#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:54:11 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179134 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/96/4309610.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4309610
loop_
_publ_author_name
'Yu-Bin Dong'
'Qiang Zhang'
'Le Wang'
'Jian-Ping Ma'
'Ru-Qi Huang'
'Da-Zhong Shen'
'De-Zhan Chen'
_publ_section_title
;
Organometallic Coordination Polymers Generated from Bent
Bis(acetylenylphenyl)oxadiazole Ligands and Ag(I) Salts
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6591
_journal_page_last               6608
_journal_paper_doi               10.1021/ic0508223
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C18 H12 Ag B F4 N2 O2'
_chemical_formula_weight         482.98
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 102.541(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   32.180(6)
_cell_length_b                   17.027(3)
_cell_length_c                   8.1453(15)
_cell_measurement_temperature    298(2)
_cell_volume                     4356.6(14)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0603
_diffrn_reflns_av_sigmaI/netI    0.0754
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -37
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            11567
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         2.28
_exptl_absorpt_coefficient_mu    0.972
_exptl_absorpt_correction_T_max  0.9263
_exptl_absorpt_correction_T_min  0.8074
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.473
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1904
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.08
_refine_diff_density_max         0.715
_refine_diff_density_min         -0.690
_refine_diff_density_rms         0.124
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     259
_refine_ls_number_reflns         4141
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.041
_refine_ls_R_factor_all          0.1100
_refine_ls_R_factor_gt           0.0720
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0985P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1718
_refine_ls_wR_factor_ref         0.1907
_reflns_number_gt                2751
_reflns_number_total             4141
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0508223si20050521_042346_6.cif
_cod_data_source_block           6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        4356.7(14)
_cod_database_code               4309610
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.148265(17) 0.60849(3) 0.06722(7) 0.0540(3) Uani 1 1 d . . .
N1 N 0.21166(17) 0.5408(3) 0.1171(6) 0.0432(13) Uani 1 1 d . . .
N2 N 0.11975(16) 0.5407(3) 0.2614(6) 0.0472(14) Uani 1 1 d . . .
C1 C 0.2501(2) 0.5621(4) 0.1467(8) 0.0437(15) Uani 1 1 d . . .
C2 C 0.2679(2) 0.6421(4) 0.1721(8) 0.0420(15) Uani 1 1 d . . .
C3 C 0.3021(2) 0.6636(4) 0.1086(8) 0.0456(16) Uani 1 1 d . . .
H3 H 0.3153 0.6272 0.0518 0.055 Uiso 1 1 calc R . .
C4 C 0.3174(2) 0.7415(4) 0.1297(8) 0.0493(17) Uani 1 1 d . . .
C5 C 0.3529(2) 0.7639(4) 0.0619(9) 0.0582(19) Uani 1 1 d . . .
C6 C 0.3849(3) 0.7742(5) 0.0102(12) 0.070(2) Uani 1 1 d . . .
H6 H 0.4099 0.7481 0.0047 0.084 Uiso 1 1 calc R . .
C7 C 0.2969(2) 0.7951(4) 0.2167(9) 0.0563(19) Uani 1 1 d . . .
H7 H 0.3066 0.8466 0.2319 0.068 Uiso 1 1 calc R . .
C8 C 0.2624(2) 0.7715(4) 0.2799(9) 0.0529(18) Uani 1 1 d . . .
H8 H 0.2489 0.8073 0.3371 0.064 Uiso 1 1 calc R . .
C9 C 0.2478(2) 0.6956(4) 0.2589(8) 0.0478(16) Uani 1 1 d . . .
H9 H 0.2246 0.6799 0.3023 0.057 Uiso 1 1 calc R . .
C10 C 0.1023(2) 0.5630(5) 0.3821(8) 0.0536(19) Uani 1 1 d . . .
C11 C 0.0956(3) 0.6408(5) 0.4383(8) 0.059(2) Uani 1 1 d . . .
C12 C 0.1221(3) 0.7012(5) 0.4105(9) 0.066(2) Uani 1 1 d . . .
H12 H 0.1448 0.6896 0.3612 0.079 Uiso 1 1 calc R . .
C13 C 0.1159(4) 0.7781(6) 0.4530(12) 0.081(3) Uani 1 1 d . . .
C14 C 0.1440(4) 0.8363(7) 0.4230(14) 0.100(4) Uani 1 1 d . . .
C15 C 0.1685(5) 0.8840(8) 0.395(2) 0.138(5) Uani 1 1 d . . .
H15 H 0.1876 0.9214 0.3730 0.166 Uiso 1 1 calc R . .
C16 C 0.0835(4) 0.7917(8) 0.5358(13) 0.106(4) Uani 1 1 d . . .
H16 H 0.0793 0.8427 0.5697 0.127 Uiso 1 1 calc R . .
C17 C 0.0568(4) 0.7332(8) 0.5710(14) 0.105(4) Uani 1 1 d . . .
H17 H 0.0353 0.7451 0.6268 0.127 Uiso 1 1 calc R . .
C18 C 0.0626(3) 0.6572(7) 0.5223(11) 0.084(3) Uani 1 1 d . . .
H18 H 0.0449 0.6172 0.5446 0.101 Uiso 1 1 calc R . .
O1 O 0.0891(2) 0.5000 0.4596(8) 0.0529(17) Uani 1 2 d S . .
O2 O 0.27730(18) 0.5000 0.1689(7) 0.0455(15) Uani 1 2 d S . .
O3 O 0.1230(3) 0.5000 -0.1400(8) 0.067(2) Uani 1 2 d S . .
H3A H 0.1372 0.5000 -0.2335 0.081 Uiso 1 2 calc SR . .
H3B H 0.0923 0.5000 -0.1810 0.081 Uiso 1 2 calc SR . .
O4 O 0.0364(3) 0.5000 0.7790(15) 0.139(4) Uani 1 2 d SD . .
B1 B 0.2189(4) 0.5000 0.6089(14) 0.055(3) Uani 1 2 d S . .
B2 B 0.0000 0.3238(16) 0.0000 0.39(4) Uiso 1 2 d SD . .
F1 F 0.2491(3) 0.5000 0.7560(10) 0.122(3) Uani 1 2 d S . .
F2 F 0.1807(2) 0.5000 0.6483(10) 0.110(3) Uani 1 2 d S . .
F3 F 0.2219(2) 0.4358(3) 0.5145(7) 0.124(2) Uani 1 1 d . . .
F5 F 0.0267(5) 0.2734(11) 0.096(2) 0.176(6) Uiso 0.50 1 d PD . .
F6 F 0.0175(6) 0.3431(13) -0.1326(19) 0.193(7) Uiso 0.50 1 d PD . .
H1O4 H 0.0094(8) 0.5000 0.76(4) 0.272 Uiso 1 2 d SD . .
H2O4 H 0.050(9) 0.5000 0.881(13) 0.751 Uiso 1 2 d SD . .
F4 F 0.0323(6) 0.3747(11) 0.042(3) 0.343(10) Uiso 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 Ag1 N1 145.9(3) 7_565 . ?
C6 Ag1 N2 113.3(3) 7_565 . ?
N1 Ag1 N2 95.62(18) . . ?
C6 Ag1 C5 29.6(2) 7_565 7_565 ?
N1 Ag1 C5 117.3(2) . 7_565 ?
N2 Ag1 C5 141.3(2) . 7_565 ?
C6 Ag1 O3 113.1(3) 7_565 . ?
N1 Ag1 O3 84.0(2) . . ?
N2 Ag1 O3 88.49(19) . . ?
C5 Ag1 O3 113.4(2) 7_565 . ?
C1 N1 N1 106.7(4) . 6_565 ?
C1 N1 Ag1 133.2(4) . . ?
N1 N1 Ag1 120.06(13) 6_565 . ?
C10 N2 N2 107.1(4) . 6_565 ?
C10 N2 Ag1 132.8(5) . . ?
N2 N2 Ag1 120.06(13) 6_565 . ?
N1 C1 O2 112.2(6) . . ?
N1 C1 C2 128.9(6) . . ?
O2 C1 C2 118.8(6) . . ?
C3 C2 C9 121.2(6) . . ?
C3 C2 C1 121.0(6) . . ?
C9 C2 C1 117.8(6) . . ?
C2 C3 C4 119.6(6) . . ?
C2 C3 H3 120.2 . . ?
C4 C3 H3 120.2 . . ?
C7 C4 C3 118.9(6) . . ?
C7 C4 C5 121.7(7) . . ?
C3 C4 C5 119.4(7) . . ?
C6 C5 C4 172.4(8) . . ?
C6 C5 Ag1 69.5(5) . 7_565 ?
C4 C5 Ag1 118.1(5) . 7_565 ?
C5 C6 Ag1 80.9(5) . 7_565 ?
C5 C6 H6 139.5 . . ?
Ag1 C6 H6 139.5 7_565 . ?
C8 C7 C4 120.2(7) . . ?
C8 C7 H7 119.9 . . ?
C4 C7 H7 119.9 . . ?
C9 C8 C7 120.5(7) . . ?
C9 C8 H8 119.7 . . ?
C7 C8 H8 119.7 . . ?
C8 C9 C2 119.6(7) . . ?
C8 C9 H9 120.2 . . ?
C2 C9 H9 120.2 . . ?
N2 C10 O1 110.7(7) . . ?
N2 C10 C11 129.5(7) . . ?
O1 C10 C11 119.8(6) . . ?
C12 C11 C18 119.1(8) . . ?
C12 C11 C10 119.6(7) . . ?
C18 C11 C10 121.3(9) . . ?
C13 C12 C11 122.5(9) . . ?
C13 C12 H12 118.7 . . ?
C11 C12 H12 118.7 . . ?
C12 C13 C16 116.6(11) . . ?
C12 C13 C14 119.7(10) . . ?
C16 C13 C14 123.6(11) . . ?
C15 C14 C13 178.0(14) . . ?
C14 C15 H15 180.0 . . ?
C13 C16 C17 123.3(11) . . ?
C13 C16 H16 118.4 . . ?
C17 C16 H16 118.4 . . ?
C18 C17 C16 119.2(10) . . ?
C18 C17 H17 120.4 . . ?
C16 C17 H17 120.4 . . ?
C17 C18 C11 119.2(11) . . ?
C17 C18 H18 120.4 . . ?
C11 C18 H18 120.4 . . ?
C10 O1 C10 104.2(7) . 6_565 ?
C1 O2 C1 102.1(7) 6_565 . ?
Ag1 O3 Ag1 94.5(2) . 6_565 ?
Ag1 O3 H3A 112.8 . . ?
Ag1 O3 H3A 112.8 6_565 . ?
Ag1 O3 H3B 112.8 . . ?
Ag1 O3 H3B 112.8 6_565 . ?
H3A O3 H3B 110.3 . . ?
H1O4 O4 H2O4 115(3) . . ?
F2 B1 F3 108.7(8) . . ?
F2 B1 F3 108.7(8) . 6_565 ?
F3 B1 F3 107.8(9) . 6_565 ?
F2 B1 F1 107.7(10) . . ?
F3 B1 F1 111.9(7) . . ?
F3 B1 F1 111.9(7) 6_565 . ?
F5 B2 F5 100(2) 2 . ?
F5 B2 F4 84.5(11) 2 2 ?
F5 B2 F4 158.1(13) . 2 ?
F5 B2 F4 158.1(13) 2 . ?
F5 B2 F4 84.5(11) . . ?
F4 B2 F4 99(2) 2 . ?
F5 B2 F6 107.0(13) 2 2 ?
F5 B2 F6 91.0(13) . 2 ?
F4 B2 F6 67.3(12) 2 2 ?
F4 B2 F6 94.2(17) . 2 ?
F5 B2 F6 91.0(13) 2 . ?
F5 B2 F6 107.0(13) . . ?
F4 B2 F6 94.2(17) 2 . ?
F4 B2 F6 67.3(12) . . ?
F6 B2 F6 152(3) 2 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C6 2.287(8) 7_565 ?
Ag1 N1 2.301(5) . ?
Ag1 N2 2.303(5) . ?
Ag1 C5 2.411(7) 7_565 ?
Ag1 O3 2.515(5) . ?
N1 C1 1.261(8) . ?
N1 N1 1.389(10) 6_565 ?
N2 C10 1.291(8) . ?
N2 N2 1.387(11) 6_565 ?
C1 O2 1.360(7) . ?
C1 C2 1.474(10) . ?
C2 C3 1.366(9) . ?
C2 C9 1.394(9) . ?
C3 C4 1.411(10) . ?
C3 H3 0.9300 . ?
C4 C7 1.405(10) . ?
C4 C5 1.426(10) . ?
C5 C6 1.206(10) . ?
C5 Ag1 2.411(7) 7_565 ?
C6 Ag1 2.287(8) 7_565 ?
C6 H6 0.9300 . ?
C7 C8 1.381(10) . ?
C7 H7 0.9300 . ?
C8 C9 1.373(9) . ?
C8 H8 0.9300 . ?
C9 H9 0.9300 . ?
C10 O1 1.359(8) . ?
C10 C11 1.432(11) . ?
C11 C12 1.385(12) . ?
C11 C18 1.411(11) . ?
C12 C13 1.379(12) . ?
C12 H12 0.9300 . ?
C13 C16 1.380(15) . ?
C13 C14 1.399(17) . ?
C14 C15 1.187(18) . ?
C15 H15 0.9300 . ?
C16 C17 1.384(16) . ?
C16 H16 0.9300 . ?
C17 C18 1.378(15) . ?
C17 H17 0.9300 . ?
C18 H18 0.9300 . ?
O1 C10 1.359(8) 6_565 ?
O2 C1 1.360(7) 6_565 ?
O3 Ag1 2.515(5) 6_565 ?
O3 H3A 0.9700 . ?
O3 H3B 0.9700 . ?
O4 H1O4 0.851(10) . ?
O4 H2O4 0.850(10) . ?
B1 F2 1.336(14) . ?
B1 F3 1.352(8) . ?
B1 F3 1.352(8) 6_565 ?
B1 F1 1.368(14) . ?
B2 F5 1.337(10) 2 ?
B2 F5 1.337(10) . ?
B2 F4 1.339(10) 2 ?
B2 F4 1.339(10) . ?
B2 F6 1.363(10) 2 ?
B2 F6 1.363(10) . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O3 H3B O4 0.97 1.76 2.719(14) 170.8 1_554
O3 H3A O1 0.97 2.64 3.206(9) 117.7 1_554
O3 H3A F2 0.97 1.86 2.796(11) 160.2 1_554
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6 Ag1 N1 C1 18.7(8) 7_565 . . . ?
N2 Ag1 N1 C1 -130.0(6) . . . . ?
C5 Ag1 N1 C1 28.8(6) 7_565 . . . ?
O3 Ag1 N1 C1 142.1(6) . . . . ?
C6 Ag1 N1 N1 -161.0(4) 7_565 . . 6_565 ?
N2 Ag1 N1 N1 50.32(15) . . . 6_565 ?
C5 Ag1 N1 N1 -150.8(2) 7_565 . . 6_565 ?
O3 Ag1 N1 N1 -37.57(15) . . . 6_565 ?
C6 Ag1 N2 C10 -32.3(7) 7_565 . . . ?
N1 Ag1 N2 C10 129.3(6) . . . . ?
C5 Ag1 N2 C10 -19.9(8) 7_565 . . . ?
O3 Ag1 N2 C10 -146.9(6) . . . . ?
C6 Ag1 N2 N2 148.1(2) 7_565 . . 6_565 ?
N1 Ag1 N2 N2 -50.32(15) . . . 6_565 ?
C5 Ag1 N2 N2 160.5(3) 7_565 . . 6_565 ?
O3 Ag1 N2 N2 33.53(17) . . . 6_565 ?
N1 N1 C1 O2 -0.5(6) 6_565 . . . ?
Ag1 N1 C1 O2 179.8(4) . . . . ?
N1 N1 C1 C2 -175.2(5) 6_565 . . . ?
Ag1 N1 C1 C2 5.1(10) . . . . ?
N1 C1 C2 C3 -141.3(7) . . . . ?
O2 C1 C2 C3 44.3(9) . . . . ?
N1 C1 C2 C9 36.9(9) . . . . ?
O2 C1 C2 C9 -137.5(6) . . . . ?
C9 C2 C3 C4 -0.5(9) . . . . ?
C1 C2 C3 C4 177.6(6) . . . . ?
C2 C3 C4 C7 0.3(9) . . . . ?
C2 C3 C4 C5 -179.5(6) . . . . ?
C7 C4 C5 C6 142(6) . . . . ?
C3 C4 C5 C6 -38(7) . . . . ?
C7 C4 C5 Ag1 -39.6(9) . . . 7_565 ?
C3 C4 C5 Ag1 140.2(5) . . . 7_565 ?
C4 C5 C6 Ag1 178(6) . . . 7_565 ?
C3 C4 C7 C8 -0.1(10) . . . . ?
C5 C4 C7 C8 179.6(6) . . . . ?
C4 C7 C8 C9 0.2(11) . . . . ?
C7 C8 C9 C2 -0.4(10) . . . . ?
C3 C2 C9 C8 0.6(10) . . . . ?
C1 C2 C9 C8 -177.6(6) . . . . ?
N2 N2 C10 O1 -2.3(6) 6_565 . . . ?
Ag1 N2 C10 O1 178.1(4) . . . . ?
N2 N2 C10 C11 178.1(6) 6_565 . . . ?
Ag1 N2 C10 C11 -1.5(11) . . . . ?
N2 C10 C11 C12 -25.7(11) . . . . ?
O1 C10 C11 C12 154.8(7) . . . . ?
N2 C10 C11 C18 154.5(8) . . . . ?
O1 C10 C11 C18 -25.0(10) . . . . ?
C18 C11 C12 C13 -3.9(12) . . . . ?
C10 C11 C12 C13 176.3(7) . . . . ?
C11 C12 C13 C16 4.2(12) . . . . ?
C11 C12 C13 C14 179.4(8) . . . . ?
C12 C13 C14 C15 8(43) . . . . ?
C16 C13 C14 C15 -177(100) . . . . ?
C12 C13 C16 C17 -2.4(15) . . . . ?
C14 C13 C16 C17 -177.3(11) . . . . ?
C13 C16 C17 C18 0.2(17) . . . . ?
C16 C17 C18 C11 0.2(15) . . . . ?
C12 C11 C18 C17 1.5(12) . . . . ?
C10 C11 C18 C17 -178.7(8) . . . . ?
N2 C10 O1 C10 3.5(9) . . . 6_565 ?
C11 C10 O1 C10 -176.8(4) . . . 6_565 ?
N1 C1 O2 C1 0.7(9) . . . 6_565 ?
C2 C1 O2 C1 176.1(3) . . . 6_565 ?
C6 Ag1 O3 Ag1 -159.5(3) 7_565 . . 6_565 ?
N1 Ag1 O3 Ag1 51.0(2) . . . 6_565 ?
N2 Ag1 O3 Ag1 -44.8(2) . . . 6_565 ?
C5 Ag1 O3 Ag1 168.2(2) 7_565 . . 6_565 ?
