#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:37:04 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179119 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/81/4308142.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4308142
loop_
_publ_author_name
'Wei-Zhong Chen'
'John D. Protasiewicz'
'Stephen A. Davis'
'James B. Updegraff'
'Li-Qing Ma'
'Phillip E. Fanwick'
'Tong Ren'
_publ_contact_author_address
; Department of Chemistry 
  Purdue University 
  560 Oval Drive
  West Lafayette, IN 47906 
  USA 
;
_publ_contact_author_email       tren@purdue.edu
_publ_contact_author_fax         '(765) 494-0239'
_publ_contact_author_name        'Dr. Ren, Tong'
_publ_contact_author_phone       '(765) 494-5466'
_publ_section_title
;
Olefin Metathesis as an Inorganic Synthetic Tool: Cross and Ring Closing
Metathesis Reactions of Diruthenium-Bound ω-Alkene-α-carboxylates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3775
_journal_page_last               3782
_journal_paper_doi               10.1021/ic070123l
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         'C40 H36 Cl9 N4 O5 Ru2'
_chemical_formula_sum            'C40 H36 Cl9 N4 O5 Ru2'
_chemical_formula_weight         1173.92
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.329(2)
_cell_angle_beta                 96.638(2)
_cell_angle_gamma                106.7400(10)
_cell_formula_units_Z            2
_cell_length_a                   11.3739(4)
_cell_length_b                   12.6997(4)
_cell_length_c                   17.7184(8)
_cell_measurement_reflns_used    9638
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.23
_cell_measurement_theta_min      2.48
_cell_volume                     2265.91(15)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker SMART APEX2 CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0229
_diffrn_reflns_av_sigmaI/netI    0.0226
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            38908
_diffrn_reflns_theta_full        28.24
_diffrn_reflns_theta_max         28.24
_diffrn_reflns_theta_min         1.92
_exptl_absorpt_coefficient_mu    1.245
_exptl_absorpt_correction_T_max  0.9290
_exptl_absorpt_correction_T_min  0.6628
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'AXScale in Apex2 (Bruker, 2004)'
_exptl_crystal_colour            'Dark red'
_exptl_crystal_density_diffrn    1.721
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       'irregular Bolck'
_exptl_crystal_F_000             1170
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.967
_refine_diff_density_min         -0.821
_refine_diff_density_rms         0.081
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.027
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     541
_refine_ls_number_reflns         11138
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.027
_refine_ls_R_factor_all          0.0310
_refine_ls_R_factor_gt           0.0261
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0307P)²+2.6300P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0648
_refine_ls_wR_factor_ref         0.0675
_reflns_number_gt                9916
_reflns_number_total             11138
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic070123l-file002_5.cif
_cod_data_source_block           comp3b
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        2265.90(15)
_cod_database_code               4308142
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.083795(15) 0.407634(13) 0.206419(9) 0.01276(4) Uani 1 1 d . . .
Ru2 Ru 0.069968(14) 0.575200(13) 0.184714(9) 0.01226(4) Uani 1 1 d . . .
N1 N -0.04160(16) 0.41795(15) 0.27914(10) 0.0151(3) Uani 1 1 d . . .
N2 N -0.03780(16) 0.59638(15) 0.26988(10) 0.0147(3) Uani 1 1 d . . .
N3 N 0.23439(16) 0.51161(14) 0.30059(10) 0.0145(3) Uani 1 1 d . . .
N4 N 0.23451(16) 0.67659(14) 0.27182(10) 0.0147(3) Uani 1 1 d . . .
O1 O -0.06331(14) 0.30236(12) 0.10944(9) 0.0173(3) Uani 1 1 d . . .
O2 O -0.09245(14) 0.46346(12) 0.09677(8) 0.0169(3) Uani 1 1 d . . .
O3 O 0.19895(14) 0.39292(13) 0.12583(9) 0.0180(3) Uani 1 1 d . . .
O4 O 0.17208(14) 0.54516(13) 0.09726(9) 0.0169(3) Uani 1 1 d . . .
O5 O 0.09845(15) 0.22013(13) 0.19975(9) 0.0209(3) Uani 1 1 d . . .
Cl1 Cl 0.02756(5) 0.72964(4) 0.14183(3) 0.01724(9) Uani 1 1 d . . .
Cl2 Cl -0.42106(5) 0.72993(6) 0.30119(4) 0.03322(13) Uani 1 1 d . . .
Cl3 Cl 0.05220(6) 1.03943(5) 0.41625(3) 0.02682(12) Uani 1 1 d . . .
Cl4 Cl 0.38820(6) 1.02523(5) 0.17775(4) 0.03194(13) Uani 1 1 d . . .
Cl5 Cl 0.40698(6) 1.09251(5) 0.49471(3) 0.02717(12) Uani 1 1 d . . .
Cl6 Cl 0.23324(6) 0.33553(5) 0.52429(3) 0.02801(12) Uani 1 1 d . . .
Cl7 Cl 0.59711(5) 0.35935(5) 0.35555(4) 0.02884(12) Uani 1 1 d . . .
Cl8 Cl -0.14875(6) 0.31085(5) 0.52490(3) 0.03002(13) Uani 1 1 d . . .
Cl9 Cl -0.30473(6) -0.01279(5) 0.21809(4) 0.03034(13) Uani 1 1 d . . .
C1 C 0.21182(19) 0.45914(18) 0.08385(12) 0.0168(4) Uani 1 1 d . . .
C2 C 0.28462(19) 0.62542(17) 0.31485(12) 0.0152(4) Uani 1 1 d . . .
H2 H 0.3584 0.6717 0.3570 0.018 Uiso 1 1 calc R . .
C3 C -0.07889(19) 0.51075(17) 0.29758(12) 0.0153(4) Uani 1 1 d . . .
H3 H -0.1370 0.5158 0.3318 0.018 Uiso 1 1 calc R . .
C4 C -0.12362(19) 0.35284(18) 0.07580(12) 0.0167(4) Uani 1 1 d . . .
C5 C 0.29714(19) 0.46230(17) 0.34769(12) 0.0154(4) Uani 1 1 d . . .
C6 C 0.4068(2) 0.44123(18) 0.33115(13) 0.0181(4) Uani 1 1 d . . .
H6 H 0.4431 0.4622 0.2900 0.022 Uiso 1 1 calc R . .
C7 C 0.46161(19) 0.38900(18) 0.37615(13) 0.0196(4) Uani 1 1 d . . .
C8 C 0.4114(2) 0.35711(18) 0.43669(13) 0.0200(4) Uani 1 1 d . . .
H8 H 0.4508 0.3220 0.4672 0.024 Uiso 1 1 calc R . .
C9 C 0.3018(2) 0.37836(18) 0.45104(12) 0.0189(4) Uani 1 1 d . . .
C10 C 0.2439(2) 0.43067(17) 0.40758(12) 0.0172(4) Uani 1 1 d . . .
H10 H 0.1689 0.4447 0.4186 0.021 Uiso 1 1 calc R . .
C11 C -0.09971(19) 0.32937(18) 0.30956(12) 0.0157(4) Uani 1 1 d . . .
C12 C -0.09583(19) 0.35930(18) 0.39269(13) 0.0175(4) Uani 1 1 d . . .
H12 H -0.0516 0.4379 0.4298 0.021 Uiso 1 1 calc R . .
C13 C -0.1576(2) 0.27253(19) 0.42042(13) 0.0199(4) Uani 1 1 d . . .
C14 C -0.2243(2) 0.15809(19) 0.36823(14) 0.0216(4) Uani 1 1 d . . .
H14 H -0.2689 0.1003 0.3878 0.026 Uiso 1 1 calc R . .
C15 C -0.2241(2) 0.13038(18) 0.28576(14) 0.0207(4) Uani 1 1 d . . .
C16 C -0.1620(2) 0.21382(18) 0.25548(13) 0.0189(4) Uani 1 1 d . . .
H16 H -0.1620 0.1925 0.1991 0.023 Uiso 1 1 calc R . .
C17 C -0.08696(19) 0.69073(18) 0.29560(12) 0.0155(4) Uani 1 1 d . . .
C18 C -0.2161(2) 0.66643(18) 0.28372(13) 0.0185(4) Uani 1 1 d . . .
H18 H -0.2734 0.5883 0.2549 0.022 Uiso 1 1 calc R . .
C19 C -0.2594(2) 0.7593(2) 0.31500(14) 0.0217(4) Uani 1 1 d . . .
C20 C -0.1797(2) 0.8740(2) 0.35642(14) 0.0223(4) Uani 1 1 d . . .
H20 H -0.2114 0.9359 0.3783 0.027 Uiso 1 1 calc R . .
C21 C -0.0516(2) 0.89543(18) 0.36490(12) 0.0196(4) Uani 1 1 d . . .
C22 C -0.0039(2) 0.80592(18) 0.33506(12) 0.0175(4) Uani 1 1 d . . .
H22 H 0.0845 0.8229 0.3414 0.021 Uiso 1 1 calc R . .
C23 C 0.29454(18) 0.80085(17) 0.29362(12) 0.0153(4) Uani 1 1 d . . .
C24 C 0.31701(19) 0.84589(18) 0.23230(13) 0.0175(4) Uani 1 1 d . . .
H24 H 0.2982 0.7945 0.1769 0.021 Uiso 1 1 calc R . .
C25 C 0.3671(2) 0.96677(19) 0.25385(14) 0.0210(4) Uani 1 1 d . . .
C26 C 0.3984(2) 1.04526(19) 0.33399(14) 0.0216(4) Uani 1 1 d . . .
H26 H 0.4339 1.1281 0.3474 0.026 Uiso 1 1 calc R . .
C27 C 0.3758(2) 0.99795(18) 0.39338(13) 0.0201(4) Uani 1 1 d . . .
C28 C 0.32451(19) 0.87735(18) 0.37497(12) 0.0171(4) Uani 1 1 d . . .
H28 H 0.3100 0.8471 0.4170 0.020 Uiso 1 1 calc R . .
C29 C 0.2776(2) 0.43516(19) 0.01484(13) 0.0210(4) Uani 1 1 d . . .
H29A H 0.3641 0.4938 0.0328 0.025 Uiso 1 1 calc R . .
H29B H 0.2327 0.4471 -0.0314 0.025 Uiso 1 1 calc R . .
C30 C 0.2859(2) 0.3120(2) -0.01541(15) 0.0264(5) Uani 1 1 d . . .
H30A H 0.3355 0.3007 0.0293 0.032 Uiso 1 1 calc R . .
H30B H 0.2001 0.2523 -0.0317 0.032 Uiso 1 1 calc R . .
C31 C 0.3467(3) 0.2946(2) -0.08641(15) 0.0320(5) Uani 1 1 d . . .
H31 H 0.3053 0.2986 -0.1346 0.038 Uiso 1 1 calc R . .
C32 C 0.4535(3) 0.2741(3) -0.08696(17) 0.0388(6) Uani 1 1 d . . .
H32A H 0.4975 0.2695 -0.0398 0.047 Uiso 1 1 calc R . .
H32B H 0.4867 0.2639 -0.1345 0.047 Uiso 1 1 calc R . .
C33 C -0.2375(2) 0.27360(18) 0.00838(12) 0.0193(4) Uani 1 1 d . . .
H33A H -0.2100 0.2340 -0.0405 0.023 Uiso 1 1 calc R . .
H33B H -0.2840 0.3220 -0.0062 0.023 Uiso 1 1 calc R . .
C34 C -0.3252(2) 0.1805(2) 0.03258(16) 0.0338(6) Uani 1 1 d . . .
H34A H -0.3941 0.1268 -0.0157 0.041 Uiso 1 1 calc R . .
H34B H -0.2774 0.1329 0.0470 0.041 Uiso 1 1 calc R . .
C35 C -0.3822(3) 0.2249(4) 0.1011(2) 0.0562(10) Uani 1 1 d . . .
H35 H -0.4240 0.1696 0.1235 0.067 Uiso 1 1 calc R . .
C36 C -0.3807(3) 0.3364(4) 0.1351(2) 0.0623(10) Uani 1 1 d . . .
H36A H -0.3401 0.3949 0.1148 0.075 Uiso 1 1 calc R . .
H36B H -0.4203 0.3565 0.1792 0.075 Uiso 1 1 calc R . .
C37 C 0.1021(3) 0.1398(2) 0.12192(14) 0.0276(5) Uani 1 1 d . . .
H37A H 0.1902 0.1480 0.1179 0.033 Uiso 1 1 calc R . .
H37B H 0.0606 0.1552 0.0763 0.033 Uiso 1 1 calc R . .
C38 C 0.0318(3) 0.0187(2) 0.12033(16) 0.0397(7) Uani 1 1 d . . .
H38A H 0.0671 -0.0400 0.0898 0.048 Uiso 1 1 calc R . .
H38B H -0.0587 -0.0065 0.0945 0.048 Uiso 1 1 calc R . .
C39 C 0.0496(2) 0.03150(19) 0.21014(14) 0.0265(5) Uani 1 1 d . . .
H39A H -0.0327 0.0034 0.2240 0.032 Uiso 1 1 calc R . .
H39B H 0.1020 -0.0139 0.2224 0.032 Uiso 1 1 calc R . .
C40 C 0.1162(2) 0.16392(19) 0.25742(13) 0.0216(4) Uani 1 1 d . . .
H40A H 0.0786 0.1918 0.3042 0.026 Uiso 1 1 calc R . .
H40B H 0.2070 0.1816 0.2782 0.026 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N3 Ru1 N1 93.14(7) . . ?
N3 Ru1 O1 178.09(6) . . ?
N1 Ru1 O1 88.76(6) . . ?
N3 Ru1 O3 90.98(6) . . ?
N1 Ru1 O3 175.69(6) . . ?
O1 Ru1 O3 87.12(6) . . ?
N3 Ru1 Ru2 89.29(5) . . ?
N1 Ru1 Ru2 89.98(5) . . ?
O1 Ru1 Ru2 90.89(4) . . ?
O3 Ru1 Ru2 88.80(4) . . ?
N3 Ru1 O5 97.73(6) . . ?
N1 Ru1 O5 98.96(6) . . ?
O1 Ru1 O5 81.79(5) . . ?
O3 Ru1 O5 81.72(5) . . ?
Ru2 Ru1 O5 168.27(4) . . ?
O4 Ru2 N2 177.10(6) . . ?
O4 Ru2 N4 89.92(6) . . ?
N2 Ru2 N4 92.15(7) . . ?
O4 Ru2 O2 88.89(6) . . ?
N2 Ru2 O2 88.92(6) . . ?
N4 Ru2 O2 176.22(6) . . ?
O4 Ru2 Ru1 88.63(4) . . ?
N2 Ru2 Ru1 89.33(5) . . ?
N4 Ru2 Ru1 89.97(5) . . ?
O2 Ru2 Ru1 86.41(4) . . ?
O4 Ru2 Cl1 89.54(4) . . ?
N2 Ru2 Cl1 92.13(5) . . ?
N4 Ru2 Cl1 99.34(5) . . ?
O2 Ru2 Cl1 84.24(4) . . ?
Ru1 Ru2 Cl1 170.508(14) . . ?
C3 N1 C11 115.62(16) . . ?
C3 N1 Ru1 119.01(13) . . ?
C11 N1 Ru1 125.28(13) . . ?
C3 N2 C17 115.19(16) . . ?
C3 N2 Ru2 118.68(13) . . ?
C17 N2 Ru2 125.66(12) . . ?
C2 N3 C5 118.00(17) . . ?
C2 N3 Ru1 120.43(13) . . ?
C5 N3 Ru1 121.25(13) . . ?
C2 N4 C23 116.98(17) . . ?
C2 N4 Ru2 118.14(13) . . ?
C23 N4 Ru2 124.71(13) . . ?
C4 O1 Ru1 117.55(13) . . ?
C4 O2 Ru2 120.80(13) . . ?
C1 O3 Ru1 118.76(13) . . ?
C1 O4 Ru2 119.52(13) . . ?
C40 O5 C37 105.50(16) . . ?
C40 O5 Ru1 136.24(12) . . ?
C37 O5 Ru1 118.01(12) . . ?
O4 C1 O3 123.41(18) . . ?
O4 C1 C29 117.52(18) . . ?
O3 C1 C29 119.07(18) . . ?
N3 C2 N4 121.52(18) . . ?
N2 C3 N1 122.03(18) . . ?
O2 C4 O1 123.49(19) . . ?
O2 C4 C33 119.76(18) . . ?
O1 C4 C33 116.75(18) . . ?
C10 C5 C6 120.50(18) . . ?
C10 C5 N3 119.00(18) . . ?
C6 C5 N3 120.43(18) . . ?
C7 C6 C5 118.46(19) . . ?
C6 C7 C8 122.48(19) . . ?
C6 C7 Cl7 119.42(17) . . ?
C8 C7 Cl7 118.09(16) . . ?
C9 C8 C7 117.53(19) . . ?
C8 C9 C10 121.90(19) . . ?
C8 C9 Cl6 118.92(16) . . ?
C10 C9 Cl6 119.17(17) . . ?
C9 C10 C5 119.12(19) . . ?
C16 C11 C12 120.56(18) . . ?
C16 C11 N1 119.48(18) . . ?
C12 C11 N1 119.95(18) . . ?
C13 C12 C11 118.9(2) . . ?
C14 C13 C12 122.2(2) . . ?
C14 C13 Cl8 119.59(16) . . ?
C12 C13 Cl8 118.25(17) . . ?
C13 C14 C15 117.52(19) . . ?
C16 C15 C14 122.3(2) . . ?
C16 C15 Cl9 118.55(17) . . ?
C14 C15 Cl9 119.18(16) . . ?
C15 C16 C11 118.51(19) . . ?
C18 C17 C22 120.50(19) . . ?
C18 C17 N2 120.18(18) . . ?
C22 C17 N2 119.29(18) . . ?
C17 C18 C19 118.3(2) . . ?
C20 C19 C18 122.7(2) . . ?
C20 C19 Cl2 118.45(17) . . ?
C18 C19 Cl2 118.80(18) . . ?
C19 C20 C21 117.31(19) . . ?
C22 C21 C20 122.1(2) . . ?
C22 C21 Cl3 119.21(17) . . ?
C20 C21 Cl3 118.72(16) . . ?
C21 C22 C17 119.0(2) . . ?
C24 C23 C28 120.13(18) . . ?
C24 C23 N4 119.24(18) . . ?
C28 C23 N4 120.55(18) . . ?
C25 C24 C23 118.51(19) . . ?
C24 C25 C26 122.9(2) . . ?
C24 C25 Cl4 119.26(17) . . ?
C26 C25 Cl4 117.82(16) . . ?
C27 C26 C25 117.24(19) . . ?
C26 C27 C28 122.2(2) . . ?
C26 C27 Cl5 119.31(16) . . ?
C28 C27 Cl5 118.45(16) . . ?
C27 C28 C23 119.03(19) . . ?
C1 C29 C30 114.70(18) . . ?
C31 C30 C29 110.74(19) . . ?
C32 C31 C30 124.6(3) . . ?
C4 C33 C34 112.05(18) . . ?
C35 C34 C33 116.1(2) . . ?
C36 C35 C34 126.3(3) . . ?
O5 C37 C38 104.73(19) . . ?
C37 C38 C39 104.8(2) . . ?
C40 C39 C38 104.45(18) . . ?
O5 C40 C39 105.63(17) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 N3 2.0279(17) . ?
Ru1 N1 2.0342(17) . ?
Ru1 O1 2.0351(14) . ?
Ru1 O3 2.0482(14) . ?
Ru1 Ru2 2.3227(2) . ?
Ru1 O5 2.4017(14) . ?
Ru2 O4 2.0482(14) . ?
Ru2 N2 2.0529(16) . ?
Ru2 N4 2.0583(17) . ?
Ru2 O2 2.0707(14) . ?
Ru2 Cl1 2.4605(5) . ?
N1 C3 1.324(3) . ?
N1 C11 1.424(2) . ?
N2 C3 1.318(2) . ?
N2 C17 1.434(2) . ?
N3 C2 1.319(3) . ?
N3 C5 1.431(2) . ?
N4 C2 1.324(3) . ?
N4 C23 1.428(2) . ?
O1 C4 1.279(2) . ?
O2 C4 1.262(2) . ?
O3 C1 1.277(2) . ?
O4 C1 1.265(2) . ?
O5 C40 1.445(2) . ?
O5 C37 1.448(3) . ?
Cl2 C19 1.738(2) . ?
Cl3 C21 1.740(2) . ?
Cl4 C25 1.740(2) . ?
Cl5 C27 1.744(2) . ?
Cl6 C9 1.738(2) . ?
Cl7 C7 1.740(2) . ?
Cl8 C13 1.743(2) . ?
Cl9 C15 1.732(2) . ?
C1 C29 1.502(3) . ?
C4 C33 1.501(3) . ?
C5 C10 1.389(3) . ?
C5 C6 1.393(3) . ?
C6 C7 1.386(3) . ?
C7 C8 1.387(3) . ?
C8 C9 1.384(3) . ?
C9 C10 1.387(3) . ?
C11 C16 1.390(3) . ?
C11 C12 1.393(3) . ?
C12 C13 1.387(3) . ?
C13 C14 1.379(3) . ?
C14 C15 1.392(3) . ?
C15 C16 1.387(3) . ?
C17 C18 1.386(3) . ?
C17 C22 1.389(3) . ?
C18 C19 1.389(3) . ?
C19 C20 1.377(3) . ?
C20 C21 1.384(3) . ?
C21 C22 1.382(3) . ?
C23 C24 1.394(3) . ?
C23 C28 1.397(3) . ?
C24 C25 1.380(3) . ?
C25 C26 1.388(3) . ?
C26 C27 1.381(3) . ?
C27 C28 1.385(3) . ?
C29 C30 1.521(3) . ?
C30 C31 1.492(3) . ?
C31 C32 1.313(4) . ?
C33 C34 1.522(3) . ?
C34 C35 1.475(5) . ?
C35 C36 1.346(6) . ?
C37 C38 1.506(3) . ?
C38 C39 1.531(3) . ?
C39 C40 1.529(3) . ?
