#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:21:43 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179106 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/68/4306854.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4306854
loop_
_publ_author_name
'Michela Costa'
'Roberto Della Pergola'
'Alessandro Fumagalli'
'Franco Laschi'
'Serena Losi'
'Piero Macchi'
'Angelo Sironi'
'Piero Zanello'
_publ_section_title
;
Mixed Co-Rh Nitrido-Encapsulated Carbonyl Clusters. Synthesis,
Solid-State Structure, and Electrochemical/EPR Characterization of the
Anions [Co10Rh(N)2(CO)21]3-, [Co10Rh2(N)2(CO)24]2-, and [Co11Rh(N)2(CO)24]2-
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              552
_journal_page_last               560
_journal_paper_doi               10.1021/ic0608288
_journal_volume                  46
_journal_year                    2007
_chemical_formula_sum            'C36 H42 Co10 N5 O22 Rh'
_chemical_formula_weight         1588.96
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.3
_audit_creation_date             2005-07-20T17:47:09-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 102.22(2)
_cell_angle_gamma                90.000(5)
_cell_formula_units_Z            4
_cell_length_a                   17.223(4)
_cell_length_b                   14.600(2)
_cell_length_c                   22.326(6)
_cell_measurement_temperature    293(2)
_cell_volume                     5487(2)
_computing_cell_refinement       'CAD4 Express (Enraf Nonius, 1994)'
_computing_data_collection       'CAD4 Express (Enraf Nonius, 1994)'
_computing_data_reduction        'XCAD4 (Harms & Wocadlo, 1995)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'scintillation LiI'
_diffrn_detector_dtime           1.195
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device       'κ-geometry diffractometer'
_diffrn_measurement_device_type  'Enraf Nonius CAD4'
_diffrn_measurement_method       'non-profiled omega scans'
_diffrn_orient_matrix_type
;
  x-axis points to radiation source
  the matrix is specified in reciprocal space
;
_diffrn_orient_matrix_UB_11      -0.048418
_diffrn_orient_matrix_UB_12      -0.000268
_diffrn_orient_matrix_UB_13      -0.033799
_diffrn_orient_matrix_UB_21      -0.004547
_diffrn_orient_matrix_UB_22      -0.067771
_diffrn_orient_matrix_UB_23      0.004351
_diffrn_orient_matrix_UB_31      -0.03402
_diffrn_orient_matrix_UB_32      0.009337
_diffrn_orient_matrix_UB_33      0.030581
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_av_unetI/netI     0.1136
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            9644
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         3.04
_diffrn_source                   'Enraf Nonius FR590'
_diffrn_standards_decay_%        14
_diffrn_standards_interval_time  240
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.306
_exptl_absorpt_correction_T_max  0.9998
_exptl_absorpt_correction_T_min  0.7031
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details
;
North A.C.T., Phillips D.C. & Mathews F.S. (1968) Acta. Cryst. A24, 351
        Number of psi-scan sets used was   1
        Theta correction was applied.
        Averaged transmission function was used.
        No Fourier smoothing was applied.
;
_exptl_crystal_density_diffrn    1.924
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3136
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_crystal_size_rad          0.1
_refine_diff_density_max         0.989
_refine_diff_density_min         -0.725
_refine_diff_density_rms         0.112
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.96
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     643
_refine_ls_number_reflns         9644
_refine_ls_number_restraints     93
_refine_ls_restrained_S_all      0.956
_refine_ls_R_factor_all          0.1799
_refine_ls_R_factor_gt           0.0487
_refine_ls_shift/su_max          0.038
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0795P)²+8.8117P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1224
_refine_ls_wR_factor_ref         0.163
_reflns_number_gt                4271
_reflns_number_total             9644
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0608288si20060515_060827_3.cif
_cod_data_source_block           mart29
_cod_database_code               4306854
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh Rh 0.21008(4) 0.27972(6) 0.46739(3) 0.0699(3) Uani 1 1 d . . .
Co1 Co 0.32313(7) 0.29458(9) 0.58483(5) 0.0541(3) Uani 1 1 d . . .
Co2 Co 0.32071(8) 0.13260(9) 0.53997(6) 0.0681(4) Uani 1 1 d . . .
Co3 Co 0.43520(7) 0.23247(9) 0.54687(5) 0.0603(4) Uani 1 1 d . . .
Co4 Co 0.34954(7) 0.36627(9) 0.48787(6) 0.0643(4) Uani 1 1 d . . .
Co5 Co 0.29090(9) 0.15106(13) 0.42287(8) 0.0991(6) Uani 1 1 d . . .
Co6 Co 0.40865(8) 0.24816(12) 0.43234(6) 0.0817(5) Uani 1 1 d . . .
Co7 Co 0.27643(8) 0.22005(10) 0.67771(5) 0.0683(4) Uani 1 1 d . . .
Co8 Co 0.26444(7) 0.06993(10) 0.62938(6) 0.0667(4) Uani 1 1 d . . .
Co9 Co 0.17971(7) 0.28569(10) 0.58840(6) 0.0660(4) Uani 1 1 d . . .
Co10 Co 0.16809(7) 0.13332(10) 0.53826(6) 0.0639(4) Uani 1 1 d . . .
N1 N 0.3343(4) 0.2369(5) 0.4851(3) 0.061(2) Uani 1 1 d . . .
N2 N 0.2578(4) 0.1894(5) 0.5930(3) 0.0573(19) Uani 1 1 d . . .
C0 C 0.1049(7) 0.3109(10) 0.4496(5) 0.103(4) Uani 1 1 d . . .
O0 O 0.0407(5) 0.3330(8) 0.4356(4) 0.152(5) Uani 1 1 d . . .
C1 C 0.3036(7) 0.4014(9) 0.6064(5) 0.089(3) Uani 1 1 d . . .
O1 O 0.2975(6) 0.4778(6) 0.6246(5) 0.128(4) Uani 1 1 d . . .
C2 C 0.3141(10) 0.0193(11) 0.5152(8) 0.143(6) Uani 1 1 d . . .
O2 O 0.3151(9) -0.0580(8) 0.5057(7) 0.213(7) Uani 1 1 d . . .
C3 C 0.5352(6) 0.2450(9) 0.5462(5) 0.092(4) Uani 1 1 d . . .
O3 O 0.6017(5) 0.2517(8) 0.5492(4) 0.140(4) Uani 1 1 d . . .
C4 C 0.3917(8) 0.4705(9) 0.5122(7) 0.105(4) Uani 1 1 d . . .
O4 O 0.4209(6) 0.5376(7) 0.5314(7) 0.163(5) Uani 1 1 d . . .
C5 C 0.2594(11) 0.0515(13) 0.3858(10) 0.197(10) Uani 1 1 d . . .
O5 O 0.2401(10) -0.0144(12) 0.3601(9) 0.298(11) Uani 1 1 d . . .
C6 C 0.4980(7) 0.2417(10) 0.4089(5) 0.098(4) Uani 1 1 d . . .
O6 O 0.5572(6) 0.2397(9) 0.3934(5) 0.157(5) Uani 1 1 d . . .
C7 C 0.3290(8) 0.2687(10) 0.7450(6) 0.101(4) Uani 1 1 d . . .
O7 O 0.3678(7) 0.3011(8) 0.7877(4) 0.163(5) Uani 1 1 d . . .
C8 C 0.2972(7) -0.0420(9) 0.6472(6) 0.090(4) Uani 1 1 d . . .
O8 O 0.3170(6) -0.1156(6) 0.6587(5) 0.126(3) Uani 1 1 d . . .
C9 C 0.1270(8) 0.3888(9) 0.5781(6) 0.096(4) Uani 1 1 d . . .
O9 O 0.0909(6) 0.4530(7) 0.5715(6) 0.155(5) Uani 1 1 d . . .
C10 C 0.1086(7) 0.0811(10) 0.4756(6) 0.106(4) Uani 1 1 d . . .
O10 O 0.0708(7) 0.0494(10) 0.4334(5) 0.187(6) Uani 1 1 d . . .
C13 C 0.4334(6) 0.2957(9) 0.6190(5) 0.088(4) Uani 1 1 d . . .
O13 O 0.4787(5) 0.3212(8) 0.6639(4) 0.146(4) Uani 1 1 d . . .
C23 C 0.4358(7) 0.1168(10) 0.5765(6) 0.099(4) Uani 1 1 d . . .
O23 O 0.4753(7) 0.0583(8) 0.6034(6) 0.172(5) Uani 1 1 d . . .
C40 C 0.2491(6) 0.4114(8) 0.4528(5) 0.073(3) Uani 1 1 d . . .
O40 O 0.2164(5) 0.4757(6) 0.4308(5) 0.127(3) Uani 1 1 d . . .
C46 C 0.3901(7) 0.3714(10) 0.4140(6) 0.112(5) Uani 1 1 d . . .
O46 O 0.3942(7) 0.4253(9) 0.3758(5) 0.189(6) Uani 1 1 d . . .
C50 C 0.1986(6) 0.2161(9) 0.3859(5) 0.094(4) Uani 1 1 d . . .
O50 O 0.1545(5) 0.2188(8) 0.3382(4) 0.145(4) Uani 1 1 d . . .
C56 C 0.3540(7) 0.1820(14) 0.3660(6) 0.152(8) Uani 1 1 d . . .
O56 O 0.3521(6) 0.1692(12) 0.3139(5) 0.222(8) Uani 1 1 d . . .
C78 C 0.2691(6) 0.1043(9) 0.7125(5) 0.087(3) Uani 1 1 d . . .
O78 O 0.2690(6) 0.0697(7) 0.7600(4) 0.127(3) Uani 1 1 d . . .
C79 C 0.1818(7) 0.2831(8) 0.6765(5) 0.086(3) Uani 1 1 d . . .
O79 O 0.1402(5) 0.3051(7) 0.7087(4) 0.118(3) Uani 1 1 d . . .
C810 C 0.1619(7) 0.0290(8) 0.5892(5) 0.081(3) Uani 1 1 d . . .
O810 O 0.1178(5) -0.0286(6) 0.5934(4) 0.111(3) Uani 1 1 d . . .
C910 C 0.0891(6) 0.2080(8) 0.5614(5) 0.082(3) Uani 1 1 d . . .
O910 O 0.0212(4) 0.2082(6) 0.5601(4) 0.110(3) Uani 1 1 d . . .
N3 N 0.4698(5) 0.0010(6) 0.2218(4) 0.111(3) Uani 1 1 d D . .
C31T C 0.4993(8) 0.0730(9) 0.2688(6) 0.148(6) Uiso 1 1 d D . .
C32T C 0.4482(9) 0.0466(10) 0.1601(6) 0.169(7) Uiso 1 1 d D . .
C33T C 0.5336(9) -0.0671(11) 0.2210(8) 0.236(11) Uiso 1 1 d D . .
C34T C 0.3983(8) -0.0439(11) 0.2355(7) 0.193(8) Uiso 1 1 d D . .
N4 N 0.5029(5) 0.4340(6) 0.2339(4) 0.088(3) Uani 1 1 d D . .
C41T C 0.4349(15) 0.4872(18) 0.2492(12) 0.172(15) Uiso 0.60(4) 1 d PD . .
C42T C 0.5653(16) 0.4992(19) 0.2213(14) 0.25(2) Uiso 0.60(4) 1 d PD . .
C43T C 0.4731(16) 0.3761(17) 0.1777(12) 0.170(15) Uiso 0.60(4) 1 d PD . .
C44T C 0.5387(17) 0.373(2) 0.2869(11) 0.204(18) Uiso 0.60(4) 1 d PD . .
C45T C 0.540(2) 0.414(3) 0.1820(16) 0.138(19) Uiso 0.40(4) 1 d PD . .
C46T C 0.464(3) 0.520(3) 0.2292(19) 0.17(2) Uiso 0.40(4) 1 d PD . .
C47T C 0.564(3) 0.426(3) 0.2922(18) 0.149(19) Uiso 0.40(4) 1 d PD . .
C48T C 0.443(3) 0.357(3) 0.236(2) 0.27(4) Uiso 0.40(4) 1 d PD . .
N5 N 0.6849(4) 0.7888(6) 0.0275(4) 0.085(3) Uani 1 1 d D . .
C51T C 0.6755(12) 0.6953(13) -0.0015(10) 0.158(11) Uiso 0.65(3) 1 d PD . .
C52T C 0.6278(10) 0.8536(12) -0.0120(9) 0.111(8) Uiso 0.65(3) 1 d PD . .
C53T C 0.7684(10) 0.8216(14) 0.0315(10) 0.165(12) Uiso 0.65(3) 1 d PD . .
C54T C 0.6668(13) 0.7844(16) 0.0901(9) 0.184(14) Uiso 0.65(3) 1 d PD . .
C55T C 0.6480(18) 0.703(2) 0.0521(14) 0.085(13) Uiso 0.35(3) 1 d PD . .
C56T C 0.700(3) 0.758(3) -0.0316(18) 0.16(2) Uiso 0.35(3) 1 d PD . .
C57T C 0.640(3) 0.862(3) 0.028(2) 0.20(3) Uiso 0.35(3) 1 d PD . .
C58T C 0.766(2) 0.793(3) 0.071(2) 0.15(2) Uiso 0.35(3) 1 d PD . .
C1S C 0.2459(9) 0.2072(11) 0.1788(7) 0.115(5) Uani 1 1 d . . .
C2S C 0.2009(8) 0.1243(10) 0.1798(7) 0.135(5) Uani 1 1 d . . .
H2S1 H 0.1452 0.1383 0.1703 0.202 Uiso 1 1 calc R . .
H2S2 H 0.2148 0.0971 0.2198 0.202 Uiso 1 1 calc R . .
H2S3 H 0.2129 0.0821 0.15 0.202 Uiso 1 1 calc R . .
C3S C 0.2137(11) 0.2874(11) 0.2029(9) 0.178(8) Uani 1 1 d . . .
H3S1 H 0.1636 0.2722 0.2128 0.267 Uiso 1 1 calc R . .
H3S2 H 0.2061 0.3352 0.1728 0.267 Uiso 1 1 calc R . .
H3S3 H 0.25 0.3078 0.2392 0.267 Uiso 1 1 calc R . .
O1S O 0.3075(6) 0.2080(8) 0.1621(5) 0.150(4) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
-7 4 6
-8 -2 6
8 2 1
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C0 Rh C50 90.9(5) . . ?
C0 Rh C40 94.2(5) . . ?
C50 Rh C40 104.9(5) . . ?
C0 Rh N1 177.0(5) . . ?
C50 Rh N1 86.4(4) . . ?
C40 Rh N1 87.5(4) . . ?
C0 Rh Co5 132.0(5) . . ?
C50 Rh Co5 45.1(3) . . ?
C40 Rh Co5 112.5(3) . . ?
N1 Rh Co5 45.04(19) . . ?
C0 Rh Co4 137.3(5) . . ?
C50 Rh Co4 106.6(3) . . ?
C40 Rh Co4 44.1(3) . . ?
N1 Rh Co4 44.9(2) . . ?
Co5 Rh Co4 82.80(5) . . ?
C0 Rh Co10 87.2(4) . . ?
C50 Rh Co10 99.7(4) . . ?
C40 Rh Co10 155.4(3) . . ?
N1 Rh Co10 92.3(2) . . ?
Co5 Rh Co10 83.78(6) . . ?
Co4 Rh Co10 125.94(5) . . ?
C0 Rh Co9 80.0(3) . . ?
C50 Rh Co9 149.8(4) . . ?
C40 Rh Co9 104.4(3) . . ?
N1 Rh Co9 101.90(18) . . ?
Co5 Rh Co9 126.22(6) . . ?
Co4 Rh Co9 99.31(5) . . ?
Co10 Rh Co9 51.55(4) . . ?
C0 Rh Co1 128.1(4) . . ?
C50 Rh Co1 139.8(3) . . ?
C40 Rh Co1 84.1(3) . . ?
N1 Rh Co1 54.41(18) . . ?
Co5 Rh Co1 94.92(5) . . ?
Co4 Rh Co1 53.59(4) . . ?
Co10 Rh Co1 75.90(4) . . ?
Co9 Rh Co1 51.02(4) . . ?
C0 Rh Co2 139.4(4) . . ?
C50 Rh Co2 94.9(3) . . ?
C40 Rh Co2 122.6(3) . . ?
N1 Rh Co2 40.1(2) . . ?
Co5 Rh Co2 52.45(5) . . ?
Co4 Rh Co2 78.84(4) . . ?
Co10 Rh Co2 52.21(4) . . ?
Co9 Rh Co2 75.03(4) . . ?
Co1 Rh Co2 50.37(4) . . ?
C1 Co1 C13 97.0(5) . . ?
C1 Co1 N2 123.4(4) . . ?
C13 Co1 N2 121.5(4) . . ?
C1 Co1 N1 130.0(4) . . ?
C13 Co1 N1 96.0(4) . . ?
N2 Co1 N1 88.4(3) . . ?
C1 Co1 Co3 131.5(4) . . ?
C13 Co1 Co3 48.9(3) . . ?
N2 Co1 Co3 104.9(2) . . ?
N1 Co1 Co3 47.97(17) . . ?
C1 Co1 Co9 77.3(4) . . ?
C13 Co1 Co9 154.9(3) . . ?
N2 Co1 Co9 49.9(2) . . ?
N1 Co1 Co9 106.44(17) . . ?
Co3 Co1 Co9 148.64(7) . . ?
C1 Co1 Co4 86.9(4) . . ?
C13 Co1 Co4 89.7(4) . . ?
N2 Co1 Co4 128.5(2) . . ?
N1 Co1 Co4 45.15(19) . . ?
Co3 Co1 Co4 63.79(5) . . ?
Co9 Co1 Co4 114.07(6) . . ?
C1 Co1 Co2 167.4(4) . . ?
C13 Co1 Co2 95.6(4) . . ?
N2 Co1 Co2 49.0(2) . . ?
N1 Co1 Co2 47.14(19) . . ?
Co3 Co1 Co2 58.04(5) . . ?
Co9 Co1 Co2 91.73(6) . . ?
Co4 Co1 Co2 92.20(6) . . ?
C1 Co1 Co7 92.5(4) . . ?
C13 Co1 Co7 97.8(4) . . ?
N2 Co1 Co7 46.5(2) . . ?
N1 Co1 Co7 132.93(19) . . ?
Co3 Co1 Co7 121.29(7) . . ?
Co9 Co1 Co7 58.63(5) . . ?
Co4 Co1 Co7 172.55(7) . . ?
Co2 Co1 Co7 86.77(6) . . ?
C1 Co1 Rh 100.9(4) . . ?
C13 Co1 Rh 141.6(3) . . ?
N2 Co1 Rh 74.7(2) . . ?
N1 Co1 Rh 47.02(17) . . ?
Co3 Co1 Rh 94.97(5) . . ?
Co9 Co1 Rh 63.15(5) . . ?
Co4 Co1 Rh 57.99(4) . . ?
Co2 Co1 Rh 68.21(5) . . ?
Co7 Co1 Rh 114.96(5) . . ?
C2 Co2 N2 126.1(5) . . ?
C2 Co2 C23 90.7(7) . . ?
N2 Co2 C23 115.7(4) . . ?
C2 Co2 N1 122.5(6) . . ?
N2 Co2 N1 101.6(3) . . ?
C23 Co2 N1 96.0(4) . . ?
C2 Co2 Co3 126.0(5) . . ?
N2 Co2 Co3 104.7(2) . . ?
C23 Co2 Co3 47.1(4) . . ?
N1 Co2 Co3 51.9(2) . . ?
C2 Co2 Co8 84.2(5) . . ?
N2 Co2 Co8 47.9(2) . . ?
C23 Co2 Co8 98.5(3) . . ?
N1 Co2 Co8 149.4(2) . . ?
Co3 Co2 Co8 126.84(7) . . ?
C2 Co2 Co1 174.3(5) . . ?
N2 Co2 Co1 48.4(2) . . ?
C23 Co2 Co1 90.8(4) . . ?
N1 Co2 Co1 62.8(2) . . ?
Co3 Co2 Co1 58.42(5) . . ?
Co8 Co2 Co1 90.15(6) . . ?
C2 Co2 Co5 77.9(6) . . ?
N2 Co2 Co5 123.8(2) . . ?
C23 Co2 Co5 113.3(3) . . ?
N1 Co2 Co5 47.2(2) . . ?
Co3 Co2 Co5 89.22(7) . . ?
Co8 Co2 Co5 143.33(8) . . ?
Co1 Co2 Co5 106.49(7) . . ?
C2 Co2 Co10 90.1(5) . . ?
N2 Co2 Co10 47.4(2) . . ?
C23 Co2 Co10 156.2(3) . . ?
N1 Co2 Co10 103.6(2) . . ?
Co3 Co2 Co10 142.77(7) . . ?
Co8 Co2 Co10 57.98(5) . . ?
Co1 Co2 Co10 86.30(6) . . ?
Co5 Co2 Co10 90.06(7) . . ?
C2 Co2 Rh 120.2(7) . . ?
N2 Co2 Rh 70.3(2) . . ?
C23 Co2 Rh 138.1(4) . . ?
N1 Co2 Rh 44.7(2) . . ?
Co3 Co2 Rh 91.04(6) . . ?
Co8 Co2 Rh 111.29(6) . . ?
Co1 Co2 Rh 61.41(4) . . ?
Co5 Co2 Rh 54.96(5) . . ?
Co10 Co2 Rh 58.98(4) . . ?
C3 Co3 C23 99.9(6) . . ?
C3 Co3 C13 98.8(5) . . ?
C23 Co3 C13 98.4(6) . . ?
C3 Co3 N1 135.9(4) . . ?
C23 Co3 N1 102.8(5) . . ?
C13 Co3 N1 114.4(4) . . ?
C3 Co3 Co2 148.9(5) . . ?
C23 Co3 Co2 53.6(4) . . ?
C13 Co3 Co2 101.0(3) . . ?
N1 Co3 Co2 52.7(2) . . ?
C3 Co3 Co1 145.4(4) . . ?
C23 Co3 Co1 99.4(4) . . ?
C13 Co3 Co1 49.9(3) . . ?
N1 Co3 Co1 65.6(2) . . ?
Co2 Co3 Co1 63.54(5) . . ?
C3 Co3 Co6 87.1(3) . . ?
C23 Co3 Co6 116.2(4) . . ?
C13 Co3 Co6 143.4(4) . . ?
N1 Co3 Co6 48.9(2) . . ?
Co2 Co3 Co6 91.13(7) . . ?
Co1 Co3 Co6 109.43(6) . . ?
C3 Co3 Co4 111.7(4) . . ?
C23 Co3 Co4 146.6(4) . . ?
C13 Co3 Co4 87.4(4) . . ?
N1 Co3 Co4 46.3(2) . . ?
Co2 Co3 Co4 93.00(6) . . ?
Co1 Co3 Co4 59.77(5) . . ?
Co6 Co3 Co4 57.30(5) . . ?
C4 Co4 C40 96.4(6) . . ?
C4 Co4 N1 158.6(5) . . ?
C40 Co4 N1 103.1(4) . . ?
C4 Co4 C46 91.7(7) . . ?
C40 Co4 C46 95.7(5) . . ?
N1 Co4 C46 94.8(5) . . ?
C4 Co4 Co6 125.8(4) . . ?
C40 Co4 Co6 118.8(3) . . ?
N1 Co4 Co6 50.2(2) . . ?
C46 Co4 Co6 48.2(4) . . ?
C4 Co4 Co1 103.6(5) . . ?
C40 Co4 Co1 100.8(3) . . ?
N1 Co4 Co1 64.5(2) . . ?
C46 Co4 Co1 155.9(4) . . ?
Co6 Co4 Co1 107.99(7) . . ?
C4 Co4 Co3 110.1(5) . . ?
C40 Co4 Co3 147.9(3) . . ?
N1 Co4 Co3 48.6(2) . . ?
C46 Co4 Co3 101.1(4) . . ?
Co6 Co4 Co3 58.97(5) . . ?
Co1 Co4 Co3 56.44(5) . . ?
C4 Co4 Rh 140.9(4) . . ?
C40 Co4 Rh 51.1(3) . . ?
N1 Co4 Rh 54.0(2) . . ?
C46 Co4 Rh 110.4(5) . . ?
Co6 Co4 Rh 92.02(6) . . ?
Co1 Co4 Rh 68.42(5) . . ?
Co3 Co4 Rh 97.09(6) . . ?
C5 Co5 C50 93.7(7) . . ?
C5 Co5 C56 92.7(10) . . ?
C50 Co5 C56 97.9(6) . . ?
C5 Co5 N1 162.3(8) . . ?
C50 Co5 N1 98.7(4) . . ?
C56 Co5 N1 98.0(6) . . ?
C5 Co5 Co6 135.2(8) . . ?
C50 Co5 Co6 110.6(4) . . ?
C56 Co5 Co6 48.4(5) . . ?
N1 Co5 Co6 50.6(2) . . ?
C5 Co5 Co2 112.3(8) . . ?
C50 Co5 Co2 117.8(4) . . ?
C56 Co5 Co2 133.5(4) . . ?
N1 Co5 Co2 50.5(2) . . ?
Co6 Co5 Co2 89.40(6) . . ?
C5 Co5 Rh 130.4(7) . . ?
C50 Co5 Rh 49.2(4) . . ?
C56 Co5 Rh 120.2(6) . . ?
N1 Co5 Rh 54.3(2) . . ?
Co6 Co5 Rh 92.78(7) . . ?
Co2 Co5 Rh 72.59(6) . . ?
C6 Co6 C56 93.6(6) . . ?
C6 Co6 C46 96.2(6) . . ?
C56 Co6 C46 107.1(7) . . ?
C6 Co6 N1 158.7(4) . . ?
C56 Co6 N1 98.9(5) . . ?
C46 Co6 N1 96.4(4) . . ?
C6 Co6 Co5 135.8(5) . . ?
C56 Co6 Co5 50.0(5) . . ?
C46 Co6 Co5 116.2(4) . . ?
N1 Co6 Co5 49.9(2) . . ?
C6 Co6 Co4 132.7(5) . . ?
C56 Co6 Co4 125.0(4) . . ?
C46 Co6 Co4 50.5(4) . . ?
N1 Co6 Co4 49.6(2) . . ?
Co5 Co6 Co4 91.47(7) . . ?
C6 Co6 Co3 108.7(4) . . ?
C56 Co6 Co3 136.0(6) . . ?
C46 Co6 Co3 107.4(4) . . ?
N1 Co6 Co3 50.9(2) . . ?
Co5 Co6 Co3 90.23(7) . . ?
Co4 Co6 Co3 63.73(5) . . ?
C7 Co7 C79 96.0(6) . . ?
C7 Co7 C78 94.5(6) . . ?
C79 Co7 C78 108.3(5) . . ?
C7 Co7 N2 154.8(5) . . ?
C79 Co7 N2 98.0(4) . . ?
C78 Co7 N2 100.8(4) . . ?
C7 Co7 Co8 137.2(5) . . ?
C79 Co7 Co8 116.5(4) . . ?
C78 Co7 Co8 50.6(4) . . ?
N2 Co7 Co8 50.7(2) . . ?
C7 Co7 Co9 132.1(5) . . ?
C79 Co7 Co9 50.8(3) . . ?
C78 Co7 Co9 125.7(3) . . ?
N2 Co7 Co9 49.8(2) . . ?
Co8 Co7 Co9 90.68(6) . . ?
C7 Co7 Co1 109.0(4) . . ?
C79 Co7 Co1 101.4(3) . . ?
C78 Co7 Co1 139.7(4) . . ?
N2 Co7 Co1 47.6(2) . . ?
Co8 Co7 Co1 91.98(6) . . ?
Co9 Co7 Co1 58.22(5) . . ?
C8 Co8 C810 92.1(5) . . ?
C8 Co8 C78 94.5(6) . . ?
C810 Co8 C78 112.7(5) . . ?
C8 Co8 N2 159.2(5) . . ?
C810 Co8 N2 96.9(4) . . ?
C78 Co8 N2 99.2(4) . . ?
C8 Co8 Co7 138.5(4) . . ?
C810 Co8 Co7 118.4(3) . . ?
C78 Co8 Co7 49.4(4) . . ?
N2 Co8 Co7 50.2(2) . . ?
C8 Co8 Co10 130.9(4) . . ?
C810 Co8 Co10 49.1(4) . . ?
C78 Co8 Co10 125.1(4) . . ?
N2 Co8 Co10 49.6(2) . . ?
Co7 Co8 Co10 90.39(6) . . ?
C8 Co8 Co2 110.7(4) . . ?
C810 Co8 Co2 102.2(4) . . ?
C78 Co8 Co2 135.9(4) . . ?
N2 Co8 Co2 49.0(2) . . ?
Co7 Co8 Co2 90.76(6) . . ?
Co10 Co8 Co2 62.12(5) . . ?
C9 Co9 C910 95.9(6) . . ?
C9 Co9 N2 165.8(5) . . ?
C910 Co9 N2 95.6(4) . . ?
C9 Co9 C79 92.7(5) . . ?
C910 Co9 C79 98.3(4) . . ?
N2 Co9 C79 93.8(4) . . ?
C9 Co9 Co10 136.3(5) . . ?
C910 Co9 Co10 49.1(3) . . ?
N2 Co9 Co10 50.2(2) . . ?
C79 Co9 Co10 114.7(4) . . ?
C9 Co9 Co1 116.2(4) . . ?
C910 Co9 Co1 140.0(3) . . ?
N2 Co9 Co1 49.9(2) . . ?
C79 Co9 Co1 103.0(3) . . ?
Co10 Co9 Co1 91.04(6) . . ?
C9 Co9 Co7 132.4(5) . . ?
C910 Co9 Co7 112.6(3) . . ?
N2 Co9 Co7 48.8(2) . . ?
C79 Co9 Co7 47.5(3) . . ?
Co10 Co9 Co7 89.58(6) . . ?
Co1 Co9 Co7 63.15(5) . . ?
C9 Co9 Rh 95.5(4) . . ?
C910 Co9 Rh 89.1(3) . . ?
N2 Co9 Rh 76.4(2) . . ?
C79 Co9 Rh 168.3(3) . . ?
Co10 Co9 Rh 63.86(5) . . ?
Co1 Co9 Rh 65.83(4) . . ?
Co7 Co9 Rh 121.14(6) . . ?
C10 Co10 C910 97.9(6) . . ?
C10 Co10 C810 91.8(6) . . ?
C910 Co10 C810 99.3(4) . . ?
C10 Co10 N2 162.8(5) . . ?
C910 Co10 N2 96.2(4) . . ?
C810 Co10 N2 95.6(4) . . ?
C10 Co10 Co9 137.7(5) . . ?
C910 Co10 Co9 49.9(4) . . ?
C810 Co10 Co9 117.0(3) . . ?
N2 Co10 Co9 50.1(2) . . ?
C10 Co10 Co8 132.1(5) . . ?
C910 Co10 Co8 112.3(3) . . ?
C810 Co10 Co8 48.5(3) . . ?
N2 Co10 Co8 48.9(2) . . ?
Co9 Co10 Co8 89.34(6) . . ?
C10 Co10 Co2 115.5(4) . . ?
C910 Co10 Co2 140.6(4) . . ?
C810 Co10 Co2 99.8(3) . . ?
N2 Co10 Co2 47.9(2) . . ?
Co9 Co10 Co2 90.69(6) . . ?
Co8 Co10 Co2 59.90(5) . . ?
C10 Co10 Rh 93.3(4) . . ?
C910 Co10 Rh 90.1(3) . . ?
C810 Co10 Rh 168.6(3) . . ?
N2 Co10 Rh 76.7(2) . . ?
Co9 Co10 Rh 64.59(5) . . ?
Co8 Co10 Rh 121.68(6) . . ?
Co2 Co10 Rh 68.81(5) . . ?
Co5 N1 Co4 135.0(4) . . ?
Co5 N1 Co6 79.6(3) . . ?
Co4 N1 Co6 80.2(3) . . ?
Co5 N1 Co3 129.7(4) . . ?
Co4 N1 Co3 85.1(3) . . ?
Co6 N1 Co3 80.2(3) . . ?
Co5 N1 Co2 82.3(3) . . ?
Co4 N1 Co2 140.2(4) . . ?
Co6 N1 Co2 128.3(4) . . ?
Co3 N1 Co2 75.3(2) . . ?
Co5 N1 Rh 80.7(3) . . ?
Co4 N1 Rh 81.1(3) . . ?
Co6 N1 Rh 128.3(3) . . ?
Co3 N1 Rh 144.9(4) . . ?
Co2 N1 Rh 95.3(3) . . ?
Co5 N1 Co1 143.5(4) . . ?
Co4 N1 Co1 70.3(2) . . ?
Co6 N1 Co1 136.5(4) . . ?
Co3 N1 Co1 66.4(2) . . ?
Co2 N1 Co1 70.1(2) . . ?
Rh N1 Co1 78.6(2) . . ?
Co7 N2 Co8 79.1(3) . . ?
Co7 N2 Co9 81.4(3) . . ?
Co8 N2 Co9 131.5(3) . . ?
Co7 N2 Co1 85.9(3) . . ?
Co8 N2 Co1 141.1(4) . . ?
Co9 N2 Co1 80.2(3) . . ?
Co7 N2 Co10 132.1(3) . . ?
Co8 N2 Co10 81.4(3) . . ?
Co9 N2 Co10 79.7(3) . . ?
Co1 N2 Co10 132.7(4) . . ?
Co7 N2 Co2 134.8(4) . . ?
Co8 N2 Co2 83.1(3) . . ?
Co9 N2 Co2 138.2(4) . . ?
Co1 N2 Co2 82.6(2) . . ?
Co10 N2 Co2 84.8(3) . . ?
O0 C0 Rh 175.9(10) . . ?
O1 C1 Co1 173.5(11) . . ?
O2 C2 Co2 172(2) . . ?
O3 C3 Co3 176.1(10) . . ?
O4 C4 Co4 176.3(15) . . ?
O5 C5 Co5 178(3) . . ?
O6 C6 Co6 178.3(14) . . ?
O7 C7 Co7 175.6(12) . . ?
O8 C8 Co8 178.6(11) . . ?
O9 C9 Co9 177.5(13) . . ?
O10 C10 Co10 177.4(14) . . ?
O13 C13 Co3 138.9(9) . . ?
O13 C13 Co1 139.9(9) . . ?
Co3 C13 Co1 81.2(4) . . ?
O23 C23 Co3 145.3(12) . . ?
O23 C23 Co2 135.4(12) . . ?
Co3 C23 Co2 79.3(5) . . ?
O40 C40 Co4 142.7(10) . . ?
O40 C40 Rh 132.4(9) . . ?
Co4 C40 Rh 84.8(4) . . ?
O46 C46 Co6 140.9(12) . . ?
O46 C46 Co4 137.5(12) . . ?
Co6 C46 Co4 81.3(5) . . ?
O50 C50 Co5 137.7(11) . . ?
O50 C50 Rh 136.6(10) . . ?
Co5 C50 Rh 85.7(4) . . ?
O56 C56 Co6 141.4(16) . . ?
O56 C56 Co5 136.7(15) . . ?
Co6 C56 Co5 81.6(5) . . ?
O78 C78 Co7 140.7(11) . . ?
O78 C78 Co8 139.3(11) . . ?
Co7 C78 Co8 80.0(4) . . ?
O79 C79 Co7 141.1(10) . . ?
O79 C79 Co9 137.0(10) . . ?
Co7 C79 Co9 81.6(4) . . ?
O810 C810 Co8 139.0(10) . . ?
O810 C810 Co10 138.6(10) . . ?
Co8 C810 Co10 82.4(5) . . ?
O910 C910 Co10 140.3(11) . . ?
O910 C910 Co9 138.8(10) . . ?
Co10 C910 Co9 81.0(4) . . ?
C34T N3 C33T 110.8(6) . . ?
C34T N3 C31T 109.9(5) . . ?
C33T N3 C31T 109.7(5) . . ?
C34T N3 C32T 109.2(5) . . ?
C33T N3 C32T 109.0(5) . . ?
C31T N3 C32T 108.2(5) . . ?
C46T N4 C45T 113.3(19) . . ?
C46T N4 C47T 111.9(18) . . ?
C45T N4 C47T 109.0(18) . . ?
C46T N4 C41T 34.6(19) . . ?
C45T N4 C41T 140.6(18) . . ?
C47T N4 C41T 106(2) . . ?
C46T N4 C42T 77(2) . . ?
C45T N4 C42T 61.7(15) . . ?
C47T N4 C42T 79.4(19) . . ?
C41T N4 C42T 109.7(6) . . ?
C46T N4 C44T 134(2) . . ?
C45T N4 C44T 109.2(18) . . ?
C47T N4 C44T 34.2(18) . . ?
C41T N4 C44T 109.7(6) . . ?
C42T N4 C44T 109.4(6) . . ?
C46T N4 C43T 111(2) . . ?
C45T N4 C43T 50.5(15) . . ?
C47T N4 C43T 136.9(19) . . ?
C41T N4 C43T 109.5(6) . . ?
C42T N4 C43T 109.2(6) . . ?
C44T N4 C43T 109.3(6) . . ?
C46T N4 C48T 109.6(18) . . ?
C45T N4 C48T 107.0(18) . . ?
C47T N4 C48T 105.6(18) . . ?
C41T N4 C48T 79(2) . . ?
C42T N4 C48T 168.7(19) . . ?
C44T N4 C48T 73(2) . . ?
C43T N4 C48T 60.2(19) . . ?
C46T C41T N4 67(4) . . ?
C46T C41T C48T 113(5) . . ?
N4 C41T C48T 51.2(16) . . ?
N4 C42T C45T 58.0(19) . . ?
N4 C42T C46T 49.3(18) . . ?
C45T C42T C46T 92(3) . . ?
N4 C42T C47T 50.1(16) . . ?
C45T C42T C47T 88(2) . . ?
C46T C42T C47T 80(2) . . ?
C45T C43T N4 63(2) . . ?
C45T C43T C48T 119(4) . . ?
N4 C43T C48T 61(2) . . ?
C47T C44T N4 72(4) . . ?
C47T C44T C48T 124(5) . . ?
N4 C44T C48T 54.2(18) . . ?
C43T C45T N4 66(2) . . ?
C43T C45T C42T 123(4) . . ?
N4 C45T C42T 60.4(18) . . ?
C41T C46T N4 78(4) . . ?
C41T C46T C42T 128(5) . . ?
N4 C46T C42T 53.6(17) . . ?
C44T C47T N4 74(4) . . ?
C44T C47T C42T 118(5) . . ?
N4 C47T C42T 50.6(15) . . ?
C43T C48T N4 59(2) . . ?
C43T C48T C44T 95(3) . . ?
N4 C48T C44T 52.8(17) . . ?
C43T C48T C41T 90(3) . . ?
N4 C48T C41T 49.8(16) . . ?
C44T C48T C41T 82(2) . . ?
C57T N5 C56T 118(2) . . ?
C57T N5 C54T 78(2) . . ?
C56T N5 C54T 159.9(18) . . ?
C57T N5 C53T 107(2) . . ?
C56T N5 C53T 78.5(17) . . ?
C54T N5 C53T 110.2(6) . . ?
C57T N5 C51T 137(2) . . ?
C56T N5 C51T 50.4(17) . . ?
C54T N5 C51T 109.7(6) . . ?
C53T N5 C51T 109.3(5) . . ?
C57T N5 C52T 36(2) . . ?
C56T N5 C52T 83.2(19) . . ?
C54T N5 C52T 109.5(5) . . ?
C53T N5 C52T 109.5(5) . . ?
C51T N5 C52T 108.7(5) . . ?
C57T N5 C58T 115(2) . . ?
C56T N5 C58T 106.0(18) . . ?
C54T N5 C58T 75.5(17) . . ?
C53T N5 C58T 37.9(15) . . ?
C51T N5 C58T 108.4(18) . . ?
C52T N5 C58T 137.9(17) . . ?
C57T N5 C55T 111.7(19) . . ?
C56T N5 C55T 103.6(17) . . ?
C54T N5 C55T 57.1(12) . . ?
C53T N5 C55T 133.8(14) . . ?
C51T N5 C55T 53.5(12) . . ?
C52T N5 C55T 116.6(13) . . ?
C58T N5 C55T 101.4(16) . . ?
C56T C51T C55T 128(3) . . ?
C56T C51T N5 63(2) . . ?
C55T C51T N5 65.4(15) . . ?
C57T C52T N5 60(3) . . ?
C57T C52T C56T 107(4) . . ?
N5 C52T C56T 47.5(13) . . ?
C58T C53T N5 72(3) . . ?
C58T C53T C56T 109(4) . . ?
N5 C53T C56T 50.0(14) . . ?
C55T C54T N5 63.7(15) . . ?
C55T C54T C57T 94(2) . . ?
N5 C54T C57T 46.5(17) . . ?
C55T C54T C58T 91(2) . . ?
N5 C54T C58T 52.8(15) . . ?
C57T C54T C58T 82.5(19) . . ?
C51T C55T C54T 119(3) . . ?
C51T C55T N5 61.2(15) . . ?
C54T C55T N5 59.2(14) . . ?
C51T C56T N5 66(2) . . ?
C51T C56T C53T 101(3) . . ?
N5 C56T C53T 51.6(14) . . ?
C51T C56T C52T 96(3) . . ?
N5 C56T C52T 49.3(14) . . ?
C53T C56T C52T 79.2(17) . . ?
C52T C57T N5 84(4) . . ?
C52T C57T C54T 132(4) . . ?
N5 C57T C54T 55.7(17) . . ?
C53T C58T N5 70(3) . . ?
C53T C58T C54T 117(4) . . ?
N5 C58T C54T 51.7(14) . . ?
O1S C1S C2S 121.8(15) . . ?
O1S C1S C3S 123.0(16) . . ?
C2S C1S C3S 115.1(14) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh C0 1.829(12) . ?
Rh C50 2.015(11) . ?
Rh C40 2.084(11) . ?
Rh N1 2.183(7) . ?
Rh Co5 2.6533(19) . ?
Rh Co4 2.6665(16) . ?
Rh Co10 2.8424(16) . ?
Rh Co9 2.8598(16) . ?
Rh Co1 2.9243(16) . ?
Rh Co2 3.0923(17) . ?
Co1 C1 1.687(14) . ?
Co1 C13 1.891(11) . ?
Co1 N2 1.936(7) . ?
Co1 N1 2.426(7) . ?
Co1 Co3 2.4409(17) . ?
Co1 Co9 2.4917(17) . ?
Co1 Co4 2.5307(18) . ?
Co1 Co2 2.5650(18) . ?
Co1 Co7 2.6149(18) . ?
Co2 C2 1.741(16) . ?
Co2 N2 1.951(7) . ?
Co2 C23 1.991(13) . ?
Co2 N1 2.000(8) . ?
Co2 Co3 2.4309(19) . ?
Co2 Co8 2.5652(19) . ?
Co2 Co5 2.570(2) . ?
Co2 Co10 2.6208(18) . ?
Co3 C3 1.735(11) . ?
Co3 C23 1.813(13) . ?
Co3 C13 1.862(11) . ?
Co3 N1 1.978(7) . ?
Co3 Co6 2.5111(19) . ?
Co3 Co4 2.6278(18) . ?
Co4 C4 1.724(14) . ?
Co4 C40 1.862(11) . ?
Co4 N1 1.906(8) . ?
Co4 C46 1.925(12) . ?
Co4 Co6 2.4662(19) . ?
Co5 C5 1.704(17) . ?
Co5 C50 1.886(11) . ?
Co5 C56 1.893(15) . ?
Co5 N1 1.902(7) . ?
Co5 Co6 2.447(2) . ?
Co6 C6 1.730(12) . ?
Co6 C56 1.849(15) . ?
Co6 C46 1.859(15) . ?
Co6 N1 1.921(7) . ?
Co7 C7 1.734(13) . ?
Co7 C79 1.866(11) . ?
Co7 C78 1.876(12) . ?
Co7 N2 1.903(7) . ?
Co7 Co8 2.432(2) . ?
Co7 Co9 2.5025(19) . ?
Co8 C8 1.747(13) . ?
Co8 C810 1.900(12) . ?
Co8 C78 1.909(11) . ?
Co8 N2 1.917(8) . ?
Co8 Co10 2.5139(19) . ?
Co9 C9 1.748(13) . ?
Co9 C910 1.921(11) . ?
Co9 N2 1.933(7) . ?
Co9 C79 1.961(10) . ?
Co9 Co10 2.479(2) . ?
Co10 C10 1.727(14) . ?
Co10 C910 1.899(11) . ?
Co10 C810 1.917(12) . ?
Co10 N2 1.937(7) . ?
C0 O0 1.130(12) . ?
C1 O1 1.199(13) . ?
C2 O2 1.149(15) . ?
C3 O3 1.138(11) . ?
C4 O4 1.142(14) . ?
C5 O5 1.133(17) . ?
C6 O6 1.144(12) . ?
C7 O7 1.143(13) . ?
C8 O8 1.140(12) . ?
C9 O9 1.117(13) . ?
C10 O10 1.125(13) . ?
C13 O13 1.193(12) . ?
C23 O23 1.173(13) . ?
C40 O40 1.151(11) . ?
C46 O46 1.172(14) . ?
C50 O50 1.172(11) . ?
C56 O56 1.173(13) . ?
C78 O78 1.174(12) . ?
C79 O79 1.163(11) . ?
C810 O810 1.150(12) . ?
C910 O910 1.163(10) . ?
N3 C34T 1.483(10) . ?
N3 C33T 1.485(11) . ?
N3 C31T 1.495(10) . ?
N3 C32T 1.504(10) . ?
N4 C46T 1.42(4) . ?
N4 C45T 1.47(4) . ?
N4 C47T 1.50(4) . ?
N4 C41T 1.50(2) . ?
N4 C42T 1.51(2) . ?
N4 C44T 1.51(2) . ?
N4 C43T 1.51(2) . ?
N4 C48T 1.53(4) . ?
C41T C46T 0.87(5) . ?
C41T C48T 1.93(5) . ?
C42T C45T 1.53(4) . ?
C42T C46T 1.82(4) . ?
C42T C47T 1.92(4) . ?
C43T C45T 1.27(4) . ?
C43T C48T 1.53(5) . ?
C44T C47T 0.88(5) . ?
C44T C48T 1.81(5) . ?
N5 C57T 1.31(4) . ?
N5 C56T 1.47(4) . ?
N5 C54T 1.496(16) . ?
N5 C53T 1.500(16) . ?
N5 C51T 1.505(16) . ?
N5 C52T 1.508(16) . ?
N5 C58T 1.52(4) . ?
N5 C55T 1.56(3) . ?
C51T C56T 1.27(4) . ?
C51T C55T 1.38(3) . ?
C52T C57T 0.88(5) . ?
C52T C56T 1.97(5) . ?
C53T C58T 0.98(4) . ?
C53T C56T 1.88(4) . ?
C54T C55T 1.46(3) . ?
C54T C57T 1.77(4) . ?
C54T C58T 1.85(4) . ?
C1S O1S 1.197(14) . ?
C1S C2S 1.441(18) . ?
C1S C3S 1.447(19) . ?
