#------------------------------------------------------------------------------
#$Date: 2018-10-05 15:19:55 +0300 (Fri, 05 Oct 2018) $
#$Revision: 211332 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/30/92/4309228.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4309228
loop_
_publ_author_name
'Thomas M. Klapötke'
'Burkhard Krumm'
'Heinrich Nöth'
'Juan Carlos Gálvez-Ruiz'
'Kurt Polborn'
'Ingo Schwab'
'Max Suter'
_publ_contact_author
;
      Heinrich Nöth
      Institut für anorganische Chemie
      Universität München
      Butenandtstr. 5-13 (Haus D)
      81377 München
      Bundesrepublik Deutschland
;
_publ_contact_author_email       H.Noeth@lrz.uni-muenchen.de
_publ_contact_author_fax         '089 2180 7865'
_publ_contact_author_phone       '089 2180 7454'
_publ_section_title
;
Kinetic and Donor Stabilization of Organotellurenyl Iodides and Azides
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5254
_journal_page_last               5265
_journal_paper_doi               10.1021/ic048219s
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C41 H65 Li O4 Si3 Te'
_chemical_formula_weight         840.74
_chemical_name_systematic
; 
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           'SHELXL-CIF-file updated by CIFRTF'
_cell_angle_alpha                90
_cell_angle_beta                 91.287(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.0393(16)
_cell_length_b                   18.740(2)
_cell_length_c                   16.900(2)
_cell_measurement_temperature    193(2)
_cell_volume                     4445.2(9)
_computing_cell_refinement       'SMART (V4.C50)'
_computing_data_collection       'SMART (V4.C50)'
_computing_data_reduction        'SAINT (V4.D50)'
_computing_molecular_graphics    'XP (SHELXTL-Ver.5)'
_computing_publication_material  'SHELXL (Sheldrick 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.970
_diffrn_measured_fraction_theta_max 0.970
_diffrn_measurement_device_type  'Siemens SMART Area-detector'
_diffrn_measurement_method       Hemisphere
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0629
_diffrn_reflns_av_sigmaI/netI    0.1451
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            22388
_diffrn_reflns_theta_full        24.71
_diffrn_reflns_theta_max         24.71
_diffrn_reflns_theta_min         1.62
_diffrn_standards_interval_time  0
_exptl_absorpt_coefficient_mu    0.786
_exptl_absorpt_correction_T_max  0.913195
_exptl_absorpt_correction_T_min  0.746287
_exptl_absorpt_correction_type   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.256
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1760
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.184
_refine_diff_density_min         -0.566
_refine_diff_density_rms         0.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.804
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     457
_refine_ls_number_reflns         7352
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.804
_refine_ls_R_factor_all          0.1023
_refine_ls_R_factor_gt           0.0447
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0467P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0930
_refine_ls_wR_factor_ref         0.0998
_reflns_number_gt                3531
_reflns_number_total             7352
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic048219ssi20041217_091943.cif
_cod_data_source_block           primero
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_hydrogen_treatment' value 'mixed ' changed to
'mixed' according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'direct methods' was changed to
'direct'.

'_atom_sites_solution_hydrogens' value 'geometrically' was changed to
'geom'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_original_cell_volume        4445.1(9)
_cod_database_code               4309228
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Te1 Te 0.24078(3) 0.20434(2) 0.422506(19) 0.04553(14) Uani 1 1 d . . .
Si1 Si 0.37264(11) 0.26027(9) 0.57305(9) 0.0477(5) Uani 1 1 d . . .
Si2 Si 0.15575(11) 0.22943(9) 0.60030(9) 0.0462(4) Uani 1 1 d . . .
Si3 Si 0.21412(11) 0.36341(8) 0.50340(8) 0.0449(4) Uani 1 1 d . . .
O1 O 0.2578(3) 0.3040(2) 0.1837(2) 0.0655(11) Uani 1 1 d . . .
O2 O 0.1435(3) 0.4444(2) 0.1540(3) 0.0813(14) Uani 1 1 d . . .
O3 O 0.2438(3) 0.3705(2) 0.0143(2) 0.0675(12) Uani 1 1 d . . .
O4 O 0.3691(3) 0.4449(2) 0.1519(2) 0.0718(13) Uani 1 1 d . . .
Li1 Li 0.2542(8) 0.3924(6) 0.1263(6) 0.069(3) Uani 1 1 d . . .
C1 C 0.2468(3) 0.2701(2) 0.5353(2) 0.0326(13) Uani 1 1 d . . .
C2 C 0.3872(4) 0.2918(3) 0.6787(3) 0.0580(16) Uani 1 1 d . . .
H2A H 0.3455 0.2639 0.7127 0.070 Uiso 1 1 calc R . .
H2B H 0.3700 0.3424 0.6819 0.070 Uiso 1 1 calc R . .
H2C H 0.4536 0.2856 0.6964 0.070 Uiso 1 1 calc R . .
C3 C 0.4216(4) 0.1681(3) 0.5724(3) 0.0648(18) Uani 1 1 d . . .
H3A H 0.3855 0.1381 0.6085 0.078 Uiso 1 1 calc R . .
H3B H 0.4887 0.1691 0.5896 0.078 Uiso 1 1 calc R . .
H3C H 0.4163 0.1485 0.5187 0.078 Uiso 1 1 calc R . .
C4 C 0.4579(4) 0.3161(3) 0.5134(3) 0.0487(16) Uani 1 1 d . . .
C5 C 0.5020(4) 0.3781(3) 0.5452(4) 0.0598(17) Uani 1 1 d . . .
H5A H 0.4875 0.3923 0.5975 0.072 Uiso 1 1 calc R . .
C6 C 0.5644(5) 0.4180(3) 0.5037(5) 0.073(2) Uani 1 1 d . . .
H6A H 0.5943 0.4585 0.5273 0.087 Uiso 1 1 calc R . .
C7 C 0.5839(5) 0.3990(4) 0.4270(5) 0.075(2) Uani 1 1 d . . .
H7A H 0.6269 0.4269 0.3974 0.089 Uiso 1 1 calc R . .
C8 C 0.5430(4) 0.3418(4) 0.3940(4) 0.0612(18) Uani 1 1 d . . .
H8A H 0.5562 0.3300 0.3406 0.073 Uiso 1 1 calc R . .
C9 C 0.4818(4) 0.2994(3) 0.4361(3) 0.0597(16) Uani 1 1 d . . .
H9A H 0.4553 0.2580 0.4117 0.072 Uiso 1 1 calc R . .
C10 C 0.1284(4) 0.2861(3) 0.6876(3) 0.0555(16) Uani 1 1 d . . .
H10A H 0.0960 0.3298 0.6696 0.067 Uiso 1 1 calc R . .
H10B H 0.1877 0.2987 0.7158 0.067 Uiso 1 1 calc R . .
H10C H 0.0869 0.2598 0.7231 0.067 Uiso 1 1 calc R . .
C11 C 0.0388(4) 0.2093(3) 0.5539(3) 0.0656(18) Uani 1 1 d . . .
H11A H 0.0028 0.2536 0.5464 0.079 Uiso 1 1 calc R . .
H11B H 0.0034 0.1770 0.5882 0.079 Uiso 1 1 calc R . .
H11C H 0.0480 0.1864 0.5025 0.079 Uiso 1 1 calc R . .
C12 C 0.1969(4) 0.1413(3) 0.6442(3) 0.0447(15) Uani 1 1 d . . .
C13 C 0.1943(5) 0.0799(3) 0.5974(3) 0.076(2) Uani 1 1 d . . .
H13A H 0.1718 0.0833 0.5442 0.091 Uiso 1 1 calc R . .
C14 C 0.2233(6) 0.0145(4) 0.6260(4) 0.094(3) Uani 1 1 d . . .
H14A H 0.2227 -0.0259 0.5920 0.113 Uiso 1 1 calc R . .
C15 C 0.2536(5) 0.0074(3) 0.7046(3) 0.078(2) Uani 1 1 d . . .
H15A H 0.2719 -0.0380 0.7251 0.094 Uiso 1 1 calc R . .
C16 C 0.2567(4) 0.0661(3) 0.7516(3) 0.0551(17) Uani 1 1 d . . .
H16A H 0.2776 0.0621 0.8052 0.066 Uiso 1 1 calc R . .
C17 C 0.2297(4) 0.1310(3) 0.7218(3) 0.0518(16) Uani 1 1 d . . .
H17A H 0.2336 0.1713 0.7558 0.062 Uiso 1 1 calc R . .
C18 C 0.2433(4) 0.4293(3) 0.5835(3) 0.0514(16) Uani 1 1 d . . .
H18A H 0.3126 0.4320 0.5915 0.062 Uiso 1 1 calc R . .
H18B H 0.2139 0.4141 0.6328 0.062 Uiso 1 1 calc R . .
H18C H 0.2187 0.4764 0.5682 0.062 Uiso 1 1 calc R . .
C19 C 0.2707(4) 0.3992(3) 0.4132(3) 0.0523(17) Uani 1 1 d . . .
H19A H 0.3397 0.4027 0.4224 0.063 Uiso 1 1 calc R . .
H19B H 0.2448 0.4466 0.4012 0.063 Uiso 1 1 calc R . .
H19C H 0.2574 0.3671 0.3685 0.063 Uiso 1 1 calc R . .
C20 C 0.0192(5) 0.4062(3) 0.5342(4) 0.0654(19) Uani 1 1 d . . .
H20A H 0.0446 0.4265 0.5816 0.079 Uiso 1 1 calc R . .
C21 C -0.0766(5) 0.4119(3) 0.5182(4) 0.069(2) Uani 1 1 d . . .
H21A H -0.1162 0.4364 0.5541 0.082 Uiso 1 1 calc R . .
C22 C -0.1145(5) 0.3832(4) 0.4524(5) 0.081(2) Uani 1 1 d . . .
H22A H -0.1813 0.3862 0.4427 0.097 Uiso 1 1 calc R . .
C23 C -0.0579(5) 0.3493(4) 0.3983(4) 0.070(2) Uani 1 1 d . . .
H23A H -0.0855 0.3304 0.3509 0.084 Uiso 1 1 calc R . .
C24 C 0.0376(5) 0.3429(3) 0.4128(3) 0.0596(17) Uani 1 1 d . . .
H24A H 0.0762 0.3190 0.3757 0.072 Uiso 1 1 calc R . .
C25 C 0.0801(4) 0.3719(3) 0.4833(3) 0.0497(16) Uani 1 1 d . . .
C26 C 0.3402(5) 0.2692(4) 0.2132(4) 0.072(2) Uani 1 1 d . . .
H26A H 0.3475 0.2769 0.2710 0.086 Uiso 1 1 calc R . .
H26B H 0.3975 0.2880 0.1872 0.086 Uiso 1 1 calc R . .
C27 C 0.3283(8) 0.1913(5) 0.1956(5) 0.120(3) Uani 1 1 d . . .
H27A H 0.3684 0.1771 0.1508 0.145 Uiso 1 1 calc R . .
H27B H 0.3467 0.1622 0.2424 0.145 Uiso 1 1 calc R . .
C28 C 0.2292(8) 0.1816(5) 0.1757(6) 0.134(4) Uani 1 1 d . . .
H28A H 0.2005 0.1456 0.2108 0.161 Uiso 1 1 calc R . .
H28B H 0.2210 0.1656 0.1201 0.161 Uiso 1 1 calc R . .
C29 C 0.1834(6) 0.2539(5) 0.1872(5) 0.115(3) Uani 1 1 d . . .
H29A H 0.1349 0.2631 0.1450 0.138 Uiso 1 1 calc R . .
H29B H 0.1522 0.2562 0.2391 0.138 Uiso 1 1 calc R . .
C30 C 0.0945(6) 0.4384(5) 0.2262(4) 0.111(3) Uani 1 1 d . . .
H30A H 0.1399 0.4277 0.2703 0.133 Uiso 1 1 calc R . .
H30B H 0.0469 0.3994 0.2227 0.133 Uiso 1 1 calc R . .
C31 C 0.0483(8) 0.5048(6) 0.2394(7) 0.158(5) Uani 1 1 d . . .
H31A H 0.0864 0.5345 0.2768 0.190 Uiso 1 1 calc R . .
H31B H -0.0155 0.4971 0.2615 0.190 Uiso 1 1 calc R . .
C32 C 0.0404(8) 0.5394(5) 0.1623(8) 0.151(5) Uani 1 1 d . . .
H32A H -0.0240 0.5321 0.1386 0.182 Uiso 1 1 calc R . .
H32B H 0.0526 0.5912 0.1671 0.182 Uiso 1 1 calc R . .
C33 C 0.1107(7) 0.5062(5) 0.1156(6) 0.147(4) Uani 1 1 d . . .
H33A H 0.0830 0.4938 0.0630 0.177 Uiso 1 1 calc R . .
H33B H 0.1644 0.5395 0.1078 0.177 Uiso 1 1 calc R . .
C34 C 0.1575(6) 0.3613(7) -0.0251(5) 0.192(6) Uani 1 1 d . . .
H34A H 0.1252 0.4081 -0.0313 0.230 Uiso 1 1 calc R . .
H34B H 0.1161 0.3299 0.0062 0.230 Uiso 1 1 calc R . .
C35 C 0.1716(8) 0.3302(5) -0.1020(5) 0.147(4) Uani 1 1 d . . .
H35A H 0.1215 0.2945 -0.1148 0.177 Uiso 1 1 calc R . .
H35B H 0.1712 0.3672 -0.1438 0.177 Uiso 1 1 calc R . .
C36 C 0.2623(8) 0.2973(6) -0.0946(6) 0.208(7) Uani 1 1 d . . .
H36A H 0.3004 0.3070 -0.1421 0.249 Uiso 1 1 calc R . .
H36B H 0.2554 0.2450 -0.0889 0.249 Uiso 1 1 calc R . .
C37 C 0.3086(7) 0.3273(6) -0.0248(5) 0.164(5) Uani 1 1 d . . .
H37A H 0.3310 0.2885 0.0108 0.197 Uiso 1 1 calc R . .
H37B H 0.3646 0.3559 -0.0401 0.197 Uiso 1 1 calc R . .
C38 C 0.4080(6) 0.4978(5) 0.1039(5) 0.111(3) Uani 1 1 d . . .
H38A H 0.3565 0.5232 0.0745 0.133 Uiso 1 1 calc R . .
H38B H 0.4510 0.4759 0.0651 0.133 Uiso 1 1 calc R . .
C39 C 0.4611(7) 0.5477(5) 0.1544(7) 0.144(4) Uani 1 1 d . . .
H39A H 0.5273 0.5529 0.1363 0.173 Uiso 1 1 calc R . .
H39B H 0.4302 0.5952 0.1538 0.173 Uiso 1 1 calc R . .
C40 C 0.4598(8) 0.5168(6) 0.2328(6) 0.152(4) Uani 1 1 d . . .
H40A H 0.5256 0.5098 0.2536 0.182 Uiso 1 1 calc R . .
H40B H 0.4258 0.5488 0.2694 0.182 Uiso 1 1 calc R . .
C41 C 0.4137(8) 0.4526(6) 0.2265(4) 0.188(6) Uani 1 1 d . . .
H41A H 0.3654 0.4491 0.2681 0.225 Uiso 1 1 calc R . .
H41B H 0.4602 0.4134 0.2349 0.225 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 Si1 C1 115.8(2) . . ?
C3 Si1 C2 105.4(3) . . ?
C1 Si1 C2 111.8(2) . . ?
C3 Si1 C4 105.8(2) . . ?
C1 Si1 C4 111.5(2) . . ?
C2 Si1 C4 105.9(2) . . ?
C11 Si2 C10 104.8(3) . . ?
C11 Si2 C1 116.7(2) . . ?
C10 Si2 C1 112.9(2) . . ?
C11 Si2 C12 104.4(3) . . ?
C10 Si2 C12 104.7(2) . . ?
C1 Si2 C12 112.3(2) . . ?
C19 Si3 C18 105.3(2) . . ?
C19 Si3 C1 117.6(2) . . ?
C18 Si3 C1 110.9(2) . . ?
C19 Si3 C25 105.1(2) . . ?
C18 Si3 C25 105.8(3) . . ?
C1 Si3 C25 111.1(2) . . ?
C29 O1 C26 106.3(5) . . ?
C29 O1 Li1 125.8(5) . . ?
C26 O1 Li1 126.2(5) . . ?
C33 O2 C30 107.6(6) . . ?
C33 O2 Li1 124.9(6) . . ?
C30 O2 Li1 125.9(5) . . ?
C34 O3 C37 105.9(6) . . ?
C34 O3 Li1 122.9(5) . . ?
C37 O3 Li1 123.3(6) . . ?
C38 O4 C41 106.0(6) . . ?
C38 O4 Li1 124.4(5) . . ?
C41 O4 Li1 127.5(5) . . ?
O2 Li1 O1 109.3(5) . . ?
O2 Li1 O4 111.6(6) . . ?
O1 Li1 O4 108.3(6) . . ?
O2 Li1 O3 107.8(6) . . ?
O1 Li1 O3 108.1(6) . . ?
O4 Li1 O3 111.8(5) . . ?
Si2 C1 Si1 114.4(2) . . ?
Si2 C1 Si3 112.5(2) . . ?
Si1 C1 Si3 114.2(2) . . ?
Si2 C1 Te1 105.0(2) . . ?
Si1 C1 Te1 104.4(2) . . ?
Si3 C1 Te1 105.01(19) . . ?
C9 C4 C5 115.3(5) . . ?
C9 C4 Si1 122.9(5) . . ?
C5 C4 Si1 121.8(4) . . ?
C6 C5 C4 122.5(6) . . ?
C5 C6 C7 119.2(6) . . ?
C8 C7 C6 120.6(6) . . ?
C7 C8 C9 121.0(6) . . ?
C8 C9 C4 121.4(6) . . ?
C17 C12 C13 115.0(5) . . ?
C17 C12 Si2 125.4(4) . . ?
C13 C12 Si2 119.5(4) . . ?
C14 C13 C12 122.1(6) . . ?
C13 C14 C15 120.2(6) . . ?
C16 C15 C14 119.0(6) . . ?
C15 C16 C17 120.1(5) . . ?
C16 C17 C12 123.5(5) . . ?
C21 C20 C25 122.1(6) . . ?
C22 C21 C20 120.2(7) . . ?
C21 C22 C23 120.8(7) . . ?
C24 C23 C22 120.0(7) . . ?
C23 C24 C25 120.6(6) . . ?
C20 C25 C24 116.2(6) . . ?
C20 C25 Si3 123.2(5) . . ?
C24 C25 Si3 120.6(5) . . ?
O1 C26 C27 107.1(6) . . ?
C28 C27 C26 105.8(7) . . ?
C27 C28 C29 105.6(8) . . ?
O1 C29 C28 105.8(7) . . ?
O2 C30 C31 107.3(7) . . ?
C30 C31 C32 105.9(9) . . ?
C33 C32 C31 105.2(9) . . ?
O2 C33 C32 109.3(8) . . ?
O3 C34 C35 110.4(8) . . ?
C36 C35 C34 103.8(8) . . ?
C35 C36 C37 106.8(8) . . ?
O3 C37 C36 109.0(7) . . ?
O4 C38 C39 108.4(7) . . ?
C40 C39 C38 105.3(8) . . ?
C41 C40 C39 107.2(8) . . ?
C40 C41 O4 111.2(8) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Te1 C1 2.270(4) . ?
Si1 C3 1.859(6) . ?
Si1 C1 1.874(5) . ?
Si1 C2 1.888(5) . ?
Si1 C4 1.896(6) . ?
Si2 C11 1.843(5) . ?
Si2 C10 1.865(5) . ?
Si2 C1 1.866(5) . ?
Si2 C12 1.896(5) . ?
Si3 C19 1.860(5) . ?
Si3 C18 1.872(5) . ?
Si3 C1 1.884(5) . ?
Si3 C25 1.911(6) . ?
O1 C29 1.407(8) . ?
O1 C26 1.409(6) . ?
O1 Li1 1.920(11) . ?
O2 C33 1.401(8) . ?
O2 C30 1.419(7) . ?
O2 Li1 1.900(12) . ?
O3 C34 1.381(8) . ?
O3 C37 1.395(8) . ?
O3 Li1 1.939(10) . ?
O4 C38 1.400(7) . ?
O4 C41 1.402(8) . ?
O4 Li1 1.931(12) . ?
C4 C9 1.393(7) . ?
C4 C5 1.417(7) . ?
C5 C6 1.359(7) . ?
C6 C7 1.378(8) . ?
C7 C8 1.333(8) . ?
C8 C9 1.379(7) . ?
C12 C17 1.393(7) . ?
C12 C13 1.396(7) . ?
C13 C14 1.374(8) . ?
C14 C15 1.392(8) . ?
C15 C16 1.357(7) . ?
C16 C17 1.367(7) . ?
C20 C21 1.369(8) . ?
C20 C25 1.385(7) . ?
C21 C22 1.336(8) . ?
C22 C23 1.380(9) . ?
C23 C24 1.363(7) . ?
C24 C25 1.427(7) . ?
C26 C27 1.498(9) . ?
C27 C28 1.435(10) . ?
C28 C29 1.514(11) . ?
C30 C31 1.423(10) . ?
C31 C32 1.456(12) . ?
C32 C33 1.421(11) . ?
C34 C35 1.443(10) . ?
C35 C36 1.418(11) . ?
C36 C37 1.449(10) . ?
C38 C39 1.459(10) . ?
C39 C40 1.446(11) . ?
C40 C41 1.370(10) . ?
