#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:12:37 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179098 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/60/4306041.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4306041
loop_
_publ_author_name
'Jason R. Price'
'Nicholas G. White'
'Alejandro Perez-Velasco'
'Geoffrey B. Jameson'
'Christopher A. Hunter'
'Sally Brooker'
_publ_section_title
;
Factors Influencing Tetranuclear [2 x 2] Grid vs Dinuclear Side-by-Side
Structures for Silver(I) Complexes of Pyridazine-Based Bis-Bidentate Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              10729
_journal_page_last               10738
_journal_paper_doi               10.1021/ic800959s
_journal_volume                  47
_journal_year                    2008
_chemical_formula_sum            'C178 H162 Ag8 B7 F28 N32 O16'
_chemical_formula_weight         4476.03
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 130.615(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   60.305(3)
_cell_length_b                   21.3256(10)
_cell_length_c                   46.174(3)
_cell_measurement_reflns_used    9951
_cell_measurement_temperature    83(2)
_cell_measurement_theta_max      26.352
_cell_measurement_theta_min      2.260
_cell_volume                     45077(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      83(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker Kappa Apex II area detector'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0869
_diffrn_reflns_av_sigmaI/netI    0.0603
_diffrn_reflns_limit_h_max       63
_diffrn_reflns_limit_h_min       -63
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       48
_diffrn_reflns_limit_l_min       -48
_diffrn_reflns_number            295222
_diffrn_reflns_theta_full        21.97
_diffrn_reflns_theta_max         21.97
_diffrn_reflns_theta_min         2.92
_exptl_absorpt_coefficient_mu    0.761
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.736
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SCALE (Bruker AXS Inc.)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.319
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             17960
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.16
_refine_diff_density_max         0.779
_refine_diff_density_min         -0.582
_refine_diff_density_rms         0.110
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.043
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2392
_refine_ls_number_reflns         27431
_refine_ls_number_restraints     2345
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.1099
_refine_ls_R_factor_gt           0.0810
_refine_ls_shift/su_max          0.010
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1619P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2269
_refine_ls_wR_factor_ref         0.2463
_reflns_number_gt                17388
_reflns_number_total             27431
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic800959s_si_001_2.cif
_cod_data_source_block           jrp69agc_squeezetwinfinal
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        45076(4)
_cod_database_code               4306041
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.60196(2) 0.21593(5) 0.67921(3) 0.0610(3) Uani 1 1 d . . .
Ag2 Ag 0.65586(2) 0.20910(6) 0.79214(3) 0.0692(3) Uani 1 1 d . . .
Ag3 Ag 0.61057(2) 0.03686(5) 0.70298(3) 0.0653(3) Uani 1 1 d . . .
Ag4 Ag 0.67061(2) 0.03091(5) 0.81623(3) 0.0656(3) Uani 1 1 d . . .
N1 N 0.6518(2) 0.2060(5) 0.7183(3) 0.053(3) Uani 1 1 d U . .
N2 N 0.6696(2) 0.2015(5) 0.7580(3) 0.060(3) Uani 1 1 d U . .
C2 C 0.6996(3) 0.1917(7) 0.7778(4) 0.068(4) Uani 1 1 d U . .
C3 C 0.7106(3) 0.1927(8) 0.7601(5) 0.083(4) Uani 1 1 d U . .
H3 H 0.7311 0.1886 0.7749 0.099 Uiso 1 1 calc R . .
C4 C 0.6925(3) 0.1996(8) 0.7202(5) 0.088(5) Uani 1 1 d U . .
H4 H 0.7000 0.1988 0.7074 0.105 Uiso 1 1 calc R . .
C5 C 0.6627(3) 0.2078(7) 0.7009(4) 0.064(4) Uani 1 1 d U . .
C6 C 0.6423(3) 0.2150(7) 0.6606(4) 0.075(4) Uani 1 1 d U . .
H6 H 0.6494 0.2189 0.6473 0.090 Uiso 1 1 calc R . .
N3 N 0.6147(2) 0.2163(5) 0.6417(3) 0.056(3) Uani 1 1 d U . .
C8 C 0.5949(3) 0.2216(3) 0.6019(4) 0.055(3) Uani 1 1 d DU . .
C9 C 0.6029(3) 0.2238(4) 0.5801(4) 0.088(5) Uani 1 1 d DU . .
H9 H 0.6230 0.2217 0.5923 0.105 Uiso 1 1 calc R . .
C10 C 0.5820(3) 0.2292(4) 0.5402(4) 0.085(5) Uani 1 1 d DU . .
H10 H 0.5878 0.2307 0.5254 0.102 Uiso 1 1 calc R . .
C11 C 0.5533(3) 0.2322(3) 0.5232(4) 0.081(4) Uani 1 1 d DU . .
C12 C 0.5455(3) 0.2300(5) 0.5451(4) 0.096(5) Uani 1 1 d DU . .
H12 H 0.5254 0.2322 0.5330 0.115 Uiso 1 1 calc R . .
C13 C 0.5661(3) 0.2247(4) 0.5845(4) 0.068(4) Uani 1 1 d DU . .
H13 H 0.5602 0.2232 0.5992 0.082 Uiso 1 1 calc R . .
O1 O 0.5347(3) 0.2375(5) 0.4835(4) 0.151(6) Uani 1 1 d DU . .
C14 C 0.5062(4) 0.2425(15) 0.4659(7) 0.202(13) Uani 1 1 d DU . .
H14A H 0.4947 0.2458 0.4383 0.303 Uiso 1 1 calc R . .
H14B H 0.5031 0.2799 0.4752 0.303 Uiso 1 1 calc R . .
H14C H 0.5000 0.2052 0.4715 0.303 Uiso 1 1 calc R . .
C16 C 0.7172(3) 0.1857(6) 0.8186(4) 0.060(3) Uani 1 1 d U . .
H16 H 0.7374 0.1759 0.8340 0.072 Uiso 1 1 calc R . .
N4 N 0.7062(2) 0.1934(5) 0.8343(3) 0.057(3) Uani 1 1 d U . .
C18 C 0.7231(2) 0.1878(3) 0.8744(4) 0.057(3) Uani 1 1 d DU . .
C19 C 0.7528(2) 0.1803(4) 0.8995(3) 0.060(3) Uani 1 1 d DU . .
H19 H 0.7630 0.1749 0.8905 0.072 Uiso 1 1 calc R . .
C20 C 0.7677(3) 0.1808(4) 0.9383(4) 0.067(4) Uani 1 1 d DU . .
H20 H 0.7883 0.1756 0.9556 0.080 Uiso 1 1 calc R . .
C21 C 0.7539(3) 0.1884(3) 0.9527(4) 0.084(5) Uani 1 1 d DU . .
C22 C 0.7239(3) 0.1959(4) 0.9271(4) 0.080(4) Uani 1 1 d DU . .
H22 H 0.7139 0.2012 0.9364 0.096 Uiso 1 1 calc R . .
C23 C 0.7084(3) 0.1958(4) 0.8885(4) 0.073(4) Uani 1 1 d DU . .
H23 H 0.6877 0.2010 0.8713 0.088 Uiso 1 1 calc R . .
O2 O 0.7665(2) 0.1896(5) 0.9905(3) 0.098(4) Uani 1 1 d DU . .
C24 C 0.7973(3) 0.1905(9) 1.0163(4) 0.104(6) Uani 1 1 d DU . .
H24A H 0.8046 0.1482 1.0185 0.155 Uiso 1 1 calc R . .
H24B H 0.8045 0.2045 1.0413 0.155 Uiso 1 1 calc R . .
H24C H 0.8041 0.2193 1.0069 0.155 Uiso 1 1 calc R . .
N31 N 0.6603(2) 0.0421(5) 0.7378(3) 0.059(3) Uani 1 1 d U . .
N32 N 0.6793(2) 0.0317(5) 0.7743(3) 0.058(3) Uani 1 1 d U . .
C32 C 0.7083(3) 0.0263(7) 0.7912(4) 0.067(4) Uani 1 1 d U . .
C33 C 0.7173(3) 0.0299(7) 0.7703(5) 0.083(5) Uani 1 1 d U . .
H33 H 0.7375 0.0279 0.7828 0.100 Uiso 1 1 calc R . .
C34 C 0.6971(4) 0.0362(8) 0.7320(5) 0.092(5) Uani 1 1 d U . .
H34 H 0.7022 0.0358 0.7165 0.111 Uiso 1 1 calc R . .
C35 C 0.6680(3) 0.0434(7) 0.7164(5) 0.071(4) Uani 1 1 d U . .
C36 C 0.6452(3) 0.0517(7) 0.6760(4) 0.071(4) Uani 1 1 d U . .
H36 H 0.6503 0.0594 0.6606 0.086 Uiso 1 1 calc R . .
N33 N 0.6184(3) 0.0489(5) 0.6601(3) 0.063(3) Uani 1 1 d U . .
C38 C 0.5947(3) 0.0547(3) 0.6193(4) 0.053(3) Uani 1 1 d DU . .
C39 C 0.5996(2) 0.0619(3) 0.5942(3) 0.049(3) Uani 1 1 d DU . .
H39 H 0.6189 0.0646 0.6032 0.059 Uiso 1 1 calc R . .
C40 C 0.5753(2) 0.0653(3) 0.5549(3) 0.055(3) Uani 1 1 d DU . .
H40 H 0.5782 0.0703 0.5371 0.066 Uiso 1 1 calc R . .
C41 C 0.5482(3) 0.0614(3) 0.5427(4) 0.080(4) Uani 1 1 d DU . .
C42 C 0.5437(3) 0.0542(4) 0.5684(4) 0.083(4) Uani 1 1 d DU . .
H42 H 0.5243 0.0516 0.5592 0.099 Uiso 1 1 calc R . .
C43 C 0.5663(3) 0.0508(4) 0.6058(4) 0.055(3) Uani 1 1 d DU . .
H43 H 0.5630 0.0458 0.6232 0.066 Uiso 1 1 calc R . .
O31 O 0.5233(2) 0.0643(5) 0.5045(3) 0.095(3) Uani 1 1 d DU . .
C44 C 0.5278(4) 0.0572(10) 0.4788(4) 0.110(6) Uani 1 1 d DU . .
H44A H 0.5355 0.0963 0.4773 0.165 Uiso 1 1 calc R . .
H44B H 0.5092 0.0469 0.4536 0.165 Uiso 1 1 calc R . .
H44C H 0.5418 0.0233 0.4874 0.165 Uiso 1 1 calc R . .
C46 C 0.7307(3) 0.0199(6) 0.8353(4) 0.066(4) Uani 1 1 d U . .
H46 H 0.7508 0.0121 0.8485 0.080 Uiso 1 1 calc R . .
N34 N 0.7211(2) 0.0254(5) 0.8536(3) 0.060(3) Uani 1 1 d U . .
C48 C 0.7412(3) 0.0230(3) 0.8936(4) 0.065(4) Uani 1 1 d DU . .
C49 C 0.7708(3) 0.0222(4) 0.9151(4) 0.082(4) Uani 1 1 d DU . .
H49 H 0.7787 0.0243 0.9029 0.098 Uiso 1 1 calc R . .
C50 C 0.7893(4) 0.0183(4) 0.9545(4) 0.092(5) Uani 1 1 d DU . .
H50 H 0.8099 0.0178 0.9693 0.110 Uiso 1 1 calc R . .
C51 C 0.7778(3) 0.0153(4) 0.9717(4) 0.088(5) Uani 1 1 d DU . .
C52 C 0.7481(4) 0.0160(5) 0.9514(5) 0.108(6) Uani 1 1 d DU . .
H52 H 0.7402 0.0139 0.9636 0.129 Uiso 1 1 calc R . .
C53 C 0.7301(4) 0.0199(5) 0.9113(5) 0.087(5) Uani 1 1 d DU . .
H53 H 0.7095 0.0204 0.8963 0.105 Uiso 1 1 calc R . .
O32 O 0.7999(3) 0.0116(6) 1.0115(4) 0.140(5) Uani 1 1 d DU . .
C54 C 0.7913(5) 0.0188(12) 1.0308(5) 0.147(9) Uani 1 1 d DU . .
H54A H 0.8081 0.0162 1.0582 0.220 Uiso 1 1 calc R . .
H54B H 0.7772 -0.0142 1.0238 0.220 Uiso 1 1 calc R . .
H54C H 0.7819 0.0599 1.0250 0.220 Uiso 1 1 calc R . .
N61 N 0.5746(2) 0.1638(6) 0.6910(3) 0.059(3) Uani 1 1 d U . .
N62 N 0.5790(2) 0.1028(5) 0.7001(3) 0.046(2) Uani 1 1 d U . .
C62 C 0.5636(3) 0.0749(7) 0.7078(4) 0.068(4) Uani 1 1 d U . .
C63 C 0.5425(3) 0.1110(7) 0.7051(4) 0.068(4) Uani 1 1 d U . .
H63 H 0.5314 0.0926 0.7107 0.081 Uiso 1 1 calc R . .
C64 C 0.5385(4) 0.1727(8) 0.6945(5) 0.080(4) Uani 1 1 d U . .
H64 H 0.5239 0.1969 0.6914 0.096 Uiso 1 1 calc R . .
C65 C 0.5550(3) 0.1978(7) 0.6886(4) 0.051(3) Uani 1 1 d U . .
C66 C 0.5545(3) 0.2632(7) 0.6804(4) 0.056(3) Uani 1 1 d U . .
H66 H 0.5414 0.2906 0.6789 0.067 Uiso 1 1 calc R . .
N63 N 0.5707(2) 0.2846(5) 0.6752(3) 0.047(3) Uani 1 1 d U . .
C68 C 0.5697(2) 0.3501(6) 0.6654(3) 0.063(3) Uani 1 1 d DU . .
C76 C 0.5684(3) 0.0083(7) 0.7167(4) 0.065(4) Uani 1 1 d U . .
H76 H 0.5577 -0.0126 0.7224 0.078 Uiso 1 1 calc R . .
N64 N 0.5860(3) -0.0216(6) 0.7171(3) 0.059(3) Uani 1 1 d U . .
C78 C 0.5917(3) -0.0861(6) 0.7258(3) 0.066(4) Uani 1 1 d DU . .
C79 C 0.6164(3) -0.1091(7) 0.7338(3) 0.091(5) Uani 1 1 d DU . .
H79 H 0.6288 -0.0820 0.7336 0.109 Uiso 1 1 calc R . .
C80 C 0.6233(4) -0.1729(7) 0.7424(3) 0.094(5) Uani 1 1 d DU . .
H80 H 0.6403 -0.1893 0.7480 0.112 Uiso 1 1 calc R . .
C81 C 0.6053(3) -0.2115(6) 0.7427(2) 0.092(5) Uani 1 1 d DU . .
C82 C 0.5806(4) -0.1874(7) 0.7346(3) 0.110(6) Uani 1 1 d DU . .
H82 H 0.5682 -0.2144 0.7348 0.133 Uiso 1 1 calc R . .
C83 C 0.5735(4) -0.1242(7) 0.7260(3) 0.097(5) Uani 1 1 d DU . .
H83 H 0.5564 -0.1079 0.7204 0.117 Uiso 1 1 calc R . .
O62 O 0.6135(4) -0.2734(6) 0.7513(3) 0.150(6) Uani 1 1 d DU . .
C84 C 0.6004(6) -0.3059(11) 0.7628(8) 0.209(13) Uani 1 1 d DU . .
H84A H 0.6043 -0.2842 0.7844 0.314 Uiso 1 1 calc R . .
H84B H 0.6083 -0.3485 0.7704 0.314 Uiso 1 1 calc R . .
H84C H 0.5792 -0.3077 0.7415 0.314 Uiso 1 1 calc R . .
N91 N 0.6280(2) 0.1455(5) 0.7982(3) 0.053(3) Uani 1 1 d U . .
N92 N 0.6333(2) 0.0842(5) 0.8069(3) 0.050(3) Uani 1 1 d U . .
C92 C 0.6162(3) 0.0509(8) 0.8107(4) 0.072(4) Uani 1 1 d U . .
C93 C 0.5949(4) 0.0764(8) 0.8082(5) 0.084(4) Uani 1 1 d U . .
H93 H 0.5837 0.0522 0.8119 0.100 Uiso 1 1 calc R . .
C94 C 0.5895(3) 0.1416(9) 0.7996(5) 0.091(5) Uani 1 1 d U . .
H94 H 0.5746 0.1632 0.7971 0.109 Uiso 1 1 calc R . .
C95 C 0.6078(3) 0.1715(6) 0.7953(4) 0.055(3) Uani 1 1 d U . .
C96 C 0.6041(3) 0.2393(7) 0.7866(4) 0.069(4) Uani 1 1 d U . .
H96 H 0.5892 0.2617 0.7838 0.083 Uiso 1 1 calc R . .
N93 N 0.6210(2) 0.2687(6) 0.7827(3) 0.055(3) Uani 1 1 d U . .
C98 C 0.6172(2) 0.3333(7) 0.7738(3) 0.063(3) Uani 1 1 d DU . .
C99 C 0.6022(2) 0.3749(7) 0.7788(3) 0.085(5) Uani 1 1 d DU . .
H99 H 0.5927 0.3608 0.7878 0.102 Uiso 1 1 calc R . .
C100 C 0.6015(3) 0.4363(8) 0.7705(3) 0.107(6) Uani 1 1 d DU . .
H100 H 0.5912 0.4645 0.7740 0.128 Uiso 1 1 calc R . .
C101 C 0.6145(2) 0.4598(7) 0.7576(2) 0.092(5) Uani 1 1 d DU . .
C102 C 0.6294(3) 0.4206(7) 0.7523(3) 0.083(4) Uani 1 1 d DU . .
H102 H 0.6388 0.4357 0.7433 0.100 Uiso 1 1 calc R . .
C103 C 0.6304(3) 0.3580(7) 0.7606(3) 0.077(4) Uani 1 1 d DU . .
H103 H 0.6408 0.3302 0.7570 0.093 Uiso 1 1 calc R . .
O91 O 0.6120(2) 0.5238(5) 0.7503(3) 0.110(4) Uani 1 1 d DU . .
C104 C 0.6253(5) 0.5428(9) 0.7353(7) 0.160(9) Uani 1 1 d DU . .
H90A H 0.6117 0.5695 0.7129 0.240 Uiso 1 1 calc R . .
H90B H 0.6302 0.5057 0.7279 0.240 Uiso 1 1 calc R . .
H90C H 0.6431 0.5664 0.7548 0.240 Uiso 1 1 calc R . .
C106 C 0.6235(3) -0.0168(7) 0.8199(4) 0.058(3) Uani 1 1 d U . .
H106 H 0.6122 -0.0430 0.8226 0.070 Uiso 1 1 calc R . .
N94 N 0.6451(2) -0.0394(5) 0.8242(3) 0.059(3) Uani 1 1 d U . .
C108 C 0.6529(3) -0.1036(6) 0.8328(3) 0.073(4) Uani 1 1 d DU . .
C109 C 0.6756(3) -0.1216(8) 0.8336(4) 0.127(7) Uani 1 1 d DU . .
H109 H 0.6853 -0.0916 0.8300 0.153 Uiso 1 1 calc R . .
C110 C 0.6837(4) -0.1845(9) 0.8398(4) 0.171(8) Uani 1 1 d DU . .
H110 H 0.6991 -0.1963 0.8403 0.206 Uiso 1 1 calc R . .
C111 C 0.6709(4) -0.2300(8) 0.8451(3) 0.158(8) Uani 1 1 d DU . .
C112 C 0.6488(4) -0.2111(7) 0.8442(3) 0.116(6) Uani 1 1 d DU . .
H112 H 0.6392 -0.2414 0.8479 0.139 Uiso 1 1 calc R . .
C113 C 0.6400(3) -0.1503(7) 0.8382(3) 0.094(5) Uani 1 1 d DU . .
H113 H 0.6245 -0.1395 0.8377 0.113 Uiso 1 1 calc R . .
O92 O 0.6786(4) -0.2927(7) 0.8513(5) 0.278(13) Uani 1 1 d DU . .
C114 C 0.7079(6) -0.3047(17) 0.8738(13) 0.33(3) Uani 1 1 d DU . .
H91A H 0.7110 -0.3501 0.8755 0.500 Uiso 1 1 calc R . .
H91B H 0.7181 -0.2876 0.8994 0.500 Uiso 1 1 calc R . .
H91C H 0.7155 -0.2850 0.8626 0.500 Uiso 1 1 calc R . .
Ag5 Ag 0.86578(3) 0.43260(6) 0.93420(4) 0.0820(4) Uani 1 1 d . . .
Ag6 Ag 0.87148(3) 0.25330(6) 0.92296(3) 0.0836(4) Uani 1 1 d . . .
Ag7 Ag 0.79766(3) 0.50001(7) 0.92500(4) 0.0991(5) Uani 1 1 d . . .
Ag8 Ag 0.81323(3) 0.31547(6) 0.93350(4) 0.0894(4) Uani 1 1 d . . .
N121 N 0.8961(2) 0.3597(5) 0.9852(3) 0.058(3) Uani 1 1 d U . .
N122 N 0.8966(3) 0.2979(6) 0.9798(3) 0.067(3) Uani 1 1 d U . .
C122 C 0.9139(3) 0.2610(7) 1.0096(4) 0.064(4) Uani 1 1 d U . .
C123 C 0.9312(3) 0.2856(8) 1.0474(4) 0.075(4) Uani 1 1 d U . .
H123 H 0.9432 0.2586 1.0688 0.089 Uiso 1 1 calc R . .
C124 C 0.9303(3) 0.3476(8) 1.0522(4) 0.072(4) Uani 1 1 d U . .
H124 H 0.9413 0.3648 1.0771 0.087 Uiso 1 1 calc R . .
C125 C 0.9128(3) 0.3869(7) 1.0197(4) 0.062(3) Uani 1 1 d U . .
C126 C 0.9095(3) 0.4511(8) 1.0215(5) 0.065(4) Uani 1 1 d U . .
H126 H 0.9197 0.4697 1.0459 0.078 Uiso 1 1 calc R . .
N123 N 0.8931(3) 0.4867(6) 0.9914(4) 0.068(3) Uani 1 1 d U . .
C128 C 0.88908(14) 0.5512(7) 0.9932(3) 0.065(4) Uani 1 1 d DU . .
C129 C 0.90516(19) 0.5857(6) 1.0267(3) 0.079(4) Uani 1 1 d DU . .
H129 H 0.9194 0.5664 1.0508 0.095 Uiso 1 1 calc R . .
C130 C 0.8997(3) 0.6489(7) 1.0237(5) 0.105(6) Uani 1 1 d DU . .
H130 H 0.9107 0.6728 1.0466 0.126 Uiso 1 1 calc R . .
C131 C 0.8799(3) 0.6788(7) 0.9905(4) 0.092(5) Uani 1 1 d DU . .
C132 C 0.8642(3) 0.6430(7) 0.9575(5) 0.082(4) Uani 1 1 d DU . .
H132 H 0.8499 0.6618 0.9333 0.098 Uiso 1 1 calc R . .
C133 C 0.8696(3) 0.5811(7) 0.9605(4) 0.072(4) Uani 1 1 d DU . .
H133 H 0.8586 0.5572 0.9377 0.086 Uiso 1 1 calc R . .
O121 O 0.8776(3) 0.7426(6) 0.9934(4) 0.134(5) Uani 1 1 d DU . .
C134 C 0.8552(5) 0.7724(9) 0.9578(6) 0.153(9) Uani 1 1 d DU . .
H13A H 0.8366 0.7510 0.9453 0.230 Uiso 1 1 calc R . .
H13B H 0.8601 0.7703 0.9414 0.230 Uiso 1 1 calc R . .
H13C H 0.8535 0.8164 0.9623 0.230 Uiso 1 1 calc R . .
C136 C 0.9148(3) 0.1950(7) 1.0035(4) 0.057(3) Uani 1 1 d U . .
H136 H 0.9268 0.1672 1.0246 0.068 Uiso 1 1 calc R . .
N124 N 0.8993(2) 0.1749(5) 0.9696(4) 0.064(3) Uani 1 1 d U . .
C138 C 0.90111(14) 0.1125(6) 0.9595(3) 0.074(4) Uani 1 1 d DU . .
C139 C 0.9198(2) 0.0675(7) 0.9857(4) 0.106(6) Uani 1 1 d DU . .
H139 H 0.9332 0.0779 1.0121 0.127 Uiso 1 1 calc R . .
C140 C 0.9196(3) 0.0072(7) 0.9745(5) 0.115(6) Uani 1 1 d DU . .
H140 H 0.9324 -0.0245 0.9923 0.138 Uiso 1 1 calc R . .
C141 C 0.8997(3) -0.0042(7) 0.9361(5) 0.112(6) Uani 1 1 d DU . .
C142 C 0.8805(3) 0.0394(8) 0.9087(6) 0.133(7) Uani 1 1 d DU . .
H142 H 0.8671 0.0290 0.8823 0.160 Uiso 1 1 calc R . .
C143 C 0.8816(3) 0.1001(8) 0.9216(5) 0.109(6) Uani 1 1 d DU . .
H143 H 0.8689 0.1320 0.9040 0.131 Uiso 1 1 calc R . .
O122 O 0.8963(4) -0.0630(7) 0.9194(4) 0.169(6) Uani 1 1 d DU . .
C144 C 0.9144(7) -0.1085(10) 0.9447(8) 0.215(13) Uani 1 1 d DU . .
H14D H 0.9137 -0.1096 0.9653 0.323 Uiso 1 1 calc R . .
H14E H 0.9344 -0.0997 0.9555 0.323 Uiso 1 1 calc R . .
H14F H 0.9082 -0.1492 0.9317 0.323 Uiso 1 1 calc R . .
N151 N 0.8325(2) 0.4503(6) 0.9827(3) 0.062(3) Uani 1 1 d U . .
N152 N 0.8372(2) 0.3889(6) 0.9848(3) 0.070(3) Uani 1 1 d U . .
C153 C 0.8719(3) 0.3996(8) 1.0520(5) 0.077(4) Uani 1 1 d U . .
H15A H 0.8855 0.3806 1.0763 0.092 Uiso 1 1 calc R . .
C155 C 0.8470(3) 0.4871(8) 1.0127(4) 0.064(4) Uani 1 1 d U . .
C156 C 0.8391(4) 0.5545(8) 1.0051(5) 0.078(4) Uani 1 1 d U . .
H156 H 0.8498 0.5832 1.0258 0.094 Uiso 1 1 calc R . .
N153 N 0.8189(3) 0.5749(7) 0.9725(4) 0.081(4) Uani 1 1 d U . .
C158 C 0.81130(14) 0.6375(8) 0.9662(4) 0.095(5) Uani 1 1 d DU . .
C159 C 0.8206(2) 0.6833(9) 0.9938(5) 0.138(7) Uani 1 1 d DU . .
H15B H 0.8344 0.6734 1.0202 0.166 Uiso 1 1 calc R . .
C160 C 0.8090(4) 0.7450(10) 0.9817(7) 0.180(10) Uani 1 1 d DU . .
H16A H 0.8150 0.7766 1.0000 0.216 Uiso 1 1 calc R . .
C161 C 0.7884(4) 0.7594(11) 0.9424(7) 0.184(10) Uani 1 1 d DU . .
C162 C 0.7787(4) 0.7161(9) 0.9144(7) 0.150(8) Uani 1 1 d DU . .
H16B H 0.7649 0.7260 0.8880 0.180 Uiso 1 1 calc R . .
C163 C 0.7907(3) 0.6564(9) 0.9278(5) 0.112(5) Uani 1 1 d DU . .
H16C H 0.7844 0.6253 0.9090 0.134 Uiso 1 1 calc R . .
N154 N 0.8468(2) 0.2612(6) 0.9903(4) 0.064(3) Uani 1 1 d U . .
C168 C 0.85072(10) 0.1980(7) 0.9914(3) 0.072(4) Uani 1 1 d DU . .
C169 C 0.86824(7) 0.1625(7) 1.0240(3) 0.099(5) Uani 1 1 d DU . .
H169 H 0.8777 0.1821 1.0480 0.119 Uiso 1 1 calc R . .
C170 C 0.8725(3) 0.1000(7) 1.0232(5) 0.100(5) Uani 1 1 d DU . .
H170 H 0.8847 0.0764 1.0462 0.120 Uiso 1 1 calc R . .
C171 C 0.8592(2) 0.0731(6) 0.9898(4) 0.091(5) Uani 1 1 d DU . .
C172 C 0.8409(2) 0.1029(6) 0.9544(4) 0.077(4) Uani 1 1 d DU . .
H172 H 0.8316 0.0826 0.9307 0.093 Uiso 1 1 calc R . .
C173 C 0.8381(2) 0.1649(6) 0.9583(4) 0.079(4) Uani 1 1 d DU . .
H173 H 0.8259 0.1883 0.9353 0.095 Uiso 1 1 calc R . .
O152 O 0.8645(3) 0.0091(6) 0.9922(4) 0.120(5) Uani 1 1 d DU . .
C174 C 0.8519(5) -0.0225(8) 0.9593(6) 0.125(7) Uani 1 1 d DU . .
H17A H 0.8308 -0.0249 0.9446 0.188 Uiso 1 1 calc R . .
H17B H 0.8601 -0.0649 0.9652 0.188 Uiso 1 1 calc R . .
H17C H 0.8558 -0.0004 0.9444 0.188 Uiso 1 1 calc R . .
N181 N 0.8168(3) 0.4433(5) 0.8784(4) 0.081(4) Uani 1 1 d U . .
N182 N 0.7954(3) 0.4608(5) 0.8755(4) 0.085(4) Uani 1 1 d U . .
C182 C 0.7672(4) 0.4645(7) 0.8419(5) 0.089(5) Uani 1 1 d U . .
C183 C 0.7626(4) 0.4538(8) 0.8095(6) 0.107(6) Uani 1 1 d U . .
H183 H 0.7433 0.4553 0.7856 0.129 Uiso 1 1 calc R . .
C184 C 0.7854(4) 0.4407(7) 0.8102(5) 0.091(4) Uani 1 1 d U . .
H184 H 0.7825 0.4358 0.7874 0.109 Uiso 1 1 calc R . .
C185 C 0.8130(3) 0.4351(7) 0.8462(5) 0.086(5) Uani 1 1 d U . .
C186 C 0.8374(3) 0.4183(7) 0.8493(4) 0.083(4) Uani 1 1 d U . .
H186 H 0.8342 0.4081 0.8268 0.100 Uiso 1 1 calc R . .
N183 N 0.8640(3) 0.4167(5) 0.8821(4) 0.073(3) Uani 1 1 d U . .
C188 C 0.8881(3) 0.4037(4) 0.8865(3) 0.065(3) Uani 1 1 d DU . .
C189 C 0.8873(3) 0.3895(4) 0.8557(4) 0.069(4) Uani 1 1 d DU . .
H189 H 0.8690 0.3865 0.8306 0.082 Uiso 1 1 calc R . .
C190 C 0.9126(3) 0.3801(4) 0.8619(3) 0.068(4) Uani 1 1 d DU . .
H190 H 0.9115 0.3707 0.8409 0.082 Uiso 1 1 calc R . .
C191 C 0.9399(3) 0.3841(3) 0.8984(3) 0.065(4) Uani 1 1 d DU . .
C192 C 0.9401(3) 0.3983(4) 0.9284(4) 0.067(4) Uani 1 1 d DU . .
H192 H 0.9583 0.4014 0.9536 0.080 Uiso 1 1 calc R . .
C193 C 0.9150(3) 0.4077(4) 0.9224(4) 0.067(4) Uani 1 1 d DU . .
H193 H 0.9161 0.4171 0.9435 0.081 Uiso 1 1 calc R . .
O181 O 0.9666(2) 0.3756(4) 0.9076(3) 0.084(3) Uani 1 1 d DU . .
C194 C 0.9664(4) 0.3720(9) 0.8770(4) 0.099(6) Uani 1 1 d DU . .
H19A H 0.9541 0.3368 0.8604 0.149 Uiso 1 1 calc R . .
H19B H 0.9864 0.3655 0.8869 0.149 Uiso 1 1 calc R . .
H19C H 0.9586 0.4111 0.8623 0.149 Uiso 1 1 calc R . .
C196 C 0.7454(3) 0.4847(7) 0.8427(5) 0.085(5) Uani 1 1 d U . .
H196 H 0.7262 0.4883 0.8188 0.102 Uiso 1 1 calc R . .
N184 N 0.7486(3) 0.4982(6) 0.8710(4) 0.081(4) Uani 1 1 d U . .
C198 C 0.7266(3) 0.5155(5) 0.8705(4) 0.089(5) Uani 1 1 d DU . .
C199 C 0.6973(3) 0.5154(5) 0.8392(5) 0.095(5) Uani 1 1 d DU . .
H199 H 0.6912 0.5031 0.8151 0.114 Uiso 1 1 calc R . .
C200 C 0.6763(4) 0.5327(5) 0.8415(5) 0.102(5) Uani 1 1 d DU . .
H200 H 0.6562 0.5321 0.8192 0.122 Uiso 1 1 calc R . .
C201 C 0.6843(3) 0.5504(5) 0.8754(5) 0.110(6) Uani 1 1 d DU . .
C202 C 0.7142(4) 0.5503(7) 0.9069(6) 0.166(8) Uani 1 1 d DU . .
H202 H 0.7204 0.5626 0.9310 0.199 Uiso 1 1 calc R . .
C203 C 0.7351(5) 0.5331(7) 0.9047(5) 0.132(7) Uani 1 1 d DU . .
H203 H 0.7552 0.5336 0.9268 0.158 Uiso 1 1 calc R . .
O182 O 0.6667(3) 0.5686(7) 0.8824(4) 0.145(6) Uani 1 1 d DU . .
C204 C 0.6371(3) 0.5783(10) 0.8505(5) 0.124(7) Uani 1 1 d DU . .
H20A H 0.6356 0.6017 0.8310 0.186 Uiso 1 1 calc R . .
H20B H 0.6278 0.6023 0.8581 0.186 Uiso 1 1 calc R . .
H20C H 0.6273 0.5377 0.8401 0.186 Uiso 1 1 calc R . .
N211 N 0.8239(3) 0.2806(6) 0.8740(4) 0.092(4) Uani 1 1 d U . .
N212 N 0.8045(3) 0.2957(5) 0.8769(3) 0.078(4) Uani 1 1 d U . .
C212 C 0.7759(4) 0.3018(7) 0.8474(4) 0.085(4) Uani 1 1 d U . .
C213 C 0.7662(4) 0.2938(8) 0.8090(4) 0.102(5) Uani 1 1 d U . .
H213 H 0.7463 0.3001 0.7871 0.122 Uiso 1 1 calc R . .
C214 C 0.7870(4) 0.2764(8) 0.8047(5) 0.112(6) Uani 1 1 d U . .
H214 H 0.7815 0.2691 0.7805 0.135 Uiso 1 1 calc R . .
C215 C 0.8159(4) 0.2710(8) 0.8391(5) 0.096(5) Uani 1 1 d U . .
C216 C 0.8373(4) 0.2535(7) 0.8376(5) 0.090(5) Uani 1 1 d U . .
H216 H 0.8316 0.2443 0.8134 0.108 Uiso 1 1 calc R . .
N213 N 0.8647(3) 0.2490(5) 0.8677(3) 0.069(3) Uani 1 1 d U . .
C218 C 0.8877(3) 0.2353(4) 0.8681(4) 0.082(4) Uani 1 1 d DU . .
C219 C 0.8845(4) 0.2239(5) 0.8359(5) 0.093(5) Uani 1 1 d DU . .
H219 H 0.8655 0.2272 0.8116 0.111 Uiso 1 1 calc R . .
C220 C 0.9073(3) 0.2082(5) 0.8374(4) 0.082(4) Uani 1 1 d DU . .
H220 H 0.9046 0.2006 0.8150 0.099 Uiso 1 1 calc R . .
C221 C 0.9342(3) 0.2043(4) 0.8733(4) 0.087(4) Uani 1 1 d DU . .
O211 O 0.9584(3) 0.1892(5) 0.8790(3) 0.100(4) Uani 1 1 d DU . .
C222 C 0.9380(4) 0.2153(5) 0.9056(5) 0.107(6) Uani 1 1 d DU . .
H222 H 0.9569 0.2121 0.9301 0.128 Uiso 1 1 calc R . .
C223 C 0.9148(3) 0.2305(5) 0.9023(4) 0.090(5) Uani 1 1 d DU . .
H223 H 0.9175 0.2381 0.9248 0.108 Uiso 1 1 calc R . .
O212 O 0.6888(2) 0.3794(5) 0.9115(3) 0.106(4) Uani 1 1 d DU . .
C224 C 0.9546(4) 0.1758(9) 0.8461(5) 0.119(7) Uani 1 1 d DU . .
H22A H 0.9386 0.1455 0.8302 0.179 Uiso 1 1 calc R . .
H22B H 0.9726 0.1581 0.8535 0.179 Uiso 1 1 calc R . .
H22C H 0.9497 0.2145 0.8315 0.179 Uiso 1 1 calc R . .
C226 C 0.7553(3) 0.3183(7) 0.8508(5) 0.085(4) Uani 1 1 d U . .
H226 H 0.7353 0.3232 0.8287 0.101 Uiso 1 1 calc R . .
N214 N 0.7632(3) 0.3268(5) 0.8836(4) 0.082(4) Uani 1 1 d U . .
C228 C 0.7434(3) 0.3406(4) 0.8872(4) 0.075(4) Uani 1 1 d DU . .
C229 C 0.7131(3) 0.3505(4) 0.8576(4) 0.079(4) Uani 1 1 d DU . .
H229 H 0.7052 0.3482 0.8319 0.094 Uiso 1 1 calc R . .
C230 C 0.6951(4) 0.3631(4) 0.8649(4) 0.085(5) Uani 1 1 d DU . .
H230 H 0.6749 0.3693 0.8441 0.102 Uiso 1 1 calc R . .
C231 C 0.7052(3) 0.3671(3) 0.9013(4) 0.087(5) Uani 1 1 d DU . .
C232 C 0.7353(3) 0.3574(4) 0.9317(5) 0.096(5) Uani 1 1 d DU . .
H232 H 0.7431 0.3596 0.9574 0.115 Uiso 1 1 calc R . .
C233 C 0.7529(3) 0.3449(5) 0.9237(4) 0.072(4) Uani 1 1 d DU . .
H233 H 0.7731 0.3387 0.9446 0.086 Uiso 1 1 calc R . .
C234 C 0.6588(3) 0.3877(10) 0.8819(5) 0.119(7) Uani 1 1 d DU . .
H23A H 0.6556 0.4218 0.8652 0.179 Uiso 1 1 calc R . .
H23B H 0.6496 0.3983 0.8925 0.179 Uiso 1 1 calc R . .
H23C H 0.6503 0.3488 0.8670 0.179 Uiso 1 1 calc R . .
B1 B 0.7918(3) 0.1142(8) 0.8457(5) 0.116(8) Uani 1 1 d DU . .
F11 F 0.81701(17) 0.1319(4) 0.8526(3) 0.104(3) Uani 1 1 d DU . .
F12 F 0.7861(2) 0.1565(5) 0.8630(3) 0.111(3) Uani 1 1 d DU . .
F13 F 0.7951(2) 0.0552(5) 0.8593(3) 0.123(4) Uani 1 1 d DU . .
F14 F 0.7690(2) 0.1168(6) 0.8064(3) 0.170(6) Uani 1 1 d DU . .
B2 B 0.6958(3) 0.1149(7) 0.6510(4) 0.083(5) Uani 1 1 d DU . .
F21 F 0.6860(2) 0.1767(4) 0.6426(3) 0.104(3) Uani 1 1 d DU . .
F22 F 0.6721(2) 0.0754(4) 0.6362(3) 0.107(3) Uani 1 1 d DU . .
F23 F 0.7160(2) 0.1063(5) 0.6899(3) 0.127(4) Uani 1 1 d DU . .
F24 F 0.7074(2) 0.1008(4) 0.6342(3) 0.110(3) Uani 1 1 d DU . .
B3 B 0.6955(3) 0.8596(7) 0.7581(5) 0.093(6) Uani 1 1 d DU . .
F31 F 0.6729(2) 0.9014(4) 0.7368(3) 0.119(4) Uani 1 1 d DU . .
F32 F 0.6859(2) 0.7978(4) 0.7523(3) 0.128(4) Uani 1 1 d DU . .
F33 F 0.7111(3) 0.8750(6) 0.7954(3) 0.177(6) Uani 1 1 d DU . .
F34 F 0.7123(3) 0.8646(6) 0.7480(5) 0.208(7) Uani 1 1 d DU . .
B4 B 0.6852(3) 0.3753(7) 0.7415(4) 0.088(6) Uani 1 1 d DU . .
F41 F 0.6891(2) 0.3341(5) 0.7673(3) 0.116(3) Uani 1 1 d DU . .
F42 F 0.6851(3) 0.4360(5) 0.7509(4) 0.137(4) Uani 1 1 d DU . .
F43 F 0.7068(2) 0.3676(5) 0.7397(3) 0.135(4) Uani 1 1 d DU . .
F44 F 0.6583(2) 0.3615(6) 0.7061(3) 0.145(5) Uani 1 1 d DU . .
B5 B 0.4967(3) 0.0152(8) 0.6187(5) 0.106(7) Uani 1 1 d DU . .
F51 F 0.4744(2) -0.0219(5) 0.5893(3) 0.130(4) Uani 1 1 d DU . .
F52 F 0.5186(2) 0.0233(6) 0.6177(3) 0.136(4) Uani 1 1 d DU . .
F53 F 0.5082(2) -0.0182(5) 0.6522(3) 0.131(4) Uani 1 1 d DU . .
F54 F 0.4868(2) 0.0721(5) 0.6213(3) 0.127(4) Uani 1 1 d DU . .
B6 B 0.6276(4) 0.2355(9) 0.8824(5) 0.153(12) Uani 1 1 d DU . .
F61 F 0.6372(2) 0.2682(6) 0.9138(3) 0.135(4) Uani 1 1 d DU . .
F62 F 0.6499(2) 0.2251(6) 0.8810(3) 0.149(5) Uani 1 1 d DU . .
F63 F 0.6062(3) 0.2711(6) 0.8504(3) 0.175(6) Uani 1 1 d DU . .
F64 F 0.6148(3) 0.1794(6) 0.8794(4) 0.173(6) Uani 1 1 d DU . .
B7 B 0.4720(5) 0.3498(10) 0.6145(6) 0.215(18) Uani 1 1 d DU . .
F71 F 0.4430(3) 0.3488(8) 0.5949(5) 0.248(9) Uani 1 1 d DU . .
F72 F 0.4826(3) 0.2904(8) 0.6310(4) 0.222(7) Uani 1 1 d DU . .
F73 F 0.4746(6) 0.3665(11) 0.5885(7) 0.339(13) Uani 1 1 d DU . .
F74 F 0.4872(6) 0.3939(11) 0.6427(7) 0.45(2) Uani 1 1 d DU . .
C241 C 0.4772(3) 0.1649(6) 0.5292(5) 0.133(6) Uani 1 1 d GDU . .
H241 H 0.4732 0.1224 0.5212 0.160 Uiso 1 1 calc R . .
C242 C 0.4943(3) 0.1795(9) 0.5676(4) 0.158(8) Uani 1 1 d GDU . .
H242 H 0.5019 0.1468 0.5859 0.189 Uiso 1 1 calc R . .
C243 C 0.5002(3) 0.2417(11) 0.5794(4) 0.159(8) Uani 1 1 d GDU . .
H243 H 0.5118 0.2517 0.6057 0.191 Uiso 1 1 calc R . .
C244 C 0.4891(4) 0.2894(7) 0.5526(6) 0.189(10) Uani 1 1 d GDU . .
H244 H 0.4931 0.3320 0.5607 0.227 Uiso 1 1 calc R . .
C245 C 0.4720(3) 0.2749(6) 0.5142(5) 0.139(7) Uani 1 1 d GDU . .
H245 H 0.4645 0.3075 0.4959 0.167 Uiso 1 1 calc R . .
C246 C 0.4661(3) 0.2126(7) 0.5024(3) 0.102(5) Uani 1 1 d GDU . .
H246 H 0.4545 0.2027 0.4761 0.122 Uiso 1 1 calc R . .
C251 C 0.7142(3) 0.0353(9) 0.9954(4) 0.144(8) Uani 1 1 d GDU . .
H251 H 0.7292 0.0455 1.0216 0.173 Uiso 1 1 calc R . .
C252 C 0.6980(4) 0.0829(6) 0.9687(6) 0.140(7) Uani 1 1 d GDU . .
H252 H 0.7021 0.1255 0.9767 0.169 Uiso 1 1 calc R . .
C253 C 0.6760(3) 0.0680(9) 0.9304(5) 0.160(7) Uani 1 1 d GDU . .
H253 H 0.6650 0.1005 0.9122 0.192 Uiso 1 1 calc R . .
C254 C 0.6701(3) 0.0057(11) 0.9189(4) 0.157(8) Uani 1 1 d GDU . .
H254 H 0.6551 -0.0044 0.8927 0.189 Uiso 1 1 calc R . .
C255 C 0.6863(4) -0.0418(7) 0.9456(5) 0.153(7) Uani 1 1 d GDU . .
H255 H 0.6823 -0.0844 0.9377 0.184 Uiso 1 1 calc R . .
C256 C 0.7083(3) -0.0270(7) 0.9839(5) 0.134(7) Uani 1 1 d GDU . .
H256 H 0.7193 -0.0595 1.0021 0.161 Uiso 1 1 calc R . .
C261 C 0.5340(5) 0.3763(9) 0.4394(6) 0.189(10) Uani 1 1 d GDU . .
H26A H 0.5264 0.3406 0.4427 0.227 Uiso 1 1 calc R . .
C262 C 0.5166(3) 0.4291(11) 0.4208(6) 0.199(11) Uani 1 1 d GDU . .
H26B H 0.4971 0.4295 0.4114 0.238 Uiso 1 1 calc R . .
C263 C 0.5277(4) 0.4814(8) 0.4160(5) 0.191(10) Uani 1 1 d GDU . .
H26C H 0.5158 0.5174 0.4033 0.230 Uiso 1 1 calc R . .
C264 C 0.5562(5) 0.4808(8) 0.4298(5) 0.185(9) Uani 1 1 d GDU . .
H26D H 0.5637 0.5165 0.4265 0.222 Uiso 1 1 calc R . .
C265 C 0.5735(3) 0.4280(10) 0.4484(5) 0.174(9) Uani 1 1 d GDU . .
H26E H 0.5930 0.4277 0.4579 0.209 Uiso 1 1 calc R . .
C266 C 0.5624(4) 0.3758(8) 0.4532(5) 0.186(10) Uani 1 1 d GDU . .
H26F H 0.5743 0.3397 0.4659 0.224 Uiso 1 1 calc R . .
C154 C 0.8672(3) 0.4625(8) 1.0487(4) 0.069(4) Uani 1 1 d U . .
H15C H 0.8776 0.4886 1.0706 0.082 Uiso 1 1 calc R . .
O61 O 0.5685(3) 0.5342(6) 0.6350(4) 0.158(6) Uani 1 1 d DU . .
C73 C 0.5851(3) 0.3687(6) 0.6545(3) 0.078(4) Uani 1 1 d DU . .
H73A H 0.5963 0.3381 0.6540 0.094 Uiso 1 1 calc R . .
C71 C 0.5691(3) 0.4737(7) 0.6449(3) 0.116(6) Uani 1 1 d DU . .
O151 O 0.7750(5) 0.8208(13) 0.9265(8) 0.287(13) Uani 1 1 d DU . .
C72 C 0.5852(3) 0.4290(7) 0.6442(3) 0.109(5) Uani 1 1 d DU . .
H72A H 0.5962 0.4397 0.6368 0.131 Uiso 1 1 calc R . .
C74 C 0.5810(6) 0.5491(10) 0.6197(7) 0.149(9) Uani 1 1 d DU . .
H74A H 0.5785 0.5941 0.6139 0.224 Uiso 1 1 calc R . .
H74B H 0.5716 0.5251 0.5962 0.224 Uiso 1 1 calc R . .
H74C H 0.6019 0.5390 0.6380 0.224 Uiso 1 1 calc R . .
C152 C 0.8568(3) 0.3647(7) 1.0198(5) 0.068(4) Uani 1 1 d U . .
C69 C 0.5538(3) 0.3947(7) 0.6660(3) 0.085(5) Uani 1 1 d DU . .
H69A H 0.5428 0.3836 0.6734 0.102 Uiso 1 1 calc R . .
C70 C 0.5535(3) 0.4562(8) 0.6558(3) 0.127(7) Uani 1 1 d DU . .
H70A H 0.5423 0.4868 0.6563 0.153 Uiso 1 1 calc R . .
C166 C 0.8608(3) 0.2939(7) 1.0205(5) 0.067(4) Uani 1 1 d U . .
H16D H 0.8743 0.2735 1.0445 0.080 Uiso 1 1 calc R . .
C164 C 0.7767(12) 0.8523(18) 0.9545(13) 0.40(4) Uani 1 1 d DU . .
H16E H 0.7678 0.8939 0.9452 0.607 Uiso 1 1 calc R . .
H16F H 0.7972 0.8567 0.9777 0.607 Uiso 1 1 calc R . .
H16G H 0.7662 0.8282 0.9604 0.607 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Ag1 N63 135.0(4) . . y
N1 Ag1 N3 71.7(4) . . y
N63 Ag1 N3 126.4(4) . . y
N1 Ag1 N61 122.4(4) . . y
N63 Ag1 N61 69.8(4) . . y
N3 Ag1 N61 144.1(4) . . y
N2 Ag2 N93 129.9(4) . . y
N2 Ag2 N91 133.0(4) . . y
N93 Ag2 N91 72.0(4) . . y
N2 Ag2 N4 72.3(4) . . y
N93 Ag2 N4 142.2(4) . . y
N91 Ag2 N4 118.0(4) . . y
N62 Ag3 N31 131.6(4) . . y
N62 Ag3 N33 120.1(4) . . y
N31 Ag3 N33 72.3(4) . . y
N62 Ag3 N64 71.9(4) . . y
N31 Ag3 N64 127.4(4) . . y
N33 Ag3 N64 144.5(4) . . y
N92 Ag4 N32 124.7(4) . . y
N92 Ag4 N34 144.3(4) . . y
N32 Ag4 N34 73.7(4) . . y
N92 Ag4 N94 71.5(4) . . y
N32 Ag4 N94 131.8(4) . . y
N34 Ag4 N94 121.8(4) . . y
C5 N1 N2 122.1(10) . . ?
C5 N1 Ag1 115.5(9) . . ?
N2 N1 Ag1 122.4(8) . . ?
N1 N2 C2 115.4(11) . . ?
N1 N2 Ag2 126.9(8) . . ?
C2 N2 Ag2 117.6(9) . . ?
C3 C2 N2 122.1(13) . . ?
C3 C2 C16 123.9(13) . . ?
N2 C2 C16 113.8(13) . . ?
C2 C3 C4 121.8(14) . . ?
C2 C3 H3 119.1 . . ?
C4 C3 H3 119.1 . . ?
C5 C4 C3 115.1(15) . . ?
C5 C4 H4 122.4 . . ?
C3 C4 H4 122.4 . . ?
N1 C5 C4 122.9(14) . . ?
N1 C5 C6 116.7(12) . . ?
C4 C5 C6 120.3(14) . . ?
N3 C6 C5 121.8(14) . . ?
N3 C6 H6 119.1 . . ?
C5 C6 H6 119.1 . . ?
C6 N3 C8 121.1(12) . . ?
C6 N3 Ag1 114.1(10) . . ?
C8 N3 Ag1 124.7(8) . . ?
C13 C8 C9 119.3(13) . . ?
C13 C8 N3 116.6(12) . . ?
C9 C8 N3 124.1(12) . . ?
C8 C9 C10 121.5(15) . . ?
C8 C9 H9 119.3 . . ?
C10 C9 H9 119.3 . . ?
C11 C10 C9 118.7(15) . . ?
C11 C10 H10 120.6 . . ?
C9 C10 H10 120.6 . . ?
C10 C11 C12 119.5(14) . . ?
C10 C11 O1 113.3(14) . . ?
C12 C11 O1 127.2(14) . . ?
C11 C12 C13 121.7(15) . . ?
C11 C12 H12 119.2 . . ?
C13 C12 H12 119.2 . . ?
C8 C13 C12 119.3(14) . . ?
C8 C13 H13 120.4 . . ?
C12 C13 H13 120.4 . . ?
C14 O1 C11 114.5(16) . . ?
O1 C14 H14A 109.5 . . ?
O1 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
O1 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
N4 C16 C2 121.1(12) . . ?
N4 C16 H16 119.5 . . ?
C2 C16 H16 119.5 . . ?
C16 N4 C18 122.1(11) . . ?
C16 N4 Ag2 115.0(9) . . ?
C18 N4 Ag2 122.7(8) . . ?
C19 C18 C23 119.5(13) . . ?
C19 C18 N4 123.1(12) . . ?
C23 C18 N4 117.2(11) . . ?
C18 C19 C20 119.0(13) . . ?
C18 C19 H19 120.5 . . ?
C20 C19 H19 120.5 . . ?
C21 C20 C19 122.6(13) . . ?
C21 C20 H20 118.7 . . ?
C19 C20 H20 118.7 . . ?
C20 C21 O2 127.5(12) . . ?
C20 C21 C22 118.0(13) . . ?
O2 C21 C22 114.5(13) . . ?
C23 C22 C21 121.0(14) . . ?
C23 C22 H22 119.5 . . ?
C21 C22 H22 119.5 . . ?
C22 C23 C18 119.8(13) . . ?
C22 C23 H23 120.1 . . ?
C18 C23 H23 120.1 . . ?
C21 O2 C24 114.1(11) . . ?
O2 C24 H24A 109.5 . . ?
O2 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
O2 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
N32 N31 C35 121.5(12) . . ?
N32 N31 Ag3 122.9(8) . . ?
C35 N31 Ag3 114.1(9) . . ?
N31 N32 C32 118.0(11) . . ?
N31 N32 Ag4 126.7(9) . . ?
C32 N32 Ag4 115.0(9) . . ?
N32 C32 C33 122.0(13) . . ?
N32 C32 C46 116.7(13) . . ?
C33 C32 C46 121.2(13) . . ?
C34 C33 C32 119.3(14) . . ?
C34 C33 H33 120.4 . . ?
C32 C33 H33 120.4 . . ?
C33 C34 C35 116.4(16) . . ?
C33 C34 H34 121.8 . . ?
C35 C34 H34 121.8 . . ?
N31 C35 C34 122.5(15) . . ?
N31 C35 C36 117.4(13) . . ?
C34 C35 C36 120.0(14) . . ?
N33 C36 C35 121.7(13) . . ?
N33 C36 H36 119.2 . . ?
C35 C36 H36 119.2 . . ?
C36 N33 C38 123.3(12) . . ?
C36 N33 Ag3 113.8(10) . . ?
C38 N33 Ag3 122.9(9) . . ?
C39 C38 C43 120.2(12) . . ?
C39 C38 N33 122.5(11) . . ?
C43 C38 N33 117.3(11) . . ?
C38 C39 C40 118.6(11) . . ?
C38 C39 H39 120.7 . . ?
C40 C39 H39 120.7 . . ?
C41 C40 C39 119.8(12) . . ?
C41 C40 H40 120.1 . . ?
C39 C40 H40 120.1 . . ?
C40 C41 O31 123.1(12) . . ?
C40 C41 C42 120.8(12) . . ?
O31 C41 C42 116.1(13) . . ?
C43 C42 C41 120.7(13) . . ?
C43 C42 H42 119.7 . . ?
C41 C42 H42 119.7 . . ?
C42 C43 C38 119.8(12) . . ?
C42 C43 H43 120.1 . . ?
C38 C43 H43 120.1 . . ?
C44 O31 C41 115.6(11) . . ?
O31 C44 H44A 109.5 . . ?
O31 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
O31 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
N34 C46 C32 117.9(13) . . ?
N34 C46 H46 121.1 . . ?
C32 C46 H46 121.1 . . ?
C46 N34 C48 119.0(11) . . ?
C46 N34 Ag4 116.2(10) . . ?
C48 N34 Ag4 124.6(9) . . ?
C53 C48 C49 119.1(14) . . ?
C53 C48 N34 117.1(13) . . ?
C49 C48 N34 123.7(13) . . ?
C48 C49 C50 120.8(14) . . ?
C48 C49 H49 119.6 . . ?
C50 C49 H49 119.6 . . ?
C51 C50 C49 119.2(15) . . ?
C51 C50 H50 120.4 . . ?
C49 C50 H50 120.4 . . ?
C50 C51 C52 122.3(15) . . ?
C50 C51 O32 110.9(14) . . ?
C52 C51 O32 126.8(14) . . ?
C51 C52 C53 116.4(16) . . ?
C51 C52 H52 121.8 . . ?
C53 C52 H52 121.8 . . ?
C48 C53 C52 122.1(16) . . ?
C48 C53 H53 118.9 . . ?
C52 C53 H53 118.9 . . ?
C54 O32 C51 115.3(15) . . ?
O32 C54 H54A 109.5 . . ?
O32 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
O32 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C65 N61 N62 122.6(11) . . ?
C65 N61 Ag1 116.6(9) . . ?
N62 N61 Ag1 120.8(8) . . ?
C62 N62 N61 119.2(11) . . ?
C62 N62 Ag3 114.1(9) . . ?
N61 N62 Ag3 126.7(8) . . ?
N62 C62 C63 118.4(14) . . ?
N62 C62 C76 117.7(13) . . ?
C63 C62 C76 123.9(14) . . ?
C64 C63 C62 119.4(14) . . ?
C64 C63 H63 120.3 . . ?
C62 C63 H63 120.3 . . ?
C65 C64 C63 119.3(16) . . ?
C65 C64 H64 120.3 . . ?
C63 C64 H64 120.3 . . ?
C64 C65 N61 121.0(14) . . ?
C64 C65 C66 124.6(14) . . ?
N61 C65 C66 114.3(11) . . ?
N63 C66 C65 122.0(11) . . ?
N63 C66 H66 119.0 . . ?
C65 C66 H66 119.0 . . ?
C66 N63 C68 122.7(10) . . ?
C66 N63 Ag1 117.3(9) . . ?
C68 N63 Ag1 120.0(8) . . ?
C73 C68 C69 117.4(14) . . ?
C73 C68 N63 119.6(11) . . ?
C69 C68 N63 123.0(13) . . ?
N64 C76 C62 121.6(14) . . ?
N64 C76 H76 119.2 . . ?
C62 C76 H76 119.2 . . ?
C76 N64 C78 123.9(12) . . ?
C76 N64 Ag3 114.7(10) . . ?
C78 N64 Ag3 121.4(9) . . ?
C83 C78 C79 121.3(14) . . ?
C83 C78 N64 122.3(14) . . ?
C79 C78 N64 116.4(12) . . ?
C78 C79 C80 119.3(15) . . ?
C78 C79 H79 120.3 . . ?
C80 C79 H79 120.3 . . ?
C81 C80 C79 119.9(16) . . ?
C81 C80 H80 120.0 . . ?
C79 C80 H80 120.0 . . ?
C80 C81 O62 116.4(15) . . ?
C80 C81 C82 119.7(14) . . ?
O62 C81 C82 123.9(15) . . ?
C81 C82 C83 121.2(16) . . ?
C81 C82 H82 119.4 . . ?
C83 C82 H82 119.4 . . ?
C78 C83 C82 118.6(16) . . ?
C78 C83 H83 120.7 . . ?
C82 C83 H83 120.7 . . ?
C81 O62 C84 113.8(16) . . ?
O62 C84 H84A 109.5 . . ?
O62 C84 H84B 109.5 . . ?
H84A C84 H84B 109.5 . . ?
O62 C84 H84C 109.5 . . ?
H84A C84 H84C 109.5 . . ?
H84B C84 H84C 109.5 . . ?
C95 N91 N92 119.0(11) . . ?
C95 N91 Ag2 117.2(9) . . ?
N92 N91 Ag2 123.7(7) . . ?
N91 N92 C92 119.7(11) . . ?
N91 N92 Ag4 123.5(8) . . ?
C92 N92 Ag4 116.8(10) . . ?
C93 C92 N92 123.2(16) . . ?
C93 C92 C106 120.8(15) . . ?
N92 C92 C106 115.9(13) . . ?
C92 C93 C94 117.3(15) . . ?
C92 C93 H93 121.4 . . ?
C94 C93 H93 121.4 . . ?
C95 C94 C93 115.2(15) . . ?
C95 C94 H94 122.4 . . ?
C93 C94 H94 122.4 . . ?
N91 C95 C94 125.6(14) . . ?
N91 C95 C96 115.0(12) . . ?
C94 C95 C96 119.4(14) . . ?
N93 C96 C95 121.1(12) . . ?
N93 C96 H96 119.5 . . ?
C95 C96 H96 119.5 . . ?
C96 N93 C98 121.0(11) . . ?
C96 N93 Ag2 114.7(10) . . ?
C98 N93 Ag2 124.3(8) . . ?
C99 C98 C103 116.9(15) . . ?
C99 C98 N93 125.3(13) . . ?
C103 C98 N93 117.7(12) . . ?
C100 C99 C98 118.6(16) . . ?
C100 C99 H99 120.7 . . ?
C98 C99 H99 120.7 . . ?
C99 C100 C101 123.9(16) . . ?
C99 C100 H100 118.1 . . ?
C101 C100 H100 118.1 . . ?
C100 C101 C102 119.4(15) . . ?
C100 C101 O91 117.9(15) . . ?
C102 C101 O91 122.7(14) . . ?
C101 C102 C103 117.6(16) . . ?
C101 C102 H102 121.2 . . ?
C103 C102 H102 121.2 . . ?
C102 C103 C98 123.6(15) . . ?
C102 C103 H103 118.2 . . ?
C98 C103 H103 118.2 . . ?
C101 O91 C104 113.2(13) . . ?
O91 C104 H90A 109.5 . . ?
O91 C104 H90B 109.5 . . ?
H90A C104 H90B 109.5 . . ?
O91 C104 H90C 109.5 . . ?
H90A C104 H90C 109.5 . . ?
H90B C104 H90C 109.5 . . ?
N94 C106 C92 119.5(12) . . ?
N94 C106 H106 120.2 . . ?
C92 C106 H106 120.2 . . ?
C106 N94 C108 121.8(11) . . ?
C106 N94 Ag4 116.2(9) . . ?
C108 N94 Ag4 121.9(9) . . ?
C113 C108 C109 117.0(16) . . ?
C113 C108 N94 128.4(15) . . ?
C109 C108 N94 114.4(12) . . ?
C110 C109 C108 118.4(17) . . ?
C110 C109 H109 120.8 . . ?
C108 C109 H109 120.8 . . ?
C111 C110 C109 124(2) . . ?
C111 C110 H110 117.9 . . ?
C109 C110 H110 117.9 . . ?
C110 C111 C112 116.2(18) . . ?
C110 C111 O92 125.0(18) . . ?
C112 C111 O92 118.8(19) . . ?
C113 C112 C111 121.9(17) . . ?
C113 C112 H112 119.1 . . ?
C111 C112 H112 119.1 . . ?
C112 C113 C108 122.3(17) . . ?
C112 C113 H113 118.9 . . ?
C108 C113 H113 118.9 . . ?
C114 O92 C111 115.6(17) . . ?
O92 C114 H91A 109.5 . . ?
O92 C114 H91B 109.5 . . ?
H91A C114 H91B 109.5 . . ?
O92 C114 H91C 109.5 . . ?
H91A C114 H91C 109.5 . . ?
H91B C114 H91C 109.5 . . ?
N123 Ag5 N181 131.0(4) . . y
N123 Ag5 N183 139.6(4) . . y
N181 Ag5 N183 72.9(5) . . y
N123 Ag5 N121 71.3(4) . . y
N181 Ag5 N121 138.9(4) . . y
N183 Ag5 N121 114.2(4) . . y
N122 Ag6 N211 120.7(5) . . y
N122 Ag6 N213 145.1(5) . . y
N211 Ag6 N213 73.2(5) . . y
N122 Ag6 N124 72.0(4) . . y
N211 Ag6 N124 140.7(5) . . y
N213 Ag6 N124 119.4(4) . . y
N153 Ag7 N151 72.3(5) . . y
N153 Ag7 N184 124.4(5) . . y
N151 Ag7 N184 143.0(5) . . y
N153 Ag7 N182 144.3(5) . . y
N151 Ag7 N182 113.0(4) . . y
N184 Ag7 N182 73.9(5) . . y
N154 Ag8 N214 141.7(5) . . y
N154 Ag8 N212 124.5(4) . . y
N214 Ag8 N212 73.1(5) . . y
N154 Ag8 N152 71.8(4) . . y
N214 Ag8 N152 118.2(4) . . y
N212 Ag8 N152 140.9(5) . . y
N122 N121 C125 123.6(12) . . ?
N122 N121 Ag5 123.4(8) . . ?
C125 N121 Ag5 113.0(10) . . ?
C122 N122 N121 119.4(12) . . ?
C122 N122 Ag6 116.6(10) . . ?
N121 N122 Ag6 124.0(9) . . ?
N122 C122 C123 120.7(14) . . ?
N122 C122 C136 118.9(13) . . ?
C123 C122 C136 120.4(14) . . ?
C124 C123 C122 119.1(14) . . ?
C124 C123 H123 120.4 . . ?
C122 C123 H123 120.4 . . ?
C123 C124 C125 119.1(15) . . ?
C123 C124 H124 120.5 . . ?
C125 C124 H124 120.5 . . ?
N121 C125 C126 118.1(14) . . ?
N121 C125 C124 118.0(15) . . ?
C126 C125 C124 123.5(15) . . ?
N123 C126 C125 123.1(15) . . ?
N123 C126 H126 118.4 . . ?
C125 C126 H126 118.4 . . ?
C126 N123 C128 123.2(13) . . ?
C126 N123 Ag5 114.2(10) . . ?
C128 N123 Ag5 122.0(9) . . ?
C133 C128 C129 118.2(14) . . ?
C133 C128 N123 117.7(12) . . ?
C129 C128 N123 124.1(11) . . ?
C130 C129 C128 117.6(13) . . ?
C130 C129 H129 121.2 . . ?
C128 C129 H129 121.2 . . ?
C131 C130 C129 123.9(15) . . ?
C131 C130 H130 118.1 . . ?
C129 C130 H130 118.1 . . ?
C130 C131 O121 115.3(15) . . ?
C130 C131 C132 117.1(15) . . ?
O121 C131 C132 127.6(13) . . ?
C133 C132 C131 118.9(15) . . ?
C133 C132 H132 120.6 . . ?
C131 C132 H132 120.6 . . ?
C128 C133 C132 124.4(15) . . ?
C128 C133 H133 117.8 . . ?
C132 C133 H133 117.8 . . ?
C131 O121 C134 113.9(14) . . ?
O121 C134 H13A 109.5 . . ?
O121 C134 H13B 109.5 . . ?
H13A C134 H13B 109.5 . . ?
O121 C134 H13C 109.5 . . ?
H13A C134 H13C 109.5 . . ?
H13B C134 H13C 109.5 . . ?
N124 C136 C122 118.7(13) . . ?
N124 C136 H136 120.7 . . ?
C122 C136 H136 120.7 . . ?
C136 N124 C138 124.2(12) . . ?
C136 N124 Ag6 113.8(9) . . ?
C138 N124 Ag6 121.4(9) . . ?
C143 C138 C139 121.8(15) . . ?
C143 C138 N124 114.5(12) . . ?
C139 C138 N124 123.7(12) . . ?
C138 C139 C140 121.1(14) . . ?
C138 C139 H139 119.5 . . ?
C140 C139 H139 119.4 . . ?
C141 C140 C139 116.0(15) . . ?
C141 C140 H140 122.0 . . ?
C139 C140 H140 122.0 . . ?
C140 C141 C142 125.1(16) . . ?
C140 C141 O122 123.8(14) . . ?
C142 C141 O122 111.1(15) . . ?
C141 C142 C143 116.7(18) . . ?
C141 C142 H142 121.6 . . ?
C143 C142 H142 121.6 . . ?
C138 C143 C142 119.3(18) . . ?
C138 C143 H143 120.3 . . ?
C142 C143 H143 120.3 . . ?
C144 O122 C141 114.5(16) . . ?
O122 C144 H14D 109.5 . . ?
O122 C144 H14E 109.5 . . ?
H14D C144 H14E 109.5 . . ?
O122 C144 H14F 109.5 . . ?
H14D C144 H14F 109.5 . . ?
H14E C144 H14F 109.5 . . ?
C155 N151 N152 123.3(13) . . ?
C155 N151 Ag7 115.1(10) . . ?
N152 N151 Ag7 121.6(9) . . ?
N151 N152 C152 116.4(13) . . ?
N151 N152 Ag8 127.8(9) . . ?
C152 N152 Ag8 115.8(11) . . ?
C152 C153 C154 118.6(15) . . ?
C152 C153 H15A 120.7 . . ?
C154 C153 H15A 120.7 . . ?
N151 C155 C154 120.3(15) . . ?
N151 C155 C156 115.9(14) . . ?
C154 C155 C156 123.7(15) . . ?
N153 C156 C155 122.5(17) . . ?
N153 C156 H156 118.7 . . ?
C155 C156 H156 118.7 . . ?
C156 N153 C158 121.6(15) . . ?
C156 N153 Ag7 114.0(12) . . ?
C158 N153 Ag7 124.4(11) . . ?
N153 C158 C159 127.0(13) . . ?
N153 C158 C163 116.2(16) . . ?
C159 C158 C163 116.7(16) . . ?
C158 C159 C160 118.9(17) . . ?
C158 C159 H15B 120.6 . . ?
C160 C159 H15B 120.6 . . ?
C161 C160 C159 120(2) . . ?
C161 C160 H16A 119.9 . . ?
C159 C160 H16A 119.9 . . ?
C162 C161 C160 123(2) . . ?
C162 C161 O151 112(2) . . ?
C160 C161 O151 125(2) . . ?
C161 C162 C163 115(2) . . ?
C161 C162 H16B 122.7 . . ?
C163 C162 H16B 122.7 . . ?
C162 C163 C158 127(2) . . ?
C162 C163 H16C 116.7 . . ?
C158 C163 H16C 116.7 . . ?
C166 N154 C168 121.6(12) . . ?
C166 N154 Ag8 115.8(10) . . ?
C168 N154 Ag8 122.5(9) . . ?
N154 C168 C169 125.3(13) . . ?
N154 C168 C173 120.5(11) . . ?
C169 C168 C173 114.1(14) . . ?
C170 C169 C168 122.2(14) . . ?
C170 C169 H169 118.9 . . ?
C168 C169 H169 118.9 . . ?
C171 C170 C169 118.4(15) . . ?
C171 C170 H170 120.8 . . ?
C169 C170 H170 120.8 . . ?
C170 C171 O152 113.6(14) . . ?
C170 C171 C172 125.9(14) . . ?
O152 C171 C172 120.5(13) . . ?
C173 C172 C171 111.1(14) . . ?
C173 C172 H172 124.4 . . ?
C171 C172 H172 124.4 . . ?
C172 C173 C168 128.3(15) . . ?
C172 C173 H173 115.9 . . ?
C168 C173 H173 115.9 . . ?
C174 O152 C171 117.8(13) . . ?
O152 C174 H17A 109.5 . . ?
O152 C174 H17B 109.5 . . ?
H17A C174 H17B 109.5 . . ?
O152 C174 H17C 109.5 . . ?
H17A C174 H17C 109.5 . . ?
H17B C174 H17C 109.5 . . ?
N182 N181 C185 119.2(14) . . ?
N182 N181 Ag5 128.0(11) . . ?
C185 N181 Ag5 112.4(10) . . ?
N181 N182 C182 124.8(15) . . ?
N181 N182 Ag7 126.3(11) . . ?
C182 N182 Ag7 108.7(11) . . ?
C183 C182 N182 116.6(17) . . ?
C183 C182 C196 124.1(17) . . ?
N182 C182 C196 119.0(17) . . ?
C182 C183 C184 121.7(18) . . ?
C182 C183 H183 119.1 . . ?
C184 C183 H183 119.1 . . ?
C183 C184 C185 116.1(18) . . ?
C183 C184 H184 122.0 . . ?
C185 C184 H184 122.0 . . ?
N181 C185 C184 120.9(15) . . ?
N181 C185 C186 119.8(15) . . ?
C184 C185 C186 119.3(17) . . ?
N183 C186 C185 121.7(16) . . ?
N183 C186 H186 119.2 . . ?
C185 C186 H186 119.2 . . ?
C186 N183 C188 124.2(14) . . ?
C186 N183 Ag5 112.9(11) . . ?
C188 N183 Ag5 122.8(9) . . ?
N183 C188 C193 118.3(13) . . ?
N183 C188 C189 123.8(12) . . ?
C193 C188 C189 117.9(13) . . ?
C190 C189 C188 120.9(13) . . ?
C190 C189 H189 119.5 . . ?
C188 C189 H189 119.5 . . ?
C189 C190 C191 121.1(13) . . ?
C189 C190 H190 119.5 . . ?
C191 C190 H190 119.5 . . ?
O181 C191 C190 125.5(12) . . ?
O181 C191 C192 117.7(11) . . ?
C190 C191 C192 116.9(12) . . ?
C193 C192 C191 122.2(13) . . ?
C193 C192 H192 118.9 . . ?
C191 C192 H192 118.9 . . ?
C192 C193 C188 121.1(14) . . ?
C192 C193 H193 119.5 . . ?
C188 C193 H193 119.5 . . ?
C191 O181 C194 116.9(10) . . ?
O181 C194 H19A 109.5 . . ?
O181 C194 H19B 109.5 . . ?
H19A C194 H19B 109.5 . . ?
O181 C194 H19C 109.5 . . ?
H19A C194 H19C 109.5 . . ?
H19B C194 H19C 109.5 . . ?
N184 C196 C182 126.8(17) . . ?
N184 C196 H196 116.6 . . ?
C182 C196 H196 116.6 . . ?
C196 N184 C198 124.8(15) . . ?
C196 N184 Ag7 110.9(12) . . ?
C198 N184 Ag7 124.0(11) . . ?
C203 C198 N184 115.4(15) . . ?
C203 C198 C199 118.6(17) . . ?
N184 C198 C199 126.0(16) . . ?
C198 C199 C200 122.1(17) . . ?
C198 C199 H199 118.9 . . ?
C200 C199 H199 118.9 . . ?
C201 C200 C199 120.3(17) . . ?
C201 C200 H200 119.8 . . ?
C199 C200 H200 119.8 . . ?
O182 C201 C200 127.7(15) . . ?
O182 C201 C202 115.6(17) . . ?
C200 C201 C202 116.8(17) . . ?
C203 C202 C201 123(2) . . ?
C203 C202 H202 118.5 . . ?
C201 C202 H202 118.5 . . ?
C198 C203 C202 119(2) . . ?
C198 C203 H203 120.4 . . ?
C202 C203 H203 120.4 . . ?
C201 O182 C204 116.7(14) . . ?
O182 C204 H20A 109.5 . . ?
O182 C204 H20B 109.5 . . ?
H20A C204 H20B 109.5 . . ?
O182 C204 H20C 109.5 . . ?
H20A C204 H20C 109.5 . . ?
H20B C204 H20C 109.5 . . ?
N212 N211 C215 120.6(15) . . ?
N212 N211 Ag6 126.4(11) . . ?
C215 N211 Ag6 112.5(12) . . ?
N211 N212 C212 124.5(15) . . ?
N211 N212 Ag8 126.5(10) . . ?
C212 N212 Ag8 108.9(12) . . ?
N212 C212 C226 124.0(16) . . ?
N212 C212 C213 117.2(17) . . ?
C226 C212 C213 118.7(15) . . ?
C214 C213 C212 119.8(16) . . ?
C214 C213 H213 120.1 . . ?
C212 C213 H213 120.1 . . ?
C215 C214 C213 114.7(18) . . ?
C215 C214 H214 122.7 . . ?
C213 C214 H214 122.7 . . ?
N211 C215 C216 118.3(16) . . ?
N211 C215 C214 123.2(19) . . ?
C216 C215 C214 118.5(18) . . ?
N213 C216 C215 122.9(16) . . ?
N213 C216 H216 118.5 . . ?
C215 C216 H216 118.5 . . ?
C216 N213 C218 126.0(14) . . ?
C216 N213 Ag6 111.5(12) . . ?
C218 N213 Ag6 122.1(9) . . ?
C223 C218 C219 117.7(16) . . ?
C223 C218 N213 117.4(14) . . ?
C219 C218 N213 124.8(13) . . ?
C220 C219 C218 123.3(16) . . ?
C220 C219 H219 118.3 . . ?
C218 C219 H219 118.3 . . ?
C219 C220 C221 115.8(15) . . ?
C219 C220 H220 122.1 . . ?
C221 C220 H220 122.1 . . ?
O211 C221 C220 122.2(13) . . ?
O211 C221 C222 115.8(14) . . ?
C220 C221 C222 122.0(15) . . ?
C221 O211 C224 116.2(12) . . ?
C223 C222 C221 119.5(16) . . ?
C223 C222 H222 120.3 . . ?
C221 C222 H222 120.3 . . ?
C218 C223 C222 121.7(16) . . ?
C218 C223 H223 119.1 . . ?
C222 C223 H223 119.1 . . ?
C231 O212 C234 116.8(12) . . ?
O211 C224 H22A 109.5 . . ?
O211 C224 H22B 109.5 . . ?
H22A C224 H22B 109.5 . . ?
O211 C224 H22C 109.5 . . ?
H22A C224 H22C 109.5 . . ?
H22B C224 H22C 109.5 . . ?
N214 C226 C212 119.9(15) . . ?
N214 C226 H226 120.0 . . ?
C212 C226 H226 120.0 . . ?
C226 N214 C228 120.3(14) . . ?
C226 N214 Ag8 114.0(12) . . ?
C228 N214 Ag8 125.7(11) . . ?
N214 C228 C233 117.8(13) . . ?
N214 C228 C229 127.3(16) . . ?
C233 C228 C229 114.9(15) . . ?
C230 C229 C228 122.0(16) . . ?
C230 C229 H229 119.0 . . ?
C228 C229 H229 119.0 . . ?
C229 C230 C231 121.7(16) . . ?
C229 C230 H230 119.1 . . ?
C231 C230 H230 119.1 . . ?
C230 C231 O212 126.1(13) . . ?
C230 C231 C232 118.2(15) . . ?
O212 C231 C232 115.6(14) . . ?
C233 C232 C231 118.9(15) . . ?
C233 C232 H232 120.6 . . ?
C231 C232 H232 120.6 . . ?
C232 C233 C228 124.3(14) . . ?
C232 C233 H233 117.9 . . ?
C228 C233 H233 117.9 . . ?
O212 C234 H23A 109.5 . . ?
O212 C234 H23B 109.5 . . ?
H23A C234 H23B 109.5 . . ?
O212 C234 H23C 109.5 . . ?
H23A C234 H23C 109.5 . . ?
H23B C234 H23C 109.5 . . ?
F13 B1 F11 109.6(12) . . ?
F13 B1 F12 110.7(13) . . ?
F11 B1 F12 109.6(12) . . ?
F13 B1 F14 111.1(13) . . ?
F11 B1 F14 107.2(13) . . ?
F12 B1 F14 108.5(12) . . ?
F24 B2 F23 111.2(12) . . ?
F24 B2 F22 109.3(12) . . ?
F23 B2 F22 108.2(11) . . ?
F24 B2 F21 109.4(11) . . ?
F23 B2 F21 110.0(12) . . ?
F22 B2 F21 108.7(11) . . ?
F33 B3 F34 111.0(14) . . ?
F33 B3 F31 107.2(12) . . ?
F34 B3 F31 108.6(12) . . ?
F33 B3 F32 109.1(12) . . ?
F34 B3 F32 108.5(13) . . ?
F31 B3 F32 112.4(12) . . ?
F43 B4 F42 109.6(13) . . ?
F43 B4 F41 110.3(11) . . ?
F42 B4 F41 111.3(12) . . ?
F43 B4 F44 109.4(12) . . ?
F42 B4 F44 109.3(12) . . ?
F41 B4 F44 106.9(12) . . ?
F52 B5 F51 112.4(12) . . ?
F52 B5 F54 111.7(13) . . ?
F51 B5 F54 112.9(13) . . ?
F52 B5 F53 107.7(12) . . ?
F51 B5 F53 105.1(12) . . ?
F54 B5 F53 106.4(12) . . ?
F61 B6 F64 112.0(14) . . ?
F61 B6 F63 108.2(14) . . ?
F64 B6 F63 107.1(14) . . ?
F61 B6 F62 112.1(14) . . ?
F64 B6 F62 110.3(14) . . ?
F63 B6 F62 106.9(14) . . ?
F71 B7 F73 105.1(16) . . ?
F71 B7 F74 115.0(17) . . ?
F73 B7 F74 105.7(16) . . ?
F71 B7 F72 106.6(15) . . ?
F73 B7 F72 116.3(17) . . ?
F74 B7 F72 108.4(16) . . ?
C242 C241 C246 120.0 . . ?
C242 C241 H241 120.0 . . ?
C246 C241 H241 120.0 . . ?
C243 C242 C241 120.0 . . ?
C243 C242 H242 120.0 . . ?
C241 C242 H242 120.0 . . ?
C244 C243 C242 120.0 . . ?
C244 C243 H243 120.0 . . ?
C242 C243 H243 120.0 . . ?
C243 C244 C245 120.0 . . ?
C243 C244 H244 120.0 . . ?
C245 C244 H244 120.0 . . ?
C246 C245 C244 120.0 . . ?
C246 C245 H245 120.0 . . ?
C244 C245 H245 120.0 . . ?
C245 C246 C241 120.0 . . ?
C245 C246 H246 120.0 . . ?
C241 C246 H246 120.0 . . ?
C252 C251 C256 120.0 . . ?
C252 C251 H251 120.0 . . ?
C256 C251 H251 120.0 . . ?
C251 C252 C253 120.0 . . ?
C251 C252 H252 120.0 . . ?
C253 C252 H252 120.0 . . ?
C254 C253 C252 120.0 . . ?
C254 C253 H253 120.0 . . ?
C252 C253 H253 120.0 . . ?
C255 C254 C253 120.0 . . ?
C255 C254 H254 120.0 . . ?
C253 C254 H254 120.0 . . ?
C254 C255 C256 120.0 . . ?
C254 C255 H255 120.0 . . ?
C256 C255 H255 120.0 . . ?
C255 C256 C251 120.0 . . ?
C255 C256 H256 120.0 . . ?
C251 C256 H256 120.0 . . ?
C262 C261 C266 120.0 . . ?
C262 C261 H26A 120.0 . . ?
C266 C261 H26A 120.0 . . ?
C263 C262 C261 120.0 . . ?
C263 C262 H26B 120.0 . . ?
C261 C262 H26B 120.0 . . ?
C262 C263 C264 120.0 . . ?
C262 C263 H26C 120.0 . . ?
C264 C263 H26C 120.0 . . ?
C263 C264 C265 120.0 . . ?
C263 C264 H26D 120.0 . . ?
C265 C264 H26D 120.0 . . ?
C266 C265 C264 120.0 . . ?
C266 C265 H26E 120.0 . . ?
C264 C265 H26E 120.0 . . ?
C265 C266 C261 120.0 . . ?
C265 C266 H26F 120.0 . . ?
C261 C266 H26F 120.0 . . ?
C153 C154 C155 118.0(15) . . ?
C153 C154 H15C 121.0 . . ?
C155 C154 H15C 121.0 . . ?
C74 O61 C71 119.6(15) . . ?
C68 C73 C72 123.8(14) . . ?
C68 C73 H73A 118.1 . . ?
C72 C73 H73A 118.1 . . ?
O61 C71 C70 120.3(17) . . ?
O61 C71 C72 120.7(15) . . ?
C70 C71 C72 119.0(16) . . ?
C164 O151 C161 106.3(19) . . ?
C73 C72 C71 118.5(16) . . ?
C73 C72 H72A 120.8 . . ?
C71 C72 H72A 120.8 . . ?
O61 C74 H74A 109.5 . . ?
O61 C74 H74B 109.5 . . ?
H74A C74 H74B 109.5 . . ?
O61 C74 H74C 109.5 . . ?
H74A C74 H74C 109.5 . . ?
H74B C74 H74C 109.5 . . ?
N152 C152 C153 123.2(16) . . ?
N152 C152 C166 114.2(14) . . ?
C153 C152 C166 122.5(15) . . ?
C68 C69 C70 120.2(17) . . ?
C68 C69 H69A 119.9 . . ?
C70 C69 H69A 119.9 . . ?
C71 C70 C69 121.1(17) . . ?
C71 C70 H70A 119.4 . . ?
C69 C70 H70A 119.4 . . ?
N154 C166 C152 122.4(14) . . ?
N154 C166 H16D 118.8 . . ?
C152 C166 H16D 118.8 . . ?
O151 C164 H16E 109.5 . . ?
O151 C164 H16F 109.5 . . ?
H16E C164 H16F 109.5 . . ?
O151 C164 H16G 109.5 . . ?
H16E C164 H16G 109.5 . . ?
H16F C164 H16G 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N1 2.295(9) . y
Ag1 N63 2.297(9) . y
Ag1 N3 2.309(11) . y
Ag1 N61 2.329(11) . y
Ag2 N2 2.216(11) . y
Ag2 N93 2.244(11) . y
Ag2 N91 2.315(11) . y
Ag2 N4 2.327(10) . y
Ag3 N62 2.301(10) . y
Ag3 N31 2.306(10) . y
Ag3 N33 2.325(12) . y
Ag3 N64 2.332(11) . y
Ag4 N92 2.297(10) . y
Ag4 N32 2.313(11) . y
Ag4 N34 2.330(10) . y
Ag4 N94 2.342(10) . y
N1 C5 1.332(16) . ?
N1 N2 1.397(15) . ?
N2 C2 1.412(16) . ?
C2 C3 1.34(2) . ?
C2 C16 1.45(2) . ?
C3 C4 1.41(2) . ?
C3 H3 0.9500 . ?
C4 C5 1.404(19) . ?
C4 H4 0.9500 . ?
C5 C6 1.42(2) . ?
C6 N3 1.279(16) . ?
C6 H6 0.9500 . ?
N3 C8 1.401(16) . ?
C8 C13 1.360(14) . ?
C8 C9 1.366(14) . ?
C9 C10 1.406(15) . ?
C9 H9 0.9500 . ?
C10 C11 1.356(15) . ?
C10 H10 0.9500 . ?
C11 C12 1.369(15) . ?
C11 O1 1.398(15) . ?
C12 C13 1.388(14) . ?
C12 H12 0.9500 . ?
C13 H13 0.9500 . ?
O1 C14 1.345(17) . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C16 N4 1.276(16) . ?
C16 H16 0.9500 . ?
N4 C18 1.422(16) . ?
C18 C19 1.371(13) . ?
C18 C23 1.411(14) . ?
C19 C20 1.385(14) . ?
C19 H19 0.9500 . ?
C20 C21 1.370(14) . ?
C20 H20 0.9500 . ?
C21 O2 1.378(13) . ?
C21 C22 1.385(14) . ?
C22 C23 1.373(14) . ?
C22 H22 0.9500 . ?
C23 H23 0.9500 . ?
O2 C24 1.407(13) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
N31 N32 1.302(14) . ?
N31 C35 1.336(17) . ?
N32 C32 1.378(16) . ?
C32 C33 1.38(2) . ?
C32 C46 1.55(2) . ?
C33 C34 1.35(2) . ?
C33 H33 0.9500 . ?
C34 C35 1.40(2) . ?
C34 H34 0.9500 . ?
C35 C36 1.44(2) . ?
C36 N33 1.272(17) . ?
C36 H36 0.9500 . ?
N33 C38 1.449(16) . ?
C38 C39 1.377(13) . ?
C38 C43 1.395(13) . ?
C39 C40 1.408(13) . ?
C39 H39 0.9500 . ?
C40 C41 1.342(14) . ?
C40 H40 0.9500 . ?
C41 O31 1.386(13) . ?
C41 C42 1.386(14) . ?
C42 C43 1.335(14) . ?
C42 H42 0.9500 . ?
C43 H43 0.9500 . ?
O31 C44 1.385(14) . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C46 N34 1.305(18) . ?
C46 H46 0.9500 . ?
N34 C48 1.403(17) . ?
C48 C53 1.355(14) . ?
C48 C49 1.367(14) . ?
C49 C50 1.384(15) . ?
C49 H49 0.9500 . ?
C50 C51 1.357(15) . ?
C50 H50 0.9500 . ?
C51 C52 1.378(15) . ?
C51 O32 1.404(15) . ?
C52 C53 1.410(15) . ?
C52 H52 0.9500 . ?
C53 H53 0.9500 . ?
O32 C54 1.302(15) . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
N61 C65 1.332(16) . ?
N61 N62 1.340(14) . ?
N62 C62 1.330(16) . ?
C62 C63 1.42(2) . ?
C62 C76 1.46(2) . ?
C63 C64 1.37(2) . ?
C63 H63 0.9500 . ?
C64 C65 1.302(19) . ?
C64 H64 0.9500 . ?
C65 C66 1.440(19) . ?
C66 N63 1.234(16) . ?
C66 H66 0.9500 . ?
N63 C68 1.457(16) . ?
C68 C73 1.367(14) . ?
C68 C69 1.368(14) . ?
C76 N64 1.226(17) . ?
C76 H76 0.9500 . ?
N64 C78 1.410(17) . ?
C78 C83 1.368(15) . ?
C78 C79 1.374(15) . ?
C79 C80 1.403(15) . ?
C79 H79 0.9500 . ?
C80 C81 1.366(15) . ?
C80 H80 0.9500 . ?
C81 O62 1.374(14) . ?
C81 C82 1.376(16) . ?
C82 C83 1.391(15) . ?
C82 H82 0.9500 . ?
C83 H83 0.9500 . ?
O62 C84 1.390(17) . ?
C84 H84A 0.9800 . ?
C84 H84B 0.9800 . ?
C84 H84C 0.9800 . ?
N91 C95 1.259(15) . ?
N91 N92 1.344(14) . ?
N92 C92 1.354(17) . ?
C92 C93 1.33(2) . ?
C92 C106 1.49(2) . ?
C93 C94 1.42(2) . ?
C93 H93 0.9500 . ?
C94 C95 1.40(2) . ?
C94 H94 0.9500 . ?
C95 C96 1.478(19) . ?
C96 N93 1.301(18) . ?
C96 H96 0.9500 . ?
N93 C98 1.414(17) . ?
C98 C99 1.386(14) . ?
C98 C103 1.390(14) . ?
C99 C100 1.355(15) . ?
C99 H99 0.9500 . ?
C100 C101 1.358(15) . ?
C100 H100 0.9500 . ?
C101 C102 1.360(15) . ?
C101 O91 1.391(14) . ?
C102 C103 1.378(15) . ?
C102 H102 0.9500 . ?
C103 H103 0.9500 . ?
O91 C104 1.413(16) . ?
C104 H90A 0.9800 . ?
C104 H90B 0.9800 . ?
C104 H90C 0.9800 . ?
C106 N94 1.275(17) . ?
C106 H106 0.9500 . ?
N94 C108 1.420(17) . ?
C108 C113 1.384(14) . ?
C108 C109 1.396(16) . ?
C109 C110 1.393(16) . ?
C109 H109 0.9500 . ?
C110 C111 1.356(17) . ?
C110 H110 0.9500 . ?
C111 C112 1.370(16) . ?
C111 O92 1.383(16) . ?
C112 C113 1.358(15) . ?
C112 H112 0.9500 . ?
C113 H113 0.9500 . ?
O92 C114 1.366(18) . ?
C114 H91A 0.9800 . ?
C114 H91B 0.9800 . ?
C114 H91C 0.9800 . ?
Ag5 N123 2.315(13) . y
Ag5 N181 2.348(13) . y
Ag5 N183 2.360(14) . y
Ag5 N121 2.387(11) . y
Ag6 N122 2.218(12) . y
Ag6 N211 2.288(15) . y
Ag6 N213 2.309(12) . y
Ag6 N124 2.354(11) . y
Ag7 N153 2.313(15) . y
Ag7 N151 2.313(12) . y
Ag7 N184 2.316(13) . y
Ag7 N182 2.356(14) . y
Ag8 N154 2.323(11) . y
Ag8 N214 2.326(13) . y
Ag8 N212 2.344(14) . y
Ag8 N152 2.385(13) . y
N121 N122 1.344(15) . ?
N121 C125 1.340(17) . ?
N122 C122 1.316(17) . ?
C122 C123 1.42(2) . ?
C122 C136 1.44(2) . ?
C123 C124 1.35(2) . ?
C123 H123 0.9500 . ?
C124 C125 1.42(2) . ?
C124 H124 0.9500 . ?
C125 C126 1.39(2) . ?
C126 N123 1.302(18) . ?
C126 H126 0.9500 . ?
N123 C128 1.409(17) . ?
C128 C133 1.325(13) . ?
C128 C129 1.387(13) . ?
C129 C130 1.371(15) . ?
C129 H129 0.9500 . ?
C130 C131 1.345(15) . ?
C130 H130 0.9500 . ?
C131 O121 1.381(14) . ?
C131 C132 1.385(15) . ?
C132 C133 1.345(14) . ?
C132 H132 0.9500 . ?
C133 H133 0.9500 . ?
O121 C134 1.430(16) . ?
C134 H13A 0.9800 . ?
C134 H13B 0.9800 . ?
C134 H13C 0.9800 . ?
C136 N124 1.269(17) . ?
C136 H136 0.9500 . ?
N124 C138 1.437(17) . ?
C138 C143 1.355(15) . ?
C138 C139 1.371(13) . ?
C139 C140 1.385(15) . ?
C139 H139 0.9500 . ?
C140 C141 1.366(15) . ?
C140 H140 0.9500 . ?
C141 C142 1.379(16) . ?
C141 O122 1.418(15) . ?
C142 C143 1.407(16) . ?
C142 H142 0.9500 . ?
C143 H143 0.9500 . ?
O122 C144 1.356(17) . ?
C144 H14D 0.9800 . ?
C144 H14E 0.9800 . ?
C144 H14F 0.9800 . ?
N151 C155 1.313(18) . ?
N151 N152 1.331(15) . ?
N152 C152 1.339(18) . ?
C153 C152 1.35(2) . ?
C153 C154 1.36(2) . ?
C153 H15A 0.9500 . ?
C155 C154 1.37(2) . ?
C155 C156 1.48(2) . ?
C156 N153 1.244(19) . ?
C156 H156 0.9500 . ?
N153 C158 1.38(2) . ?
C158 C159 1.402(16) . ?
C158 C163 1.410(15) . ?
C159 C160 1.423(17) . ?
C159 H15B 0.9500 . ?
C160 C161 1.411(18) . ?
C160 H16A 0.9500 . ?
C161 C162 1.372(17) . ?
C161 O151 1.462(18) . ?
C162 C163 1.395(16) . ?
C162 H16B 0.9500 . ?
C163 H16C 0.9500 . ?
N154 C166 1.271(18) . ?
N154 C168 1.365(17) . ?
C168 C169 1.375(11) . ?
C168 C173 1.378(14) . ?
C169 C170 1.361(15) . ?
C169 H169 0.9500 . ?
C170 C171 1.323(15) . ?
C170 H170 0.9500 . ?
C171 O152 1.390(13) . ?
C171 C172 1.393(14) . ?
C172 C173 1.358(14) . ?
C172 H172 0.9500 . ?
C173 H173 0.9500 . ?
O152 C174 1.353(15) . ?
C174 H17A 0.9800 . ?
C174 H17B 0.9800 . ?
C174 H17C 0.9800 . ?
N181 N182 1.258(17) . ?
N181 C185 1.36(2) . ?
N182 C182 1.37(2) . ?
C182 C183 1.36(2) . ?
C182 C196 1.40(2) . ?
C183 C184 1.38(2) . ?
C183 H183 0.9500 . ?
C184 C185 1.40(2) . ?
C184 H184 0.9500 . ?
C185 C186 1.43(2) . ?
C186 N183 1.306(18) . ?
C186 H186 0.9500 . ?
N183 C188 1.361(17) . ?
C188 C193 1.373(14) . ?
C188 C189 1.421(14) . ?
C189 C190 1.374(14) . ?
C189 H189 0.9500 . ?
C190 C191 1.395(13) . ?
C190 H190 0.9500 . ?
C191 O181 1.388(12) . ?
C191 C192 1.409(14) . ?
C192 C193 1.364(14) . ?
C192 H192 0.9500 . ?
C193 H193 0.9500 . ?
O181 C194 1.407(13) . ?
C194 H19A 0.9800 . ?
C194 H19B 0.9800 . ?
C194 H19C 0.9800 . ?
C196 N184 1.22(2) . ?
C196 H196 0.9500 . ?
N184 C198 1.37(2) . ?
C198 C203 1.356(16) . ?
C198 C199 1.374(14) . ?
C199 C200 1.385(16) . ?
C199 H199 0.9500 . ?
C200 C201 1.358(16) . ?
C200 H200 0.9500 . ?
C201 O182 1.354(15) . ?
C201 C202 1.397(16) . ?
C202 C203 1.377(17) . ?
C202 H202 0.9500 . ?
C203 H203 0.9500 . ?
O182 C204 1.407(15) . ?
C204 H20A 0.9800 . ?
C204 H20B 0.9800 . ?
C204 H20C 0.9800 . ?
N211 N212 1.303(18) . ?
N211 C215 1.36(2) . ?
N212 C212 1.336(19) . ?
C212 C226 1.40(2) . ?
C212 C213 1.47(2) . ?
C213 C214 1.44(3) . ?
C213 H213 0.9500 . ?
C214 C215 1.40(2) . ?
C214 H214 0.9500 . ?
C215 C216 1.39(2) . ?
C216 N213 1.298(19) . ?
C216 H216 0.9500 . ?
N213 C218 1.408(19) . ?
C218 C223 1.346(15) . ?
C218 C219 1.386(15) . ?
C219 C220 1.372(15) . ?
C219 H219 0.9500 . ?
C220 C221 1.374(15) . ?
C220 H220 0.9500 . ?
C221 O211 1.344(14) . ?
C221 C222 1.373(15) . ?
O211 C224 1.410(14) . ?
C222 C223 1.349(15) . ?
C222 H222 0.9500 . ?
C223 H223 0.9500 . ?
O212 C231 1.373(14) . ?
O212 C234 1.396(14) . ?
C224 H22A 0.9800 . ?
C224 H22B 0.9800 . ?
C224 H22C 0.9800 . ?
C226 N214 1.27(2) . ?
C226 H226 0.9500 . ?
N214 C228 1.347(19) . ?
C228 C233 1.383(15) . ?
C228 C229 1.412(14) . ?
C229 C230 1.354(15) . ?
C229 H229 0.9500 . ?
C230 C231 1.368(15) . ?
C230 H230 0.9500 . ?
C231 C232 1.408(15) . ?
C232 C233 1.361(15) . ?
C232 H232 0.9500 . ?
C233 H233 0.9500 . ?
C234 H23A 0.9800 . ?
C234 H23B 0.9800 . ?
C234 H23C 0.9800 . ?
B1 F13 1.360(15) . ?
B1 F11 1.385(15) . ?
B1 F12 1.390(15) . ?
B1 F14 1.393(15) . ?
B2 F24 1.376(14) . ?
B2 F23 1.379(14) . ?
B2 F22 1.395(14) . ?
B2 F21 1.394(14) . ?
B3 F33 1.361(15) . ?
B3 F34 1.363(15) . ?
B3 F31 1.371(14) . ?
B3 F32 1.394(14) . ?
B4 F43 1.366(15) . ?
B4 F42 1.366(14) . ?
B4 F41 1.374(15) . ?
B4 F44 1.392(14) . ?
B5 F52 1.364(15) . ?
B5 F51 1.378(15) . ?
B5 F54 1.391(15) . ?
B5 F53 1.406(16) . ?
B6 F61 1.354(16) . ?
B6 F64 1.381(16) . ?
B6 F63 1.393(17) . ?
B6 F62 1.402(17) . ?
B7 F71 1.345(17) . ?
B7 F73 1.357(18) . ?
B7 F74 1.368(17) . ?
B7 F72 1.402(17) . ?
C241 C242 1.3900 . ?
C241 C246 1.3900 . ?
C241 H241 0.9500 . ?
C242 C243 1.3900 . ?
C242 H242 0.9500 . ?
C243 C244 1.3900 . ?
C243 H243 0.9500 . ?
C244 C245 1.3900 . ?
C244 H244 0.9500 . ?
C245 C246 1.3900 . ?
C245 H245 0.9500 . ?
C246 H246 0.9500 . ?
C251 C252 1.3900 . ?
C251 C256 1.3900 . ?
C251 H251 0.9500 . ?
C252 C253 1.3900 . ?
C252 H252 0.9500 . ?
C253 C254 1.3900 . ?
C253 H253 0.9500 . ?
C254 C255 1.3900 . ?
C254 H254 0.9500 . ?
C255 C256 1.3900 . ?
C255 H255 0.9500 . ?
C256 H256 0.9500 . ?
C261 C262 1.3900 . ?
C261 C266 1.3900 . ?
C261 H26A 0.9500 . ?
C262 C263 1.3900 . ?
C262 H26B 0.9500 . ?
C263 C264 1.3900 . ?
C263 H26C 0.9500 . ?
C264 C265 1.3900 . ?
C264 H26D 0.9500 . ?
C265 C266 1.3900 . ?
C265 H26E 0.9500 . ?
C266 H26F 0.9500 . ?
C154 H15C 0.9500 . ?
O61 C74 1.364(16) . ?
O61 C71 1.362(14) . ?
C73 C72 1.373(15) . ?
C73 H73A 0.9500 . ?
C71 C70 1.375(16) . ?
C71 C72 1.376(16) . ?
O151 C164 1.40(2) . ?
C72 H72A 0.9500 . ?
C74 H74A 0.9800 . ?
C74 H74B 0.9800 . ?
C74 H74C 0.9800 . ?
C152 C166 1.53(2) . ?
C69 C70 1.391(16) . ?
C69 H69A 0.9500 . ?
C70 H70A 0.9500 . ?
C166 H16D 0.9500 . ?
C164 H16E 0.9800 . ?
C164 H16F 0.9800 . ?
C164 H16G 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N63 Ag1 N1 C5 -121.2(10) . . . . ?
N3 Ag1 N1 C5 2.4(9) . . . . ?
N61 Ag1 N1 C5 145.6(9) . . . . ?
N63 Ag1 N1 N2 55.7(10) . . . . ?
N3 Ag1 N1 N2 179.3(10) . . . . ?
N61 Ag1 N1 N2 -37.5(10) . . . . ?
C5 N1 N2 C2 -7.1(17) . . . . ?
Ag1 N1 N2 C2 176.2(9) . . . . ?
C5 N1 N2 Ag2 172.2(9) . . . . ?
Ag1 N1 N2 Ag2 -4.5(13) . . . . ?
N93 Ag2 N2 N1 -34.6(12) . . . . ?
N91 Ag2 N2 N1 68.7(11) . . . . ?
N4 Ag2 N2 N1 -179.2(10) . . . . ?
N93 Ag2 N2 C2 144.7(9) . . . . ?
N91 Ag2 N2 C2 -112.0(10) . . . . ?
N4 Ag2 N2 C2 0.1(9) . . . . ?
N1 N2 C2 C3 6.2(19) . . . . ?
Ag2 N2 C2 C3 -173.2(12) . . . . ?
N1 N2 C2 C16 -178.6(11) . . . . ?
Ag2 N2 C2 C16 2.1(15) . . . . ?
N2 C2 C3 C4 -4(2) . . . . ?
C16 C2 C3 C4 -178.9(15) . . . . ?
C2 C3 C4 C5 2(2) . . . . ?
N2 N1 C5 C4 6(2) . . . . ?
Ag1 N1 C5 C4 -177.0(12) . . . . ?
N2 N1 C5 C6 -177.5(12) . . . . ?
Ag1 N1 C5 C6 -0.6(17) . . . . ?
C3 C4 C5 N1 -3(2) . . . . ?
C3 C4 C5 C6 -179.7(15) . . . . ?
N1 C5 C6 N3 -4(2) . . . . ?
C4 C5 C6 N3 172.9(15) . . . . ?
C5 C6 N3 C8 -178.1(12) . . . . ?
C5 C6 N3 Ag1 5.7(18) . . . . ?
N1 Ag1 N3 C6 -4.2(10) . . . . ?
N63 Ag1 N3 C6 128.8(10) . . . . ?
N61 Ag1 N3 C6 -124.5(11) . . . . ?
N1 Ag1 N3 C8 179.8(9) . . . . ?
N63 Ag1 N3 C8 -47.2(9) . . . . ?
N61 Ag1 N3 C8 59.6(10) . . . . ?
C6 N3 C8 C13 -177.9(11) . . . . ?
Ag1 N3 C8 C13 -2.2(9) . . . . ?
C6 N3 C8 C9 2.1(15) . . . . ?
Ag1 N3 C8 C9 177.8(5) . . . . ?
C13 C8 C9 C10 -0.01(15) . . . . ?
N3 C8 C9 C10 -180.0(7) . . . . ?
C8 C9 C10 C11 -0.03(15) . . . . ?
C9 C10 C11 C12 0.1(3) . . . . ?
C9 C10 C11 O1 179.96(19) . . . . ?
C10 C11 C12 C13 0.0(5) . . . . ?
O1 C11 C12 C13 -179.9(3) . . . . ?
C9 C8 C13 C12 0.0(3) . . . . ?
N3 C8 C13 C12 180.0(7) . . . . ?
C11 C12 C13 C8 0.0(5) . . . . ?
C10 C11 O1 C14 -178.2(17) . . . . ?
C12 C11 O1 C14 1.7(18) . . . . ?
C3 C2 C16 N4 170.5(14) . . . . ?
N2 C2 C16 N4 -4.7(19) . . . . ?
C2 C16 N4 C18 -180.0(11) . . . . ?
C2 C16 N4 Ag2 4.8(16) . . . . ?
N2 Ag2 N4 C16 -2.5(9) . . . . ?
N93 Ag2 N4 C16 -136.1(10) . . . . ?
N91 Ag2 N4 C16 127.3(9) . . . . ?
N2 Ag2 N4 C18 -177.8(9) . . . . ?
N93 Ag2 N4 C18 48.7(11) . . . . ?
N91 Ag2 N4 C18 -47.9(9) . . . . ?
C16 N4 C18 C19 7.0(14) . . . . ?
Ag2 N4 C18 C19 -178.1(5) . . . . ?
C16 N4 C18 C23 -178.4(10) . . . . ?
Ag2 N4 C18 C23 -3.5(9) . . . . ?
C23 C18 C19 C20 0.00(14) . . . . ?
N4 C18 C19 C20 174.4(7) . . . . ?
C18 C19 C20 C21 0.02(15) . . . . ?
C19 C20 C21 O2 -179.9(2) . . . . ?
C19 C20 C21 C22 0.0(3) . . . . ?
C20 C21 C22 C23 0.0(4) . . . . ?
O2 C21 C22 C23 179.9(3) . . . . ?
C21 C22 C23 C18 0.1(4) . . . . ?
C19 C18 C23 C22 0.0(3) . . . . ?
N4 C18 C23 C22 -174.8(7) . . . . ?
C20 C21 O2 C24 8.1(12) . . . . ?
C22 C21 O2 C24 -171.9(11) . . . . ?
N62 Ag3 N31 N32 72.9(11) . . . . ?
N33 Ag3 N31 N32 -172.2(11) . . . . ?
N64 Ag3 N31 N32 -26.0(12) . . . . ?
N62 Ag3 N31 C35 -120.6(10) . . . . ?
N33 Ag3 N31 C35 -5.7(9) . . . . ?
N64 Ag3 N31 C35 140.5(9) . . . . ?
C35 N31 N32 C32 4.5(19) . . . . ?
Ag3 N31 N32 C32 170.0(9) . . . . ?
C35 N31 N32 Ag4 177.8(10) . . . . ?
Ag3 N31 N32 Ag4 -16.7(14) . . . . ?
N92 Ag4 N32 N31 -25.4(12) . . . . ?
N34 Ag4 N32 N31 -171.1(11) . . . . ?
N94 Ag4 N32 N31 70.4(12) . . . . ?
N92 Ag4 N32 C32 148.1(9) . . . . ?
N34 Ag4 N32 C32 2.3(9) . . . . ?
N94 Ag4 N32 C32 -116.1(9) . . . . ?
N31 N32 C32 C33 -2(2) . . . . ?
Ag4 N32 C32 C33 -176.0(12) . . . . ?
N31 N32 C32 C46 174.7(11) . . . . ?
Ag4 N32 C32 C46 0.7(15) . . . . ?
N32 C32 C33 C34 -3(2) . . . . ?
C46 C32 C33 C34 -179.2(15) . . . . ?
C32 C33 C34 C35 5(2) . . . . ?
N32 N31 C35 C34 -3(2) . . . . ?
Ag3 N31 C35 C34 -169.3(12) . . . . ?
N32 N31 C35 C36 176.5(13) . . . . ?
Ag3 N31 C35 C36 9.8(17) . . . . ?
C33 C34 C35 N31 -2(2) . . . . ?
C33 C34 C35 C36 178.8(15) . . . . ?
N31 C35 C36 N33 -10(2) . . . . ?
C34 C35 C36 N33 169.3(15) . . . . ?
C35 C36 N33 C38 -177.6(12) . . . . ?
C35 C36 N33 Ag3 4.2(19) . . . . ?
N62 Ag3 N33 C36 129.1(10) . . . . ?
N31 Ag3 N33 C36 0.8(10) . . . . ?
N64 Ag3 N33 C36 -129.7(11) . . . . ?
N62 Ag3 N33 C38 -49.1(9) . . . . ?
N31 Ag3 N33 C38 -177.4(9) . . . . ?
N64 Ag3 N33 C38 52.1(11) . . . . ?
C36 N33 C38 C39 1.8(15) . . . . ?
Ag3 N33 C38 C39 179.9(4) . . . . ?
C36 N33 C38 C43 -180.0(11) . . . . ?
Ag3 N33 C38 C43 -1.9(9) . . . . ?
C43 C38 C39 C40 0.01(14) . . . . ?
N33 C38 C39 C40 178.1(7) . . . . ?
C38 C39 C40 C41 0.02(15) . . . . ?
C39 C40 C41 O31 -180.0(2) . . . . ?
C39 C40 C41 C42 0.0(3) . . . . ?
C40 C41 C42 C43 0.0(4) . . . . ?
O31 C41 C42 C43 179.9(3) . . . . ?
C41 C42 C43 C38 0.1(4) . . . . ?
C39 C38 C43 C42 -0.1(3) . . . . ?
N33 C38 C43 C42 -178.3(7) . . . . ?
C40 C41 O31 C44 14.1(12) . . . . ?
C42 C41 O31 C44 -165.9(12) . . . . ?
N32 C32 C46 N34 -5.9(19) . . . . ?
C33 C32 C46 N34 170.7(14) . . . . ?
C32 C46 N34 C48 -176.8(10) . . . . ?
C32 C46 N34 Ag4 8.0(16) . . . . ?
N92 Ag4 N34 C46 -133.2(10) . . . . ?
N32 Ag4 N34 C46 -5.7(9) . . . . ?
N94 Ag4 N34 C46 123.8(10) . . . . ?
N92 Ag4 N34 C48 51.9(12) . . . . ?
N32 Ag4 N34 C48 179.4(9) . . . . ?
N94 Ag4 N34 C48 -51.1(10) . . . . ?
C46 N34 C48 C53 -170.8(10) . . . . ?
Ag4 N34 C48 C53 4.0(10) . . . . ?
C46 N34 C48 C49 7.8(14) . . . . ?
Ag4 N34 C48 C49 -177.4(5) . . . . ?
C53 C48 C49 C50 0.00(15) . . . . ?
N34 C48 C49 C50 -178.6(8) . . . . ?
C48 C49 C50 C51 -0.03(15) . . . . ?
C49 C50 C51 C52 0.0(4) . . . . ?
C49 C50 C51 O32 179.94(18) . . . . ?
C50 C51 C52 C53 0.0(4) . . . . ?
O32 C51 C52 C53 -179.9(3) . . . . ?
C49 C48 C53 C52 0.0(3) . . . . ?
N34 C48 C53 C52 178.7(7) . . . . ?
C51 C52 C53 C48 0.0(4) . . . . ?
C50 C51 O32 C54 169.3(15) . . . . ?
C52 C51 O32 C54 -10.8(16) . . . . ?
N1 Ag1 N61 C65 132.9(9) . . . . ?
N63 Ag1 N61 C65 1.6(9) . . . . ?
N3 Ag1 N61 C65 -123.2(10) . . . . ?
N1 Ag1 N61 N62 -46.3(10) . . . . ?
N63 Ag1 N61 N62 -177.5(9) . . . . ?
N3 Ag1 N61 N62 57.6(11) . . . . ?
C65 N61 N62 C62 -1.1(17) . . . . ?
Ag1 N61 N62 C62 178.0(9) . . . . ?
C65 N61 N62 Ag3 177.3(9) . . . . ?
Ag1 N61 N62 Ag3 -3.6(12) . . . . ?
N31 Ag3 N62 C62 -124.2(9) . . . . ?
N33 Ag3 N62 C62 143.3(9) . . . . ?
N64 Ag3 N62 C62 0.1(9) . . . . ?
N31 Ag3 N62 N61 57.4(11) . . . . ?
N33 Ag3 N62 N61 -35.1(10) . . . . ?
N64 Ag3 N62 N61 -178.3(10) . . . . ?
N61 N62 C62 C63 1.2(19) . . . . ?
Ag3 N62 C62 C63 -177.3(10) . . . . ?
N61 N62 C62 C76 178.6(11) . . . . ?
Ag3 N62 C62 C76 0.0(16) . . . . ?
N62 C62 C63 C64 1(2) . . . . ?
C76 C62 C63 C64 -176.4(14) . . . . ?
C62 C63 C64 C65 -3(2) . . . . ?
C63 C64 C65 N61 3(2) . . . . ?
C63 C64 C65 C66 -174.7(13) . . . . ?
N62 N61 C65 C64 -1(2) . . . . ?
Ag1 N61 C65 C64 179.6(11) . . . . ?
N62 N61 C65 C66 176.9(11) . . . . ?
Ag1 N61 C65 C66 -2.2(14) . . . . ?
C64 C65 C66 N63 179.8(14) . . . . ?
N61 C65 C66 N63 1.7(19) . . . . ?
C65 C66 N63 C68 177.6(10) . . . . ?
C65 C66 N63 Ag1 -0.2(17) . . . . ?
N1 Ag1 N63 C66 -116.8(10) . . . . ?
N3 Ag1 N63 C66 142.5(10) . . . . ?
N61 Ag1 N63 C66 -0.7(9) . . . . ?
N1 Ag1 N63 C68 65.4(9) . . . . ?
N3 Ag1 N63 C68 -35.3(9) . . . . ?
N61 Ag1 N63 C68 -178.5(8) . . . . ?
C66 N63 C68 C73 -170.4(10) . . . . ?
Ag1 N63 C68 C73 7.3(10) . . . . ?
C66 N63 C68 C69 8.7(15) . . . . ?
Ag1 N63 C68 C69 -173.6(5) . . . . ?
N62 C62 C76 N64 0(2) . . . . ?
C63 C62 C76 N64 176.8(14) . . . . ?
C62 C76 N64 C78 179.5(11) . . . . ?
C62 C76 N64 Ag3 0.5(17) . . . . ?
N62 Ag3 N64 C76 -0.3(10) . . . . ?
N31 Ag3 N64 C76 128.6(10) . . . . ?
N33 Ag3 N64 C76 -117.2(11) . . . . ?
N62 Ag3 N64 C78 -179.4(9) . . . . ?
N31 Ag3 N64 C78 -50.4(10) . . . . ?
N33 Ag3 N64 C78 63.8(11) . . . . ?
C76 N64 C78 C83 15.6(16) . . . . ?
Ag3 N64 C78 C83 -165.4(6) . . . . ?
C76 N64 C78 C79 -165.0(12) . . . . ?
Ag3 N64 C78 C79 13.9(10) . . . . ?
C83 C78 C79 C80 -0.01(15) . . . . ?
N64 C78 C79 C80 -179.4(8) . . . . ?
C78 C79 C80 C81 -0.02(15) . . . . ?
C79 C80 C81 O62 179.96(19) . . . . ?
C79 C80 C81 C82 0.0(3) . . . . ?
C80 C81 C82 C83 0.0(4) . . . . ?
O62 C81 C82 C83 -179.9(3) . . . . ?
C79 C78 C83 C82 0.0(3) . . . . ?
N64 C78 C83 C82 179.3(8) . . . . ?
C81 C82 C83 C78 0.0(4) . . . . ?
C80 C81 O62 C84 161.2(16) . . . . ?
C82 C81 O62 C84 -18.9(17) . . . . ?
N2 Ag2 N91 C95 -131.1(9) . . . . ?
N93 Ag2 N91 C95 -2.8(9) . . . . ?
N4 Ag2 N91 C95 137.5(9) . . . . ?
N2 Ag2 N91 N92 53.5(11) . . . . ?
N93 Ag2 N91 N92 -178.3(10) . . . . ?
N4 Ag2 N91 N92 -38.0(10) . . . . ?
C95 N91 N92 C92 3.1(17) . . . . ?
Ag2 N91 N92 C92 178.5(9) . . . . ?
C95 N91 N92 Ag4 -176.9(9) . . . . ?
Ag2 N91 N92 Ag4 -1.5(12) . . . . ?
N32 Ag4 N92 N91 -51.0(10) . . . . ?
N34 Ag4 N92 N91 61.3(12) . . . . ?
N94 Ag4 N92 N91 -179.5(10) . . . . ?
N32 Ag4 N92 C92 129.0(9) . . . . ?
N34 Ag4 N92 C92 -118.7(10) . . . . ?
N94 Ag4 N92 C92 0.5(9) . . . . ?
N91 N92 C92 C93 -4(2) . . . . ?
Ag4 N92 C92 C93 176.3(13) . . . . ?
N91 N92 C92 C106 179.1(11) . . . . ?
Ag4 N92 C92 C106 -0.9(16) . . . . ?
N92 C92 C93 C94 2(2) . . . . ?
C106 C92 C93 C94 179.4(14) . . . . ?
C92 C93 C94 C95 -1(2) . . . . ?
N92 N91 C95 C94 -1(2) . . . . ?
Ag2 N91 C95 C94 -177.2(12) . . . . ?
N92 N91 C95 C96 178.4(11) . . . . ?
Ag2 N91 C95 C96 2.7(15) . . . . ?
C93 C94 C95 N91 0(2) . . . . ?
C93 C94 C95 C96 -179.7(13) . . . . ?
N91 C95 C96 N93 -0.6(19) . . . . ?
C94 C95 C96 N93 179.3(14) . . . . ?
C95 C96 N93 C98 179.1(10) . . . . ?
C95 C96 N93 Ag2 -1.9(16) . . . . ?
N2 Ag2 N93 C96 133.8(9) . . . . ?
N91 Ag2 N93 C96 2.3(9) . . . . ?
N4 Ag2 N93 C96 -110.5(10) . . . . ?
N2 Ag2 N93 C98 -47.2(10) . . . . ?
N91 Ag2 N93 C98 -178.7(9) . . . . ?
N4 Ag2 N93 C98 68.5(11) . . . . ?
C96 N93 C98 C99 19.1(14) . . . . ?
Ag2 N93 C98 C99 -159.9(6) . . . . ?
C96 N93 C98 C103 -163.8(10) . . . . ?
Ag2 N93 C98 C103 17.3(10) . . . . ?
C103 C98 C99 C100 0.00(14) . . . . ?
N93 C98 C99 C100 177.1(8) . . . . ?
C98 C99 C100 C101 0.01(16) . . . . ?
C99 C100 C101 C102 0.0(3) . . . . ?
C99 C100 C101 O91 -179.97(19) . . . . ?
C100 C101 C102 C103 0.0(4) . . . . ?
O91 C101 C102 C103 180.0(3) . . . . ?
C101 C102 C103 C98 0.0(5) . . . . ?
C99 C98 C103 C102 0.0(3) . . . . ?
N93 C98 C103 C102 -177.4(8) . . . . ?
C100 C101 O91 C104 -177.3(13) . . . . ?
C102 C101 O91 C104 2.7(14) . . . . ?
C93 C92 C106 N94 -176.3(15) . . . . ?
N92 C92 C106 N94 0.9(19) . . . . ?
C92 C106 N94 C108 -179.7(11) . . . . ?
C92 C106 N94 Ag4 -0.5(16) . . . . ?
N92 Ag4 N94 C106 0.0(9) . . . . ?
N32 Ag4 N94 C106 -120.4(10) . . . . ?
N34 Ag4 N94 C106 143.2(9) . . . . ?
N92 Ag4 N94 C108 179.2(9) . . . . ?
N32 Ag4 N94 C108 58.9(10) . . . . ?
N34 Ag4 N94 C108 -37.6(10) . . . . ?
C106 N94 C108 C113 -0.8(16) . . . . ?
Ag4 N94 C108 C113 -180.0(6) . . . . ?
C106 N94 C108 C109 175.3(11) . . . . ?
Ag4 N94 C108 C109 -3.9(11) . . . . ?
C113 C108 C109 C110 -0.04(14) . . . . ?
N94 C108 C109 C110 -176.6(8) . . . . ?
C108 C109 C110 C111 0.00(16) . . . . ?
C109 C110 C111 C112 -0.1(3) . . . . ?
C109 C110 C111 O92 180.0(2) . . . . ?
C110 C111 C112 C113 0.2(4) . . . . ?
O92 C111 C112 C113 -179.8(3) . . . . ?
C111 C112 C113 C108 -0.3(5) . . . . ?
C109 C108 C113 C112 0.2(3) . . . . ?
N94 C108 C113 C112 176.2(10) . . . . ?
C110 C111 O92 C114 38(3) . . . . ?
C112 C111 O92 C114 -142(3) . . . . ?
N123 Ag5 N121 N122 -179(100) . . . . ?
N181 Ag5 N121 N122 48.9(13) . . . . ?
N183 Ag5 N121 N122 -42.5(11) . . . . ?
N123 Ag5 N121 C125 0.0(8) . . . . ?
N181 Ag5 N121 C125 -131.8(9) . . . . ?
N183 Ag5 N121 C125 136.8(9) . . . . ?
C125 N121 N122 C122 1.2(19) . . . . ?
Ag5 N121 N122 C122 -179.7(10) . . . . ?
C125 N121 N122 Ag6 -175.3(9) . . . . ?
Ag5 N121 N122 Ag6 3.9(14) . . . . ?
N211 Ag6 N122 C122 139.8(10) . . . . ?
N213 Ag6 N122 C122 -114.8(11) . . . . ?
N124 Ag6 N122 C122 1.0(10) . . . . ?
N211 Ag6 N122 N121 -43.6(12) . . . . ?
N213 Ag6 N122 N121 61.7(13) . . . . ?
N124 Ag6 N122 N121 177.5(11) . . . . ?
N121 N122 C122 C123 2(2) . . . . ?
Ag6 N122 C122 C123 179.0(11) . . . . ?
N121 N122 C122 C136 -178.3(11) . . . . ?
Ag6 N122 C122 C136 -1.6(17) . . . . ?
N122 C122 C123 C124 -2(2) . . . . ?
C136 C122 C123 C124 178.7(13) . . . . ?
C122 C123 C124 C125 -2(2) . . . . ?
N122 N121 C125 C126 -177.6(12) . . . . ?
Ag5 N121 C125 C126 3.2(15) . . . . ?
N122 N121 C125 C124 -4.8(19) . . . . ?
Ag5 N121 C125 C124 176.0(10) . . . . ?
C123 C124 C125 N121 5(2) . . . . ?
C123 C124 C125 C126 177.3(14) . . . . ?
N121 C125 C126 N123 -7(2) . . . . ?
C124 C125 C126 N123 -179.3(13) . . . . ?
C125 C126 N123 C128 178.2(11) . . . . ?
C125 C126 N123 Ag5 6.6(17) . . . . ?
N181 Ag5 N123 C126 136.3(10) . . . . ?
N183 Ag5 N123 C126 -108.9(10) . . . . ?
N121 Ag5 N123 C126 -3.2(9) . . . . ?
N181 Ag5 N123 C128 -35.5(11) . . . . ?
N183 Ag5 N123 C128 79.4(10) . . . . ?
N121 Ag5 N123 C128 -175.0(9) . . . . ?
C126 N123 C128 C133 -173.1(10) . . . . ?
Ag5 N123 C128 C133 -2.1(10) . . . . ?
C126 N123 C128 C129 9.9(15) . . . . ?
Ag5 N123 C128 C129 -179.1(5) . . . . ?
C133 C128 C129 C130 -0.02(15) . . . . ?
N123 C128 C129 C130 177.0(8) . . . . ?
C128 C129 C130 C131 0.07(16) . . . . ?
C129 C130 C131 O121 -179.91(18) . . . . ?
C129 C130 C131 C132 -0.1(3) . . . . ?
C130 C131 C132 C133 0.2(4) . . . . ?
O121 C131 C132 C133 179.9(3) . . . . ?
C129 C128 C133 C132 0.1(4) . . . . ?
N123 C128 C133 C132 -177.1(8) . . . . ?
C131 C132 C133 C128 -0.1(5) . . . . ?
C130 C131 O121 C134 -176.7(14) . . . . ?
C132 C131 O121 C134 3.6(15) . . . . ?
N122 C122 C136 N124 1(2) . . . . ?
C123 C122 C136 N124 -179.2(13) . . . . ?
C122 C136 N124 C138 171.4(10) . . . . ?
C122 C136 N124 Ag6 -0.4(15) . . . . ?
N122 Ag6 N124 C136 -0.3(9) . . . . ?
N211 Ag6 N124 C136 -117.1(10) . . . . ?
N213 Ag6 N124 C136 143.4(9) . . . . ?
N122 Ag6 N124 C138 -172.3(9) . . . . ?
N211 Ag6 N124 C138 70.8(11) . . . . ?
N213 Ag6 N124 C138 -28.6(9) . . . . ?
C136 N124 C138 C143 177.2(11) . . . . ?
Ag6 N124 C138 C143 -11.6(10) . . . . ?
C136 N124 C138 C139 0.2(16) . . . . ?
Ag6 N124 C138 C139 171.3(6) . . . . ?
C143 C138 C139 C140 -0.05(16) . . . . ?
N124 C138 C139 C140 176.7(9) . . . . ?
C138 C139 C140 C141 0.02(15) . . . . ?
C139 C140 C141 C142 -0.1(4) . . . . ?
C139 C140 C141 O122 -179.9(2) . . . . ?
C140 C141 C142 C143 0.1(5) . . . . ?
O122 C141 C142 C143 -180.0(3) . . . . ?
C139 C138 C143 C142 0.1(3) . . . . ?
N124 C138 C143 C142 -177.0(8) . . . . ?
C141 C142 C143 C138 -0.1(4) . . . . ?
C140 C141 O122 C144 0(2) . . . . ?
C142 C141 O122 C144 -179.5(19) . . . . ?
N153 Ag7 N151 C155 -1.1(9) . . . . ?
N184 Ag7 N151 C155 -125.3(11) . . . . ?
N182 Ag7 N151 C155 141.1(9) . . . . ?
N153 Ag7 N151 N152 178.9(11) . . . . ?
N184 Ag7 N151 N152 54.7(13) . . . . ?
N182 Ag7 N151 N152 -38.9(11) . . . . ?
C155 N151 N152 C152 3.6(19) . . . . ?
Ag7 N151 N152 C152 -176.4(9) . . . . ?
C155 N151 N152 Ag8 -179.6(10) . . . . ?
Ag7 N151 N152 Ag8 0.3(15) . . . . ?
N154 Ag8 N152 N151 -178.7(12) . . . . ?
N214 Ag8 N152 N151 -39.1(13) . . . . ?
N212 Ag8 N152 N151 58.6(13) . . . . ?
N154 Ag8 N152 C152 -2.0(10) . . . . ?
N214 Ag8 N152 C152 137.6(10) . . . . ?
N212 Ag8 N152 C152 -124.7(10) . . . . ?
N152 N151 C155 C154 -3(2) . . . . ?
Ag7 N151 C155 C154 176.6(10) . . . . ?
N152 N151 C155 C156 179.5(12) . . . . ?
Ag7 N151 C155 C156 -0.5(15) . . . . ?
N151 C155 C156 N153 3(2) . . . . ?
C154 C155 C156 N153 -173.5(15) . . . . ?
C155 C156 N153 C158 177.9(11) . . . . ?
C155 C156 N153 Ag7 -4.4(18) . . . . ?
N151 Ag7 N153 C156 2.9(11) . . . . ?
N184 Ag7 N153 C156 145.9(11) . . . . ?
N182 Ag7 N153 C156 -102.1(13) . . . . ?
N151 Ag7 N153 C158 -179(100) . . . . ?
N184 Ag7 N153 C158 -36.5(12) . . . . ?
N182 Ag7 N153 C158 75.5(13) . . . . ?
C156 N153 C158 C159 -11.4(18) . . . . ?
Ag7 N153 C158 C159 171.1(7) . . . . ?
C156 N153 C158 C163 172.2(12) . . . . ?
Ag7 N153 C158 C163 -5.3(12) . . . . ?
N153 C158 C159 C160 -176.4(10) . . . . ?
C163 C158 C159 C160 -0.02(14) . . . . ?
C158 C159 C160 C161 0.01(14) . . . . ?
C159 C160 C161 C162 0.0(3) . . . . ?
C159 C160 C161 O151 180.0(2) . . . . ?
C160 C161 C162 C163 0.1(4) . . . . ?
O151 C161 C162 C163 -179.9(3) . . . . ?
C161 C162 C163 C158 -0.1(4) . . . . ?
N153 C158 C163 C162 176.9(9) . . . . ?
C159 C158 C163 C162 0.1(3) . . . . ?
N214 Ag8 N154 C166 -110.5(11) . . . . ?
N212 Ag8 N154 C166 142.0(10) . . . . ?
N152 Ag8 N154 C166 2.1(10) . . . . ?
N214 Ag8 N154 C168 67.6(12) . . . . ?
N212 Ag8 N154 C168 -39.9(10) . . . . ?
N152 Ag8 N154 C168 -180(100) . . . . ?
C166 N154 C168 C169 4.1(15) . . . . ?
Ag8 N154 C168 C169 -173.9(5) . . . . ?
C166 N154 C168 C173 -171.8(10) . . . . ?
Ag8 N154 C168 C173 10.2(10) . . . . ?
N154 C168 C169 C170 -176.2(7) . . . . ?
C173 C168 C169 C170 -0.03(15) . . . . ?
C168 C169 C170 C171 -0.03(16) . . . . ?
C169 C170 C171 O152 -178.6(7) . . . . ?
C169 C170 C171 C172 0.0(4) . . . . ?
C170 C171 C172 C173 0.0(5) . . . . ?
O152 C171 C172 C173 178.6(8) . . . . ?
C171 C172 C173 C168 -0.1(5) . . . . ?
N154 C168 C173 C172 176.5(7) . . . . ?
C169 C168 C173 C172 0.1(4) . . . . ?
C170 C171 O152 C174 -179.8(15) . . . . ?
C172 C171 O152 C174 1.5(19) . . . . ?
N123 Ag5 N181 N182 -30.8(16) . . . . ?
N183 Ag5 N181 N182 -172.8(14) . . . . ?
N121 Ag5 N181 N182 79.8(13) . . . . ?
N123 Ag5 N181 C185 142.0(10) . . . . ?
N183 Ag5 N181 C185 -0.1(10) . . . . ?
N121 Ag5 N181 C185 -107.5(12) . . . . ?
C185 N181 N182 C182 9(2) . . . . ?
Ag5 N181 N182 C182 -178.4(11) . . . . ?
C185 N181 N182 Ag7 -165.4(11) . . . . ?
Ag5 N181 N182 Ag7 6.9(19) . . . . ?
N153 Ag7 N182 N181 54.1(16) . . . . ?
N151 Ag7 N182 N181 -37.3(14) . . . . ?
N184 Ag7 N182 N181 -178.7(14) . . . . ?
N153 Ag7 N182 C182 -121.2(12) . . . . ?
N151 Ag7 N182 C182 147.3(10) . . . . ?
N184 Ag7 N182 C182 6.0(11) . . . . ?
N181 N182 C182 C183 -6(2) . . . . ?
Ag7 N182 C182 C183 169.4(13) . . . . ?
N181 N182 C182 C196 179.9(15) . . . . ?
Ag7 N182 C182 C196 -4.7(19) . . . . ?
N182 C182 C183 C184 -1(3) . . . . ?
C196 C182 C183 C184 172.7(17) . . . . ?
C182 C183 C184 C185 4(3) . . . . ?
N182 N181 C185 C184 -5(2) . . . . ?
Ag5 N181 C185 C184 -178.9(12) . . . . ?
N182 N181 C185 C186 176.8(14) . . . . ?
Ag5 N181 C185 C186 3.3(19) . . . . ?
C183 C184 C185 N181 -1(2) . . . . ?
C183 C184 C185 C186 176.8(16) . . . . ?
N181 C185 C186 N183 -7(2) . . . . ?
C184 C185 C186 N183 175.1(15) . . . . ?
C185 C186 N183 C188 -177.1(13) . . . . ?
C185 C186 N183 Ag5 6.5(19) . . . . ?
N123 Ag5 N183 C186 -137.6(10) . . . . ?
N181 Ag5 N183 C186 -3.3(10) . . . . ?
N121 Ag5 N183 C186 133.3(10) . . . . ?
N123 Ag5 N183 C188 46.0(12) . . . . ?
N181 Ag5 N183 C188 -179.8(10) . . . . ?
N121 Ag5 N183 C188 -43.2(10) . . . . ?
C186 N183 C188 C193 175.7(11) . . . . ?
Ag5 N183 C188 C193 -8.2(10) . . . . ?
C186 N183 C188 C189 -0.8(16) . . . . ?
Ag5 N183 C188 C189 175.3(5) . . . . ?
N183 C188 C189 C190 176.5(8) . . . . ?
C193 C188 C189 C190 -0.02(14) . . . . ?
C188 C189 C190 C191 0.06(15) . . . . ?
C189 C190 C191 O181 -179.9(2) . . . . ?
C189 C190 C191 C192 -0.1(3) . . . . ?
O181 C191 C192 C193 179.9(3) . . . . ?
C190 C191 C192 C193 0.1(4) . . . . ?
C191 C192 C193 C188 -0.1(5) . . . . ?
N183 C188 C193 C192 -176.7(8) . . . . ?
C189 C188 C193 C192 0.0(3) . . . . ?
C190 C191 O181 C194 10.2(11) . . . . ?
C192 C191 O181 C194 -169.6(11) . . . . ?
C183 C182 C196 N184 -175.9(18) . . . . ?
N182 C182 C196 N184 -2(3) . . . . ?
C182 C196 N184 C198 -177.4(15) . . . . ?
C182 C196 N184 Ag7 8(2) . . . . ?
N153 Ag7 N184 C196 138.6(11) . . . . ?
N151 Ag7 N184 C196 -114.1(13) . . . . ?
N182 Ag7 N184 C196 -7.2(12) . . . . ?
N153 Ag7 N184 C198 -36.0(13) . . . . ?
N151 Ag7 N184 C198 71.3(13) . . . . ?
N182 Ag7 N184 C198 178.3(12) . . . . ?
C196 N184 C198 C203 -175.2(14) . . . . ?
Ag7 N184 C198 C203 -1.4(13) . . . . ?
C196 N184 C198 C199 6(2) . . . . ?
Ag7 N184 C198 C199 179.8(6) . . . . ?
C203 C198 C199 C200 0.01(15) . . . . ?
N184 C198 C199 C200 178.8(11) . . . . ?
C198 C199 C200 C201 -0.07(16) . . . . ?
C199 C200 C201 O182 179.9(3) . . . . ?
C199 C200 C201 C202 0.1(3) . . . . ?
O182 C201 C202 C203 -179.9(3) . . . . ?
C200 C201 C202 C203 -0.1(5) . . . . ?
N184 C198 C203 C202 -179.0(10) . . . . ?
C199 C198 C203 C202 0.0(3) . . . . ?
C201 C202 C203 C198 0.1(5) . . . . ?
C200 C201 O182 C204 -9.0(14) . . . . ?
C202 C201 O182 C204 170.7(13) . . . . ?
N122 Ag6 N211 N212 -35.1(15) . . . . ?
N213 Ag6 N211 N212 -179.9(14) . . . . ?
N124 Ag6 N211 N212 64.0(15) . . . . ?
N122 Ag6 N211 C215 153.8(11) . . . . ?
N213 Ag6 N211 C215 9.0(11) . . . . ?
N124 Ag6 N211 C215 -107.1(14) . . . . ?
C215 N211 N212 C212 1(2) . . . . ?
Ag6 N211 N212 C212 -169.0(11) . . . . ?
C215 N211 N212 Ag8 -179.2(11) . . . . ?
Ag6 N211 N212 Ag8 10.4(18) . . . . ?
N154 Ag8 N212 N211 -37.6(14) . . . . ?
N214 Ag8 N212 N211 -179.4(13) . . . . ?
N152 Ag8 N212 N211 66.5(14) . . . . ?
N154 Ag8 N212 C212 141.9(9) . . . . ?
N214 Ag8 N212 C212 0.1(10) . . . . ?
N152 Ag8 N212 C212 -114.0(11) . . . . ?
N211 N212 C212 C226 -179.7(15) . . . . ?
Ag8 N212 C212 C226 0.8(19) . . . . ?
N211 N212 C212 C213 -3(2) . . . . ?
Ag8 N212 C212 C213 177.5(12) . . . . ?
N212 C212 C213 C214 4(2) . . . . ?
C226 C212 C213 C214 -179.5(17) . . . . ?
C212 C213 C214 C215 -3(3) . . . . ?
N212 N211 C215 C216 -178.4(15) . . . . ?
Ag6 N211 C215 C216 -7(2) . . . . ?
N212 N211 C215 C214 0(3) . . . . ?
Ag6 N211 C215 C214 171.5(14) . . . . ?
C213 C214 C215 N211 1(3) . . . . ?
C213 C214 C215 C216 179.1(17) . . . . ?
N211 C215 C216 N213 -4(3) . . . . ?
C214 C215 C216 N213 178.0(16) . . . . ?
C215 C216 N213 C218 -175.8(14) . . . . ?
C215 C216 N213 Ag6 12(2) . . . . ?
N122 Ag6 N213 C216 -130.7(11) . . . . ?
N211 Ag6 N213 C216 -10.7(10) . . . . ?
N124 Ag6 N213 C216 128.5(10) . . . . ?
N122 Ag6 N213 C218 56.5(12) . . . . ?
N211 Ag6 N213 C218 176.6(10) . . . . ?
N124 Ag6 N213 C218 -44.2(10) . . . . ?
C216 N213 C218 C223 -177.9(12) . . . . ?
Ag6 N213 C218 C223 -6.2(11) . . . . ?
C216 N213 C218 C219 -0.5(18) . . . . ?
Ag6 N213 C218 C219 171.1(5) . . . . ?
C223 C218 C219 C220 0.03(16) . . . . ?
N213 C218 C219 C220 -177.3(9) . . . . ?
C218 C219 C220 C221 -0.08(15) . . . . ?
C219 C220 C221 O211 179.8(2) . . . . ?
C219 C220 C221 C222 0.1(3) . . . . ?
C220 C221 O211 C224 -1.8(12) . . . . ?
C222 C221 O211 C224 177.9(12) . . . . ?
O211 C221 C222 C223 -179.8(3) . . . . ?
C220 C221 C222 C223 -0.1(5) . . . . ?
C219 C218 C223 C222 0.0(4) . . . . ?
N213 C218 C223 C222 177.5(9) . . . . ?
C221 C222 C223 C218 0.1(5) . . . . ?
N212 C212 C226 N214 -2(3) . . . . ?
C213 C212 C226 N214 -178.5(15) . . . . ?
C212 C226 N214 C228 -177.7(13) . . . . ?
C212 C226 N214 Ag8 1.8(19) . . . . ?
N154 Ag8 N214 C226 -125.8(12) . . . . ?
N212 Ag8 N214 C226 -1.0(11) . . . . ?
N152 Ag8 N214 C226 138.2(11) . . . . ?
N154 Ag8 N214 C228 53.7(13) . . . . ?
N212 Ag8 N214 C228 178.4(11) . . . . ?
N152 Ag8 N214 C228 -42.4(11) . . . . ?
C226 N214 C228 C233 175.4(11) . . . . ?
Ag8 N214 C228 C233 -4.0(12) . . . . ?
C226 N214 C228 C229 -3.5(18) . . . . ?
Ag8 N214 C228 C229 177.1(5) . . . . ?
N214 C228 C229 C230 178.8(9) . . . . ?
C233 C228 C229 C230 -0.04(14) . . . . ?
C228 C229 C230 C231 0.10(16) . . . . ?
C229 C230 C231 O212 -179.8(2) . . . . ?
C229 C230 C231 C232 -0.2(3) . . . . ?
C234 O212 C231 C230 1.0(12) . . . . ?
C234 O212 C231 C232 -178.6(12) . . . . ?
C230 C231 C232 C233 0.3(4) . . . . ?
O212 C231 C232 C233 179.9(3) . . . . ?
C231 C232 C233 C228 -0.3(5) . . . . ?
N214 C228 C233 C232 -178.9(9) . . . . ?
C229 C228 C233 C232 0.1(4) . . . . ?
C246 C241 C242 C243 0.0 . . . . ?
C241 C242 C243 C244 0.0 . . . . ?
C242 C243 C244 C245 0.0 . . . . ?
C243 C244 C245 C246 0.0 . . . . ?
C244 C245 C246 C241 0.0 . . . . ?
C242 C241 C246 C245 0.0 . . . . ?
C256 C251 C252 C253 0.0 . . . . ?
C251 C252 C253 C254 0.0 . . . . ?
C252 C253 C254 C255 0.0 . . . . ?
C253 C254 C255 C256 0.0 . . . . ?
C254 C255 C256 C251 0.0 . . . . ?
C252 C251 C256 C255 0.0 . . . . ?
C266 C261 C262 C263 0.0 . . . . ?
C261 C262 C263 C264 0.0 . . . . ?
C262 C263 C264 C265 0.0 . . . . ?
C263 C264 C265 C266 0.0 . . . . ?
C264 C265 C266 C261 0.0 . . . . ?
C262 C261 C266 C265 0.0 . . . . ?
C152 C153 C154 C155 1(2) . . . . ?
N151 C155 C154 C153 1(2) . . . . ?
C156 C155 C154 C153 178.0(13) . . . . ?
C69 C68 C73 C72 -0.1(4) . . . . ?
N63 C68 C73 C72 179.0(8) . . . . ?
C74 O61 C71 C70 -171.6(16) . . . . ?
C74 O61 C71 C72 8.3(17) . . . . ?
C162 C161 O151 C164 157(3) . . . . ?
C160 C161 O151 C164 -23(3) . . . . ?
C68 C73 C72 C71 0.2(5) . . . . ?
O61 C71 C72 C73 179.9(3) . . . . ?
C70 C71 C72 C73 -0.1(4) . . . . ?
N151 N152 C152 C153 -2(2) . . . . ?
Ag8 N152 C152 C153 -178.9(12) . . . . ?
N151 N152 C152 C166 178.7(11) . . . . ?
Ag8 N152 C152 C166 1.6(15) . . . . ?
C154 C153 C152 N152 0(2) . . . . ?
C154 C153 C152 C166 179.2(13) . . . . ?
C73 C68 C69 C70 0.06(15) . . . . ?
N63 C68 C69 C70 -179.1(8) . . . . ?
O61 C71 C70 C69 180.0(2) . . . . ?
C72 C71 C70 C69 0.0(3) . . . . ?
C68 C69 C70 C71 0.00(15) . . . . ?
C168 N154 C166 C152 179.8(10) . . . . ?
Ag8 N154 C166 C152 -2.1(17) . . . . ?
N152 C152 C166 N154 0(2) . . . . ?
C153 C152 C166 N154 -179.2(14) . . . . ?
