#------------------------------------------------------------------------------
#$Date: 2023-12-08 16:16:31 +0200 (Fri, 08 Dec 2023) $
#$Revision: 288183 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/30/98/4309806.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4309806
loop_
_publ_author_name
'Mahé, N.'
'Guillou, O.'
'Daiguebonne, C.'
'Gérault, Y.'
'Caneschi, A.'
'Sangregorio, C.'
'Chane-Ching, J. Y.'
'Car, P. E.'
'Roisnel, T.'
_publ_section_title
;
 Polynuclear Lanthanide Hydroxo Complexes: New Chemical Precursors for
 Coordination Polymers
;
_journal_coden_ASTM              INOCAJ
_journal_issue                   22
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              7743
_journal_page_last               7750
_journal_paper_doi               10.1021/ic0401086
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'N8 O49 Yb6'
_chemical_formula_weight         1934.32
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                96.5240(7)
_cell_angle_beta                 108.7010(7)
_cell_angle_gamma                110.7920(11)
_cell_formula_units_Z            1
_cell_length_a                   9.99500(10)
_cell_length_b                   10.0266(2)
_cell_length_c                   11.3080(2)
_cell_measurement_temperature    298(2)
_cell_volume                     969.84(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0331
_diffrn_reflns_av_sigmaI/netI    0.0529
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            10145
_diffrn_reflns_theta_full        32.10
_diffrn_reflns_theta_max         32.10
_diffrn_reflns_theta_min         2.37
_exptl_absorpt_coefficient_mu    14.471
_exptl_crystal_density_diffrn    3.312
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             868
_refine_diff_density_max         3.546
_refine_diff_density_min         -3.650
_refine_diff_density_rms         0.331
_refine_ls_extinction_coef       0.0120(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.084
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     287
_refine_ls_number_reflns         6737
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.084
_refine_ls_R_factor_all          0.0429
_refine_ls_R_factor_gt           0.0360
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0373P)²+3.6139P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0851
_refine_ls_wR_factor_ref         0.0890
_reflns_number_gt                5985
_reflns_number_total             6737
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0401086_5.cif
_cod_data_source_block           ybno
_cod_depositor_comments
;
The following automatic conversions were performed:

data name '_atom_site_symetry_multiplicity' was replaced with
'_atom_site_symmetry_multiplicity' as specified in the replacement
file 'data/replacement-values/replacement_tags.lst'.

Automatic conversion script
Id: cif_correct_tags 9268 2022-04-12 08:56:07Z antanas 
;
_cod_database_code               4309806
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Yb1 Yb 0.64981(2) 0.76292(2) 0.52205(2) 0.01365(7) Uani 1 1 d . . .
Yb2 Yb 0.73981(2) 0.47993(2) 0.61547(2) 0.01253(7) Uani 1 1 d . . .
Yb3 Yb 0.47939(2) 0.56751(2) 0.70506(2) 0.01302(7) Uani 1 1 d . . .
O O 0.5000 0.5000 0.5000 0.0141(9) Uani 1 2 d S . .
O1 O 0.7478(4) 0.6064(4) 0.4578(4) 0.0163(7) Uani 1 1 d . . .
O2 O 0.7214(4) 0.6851(4) 0.7059(3) 0.0144(7) Uani 1 1 d . . .
O3 O 0.4589(4) 0.6325(4) 0.3200(4) 0.0153(7) Uani 1 1 d . . .
O4 O 0.4291(4) 0.7096(4) 0.5668(4) 0.0154(7) Uani 1 1 d . . .
N1 N 0.6750(6) 0.9765(6) 0.3660(5) 0.0255(10) Uani 1 1 d . . .
O11 O 0.5895(6) 0.9553(6) 0.4303(5) 0.0344(11) Uani 1 1 d . . .
O12 O 0.7438(6) 0.8924(6) 0.3677(6) 0.0373(12) Uani 1 1 d . . .
O13 O 0.6906(7) 1.0737(7) 0.3083(6) 0.0483(15) Uani 1 1 d . . .
N2 N 0.8932(6) 0.2822(5) 0.5994(5) 0.0208(9) Uani 1 1 d . . .
O21 O 0.9130(5) 0.3928(5) 0.5526(5) 0.0283(9) Uani 1 1 d . . .
O22 O 0.7925(5) 0.2517(5) 0.6491(4) 0.0259(9) Uani 1 1 d . . .
O23 O 0.9675(6) 0.2071(6) 0.5950(6) 0.0379(12) Uani 1 1 d . . .
N3 N 0.2430(6) 0.4972(7) 0.8121(5) 0.0248(11) Uani 1 1 d . . .
O31 O 0.1443(5) 0.4648(7) 0.8581(5) 0.0373(13) Uani 1 1 d . . .
O32 O 0.2550(5) 0.5878(5) 0.7439(4) 0.0271(9) Uani 1 1 d . . .
O33 O 0.3410(6) 0.4406(6) 0.8321(5) 0.0322(11) Uani 1 1 d . . .
OW11 O 0.9326(6) 0.9074(6) 0.6209(6) 0.0388(12) Uani 1 1 d . . .
OW12 O 0.7184(6) 0.9692(5) 0.6960(5) 0.0304(10) Uani 1 1 d . . .
OW21 O 1.0010(5) 0.6699(5) 0.7023(4) 0.0274(9) Uani 1 1 d . . .
OW22 O 0.8649(5) 0.4985(5) 0.8432(4) 0.0270(9) Uani 1 1 d . . .
OW31 O 0.5573(5) 0.8120(6) 0.8459(5) 0.0312(10) Uani 1 1 d . . .
OW32 O 0.6552(5) 0.5959(6) 0.9151(4) 0.0271(9) Uani 1 1 d . . .
N4 N 0.3195(8) 0.7875(7) 0.0390(6) 0.0372(14) Uani 1 1 d . . .
O41 O 0.4217(8) 0.7450(8) 0.0934(7) 0.0591(18) Uani 1 1 d . . .
O42 O 0.3289(8) 0.8526(8) -0.0455(6) 0.0537(17) Uani 1 1 d . . .
O43 O 0.2023(10) 0.7543(9) 0.0679(8) 0.068(2) Uani 1 1 d . . .
OW1 O 0.7691(10) 0.8982(9) 0.1031(7) 0.072(2) Uani 1 1 d . . .
OW2 O 0.0330(11) 0.1490(11) 0.0596(10) 0.108(4) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Yb1 O2 80.08(14) . . ?
O1 Yb1 O3 79.16(14) . . ?
O2 Yb1 O3 129.84(13) . . ?
O1 Yb1 O4 129.40(14) . . ?
O2 Yb1 O4 79.77(13) . . ?
O3 Yb1 O4 79.26(13) . . ?
O1 Yb1 OW12 140.77(16) . . ?
O2 Yb1 OW12 75.24(15) . . ?
O3 Yb1 OW12 139.81(16) . . ?
O4 Yb1 OW12 75.37(15) . . ?
O1 Yb1 OW11 75.78(16) . . ?
O2 Yb1 OW11 77.20(17) . . ?
O3 Yb1 OW11 138.58(16) . . ?
O4 Yb1 OW11 141.66(16) . . ?
OW12 Yb1 OW11 69.37(19) . . ?
O1 Yb1 O11 131.28(15) . . ?
O2 Yb1 O11 145.77(15) . . ?
O3 Yb1 O11 76.81(16) . . ?
O4 Yb1 O11 86.37(15) . . ?
OW12 Yb1 O11 71.00(17) . . ?
OW11 Yb1 O11 95.83(19) . . ?
O1 Yb1 O 64.78(9) . . ?
O2 Yb1 O 65.09(9) . . ?
O3 Yb1 O 64.76(9) . . ?
O4 Yb1 O 64.63(10) . . ?
OW12 Yb1 O 127.08(11) . . ?
OW11 Yb1 O 128.62(13) . . ?
O11 Yb1 O 134.82(13) . . ?
O1 Yb1 O12 82.15(15) . . ?
O2 Yb1 O12 145.13(16) . . ?
O3 Yb1 O12 74.91(16) . . ?
O4 Yb1 O12 133.81(15) . . ?
OW12 Yb1 O12 101.40(18) . . ?
OW11 Yb1 O12 69.45(19) . . ?
O11 Yb1 O12 50.92(17) . . ?
O Yb1 O12 131.18(14) . . ?
O1 Yb1 N1 107.08(15) . . ?
O2 Yb1 N1 154.87(14) . . ?
O3 Yb1 N1 75.24(14) . . ?
O4 Yb1 N1 110.70(15) . . ?
OW12 Yb1 N1 85.19(16) . . ?
OW11 Yb1 N1 81.26(17) . . ?
O11 Yb1 N1 25.47(16) . . ?
O Yb1 N1 139.96(11) . . ?
O12 Yb1 N1 25.48(16) . . ?
O1 Yb1 Yb3 98.79(9) . . ?
O2 Yb1 Yb3 41.06(9) . . ?
O3 Yb1 Yb3 98.81(9) . . ?
O4 Yb1 Yb3 41.35(10) . . ?
OW12 Yb1 Yb3 82.05(11) . . ?
OW11 Yb1 Yb3 117.13(14) . . ?
O11 Yb1 Yb3 126.29(12) . . ?
O Yb1 Yb3 45.035(5) . . ?
O12 Yb1 Yb3 173.41(13) . . ?
N1 Yb1 Yb3 151.57(11) . . ?
O1 Yb1 Yb2 41.69(9) . . ?
O2 Yb1 Yb2 41.14(10) . . ?
O3 Yb1 Yb2 98.67(10) . . ?
O4 Yb1 Yb2 98.35(10) . . ?
OW12 Yb1 Yb2 115.35(12) . . ?
OW11 Yb1 Yb2 83.86(13) . . ?
O11 Yb1 Yb2 172.82(11) . . ?
O Yb1 Yb2 44.784(5) . . ?
O12 Yb1 Yb2 122.76(12) . . ?
N1 Yb1 Yb2 148.22(11) . . ?
Yb3 Yb1 Yb2 59.541(6) . . ?
O2 Yb2 O3 80.96(13) . 2_666 ?
O2 Yb2 O4 131.12(13) . 2_666 ?
O3 Yb2 O4 79.65(13) 2_666 2_666 ?
O2 Yb2 O1 79.81(14) . . ?
O3 Yb2 O1 130.62(13) 2_666 . ?
O4 Yb2 O1 79.77(13) 2_666 . ?
O2 Yb2 OW21 75.16(14) . . ?
O3 Yb2 OW21 140.08(14) 2_666 . ?
O4 Yb2 OW21 139.66(15) 2_666 . ?
O1 Yb2 OW21 75.90(15) . . ?
O2 Yb2 O 65.78(9) . . ?
O3 Yb2 O 65.51(9) 2_666 . ?
O4 Yb2 O 65.34(9) 2_666 . ?
O1 Yb2 O 65.11(9) . . ?
OW21 Yb2 O 128.19(12) . . ?
O2 Yb2 OW22 79.59(15) . . ?
O3 Yb2 OW22 74.61(14) 2_666 . ?
O4 Yb2 OW22 135.62(15) 2_666 . ?
O1 Yb2 OW22 143.60(14) . . ?
OW21 Yb2 OW22 69.98(16) . . ?
O Yb2 OW22 129.96(11) . . ?
O2 Yb2 O21 143.69(14) . . ?
O3 Yb2 O21 132.16(14) 2_666 . ?
O4 Yb2 O21 77.19(15) 2_666 . ?
O1 Yb2 O21 85.14(15) . . ?
OW21 Yb2 O21 69.17(16) . . ?
O Yb2 O21 135.01(12) . . ?
OW22 Yb2 O21 94.15(17) . . ?
O2 Yb2 O22 147.11(14) . . ?
O3 Yb2 O22 82.55(13) 2_666 . ?
O4 Yb2 O22 72.67(14) 2_666 . ?
O1 Yb2 O22 131.65(14) . . ?
OW21 Yb2 O22 100.78(15) . . ?
O Yb2 O22 130.46(10) . . ?
OW22 Yb2 O22 68.66(16) . . ?
O21 Yb2 O22 50.75(14) . . ?
O2 Yb2 N2 154.47(13) . . ?
O3 Yb2 N2 107.86(14) 2_666 . ?
O4 Yb2 N2 74.41(13) 2_666 . ?
O1 Yb2 N2 108.95(14) . . ?
OW21 Yb2 N2 83.66(15) . . ?
O Yb2 N2 139.75(10) . . ?
OW22 Yb2 N2 79.88(16) . . ?
O21 Yb2 N2 25.19(14) . . ?
O22 Yb2 N2 25.60(13) . . ?
O2 Yb2 Yb3 41.46(9) . . ?
O3 Yb2 Yb3 42.28(10) 2_666 . ?
O4 Yb2 Yb3 99.81(9) 2_666 . ?
O1 Yb2 Yb3 99.02(10) . . ?
OW21 Yb2 Yb3 115.35(11) . . ?
O Yb2 Yb3 45.409(5) . . ?
OW22 Yb2 Yb3 84.71(12) . . ?
O21 Yb2 Yb3 174.42(10) . . ?
O22 Yb2 Yb3 123.99(9) . . ?
N2 Yb2 Yb3 149.59(10) . . ?
O2 Yb2 Yb1 41.27(9) . . ?
O3 Yb2 Yb1 100.01(10) 2_666 . ?
O4 Yb2 Yb1 99.67(10) 2_666 . ?
O1 Yb2 Yb1 41.28(10) . . ?
OW21 Yb2 Yb1 82.55(12) . . ?
O Yb2 Yb1 45.640(5) . . ?
OW22 Yb2 Yb1 119.84(12) . . ?
O21 Yb2 Yb1 124.74(11) . . ?
O22 Yb2 Yb1 171.47(11) . . ?
N2 Yb2 Yb1 149.67(10) . . ?
Yb3 Yb2 Yb1 60.178(6) . . ?
O2 Yb3 O4 80.53(13) . . ?
O2 Yb3 O3 80.77(13) . 2_666 ?
O4 Yb3 O3 130.59(13) . 2_666 ?
O2 Yb3 O1 130.57(13) . 2_666 ?
O4 Yb3 O1 79.93(14) . 2_666 ?
O3 Yb3 O1 78.53(14) 2_666 2_666 ?
O2 Yb3 OW32 74.31(14) . . ?
O4 Yb3 OW32 139.04(16) . . ?
O3 Yb3 OW32 76.61(15) 2_666 . ?
O1 Yb3 OW32 140.62(16) 2_666 . ?
O2 Yb3 O 65.72(9) . . ?
O4 Yb3 O 65.44(9) . . ?
O3 Yb3 O 65.17(9) 2_666 . ?
O1 Yb3 O 64.85(9) 2_666 . ?
OW32 Yb3 O 127.68(11) . . ?
O2 Yb3 O33 142.80(14) . . ?
O4 Yb3 O33 132.67(14) . . ?
O3 Yb3 O33 85.33(15) 2_666 . ?
O1 Yb3 O33 79.06(16) 2_666 . ?
OW32 Yb3 O33 68.94(16) . . ?
O Yb3 O33 136.55(14) . . ?
O2 Yb3 OW31 80.75(15) . . ?
O4 Yb3 OW31 74.81(16) . . ?
O3 Yb3 OW31 144.83(15) 2_666 . ?
O1 Yb3 OW31 135.26(15) 2_666 . ?
OW32 Yb3 OW31 69.69(18) . . ?
O Yb3 OW31 130.89(12) . . ?
O33 Yb3 OW31 91.67(18) . . ?
O2 Yb3 O32 147.89(15) . . ?
O4 Yb3 O32 81.78(14) . . ?
O3 Yb3 O32 130.54(15) 2_666 . ?
O1 Yb3 O32 71.49(15) 2_666 . ?
OW32 Yb3 O32 103.22(15) . . ?
O Yb3 O32 128.59(11) . . ?
O33 Yb3 O32 51.38(16) . . ?
OW31 Yb3 O32 68.83(16) . . ?
O2 Yb3 N3 156.00(14) . . ?
O4 Yb3 N3 107.09(15) . . ?
O3 Yb3 N3 108.42(15) 2_666 . ?
O1 Yb3 N3 73.42(14) 2_666 . ?
OW32 Yb3 N3 86.10(15) . . ?
O Yb3 N3 138.26(10) . . ?
O33 Yb3 N3 25.84(15) . . ?
OW31 Yb3 N3 79.51(16) . . ?
O32 Yb3 N3 25.54(16) . . ?
O2 Yb3 Yb2 41.59(10) . . ?
O4 Yb3 Yb2 99.58(9) . . ?
O3 Yb3 Yb2 41.95(9) 2_666 . ?
O1 Yb3 Yb2 98.70(10) 2_666 . ?
OW32 Yb3 Yb2 82.47(11) . . ?
O Yb3 Yb2 45.212(5) . . ?
O33 Yb3 Yb2 125.23(12) . . ?
OW31 Yb3 Yb2 121.34(11) . . ?
O32 Yb3 Yb2 169.79(11) . . ?
N3 Yb3 Yb2 150.08(12) . . ?
O2 Yb3 Yb1 41.32(9) . . ?
O4 Yb3 Yb1 41.89(9) . . ?
O3 Yb3 Yb1 99.80(9) 2_666 . ?
O1 Yb3 Yb1 99.69(9) 2_666 . ?
OW32 Yb3 Yb1 114.25(11) . . ?
O Yb3 Yb1 45.697(5) . . ?
O33 Yb3 Yb1 174.42(11) . . ?
OW31 Yb3 Yb1 85.41(12) . . ?
O32 Yb3 Yb1 123.04(11) . . ?
N3 Yb3 Yb1 148.58(12) . . ?
Yb2 Yb3 Yb1 60.282(6) . . ?
Yb2 O Yb2 180.0 2_666 . ?
Yb2 O Yb3 89.379(7) 2_666 2_666 ?
Yb2 O Yb3 90.621(7) . 2_666 ?
Yb2 O Yb3 90.621(7) 2_666 . ?
Yb2 O Yb3 89.379(7) . . ?
Yb3 O Yb3 180.0 2_666 . ?
Yb2 O Yb1 89.576(7) 2_666 2_666 ?
Yb2 O Yb1 90.424(7) . 2_666 ?
Yb3 O Yb1 89.268(7) 2_666 2_666 ?
Yb3 O Yb1 90.732(7) . 2_666 ?
Yb2 O Yb1 90.424(7) 2_666 . ?
Yb2 O Yb1 89.576(7) . . ?
Yb3 O Yb1 90.732(7) 2_666 . ?
Yb3 O Yb1 89.268(7) . . ?
Yb1 O Yb1 180.0 2_666 . ?
Yb1 O1 Yb2 97.03(14) . . ?
Yb1 O1 Yb3 98.33(14) . 2_666 ?
Yb2 O1 Yb3 96.70(14) . 2_666 ?
Yb3 O2 Yb2 96.94(14) . . ?
Yb3 O2 Yb1 97.61(13) . . ?
Yb2 O2 Yb1 97.58(14) . . ?
Yb2 O3 Yb1 97.79(14) 2_666 . ?
Yb2 O3 Yb3 95.77(14) 2_666 2_666 ?
Yb1 O3 Yb3 97.94(14) . 2_666 ?
Yb3 O4 Yb2 97.57(14) . 2_666 ?
Yb3 O4 Yb1 96.76(14) . . ?
Yb2 O4 Yb1 97.40(14) 2_666 . ?
O13 N1 O12 122.9(6) . . ?
O13 N1 O11 121.8(6) . . ?
O12 N1 O11 115.3(5) . . ?
O13 N1 Yb1 175.6(5) . . ?
O12 N1 Yb1 58.9(3) . . ?
O11 N1 Yb1 56.4(3) . . ?
N1 O11 Yb1 98.1(4) . . ?
N1 O12 Yb1 95.6(4) . . ?
O23 N2 O21 121.3(5) . . ?
O23 N2 O22 122.2(5) . . ?
O21 N2 O22 116.5(5) . . ?
O23 N2 Yb2 175.6(4) . . ?
O21 N2 Yb2 55.6(3) . . ?
O22 N2 Yb2 61.1(3) . . ?
N2 O21 Yb2 99.2(3) . . ?
N2 O22 Yb2 93.3(3) . . ?
O31 N3 O32 122.8(6) . . ?
O31 N3 O33 121.0(6) . . ?
O32 N3 O33 116.2(5) . . ?
O31 N3 Yb3 178.4(5) . . ?
O32 N3 Yb3 58.8(3) . . ?
O33 N3 Yb3 57.4(3) . . ?
N3 O32 Yb3 95.7(3) . . ?
N3 O33 Yb3 96.8(3) . . ?
O42 N4 O41 121.0(7) . . ?
O42 N4 O43 120.7(8) . . ?
O41 N4 O43 118.2(7) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Yb1 O1 2.289(4) . ?
Yb1 O2 2.292(4) . ?
Yb1 O3 2.308(4) . ?
Yb1 O4 2.313(4) . ?
Yb1 OW12 2.412(5) . ?
Yb1 OW11 2.457(5) . ?
Yb1 O11 2.457(5) . ?
Yb1 O 2.4623(2) . ?
Yb1 O12 2.513(5) . ?
Yb1 N1 2.919(5) . ?
Yb1 Yb3 3.4403(3) . ?
Yb1 Yb2 3.4438(3) . ?
Yb2 O2 2.286(4) . ?
Yb2 O3 2.297(4) 2_666 ?
Yb2 O4 2.305(4) 2_666 ?
Yb2 O1 2.308(4) . ?
Yb2 OW21 2.410(4) . ?
Yb2 O 2.4260(2) . ?
Yb2 OW22 2.427(4) . ?
Yb2 O21 2.447(5) . ?
Yb2 O22 2.566(5) . ?
Yb2 N2 2.927(5) . ?
Yb2 Yb3 3.4181(3) . ?
Yb3 O2 2.280(4) . ?
Yb3 O4 2.289(4) . ?
Yb3 O3 2.311(4) 2_666 ?
Yb3 O1 2.316(4) 2_666 ?
Yb3 OW32 2.372(4) . ?
Yb3 O 2.4343(2) . ?
Yb3 O33 2.457(4) . ?
Yb3 OW31 2.473(5) . ?
Yb3 O32 2.490(4) . ?
Yb3 N3 2.896(5) . ?
O Yb2 2.4260(2) 2_666 ?
O Yb3 2.4343(2) 2_666 ?
O Yb1 2.4623(2) 2_666 ?
O1 Yb3 2.316(4) 2_666 ?
O3 Yb2 2.297(4) 2_666 ?
O3 Yb3 2.311(4) 2_666 ?
O4 Yb2 2.305(4) 2_666 ?
N1 O13 1.226(7) . ?
N1 O12 1.262(7) . ?
N1 O11 1.268(7) . ?
N2 O23 1.238(7) . ?
N2 O21 1.262(7) . ?
N2 O22 1.267(6) . ?
N3 O31 1.221(6) . ?
N3 O32 1.255(7) . ?
N3 O33 1.271(7) . ?
N4 O42 1.226(8) . ?
N4 O41 1.253(9) . ?
N4 O43 1.258(9) . ?
