#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:07:27 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179094 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/56/4305667.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305667
loop_
_publ_author_name
'José M. Casas'
'Beatriz E. Diosdado'
'Juan Forniés'
'Antonio Martín'
'Angel J. Rueda'
'A. Guy Orpen'
_publ_section_title
;
Synthesis of Binuclear Platinum Complexes Containing the Ligands
8-Naphthyridine, 2-Aminopyridine, and 7-Azaindolate. An Experimental Study
of the Steric Hindrance of the Bulky Pentafluorophenyl Ligands in the
Synthesis of Binuclear Complexes
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8767
_journal_page_last               8775
_journal_paper_doi               10.1021/ic8006475
_journal_volume                  47
_journal_year                    2008
_chemical_formula_sum            'C36 H16 Cl4 F20 N4 Pt2'
_chemical_formula_weight         1416.51
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                97.550(11)
_cell_angle_beta                 94.610(6)
_cell_angle_gamma                100.28(2)
_cell_formula_units_Z            2
_cell_length_a                   10.326(2)
_cell_length_b                   11.2017(13)
_cell_length_c                   18.241(2)
_cell_measurement_reflns_used    75
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      30.1
_cell_measurement_theta_min      20.7
_cell_volume                     2046.4(5)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      200(2)
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_method       'profile data from q/2q scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0197
_diffrn_reflns_av_sigmaI/netI    0.0315
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            7600
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.02
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    7.218
_exptl_absorpt_correction_T_max  0.697
_exptl_absorpt_correction_T_min  0.128
_exptl_absorpt_correction_type   psi-scan
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.299
_exptl_crystal_description       plate
_exptl_crystal_F_000             1328
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.230
_refine_diff_density_min         -2.188
_refine_diff_density_rms         0.215
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.039
_refine_ls_goodness_of_fit_obs   1.052
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     598
_refine_ls_number_reflns         7170
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.054
_refine_ls_restrained_S_obs      1.052
_refine_ls_R_factor_all          0.0554
_refine_ls_R_factor_obs          0.0462
_refine_ls_shift/esd_max         0.001
_refine_ls_shift/esd_mean        0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1200P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.1514
_refine_ls_wR_factor_obs         0.1390
_reflns_number_observed          6137
_reflns_number_total             7172
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ic8006475_si_001_1.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' tag value 'psi-scans' was replaced
with 'psi-scan' value.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.1200P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.1200P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2046.2(5)
_cod_database_code               4305667
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Pt1 Pt 0.06472(3) 0.33873(3) 0.372351(15) 0.02280(14) Uani 1 d . .
Pt2 Pt 0.14678(3) 0.34802(3) 0.15804(2) 0.02558(14) Uani 1 d . .
F1 F 0.3557(6) 0.3104(7) 0.3437(3) 0.050(2) Uani 1 d . .
F2 F 0.5723(6) 0.3159(7) 0.4342(4) 0.059(2) Uani 1 d . .
F3 F 0.5672(6) 0.3536(6) 0.5851(3) 0.050(2) Uani 1 d . .
F4 F 0.3399(7) 0.3860(7) 0.6412(3) 0.059(2) Uani 1 d . .
F5 F 0.1235(5) 0.3892(5) 0.5530(3) 0.0378(13) Uani 1 d . .
F6 F -0.1369(5) 0.3467(5) 0.4957(3) 0.0340(12) Uani 1 d . .
F7 F -0.2777(6) 0.1680(6) 0.5557(3) 0.052(2) Uani 1 d . .
F8 F -0.2660(7) -0.0713(6) 0.5122(4) 0.059(2) Uani 1 d . .
F9 F -0.1011(7) -0.1300(5) 0.4082(4) 0.054(2) Uani 1 d . .
F10 F 0.0452(6) 0.0475(5) 0.3489(3) 0.0460(14) Uani 1 d . .
F11 F 0.0535(8) 0.1863(7) 0.0009(4) 0.067(2) Uani 1 d . .
F12 F 0.1426(8) -0.0032(8) -0.0716(4) 0.075(2) Uani 1 d . .
F13 F 0.3487(8) -0.0891(7) -0.0086(4) 0.070(2) Uani 1 d . .
F14 F 0.4669(7) 0.0200(7) 0.1280(4) 0.069(2) Uani 1 d . .
F15 F 0.3774(6) 0.2051(6) 0.2020(3) 0.051(2) Uani 1 d . .
F16 F 0.1582(8) 0.4540(7) 0.0040(3) 0.070(2) Uani 1 d . .
F17 F 0.3450(12) 0.6129(9) -0.0445(4) 0.108(4) Uani 1 d . .
F18 F 0.5743(10) 0.7153(8) 0.0436(6) 0.113(4) Uani 1 d . .
F19 F 0.6122(8) 0.6528(8) 0.1808(5) 0.090(3) Uani 1 d . .
F20 F 0.4269(6) 0.4970(7) 0.2327(3) 0.056(2) Uani 1 d . .
N1 N -0.1021(6) 0.3219(7) 0.2950(3) 0.026(2) Uani 1 d . .
N2 N 0.0061(8) 0.2178(8) 0.2041(4) 0.034(2) Uani 1 d . .
H2A H -0.0204(8) 0.1481(8) 0.1696(4) 0.040 Uiso 1 calc R .
H2B H 0.0476(8) 0.1960(8) 0.2455(4) 0.040 Uiso 1 calc R .
N3 N 0.0686(7) 0.4957(6) 0.2071(4) 0.0256(15) Uani 1 d . .
N4 N 0.1720(7) 0.4902(7) 0.3246(4) 0.029(2) Uani 1 d . .
H4A H 0.2157(7) 0.5496(7) 0.3625(4) 0.035 Uiso 1 calc R .
H4B H 0.2348(7) 0.4622(7) 0.2974(4) 0.035 Uiso 1 calc R .
C1 C 0.2273(8) 0.3482(8) 0.4437(4) 0.023(2) Uani 1 d . .
C2 C 0.3460(9) 0.3292(9) 0.4178(5) 0.033(2) Uani 1 d . .
C3 C 0.4608(9) 0.3315(9) 0.4642(6) 0.036(2) Uani 1 d . .
C4 C 0.4573(9) 0.3511(9) 0.5382(5) 0.032(2) Uani 1 d . .
C5 C 0.3435(10) 0.3673(9) 0.5676(4) 0.035(2) Uani 1 d . .
C6 C 0.2342(9) 0.3682(8) 0.5204(5) 0.027(2) Uani 1 d . .
C7 C -0.0374(8) 0.2040(8) 0.4193(4) 0.023(2) Uani 1 d . .
C8 C -0.1246(8) 0.2288(7) 0.4717(4) 0.025(2) Uani 1 d . .
C9 C -0.1994(10) 0.1385(9) 0.5041(5) 0.036(2) Uani 1 d . .
C10 C -0.1920(10) 0.0171(9) 0.4824(5) 0.038(2) Uani 1 d . .
C11 C -0.1093(10) -0.0087(8) 0.4294(5) 0.035(2) Uani 1 d . .
C12 C -0.0347(9) 0.0823(9) 0.4018(5) 0.031(2) Uani 1 d . .
C13 C 0.2150(9) 0.2063(9) 0.1047(5) 0.031(2) Uani 1 d . .
C14 C 0.1586(10) 0.1486(10) 0.0335(5) 0.041(2) Uani 1 d . .
C15 C 0.2024(11) 0.0512(11) -0.0046(5) 0.045(3) Uani 1 d . .
C16 C 0.3049(11) 0.0073(10) 0.0269(6) 0.049(3) Uani 1 d . .
C17 C 0.3656(10) 0.0627(10) 0.0967(6) 0.043(2) Uani 1 d . .
C18 C 0.3186(10) 0.1575(10) 0.1328(5) 0.039(2) Uani 1 d . .
C19 C 0.2869(9) 0.4651(9) 0.1189(5) 0.036(2) Uani 1 d . .
C20 C 0.2713(12) 0.5039(11) 0.0495(5) 0.049(3) Uani 1 d . .
C21 C 0.3670(18) 0.5828(14) 0.0253(7) 0.070(4) Uani 1 d . .
C22 C 0.4809(15) 0.6341(13) 0.0681(9) 0.073(4) Uani 1 d . .
C23 C 0.5004(11) 0.6033(10) 0.1380(7) 0.053(3) Uani 1 d . .
C24 C 0.4023(9) 0.5213(10) 0.1610(5) 0.038(2) Uani 1 d . .
C25 C -0.2110(9) 0.3668(8) 0.3149(5) 0.030(2) Uani 1 d . .
H25 H -0.2092(9) 0.4053(8) 0.3647(5) 0.036 Uiso 1 calc R .
C26 C -0.3219(9) 0.3595(10) 0.2675(5) 0.035(2) Uani 1 d . .
H26 H -0.3941(9) 0.3946(10) 0.2833(5) 0.042 Uiso 1 calc R .
C27 C -0.3267(9) 0.2984(9) 0.1941(5) 0.036(2) Uani 1 d . .
H27 H -0.4035(9) 0.2891(9) 0.1599(5) 0.043 Uiso 1 calc R .
C28 C -0.2186(9) 0.2532(9) 0.1735(5) 0.035(2) Uani 1 d . .
H28 H -0.2189(9) 0.2140(9) 0.1240(5) 0.042 Uiso 1 calc R .
C29 C -0.1086(8) 0.2644(8) 0.2244(4) 0.025(2) Uani 1 d . .
C30 C -0.0150(10) 0.5420(10) 0.1609(5) 0.037(2) Uani 1 d . .
H30 H -0.0289(10) 0.5096(10) 0.1095(5) 0.045 Uiso 1 calc R .
C31 C -0.0782(11) 0.6324(10) 0.1865(6) 0.045(2) Uani 1 d . .
H31 H -0.1384(11) 0.6610(10) 0.1540(6) 0.055 Uiso 1 calc R .
C32 C -0.0534(12) 0.6837(10) 0.2624(6) 0.048(3) Uani 1 d . .
H32 H -0.0953(12) 0.7485(10) 0.2813(6) 0.058 Uiso 1 calc R .
C33 C 0.0302(11) 0.6400(10) 0.3075(5) 0.044(2) Uani 1 d . .
H33 H 0.0483(11) 0.6739(10) 0.3587(5) 0.052 Uiso 1 calc R .
C34 C 0.0907(9) 0.5434(8) 0.2784(4) 0.030(2) Uani 1 d . .
C35 C 0.2196(14) 0.9131(12) 0.2401(8) 0.094(5) Uani 1 d D .
H35A H 0.2883(14) 0.9885(12) 0.2450(8) 0.113 Uiso 1 calc R .
H35B H 0.1887(14) 0.9060(12) 0.2896(8) 0.113 Uiso 1 calc R .
Cl1 Cl 0.2885(6) 0.7856(5) 0.2105(4) 0.134(2) Uani 1 d D .
Cl2 Cl 0.0861(5) 0.9251(4) 0.1772(3) 0.0971(13) Uani 1 d D .
C36 C 0.3693(23) 0.0912(17) 0.7215(17) 0.080(7) Uani 0.50 d PD 1
H36A H 0.3540(23) 0.1448(17) 0.6839(17) 0.096 Uiso 0.50 calc PR 1
H36B H 0.4409(23) 0.1370(17) 0.7595(17) 0.096 Uiso 0.50 calc PR 1
Cl3 Cl 0.4149(17) -0.0413(13) 0.6794(9) 0.143(3) Uani 0.50 d PD 1
Cl4 Cl 0.2249(14) 0.0498(16) 0.7630(9) 0.143(3) Uani 0.50 d PD 1
C37 C 0.3777(41) -0.0550(18) 0.6937(20) 0.080(7) Uani 0.50 d PD 2
H37A H 0.4336(41) -0.0953(18) 0.7254(20) 0.096 Uiso 0.50 calc PR 2
H37B H 0.3113(41) -0.1196(18) 0.6618(20) 0.096 Uiso 0.50 calc PR 2
Cl5 Cl 0.4752(13) 0.0310(12) 0.6388(7) 0.143(3) Uani 0.50 d PD 2
Cl6 Cl 0.2974(16) 0.0424(16) 0.7496(9) 0.143(3) Uani 0.50 d PD 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C7 Pt1 C1 91.5(3) . . ?
C7 Pt1 N1 88.2(3) . . ?
C1 Pt1 N1 177.3(3) . . ?
C7 Pt1 N4 177.6(3) . . ?
C1 Pt1 N4 88.7(3) . . ?
N1 Pt1 N4 91.8(3) . . ?
C19 Pt2 C13 89.3(4) . . ?
C19 Pt2 N3 90.3(3) . . ?
C13 Pt2 N3 176.3(3) . . ?
C19 Pt2 N2 176.3(3) . . ?
C13 Pt2 N2 89.0(3) . . ?
N3 Pt2 N2 91.5(3) . . ?
C29 N1 C25 116.9(7) . . ?
C29 N1 Pt1 122.2(5) . . ?
C25 N1 Pt1 120.8(5) . . ?
C29 N2 Pt2 113.4(6) . . ?
C34 N3 C30 118.9(8) . . ?
C34 N3 Pt2 125.1(6) . . ?
C30 N3 Pt2 116.0(6) . . ?
C34 N4 Pt1 113.6(5) . . ?
C6 C1 C2 113.0(7) . . ?
C6 C1 Pt1 126.1(6) . . ?
C2 C1 Pt1 120.9(6) . . ?
F1 C2 C1 120.1(7) . . ?
F1 C2 C3 116.2(8) . . ?
C1 C2 C3 123.7(8) . . ?
F2 C3 C4 121.6(8) . . ?
F2 C3 C2 119.6(9) . . ?
C4 C3 C2 118.8(9) . . ?
C3 C4 F3 120.4(8) . . ?
C3 C4 C5 120.8(8) . . ?
F3 C4 C5 118.8(8) . . ?
F4 C5 C4 120.7(8) . . ?
F4 C5 C6 120.5(9) . . ?
C4 C5 C6 118.7(8) . . ?
C5 C6 F5 116.3(7) . . ?
C5 C6 C1 125.0(8) . . ?
F5 C6 C1 118.7(7) . . ?
C12 C7 C8 113.8(8) . . ?
C12 C7 Pt1 124.8(6) . . ?
C8 C7 Pt1 121.3(6) . . ?
F6 C8 C9 116.0(8) . . ?
F6 C8 C7 120.7(7) . . ?
C9 C8 C7 123.2(8) . . ?
F7 C9 C10 120.4(8) . . ?
F7 C9 C8 120.5(9) . . ?
C10 C9 C8 119.1(9) . . ?
F8 C10 C11 122.2(9) . . ?
F8 C10 C9 119.6(9) . . ?
C11 C10 C9 118.2(8) . . ?
C12 C11 C10 120.6(8) . . ?
C12 C11 F9 121.3(9) . . ?
C10 C11 F9 118.1(8) . . ?
C11 C12 C7 125.0(8) . . ?
C11 C12 F10 116.4(8) . . ?
C7 C12 F10 118.5(8) . . ?
C18 C13 C14 113.9(9) . . ?
C18 C13 Pt2 124.8(7) . . ?
C14 C13 Pt2 121.3(7) . . ?
F11 C14 C15 117.7(8) . . ?
F11 C14 C13 119.3(9) . . ?
C15 C14 C13 123.0(9) . . ?
F12 C15 C16 119.5(10) . . ?
F12 C15 C14 120.7(10) . . ?
C16 C15 C14 119.8(9) . . ?
F13 C16 C15 121.2(9) . . ?
F13 C16 C17 119.4(10) . . ?
C15 C16 C17 119.4(9) . . ?
F14 C17 C18 121.4(9) . . ?
F14 C17 C16 119.7(9) . . ?
C18 C17 C16 118.9(10) . . ?
F15 C18 C17 116.8(9) . . ?
F15 C18 C13 118.2(8) . . ?
C17 C18 C13 125.0(9) . . ?
C24 C19 C20 113.9(9) . . ?
C24 C19 Pt2 122.2(7) . . ?
C20 C19 Pt2 123.7(8) . . ?
C21 C20 F16 119.7(10) . . ?
C21 C20 C19 122.1(12) . . ?
F16 C20 C19 118.1(10) . . ?
C20 C21 C22 122.0(11) . . ?
C20 C21 F17 118.2(15) . . ?
C22 C21 F17 119.8(14) . . ?
C21 C22 F18 121.2(15) . . ?
C21 C22 C23 118.8(11) . . ?
F18 C22 C23 120.0(15) . . ?
F19 C23 C24 122.3(11) . . ?
F19 C23 C22 119.6(11) . . ?
C24 C23 C22 118.1(11) . . ?
C19 C24 C23 125.0(10) . . ?
C19 C24 F20 120.0(8) . . ?
C23 C24 F20 115.0(9) . . ?
C26 C25 N1 123.8(8) . . ?
C25 C26 C27 118.2(9) . . ?
C28 C27 C26 118.6(8) . . ?
C27 C28 C29 120.2(8) . . ?
N1 C29 C28 122.2(8) . . ?
N1 C29 N2 116.5(7) . . ?
C28 C29 N2 121.3(8) . . ?
C31 C30 N3 121.9(8) . . ?
C30 C31 C32 119.0(9) . . ?
C33 C32 C31 119.3(9) . . ?
C32 C33 C34 119.4(9) . . ?
N3 C34 N4 117.3(8) . . ?
N3 C34 C33 121.5(8) . . ?
N4 C34 C33 121.2(8) . . ?
Cl1 C35 Cl2 111.4(7) . . ?
Cl3 C36 Cl4 108.7(14) . . ?
Cl5 C37 Cl6 109.0(14) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C7 2.009(8) . ?
Pt1 C1 2.018(8) . ?
Pt1 N1 2.102(6) . ?
Pt1 N4 2.177(7) . ?
Pt2 C19 2.014(9) . ?
Pt2 C13 2.017(9) . ?
Pt2 N3 2.096(7) . ?
Pt2 N2 2.169(8) . ?
F1 C2 1.354(10) . ?
F2 C3 1.342(11) . ?
F3 C4 1.360(9) . ?
F4 C5 1.336(10) . ?
F5 C6 1.372(10) . ?
F6 C8 1.367(10) . ?
F7 C9 1.335(11) . ?
F8 C10 1.342(11) . ?
F9 C11 1.382(10) . ?
F10 C12 1.381(10) . ?
F11 C14 1.355(12) . ?
F12 C15 1.339(11) . ?
F13 C16 1.352(11) . ?
F14 C17 1.342(12) . ?
F15 C18 1.354(10) . ?
F16 C20 1.363(13) . ?
F17 C21 1.372(14) . ?
F18 C22 1.349(14) . ?
F19 C23 1.328(14) . ?
F20 C24 1.384(11) . ?
N1 C29 1.352(10) . ?
N1 C25 1.367(11) . ?
N2 C29 1.434(11) . ?
N3 C34 1.326(11) . ?
N3 C30 1.371(11) . ?
N4 C34 1.402(11) . ?
C1 C6 1.382(11) . ?
C1 C2 1.389(12) . ?
C2 C3 1.395(13) . ?
C3 C4 1.344(13) . ?
C4 C5 1.360(14) . ?
C5 C6 1.366(12) . ?
C7 C12 1.365(12) . ?
C7 C8 1.400(12) . ?
C8 C9 1.387(12) . ?
C9 C10 1.382(14) . ?
C10 C11 1.376(14) . ?
C11 C12 1.342(13) . ?
C13 C18 1.378(13) . ?
C13 C14 1.402(12) . ?
C14 C15 1.381(15) . ?
C15 C16 1.36(2) . ?
C16 C17 1.386(14) . ?
C17 C18 1.360(14) . ?
C19 C24 1.365(14) . ?
C19 C20 1.397(13) . ?
C20 C21 1.35(2) . ?
C21 C22 1.35(2) . ?
C22 C23 1.37(2) . ?
C23 C24 1.373(14) . ?
C25 C26 1.362(12) . ?
C26 C27 1.414(13) . ?
C27 C28 1.365(14) . ?
C28 C29 1.385(12) . ?
C30 C31 1.354(14) . ?
C31 C32 1.411(15) . ?
C32 C33 1.344(15) . ?
C33 C34 1.410(14) . ?
C35 Cl1 1.749(9) . ?
C35 Cl2 1.757(9) . ?
C36 Cl3 1.738(10) . ?
C36 Cl4 1.743(10) . ?
C37 Cl5 1.736(10) . ?
C37 Cl6 1.756(10) . ?
