#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:48:10 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179129 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/91/4309102.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4309102
loop_
_publ_author_name
'Yu-Bin Dong'
'Hai-Ying Wang'
'Jian-Ping Ma'
'Da-Zhong Shen'
'Ru-Qi Huang'
_publ_section_title
;
Synthesis and Characterization of New Coordination Polymers Generated from
Bent Bis(Cyanophenyl)oxadiazole Ligands and Ag(I) Salts
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4679
_journal_page_last               4692
_journal_paper_doi               10.1021/ic050218s
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C16 H12 Ag2 N4 O9 P2'
_chemical_formula_weight         681.98
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.191(4)
_cell_angle_beta                 97.322(4)
_cell_angle_gamma                107.392(4)
_cell_formula_units_Z            2
_cell_length_a                   7.956(2)
_cell_length_b                   9.938(3)
_cell_length_c                   14.242(4)
_cell_measurement_reflns_used    1242
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.251
_cell_measurement_theta_min      2.281
_cell_volume                     1004.3(5)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0255
_diffrn_reflns_av_sigmaI/netI    0.0582
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            5228
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.28
_exptl_absorpt_coefficient_mu    2.171
_exptl_absorpt_correction_T_max  0.9182
_exptl_absorpt_correction_T_min  0.6706
_exptl_absorpt_correction_type   mu;ti-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.255
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plane
_exptl_crystal_F_000             664
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.04
_refine_diff_density_max         3.273
_refine_diff_density_min         -2.670
_refine_diff_density_rms         0.154
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     298
_refine_ls_number_reflns         3482
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.040
_refine_ls_R_factor_all          0.0995
_refine_ls_R_factor_gt           0.0775
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0466P)²+14.7279P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1648
_refine_ls_wR_factor_ref         0.1796
_reflns_number_gt                2640
_reflns_number_total             3482
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic050218ssi20050210_123644_7.cif
_cod_data_source_block           -7-41119b1m
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4309102
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.81995(13) 0.57962(10) 0.53756(8) 0.0585(3) Uani 1 1 d . . .
Ag2 Ag 0.5633(2) 0.90780(10) 0.90107(9) 0.1035(6) Uani 1 1 d . . .
N1 N 0.6328(11) 1.1562(8) 0.9296(6) 0.0320(18) Uani 1 1 d . . .
N2 N 0.5908(10) 1.2328(8) 1.0168(6) 0.0311(17) Uani 1 1 d . . .
N3 N 0.4040(15) 1.5361(11) 1.3957(7) 0.058(3) Uani 1 1 d . . .
N4 N 0.8175(14) 0.8130(11) 0.5519(8) 0.054(2) Uani 1 1 d . . .
C1 C 0.8265(14) 0.9295(12) 0.5981(8) 0.042(2) Uani 1 1 d . . .
C2 C 0.8401(13) 1.0777(10) 0.6596(7) 0.034(2) Uani 1 1 d . . .
C3 C 0.7759(12) 1.0939(10) 0.7459(7) 0.031(2) Uani 1 1 d . . .
H3 H 0.7209 1.0112 0.7640 0.037 Uiso 1 1 calc R . .
C4 C 0.7957(12) 1.2380(10) 0.8056(7) 0.030(2) Uani 1 1 d . . .
C5 C 0.8738(13) 1.3587(11) 0.7779(7) 0.036(2) Uani 1 1 d . . .
H5 H 0.8850 1.4539 0.8181 0.043 Uiso 1 1 calc R . .
C6 C 0.9362(14) 1.3412(11) 0.6910(8) 0.041(2) Uani 1 1 d . . .
H6 H 0.9896 1.4244 0.6730 0.049 Uiso 1 1 calc R . .
C7 C 0.9197(14) 1.1994(12) 0.6300(8) 0.042(2) Uani 1 1 d . . .
H7 H 0.9608 1.1863 0.5710 0.050 Uiso 1 1 calc R . .
C8 C 0.7229(12) 1.2558(9) 0.8952(7) 0.028(2) Uani 1 1 d . . .
C9 C 0.6617(12) 1.3743(10) 1.0293(7) 0.031(2) Uani 1 1 d . . .
C10 C 0.6567(12) 1.5010(10) 1.1080(7) 0.031(2) Uani 1 1 d . . .
C11 C 0.5747(13) 1.4765(10) 1.1852(7) 0.034(2) Uani 1 1 d . . .
H11 H 0.5260 1.3799 1.1867 0.041 Uiso 1 1 calc R . .
C12 C 0.5657(13) 1.5959(11) 1.2596(7) 0.034(2) Uani 1 1 d . . .
C13 C 0.6361(14) 1.7413(10) 1.2580(7) 0.037(2) Uani 1 1 d . . .
H13 H 0.6296 1.8216 1.3081 0.045 Uiso 1 1 calc R . .
C14 C 0.7157(13) 1.7635(10) 1.1800(7) 0.037(2) Uani 1 1 d . . .
H14 H 0.7631 1.8600 1.1779 0.044 Uiso 1 1 calc R . .
C15 C 0.7262(12) 1.6451(10) 1.1051(7) 0.032(2) Uani 1 1 d . . .
H15 H 0.7796 1.6620 1.0531 0.039 Uiso 1 1 calc R . .
C16 C 0.4756(14) 1.5642(11) 1.3372(8) 0.042(2) Uani 1 1 d . . .
O1 O 0.7453(9) 1.3959(6) 0.9550(5) 0.0330(15) Uani 1 1 d . . .
O2 O 0.8184(17) 0.8473(18) 0.8534(12) 0.133(5) Uani 1 1 d . . .
O3 O 1.1466(14) 0.9340(10) 0.9001(8) 0.086(3) Uani 1 1 d . . .
H3A H 1.1517 0.9981 0.9522 0.129 Uiso 1 1 calc R . .
O4 O 0.9733(13) 0.7208(10) 0.9374(7) 0.073(3) Uani 1 1 d . . .
O5 O 0.9836(16) 0.7087(11) 0.7732(7) 0.095(4) Uani 1 1 d . . .
H5A H 0.9921 0.7529 0.7323 0.142 Uiso 1 1 calc R . .
O6 O 0.5768(14) 0.2145(11) 0.2799(7) 0.081(3) Uani 1 1 d . . .
O7 O 0.7827(11) 0.1054(8) 0.3385(7) 0.069(3) Uani 1 1 d . . .
H7A H 0.8342 0.1117 0.2928 0.103 Uiso 1 1 calc R . .
O8 O 0.6009(12) 0.1675(10) 0.4367(6) 0.071(3) Uani 1 1 d . . .
H8 H 0.5364 0.2158 0.4549 0.107 Uiso 1 1 calc R . .
O9 O 0.8506(10) 0.3689(8) 0.4226(6) 0.059(2) Uani 1 1 d . . .
P1 P 0.9707(5) 0.8097(4) 0.8712(3) 0.0648(9) Uani 1 1 d . . .
P2 P 0.7034(4) 0.2285(3) 0.3643(2) 0.0430(7) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N4 Ag1 N3 109.2(4) . 2_677 ?
N4 Ag1 O9 141.2(3) . . ?
N3 Ag1 O9 100.5(3) 2_677 . ?
N4 Ag1 O9 100.5(3) . 2_766 ?
N3 Ag1 O9 130.8(3) 2_677 2_766 ?
O9 Ag1 O9 76.8(3) . 2_766 ?
N2 Ag2 N1 128.5(3) 2_677 . ?
N2 Ag2 O2 115.0(4) 2_677 . ?
N1 Ag2 O2 106.6(4) . . ?
N2 Ag2 O6 107.9(3) 2_677 2_666 ?
N1 Ag2 O6 105.5(3) . 2_666 ?
O2 Ag2 O6 83.6(4) . 2_666 ?
N2 Ag2 Ag2 64.01(19) 2_677 2_677 ?
N1 Ag2 Ag2 64.60(19) . 2_677 ?
O2 Ag2 Ag2 141.8(4) . 2_677 ?
O6 Ag2 Ag2 134.4(3) 2_666 2_677 ?
C8 N1 N2 107.1(7) . . ?
C8 N1 Ag2 137.8(6) . . ?
N2 N1 Ag2 114.4(5) . . ?
C9 N2 N1 106.2(7) . . ?
C9 N2 Ag2 137.0(6) . 2_677 ?
N1 N2 Ag2 116.7(5) . 2_677 ?
C16 N3 Ag1 158.8(10) . 2_677 ?
C1 N4 Ag1 151.9(10) . . ?
N4 C1 C2 178.4(13) . . ?
C3 C2 C7 122.0(9) . . ?
C3 C2 C1 119.2(9) . . ?
C7 C2 C1 118.8(9) . . ?
C2 C3 C4 118.2(8) . . ?
C2 C3 H3 120.9 . . ?
C4 C3 H3 120.9 . . ?
C5 C4 C3 120.7(9) . . ?
C5 C4 C8 120.7(8) . . ?
C3 C4 C8 118.5(8) . . ?
C4 C5 C6 120.7(9) . . ?
C4 C5 H5 119.6 . . ?
C6 C5 H5 119.6 . . ?
C5 C6 C7 120.2(9) . . ?
C5 C6 H6 119.9 . . ?
C7 C6 H6 119.9 . . ?
C6 C7 C2 118.3(9) . . ?
C6 C7 H7 120.9 . . ?
C2 C7 H7 120.9 . . ?
N1 C8 O1 110.8(8) . . ?
N1 C8 C4 130.2(8) . . ?
O1 C8 C4 118.9(8) . . ?
N2 C9 O1 111.3(8) . . ?
N2 C9 C10 128.5(8) . . ?
O1 C9 C10 120.2(8) . . ?
C15 C10 C11 119.8(8) . . ?
C15 C10 C9 120.9(8) . . ?
C11 C10 C9 119.2(8) . . ?
C12 C11 C10 119.9(9) . . ?
C12 C11 H11 120.1 . . ?
C10 C11 H11 120.1 . . ?
C11 C12 C13 120.9(9) . . ?
C11 C12 C16 117.7(9) . . ?
C13 C12 C16 121.4(9) . . ?
C14 C13 C12 118.5(9) . . ?
C14 C13 H13 120.8 . . ?
C12 C13 H13 120.8 . . ?
C15 C14 C13 121.3(9) . . ?
C15 C14 H14 119.3 . . ?
C13 C14 H14 119.3 . . ?
C14 C15 C10 119.6(9) . . ?
C14 C15 H15 120.2 . . ?
C10 C15 H15 120.2 . . ?
N3 C16 C12 178.3(12) . . ?
C9 O1 C8 104.5(7) . . ?
P1 O2 Ag2 152.9(10) . . ?
P1 O3 H3A 109.5 . . ?
P1 O5 H5A 109.5 . . ?
P2 O6 Ag2 148.6(7) . 2_666 ?
P2 O7 H7A 109.5 . . ?
P2 O8 H8 109.5 . . ?
P2 O9 Ag1 125.7(5) . . ?
P2 O9 Ag1 129.1(5) . 2_766 ?
Ag1 O9 Ag1 103.2(3) . 2_766 ?
O2 P1 O4 117.3(8) . . ?
O2 P1 O3 115.9(8) . . ?
O4 P1 O3 109.0(6) . . ?
O2 P1 O5 108.4(9) . . ?
O4 P1 O5 102.6(6) . . ?
O3 P1 O5 101.6(7) . . ?
O6 P2 O9 122.7(6) . . ?
O6 P2 O7 110.2(6) . . ?
O9 P2 O7 108.3(5) . . ?
O6 P2 O8 109.0(6) . . ?
O9 P2 O8 108.8(5) . . ?
O7 P2 O8 94.1(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N4 2.277(10) . ?
Ag1 N3 2.284(10) 2_677 ?
Ag1 O9 2.371(8) . ?
Ag1 O9 2.472(8) 2_766 ?
Ag2 N2 2.253(7) 2_677 ?
Ag2 N1 2.265(7) . ?
Ag2 O2 2.407(12) . ?
Ag2 O6 2.464(9) 2_666 ?
Ag2 Ag2 3.356(2) 2_677 ?
N1 C8 1.293(11) . ?
N1 N2 1.401(10) . ?
N2 C9 1.300(11) . ?
N2 Ag2 2.253(7) 2_677 ?
N3 C16 1.119(13) . ?
N3 Ag1 2.284(10) 2_677 ?
N4 C1 1.137(13) . ?
C1 C2 1.452(14) . ?
C2 C3 1.377(13) . ?
C2 C7 1.391(14) . ?
C3 C4 1.397(13) . ?
C3 H3 0.9300 . ?
C4 C5 1.364(13) . ?
C4 C8 1.456(12) . ?
C5 C6 1.378(14) . ?
C5 H5 0.9300 . ?
C6 C7 1.391(14) . ?
C6 H6 0.9300 . ?
C7 H7 0.9300 . ?
C8 O1 1.359(10) . ?
C9 O1 1.353(11) . ?
C9 C10 1.448(13) . ?
C10 C15 1.387(12) . ?
C10 C11 1.389(13) . ?
C11 C12 1.381(13) . ?
C11 H11 0.9300 . ?
C12 C13 1.392(13) . ?
C12 C16 1.447(14) . ?
C13 C14 1.384(14) . ?
C13 H13 0.9300 . ?
C14 C15 1.382(13) . ?
C14 H14 0.9300 . ?
C15 H15 0.9300 . ?
O2 P1 1.384(11) . ?
O3 P1 1.480(9) . ?
O3 H3A 0.8200 . ?
O4 P1 1.464(9) . ?
O5 P1 1.511(10) . ?
O5 H5A 0.8200 . ?
O6 P2 1.413(9) . ?
O6 Ag2 2.464(9) 2_666 ?
O7 P2 1.516(8) . ?
O7 H7A 0.8200 . ?
O8 P2 1.537(8) . ?
O8 H8 0.8200 . ?
O9 P2 1.462(8) . ?
O9 Ag1 2.472(8) 2_766 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O5 H5A O7 0.82 2.44 3.122(14) 141.1 2_766
O7 H7A O5 0.82 2.43 3.122(14) 142.6 2_766
O8 H8 N3 0.82 2.64 3.248(14) 132.6 2_677
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 Ag2 N1 C8 176.5(9) 2_677 . . . ?
O2 Ag2 N1 C8 33.2(11) . . . . ?
O6 Ag2 N1 C8 -54.6(10) 2_666 . . . ?
Ag2 Ag2 N1 C8 173.2(10) 2_677 . . . ?
N2 Ag2 N1 N2 7.8(9) 2_677 . . . ?
O2 Ag2 N1 N2 -135.5(7) . . . . ?
O6 Ag2 N1 N2 136.7(6) 2_666 . . . ?
Ag2 Ag2 N1 N2 4.5(5) 2_677 . . . ?
C8 N1 N2 C9 -0.9(10) . . . . ?
Ag2 N1 N2 C9 171.2(6) . . . . ?
C8 N1 N2 Ag2 -178.9(6) . . . 2_677 ?
Ag2 N1 N2 Ag2 -6.8(8) . . . 2_677 ?
N3 Ag1 N4 C1 58(2) 2_677 . . . ?
O9 Ag1 N4 C1 -163.9(17) . . . . ?
O9 Ag1 N4 C1 -82(2) 2_766 . . . ?
Ag1 N4 C1 C2 16(43) . . . . ?
N4 C1 C2 C3 -49(42) . . . . ?
N4 C1 C2 C7 130(42) . . . . ?
C7 C2 C3 C4 -1.2(15) . . . . ?
C1 C2 C3 C4 178.0(9) . . . . ?
C2 C3 C4 C5 1.1(14) . . . . ?
C2 C3 C4 C8 178.0(9) . . . . ?
C3 C4 C5 C6 -0.6(15) . . . . ?
C8 C4 C5 C6 -177.4(9) . . . . ?
C4 C5 C6 C7 0.2(16) . . . . ?
C5 C6 C7 C2 -0.4(16) . . . . ?
C3 C2 C7 C6 0.9(15) . . . . ?
C1 C2 C7 C6 -178.3(10) . . . . ?
N2 N1 C8 O1 0.5(10) . . . . ?
Ag2 N1 C8 O1 -168.7(7) . . . . ?
N2 N1 C8 C4 -178.3(9) . . . . ?
Ag2 N1 C8 C4 12.4(17) . . . . ?
C5 C4 C8 N1 174.1(10) . . . . ?
C3 C4 C8 N1 -2.8(15) . . . . ?
C5 C4 C8 O1 -4.6(14) . . . . ?
C3 C4 C8 O1 178.4(8) . . . . ?
N1 N2 C9 O1 1.0(10) . . . . ?
Ag2 N2 C9 O1 178.4(6) 2_677 . . . ?
N1 N2 C9 C10 179.7(9) . . . . ?
Ag2 N2 C9 C10 -3.0(16) 2_677 . . . ?
N2 C9 C10 C15 -174.2(9) . . . . ?
O1 C9 C10 C15 4.4(14) . . . . ?
N2 C9 C10 C11 3.3(15) . . . . ?
O1 C9 C10 C11 -178.1(8) . . . . ?
C15 C10 C11 C12 -1.2(15) . . . . ?
C9 C10 C11 C12 -178.7(9) . . . . ?
C10 C11 C12 C13 0.8(15) . . . . ?
C10 C11 C12 C16 178.7(9) . . . . ?
C11 C12 C13 C14 -0.2(15) . . . . ?
C16 C12 C13 C14 -178.0(9) . . . . ?
C12 C13 C14 C15 -0.1(15) . . . . ?
C13 C14 C15 C10 -0.3(15) . . . . ?
C11 C10 C15 C14 1.0(14) . . . . ?
C9 C10 C15 C14 178.5(9) . . . . ?
Ag1 N3 C16 C12 -34(45) 2_677 . . . ?
C11 C12 C16 N3 -17(43) . . . . ?
C13 C12 C16 N3 161(42) . . . . ?
N2 C9 O1 C8 -0.7(10) . . . . ?
C10 C9 O1 C8 -179.5(8) . . . . ?
N1 C8 O1 C9 0.1(10) . . . . ?
C4 C8 O1 C9 179.1(8) . . . . ?
N2 Ag2 O2 P1 -42(2) 2_677 . . . ?
N1 Ag2 O2 P1 107(2) . . . . ?
O6 Ag2 O2 P1 -149(2) 2_666 . . . ?
Ag2 Ag2 O2 P1 37(3) 2_677 . . . ?
N4 Ag1 O9 P2 -104.4(7) . . . . ?
N3 Ag1 O9 P2 35.5(7) 2_677 . . . ?
O9 Ag1 O9 P2 165.2(9) 2_766 . . . ?
N4 Ag1 O9 Ag1 90.4(6) . . . 2_766 ?
N3 Ag1 O9 Ag1 -129.7(4) 2_677 . . 2_766 ?
O9 Ag1 O9 Ag1 0.0 2_766 . . 2_766 ?
Ag2 O2 P1 O4 31(3) . . . . ?
Ag2 O2 P1 O3 -100(2) . . . . ?
Ag2 O2 P1 O5 147(2) . . . . ?
Ag2 O6 P2 O9 120.5(11) 2_666 . . . ?
Ag2 O6 P2 O7 -8.9(14) 2_666 . . . ?
Ag2 O6 P2 O8 -110.9(12) 2_666 . . . ?
Ag1 O9 P2 O6 74.8(9) . . . . ?
Ag1 O9 P2 O6 -124.0(8) 2_766 . . . ?
Ag1 O9 P2 O7 -155.1(6) . . . . ?
Ag1 O9 P2 O7 6.2(8) 2_766 . . . ?
Ag1 O9 P2 O8 -54.0(8) . . . . ?
Ag1 O9 P2 O8 107.3(7) 2_766 . . . ?
