#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:32:23 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179145 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/06/4310639.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4310639
loop_
_publ_author_name
'J. R. Salvador'
'J. R. Gour'
'D. Bilc'
'S. D. Mahanti'
'M. G. Kanatzidis'
_publ_section_title
;
 Stabilization of New Forms of the Intermetallic Phases β-RENiGe2 (RE =
 Dy, Ho, Er, Tm, Yb, Lu) in Liquid Indium
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1403
_journal_page_last               1410
_journal_paper_doi               10.1021/ic035303j
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'Ge2 Ni Yb'
_chemical_formula_weight         376.93
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   4.0935(6)
_cell_length_b                   8.4277(13)
_cell_length_c                   15.751(2)
_cell_measurement_temperature    293(2)
_cell_volume                     543.39(13)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0602
_diffrn_reflns_av_sigmaI/netI    0.0294
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            2432
_diffrn_reflns_theta_full        27.15
_diffrn_reflns_theta_max         27.15
_diffrn_reflns_theta_min         2.59
_exptl_absorpt_coefficient_mu    62.466
_exptl_crystal_density_diffrn    9.215
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             648
_refine_diff_density_max         7.009
_refine_diff_density_min         -4.913
_refine_diff_density_rms         1.405
_refine_ls_extinction_coef       0.0055(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.183
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     30
_refine_ls_number_reflns         377
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.183
_refine_ls_R_factor_all          0.0454
_refine_ls_R_factor_gt           0.0443
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0745P)²+3.7140P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1018
_refine_ls_wR_factor_ref         0.1033
_reflns_number_gt                359
_reflns_number_total             377
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic035303jsi20031111_122754_3.cif
_cod_data_source_block           ybnige2m
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        543.40(14)
_cod_database_code               4310639
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Yb1 Yb 0.0000 0.0000 0.29667(4) 0.0061(4) Uani 1 4 d S . .
Yb2 Yb 0.0000 0.23885(9) 0.5000 0.0087(4) Uani 1 4 d S . .
Ge3 Ge 0.0000 0.34296(15) 0.30344(8) 0.0087(5) Uani 1 2 d S . .
Ge2 Ge 0.0000 0.0000 0.07936(13) 0.0144(5) Uani 1 4 d S . .
Ge1 Ge -0.5000 0.0000 0.42308(12) 0.0074(5) Uani 1 4 d S . .
Ni Ni 0.0000 0.25151(18) 0.14754(12) 0.0083(5) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge1 Yb1 Ge1 91.58(6) 1_655 . ?
Ge1 Yb1 Ge3 88.53(2) 1_655 . ?
Ge1 Yb1 Ge3 88.53(2) . . ?
Ge1 Yb1 Ge3 88.53(2) 1_655 2 ?
Ge1 Yb1 Ge3 88.53(2) . 2 ?
Ge3 Yb1 Ge3 175.77(6) . 2 ?
Ge1 Yb1 Ge3 152.15(3) 1_655 14_445 ?
Ge1 Yb1 Ge3 82.73(3) . 14_445 ?
Ge3 Yb1 Ge3 118.40(3) . 14_445 ?
Ge3 Yb1 Ge3 64.18(3) 2 14_445 ?
Ge1 Yb1 Ge3 82.73(3) 1_655 13 ?
Ge1 Yb1 Ge3 152.15(3) . 13 ?
Ge3 Yb1 Ge3 64.18(3) . 13 ?
Ge3 Yb1 Ge3 118.40(3) 2 13 ?
Ge3 Yb1 Ge3 114.19(5) 14_445 13 ?
Ge1 Yb1 Ge3 152.15(3) 1_655 13_455 ?
Ge1 Yb1 Ge3 82.73(3) . 13_455 ?
Ge3 Yb1 Ge3 64.18(3) . 13_455 ?
Ge3 Yb1 Ge3 118.40(3) 2 13_455 ?
Ge3 Yb1 Ge3 54.24(5) 14_445 13_455 ?
Ge3 Yb1 Ge3 89.67(4) 13 13_455 ?
Ge1 Yb1 Ge3 82.73(3) 1_655 14_545 ?
Ge1 Yb1 Ge3 152.15(3) . 14_545 ?
Ge3 Yb1 Ge3 118.40(3) . 14_545 ?
Ge3 Yb1 Ge3 64.18(3) 2 14_545 ?
Ge3 Yb1 Ge3 89.67(4) 14_445 14_545 ?
Ge3 Yb1 Ge3 54.24(5) 13 14_545 ?
Ge3 Yb1 Ge3 114.19(5) 13_455 14_545 ?
Ge1 Yb1 Ni 47.14(3) 1_655 13 ?
Ge1 Yb1 Ni 106.23(4) . 13 ?
Ge3 Yb1 Ni 45.96(2) . 13 ?
Ge3 Yb1 Ni 132.37(3) 2 13 ?
Ge3 Yb1 Ni 160.12(4) 14_445 13 ?
Ge3 Yb1 Ni 51.09(4) 13 13 ?
Ge3 Yb1 Ni 108.41(4) 13_455 13 ?
Ge3 Yb1 Ni 89.79(3) 14_545 13 ?
Ge1 Yb1 Ni 106.23(4) 1_655 14_445 ?
Ge1 Yb1 Ni 47.14(3) . 14_445 ?
Ge3 Yb1 Ni 132.37(3) . 14_445 ?
Ge3 Yb1 Ni 45.96(2) 2 14_445 ?
Ge3 Yb1 Ni 51.09(4) 14_445 14_445 ?
Ge3 Yb1 Ni 160.12(4) 13 14_445 ?
Ge3 Yb1 Ni 89.79(3) 13_455 14_445 ?
Ge3 Yb1 Ni 108.41(4) 14_545 14_445 ?
Ni Yb1 Ni 146.60(8) 13 14_445 ?
Ge1 Yb1 Ni 47.14(3) 1_655 14_545 ?
Ge1 Yb1 Ni 106.23(4) . 14_545 ?
Ge3 Yb1 Ni 132.37(3) . 14_545 ?
Ge3 Yb1 Ni 45.96(2) 2 14_545 ?
Ge3 Yb1 Ni 108.41(4) 14_445 14_545 ?
Ge3 Yb1 Ni 89.79(3) 13 14_545 ?
Ge3 Yb1 Ni 160.12(4) 13_455 14_545 ?
Ge3 Yb1 Ni 51.09(4) 14_545 14_545 ?
Ni Yb1 Ni 86.47(5) 13 14_545 ?
Ni Yb1 Ni 84.05(4) 14_445 14_545 ?
Ge1 Yb1 Ni 106.23(4) 1_655 13_455 ?
Ge1 Yb1 Ni 47.14(3) . 13_455 ?
Ge3 Yb1 Ni 45.96(2) . 13_455 ?
Ge3 Yb1 Ni 132.37(3) 2 13_455 ?
Ge3 Yb1 Ni 89.79(3) 14_445 13_455 ?
Ge3 Yb1 Ni 108.41(4) 13 13_455 ?
Ge3 Yb1 Ni 51.09(4) 13_455 13_455 ?
Ge3 Yb1 Ni 160.12(4) 14_545 13_455 ?
Ni Yb1 Ni 84.05(4) 13 13_455 ?
Ni Yb1 Ni 86.47(5) 14_445 13_455 ?
Ni Yb1 Ni 146.60(8) 14_545 13_455 ?
Ni Yb2 Ni 82.71(5) 6 6_455 ?
Ni Yb2 Ni 176.99(6) 6 13_455 ?
Ni Yb2 Ni 97.21(5) 6_455 13_455 ?
Ni Yb2 Ni 97.21(5) 6 13 ?
Ni Yb2 Ni 176.99(6) 6_455 13 ?
Ni Yb2 Ni 82.71(5) 13_455 13 ?
Ni Yb2 Ge1 137.96(4) 6 . ?
Ni Yb2 Ge1 82.80(4) 6_455 . ?
Ni Yb2 Ge1 44.87(4) 13_455 . ?
Ni Yb2 Ge1 99.16(4) 13 . ?
Ni Yb2 Ge1 99.16(4) 6 9_456 ?
Ni Yb2 Ge1 44.87(4) 6_455 9_456 ?
Ni Yb2 Ge1 82.80(4) 13_455 9_456 ?
Ni Yb2 Ge1 137.96(4) 13 9_456 ?
Ge1 Yb2 Ge1 45.76(7) . 9_456 ?
Ni Yb2 Ge1 44.87(4) 6 9_556 ?
Ni Yb2 Ge1 99.16(4) 6_455 9_556 ?
Ni Yb2 Ge1 137.96(4) 13_455 9_556 ?
Ni Yb2 Ge1 82.80(4) 13 9_556 ?
Ge1 Yb2 Ge1 99.52(3) . 9_556 ?
Ge1 Yb2 Ge1 82.12(3) 9_456 9_556 ?
Ni Yb2 Ge1 82.80(4) 6 1_655 ?
Ni Yb2 Ge1 137.96(4) 6_455 1_655 ?
Ni Yb2 Ge1 99.16(4) 13_455 1_655 ?
Ni Yb2 Ge1 44.87(4) 13 1_655 ?
Ge1 Yb2 Ge1 82.12(3) . 1_655 ?
Ge1 Yb2 Ge1 99.52(3) 9_456 1_655 ?
Ge1 Yb2 Ge1 45.76(7) 9_556 1_655 ?
Ni Yb2 Ge3 135.61(3) 6 . ?
Ni Yb2 Ge3 135.61(3) 6_455 . ?
Ni Yb2 Ge3 43.20(3) 13_455 . ?
Ni Yb2 Ge3 43.20(3) 13 . ?
Ge1 Yb2 Ge3 78.58(4) . . ?
Ge1 Yb2 Ge3 123.38(4) 9_456 . ?
Ge1 Yb2 Ge3 123.38(4) 9_556 . ?
Ge1 Yb2 Ge3 78.58(4) 1_655 . ?
Ni Yb2 Ge3 43.20(3) 6 10_556 ?
Ni Yb2 Ge3 43.20(3) 6_455 10_556 ?
Ni Yb2 Ge3 135.61(3) 13_455 10_556 ?
Ni Yb2 Ge3 135.61(3) 13 10_556 ?
Ge1 Yb2 Ge3 123.38(4) . 10_556 ?
Ge1 Yb2 Ge3 78.58(4) 9_456 10_556 ?
Ge1 Yb2 Ge3 78.58(4) 9_556 10_556 ?
Ge1 Yb2 Ge3 123.38(4) 1_655 10_556 ?
Ge3 Yb2 Ge3 148.35(5) . 10_556 ?
Ni Yb2 Ge2 43.84(4) 6 5 ?
Ni Yb2 Ge2 96.29(4) 6_455 5 ?
Ni Yb2 Ge2 133.30(4) 13_455 5 ?
Ni Yb2 Ge2 81.66(4) 13 5 ?
Ge1 Yb2 Ge2 177.62(2) . 5 ?
Ge1 Yb2 Ge2 134.47(5) 9_456 5 ?
Ge1 Yb2 Ge2 82.79(2) 9_556 5 ?
Ge1 Yb2 Ge2 99.97(2) 1_655 5 ?
Ge3 Yb2 Ge2 100.67(4) . 5 ?
Ge3 Yb2 Ge2 56.37(4) 10_556 5 ?
Ni Yb2 Ge2 96.29(4) 6 5_455 ?
Ni Yb2 Ge2 43.84(4) 6_455 5_455 ?
Ni Yb2 Ge2 81.66(4) 13_455 5_455 ?
Ni Yb2 Ge2 133.30(4) 13 5_455 ?
Ge1 Yb2 Ge2 99.97(2) . 5_455 ?
Ge1 Yb2 Ge2 82.79(2) 9_456 5_455 ?
Ge1 Yb2 Ge2 134.47(5) 9_556 5_455 ?
Ge1 Yb2 Ge2 177.62(2) 1_655 5_455 ?
Ge3 Yb2 Ge2 100.67(4) . 5_455 ?
Ge3 Yb2 Ge2 56.37(4) 10_556 5_455 ?
Ge2 Yb2 Ge2 77.92(3) 5 5_455 ?
Ni Ge3 Ni 123.10(9) 13 13_455 ?
Ni Ge3 Ni 102.36(6) 13 . ?
Ni Ge3 Ni 102.36(6) 13_455 . ?
Ni Ge3 Ge3 110.00(5) 13 2_565 ?
Ni Ge3 Ge3 110.00(5) 13_455 2_565 ?
Ni Ge3 Ge3 107.42(5) . 2_565 ?
Ni Ge3 Yb1 70.76(5) 13 . ?
Ni Ge3 Yb1 70.76(5) 13_455 . ?
Ni Ge3 Yb1 70.46(5) . . ?
Ge3 Ge3 Yb1 177.89(3) 2_565 . ?
Ni Ge3 Yb1 73.51(4) 13 13 ?
Ni Ge3 Yb1 162.93(6) 13_455 13 ?
Ni Ge3 Yb1 67.56(4) . 13 ?
Ge3 Ge3 Yb1 62.88(2) 2_565 13 ?
Yb1 Ge3 Yb1 115.82(3) . 13 ?
Ni Ge3 Yb1 162.93(6) 13 13_455 ?
Ni Ge3 Yb1 73.51(4) 13_455 13_455 ?
Ni Ge3 Yb1 67.56(4) . 13_455 ?
Ge3 Ge3 Yb1 62.88(2) 2_565 13_455 ?
Yb1 Ge3 Yb1 115.82(3) . 13_455 ?
Yb1 Ge3 Yb1 89.67(4) 13 13_455 ?
Ni Ge3 Yb2 65.65(5) 13 . ?
Ni Ge3 Yb2 65.65(5) 13_455 . ?
Ni Ge3 Yb2 146.75(6) . . ?
Ge3 Ge3 Yb2 105.82(3) 2_565 . ?
Yb1 Ge3 Yb2 76.29(3) . . ?
Yb1 Ge3 Yb2 130.31(3) 13 . ?
Yb1 Ge3 Yb2 130.31(3) 13_455 . ?
Ni Ge2 Ni 126.26(13) . 2 ?
Ni Ge2 Ge2 116.87(6) . 9 ?
Ni Ge2 Ge2 116.87(6) 2 9 ?
Ni Ge2 Yb2 140.960(11) . 5_444 ?
Ni Ge2 Yb2 64.56(4) 2 5_444 ?
Ge2 Ge2 Yb2 67.42(3) 9 5_444 ?
Ni Ge2 Yb2 64.56(4) . 13 ?
Ni Ge2 Yb2 140.960(11) 2 13 ?
Ge2 Ge2 Yb2 67.42(3) 9 13 ?
Yb2 Ge2 Yb2 134.83(7) 5_444 13 ?
Ni Ge2 Yb2 140.960(11) . 5_544 ?
Ni Ge2 Yb2 64.56(4) 2 5_544 ?
Ge2 Ge2 Yb2 67.42(3) 9 5_544 ?
Yb2 Ge2 Yb2 77.92(3) 5_444 5_544 ?
Yb2 Ge2 Yb2 85.09(3) 13 5_544 ?
Ni Ge2 Yb2 64.56(4) . 13_455 ?
Ni Ge2 Yb2 140.960(11) 2 13_455 ?
Ge2 Ge2 Yb2 67.42(3) 9 13_455 ?
Yb2 Ge2 Yb2 85.09(3) 5_444 13_455 ?
Yb2 Ge2 Yb2 77.92(3) 13 13_455 ?
Yb2 Ge2 Yb2 134.83(7) 5_544 13_455 ?
Ni Ge2 Yb1 63.13(6) . . ?
Ni Ge2 Yb1 63.13(6) 2 . ?
Ge2 Ge2 Yb1 180.0 9 . ?
Yb2 Ge2 Yb1 112.58(3) 5_444 . ?
Yb2 Ge2 Yb1 112.58(3) 13 . ?
Yb2 Ge2 Yb1 112.58(3) 5_544 . ?
Yb2 Ge2 Yb1 112.58(3) 13_455 . ?
Ni Ge1 Ni 124.04(12) 14_445 13_455 ?
Ni Ge1 Ge1 117.98(6) 14_445 9_456 ?
Ni Ge1 Ge1 117.98(6) 13_455 9_456 ?
Ni Ge1 Yb1 70.91(5) 14_445 . ?
Ni Ge1 Yb1 70.91(5) 13_455 . ?
Ge1 Ge1 Yb1 134.21(3) 9_456 . ?
Ni Ge1 Yb1 70.90(5) 14_445 1_455 ?
Ni Ge1 Yb1 70.90(5) 13_455 1_455 ?
Ge1 Ge1 Yb1 134.21(3) 9_456 1_455 ?
Yb1 Ge1 Yb1 91.58(6) . 1_455 ?
Ni Ge1 Yb2 67.16(3) 14_445 9_456 ?
Ni Ge1 Yb2 138.844(12) 13_455 9_456 ?
Ge1 Ge1 Yb2 67.12(3) 9_456 9_456 ?
Yb1 Ge1 Yb2 137.90(3) . 9_456 ?
Yb1 Ge1 Yb2 78.481(14) 1_455 9_456 ?
Ni Ge1 Yb2 138.844(12) 14_445 1_455 ?
Ni Ge1 Yb2 67.16(3) 13_455 1_455 ?
Ge1 Ge1 Yb2 67.12(3) 9_456 1_455 ?
Yb1 Ge1 Yb2 137.90(3) . 1_455 ?
Yb1 Ge1 Yb2 78.481(14) 1_455 1_455 ?
Yb2 Ge1 Yb2 80.48(3) 9_456 1_455 ?
Ni Ge1 Yb2 67.16(3) 14_445 9_556 ?
Ni Ge1 Yb2 138.844(12) 13_455 9_556 ?
Ge1 Ge1 Yb2 67.12(3) 9_456 9_556 ?
Yb1 Ge1 Yb2 78.480(14) . 9_556 ?
Yb1 Ge1 Yb2 137.90(3) 1_455 9_556 ?
Yb2 Ge1 Yb2 82.12(3) 9_456 9_556 ?
Yb2 Ge1 Yb2 134.24(7) 1_455 9_556 ?
Ni Ge1 Yb2 138.845(12) 14_445 . ?
Ni Ge1 Yb2 67.16(3) 13_455 . ?
Ge1 Ge1 Yb2 67.12(3) 9_456 . ?
Yb1 Ge1 Yb2 78.481(14) . . ?
Yb1 Ge1 Yb2 137.90(3) 1_455 . ?
Yb2 Ge1 Yb2 134.24(7) 9_456 . ?
Yb2 Ge1 Yb2 82.12(3) 1_455 . ?
Yb2 Ge1 Yb2 80.48(3) 9_556 . ?
Ge3 Ni Ge3 123.10(9) 13 13_455 ?
Ge3 Ni Ge1 117.23(5) 13 13_455 ?
Ge3 Ni Ge1 117.23(5) 13_455 13_455 ?
Ge3 Ni Ge2 81.07(5) 13 . ?
Ge3 Ni Ge2 81.07(5) 13_455 . ?
Ge1 Ni Ge2 125.15(11) 13_455 . ?
Ge3 Ni Ge3 77.64(6) 13 . ?
Ge3 Ni Ge3 77.64(6) 13_455 . ?
Ge1 Ni Ge3 100.55(8) 13_455 . ?
Ge2 Ni Ge3 134.30(9) . . ?
Ge3 Ni Yb1 63.28(4) 13 13 ?
Ge3 Ni Yb1 136.68(8) 13_455 13 ?
Ge1 Ni Yb1 61.96(4) 13_455 13 ?
Ge2 Ni Yb1 137.81(2) . 13 ?
Ge3 Ni Yb1 61.36(4) . 13 ?
Ge3 Ni Yb1 136.68(8) 13 13_455 ?
Ge3 Ni Yb1 63.28(4) 13_455 13_455 ?
Ge1 Ni Yb1 61.96(4) 13_455 13_455 ?
Ge2 Ni Yb1 137.81(2) . 13_455 ?
Ge3 Ni Yb1 61.36(4) . 13_455 ?
Yb1 Ni Yb1 84.05(4) 13 13_455 ?
Ge3 Ni Yb2 147.00(7) 13 13_455 ?
Ge3 Ni Yb2 71.15(4) 13_455 13_455 ?
Ge1 Ni Yb2 67.97(5) 13_455 13_455 ?
Ge2 Ni Yb2 71.60(5) . 13_455 ?
Ge3 Ni Yb2 135.07(3) . 13_455 ?
Yb1 Ni Yb2 129.79(6) 13 13_455 ?
Yb1 Ni Yb2 75.84(3) 13_455 13_455 ?
Ge3 Ni Yb2 71.15(4) 13 13 ?
Ge3 Ni Yb2 147.00(7) 13_455 13 ?
Ge1 Ni Yb2 67.97(5) 13_455 13 ?
Ge2 Ni Yb2 71.60(5) . 13 ?
Ge3 Ni Yb2 135.07(3) . 13 ?
Yb1 Ni Yb2 75.84(3) 13 13 ?
Yb1 Ni Yb2 129.79(6) 13_455 13 ?
Yb2 Ni Yb2 82.71(5) 13_455 13 ?
Ge3 Ni Yb1 61.62(5) 13 . ?
Ge3 Ni Yb1 61.62(5) 13_455 . ?
Ge1 Ni Yb1 160.04(9) 13_455 . ?
Ge2 Ni Yb1 74.81(6) . . ?
Ge3 Ni Yb1 59.49(5) . . ?
Yb1 Ni Yb1 104.21(5) 13 . ?
Yb1 Ni Yb1 104.21(5) 13_455 . ?
Yb2 Ni Yb1 125.07(4) 13_455 . ?
Yb2 Ni Yb1 125.07(4) 13 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Yb1 Ge1 2.8554(14) 1_655 ?
Yb1 Ge1 2.8555(14) . ?
Yb1 Ge3 2.8924(14) . ?
Yb1 Ge3 2.8924(14) 2 ?
Yb1 Ge3 2.9030(10) 14_445 ?
Yb1 Ge3 2.9030(10) 13 ?
Yb1 Ge3 2.9030(10) 13_455 ?
Yb1 Ge3 2.9030(10) 14_545 ?
Yb1 Ni 3.0573(12) 13 ?
Yb1 Ni 3.0573(12) 14_445 ?
Yb1 Ni 3.0573(12) 14_545 ?
Yb1 Ni 3.0573(12) 13_455 ?
Yb2 Ni 3.0979(15) 6 ?
Yb2 Ni 3.0979(15) 6_455 ?
Yb2 Ni 3.0979(15) 13_455 ?
Yb2 Ni 3.0979(15) 13 ?
Yb2 Ge1 3.1159(9) . ?
Yb2 Ge1 3.1159(9) 9_456 ?
Yb2 Ge1 3.1159(9) 9_556 ?
Yb2 Ge1 3.1159(9) 1_655 ?
Yb2 Ge3 3.2179(13) . ?
Yb2 Ge3 3.2179(13) 10_556 ?
Yb2 Ge2 3.2551(10) 5 ?
Yb2 Ge2 3.2551(10) 5_455 ?
Ge3 Ni 2.3279(10) 13 ?
Ge3 Ni 2.3279(10) 13_455 ?
Ge3 Ni 2.574(2) . ?
Ge3 Ge3 2.647(3) 2_565 ?
Ge3 Yb1 2.9030(10) 13 ?
Ge3 Yb1 2.9030(10) 13_455 ?
Ge2 Ni 2.3762(18) . ?
Ge2 Ni 2.3762(18) 2 ?
Ge2 Ge2 2.500(4) 9 ?
Ge2 Yb2 3.2551(10) 5_444 ?
Ge2 Yb2 3.2551(10) 13 ?
Ge2 Yb2 3.2551(10) 5_544 ?
Ge2 Yb2 3.2551(10) 13_455 ?
Ge1 Ni 2.3713(19) 14_445 ?
Ge1 Ni 2.3713(19) 13_455 ?
Ge1 Ge1 2.423(4) 9_456 ?
Ge1 Yb1 2.8555(14) 1_455 ?
Ge1 Yb2 3.1159(9) 9_456 ?
Ge1 Yb2 3.1159(9) 1_455 ?
Ge1 Yb2 3.1159(9) 9_556 ?
Ni Ge3 2.3279(10) 13 ?
Ni Ge3 2.3279(10) 13_455 ?
Ni Ge1 2.3713(19) 13_455 ?
Ni Yb1 3.0573(12) 13 ?
Ni Yb1 3.0573(12) 13_455 ?
Ni Yb2 3.0979(15) 13_455 ?
Ni Yb2 3.0979(15) 13 ?
