#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:54:11 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179134 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/96/4309698.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4309698
loop_
_publ_author_name
'Neeladri Das'
'Ashutosh Ghosh'
'Atta M. Arif'
'Peter J. Stang'
_publ_section_title
;
Self-Assembly of Neutral Platinum-Based Supramolecular Ensembles
Incorporating Oxocarbon Dianions and Oxalate
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              7130
_journal_page_last               7137
_journal_paper_doi               10.1021/ic050919p
_journal_volume                  44
_journal_year                    2005
_chemical_formula_moiety         'C84 H136 O8 P8 Pt4, 2(C H2 Cl2)'
_chemical_formula_sum            'C86 H140 Cl4 O8 P8 Pt4'
_chemical_formula_weight         2471.90
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 104.6539(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   17.5260(3)
_cell_length_b                   14.8251(3)
_cell_length_c                   18.8229(3)
_cell_measurement_reflns_used    9708
_cell_measurement_temperature    150(1)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      1.018
_cell_volume                     4731.57(15)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius COLLECT'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'WinGX, Ortep3'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR97
_diffrn_ambient_temperature      150(1)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Nonius KappaCCD Diffractometer'
_diffrn_measurement_method       'Phi plus Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0269
_diffrn_reflns_av_sigmaI/netI    0.0485
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            18458
_diffrn_reflns_theta_full        27.46
_diffrn_reflns_theta_max         27.46
_diffrn_reflns_theta_min         2.24
_exptl_absorpt_coefficient_mu    6.194
_exptl_absorpt_correction_T_max  0.4568
_exptl_absorpt_correction_T_min  0.3066
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'DENZO-SMN (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.735
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prsim
_exptl_crystal_F_000             2440
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.15
_refine_diff_density_max         2.400
_refine_diff_density_min         -1.443
_refine_diff_density_rms         0.165
_refine_ls_extinction_coef       0.00033(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     522
_refine_ls_number_reflns         10795
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.040
_refine_ls_R_factor_all          0.0594
_refine_ls_R_factor_gt           0.0396
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0285P)²+21.4282P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0794
_refine_ls_wR_factor_ref         0.0867
_reflns_number_gt                8290
_reflns_number_total             10795
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic050919psi20050607_050759.cif
_cod_data_source_block           pjs220
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4309698
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.029959(11) 0.469196(14) 0.229638(10) 0.01741(7) Uani 1 1 d . . .
Pt2 Pt 0.260410(11) 0.535265(14) -0.041887(10) 0.01769(7) Uani 1 1 d . A .
P1 P 0.00519(9) 0.32899(10) 0.17566(8) 0.0244(3) Uani 1 1 d . . .
P2 P 0.05549(9) 0.61310(10) 0.27809(8) 0.0243(3) Uani 1 1 d . . .
P3 P 0.23901(9) 0.38345(10) -0.06321(8) 0.0245(3) Uani 1 1 d . . .
P4 P 0.29482(10) 0.68242(11) -0.01042(9) 0.0303(4) Uani 1 1 d . . .
O1 O 0.0959(2) 0.4976(3) 0.15182(19) 0.0232(8) Uani 1 1 d . A .
O2 O 0.2522(3) 0.4479(3) 0.2843(2) 0.0414(12) Uani 1 1 d . . .
O3 O 0.3609(3) 0.4797(4) 0.1688(3) 0.0500(13) Uani 1 1 d . A .
O4 O 0.1987(2) 0.5239(3) 0.0411(2) 0.0242(8) Uani 1 1 d . . .
C1 C 0.1702(3) 0.4903(4) 0.1597(3) 0.0222(12) Uani 1 1 d . . .
C2 C 0.2402(3) 0.4686(4) 0.2193(3) 0.0270(13) Uani 1 1 d . A .
C3 C 0.2905(4) 0.4827(4) 0.1661(3) 0.0316(14) Uani 1 1 d . . .
C4 C 0.2173(3) 0.5025(4) 0.1085(3) 0.0233(12) Uani 1 1 d . A .
C5 C 0.3044(3) 0.5488(4) -0.1301(3) 0.0210(11) Uani 1 1 d . . .
C6 C 0.3845(3) 0.5502(4) -0.1235(3) 0.0247(12) Uani 1 1 d . A .
H6 H 0.4191 0.5431 -0.0760 0.030 Uiso 1 1 calc R . .
C7 C 0.4177(3) 0.5615(4) -0.1841(3) 0.0276(13) Uani 1 1 d . . .
H7 H 0.4734 0.5614 -0.1767 0.033 Uiso 1 1 calc R A .
C8 C 0.3700(3) 0.5725(4) -0.2530(3) 0.0264(13) Uani 1 1 d . A .
H8 H 0.3925 0.5812 -0.2934 0.032 Uiso 1 1 calc R . .
C9 C 0.2864(3) 0.5709(4) -0.2646(3) 0.0220(11) Uani 1 1 d . . .
C10 C 0.2365(3) 0.5808(4) -0.3346(3) 0.0230(12) Uani 1 1 d . A .
H10 H 0.2594 0.5895 -0.3748 0.028 Uiso 1 1 calc R . .
C11 C 0.1541(3) 0.5786(4) -0.3486(3) 0.0210(11) Uani 1 1 d . . .
C12 C 0.1058(3) 0.5922(4) -0.4207(3) 0.0254(12) Uani 1 1 d . A .
H12 H 0.1292 0.6014 -0.4604 0.030 Uiso 1 1 calc R . .
C13 C 0.0258(3) 0.5918(4) -0.4327(3) 0.0276(13) Uani 1 1 d . . .
H13 H -0.0063 0.6019 -0.4809 0.033 Uiso 1 1 calc R A .
C14 C -0.0097(3) 0.5768(4) -0.3747(3) 0.0240(12) Uani 1 1 d . A .
H14 H -0.0656 0.5783 -0.3850 0.029 Uiso 1 1 calc R . .
C15 C 0.0327(3) 0.5598(4) -0.3033(3) 0.0204(11) Uani 1 1 d . . .
C16 C 0.1186(3) 0.5634(4) -0.2883(3) 0.0210(11) Uani 1 1 d . A .
C17 C 0.1700(3) 0.5534(4) -0.2176(3) 0.0199(11) Uani 1 1 d . . .
H17 H 0.1473 0.5430 -0.1775 0.024 Uiso 1 1 calc R A .
C18 C 0.2523(3) 0.5579(4) -0.2033(3) 0.0196(11) Uani 1 1 d . A .
C19 C -0.0430(4) 0.2483(4) 0.2222(4) 0.0359(15) Uani 1 1 d . . .
H19A H -0.0136 0.2463 0.2745 0.043 Uiso 1 1 calc R . .
H19B H -0.0967 0.2710 0.2202 0.043 Uiso 1 1 calc R . .
C20 C -0.0507(4) 0.1514(4) 0.1925(4) 0.0437(17) Uani 1 1 d . . .
H20A H -0.0773 0.1141 0.2218 0.066 Uiso 1 1 calc R . .
H20B H 0.0020 0.1268 0.1955 0.066 Uiso 1 1 calc R . .
H20C H -0.0815 0.1515 0.1412 0.066 Uiso 1 1 calc R . .
C21 C 0.0900(4) 0.2718(4) 0.1588(4) 0.0364(15) Uani 1 1 d . . .
H21A H 0.0718 0.2199 0.1258 0.044 Uiso 1 1 calc R . .
H21B H 0.1184 0.3137 0.1335 0.044 Uiso 1 1 calc R . .
C22 C 0.1462(4) 0.2384(6) 0.2286(4) 0.056(2) Uani 1 1 d . . .
H22A H 0.1911 0.2083 0.2165 0.084 Uiso 1 1 calc R . .
H22B H 0.1188 0.1956 0.2532 0.084 Uiso 1 1 calc R . .
H22C H 0.1651 0.2896 0.2612 0.084 Uiso 1 1 calc R . .
C23 C -0.0612(4) 0.3363(4) 0.0822(3) 0.0327(14) Uani 1 1 d . . .
H23A H -0.0734 0.2745 0.0627 0.039 Uiso 1 1 calc R . .
H23B H -0.1114 0.3647 0.0853 0.039 Uiso 1 1 calc R . .
C24 C -0.0275(4) 0.3890(5) 0.0295(3) 0.0415(16) Uani 1 1 d . . .
H24A H -0.0656 0.3903 -0.0187 0.062 Uiso 1 1 calc R . .
H24B H 0.0214 0.3604 0.0248 0.062 Uiso 1 1 calc R . .
H24C H -0.0163 0.4508 0.0477 0.062 Uiso 1 1 calc R . .
C25 C -0.0297(4) 0.6881(5) 0.2686(4) 0.0413(16) Uani 1 1 d . . .
H25A H -0.0106 0.7511 0.2723 0.050 Uiso 1 1 calc R . .
H25B H -0.0646 0.6800 0.2187 0.050 Uiso 1 1 calc R . .
C26 C -0.0786(4) 0.6750(5) 0.3235(4) 0.0465(18) Uani 1 1 d . . .
H26A H -0.1224 0.7181 0.3132 0.070 Uiso 1 1 calc R . .
H26B H -0.0456 0.6850 0.3732 0.070 Uiso 1 1 calc R . .
H26C H -0.0996 0.6134 0.3195 0.070 Uiso 1 1 calc R . .
C27 C 0.1032(3) 0.6195(5) 0.3757(3) 0.0336(14) Uani 1 1 d . . .
H27A H 0.1065 0.6835 0.3911 0.040 Uiso 1 1 calc R . .
H27B H 0.0703 0.5874 0.4032 0.040 Uiso 1 1 calc R . .
C28 C 0.1862(4) 0.5786(5) 0.3956(4) 0.0414(17) Uani 1 1 d . . .
H28A H 0.2088 0.5838 0.4487 0.062 Uiso 1 1 calc R . .
H28B H 0.2196 0.6110 0.3695 0.062 Uiso 1 1 calc R . .
H28C H 0.1833 0.5149 0.3815 0.062 Uiso 1 1 calc R . .
C29 C 0.1188(4) 0.6782(4) 0.2340(4) 0.0354(15) Uani 1 1 d . . .
H29A H 0.1667 0.6422 0.2351 0.043 Uiso 1 1 calc R . .
H29B H 0.0907 0.6873 0.1819 0.043 Uiso 1 1 calc R . .
C30 C 0.1442(5) 0.7696(6) 0.2681(5) 0.062(2) Uani 1 1 d . . .
H30A H 0.1782 0.7993 0.2412 0.092 Uiso 1 1 calc R . .
H30B H 0.1732 0.7616 0.3196 0.092 Uiso 1 1 calc R . .
H30C H 0.0974 0.8070 0.2657 0.092 Uiso 1 1 calc R . .
C31 C 0.1425(4) 0.3500(5) -0.0512(4) 0.0401(16) Uani 1 1 d . . .
H31A H 0.1358 0.3778 -0.0054 0.048 Uiso 1 1 calc R . .
H31B H 0.1014 0.3758 -0.0923 0.048 Uiso 1 1 calc R . .
C32 C 0.1272(5) 0.2479(5) -0.0478(5) 0.057(2) Uani 1 1 d . . .
H32A H 0.0741 0.2379 -0.0413 0.086 Uiso 1 1 calc R . .
H32B H 0.1662 0.2214 -0.0063 0.086 Uiso 1 1 calc R . .
H32C H 0.1316 0.2194 -0.0935 0.086 Uiso 1 1 calc R . .
C33 C 0.3094(4) 0.3182(4) 0.0064(4) 0.0393(16) Uani 1 1 d . . .
H33A H 0.2918 0.3181 0.0523 0.047 Uiso 1 1 calc R . .
H33B H 0.3092 0.2550 -0.0106 0.047 Uiso 1 1 calc R . .
C34 C 0.3939(4) 0.3544(5) 0.0228(4) 0.0481(19) Uani 1 1 d . . .
H34A H 0.4283 0.3167 0.0604 0.072 Uiso 1 1 calc R . .
H34B H 0.3949 0.4166 0.0407 0.072 Uiso 1 1 calc R . .
H34C H 0.4124 0.3531 -0.0221 0.072 Uiso 1 1 calc R . .
C35 C 0.2384(4) 0.3337(4) -0.1526(3) 0.0326(14) Uani 1 1 d . . .
H35A H 0.2134 0.2735 -0.1552 0.039 Uiso 1 1 calc R . .
H35B H 0.2043 0.3715 -0.1912 0.039 Uiso 1 1 calc R . .
C36 C 0.3181(4) 0.3224(5) -0.1716(4) 0.0418(17) Uani 1 1 d . . .
H36A H 0.3097 0.2951 -0.2204 0.063 Uiso 1 1 calc R . .
H36B H 0.3524 0.2833 -0.1351 0.063 Uiso 1 1 calc R . .
H36C H 0.3431 0.3816 -0.1714 0.063 Uiso 1 1 calc R . .
C37 C 0.4016(4) 0.6999(5) 0.0184(4) 0.0409(16) Uani 1 1 d . A .
H37A H 0.4241 0.6904 -0.0243 0.049 Uiso 1 1 calc R . .
H37B H 0.4124 0.7631 0.0348 0.049 Uiso 1 1 calc R . .
C38 C 0.4424(4) 0.6366(6) 0.0804(4) 0.052(2) Uani 1 1 d . . .
H38A H 0.4993 0.6487 0.0938 0.078 Uiso 1 1 calc R A .
H38B H 0.4330 0.5739 0.0641 0.078 Uiso 1 1 calc R . .
H38C H 0.4212 0.6466 0.1232 0.078 Uiso 1 1 calc R . .
C39 C 0.2583(10) 0.7575(10) -0.0953(12) 0.032(3) Uani 0.574(14) 1 d P A 1
H39A H 0.2835 0.7354 -0.1335 0.038 Uiso 0.574(14) 1 calc PR A 1
H39B H 0.2009 0.7468 -0.1139 0.038 Uiso 0.574(14) 1 calc PR A 1
C40 C 0.2706(12) 0.8586(12) -0.0898(11) 0.053(5) Uani 0.574(14) 1 d P A 1
H40A H 0.2484 0.8862 -0.1379 0.080 Uiso 0.574(14) 1 calc PR A 1
H40B H 0.3271 0.8718 -0.0739 0.080 Uiso 0.574(14) 1 calc PR A 1
H40C H 0.2442 0.8833 -0.0540 0.080 Uiso 0.574(14) 1 calc PR A 1
C41 C 0.2485(8) 0.7232(9) 0.0570(8) 0.034(3) Uani 0.574(14) 1 d P A 1
H41A H 0.1908 0.7246 0.0352 0.041 Uiso 0.574(14) 1 calc PR A 1
H41B H 0.2584 0.6795 0.0981 0.041 Uiso 0.574(14) 1 calc PR A 1
C42 C 0.2743(9) 0.8161(8) 0.0883(7) 0.049(4) Uani 0.574(14) 1 d P A 1
H42A H 0.2464 0.8313 0.1257 0.074 Uiso 0.574(14) 1 calc PR A 1
H42B H 0.2618 0.8609 0.0487 0.074 Uiso 0.574(14) 1 calc PR A 1
H42C H 0.3312 0.8159 0.1104 0.074 Uiso 0.574(14) 1 calc PR A 1
C39' C 0.2619(19) 0.769(2) -0.0718(14) 0.045(9) Uiso 0.426(14) 1 d P A 2
H39C H 0.2735 0.7523 -0.1189 0.054 Uiso 0.426(14) 1 calc PR A 2
H39D H 0.2037 0.7718 -0.0809 0.054 Uiso 0.426(14) 1 calc PR A 2
C40' C 0.2941(14) 0.8673(16) -0.0525(13) 0.044(5) Uani 0.426(14) 1 d P A 2
H40D H 0.2718 0.9077 -0.0938 0.066 Uiso 0.426(14) 1 calc PR A 2
H40E H 0.3518 0.8671 -0.0430 0.066 Uiso 0.426(14) 1 calc PR A 2
H40F H 0.2790 0.8885 -0.0087 0.066 Uiso 0.426(14) 1 calc PR A 2
C41' C 0.2790(11) 0.7241(13) 0.0810(10) 0.031(5) Uiso 0.426(14) 1 d P A 2
H41C H 0.2968 0.6768 0.1187 0.037 Uiso 0.426(14) 1 calc PR A 2
H41D H 0.3121 0.7782 0.0968 0.037 Uiso 0.426(14) 1 calc PR A 2
C42' C 0.1946(9) 0.7472(13) 0.0771(9) 0.044(5) Uani 0.426(14) 1 d P A 2
H42D H 0.1898 0.7656 0.1258 0.065 Uiso 0.426(14) 1 calc PR A 2
H42E H 0.1612 0.6943 0.0607 0.065 Uiso 0.426(14) 1 calc PR A 2
H42F H 0.1775 0.7969 0.0423 0.065 Uiso 0.426(14) 1 calc PR A 2
C43 C 0.0638(8) 0.9299(9) 0.0604(7) 0.065(4) Uiso 0.678(5) 1 d PD B 1
H43A H 0.1021 0.8794 0.0696 0.077 Uiso 0.678(5) 1 calc PR B 1
H43B H 0.0219 0.9165 0.0155 0.077 Uiso 0.678(5) 1 calc PR B 1
Cl1 Cl 0.0218(4) 0.9459(5) 0.1386(4) 0.154(3) Uiso 0.678(5) 1 d PD . .
Cl2 Cl 0.1095(6) 1.0287(6) 0.0512(5) 0.210(4) Uiso 0.678(5) 1 d PD . .
C43' C 0.0970(11) 0.9358(11) 0.0989(9) 0.055(6) Uiso 0.322(5) 1 d PD B 2
H43C H 0.0872 0.8833 0.0653 0.066 Uiso 0.322(5) 1 calc PR B 2
H43D H 0.1461 0.9240 0.1373 0.066 Uiso 0.322(5) 1 calc PR B 2
Cl1' Cl 0.0439(6) 0.8802(8) 0.0071(6) 0.103(3) Uiso 0.322(5) 1 d PD B 3
Cl2' Cl 0.0764(5) 0.8446(6) 0.0450(5) 0.077(3) Uiso 0.322(5) 1 d PD B 4
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C15 Pt1 O1 179.17(18) 3_565 . ?
C15 Pt1 P1 92.09(16) 3_565 . ?
O1 Pt1 P1 87.11(11) . . ?
C15 Pt1 P2 90.56(16) 3_565 . ?
O1 Pt1 P2 90.24(11) . . ?
P1 Pt1 P2 177.01(5) . . ?
C5 Pt2 O4 172.15(19) . . ?
C5 Pt2 P3 91.91(16) . . ?
O4 Pt2 P3 87.70(11) . . ?
C5 Pt2 P4 89.29(16) . . ?
O4 Pt2 P4 92.00(11) . . ?
P3 Pt2 P4 173.35(6) . . ?
C21 P1 C19 106.2(3) . . ?
C21 P1 C23 102.0(3) . . ?
C19 P1 C23 103.9(3) . . ?
C21 P1 Pt1 115.4(2) . . ?
C19 P1 Pt1 116.1(2) . . ?
C23 P1 Pt1 111.7(2) . . ?
C27 P2 C29 104.8(3) . . ?
C27 P2 C25 102.9(3) . . ?
C29 P2 C25 102.1(3) . . ?
C27 P2 Pt1 116.0(2) . . ?
C29 P2 Pt1 112.8(2) . . ?
C25 P2 Pt1 116.6(2) . . ?
C31 P3 C33 104.2(3) . . ?
C31 P3 C35 102.3(3) . . ?
C33 P3 C35 106.8(3) . . ?
C31 P3 Pt2 111.0(2) . . ?
C33 P3 Pt2 110.0(2) . . ?
C35 P3 Pt2 121.1(2) . . ?
C39' P4 C41 95.1(10) . . ?
C39' P4 C37 103.7(11) . . ?
C41 P4 C37 111.0(5) . . ?
C39' P4 C41' 105.1(10) . . ?
C41 P4 C41' 18.5(5) . . ?
C37 P4 C41' 93.3(6) . . ?
C39' P4 C39 13.4(11) . . ?
C41 P4 C39 106.3(7) . . ?
C37 P4 C39 105.4(5) . . ?
C41' P4 C39 117.9(8) . . ?
C39' P4 Pt2 120.8(9) . . ?
C41 P4 Pt2 111.6(4) . . ?
C37 P4 Pt2 113.1(2) . . ?
C41' P4 Pt2 116.7(6) . . ?
C39 P4 Pt2 109.0(6) . . ?
C1 O1 Pt1 128.2(3) . . ?
C4 O4 Pt2 135.0(4) . . ?
O1 C1 C4 130.9(5) . . ?
O1 C1 C2 137.4(5) . . ?
C4 C1 C2 91.7(4) . . ?
O2 C2 C1 135.5(5) . . ?
O2 C2 C3 135.7(5) . . ?
C1 C2 C3 88.8(4) . . ?
O3 C3 C4 135.5(6) . . ?
O3 C3 C2 136.2(6) . . ?
C4 C3 C2 88.3(4) . . ?
O4 C4 C1 131.4(5) . . ?
O4 C4 C3 137.4(5) . . ?
C1 C4 C3 91.2(4) . . ?
C6 C5 C18 117.8(5) . . ?
C6 C5 Pt2 121.5(4) . . ?
C18 C5 Pt2 120.7(4) . . ?
C5 C6 C7 123.1(5) . . ?
C5 C6 H6 118.4 . . ?
C7 C6 H6 118.4 . . ?
C8 C7 C6 120.1(5) . . ?
C8 C7 H7 119.9 . . ?
C6 C7 H7 119.9 . . ?
C7 C8 C9 120.2(5) . . ?
C7 C8 H8 119.9 . . ?
C9 C8 H8 119.9 . . ?
C10 C9 C8 121.1(5) . . ?
C10 C9 C18 119.0(5) . . ?
C8 C9 C18 119.9(5) . . ?
C9 C10 C11 123.0(5) . . ?
C9 C10 H10 118.5 . . ?
C11 C10 H10 118.5 . . ?
C10 C11 C12 120.8(5) . . ?
C10 C11 C16 119.0(5) . . ?
C12 C11 C16 120.2(5) . . ?
C13 C12 C11 119.8(5) . . ?
C13 C12 H12 120.1 . . ?
C11 C12 H12 120.1 . . ?
C12 C13 C14 120.7(5) . . ?
C12 C13 H13 119.6 . . ?
C14 C13 H13 119.6 . . ?
C15 C14 C13 123.3(5) . . ?
C15 C14 H14 118.4 . . ?
C13 C14 H14 118.4 . . ?
C14 C15 C16 117.1(5) . . ?
C14 C15 Pt1 117.0(4) . 3_565 ?
C16 C15 Pt1 125.9(4) . 3_565 ?
C17 C16 C11 117.2(5) . . ?
C17 C16 C15 124.0(5) . . ?
C11 C16 C15 118.8(5) . . ?
C18 C17 C16 123.9(5) . . ?
C18 C17 H17 118.1 . . ?
C16 C17 H17 118.1 . . ?
C17 C18 C9 117.9(5) . . ?
C17 C18 C5 123.3(5) . . ?
C9 C18 C5 118.8(5) . . ?
C20 C19 P1 116.7(4) . . ?
C20 C19 H19A 108.1 . . ?
P1 C19 H19A 108.1 . . ?
C20 C19 H19B 108.1 . . ?
P1 C19 H19B 108.1 . . ?
H19A C19 H19B 107.3 . . ?
C19 C20 H20A 109.5 . . ?
C19 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C19 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C22 C21 P1 112.7(5) . . ?
C22 C21 H21A 109.1 . . ?
P1 C21 H21A 109.1 . . ?
C22 C21 H21B 109.1 . . ?
P1 C21 H21B 109.1 . . ?
H21A C21 H21B 107.8 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C24 C23 P1 113.7(4) . . ?
C24 C23 H23A 108.8 . . ?
P1 C23 H23A 108.8 . . ?
C24 C23 H23B 108.8 . . ?
P1 C23 H23B 108.8 . . ?
H23A C23 H23B 107.7 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 P2 116.4(5) . . ?
C26 C25 H25A 108.2 . . ?
P2 C25 H25A 108.2 . . ?
C26 C25 H25B 108.2 . . ?
P2 C25 H25B 108.2 . . ?
H25A C25 H25B 107.4 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C28 C27 P2 113.1(4) . . ?
C28 C27 H27A 108.9 . . ?
P2 C27 H27A 109.0 . . ?
C28 C27 H27B 108.9 . . ?
P2 C27 H27B 108.9 . . ?
H27A C27 H27B 107.8 . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C30 C29 P2 115.3(5) . . ?
C30 C29 H29A 108.5 . . ?
P2 C29 H29A 108.5 . . ?
C30 C29 H29B 108.5 . . ?
P2 C29 H29B 108.5 . . ?
H29A C29 H29B 107.5 . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 P3 116.5(5) . . ?
C32 C31 H31A 108.2 . . ?
P3 C31 H31A 108.2 . . ?
C32 C31 H31B 108.2 . . ?
P3 C31 H31B 108.2 . . ?
H31A C31 H31B 107.3 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 P3 113.7(5) . . ?
C34 C33 H33A 108.8 . . ?
P3 C33 H33A 108.8 . . ?
C34 C33 H33B 108.8 . . ?
P3 C33 H33B 108.8 . . ?
H33A C33 H33B 107.7 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C36 C35 P3 117.5(5) . . ?
C36 C35 H35A 107.9 . . ?
P3 C35 H35A 107.9 . . ?
C36 C35 H35B 107.9 . . ?
P3 C35 H35B 107.9 . . ?
H35A C35 H35B 107.2 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 P4 112.7(5) . . ?
C38 C37 H37A 109.1 . . ?
P4 C37 H37A 109.1 . . ?
C38 C37 H37B 109.1 . . ?
P4 C37 H37B 109.1 . . ?
H37A C37 H37B 107.8 . . ?
C37 C38 H38A 109.5 . . ?
C37 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C37 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C40 C39 P4 120.3(15) . . ?
C40 C39 H39A 107.2 . . ?
P4 C39 H39A 107.2 . . ?
C40 C39 H39B 107.2 . . ?
P4 C39 H39B 107.2 . . ?
H39A C39 H39B 106.9 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C41 P4 116.0(9) . . ?
C42 C41 H41A 108.3 . . ?
P4 C41 H41A 108.3 . . ?
C42 C41 H41B 108.3 . . ?
P4 C41 H41B 108.3 . . ?
H41A C41 H41B 107.4 . . ?
C41 C42 H42A 109.5 . . ?
C41 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C41 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C40' C39' P4 119.7(18) . . ?
C40' C39' H39C 107.4 . . ?
P4 C39' H39C 107.4 . . ?
C40' C39' H39D 107.4 . . ?
P4 C39' H39D 107.4 . . ?
H39C C39' H39D 106.9 . . ?
C39' C40' H40D 109.5 . . ?
C39' C40' H40E 109.5 . . ?
H40D C40' H40E 109.5 . . ?
C39' C40' H40F 109.5 . . ?
H40D C40' H40F 109.5 . . ?
H40E C40' H40F 109.5 . . ?
C42' C41' P4 113.3(12) . . ?
C42' C41' H41C 108.9 . . ?
P4 C41' H41C 108.9 . . ?
C42' C41' H41D 108.9 . . ?
P4 C41' H41D 108.9 . . ?
H41C C41' H41D 107.7 . . ?
C41' C42' H42D 109.5 . . ?
C41' C42' H42E 109.5 . . ?
H42D C42' H42E 109.5 . . ?
C41' C42' H42F 109.5 . . ?
H42D C42' H42F 109.5 . . ?
H42E C42' H42F 109.5 . . ?
Cl2 C43 Cl1 105.5(8) . . ?
Cl2 C43 H43A 110.6 . . ?
Cl1 C43 H43A 110.6 . . ?
Cl2 C43 H43B 110.6 . . ?
Cl1 C43 H43B 110.6 . . ?
H43A C43 H43B 108.8 . . ?
C43' Cl1 C43 26.4(7) . . ?
C43' Cl2 C43 27.7(7) . . ?
Cl1 C43' Cl2 112.7(11) . . ?
Cl1 C43' H43C 109.0 . . ?
Cl2 C43' H43C 109.0 . . ?
Cl1 C43' H43D 109.0 . . ?
Cl2 C43' H43D 109.0 . . ?
H43C C43' H43D 107.8 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C15 2.022(5) 3_565 ?
Pt1 O1 2.125(3) . ?
Pt1 P1 2.3061(15) . ?
Pt1 P2 2.3188(15) . ?
Pt2 C5 2.010(5) . ?
Pt2 O4 2.119(3) . ?
Pt2 P3 2.3002(15) . ?
Pt2 P4 2.3007(16) . ?
P1 C21 1.807(6) . ?
P1 C19 1.813(6) . ?
P1 C23 1.851(6) . ?
P2 C27 1.818(6) . ?
P2 C29 1.821(6) . ?
P2 C25 1.834(7) . ?
P3 C31 1.831(6) . ?
P3 C33 1.832(7) . ?
P3 C35 1.835(6) . ?
P4 C39' 1.73(3) . ?
P4 C41 1.777(12) . ?
P4 C37 1.830(7) . ?
P4 C41' 1.913(18) . ?
P4 C39 1.920(17) . ?
O1 C1 1.277(7) . ?
O2 C2 1.228(7) . ?
O3 C3 1.222(7) . ?
O4 C4 1.268(6) . ?
C1 C4 1.431(7) . ?
C1 C2 1.472(8) . ?
C2 C3 1.506(8) . ?
C3 C4 1.485(8) . ?
C5 C6 1.378(7) . ?
C5 C18 1.453(7) . ?
C6 C7 1.415(8) . ?
C6 H6 0.9500 . ?
C7 C8 1.364(8) . ?
C7 H7 0.9500 . ?
C8 C9 1.426(8) . ?
C8 H8 0.9500 . ?
C9 C10 1.393(8) . ?
C9 C18 1.441(7) . ?
C10 C11 1.403(8) . ?
C10 H10 0.9500 . ?
C11 C12 1.421(8) . ?
C11 C16 1.443(7) . ?
C12 C13 1.362(8) . ?
C12 H12 0.9500 . ?
C13 C14 1.404(7) . ?
C13 H13 0.9500 . ?
C14 C15 1.384(7) . ?
C14 H14 0.9500 . ?
C15 C16 1.460(8) . ?
C15 Pt1 2.022(5) 3_565 ?
C16 C17 1.413(7) . ?
C17 C18 1.400(7) . ?
C17 H17 0.9500 . ?
C19 C20 1.534(9) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 C22 1.511(9) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C24 1.497(9) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.513(9) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 C28 1.532(9) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 C30 1.517(10) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.542(10) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.530(9) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 C36 1.537(8) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.528(10) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C39 C40 1.51(2) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 C42 1.521(16) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C39' C40' 1.57(4) . ?
C39' H39C 0.9900 . ?
C39' H39D 0.9900 . ?
C40' H40D 0.9800 . ?
C40' H40E 0.9800 . ?
C40' H40F 0.9800 . ?
C41' C42' 1.50(2) . ?
C41' H41C 0.9900 . ?
C41' H41D 0.9900 . ?
C42' H42D 0.9800 . ?
C42' H42E 0.9800 . ?
C42' H42F 0.9800 . ?
C43 Cl2 1.699(13) . ?
C43 Cl1 1.822(12) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
Cl1 C43' 1.679(16) . ?
Cl2 C43' 1.688(16) . ?
C43' H43C 0.9900 . ?
C43' H43D 0.9900 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C15 Pt1 P1 C21 -133.3(3) 3_565 . . . ?
O1 Pt1 P1 C21 46.5(3) . . . . ?
P2 Pt1 P1 C21 74.2(11) . . . . ?
C15 Pt1 P1 C19 -8.0(3) 3_565 . . . ?
O1 Pt1 P1 C19 171.8(3) . . . . ?
P2 Pt1 P1 C19 -160.6(10) . . . . ?
C15 Pt1 P1 C23 110.9(3) 3_565 . . . ?
O1 Pt1 P1 C23 -69.3(2) . . . . ?
P2 Pt1 P1 C23 -41.7(11) . . . . ?
C15 Pt1 P2 C27 56.5(3) 3_565 . . . ?
O1 Pt1 P2 C27 -123.3(2) . . . . ?
P1 Pt1 P2 C27 -150.9(10) . . . . ?
C15 Pt1 P2 C29 177.4(3) 3_565 . . . ?
O1 Pt1 P2 C29 -2.4(3) . . . . ?
P1 Pt1 P2 C29 -30.0(11) . . . . ?
C15 Pt1 P2 C25 -64.9(3) 3_565 . . . ?
O1 Pt1 P2 C25 115.3(3) . . . . ?
P1 Pt1 P2 C25 87.7(10) . . . . ?
C5 Pt2 P3 C31 -136.5(3) . . . . ?
O4 Pt2 P3 C31 35.7(3) . . . . ?
P4 Pt2 P3 C31 123.2(5) . . . . ?
C5 Pt2 P3 C33 108.7(3) . . . . ?
O4 Pt2 P3 C33 -79.1(3) . . . . ?
P4 Pt2 P3 C33 8.4(5) . . . . ?
C5 Pt2 P3 C35 -16.6(3) . . . . ?
O4 Pt2 P3 C35 155.5(3) . . . . ?
P4 Pt2 P3 C35 -116.9(5) . . . . ?
C5 Pt2 P4 C39' 55.4(12) . . . . ?
O4 Pt2 P4 C39' -116.8(12) . . . . ?
P3 Pt2 P4 C39' 155.9(12) . . . . ?
C5 Pt2 P4 C41 165.8(6) . . . . ?
O4 Pt2 P4 C41 -6.5(6) . . . . ?
P3 Pt2 P4 C41 -93.8(7) . . . . ?
C5 Pt2 P4 C37 -68.2(3) . . . . ?
O4 Pt2 P4 C37 119.6(3) . . . . ?
P3 Pt2 P4 C37 32.3(5) . . . . ?
C5 Pt2 P4 C41' -174.8(7) . . . . ?
O4 Pt2 P4 C41' 13.0(7) . . . . ?
P3 Pt2 P4 C41' -74.3(8) . . . . ?
C5 Pt2 P4 C39 48.6(5) . . . . ?
O4 Pt2 P4 C39 -123.6(5) . . . . ?
P3 Pt2 P4 C39 149.1(6) . . . . ?
C15 Pt1 O1 C1 -78(12) 3_565 . . . ?
P1 Pt1 O1 C1 -95.8(4) . . . . ?
P2 Pt1 O1 C1 85.6(4) . . . . ?
C5 Pt2 O4 C4 172.9(13) . . . . ?
P3 Pt2 O4 C4 85.7(5) . . . . ?
P4 Pt2 O4 C4 -87.7(5) . . . . ?
Pt1 O1 C1 C4 175.3(5) . . . . ?
Pt1 O1 C1 C2 -5.4(10) . . . . ?
O1 C1 C2 O2 1.4(13) . . . . ?
C4 C1 C2 O2 -179.1(8) . . . . ?
O1 C1 C2 C3 -178.6(7) . . . . ?
C4 C1 C2 C3 0.8(5) . . . . ?
O2 C2 C3 O3 -1.1(14) . . . . ?
C1 C2 C3 O3 178.9(8) . . . . ?
O2 C2 C3 C4 179.1(8) . . . . ?
C1 C2 C3 C4 -0.8(5) . . . . ?
Pt2 O4 C4 C1 -174.9(4) . . . . ?
Pt2 O4 C4 C3 7.2(11) . . . . ?
O1 C1 C4 O4 0.1(11) . . . . ?
C2 C1 C4 O4 -179.5(6) . . . . ?
O1 C1 C4 C3 178.7(6) . . . . ?
C2 C1 C4 C3 -0.9(5) . . . . ?
O3 C3 C4 O4 -0.5(14) . . . . ?
C2 C3 C4 O4 179.3(7) . . . . ?
O3 C3 C4 C1 -178.9(8) . . . . ?
C2 C3 C4 C1 0.8(5) . . . . ?
O4 Pt2 C5 C6 174.2(11) . . . . ?
P3 Pt2 C5 C6 -98.8(5) . . . . ?
P4 Pt2 C5 C6 74.7(5) . . . . ?
O4 Pt2 C5 C18 -5.5(17) . . . . ?
P3 Pt2 C5 C18 81.5(4) . . . . ?
P4 Pt2 C5 C18 -105.0(4) . . . . ?
C18 C5 C6 C7 1.1(8) . . . . ?
Pt2 C5 C6 C7 -178.6(4) . . . . ?
C5 C6 C7 C8 0.5(9) . . . . ?
C6 C7 C8 C9 -1.2(9) . . . . ?
C7 C8 C9 C10 -179.2(6) . . . . ?
C7 C8 C9 C18 0.2(9) . . . . ?
C8 C9 C10 C11 179.2(5) . . . . ?
C18 C9 C10 C11 -0.2(8) . . . . ?
C9 C10 C11 C12 177.9(5) . . . . ?
C9 C10 C11 C16 -1.4(8) . . . . ?
C10 C11 C12 C13 -178.5(6) . . . . ?
C16 C11 C12 C13 0.8(8) . . . . ?
C11 C12 C13 C14 -1.0(9) . . . . ?
C12 C13 C14 C15 -1.4(9) . . . . ?
C13 C14 C15 C16 3.8(8) . . . . ?
C13 C14 C15 Pt1 -175.6(5) . . . 3_565 ?
C10 C11 C16 C17 1.3(8) . . . . ?
C12 C11 C16 C17 -178.0(5) . . . . ?
C10 C11 C16 C15 -179.1(5) . . . . ?
C12 C11 C16 C15 1.7(8) . . . . ?
C14 C15 C16 C17 175.8(5) . . . . ?
Pt1 C15 C16 C17 -4.9(8) 3_565 . . . ?
C14 C15 C16 C11 -3.8(8) . . . . ?
Pt1 C15 C16 C11 175.5(4) 3_565 . . . ?
C11 C16 C17 C18 0.4(8) . . . . ?
C15 C16 C17 C18 -179.3(5) . . . . ?
C16 C17 C18 C9 -1.9(8) . . . . ?
C16 C17 C18 C5 179.1(5) . . . . ?
C10 C9 C18 C17 1.8(8) . . . . ?
C8 C9 C18 C17 -177.6(5) . . . . ?
C10 C9 C18 C5 -179.2(5) . . . . ?
C8 C9 C18 C5 1.4(8) . . . . ?
C6 C5 C18 C17 176.9(5) . . . . ?
Pt2 C5 C18 C17 -3.3(7) . . . . ?
C6 C5 C18 C9 -2.0(8) . . . . ?
Pt2 C5 C18 C9 177.7(4) . . . . ?
C21 P1 C19 C20 -42.8(6) . . . . ?
C23 P1 C19 C20 64.3(6) . . . . ?
Pt1 P1 C19 C20 -172.6(4) . . . . ?
C19 P1 C21 C22 -58.5(6) . . . . ?
C23 P1 C21 C22 -167.0(5) . . . . ?
Pt1 P1 C21 C22 71.7(6) . . . . ?
C21 P1 C23 C24 -61.0(6) . . . . ?
C19 P1 C23 C24 -171.3(5) . . . . ?
Pt1 P1 C23 C24 62.8(5) . . . . ?
C27 P2 C25 C26 -47.8(6) . . . . ?
C29 P2 C25 C26 -156.2(5) . . . . ?
Pt1 P2 C25 C26 80.4(5) . . . . ?
C29 P2 C27 C28 -61.1(6) . . . . ?
C25 P2 C27 C28 -167.5(5) . . . . ?
Pt1 P2 C27 C28 64.0(5) . . . . ?
C27 P2 C29 C30 -47.3(6) . . . . ?
C25 P2 C29 C30 59.7(6) . . . . ?
Pt1 P2 C29 C30 -174.3(5) . . . . ?
C33 P3 C31 C32 -49.3(6) . . . . ?
C35 P3 C31 C32 61.9(6) . . . . ?
Pt2 P3 C31 C32 -167.6(5) . . . . ?
C31 P3 C33 C34 -162.7(5) . . . . ?
C35 P3 C33 C34 89.5(6) . . . . ?
Pt2 P3 C33 C34 -43.7(6) . . . . ?
C31 P3 C35 C36 -162.0(5) . . . . ?
C33 P3 C35 C36 -52.8(6) . . . . ?
Pt2 P3 C35 C36 74.0(5) . . . . ?
C39' P4 C37 C38 173.1(10) . . . . ?
C41 P4 C37 C38 72.1(7) . . . . ?
C41' P4 C37 C38 66.7(8) . . . . ?
C39 P4 C37 C38 -173.2(8) . . . . ?
Pt2 P4 C37 C38 -54.3(6) . . . . ?
C39' P4 C39 C40 24(6) . . . . ?
C41 P4 C39 C40 57.5(14) . . . . ?
C37 P4 C39 C40 -60.4(14) . . . . ?
C41' P4 C39 C40 41.9(16) . . . . ?
Pt2 P4 C39 C40 178.0(12) . . . . ?
C39' P4 C41 C42 -60.7(15) . . . . ?
C37 P4 C41 C42 46.1(13) . . . . ?
C41' P4 C41 C42 63(2) . . . . ?
C39 P4 C41 C42 -68.0(13) . . . . ?
Pt2 P4 C41 C42 173.3(10) . . . . ?
C41 P4 C39' C40' 68(2) . . . . ?
C37 P4 C39' C40' -45(2) . . . . ?
C41' P4 C39' C40' 52(2) . . . . ?
C39 P4 C39' C40' -144(8) . . . . ?
Pt2 P4 C39' C40' -172.8(16) . . . . ?
C39' P4 C41' C42' 58.5(18) . . . . ?
C41 P4 C41' C42' -0.2(19) . . . . ?
C37 P4 C41' C42' 163.6(13) . . . . ?
C39 P4 C41' C42' 54.2(16) . . . . ?
Pt2 P4 C41' C42' -78.5(14) . . . . ?
Cl2 C43 Cl1 C43' -66.3(15) . . . . ?
Cl1 C43 Cl2 C43' 60.5(14) . . . . ?
C43 Cl1 C43' Cl2 74.3(17) . . . . ?
C43 Cl2 C43' Cl1 -80.7(18) . . . . ?
