#------------------------------------------------------------------------------
#$Date: 2016-03-23 02:35:23 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179191 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/33/4313372.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4313372
loop_
_publ_author_name
'Richard D. Adams'
'Burjor Captain'
'Wei Fu'
'Perry J. Pellechia'
'Mark D. Smith'
_publ_section_title
;
 Remarkable Dynamical Opening and Closing of Platinum and Palladium
 Pentaruthenium Carbido Carbonyl Cluster Complexes
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2094
_journal_page_last               2101
_journal_paper_doi               10.1021/ic020656o
_journal_volume                  42
_journal_year                    2003
_chemical_formula_sum            'C28 H27 O15 P Pt Ru5'
_chemical_formula_weight         1334.91
_chemical_name_systematic
;
  ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 92.113(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   14.1957(12)
_cell_length_b                   18.0213(15)
_cell_length_c                   29.027(2)
_cell_measurement_reflns_used    9240
_cell_measurement_temperature    190(2)
_cell_measurement_theta_max      28.29
_cell_measurement_theta_min      2.27
_cell_volume                     7420.8(10)
_computing_cell_refinement       'SAINT+ NT V6.02a (Bruker, 1998)'
_computing_data_collection       'SMART NT V5.619 (Bruker, 2000)'
_computing_data_reduction        'SAINT+ NT V6.02a'
_computing_molecular_graphics    'SHELXTL V5.1 (Sheldrick, 1997)'
_computing_publication_material  'SHELXTL V5.1'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      190(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker SMART APEX CCD diffractometer'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0595
_diffrn_reflns_av_sigmaI/netI    0.0504
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            78232
_diffrn_reflns_theta_full        28.31
_diffrn_reflns_theta_max         28.31
_diffrn_reflns_theta_min         1.33
_diffrn_standards_decay_%        <1
_exptl_absorpt_coefficient_mu    5.847
_exptl_absorpt_correction_T_max  0.583
_exptl_absorpt_correction_T_min  0.389
_exptl_absorpt_correction_type   SADABS
_exptl_absorpt_process_details   '(SADABS, Bruker, 1997)'
_exptl_crystal_colour            dark_red
_exptl_crystal_density_diffrn    2.390
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       fragment
_exptl_crystal_F_000             5024
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.745
_refine_diff_density_min         -1.411
_refine_diff_density_rms         0.182
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     919
_refine_ls_number_reflns         18439
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.0515
_refine_ls_R_factor_gt           0.0379
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
; calc
  [0.00000+1.00000exp(0.50(sinθ/λ)²)]/
    [σ²(Fo²)+0.0000+0.0000*P+(0.0371P)²+0.0000sinθ/λ]
  where P = 0.33333Fo² + 0.66667Fc²
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0764
_refine_ls_wR_factor_ref         0.0809
_reflns_number_gt                14877
_reflns_number_total             18439
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic020656o_3.cif
_cod_data_source_block           bcr5p1s
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        7420.9(11)
_cod_database_code               4313372
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.049798(15) 0.765520(12) 0.479155(8) 0.02271(5) Uani 1 1 d . . .
Pt11 Pt 0.181025(15) 0.008007(11) 0.260042(7) 0.02086(5) Uani 1 1 d . . .
Ru1 Ru 0.24914(3) 0.72383(2) 0.535885(15) 0.01920(9) Uani 1 1 d . . .
Ru2 Ru 0.21360(3) 0.71656(2) 0.437563(15) 0.02022(9) Uani 1 1 d . . .
Ru3 Ru 0.20816(3) 0.85709(2) 0.485562(16) 0.02088(9) Uani 1 1 d . . .
Ru4 Ru 0.39233(3) 0.82955(2) 0.523282(16) 0.02194(9) Uani 1 1 d . . .
Ru5 Ru 0.39563(3) 0.68852(2) 0.477241(16) 0.02099(9) Uani 1 1 d . . .
Ru11 Ru 0.35125(3) 0.01448(2) 0.192995(15) 0.02087(9) Uani 1 1 d . . .
Ru12 Ru 0.35631(3) 0.07292(2) 0.285219(15) 0.02020(9) Uani 1 1 d . . .
Ru13 Ru 0.34225(3) -0.08349(2) 0.270537(15) 0.02017(9) Uani 1 1 d . . .
Ru14 Ru 0.50701(3) -0.07884(2) 0.217154(16) 0.02170(9) Uani 1 1 d . . .
Ru15 Ru 0.51815(3) 0.07806(2) 0.230181(16) 0.02164(9) Uani 1 1 d . . .
P1 P -0.10802(10) 0.74272(8) 0.49356(5) 0.0235(3) Uani 1 1 d . . .
P11 P 0.01696(10) 0.01960(8) 0.25108(5) 0.0226(3) Uani 1 1 d . . .
O11 O 0.1559(4) 0.7985(3) 0.61666(17) 0.0560(14) Uani 1 1 d . . .
O12 O 0.1498(3) 0.5744(2) 0.53948(17) 0.0470(12) Uani 1 1 d . . .
O13 O 0.3954(3) 0.6544(3) 0.60165(16) 0.0454(12) Uani 1 1 d . . .
O21 O 0.0320(3) 0.7397(3) 0.37991(16) 0.0530(14) Uani 1 1 d . . .
O22 O 0.1675(3) 0.5532(2) 0.42026(16) 0.0445(12) Uani 1 1 d . . .
O23 O 0.2839(3) 0.7409(2) 0.34212(14) 0.0361(10) Uani 1 1 d . . .
O31 O 0.0199(3) 0.9193(3) 0.4495(2) 0.0556(15) Uani 1 1 d . . .
O32 O 0.1493(3) 0.9572(3) 0.56387(17) 0.0486(13) Uani 1 1 d . . .
O33 O 0.2678(4) 0.9791(3) 0.4211(2) 0.0624(16) Uani 1 1 d . . .
O41 O 0.3522(3) 0.9558(3) 0.58972(17) 0.0475(12) Uani 1 1 d . . .
O42 O 0.5524(3) 0.7813(3) 0.58945(18) 0.0484(13) Uani 1 1 d . . .
O43 O 0.5132(4) 0.9267(3) 0.46332(19) 0.0615(15) Uani 1 1 d . . .
O51 O 0.3628(3) 0.5235(2) 0.4596(2) 0.0518(14) Uani 1 1 d . . .
O52 O 0.5651(3) 0.6400(3) 0.53660(17) 0.0475(12) Uani 1 1 d . . .
O53 O 0.5111(3) 0.7090(3) 0.39210(16) 0.0432(12) Uani 1 1 d . . .
O111 O 0.2203(3) -0.1001(3) 0.14734(16) 0.0408(11) Uani 1 1 d . . .
O112 O 0.2637(3) 0.1671(2) 0.17306(16) 0.0433(12) Uani 1 1 d . . .
O113 O 0.4538(3) 0.0254(3) 0.10324(16) 0.0492(13) Uani 1 1 d . . .
O121 O 0.1860(3) 0.0989(3) 0.34317(17) 0.0509(13) Uani 1 1 d . . .
O122 O 0.3304(3) 0.2412(2) 0.28524(19) 0.0513(14) Uani 1 1 d . . .
O123 O 0.4423(3) 0.0616(3) 0.38136(16) 0.0474(12) Uani 1 1 d . . .
O131 O 0.1727(3) -0.1101(3) 0.32895(18) 0.0516(14) Uani 1 1 d . . .
O132 O 0.2742(4) -0.2344(2) 0.23544(17) 0.0489(13) Uani 1 1 d . . .
O133 O 0.4332(4) -0.1358(3) 0.36076(16) 0.0478(13) Uani 1 1 d . . .
O141 O 0.4550(3) -0.2357(2) 0.18704(15) 0.0375(11) Uani 1 1 d . . .
O142 O 0.6415(4) -0.0837(3) 0.13767(18) 0.0548(14) Uani 1 1 d . . .
O143 O 0.6562(4) -0.1237(3) 0.2895(2) 0.0560(14) Uani 1 1 d . . .
O151 O 0.4775(3) 0.2406(2) 0.20828(15) 0.0366(10) Uani 1 1 d . . .
O152 O 0.6543(3) 0.1088(3) 0.31135(17) 0.0461(12) Uani 1 1 d . . .
O153 O 0.6668(3) 0.0789(2) 0.15722(17) 0.0480(13) Uani 1 1 d . . .
C1 C 0.3053(4) 0.7757(3) 0.47740(17) 0.0188(10) Uani 1 1 d . . .
C11 C 0.1870(5) 0.7732(3) 0.5851(2) 0.0349(14) Uani 1 1 d . . .
C12 C 0.1810(4) 0.6327(3) 0.5356(2) 0.0277(12) Uani 1 1 d . . .
C13 C 0.3441(4) 0.6825(3) 0.5758(2) 0.0332(14) Uani 1 1 d . . .
C21 C 0.0805(4) 0.7364(4) 0.4128(2) 0.0331(14) Uani 1 1 d . . .
C22 C 0.1855(4) 0.6141(4) 0.4267(2) 0.0327(14) Uani 1 1 d . . .
C23 C 0.2565(4) 0.7319(3) 0.37785(19) 0.0246(12) Uani 1 1 d . . .
C31 C 0.0720(4) 0.8740(3) 0.4639(2) 0.0316(14) Uani 1 1 d . . .
C32 C 0.1744(4) 0.9213(3) 0.5347(2) 0.0308(13) Uani 1 1 d . . .
C33 C 0.2453(4) 0.9330(3) 0.4454(2) 0.0338(14) Uani 1 1 d . . .
C41 C 0.3656(4) 0.9077(3) 0.5647(2) 0.0303(13) Uani 1 1 d . . .
C42 C 0.4942(4) 0.7988(3) 0.5639(2) 0.0316(14) Uani 1 1 d . . .
C43 C 0.4682(4) 0.8902(3) 0.4855(2) 0.0355(14) Uani 1 1 d . . .
C51 C 0.3731(4) 0.5851(3) 0.4660(2) 0.0337(14) Uani 1 1 d . . .
C52 C 0.5026(4) 0.6608(3) 0.5150(2) 0.0304(13) Uani 1 1 d . . .
C53 C 0.4685(4) 0.7029(3) 0.4239(2) 0.0297(13) Uani 1 1 d . . .
C61 C -0.1200(4) 0.7574(4) 0.5578(2) 0.0371(15) Uani 1 1 d . . .
C62 C -0.0695(5) 0.8296(4) 0.5719(2) 0.0460(18) Uani 1 1 d . . .
H62A H -0.1030 0.8719 0.5578 0.069 Uiso 1 1 calc R . .
H62B H -0.0047 0.8284 0.5613 0.069 Uiso 1 1 calc R . .
H62C H -0.0685 0.8346 0.6055 0.069 Uiso 1 1 calc R . .
C63 C -0.0663(5) 0.6954(5) 0.5843(2) 0.051(2) Uani 1 1 d . . .
H63A H -0.0667 0.7055 0.6174 0.077 Uiso 1 1 calc R . .
H63B H -0.0011 0.6936 0.5744 0.077 Uiso 1 1 calc R . .
H63C H -0.0970 0.6476 0.5778 0.077 Uiso 1 1 calc R . .
C64 C -0.2205(5) 0.7588(4) 0.5752(3) 0.053(2) Uani 1 1 d . . .
H64A H -0.2181 0.7629 0.6089 0.079 Uiso 1 1 calc R . .
H64B H -0.2532 0.7130 0.5660 0.079 Uiso 1 1 calc R . .
H64C H -0.2544 0.8016 0.5619 0.079 Uiso 1 1 calc R . .
C65 C -0.0179(4) -0.0340(3) 0.1960(2) 0.0329(14) Uani 1 1 d . . .
C66 C -0.1246(5) -0.0452(4) 0.1868(2) 0.0459(18) Uani 1 1 d . . .
H66A H -0.1356 -0.0669 0.1561 0.069 Uiso 1 1 calc R . .
H66B H -0.1568 0.0028 0.1883 0.069 Uiso 1 1 calc R . .
H66C H -0.1492 -0.0786 0.2101 0.069 Uiso 1 1 calc R . .
C67 C 0.0278(5) -0.1112(3) 0.1989(2) 0.0373(15) Uani 1 1 d . . .
H67A H 0.0289 -0.1330 0.1679 0.056 Uiso 1 1 calc R . .
H67B H -0.0087 -0.1433 0.2189 0.056 Uiso 1 1 calc R . .
H67C H 0.0924 -0.1068 0.2116 0.056 Uiso 1 1 calc R . .
C68 C 0.0226(5) 0.0065(4) 0.1549(2) 0.0391(16) Uani 1 1 d . . .
H68A H 0.0900 0.0156 0.1609 0.059 Uiso 1 1 calc R . .
H68B H -0.0101 0.0539 0.1502 0.059 Uiso 1 1 calc R . .
H68C H 0.0138 -0.0241 0.1271 0.059 Uiso 1 1 calc R . .
C71 C -0.1358(4) 0.6413(3) 0.4788(2) 0.0303(13) Uani 1 1 d . . .
C72 C -0.0499(4) 0.5934(3) 0.4912(3) 0.0422(17) Uani 1 1 d . . .
H72A H -0.0383 0.5939 0.5247 0.063 Uiso 1 1 calc R . .
H72B H 0.0053 0.6132 0.4760 0.063 Uiso 1 1 calc R . .
H72C H -0.0617 0.5424 0.4808 0.063 Uiso 1 1 calc R . .
C73 C -0.2205(5) 0.6082(3) 0.5023(3) 0.0432(17) Uani 1 1 d . . .
H73A H -0.2294 0.5567 0.4923 0.065 Uiso 1 1 calc R . .
H73B H -0.2770 0.6371 0.4940 0.065 Uiso 1 1 calc R . .
H73C H -0.2093 0.6095 0.5358 0.065 Uiso 1 1 calc R . .
C74 C -0.1526(5) 0.6336(4) 0.4264(2) 0.0462(18) Uani 1 1 d . . .
H74A H -0.0990 0.6546 0.4106 0.069 Uiso 1 1 calc R . .
H74B H -0.2103 0.6603 0.4168 0.069 Uiso 1 1 calc R . .
H74C H -0.1594 0.5810 0.4183 0.069 Uiso 1 1 calc R . .
C75 C -0.0146(4) 0.1224(3) 0.2424(2) 0.0303(13) Uani 1 1 d . . .
C76 C -0.1091(4) 0.1373(4) 0.2167(2) 0.0402(16) Uani 1 1 d . . .
H76A H -0.1600 0.1136 0.2333 0.060 Uiso 1 1 calc R . .
H76B H -0.1074 0.1167 0.1855 0.060 Uiso 1 1 calc R . .
H76C H -0.1202 0.1909 0.2149 0.060 Uiso 1 1 calc R . .
C77 C -0.0167(5) 0.1629(4) 0.2887(2) 0.0420(16) Uani 1 1 d . . .
H77A H -0.0226 0.2164 0.2833 0.063 Uiso 1 1 calc R . .
H77B H 0.0417 0.1527 0.3066 0.063 Uiso 1 1 calc R . .
H77C H -0.0707 0.1454 0.3058 0.063 Uiso 1 1 calc R . .
C78 C 0.0637(4) 0.1593(3) 0.2156(2) 0.0349(14) Uani 1 1 d . . .
H78A H 0.0474 0.2113 0.2096 0.052 Uiso 1 1 calc R . .
H78B H 0.0707 0.1333 0.1863 0.052 Uiso 1 1 calc R . .
H78C H 0.1232 0.1568 0.2338 0.052 Uiso 1 1 calc R . .
C81 C -0.1986(4) 0.8046(4) 0.4608(3) 0.0409(16) Uani 1 1 d . . .
C82 C -0.3001(4) 0.7745(4) 0.4611(3) 0.0494(19) Uani 1 1 d . . .
H82A H -0.3430 0.8101 0.4458 0.074 Uiso 1 1 calc R . .
H82B H -0.3185 0.7673 0.4930 0.074 Uiso 1 1 calc R . .
H82C H -0.3034 0.7270 0.4447 0.074 Uiso 1 1 calc R . .
C83 C -0.1695(5) 0.8141(4) 0.4115(3) 0.054(2) Uani 1 1 d . . .
H83A H -0.2147 0.8465 0.3949 0.081 Uiso 1 1 calc R . .
H83B H -0.1685 0.7655 0.3963 0.081 Uiso 1 1 calc R . .
H83C H -0.1066 0.8363 0.4112 0.081 Uiso 1 1 calc R . .
C84 C -0.1997(5) 0.8821(4) 0.4831(3) 0.063(3) Uani 1 1 d . . .
H84A H -0.1348 0.8995 0.4884 0.094 Uiso 1 1 calc R . .
H84B H -0.2310 0.8793 0.5126 0.094 Uiso 1 1 calc R . .
H84C H -0.2339 0.9167 0.4625 0.094 Uiso 1 1 calc R . .
C85 C -0.0537(4) -0.0182(3) 0.3006(2) 0.0299(13) Uani 1 1 d . . .
C86 C -0.1567(4) 0.0078(4) 0.3002(3) 0.0437(17) Uani 1 1 d . . .
H86A H -0.1870 -0.0027 0.2701 0.066 Uiso 1 1 calc R . .
H86B H -0.1587 0.0613 0.3062 0.066 Uiso 1 1 calc R . .
H86C H -0.1901 -0.0186 0.3242 0.066 Uiso 1 1 calc R . .
C87 C -0.0061(4) 0.0048(4) 0.3473(2) 0.0346(14) Uani 1 1 d . . .
H87A H -0.0095 0.0588 0.3508 0.052 Uiso 1 1 calc R . .
H87B H 0.0601 -0.0108 0.3483 0.052 Uiso 1 1 calc R . .
H87C H -0.0388 -0.0190 0.3725 0.052 Uiso 1 1 calc R . .
C88 C -0.0544(5) -0.1039(4) 0.3000(2) 0.0429(17) Uani 1 1 d . . .
H88A H -0.0799 -0.1224 0.3287 0.064 Uiso 1 1 calc R . .
H88B H 0.0101 -0.1223 0.2971 0.064 Uiso 1 1 calc R . .
H88C H -0.0938 -0.1214 0.2738 0.064 Uiso 1 1 calc R . .
C101 C 0.4350(4) -0.0040(3) 0.25330(18) 0.0203(11) Uani 1 1 d . . .
C111 C 0.2644(4) -0.0580(3) 0.1674(2) 0.0283(13) Uani 1 1 d . . .
C112 C 0.2914(4) 0.1092(3) 0.1828(2) 0.0307(13) Uani 1 1 d . . .
C113 C 0.4199(5) 0.0196(4) 0.1378(2) 0.0338(14) Uani 1 1 d . . .
C121 C 0.2272(4) 0.0754(3) 0.3128(2) 0.0263(12) Uani 1 1 d . . .
C122 C 0.3423(4) 0.1783(3) 0.2844(2) 0.0333(14) Uani 1 1 d . . .
C123 C 0.4113(4) 0.0684(3) 0.3455(2) 0.0316(14) Uani 1 1 d . . .
C131 C 0.2158(4) -0.0829(3) 0.3007(2) 0.0313(13) Uani 1 1 d . . .
C132 C 0.3018(4) -0.1788(3) 0.2479(2) 0.0313(14) Uani 1 1 d . . .
C133 C 0.3982(4) -0.1182(3) 0.3267(2) 0.0285(13) Uani 1 1 d . . .
C141 C 0.4715(4) -0.1774(3) 0.1993(2) 0.0280(13) Uani 1 1 d . . .
C142 C 0.5923(4) -0.0791(3) 0.1675(2) 0.0337(14) Uani 1 1 d . . .
C143 C 0.6017(4) -0.1083(3) 0.2625(2) 0.0331(14) Uani 1 1 d . . .
C151 C 0.4913(4) 0.1804(3) 0.2173(2) 0.0276(12) Uani 1 1 d . . .
C152 C 0.6062(4) 0.0971(3) 0.2805(2) 0.0282(13) Uani 1 1 d . . .
C153 C 0.6116(4) 0.0762(3) 0.1844(2) 0.0324(14) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C31 Pt1 C21 90.1(3) . . ?
C31 Pt1 P1 111.50(17) . . ?
C21 Pt1 P1 111.17(17) . . ?
C31 Pt1 Ru3 46.72(16) . . ?
C21 Pt1 Ru3 90.87(17) . . ?
P1 Pt1 Ru3 150.46(4) . . ?
C31 Pt1 Ru2 94.08(17) . . ?
C21 Pt1 Ru2 46.27(17) . . ?
P1 Pt1 Ru2 147.18(4) . . ?
Ru3 Pt1 Ru2 62.314(14) . . ?
C121 Pt11 C131 88.9(2) . . ?
C121 Pt11 P11 108.67(16) . . ?
C131 Pt11 P11 110.45(17) . . ?
C121 Pt11 Ru12 45.90(15) . . ?
C131 Pt11 Ru12 89.49(17) . . ?
P11 Pt11 Ru12 148.79(4) . . ?
C121 Pt11 Ru13 91.71(16) . . ?
C131 Pt11 Ru13 45.68(16) . . ?
P11 Pt11 Ru13 149.43(4) . . ?
Ru12 Pt11 Ru13 60.749(14) . . ?
C121 Pt11 Ru11 102.02(16) . . ?
C131 Pt11 Ru11 102.04(16) . . ?
P11 Pt11 Ru11 135.05(4) . . ?
Ru12 Pt11 Ru11 57.121(13) . . ?
Ru13 Pt11 Ru11 56.888(13) . . ?
C13 Ru1 C12 90.8(2) . . ?
C13 Ru1 C11 93.6(3) . . ?
C12 Ru1 C11 98.9(3) . . ?
C13 Ru1 C1 112.5(2) . . ?
C12 Ru1 C1 125.6(2) . . ?
C11 Ru1 C1 126.0(2) . . ?
C13 Ru1 Ru5 75.87(19) . . ?
C12 Ru1 Ru5 100.91(18) . . ?
C11 Ru1 Ru5 157.6(2) . . ?
C1 Ru1 Ru5 46.04(14) . . ?
C13 Ru1 Ru4 81.06(17) . . ?
C12 Ru1 Ru4 161.78(18) . . ?
C11 Ru1 Ru4 97.87(19) . . ?
C1 Ru1 Ru4 45.86(14) . . ?
Ru5 Ru1 Ru4 61.380(16) . . ?
C13 Ru1 Ru3 140.17(18) . . ?
C12 Ru1 Ru3 128.89(17) . . ?
C11 Ru1 Ru3 84.34(19) . . ?
C1 Ru1 Ru3 45.22(14) . . ?
Ru5 Ru1 Ru3 91.253(18) . . ?
Ru4 Ru1 Ru3 60.021(16) . . ?
C13 Ru1 Ru2 132.9(2) . . ?
C12 Ru1 Ru2 83.47(18) . . ?
C11 Ru1 Ru2 133.5(2) . . ?
C1 Ru1 Ru2 44.31(14) . . ?
Ru5 Ru1 Ru2 59.745(16) . . ?
Ru4 Ru1 Ru2 90.169(17) . . ?
Ru3 Ru1 Ru2 60.497(15) . . ?
C23 Ru2 C22 93.6(2) . . ?
C23 Ru2 C1 103.1(2) . . ?
C22 Ru2 C1 137.1(2) . . ?
C23 Ru2 C21 88.6(2) . . ?
C22 Ru2 C21 85.7(3) . . ?
C1 Ru2 C21 133.2(2) . . ?
C23 Ru2 Pt1 130.83(17) . . ?
C22 Ru2 Pt1 101.74(19) . . ?
C1 Ru2 Pt1 96.60(14) . . ?
C21 Ru2 Pt1 47.20(17) . . ?
C23 Ru2 Ru5 94.54(17) . . ?
C22 Ru2 Ru5 94.40(19) . . ?
C1 Ru2 Ru5 45.67(15) . . ?
C21 Ru2 Ru5 176.80(18) . . ?
Pt1 Ru2 Ru5 129.754(19) . . ?
C23 Ru2 Ru1 148.83(17) . . ?
C22 Ru2 Ru1 103.60(18) . . ?
C1 Ru2 Ru1 47.30(14) . . ?
C21 Ru2 Ru1 118.03(17) . . ?
Pt1 Ru2 Ru1 71.146(14) . . ?
Ru5 Ru2 Ru1 58.825(15) . . ?
C23 Ru2 Ru3 109.31(16) . . ?
C22 Ru2 Ru3 156.26(18) . . ?
C1 Ru2 Ru3 44.62(15) . . ?
C21 Ru2 Ru3 88.61(17) . . ?
Pt1 Ru2 Ru3 58.634(13) . . ?
Ru5 Ru2 Ru3 90.027(17) . . ?
Ru1 Ru2 Ru3 59.351(15) . . ?
C33 Ru3 C32 96.1(3) . . ?
C33 Ru3 C1 104.2(2) . . ?
C32 Ru3 C1 135.5(2) . . ?
C33 Ru3 C31 89.1(2) . . ?
C32 Ru3 C31 83.0(3) . . ?
C1 Ru3 C31 135.5(2) . . ?
C33 Ru3 Pt1 129.1(2) . . ?
C32 Ru3 Pt1 100.61(18) . . ?
C1 Ru3 Pt1 96.55(14) . . ?
C31 Ru3 Pt1 46.67(16) . . ?
C33 Ru3 Ru4 95.21(18) . . ?
C32 Ru3 Ru4 94.05(18) . . ?
C1 Ru3 Ru4 45.59(14) . . ?
C31 Ru3 Ru4 175.06(18) . . ?
Pt1 Ru3 Ru4 130.570(19) . . ?
C33 Ru3 Ru1 150.34(18) . . ?
C32 Ru3 Ru1 100.30(18) . . ?
C1 Ru3 Ru1 47.75(14) . . ?
C31 Ru3 Ru1 117.22(16) . . ?
Pt1 Ru3 Ru1 71.670(14) . . ?
Ru4 Ru3 Ru1 59.293(15) . . ?
C33 Ru3 Ru2 108.9(2) . . ?
C32 Ru3 Ru2 154.31(18) . . ?
C1 Ru3 Ru2 44.12(14) . . ?
C31 Ru3 Ru2 91.39(18) . . ?
Pt1 Ru3 Ru2 59.052(13) . . ?
Ru4 Ru3 Ru2 89.552(17) . . ?
Ru1 Ru3 Ru2 60.152(16) . . ?
C41 Ru4 C43 94.0(3) . . ?
C41 Ru4 C42 89.3(3) . . ?
C43 Ru4 C42 95.2(3) . . ?
C41 Ru4 C1 129.7(2) . . ?
C43 Ru4 C1 103.8(2) . . ?
C42 Ru4 C1 133.9(2) . . ?
C41 Ru4 Ru1 104.92(18) . . ?
C43 Ru4 Ru1 152.3(2) . . ?
C42 Ru4 Ru1 104.84(18) . . ?
C1 Ru4 Ru1 48.54(14) . . ?
C41 Ru4 Ru3 84.97(17) . . ?
C43 Ru4 Ru3 102.0(2) . . ?
C42 Ru4 Ru3 162.13(19) . . ?
C1 Ru4 Ru3 45.67(14) . . ?
Ru1 Ru4 Ru3 60.686(16) . . ?
C41 Ru4 Ru5 163.29(19) . . ?
C43 Ru4 Ru5 102.68(19) . . ?
C42 Ru4 Ru5 90.32(18) . . ?
C1 Ru4 Ru5 44.93(14) . . ?
Ru1 Ru4 Ru5 59.120(15) . . ?
Ru3 Ru4 Ru5 90.332(18) . . ?
C52 Ru5 C53 93.3(2) . . ?
C52 Ru5 C51 88.1(3) . . ?
C53 Ru5 C51 94.9(3) . . ?
C52 Ru5 C1 133.8(2) . . ?
C53 Ru5 C1 105.0(2) . . ?
C51 Ru5 C1 130.7(2) . . ?
C52 Ru5 Ru1 107.64(18) . . ?
C53 Ru5 Ru1 153.56(18) . . ?
C51 Ru5 Ru1 101.60(17) . . ?
C1 Ru5 Ru1 48.76(14) . . ?
C52 Ru5 Ru2 167.16(18) . . ?
C53 Ru5 Ru2 99.18(18) . . ?
C51 Ru5 Ru2 87.71(19) . . ?
C1 Ru5 Ru2 45.26(14) . . ?
Ru1 Ru5 Ru2 61.430(16) . . ?
C52 Ru5 Ru4 89.49(18) . . ?
C53 Ru5 Ru4 105.99(18) . . ?
C51 Ru5 Ru4 159.08(19) . . ?
C1 Ru5 Ru4 44.95(14) . . ?
Ru1 Ru5 Ru4 59.500(15) . . ?
Ru2 Ru5 Ru4 90.062(17) . . ?
C113 Ru11 C112 93.7(3) . . ?
C113 Ru11 C111 92.8(2) . . ?
C112 Ru11 C111 105.7(2) . . ?
C113 Ru11 C101 114.6(2) . . ?
C112 Ru11 C101 120.0(2) . . ?
C111 Ru11 C101 123.2(2) . . ?
C113 Ru11 Ru15 81.56(19) . . ?
C112 Ru11 Ru15 93.32(18) . . ?
C111 Ru11 Ru15 160.51(17) . . ?
C101 Ru11 Ru15 45.83(14) . . ?
C113 Ru11 Ru14 79.6(2) . . ?
C112 Ru11 Ru14 153.70(18) . . ?
C111 Ru11 Ru14 100.05(17) . . ?
C101 Ru11 Ru14 44.93(14) . . ?
Ru15 Ru11 Ru14 60.655(16) . . ?
C113 Ru11 Ru13 136.7(2) . . ?
C112 Ru11 Ru13 129.38(18) . . ?
C111 Ru11 Ru13 80.70(18) . . ?
C101 Ru11 Ru13 44.79(14) . . ?
Ru15 Ru11 Ru13 90.623(18) . . ?
Ru14 Ru11 Ru13 59.950(15) . . ?
C113 Ru11 Ru12 140.18(19) . . ?
C112 Ru11 Ru12 79.25(18) . . ?
C111 Ru11 Ru12 126.94(17) . . ?
C101 Ru11 Ru12 44.76(14) . . ?
Ru15 Ru11 Ru12 60.095(15) . . ?
Ru14 Ru11 Ru12 89.686(18) . . ?
Ru13 Ru11 Ru12 59.665(16) . . ?
C113 Ru11 Pt11 160.86(19) . . ?
C112 Ru11 Pt11 77.54(18) . . ?
C111 Ru11 Pt11 73.71(16) . . ?
C101 Ru11 Pt11 84.45(15) . . ?
Ru15 Ru11 Pt11 115.552(18) . . ?
Ru14 Ru11 Pt11 115.553(17) . . ?
Ru13 Ru11 Pt11 55.711(12) . . ?
Ru12 Ru11 Pt11 55.496(13) . . ?
C123 Ru12 C122 95.4(3) . . ?
C123 Ru12 C101 100.3(2) . . ?
C122 Ru12 C101 137.2(2) . . ?
C123 Ru12 C121 89.1(2) . . ?
C122 Ru12 C121 83.6(2) . . ?
C101 Ru12 C121 135.8(2) . . ?
C123 Ru12 Pt11 123.47(18) . . ?
C122 Ru12 Pt11 108.57(18) . . ?
C101 Ru12 Pt11 95.38(15) . . ?
C121 Ru12 Pt11 46.33(15) . . ?
C123 Ru12 Ru15 101.94(18) . . ?
C122 Ru12 Ru15 92.66(18) . . ?
C101 Ru12 Ru15 45.23(15) . . ?
C121 Ru12 Ru15 168.68(17) . . ?
Pt11 Ru12 Ru15 126.172(19) . . ?
C123 Ru12 Ru13 96.89(18) . . ?
C122 Ru12 Ru13 166.6(2) . . ?
C101 Ru12 Ru13 45.04(15) . . ?
C121 Ru12 Ru13 91.21(16) . . ?
Pt11 Ru12 Ru13 59.745(13) . . ?
Ru15 Ru12 Ru13 90.100(17) . . ?
C123 Ru12 Ru11 147.27(18) . . ?
C122 Ru12 Ru11 110.7(2) . . ?
C101 Ru12 Ru11 47.06(15) . . ?
C121 Ru12 Ru11 112.54(16) . . ?
Pt11 Ru12 Ru11 67.383(14) . . ?
Ru15 Ru12 Ru11 58.837(15) . . ?
Ru13 Ru12 Ru11 60.029(15) . . ?
C133 Ru13 C132 96.3(3) . . ?
C133 Ru13 C101 101.0(2) . . ?
C132 Ru13 C101 137.7(2) . . ?
C133 Ru13 C131 88.8(2) . . ?
C132 Ru13 C131 83.9(2) . . ?
C101 Ru13 C131 134.3(2) . . ?
C133 Ru13 Pt11 126.69(18) . . ?
C132 Ru13 Pt11 104.73(19) . . ?
C101 Ru13 Pt11 95.27(14) . . ?
C131 Ru13 Pt11 46.94(17) . . ?
C133 Ru13 Ru14 98.70(18) . . ?
C132 Ru13 Ru14 94.66(18) . . ?
C101 Ru13 Ru14 44.81(15) . . ?
C131 Ru13 Ru14 172.44(17) . . ?
Pt11 Ru13 Ru14 126.905(18) . . ?
C133 Ru13 Ru12 99.96(17) . . ?
C132 Ru13 Ru12 162.27(19) . . ?
C101 Ru13 Ru12 45.16(15) . . ?
C131 Ru13 Ru12 89.36(17) . . ?
Pt11 Ru13 Ru12 59.506(13) . . ?
Ru14 Ru13 Ru12 89.878(17) . . ?
C133 Ru13 Ru11 148.23(17) . . ?
C132 Ru13 Ru11 107.68(18) . . ?
C101 Ru13 Ru11 47.22(15) . . ?
C131 Ru13 Ru11 113.70(17) . . ?
Pt11 Ru13 Ru11 67.401(14) . . ?
Ru14 Ru13 Ru11 59.639(15) . . ?
Ru12 Ru13 Ru11 60.306(15) . . ?
C141 Ru14 C142 87.8(2) . . ?
C141 Ru14 C143 95.7(2) . . ?
C142 Ru14 C143 93.9(3) . . ?
C141 Ru14 C101 129.1(2) . . ?
C142 Ru14 C101 137.9(2) . . ?
C143 Ru14 C101 100.6(2) . . ?
C141 Ru14 Ru11 106.70(18) . . ?
C142 Ru14 Ru11 108.87(19) . . ?
C143 Ru14 Ru11 148.24(18) . . ?
C101 Ru14 Ru11 47.68(15) . . ?
C141 Ru14 Ru13 84.63(17) . . ?
C142 Ru14 Ru13 164.1(2) . . ?
C143 Ru14 Ru13 100.77(19) . . ?
C101 Ru14 Ru13 45.09(15) . . ?
Ru11 Ru14 Ru13 60.411(16) . . ?
C141 Ru14 Ru15 165.45(18) . . ?
C142 Ru14 Ru15 93.93(17) . . ?
C143 Ru14 Ru15 98.59(17) . . ?
C101 Ru14 Ru15 45.06(15) . . ?
Ru11 Ru14 Ru15 59.086(15) . . ?
Ru13 Ru14 Ru15 89.983(17) . . ?
C153 Ru15 C151 91.1(2) . . ?
C153 Ru15 C152 94.8(3) . . ?
C151 Ru15 C152 95.5(2) . . ?
C153 Ru15 C101 130.3(2) . . ?
C151 Ru15 C101 130.8(2) . . ?
C152 Ru15 C101 104.5(2) . . ?
C153 Ru15 Ru11 108.83(19) . . ?
C151 Ru15 Ru11 99.13(17) . . ?
C152 Ru15 Ru11 151.82(17) . . ?
C101 Ru15 Ru11 48.34(15) . . ?
C153 Ru15 Ru12 169.73(19) . . ?
C151 Ru15 Ru12 88.98(17) . . ?
C152 Ru15 Ru12 95.45(17) . . ?
C101 Ru15 Ru12 45.33(15) . . ?
Ru11 Ru15 Ru12 61.067(16) . . ?
C153 Ru15 Ru14 85.85(17) . . ?
C151 Ru15 Ru14 156.47(17) . . ?
C152 Ru15 Ru14 108.00(16) . . ?
C101 Ru15 Ru14 44.76(15) . . ?
Ru11 Ru15 Ru14 60.259(15) . . ?
Ru12 Ru15 Ru14 90.012(17) . . ?
C61 P1 C71 109.1(3) . . ?
C61 P1 C81 108.8(3) . . ?
C71 P1 C81 108.3(3) . . ?
C61 P1 Pt1 105.87(19) . . ?
C71 P1 Pt1 108.65(19) . . ?
C81 P1 Pt1 116.0(2) . . ?
C85 P11 C65 108.7(3) . . ?
C85 P11 C75 108.5(3) . . ?
C65 P11 C75 109.0(3) . . ?
C85 P11 Pt11 115.63(19) . . ?
C65 P11 Pt11 105.83(19) . . ?
C75 P11 Pt11 109.05(19) . . ?
Ru2 C1 Ru5 89.1(2) . . ?
Ru2 C1 Ru4 174.0(3) . . ?
Ru5 C1 Ru4 90.1(2) . . ?
Ru2 C1 Ru3 91.3(2) . . ?
Ru5 C1 Ru3 172.2(3) . . ?
Ru4 C1 Ru3 88.75(19) . . ?
Ru2 C1 Ru1 88.40(19) . . ?
Ru5 C1 Ru1 85.20(19) . . ?
Ru4 C1 Ru1 85.59(19) . . ?
Ru3 C1 Ru1 87.03(19) . . ?
O11 C11 Ru1 173.7(6) . . ?
O12 C12 Ru1 170.6(5) . . ?
O13 C13 Ru1 174.1(5) . . ?
O21 C21 Ru2 145.1(5) . . ?
O21 C21 Pt1 128.1(5) . . ?
Ru2 C21 Pt1 86.5(2) . . ?
O22 C22 Ru2 179.2(6) . . ?
O23 C23 Ru2 178.9(5) . . ?
O31 C31 Pt1 130.5(5) . . ?
O31 C31 Ru3 142.9(5) . . ?
Pt1 C31 Ru3 86.6(2) . . ?
O32 C32 Ru3 175.9(6) . . ?
O33 C33 Ru3 179.8(7) . . ?
O41 C41 Ru4 178.0(5) . . ?
O42 C42 Ru4 177.3(6) . . ?
O43 C43 Ru4 179.3(6) . . ?
O51 C51 Ru5 177.7(6) . . ?
O52 C52 Ru5 175.9(6) . . ?
O53 C53 Ru5 177.7(6) . . ?
C64 C61 C62 109.2(5) . . ?
C64 C61 C63 107.3(6) . . ?
C62 C61 C63 105.3(6) . . ?
C64 C61 P1 116.5(5) . . ?
C62 C61 P1 108.8(4) . . ?
C63 C61 P1 109.2(4) . . ?
C68 C65 C67 107.7(5) . . ?
C68 C65 C66 108.7(5) . . ?
C67 C65 C66 107.5(5) . . ?
C68 C65 P11 108.5(4) . . ?
C67 C65 P11 108.4(4) . . ?
C66 C65 P11 115.7(4) . . ?
C73 C71 C72 107.9(5) . . ?
C73 C71 C74 108.1(5) . . ?
C72 C71 C74 106.0(5) . . ?
C73 C71 P1 115.7(4) . . ?
C72 C71 P1 109.3(4) . . ?
C74 C71 P1 109.3(4) . . ?
C77 C75 C78 106.1(5) . . ?
C77 C75 C76 107.4(5) . . ?
C78 C75 C76 108.4(5) . . ?
C77 C75 P11 110.9(4) . . ?
C78 C75 P11 108.4(4) . . ?
C76 C75 P11 115.3(4) . . ?
C83 C81 C84 107.6(6) . . ?
C83 C81 C82 109.4(6) . . ?
C84 C81 C82 107.1(6) . . ?
C83 C81 P1 109.3(5) . . ?
C84 C81 P1 109.6(5) . . ?
C82 C81 P1 113.7(4) . . ?
C86 C85 C88 107.4(5) . . ?
C86 C85 C87 107.9(5) . . ?
C88 C85 C87 106.2(5) . . ?
C86 C85 P11 114.5(4) . . ?
C88 C85 P11 110.6(4) . . ?
C87 C85 P11 109.9(4) . . ?
Ru14 C101 Ru13 90.1(2) . . ?
Ru14 C101 Ru15 90.2(2) . . ?
Ru13 C101 Ru15 173.8(3) . . ?
Ru14 C101 Ru12 175.6(3) . . ?
Ru13 C101 Ru12 89.8(2) . . ?
Ru15 C101 Ru12 89.4(2) . . ?
Ru14 C101 Ru11 87.4(2) . . ?
Ru13 C101 Ru11 88.0(2) . . ?
Ru15 C101 Ru11 85.82(19) . . ?
Ru12 C101 Ru11 88.18(19) . . ?
O111 C111 Ru11 170.9(5) . . ?
O112 C112 Ru11 172.0(6) . . ?
O113 C113 Ru11 174.0(6) . . ?
O121 C121 Ru12 143.0(5) . . ?
O121 C121 Pt11 129.3(5) . . ?
Ru12 C121 Pt11 87.8(2) . . ?
O122 C122 Ru12 176.7(6) . . ?
O123 C123 Ru12 175.9(5) . . ?
O131 C131 Ru13 144.0(5) . . ?
O131 C131 Pt11 128.4(5) . . ?
Ru13 C131 Pt11 87.4(2) . . ?
O132 C132 Ru13 176.9(6) . . ?
O133 C133 Ru13 176.8(5) . . ?
O141 C141 Ru14 175.8(5) . . ?
O142 C142 Ru14 175.8(5) . . ?
O143 C143 Ru14 178.0(6) . . ?
O151 C151 Ru15 177.4(5) . . ?
O152 C152 Ru15 176.7(5) . . ?
O153 C153 Ru15 176.6(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C31 2.032(6) . ?
Pt1 C21 2.059(6) . ?
Pt1 P1 2.3307(14) . ?
Pt1 Ru3 2.7894(5) . ?
Pt1 Ru2 2.8018(5) . ?
Pt11 C121 2.042(5) . ?
Pt11 C131 2.069(6) . ?
Pt11 P11 2.3432(14) . ?
Pt11 Ru12 2.8213(5) . ?
Pt11 Ru13 2.8282(5) . ?
Pt11 Ru11 3.1603(5) . ?
Ru1 C13 1.897(6) . ?
Ru1 C12 1.906(6) . ?
Ru1 C11 1.925(6) . ?
Ru1 C1 2.119(5) . ?
Ru1 Ru5 2.8086(6) . ?
Ru1 Ru4 2.8196(6) . ?
Ru1 Ru3 2.8595(6) . ?
Ru1 Ru2 2.8829(6) . ?
Ru2 C23 1.879(6) . ?
Ru2 C22 1.913(6) . ?
Ru2 C1 2.014(5) . ?
Ru2 C21 2.028(6) . ?
Ru2 Ru5 2.8355(6) . ?
Ru2 Ru3 2.8928(6) . ?
Ru3 C33 1.886(6) . ?
Ru3 C32 1.911(6) . ?
Ru3 C1 2.032(5) . ?
Ru3 C31 2.034(6) . ?
Ru3 Ru4 2.8407(7) . ?
Ru4 C41 1.900(6) . ?
Ru4 C43 1.909(6) . ?
Ru4 C42 1.915(6) . ?
Ru4 C1 2.030(5) . ?
Ru4 Ru5 2.8726(6) . ?
Ru5 C52 1.906(6) . ?
Ru5 C53 1.910(6) . ?
Ru5 C51 1.917(6) . ?
Ru5 C1 2.029(5) . ?
Ru11 C113 1.908(6) . ?
Ru11 C112 1.925(6) . ?
Ru11 C111 1.926(6) . ?
Ru11 C101 2.106(5) . ?
Ru11 Ru15 2.8112(6) . ?
Ru11 Ru14 2.8450(6) . ?
Ru11 Ru13 2.8672(6) . ?
Ru11 Ru12 2.8752(6) . ?
Ru12 C123 1.892(7) . ?
Ru12 C122 1.909(6) . ?
Ru12 C101 2.025(5) . ?
Ru12 C121 2.028(6) . ?
Ru12 Ru15 2.8478(6) . ?
Ru12 Ru13 2.8567(6) . ?
Ru13 C133 1.893(6) . ?
Ru13 C132 1.918(6) . ?
Ru13 C101 2.021(5) . ?
Ru13 C131 2.026(6) . ?
Ru13 Ru14 2.8540(6) . ?
Ru14 C141 1.913(6) . ?
Ru14 C142 1.916(6) . ?
Ru14 C143 1.921(7) . ?
Ru14 C101 2.011(5) . ?
Ru14 Ru15 2.8562(6) . ?
Ru15 C153 1.912(6) . ?
Ru15 C151 1.917(6) . ?
Ru15 C152 1.918(6) . ?
Ru15 C101 2.022(5) . ?
P1 C61 1.897(7) . ?
P1 C71 1.914(6) . ?
P1 C81 1.926(7) . ?
P11 C85 1.907(6) . ?
P11 C65 1.917(6) . ?
P11 C75 1.921(6) . ?
O11 C11 1.127(7) . ?
O12 C12 1.148(7) . ?
O13 C13 1.144(7) . ?
O21 C21 1.158(7) . ?
O22 C22 1.140(7) . ?
O23 C23 1.133(7) . ?
O31 C31 1.167(7) . ?
O32 C32 1.135(7) . ?
O33 C33 1.143(7) . ?
O41 C41 1.150(7) . ?
O42 C42 1.134(7) . ?
O43 C43 1.134(7) . ?
O51 C51 1.134(7) . ?
O52 C52 1.131(7) . ?
O53 C53 1.129(7) . ?
O111 C111 1.132(7) . ?
O112 C112 1.147(7) . ?
O113 C113 1.134(7) . ?
O121 C121 1.157(7) . ?
O122 C122 1.146(7) . ?
O123 C123 1.121(7) . ?
O131 C131 1.150(7) . ?
O132 C132 1.131(7) . ?
O133 C133 1.136(7) . ?
O141 C141 1.130(6) . ?
O142 C142 1.136(7) . ?
O143 C143 1.117(7) . ?
O151 C151 1.132(7) . ?
O152 C152 1.126(7) . ?
O153 C153 1.134(7) . ?
C61 C64 1.531(8) . ?
C61 C62 1.534(9) . ?
C61 C63 1.542(10) . ?
C65 C68 1.531(9) . ?
C65 C67 1.536(8) . ?
C65 C66 1.541(8) . ?
C71 C73 1.526(8) . ?
C71 C72 1.526(8) . ?
C71 C74 1.538(9) . ?
C75 C77 1.530(9) . ?
C75 C78 1.532(8) . ?
C75 C76 1.534(8) . ?
C81 C83 1.516(10) . ?
C81 C84 1.538(10) . ?
C81 C82 1.540(8) . ?
C85 C86 1.535(8) . ?
C85 C88 1.545(9) . ?
C85 C87 1.551(8) . ?
