#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/34/4313452.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4313452
loop_
_publ_author_name
'Megumu Munakata'
'Liang Ping Wu'
'Takayoshi Kuroda-Sowa'
'Masahiko Maekawa'
'Yusaku Suenaga'
'Tetsuhiro Ohta'
'Hisashi Konaka'
_publ_section_title
;
 Construction of the Multidecker Anthracene-Silver(I) System by
 Intramolecular π-π Interactions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2553
_journal_page_last               2558
_journal_paper_doi               10.1021/ic020379l
_journal_volume                  42
_journal_year                    2003
_chemical_formula_moiety         'C36 H24 Ag4 F12 O12 S4 '
_chemical_formula_sum            'C36 H24 Ag4 F12 O12 S4'
_chemical_formula_weight         1436.27
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                94.67(3)
_cell_angle_beta                 112.93(3)
_cell_angle_gamma                107.97(3)
_cell_formula_units_Z            1
_cell_length_a                   10.622(5)
_cell_length_b                   11.474(4)
_cell_length_c                   10.426(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      18.9
_cell_measurement_theta_min      15.5
_cell_volume                     1083.3(9)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  SHELXL97
_computing_structure_solution    SIR88
_diffrn_measured_fraction_theta_full 1.00
_diffrn_measured_fraction_theta_max 1.00
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       ω-2θ
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.012
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            5237
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_standards_decay_%        1.20
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    2.082
_exptl_absorpt_correction_T_max  0.659
_exptl_absorpt_correction_T_min  0.604
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.202
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             696.0
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.250
_exptl_crystal_size_min          0.200
_refine_diff_density_max         2.07
_refine_diff_density_min         -1.85
_refine_ls_extinction_coef       0.0000
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     316
_refine_ls_number_reflns         3993
_refine_ls_R_factor_gt           0.0535
_refine_ls_shift/su_max          0.0020
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[σ²(Fo²) + (0.0809P)²+4.0909P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1567
_reflns_number_gt                3993
_reflns_number_total             4967
_reflns_threshold_expression     >2.0sigma(I)
_cod_data_source_file            ic020379l_2.cif
_cod_data_source_block           '[Ag2(dpan)0.5_(CF3SO3)2(be'
_cod_original_cell_volume        1083.2(9)
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C36 H24 Ag4 F12 O12 S4 '
_cod_database_code               4313452
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag(1) Ag 1.12251(6) 0.24051(5) 0.91964(5) 0.0531(2) Uani 1.00 d . . .
Ag(2) Ag 1.66850(5) 0.39905(5) 0.91156(6) 0.0532(2) Uani 1.00 d . . .
S(1) S 1.0271(1) 0.3985(1) 1.1443(1) 0.0299(2) Uani 1.00 d . . .
S(2) S 1.5010(2) 0.3821(2) 1.1404(2) 0.0508(4) Uani 1.00 d . . .
F(1) F 0.8828(7) 0.2369(5) 1.2457(6) 0.097(2) Uani 1.00 d . . .
F(2) F 1.1147(8) 0.2846(6) 1.3492(6) 0.097(2) Uani 1.00 d . . .
F(3) F 1.0225(7) 0.4168(5) 1.3929(5) 0.082(2) Uani 1.00 d . . .
F(4) F 1.546(2) 0.229(1) 1.300(2) 0.154(6) Uani 0.60 d P . .
F(5) F 1.680(1) 0.387(1) 1.394(1) 0.223(7) Uani 1.00 d . . .
F(6) F 1.591(3) 0.477(3) 1.390(2) 0.18(1) Uani 0.40 d P . .
F(7) F 1.451(1) 0.324(1) 1.352(1) 0.208(6) Uani 1.00 d . . .
O(1) O 0.9147(5) 0.4507(5) 1.1019(5) 0.053(1) Uani 1.00 d . . .
O(2) O 0.9983(5) 0.2915(4) 1.0388(5) 0.0455(9) Uani 1.00 d . . .
O(3) O 1.1738(5) 0.4913(4) 1.2079(5) 0.055(1) Uani 1.00 d . . .
O(4) O 1.371(1) 0.329(2) 1.065(1) 0.31(1) Uani 1.00 d . . .
O(5) O 1.6211(8) 0.421(1) 1.1169(8) 0.150(5) Uani 1.00 d . . .
O(6) O 1.511(2) 0.513(1) 1.186(1) 0.169(5) Uani 1.00 d . . .
C(1) C 1.0766(6) 0.3176(5) 0.7013(6) 0.035(1) Uani 1.00 d . . .
C(2) C 1.1537(5) 0.2441(4) 0.6850(5) 0.0303(10) Uani 1.00 d . . .
C(3) C 1.0783(5) 0.1203(4) 0.5924(5) 0.0231(8) Uani 1.00 d . . .
C(4) C 1.1566(5) 0.0477(4) 0.5733(5) 0.0241(8) Uani 1.00 d . . .
C(5) C 0.9208(5) 0.0737(4) 0.5196(5) 0.0234(8) Uani 1.00 d . . .
C(6) C 0.8452(5) 0.1507(5) 0.5440(6) 0.032(1) Uani 1.00 d . . .
C(7) C 0.9199(6) 0.2684(5) 0.6312(6) 0.037(1) Uani 1.00 d . . .
C(8) C 1.3205(5) 0.0965(4) 0.6493(5) 0.0269(9) Uani 1.00 d . . .
C(9) C 1.3923(6) 0.0549(6) 0.7678(7) 0.048(1) Uani 1.00 d . . .
C(10) C 1.5443(7) 0.0975(8) 0.8354(8) 0.061(2) Uani 1.00 d . . .
C(11) C 1.6282(6) 0.1826(7) 0.7862(8) 0.052(2) Uani 1.00 d . . .
C(12) C 1.5583(6) 0.2260(7) 0.6704(8) 0.054(2) Uani 1.00 d . . .
C(13) C 1.4044(6) 0.1831(6) 0.6019(7) 0.045(1) Uani 1.00 d . . .
C(14) C 1.0114(9) 0.3306(6) 1.2917(8) 0.055(2) Uani 1.00 d . . .
C(15) C 1.557(1) 0.354(2) 1.316(1) 0.111(5) Uani 1.00 d . . .
C(16) C 1.125(2) 0.0334(10) 1.119(2) 0.111(5) Uani 1.00 d . . .
C(17) C 1.125(1) 0.0229(9) 0.992(2) 0.097(4) Uani 1.00 d . . .
C(18) C 1.003(3) -0.0080(10) 0.875(1) 0.104(5) Uani 1.00 d . . .
H(1) H 1.1283 0.4009 0.7593 0.0425 Uiso 1.00 calc . . .
H(2) H 1.2580 0.2761 0.7360 0.0364 Uiso 1.00 calc . . .
H(3) H 0.7407 0.1191 0.4983 0.0388 Uiso 1.00 calc . . .
H(4) H 0.8671 0.3178 0.6453 0.0444 Uiso 1.00 calc . . .
H(5) H 1.3364 -0.0037 0.8030 0.0581 Uiso 1.00 calc . . .
H(6) H 1.5916 0.0681 0.9168 0.0732 Uiso 1.00 calc . . .
H(7) H 1.7325 0.2105 0.8318 0.0629 Uiso 1.00 calc . . .
H(8) H 1.6148 0.2853 0.6364 0.0646 Uiso 1.00 calc . . .
H(9) H 1.3572 0.2139 0.5220 0.0545 Uiso 1.00 calc . . .
H(10) H 1.2138 0.0586 1.2040 0.1332 Uiso 1.00 calc . . .
H(11) H 1.2154 0.0379 0.9863 0.1167 Uiso 1.00 calc . . .
H(12) H 1.0062 -0.0122 0.7851 0.1243 Uiso 1.00 calc . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.897 1.101
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
S S 0.125 0.123
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
F F 0.017 0.010
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
O O 0.011 0.006
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
C C 0.003 0.002
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
H H 0.000 0.000
;International Tables for Crystallography
(1992, Vol. C, Table 6.1.1.4)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O(2) Ag(1) O(4) 109.2(4) . . . yes
O(2) Ag(1) C(1) 112.5(2) . . . yes
O(4) Ag(1) C(1) 107.7(4) . . . yes
O(1) Ag(2) O(3) 79.2(2) 1_655 . 2_867 yes
O(1) Ag(2) O(5) 79.8(2) 1_655 . . yes
O(1) Ag(2) O(6) 141.3(3) 1_655 . 2_867 yes
O(1) Ag(2) C(11) 99.1(2) 1_655 . . yes
O(1) Ag(2) C(12) 122.6(2) 1_655 . . yes
O(3) Ag(2) O(5) 144.3(3) 2_867 . . yes
O(3) Ag(2) O(6) 94.6(4) 2_867 . 2_867 yes
O(3) Ag(2) C(11) 92.1(2) 2_867 . . yes
O(3) Ag(2) C(12) 79.1(2) 2_867 . . yes
O(5) Ag(2) O(6) 84.2(5) . . 2_867 yes
O(5) Ag(2) C(11) 119.6(4) . . . yes
O(5) Ag(2) C(12) 136.6(3) . . . yes
O(6) Ag(2) C(11) 119.4(3) 2_867 . . yes
O(6) Ag(2) C(12) 92.8(3) 2_867 . . yes
C(11) Ag(2) C(12) 30.5(2) . . . yes
O(1) S(1) O(2) 113.7(3) . . . yes
O(1) S(1) O(3) 113.8(3) . . . yes
O(1) S(1) C(14) 103.8(4) . . . yes
O(2) S(1) O(3) 116.1(3) . . . yes
O(2) S(1) C(14) 103.7(3) . . . yes
O(3) S(1) C(14) 103.8(3) . . . yes
O(4) S(2) O(5) 134.7(8) . . . yes
O(4) S(2) O(6) 101(1) . . . yes
O(4) S(2) C(15) 113.4(9) . . . yes
O(5) S(2) O(6) 93.7(9) . . . yes
O(5) S(2) C(15) 107.5(6) . . . yes
O(6) S(2) C(15) 94.2(8) . . . yes
Ag(2) O(1) S(1) 138.4(3) 1_455 . . yes
Ag(1) O(2) S(1) 135.4(3) . . . yes
Ag(2) O(3) S(1) 129.6(3) 2_867 . . yes
Ag(1) O(4) S(2) 176(1) . . . yes
Ag(2) O(5) S(2) 135.0(4) . . . yes
Ag(2) O(6) S(2) 127.7(6) 2_867 . . yes
Ag(1) C(1) C(2) 80.5(3) . . . yes
Ag(1) C(1) C(7) 101.3(4) . . . yes
Ag(1) C(1) H(1) 88.3 . . . no
C(2) C(1) C(7) 120.0(4) . . . yes
C(2) C(1) H(1) 120.0 . . . no
C(7) C(1) H(1) 120.0 . . . no
C(1) C(2) C(3) 121.0(4) . . . yes
C(1) C(2) H(2) 119.5 . . . no
C(3) C(2) H(2) 119.5 . . . no
C(2) C(3) C(4) 120.9(4) . . . yes
C(2) C(3) C(5) 118.1(5) . . . yes
C(4) C(3) C(5) 121.0(4) . . . yes
C(3) C(4) C(5) 119.5(4) . . 2_756 yes
C(3) C(4) C(8) 120.8(4) . . . yes
C(5) C(4) C(8) 119.7(5) 2_756 . . yes
C(3) C(5) C(4) 119.4(5) . . 2_756 yes
C(3) C(5) C(6) 119.0(4) . . . yes
C(4) C(5) C(6) 121.5(4) 2_756 . . yes
C(5) C(6) C(7) 121.5(5) . . . yes
C(5) C(6) H(3) 119.3 . . . no
C(7) C(6) H(3) 119.3 . . . no
C(1) C(7) C(6) 120.3(6) . . . yes
C(1) C(7) H(4) 119.9 . . . no
C(6) C(7) H(4) 119.9 . . . no
C(4) C(8) C(9) 121.0(5) . . . yes
C(4) C(8) C(13) 120.6(5) . . . yes
C(9) C(8) C(13) 118.4(5) . . . yes
C(8) C(9) C(10) 120.8(7) . . . yes
C(8) C(9) H(5) 119.6 . . . no
C(10) C(9) H(5) 119.6 . . . no
C(9) C(10) C(11) 120.7(7) . . . yes
C(9) C(10) H(6) 119.6 . . . no
C(11) C(10) H(6) 119.7 . . . no
Ag(2) C(11) C(10) 105.8(6) . . . yes
Ag(2) C(11) C(12) 79.9(5) . . . yes
Ag(2) C(11) H(7) 84.6 . . . no
C(10) C(11) C(12) 118.9(6) . . . yes
C(10) C(11) H(7) 120.5 . . . no
C(12) C(11) H(7) 120.5 . . . no
Ag(2) C(12) C(11) 69.6(4) . . . yes
Ag(2) C(12) C(13) 111.4(6) . . . yes
Ag(2) C(12) H(8) 89.0 . . . no
C(11) C(12) C(13) 120.4(7) . . . yes
C(11) C(12) H(8) 119.7 . . . no
C(13) C(12) H(8) 119.8 . . . no
C(8) C(13) C(12) 120.7(6) . . . yes
C(8) C(13) H(9) 119.6 . . . no
C(12) C(13) H(9) 119.7 . . . no
S(1) C(14) F(1) 110.3(5) . . . yes
S(1) C(14) F(2) 111.3(7) . . . yes
S(1) C(14) F(3) 110.6(5) . . . yes
F(1) C(14) F(2) 107.4(6) . . . yes
F(1) C(14) F(3) 108.6(9) . . . yes
F(2) C(14) F(3) 108.5(6) . . . yes
S(2) C(15) F(4) 105.7(10) . . . yes
S(2) C(15) F(5) 120(1) . . . yes
S(2) C(15) F(6) 97(1) . . . yes
S(2) C(15) F(7) 112.4(9) . . . yes
F(4) C(15) F(5) 90(1) . . . yes
F(4) C(15) F(6) 156(1) . . . yes
F(4) C(15) F(7) 88(1) . . . yes
F(5) C(15) F(6) 75(1) . . . yes
F(5) C(15) F(7) 124(1) . . . yes
F(6) C(15) F(7) 84(1) . . . yes
C(17) C(16) C(18) 118(1) . . 2_757 yes
C(17) C(16) H(10) 120.8 . . . no
C(18) C(16) H(10) 120.7 2_757 . . no
C(16) C(17) C(18) 121(1) . . . yes
C(16) C(17) H(11) 119.4 . . . no
C(18) C(17) H(11) 119.5 . . . no
C(16) C(18) C(17) 120(1) 2_757 . . yes
C(16) C(18) H(12) 119.9 2_757 . . no
C(17) C(18) H(12) 119.7 . . . no
O(2) Ag(1) O(4) 109.2(4) . . . yes
O(2) Ag(1) C(1) 112.5(2) . . . yes
O(2) Ag(1) C(2) 143.8(2) . . . yes
O(2) Ag(1) C(18) 97.7(6) . . . yes
O(2) Ag(1) C(17) 99.2(5) . . . yes
O(4) Ag(1) C(1) 107.7(4) . . . yes
O(4) Ag(1) C(2) 94.0(4) . . . yes
O(4) Ag(1) C(18) 115.5(7) . . . yes
O(4) Ag(1) C(17) 88.6(6) . . . yes
C(1) Ag(1) C(2) 31.8(2) . . . yes
C(1) Ag(1) C(18) 114.1(3) . . . yes
C(1) Ag(1) C(17) 136.0(5) . . . yes
C(2) Ag(1) C(18) 96.8(4) . . . yes
C(2) Ag(1) C(17) 109.1(5) . . . yes
C(18) Ag(1) C(17) 28.4(5) . . . yes
O(6) Ag(2) O(5) 84.2(5) 2_867 . . yes
O(6) Ag(2) O(1) 141.3(3) 2_867 . 1_655 yes
O(6) Ag(2) C(11) 119.4(3) 2_867 . . yes
O(6) Ag(2) O(3) 94.6(4) 2_867 . 2_867 yes
O(6) Ag(2) C(12) 92.8(3) 2_867 . . yes
O(5) Ag(2) O(1) 79.8(2) . . 1_655 yes
O(5) Ag(2) C(11) 119.6(4) . . . yes
O(5) Ag(2) O(3) 144.3(3) . . 2_867 yes
O(5) Ag(2) C(12) 136.6(3) . . . yes
O(1) Ag(2) C(11) 99.1(2) 1_655 . . yes
O(1) Ag(2) O(3) 79.2(2) 1_655 . 2_867 yes
O(1) Ag(2) C(12) 122.6(2) 1_655 . . yes
C(11) Ag(2) O(3) 92.1(2) . . 2_867 yes
C(11) Ag(2) C(12) 30.5(2) . . . yes
O(3) Ag(2) C(12) 79.1(2) 2_867 . . yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag(1) O(2) 2.294(6) . . yes
Ag(1) O(4) 2.296(9) . . yes
Ag(1) C(1) 2.435(6) . . yes
Ag(2) O(1) 2.436(4) . 1_655 yes
Ag(2) O(3) 2.553(6) . 2_867 yes
Ag(2) O(5) 2.39(1) . . yes
Ag(2) O(6) 2.36(2) . 2_867 yes
Ag(2) C(11) 2.537(8) . . yes
Ag(2) C(12) 2.664(7) . . yes
S(1) O(1) 1.433(6) . . yes
S(1) O(2) 1.448(5) . . yes
S(1) O(3) 1.434(4) . . yes
S(1) C(14) 1.820(9) . . yes
S(2) O(4) 1.206(9) . . yes
S(2) O(5) 1.341(10) . . yes
S(2) O(6) 1.49(1) . . yes
S(2) C(15) 1.78(1) . . yes
F(1) C(14) 1.323(9) . . yes
F(2) C(14) 1.32(1) . . yes
F(3) C(14) 1.33(1) . . yes
F(4) C(15) 1.40(2) . . yes
F(5) C(15) 1.16(1) . . yes
F(6) C(15) 1.41(4) . . yes
F(7) C(15) 1.28(2) . . yes
C(1) C(2) 1.386(9) . . yes
C(1) C(7) 1.424(8) . . yes
C(1) H(1) 0.951 . . no
C(2) C(3) 1.437(6) . . yes
C(2) H(2) 0.951 . . no
C(3) C(4) 1.399(8) . . yes
C(3) C(5) 1.433(6) . . yes
C(4) C(5) 1.417(6) . 2_756 yes
C(4) C(8) 1.490(6) . . yes
C(5) C(6) 1.432(9) . . yes
C(6) C(7) 1.362(7) . . yes
C(6) H(3) 0.950 . . no
C(7) H(4) 0.951 . . no
C(8) C(9) 1.386(9) . . yes
C(8) C(13) 1.379(9) . . yes
C(9) C(10) 1.383(9) . . yes
C(9) H(5) 0.950 . . no
C(10) C(11) 1.38(1) . . yes
C(10) H(6) 0.952 . . no
C(11) C(12) 1.37(1) . . yes
C(11) H(7) 0.950 . . no
C(12) C(13) 1.401(8) . . yes
C(12) H(8) 0.950 . . no
C(13) H(9) 0.950 . . no
C(16) C(17) 1.32(3) . . yes
C(16) C(18) 1.32(3) . 2_757 yes
C(16) H(10) 0.950 . . no
C(17) C(18) 1.31(2) . . yes
C(17) H(11) 0.950 . . no
C(18) H(12) 0.950 . . no
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_1
_geom_contact_site_symmetry_2
_geom_contact_publ_flag
Ag(2) O(3) 2.553(6) . 2_867 ?
Ag(2) C(11) 2.537(8) . . ?
Ag(2) C(12) 2.664(7) . . ?
S(1) O(1) 3.355(6) . 2_767 ?
F(1) C(6) 3.469(10) . 1_556 ?
F(1) C(5) 3.501(8) . 1_556 ?
F(2) C(3) 3.350(8) . 1_556 ?
F(2) F(6) 3.39(2) . 2_868 ?
F(2) C(2) 3.450(9) . 1_556 ?
F(3) F(5) 3.05(1) . 2_868 ?
F(3) F(3) 3.09(1) . 2_768 ?
F(3) C(1) 3.395(8) . 1_556 ?
F(3) C(7) 3.452(9) . 1_556 ?
F(3) C(7) 3.521(8) . 2_767 ?
F(3) F(5) 3.55(2) . 1_455 ?
F(3) F(6) 3.56(2) . 2_868 ?
F(4) C(10) 3.58(2) . 2_857 ?
F(4) C(9) 3.58(2) . 2_857 ?
F(5) C(7) 3.50(2) . 1_656 ?
F(7) C(13) 3.29(2) . 1_556 ?
F(7) C(12) 3.47(2) . 1_556 ?
O(1) O(5) 3.10(1) . 1_455 ?
O(1) C(1) 3.178(8) . 2_767 ?
O(1) O(3) 3.182(7) . 2_767 ?
O(1) O(1) 3.35(1) . 2_767 ?
O(1) O(2) 3.440(7) . 2_767 ?
O(1) C(7) 3.529(7) . 2_767 ?
O(2) C(11) 3.510(7) . 1_455 ?
Ag(1) C(2) 2.595(6) . . ?
Ag(1) C(18) 2.65(1) . . ?
Ag(1) C(17) 2.67(1) . . ?
Ag(2) C(11) 2.537(8) . . ?
Ag(2) O(3) 2.553(6) . 2_867 ?
Ag(2) C(12) 2.664(7) . . ?
