#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:52:49 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179159 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/20/4312048.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4312048
loop_
_publ_author_name
'Ramasamy Pothiraja'
'Malaichamy Sathiyendiran'
'Ray J. Butcher'
'Ramaswamy Murugavel'
_publ_section_title
;
 Cobalt and Manganese Nets via Their Wires: Facile Transformation in
 Metal-Diorganophosphates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              7585
_journal_page_last               7587
_journal_paper_doi               10.1021/ic048781i
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'C36 H56 Co N4 O10 P2'
_chemical_formula_weight         825.72
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 92.77(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.846(3)
_cell_length_b                   11.452(2)
_cell_length_c                   23.008(5)
_cell_measurement_temperature    293(2)
_cell_volume                     4170.3(14)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1561
_diffrn_reflns_av_sigmaI/netI    0.0978
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            61006
_diffrn_reflns_theta_full        24.75
_diffrn_reflns_theta_max         24.75
_diffrn_reflns_theta_min         1.77
_exptl_absorpt_coefficient_mu    0.545
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.315
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1748
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_refine_diff_density_max         5.534
_refine_diff_density_min         -1.482
_refine_diff_density_rms         0.138
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     482
_refine_ls_number_reflns         7112
_refine_ls_number_restraints     384
_refine_ls_restrained_S_all      0.994
_refine_ls_R_factor_all          0.1512
_refine_ls_R_factor_gt           0.0954
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1362P)²+10.9642P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2337
_refine_ls_wR_factor_ref         0.2597
_reflns_number_gt                4186
_reflns_number_total             7112
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic048781isi20041001_043405_2.cif
_cod_data_source_block           Co-grid(Compound2)
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        4170.3(15)
_cod_database_code               4312048
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.0000 0.0000 0.0000 0.0084(3) Uani 1 2 d SU . .
Co2 Co 0.5000 0.42905(12) 0.7500 0.0156(4) Uani 1 2 d SU . .
P1 P 0.22234(13) 0.02506(17) 0.00017(8) 0.0183(5) Uani 1 1 d U . .
P2 P 0.27728(13) 0.42505(16) 0.75443(8) 0.0153(4) Uani 1 1 d U . .
O1 O 0.1305(3) 0.0058(4) 0.00640(19) 0.0151(11) Uani 1 1 d U . .
O2 O 0.2654(4) 0.0560(4) 0.0626(2) 0.0216(12) Uani 1 1 d U . .
O3 O 0.2554(4) -0.1002(5) -0.0125(2) 0.0282(13) Uani 1 1 d U . .
O4 O 0.2470(3) 0.1114(4) -0.0440(2) 0.0231(12) Uani 1 1 d U . .
O5 O 0.3709(3) 0.4322(4) 0.7466(2) 0.0224(12) Uani 1 1 d U . .
O6 O 0.2290(4) 0.4135(5) 0.6928(2) 0.0243(12) Uani 1 1 d U . .
O7 O 0.2544(4) 0.5580(5) 0.7694(2) 0.0273(13) Uani 1 1 d U . .
O8 O 0.2493(4) 0.3398(5) 0.7970(2) 0.0287(13) Uani 1 1 d U . .
N1 N 0.0012(4) -0.0098(5) -0.0953(2) 0.0141(13) Uani 1 1 d U . .
N2 N 0.0043(4) -0.1902(4) 0.0022(2) 0.0091(11) Uani 1 1 d U . .
N3 N 0.5029(4) 0.4385(5) 0.8478(3) 0.0210(14) Uani 1 1 d U . .
N4 N 0.5000 0.6117(8) 0.7500 0.027(2) Uani 1 2 d SU . .
N5 N 0.5000 0.2421(8) 0.7500 0.0183(19) Uani 1 2 d SU . .
C1 C 0.2984(6) 0.1684(7) 0.0850(4) 0.0289(19) Uani 1 1 d U . .
C2 C 0.3805(6) 0.1939(9) 0.0545(6) 0.054(3) Uani 1 1 d U . .
H2C H 0.4198 0.1321 0.0591 0.200 Uiso 1 1 d R . .
H2A H 0.3650 0.2036 0.0148 0.200 Uiso 1 1 d R . .
H2B H 0.4059 0.2629 0.0692 0.200 Uiso 1 1 d R . .
C3 C 0.3152(8) 0.1474(9) 0.1492(4) 0.052(3) Uani 1 1 d U . .
H3B H 0.3541 0.0850 0.1529 0.200 Uiso 1 1 d R . .
H3A H 0.3387 0.2131 0.1686 0.200 Uiso 1 1 d R . .
H3C H 0.2636 0.1266 0.1658 0.200 Uiso 1 1 d R . .
C4 C 0.2335(6) 0.2654(8) 0.0744(4) 0.035(2) Uani 1 1 d U . .
H4B H 0.2248 0.2820 0.0345 0.200 Uiso 1 1 d R . .
H4C H 0.1810 0.2449 0.0899 0.200 Uiso 1 1 d R . .
H4A H 0.2559 0.3316 0.0939 0.200 Uiso 1 1 d R . .
C5 C 0.3427(6) -0.1400(8) -0.0222(4) 0.033(2) Uani 1 1 d U . .
C6 C 0.3307(9) -0.2641(10) -0.0462(6) 0.078(4) Uani 1 1 d U . .
H6B H 0.3013 -0.3058 -0.0182 0.200 Uiso 1 1 d R . .
H6A H 0.2955 -0.2562 -0.0803 0.200 Uiso 1 1 d R . .
H6C H 0.3809 -0.3047 -0.0547 0.200 Uiso 1 1 d R . .
C7 C 0.3860(8) -0.0581(15) -0.0638(6) 0.095(6) Uani 1 1 d U . .
H7A H 0.3985 0.0150 -0.0470 0.200 Uiso 1 1 d R . .
H7C H 0.4371 -0.0950 -0.0733 0.200 Uiso 1 1 d R . .
H7B H 0.3507 -0.0481 -0.0977 0.200 Uiso 1 1 d R . .
C8 C 0.3939(6) -0.1490(9) 0.0348(4) 0.041(2) Uani 1 1 d U . .
H8C H 0.3634 -0.1950 0.0606 0.200 Uiso 1 1 d R . .
H8B H 0.4439 -0.1885 0.0250 0.200 Uiso 1 1 d R . .
H8A H 0.4088 -0.0777 0.0528 0.200 Uiso 1 1 d R . .
C9 C -0.0687(5) -0.0357(7) -0.1275(3) 0.0214(17) Uani 1 1 d U . .
H9 H -0.1170 -0.0524 -0.1087 0.050 Uiso 1 1 d R . .
C10 C -0.0724(5) -0.0406(8) -0.1869(3) 0.0249(18) Uani 1 1 d U . .
H10 H -0.1221 -0.0612 -0.2065 0.050 Uiso 1 1 d R . .
C11 C 0.0003(4) -0.0185(5) -0.2177(3) 0.0102(14) Uani 1 1 d U . .
C12 C 0.0731(5) 0.0060(7) -0.1854(3) 0.0191(16) Uani 1 1 d U . .
H12 H 0.1227 0.0217 -0.2031 0.050 Uiso 1 1 d R . .
C13 C 0.0702(5) 0.0105(7) -0.1247(3) 0.0188(16) Uani 1 1 d U . .
H13 H 0.1193 0.0298 -0.1040 0.050 Uiso 1 1 d R . .
C14 C 0.0616(5) -0.2517(7) -0.0256(3) 0.0234(17) Uani 1 1 d U . .
H14 H 0.1028 -0.2124 -0.0443 0.050 Uiso 1 1 d R . .
C15 C 0.0621(5) -0.3706(7) -0.0283(3) 0.0251(18) Uani 1 1 d U . .
H15 H 0.1025 -0.4082 -0.0484 0.050 Uiso 1 1 d R . .
C16 C 0.0007(4) -0.4337(6) 0.0004(3) 0.0125(15) Uani 1 1 d U . .
C17 C -0.0573(5) -0.3701(7) 0.0303(4) 0.0260(18) Uani 1 1 d U . .
H17 H -0.0985 -0.4071 0.0501 0.050 Uiso 1 1 d R . .
C18 C -0.0537(5) -0.2505(7) 0.0294(4) 0.0259(18) Uani 1 1 d U . .
H18 H -0.0927 -0.2108 0.0500 0.050 Uiso 1 1 d R . .
C19 C 0.1986(6) 0.3031(8) 0.6645(4) 0.031(2) Uani 1 1 d U . .
C20 C 0.1131(7) 0.2736(10) 0.6885(6) 0.061(3) Uani 1 1 d U . .
H20B H 0.0725 0.3337 0.6830 0.200 Uiso 1 1 d R . .
H20C H 0.0915 0.2048 0.6710 0.200 Uiso 1 1 d R . .
H20A H 0.1240 0.2610 0.7285 0.200 Uiso 1 1 d R . .
C21 C 0.1889(8) 0.3355(10) 0.6004(4) 0.061(3) Uani 1 1 d U . .
H21A H 0.1468 0.3939 0.5970 0.200 Uiso 1 1 d R . .
H21C H 0.2407 0.3643 0.5870 0.200 Uiso 1 1 d R . .
H21B H 0.1712 0.2705 0.5780 0.200 Uiso 1 1 d R . .
C22 C 0.2625(7) 0.2053(8) 0.6737(4) 0.042(2) Uani 1 1 d U . .
H22B H 0.3128 0.2300 0.6565 0.200 Uiso 1 1 d R . .
H22C H 0.2741 0.1914 0.7135 0.200 Uiso 1 1 d R . .
H22A H 0.2426 0.1363 0.6555 0.200 Uiso 1 1 d R . .
C23 C 0.1673(6) 0.6048(8) 0.7785(4) 0.033(2) Uani 1 1 d U . .
C24 C 0.1090(8) 0.5145(12) 0.8065(6) 0.075(5) Uani 1 1 d U . .
H24C H 0.0993 0.4479 0.7833 0.200 Uiso 1 1 d R . .
H24B H 0.1364 0.4926 0.8422 0.200 Uiso 1 1 d R . .
H24A H 0.0564 0.5504 0.8135 0.200 Uiso 1 1 d R . .
C25 C 0.1284(6) 0.6353(9) 0.7189(4) 0.041(2) Uani 1 1 d U . .
H25C H 0.1155 0.5668 0.6977 0.200 Uiso 1 1 d R . .
H25A H 0.0777 0.6767 0.7246 0.200 Uiso 1 1 d R . .
H25B H 0.1657 0.6818 0.6979 0.200 Uiso 1 1 d R . .
C26 C 0.1832(10) 0.7127(15) 0.8142(8) 0.117(8) Uani 1 1 d U . .
H26B H 0.2094 0.6957 0.8508 0.200 Uiso 1 1 d R . .
H26C H 0.2205 0.7581 0.7926 0.200 Uiso 1 1 d R . .
H26A H 0.1322 0.7543 0.8190 0.200 Uiso 1 1 d R . .
C27 C 0.5720(5) 0.4740(7) 0.8784(3) 0.0196(16) Uani 1 1 d U . .
H27 H 0.6219 0.4799 0.8597 0.050 Uiso 1 1 d R . .
C28 C 0.5729(5) 0.4965(6) 0.9373(3) 0.0170(16) Uani 1 1 d U . .
H28 H 0.6235 0.5145 0.9565 0.050 Uiso 1 1 d R . .
C29 C 0.5002(5) 0.4871(5) 0.9684(3) 0.0096(14) Uani 1 1 d U . .
C30 C 0.4295(5) 0.4474(7) 0.9365(3) 0.0229(17) Uani 1 1 d U . .
H30 H 0.3792 0.4394 0.9544 0.050 Uiso 1 1 d R . .
C31 C 0.4327(5) 0.4235(7) 0.8774(3) 0.0239(17) Uani 1 1 d U . .
H31 H 0.3836 0.4008 0.8577 0.050 Uiso 1 1 d R . .
C32 C 0.4434(5) 0.6786(7) 0.7790(3) 0.0221(17) Uani 1 1 d U . .
H32 H 0.3998 0.6391 0.7950 0.050 Uiso 1 1 d R . .
C33 C 0.4423(5) 0.7996(7) 0.7801(3) 0.0228(17) Uani 1 1 d U . .
H33 H 0.3986 0.8371 0.7970 0.050 Uiso 1 1 d R . .
C34 C 0.5000 0.8680(10) 0.7500 0.023(2) Uani 1 2 d SU . .
C35 C 0.5000 0.9934(10) 0.7500 0.023(2) Uani 1 2 d SU . .
C36 C 0.5628(6) 1.0600(7) 0.7236(3) 0.0246(18) Uani 1 1 d U . .
H36 H 0.6022 1.0227 0.7024 0.050 Uiso 1 1 d R . .
C37 C 0.5597(5) 0.1793(7) 0.7243(3) 0.0233(18) Uani 1 1 d U . .
H37 H 0.5986 0.2189 0.7037 0.050 Uiso 1 1 d R . .
O9 O 0.7608(4) 0.6485(5) 0.0812(2) 0.0318(14) Uani 1 1 d U . .
H111 H 0.7599 0.7145 0.0705 0.100 Uiso 1 1 d R . .
H112 H 0.7579 0.6525 0.1165 0.100 Uiso 1 1 d R . .
O10 O 0.2612(4) 0.8985(5) 0.3327(2) 0.0285(13) Uani 1 1 d U . .
H211 H 0.2435 0.8834 0.3617 0.100 Uiso 1 1 d R . .
H212 H 0.2545 0.8284 0.3137 0.100 Uiso 1 1 d R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Co1 O1 180.0 3 . ?
O1 Co1 N2 90.0(2) 3 3 ?
O1 Co1 N2 90.0(2) . 3 ?
O1 Co1 N2 90.0(2) 3 . ?
O1 Co1 N2 90.0(2) . . ?
N2 Co1 N2 180.0 3 . ?
O1 Co1 N1 90.9(2) 3 3 ?
O1 Co1 N1 89.1(2) . 3 ?
N2 Co1 N1 88.3(2) 3 3 ?
N2 Co1 N1 91.7(2) . 3 ?
O1 Co1 N1 89.1(2) 3 . ?
O1 Co1 N1 90.9(2) . . ?
N2 Co1 N1 91.7(2) 3 . ?
N2 Co1 N1 88.3(2) . . ?
N1 Co1 N1 180.000(14) 3 . ?
O5 Co2 O5 178.0(3) 2_656 . ?
O5 Co2 N4 88.98(15) 2_656 . ?
O5 Co2 N4 88.98(15) . . ?
O5 Co2 N5 91.02(15) 2_656 . ?
O5 Co2 N5 91.02(15) . . ?
N4 Co2 N5 180.000(4) . . ?
O5 Co2 N3 90.5(2) 2_656 2_656 ?
O5 Co2 N3 89.4(2) . 2_656 ?
N4 Co2 N3 87.26(17) . 2_656 ?
N5 Co2 N3 92.74(16) . 2_656 ?
O5 Co2 N3 89.4(2) 2_656 . ?
O5 Co2 N3 90.5(2) . . ?
N4 Co2 N3 87.26(16) . . ?
N5 Co2 N3 92.74(17) . . ?
N3 Co2 N3 174.5(3) 2_656 . ?
O4 P1 O1 117.2(3) . . ?
O4 P1 O3 112.5(3) . . ?
O1 P1 O3 102.8(3) . . ?
O4 P1 O2 110.6(3) . . ?
O1 P1 O2 108.9(3) . . ?
O3 P1 O2 103.8(3) . . ?
O8 P2 O5 116.6(3) . . ?
O8 P2 O6 113.2(3) . . ?
O5 P2 O6 109.4(3) . . ?
O8 P2 O7 114.1(3) . . ?
O5 P2 O7 102.0(3) . . ?
O6 P2 O7 99.7(3) . . ?
P1 O1 Co1 168.3(3) . . ?
C1 O2 P1 129.6(5) . . ?
C5 O3 P1 129.5(5) . . ?
P2 O5 Co2 170.0(3) . . ?
C19 O6 P2 126.4(5) . . ?
C23 O7 P2 125.9(5) . . ?
C13 N1 C9 115.7(6) . . ?
C13 N1 Co1 123.0(5) . . ?
C9 N1 Co1 121.3(5) . . ?
C18 N2 C14 116.9(6) . . ?
C18 N2 Co1 120.5(5) . . ?
C14 N2 Co1 122.5(5) . . ?
C27 N3 C31 116.6(6) . . ?
C27 N3 Co2 121.2(5) . . ?
C31 N3 Co2 121.6(5) . . ?
C32 N4 C32 112.3(9) 2_656 . ?
C32 N4 Co2 123.8(4) 2_656 . ?
C32 N4 Co2 123.8(4) . . ?
C37 N5 C37 115.4(9) . 2_656 ?
C37 N5 Co2 122.3(5) . . ?
C37 N5 Co2 122.3(5) 2_656 . ?
O2 C1 C3 104.3(7) . . ?
O2 C1 C4 110.8(7) . . ?
C3 C1 C4 111.0(8) . . ?
O2 C1 C2 107.5(7) . . ?
C3 C1 C2 111.5(9) . . ?
C4 C1 C2 111.6(8) . . ?
O3 C5 C8 110.9(6) . . ?
O3 C5 C7 110.8(7) . . ?
C8 C5 C7 110.3(10) . . ?
O3 C5 C6 103.8(8) . . ?
C8 C5 C6 107.6(9) . . ?
C7 C5 C6 113.3(10) . . ?
N1 C9 C10 124.0(7) . . ?
C9 C10 C11 120.1(7) . . ?
C12 C11 C10 116.9(6) . . ?
C12 C11 C11 120.4(8) . 2_554 ?
C10 C11 C11 122.6(8) . 2_554 ?
C11 C12 C13 118.7(7) . . ?
N1 C13 C12 124.6(7) . . ?
N2 C14 C15 123.7(6) . . ?
C14 C15 C16 119.2(6) . . ?
C17 C16 C15 117.1(6) . . ?
C17 C16 C16 121.6(7) . 3_545 ?
C15 C16 C16 121.3(7) . 3_545 ?
C18 C17 C16 119.4(6) . . ?
N2 C18 C17 123.7(7) . . ?
O6 C19 C22 111.5(7) . . ?
O6 C19 C21 103.4(7) . . ?
C22 C19 C21 110.5(8) . . ?
O6 C19 C20 107.7(7) . . ?
C22 C19 C20 112.6(9) . . ?
C21 C19 C20 110.8(9) . . ?
C26 C23 O7 103.9(9) . . ?
C26 C23 C25 110.8(10) . . ?
O7 C23 C25 107.0(7) . . ?
C26 C23 C24 114.3(12) . . ?
O7 C23 C24 112.9(7) . . ?
C25 C23 C24 107.7(9) . . ?
N3 C27 C28 123.0(7) . . ?
C27 C28 C29 121.4(7) . . ?
C30 C29 C28 115.0(6) . . ?
C30 C29 C29 122.8(8) . 3_667 ?
C28 C29 C29 122.1(8) . 3_667 ?
C29 C30 C31 121.1(7) . . ?
N3 C31 C30 122.8(8) . . ?
N4 C32 C33 125.0(7) . . ?
C32 C33 C34 122.5(7) . . ?
C33 C34 C33 112.5(10) 2_656 . ?
C33 C34 C35 123.8(5) 2_656 . ?
C33 C34 C35 123.8(5) . . ?
C36 C35 C36 114.7(10) 2_656 . ?
C36 C35 C34 122.6(5) 2_656 . ?
C36 C35 C34 122.6(5) . . ?
C37 C36 C35 120.5(8) 1_565 . ?
N5 C37 C36 124.4(7) . 1_545 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 O1 2.067(5) 3 ?
Co1 O1 2.067(5) . ?
Co1 N2 2.180(5) 3 ?
Co1 N2 2.180(5) . ?
Co1 N1 2.196(5) 3 ?
Co1 N1 2.196(5) . ?
Co2 O5 2.044(6) 2_656 ?
Co2 O5 2.044(6) . ?
Co2 N4 2.092(9) . ?
Co2 N5 2.141(9) . ?
Co2 N3 2.250(6) 2_656 ?
Co2 N3 2.250(6) . ?
P1 O4 1.484(5) . ?
P1 O1 1.486(5) . ?
P1 O3 1.559(6) . ?
P1 O2 1.599(5) . ?
P2 O8 1.466(6) . ?
P2 O5 1.505(6) . ?
P2 O6 1.585(5) . ?
P2 O7 1.607(5) . ?
O2 C1 1.474(9) . ?
O3 C5 1.483(10) . ?
O6 C19 1.491(10) . ?
O7 C23 1.504(10) . ?
N1 C13 1.335(9) . ?
N1 C9 1.336(10) . ?
N2 C18 1.331(9) . ?
N2 C14 1.336(9) . ?
N3 C27 1.336(10) . ?
N3 C31 1.345(10) . ?
N4 C32 1.377(9) 2_656 ?
N4 C32 1.377(9) . ?
N5 C37 1.347(9) . ?
N5 C37 1.347(9) 2_656 ?
C1 C3 1.506(12) . ?
C1 C4 1.526(13) . ?
C1 C2 1.536(13) . ?
C5 C8 1.510(13) . ?
C5 C7 1.527(15) . ?
C5 C6 1.533(14) . ?
C9 C10 1.365(11) . ?
C10 C11 1.404(10) . ?
C11 C12 1.370(11) . ?
C11 C11 1.486(12) 2_554 ?
C12 C13 1.400(9) . ?
C14 C15 1.362(11) . ?
C15 C16 1.403(10) . ?
C16 C17 1.381(10) . ?
C16 C16 1.519(13) 3_545 ?
C17 C18 1.371(11) . ?
C19 C22 1.518(13) . ?
C19 C21 1.520(13) . ?
C19 C20 1.526(14) . ?
C23 C26 1.498(15) . ?
C23 C25 1.517(12) . ?
C23 C24 1.547(15) . ?
C27 C28 1.380(10) . ?
C28 C29 1.389(10) . ?
C29 C30 1.386(11) . ?
C29 C29 1.485(12) 3_667 ?
C30 C31 1.388(11) . ?
C32 C33 1.385(11) . ?
C33 C34 1.411(10) . ?
C34 C33 1.411(10) 2_656 ?
C34 C35 1.436(16) . ?
C35 C36 1.413(10) 2_656 ?
C35 C36 1.413(10) . ?
C36 C37 1.367(11) 1_565 ?
C37 C36 1.367(11) 1_545 ?
