#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:35:19 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179147 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/08/4310809.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4310809
loop_
_publ_author_name
'Sheba D. Bergman'
'Israel Goldberg'
'Andrea Barbieri'
'Francesco Barigelletti'
'Moshe Kol'
_publ_section_title
;
 Mononuclear and Dinuclear Complexes of Dibenzoeilatin: Synthesis,
 Structure, and Electrochemical and Photophysical Properties
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2355
_journal_page_last               2367
_journal_paper_doi               10.1021/ic0354062
_journal_volume                  43
_journal_year                    2004
_chemical_formula_moiety
'(C32 H16 N4), 4(C10 H8 N2), 2(Os Cl2), 14(H2 O)'
_chemical_formula_sum            'C72 H76 Cl4 N12 O14 Os2'
_chemical_formula_weight         1855.65
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                102.0240(7)
_cell_angle_beta                 97.4120(7)
_cell_angle_gamma                95.6780(14)
_cell_formula_units_Z            1
_cell_length_a                   9.6320(2)
_cell_length_b                   12.7620(2)
_cell_length_c                   16.0470(3)
_cell_measurement_reflns_used    7701
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      28.25
_cell_measurement_theta_min      2.32
_cell_volume                     1896.99(6)
_computing_cell_refinement       Denzo
_computing_data_collection       'Collect, Nonius B.V.'
_computing_data_reduction        Denzo
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    DIRDIF-96
_diffrn_ambient_temperature      110(2)
_diffrn_detector_area_resol_mean '56 microns'
_diffrn_measured_fraction_theta_full 0.945
_diffrn_measured_fraction_theta_max 0.945
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       '1 deg. Phi & Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0310
_diffrn_reflns_av_sigmaI/netI    0.0519
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            15826
_diffrn_reflns_theta_full        28.25
_diffrn_reflns_theta_max         28.25
_diffrn_reflns_theta_min         2.32
_exptl_absorpt_coefficient_mu    3.557
_exptl_absorpt_correction_T_max  0.6175
_exptl_absorpt_correction_T_min  0.4150
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'Blessing, 1995'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.624
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallelpiped
_exptl_crystal_F_000             924
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.243
_refine_diff_density_min         -1.712
_refine_diff_density_rms         0.144
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.052
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     524
_refine_ls_number_reflns         8687
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.052
_refine_ls_R_factor_all          0.0434
_refine_ls_R_factor_gt           0.0356
_refine_ls_shift/su_max          0.171
_refine_ls_shift/su_mean         0.008
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0403P)²+3.4567P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0838
_refine_ls_wR_factor_ref         0.0877
_reflns_number_gt                7701
_reflns_number_total             8687
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0354062si20040209_095757_3.cif
_cod_data_source_block           mk106
_cod_database_code               4310809
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Os Os 1.045618(15) 0.747191(12) 0.204579(10) 0.01517(6) Uani 1 1 d . . .
Cl1 Cl 0.23485(13) 0.13899(10) 0.16034(8) 0.0343(3) Uani 1 1 d . . .
Cl2A Cl 0.6884(3) 0.2046(3) 0.42499(19) 0.0351(10) Uani 0.546(9) 1 d P . .
Cl2B Cl 0.4470(7) 0.2944(4) 0.4463(4) 0.0396(15) Uani 0.454(9) 1 d P . .
N1 N 1.1376(3) 0.6963(3) 0.0947(2) 0.0136(6) Uani 1 1 d . . .
N2 N 0.8900(3) 0.6311(3) 0.1280(2) 0.0152(7) Uani 1 1 d . . .
N3 N 1.2207(3) 0.8420(3) 0.2850(2) 0.0181(7) Uani 1 1 d . . .
N4 N 1.1455(4) 0.6318(3) 0.2568(2) 0.0192(7) Uani 1 1 d . . .
N5 N 0.9521(4) 0.8734(3) 0.1709(2) 0.0191(7) Uani 1 1 d . . .
N6 N 0.9508(4) 0.8005(3) 0.3110(2) 0.0217(8) Uani 1 1 d . . .
C1 C 0.7480(4) 0.6067(3) 0.1351(3) 0.0158(8) Uani 1 1 d . . .
C2 C 0.6809(4) 0.6876(3) 0.1814(3) 0.0205(9) Uani 1 1 d . . .
H2 H 0.7337 0.7558 0.2086 0.025 Uiso 1 1 calc R . .
C3 C 0.5398(4) 0.6698(4) 0.1880(3) 0.0230(9) Uani 1 1 d . . .
H3 H 0.4963 0.7250 0.2202 0.028 Uiso 1 1 calc R . .
C4 C 0.4607(4) 0.5705(3) 0.1473(3) 0.0191(8) Uani 1 1 d . . .
H4 H 0.3636 0.5584 0.1523 0.023 Uiso 1 1 calc R . .
C5 C 0.5218(4) 0.4906(3) 0.1004(3) 0.0173(8) Uani 1 1 d . . .
H5 H 0.4654 0.4244 0.0720 0.021 Uiso 1 1 calc R . .
C6 C 0.6678(4) 0.5043(3) 0.0931(3) 0.0166(8) Uani 1 1 d . . .
C7 C 0.7343(4) 0.4253(3) 0.0397(3) 0.0145(8) Uani 1 1 d . . .
C8 C 1.3195(4) 0.6862(3) -0.0017(3) 0.0164(8) Uani 1 1 d . . .
C9 C 1.4296(4) 0.7443(3) -0.0307(3) 0.0186(8) Uani 1 1 d . . .
H9 H 1.4692 0.7094 -0.0786 0.022 Uiso 1 1 calc R . .
C10 C 1.4808(4) 0.8504(3) 0.0088(3) 0.0218(9) Uani 1 1 d . . .
H10 H 1.5584 0.8863 -0.0096 0.026 Uiso 1 1 calc R . .
C11 C 1.4175(5) 0.9049(3) 0.0764(3) 0.0224(9) Uani 1 1 d . . .
H11 H 1.4532 0.9777 0.1041 0.027 Uiso 1 1 calc R . .
C12 C 1.3040(4) 0.8536(3) 0.1028(3) 0.0180(8) Uani 1 1 d . . .
H12 H 1.2590 0.8926 0.1466 0.022 Uiso 1 1 calc R . .
C13 C 1.2539(4) 0.7442(3) 0.0659(3) 0.0146(8) Uani 1 1 d . . .
C14 C 1.0756(4) 0.6004(3) 0.0471(2) 0.0132(7) Uani 1 1 d . . .
C15 C 0.8647(4) 0.4627(3) 0.0198(3) 0.0153(8) Uani 1 1 d . . .
C16 C 0.9388(4) 0.5640(3) 0.0663(3) 0.0135(7) Uani 1 1 d . . .
C17 C 1.2496(4) 0.9496(3) 0.2986(3) 0.0227(9) Uani 1 1 d . . .
H17 H 1.1840 0.9881 0.2719 0.027 Uiso 1 1 calc R . .
C18 C 1.3704(4) 1.0066(4) 0.3496(3) 0.0240(9) Uani 1 1 d . . .
H18 H 1.3888 1.0827 0.3567 0.029 Uiso 1 1 calc R . .
C19 C 1.4648(5) 0.9514(4) 0.3905(3) 0.0267(10) Uani 1 1 d . . .
H19 H 1.5496 0.9892 0.4251 0.032 Uiso 1 1 calc R . .
C20 C 1.4349(4) 0.8414(4) 0.3806(3) 0.0241(9) Uani 1 1 d . . .
H20 H 1.4974 0.8026 0.4093 0.029 Uiso 1 1 calc R . .
C21 C 1.3112(4) 0.7878(3) 0.3277(3) 0.0198(8) Uani 1 1 d . . .
C22 C 1.2691(4) 0.6700(4) 0.3115(3) 0.0225(9) Uani 1 1 d . . .
C23 C 1.3478(5) 0.6015(4) 0.3491(3) 0.0354(12) Uani 1 1 d . . .
H23 H 1.4325 0.6299 0.3879 0.042 Uiso 1 1 calc R . .
C24 C 1.3019(6) 0.4918(4) 0.3295(4) 0.0470(16) Uani 1 1 d . . .
H24 H 1.3552 0.4434 0.3534 0.056 Uiso 1 1 calc R . .
C25 C 1.1772(5) 0.4548(4) 0.2746(4) 0.0379(13) Uani 1 1 d . . .
H25 H 1.1427 0.3799 0.2603 0.045 Uiso 1 1 calc R . .
C26 C 1.1023(5) 0.5260(4) 0.2403(3) 0.0273(10) Uani 1 1 d . . .
H26 H 1.0156 0.4986 0.2031 0.033 Uiso 1 1 calc R . .
C27 C 0.9360(4) 0.8953(3) 0.0920(3) 0.0210(9) Uani 1 1 d . . .
H27 H 0.9755 0.8521 0.0476 0.025 Uiso 1 1 calc R . .
C28 C 0.8645(5) 0.9780(4) 0.0728(3) 0.0262(10) Uani 1 1 d . . .
H28 H 0.8548 0.9911 0.0163 0.031 Uiso 1 1 calc R . .
C29 C 0.8069(5) 1.0420(4) 0.1376(4) 0.0318(11) Uani 1 1 d . . .
H29 H 0.7578 1.0996 0.1259 0.038 Uiso 1 1 calc R . .
C30 C 0.8219(5) 1.0208(4) 0.2194(3) 0.0297(10) Uani 1 1 d . . .
H30 H 0.7840 1.0642 0.2644 0.036 Uiso 1 1 calc R . .
C31 C 0.8928(4) 0.9356(4) 0.2347(3) 0.0241(9) Uani 1 1 d . . .
C32 C 0.8997(4) 0.8972(4) 0.3162(3) 0.0238(9) Uani 1 1 d . . .
C33 C 0.8499(5) 0.9487(5) 0.3890(3) 0.0359(12) Uani 1 1 d . . .
H33 H 0.8166 1.0167 0.3912 0.043 Uiso 1 1 calc R A 1
C34 C 0.8488(5) 0.9008(5) 0.4584(3) 0.0415(14) Uani 1 1 d . . .
H34 H 0.8141 0.9352 0.5085 0.050 Uiso 1 1 calc R A 1
C35 C 0.8982(6) 0.8030(6) 0.4545(4) 0.0473(18) Uani 1 1 d . . .
H35 H 0.8975 0.7690 0.5018 0.057 Uiso 1 1 calc R A 1
C36 C 0.9519(5) 0.7515(6) 0.3772(4) 0.0359(16) Uani 1 1 d . . .
H36 H 0.9871 0.6840 0.3738 0.043 Uiso 1 1 calc R A 1
O37 O 0.1578(4) 0.2031(3) 0.3453(3) 0.0441(9) Uani 1 1 d . . .
O38 O 0.9752(4) 0.2622(3) 0.0991(3) 0.0468(10) Uani 1 1 d . . .
O39 O 0.8035(5) 0.3339(3) 0.2195(3) 0.0568(12) Uani 1 1 d . . .
O40 O 1.2347(5) 0.3365(4) 0.0633(3) 0.0674(14) Uani 1 1 d . . .
O41 O 0.9407(5) 0.3174(5) 0.3812(3) 0.0731(16) Uani 1 1 d . . .
O42 O 0.5639(5) 0.2006(5) 0.2333(3) 0.0762(15) Uani 1 1 d . . .
O43A O 0.4074(15) 0.2975(13) 0.4661(9) 0.042(4) Uani 0.546(9) 1 d P . .
O43B O 0.720(2) 0.1683(13) 0.4393(18) 0.121(8) Uani 0.454(9) 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N5 Os N6 78.58(14) . . ?
N5 Os N2 93.60(13) . . ?
N6 Os N2 101.95(13) . . ?
N5 Os N1 99.58(13) . . ?
N6 Os N1 178.11(12) . . ?
N2 Os N1 77.66(13) . . ?
N5 Os N3 96.13(13) . . ?
N6 Os N3 81.33(13) . . ?
N2 Os N3 170.18(13) . . ?
N1 Os N3 99.36(13) . . ?
N5 Os N4 171.89(13) . . ?
N6 Os N4 94.73(14) . . ?
N2 Os N4 92.28(13) . . ?
N1 Os N4 87.14(13) . . ?
N3 Os N4 78.17(14) . . ?
C14 N1 C13 116.6(3) . . ?
C14 N1 Os 112.8(3) . . ?
C13 N1 Os 130.6(3) . . ?
C16 N2 C1 116.0(3) . . ?
C16 N2 Os 113.0(2) . . ?
C1 N2 Os 130.7(3) . . ?
C17 N3 C21 118.4(4) . . ?
C17 N3 Os 125.7(3) . . ?
C21 N3 Os 115.9(3) . . ?
C26 N4 C22 117.6(4) . . ?
C26 N4 Os 126.7(3) . . ?
C22 N4 Os 115.7(3) . . ?
C27 N5 C31 118.3(4) . . ?
C27 N5 Os 125.9(3) . . ?
C31 N5 Os 115.6(3) . . ?
C36 N6 C32 120.1(4) . . ?
C36 N6 Os 123.2(4) . . ?
C32 N6 Os 116.2(3) . . ?
N2 C1 C2 118.4(4) . . ?
N2 C1 C6 122.1(4) . . ?
C2 C1 C6 119.5(4) . . ?
C3 C2 C1 121.1(4) . . ?
C3 C2 H2 119.5 . . ?
C1 C2 H2 119.5 . . ?
C2 C3 C4 119.9(4) . . ?
C2 C3 H3 120.0 . . ?
C4 C3 H3 120.0 . . ?
C5 C4 C3 120.6(4) . . ?
C5 C4 H4 119.7 . . ?
C3 C4 H4 119.7 . . ?
C4 C5 C6 121.5(4) . . ?
C4 C5 H5 119.2 . . ?
C6 C5 H5 119.2 . . ?
C5 C6 C1 117.3(4) . . ?
C5 C6 C7 123.3(4) . . ?
C1 C6 C7 119.1(3) . . ?
C15 C7 C6 115.7(4) . . ?
C15 C7 C8 116.3(4) . 2_765 ?
C6 C7 C8 128.0(4) . 2_765 ?
C9 C8 C13 117.5(4) . . ?
C9 C8 C7 123.5(4) . 2_765 ?
C13 C8 C7 118.9(4) . 2_765 ?
C10 C9 C8 121.8(4) . . ?
C10 C9 H9 119.1 . . ?
C8 C9 H9 119.1 . . ?
C9 C10 C11 119.7(4) . . ?
C9 C10 H10 120.2 . . ?
C11 C10 H10 120.2 . . ?
C12 C11 C10 120.4(4) . . ?
C12 C11 H11 119.8 . . ?
C10 C11 H11 119.8 . . ?
C11 C12 C13 120.8(4) . . ?
C11 C12 H12 119.6 . . ?
C13 C12 H12 119.6 . . ?
N1 C13 C12 118.4(4) . . ?
N1 C13 C8 121.9(3) . . ?
C12 C13 C8 119.6(4) . . ?
N1 C14 C15 123.8(3) . 2_765 ?
N1 C14 C16 115.5(3) . . ?
C15 C14 C16 120.7(3) 2_765 . ?
C7 C15 C16 120.3(4) . . ?
C7 C15 C14 120.3(4) . 2_765 ?
C16 C15 C14 119.4(3) . 2_765 ?
N2 C16 C15 124.2(3) . . ?
N2 C16 C14 116.0(3) . . ?
C15 C16 C14 119.8(3) . . ?
N3 C17 C18 122.6(4) . . ?
N3 C17 H17 118.7 . . ?
C18 C17 H17 118.7 . . ?
C17 C18 C19 119.1(4) . . ?
C17 C18 H18 120.5 . . ?
C19 C18 H18 120.5 . . ?
C20 C19 C18 119.6(4) . . ?
C20 C19 H19 120.2 . . ?
C18 C19 H19 120.2 . . ?
C19 C20 C21 118.8(4) . . ?
C19 C20 H20 120.6 . . ?
C21 C20 H20 120.6 . . ?
N3 C21 C20 121.4(4) . . ?
N3 C21 C22 114.9(4) . . ?
C20 C21 C22 123.6(4) . . ?
N4 C22 C23 121.6(4) . . ?
N4 C22 C21 115.2(4) . . ?
C23 C22 C21 123.2(4) . . ?
C24 C23 C22 119.6(5) . . ?
C24 C23 H23 120.2 . . ?
C22 C23 H23 120.2 . . ?
C25 C24 C23 118.1(5) . . ?
C25 C24 H24 120.9 . . ?
C23 C24 H24 120.9 . . ?
C24 C25 C26 120.0(5) . . ?
C24 C25 H25 120.0 . . ?
C26 C25 H25 120.0 . . ?
N4 C26 C25 123.1(4) . . ?
N4 C26 H26 118.5 . . ?
C25 C26 H26 118.5 . . ?
N5 C27 C28 122.7(4) . . ?
N5 C27 H27 118.6 . . ?
C28 C27 H27 118.6 . . ?
C27 C28 C29 119.0(4) . . ?
C27 C28 H28 120.5 . . ?
C29 C28 H28 120.5 . . ?
C30 C29 C28 119.4(4) . . ?
C30 C29 H29 120.3 . . ?
C28 C29 H29 120.3 . . ?
C29 C30 C31 119.2(5) . . ?
C29 C30 H30 120.4 . . ?
C31 C30 H30 120.4 . . ?
N5 C31 C30 121.4(4) . . ?
N5 C31 C32 114.7(4) . . ?
C30 C31 C32 123.7(4) . . ?
N6 C32 C33 122.1(5) . . ?
N6 C32 C31 113.5(4) . . ?
C33 C32 C31 124.3(4) . . ?
C34 C33 C32 119.6(5) . . ?
C34 C33 H33 120.2 . . ?
C32 C33 H33 120.2 . . ?
C35 C34 C33 119.5(5) . . ?
C35 C34 H34 120.2 . . ?
C33 C34 H34 120.2 . . ?
C34 C35 C36 119.5(6) . . ?
C34 C35 H35 120.3 . . ?
C36 C35 H35 120.2 . . ?
N6 C36 C35 119.2(6) . . ?
N6 C36 H36 120.4 . . ?
C35 C36 H36 120.4 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Os N5 2.055(3) . ?
Os N6 2.063(4) . ?
Os N2 2.069(3) . ?
Os N1 2.087(3) . ?
Os N3 2.087(3) . ?
Os N4 2.093(3) . ?
N1 C14 1.337(5) . ?
N1 C13 1.400(5) . ?
N2 C16 1.335(5) . ?
N2 C1 1.397(5) . ?
N3 C17 1.340(5) . ?
N3 C21 1.368(5) . ?
N4 C26 1.334(6) . ?
N4 C22 1.365(5) . ?
N5 C27 1.345(5) . ?
N5 C31 1.381(6) . ?
N6 C36 1.339(7) . ?
N6 C32 1.363(6) . ?
C1 C2 1.404(6) . ?
C1 C6 1.434(6) . ?
C2 C3 1.378(6) . ?
C2 H2 0.9500 . ?
C3 C4 1.395(6) . ?
C3 H3 0.9500 . ?
C4 C5 1.366(6) . ?
C4 H4 0.9500 . ?
C5 C6 1.423(5) . ?
C5 H5 0.9500 . ?
C6 C7 1.440(6) . ?
C7 C15 1.399(5) . ?
C7 C8 1.440(5) 2_765 ?
C8 C9 1.416(5) . ?
C8 C13 1.434(6) . ?
C8 C7 1.440(5) 2_765 ?
C9 C10 1.382(6) . ?
C9 H9 0.9500 . ?
C10 C11 1.404(6) . ?
C10 H10 0.9500 . ?
C11 C12 1.377(6) . ?
C11 H11 0.9500 . ?
C12 C13 1.408(6) . ?
C12 H12 0.9500 . ?
C14 C15 1.422(6) 2_765 ?
C14 C16 1.446(5) . ?
C15 C16 1.419(5) . ?
C15 C14 1.422(6) 2_765 ?
C17 C18 1.375(6) . ?
C17 H17 0.9500 . ?
C18 C19 1.385(6) . ?
C18 H18 0.9500 . ?
C19 C20 1.377(6) . ?
C19 H19 0.9500 . ?
C20 C21 1.393(6) . ?
C20 H20 0.9500 . ?
C21 C22 1.478(6) . ?
C22 C23 1.391(6) . ?
C23 C24 1.383(7) . ?
C23 H23 0.9500 . ?
C24 C25 1.372(7) . ?
C24 H24 0.9500 . ?
C25 C26 1.372(7) . ?
C25 H25 0.9500 . ?
C26 H26 0.9500 . ?
C27 C28 1.381(6) . ?
C27 H27 0.9500 . ?
C28 C29 1.394(7) . ?
C28 H28 0.9500 . ?
C29 C30 1.386(7) . ?
C29 H29 0.9500 . ?
C30 C31 1.388(6) . ?
C30 H30 0.9500 . ?
C31 C32 1.485(7) . ?
C32 C33 1.384(7) . ?
C33 C34 1.378(8) . ?
C33 H33 0.9500 . ?
C34 C35 1.371(9) . ?
C34 H34 0.9500 . ?
C35 C36 1.461(8) . ?
C35 H35 0.9500 . ?
C36 H36 0.9500 . ?
