?
Sb6B Sm2 3.548(8) 9 ?
