#------------------------------------------------------------------------------
#$Date: 2016-03-23 02:44:31 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179202 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/37/4313718.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4313718
loop_
_publ_author_name
'Marie-Line Lehaire'
'Axel Schulz'
'Rosario Scopelliti'
'Kay Severin'
_publ_contact_author_address
;
Institut de Chimie Moléculaire et Biologique
École Polytechnique Fédérale de Lausanne
1015 Lausanne
Switzerland
;
_publ_contact_author_email       kay.severin@epfl.ch
_publ_contact_author_fax         '+41 21 693 9305'
_publ_contact_author_name        'Kay Severin'
_publ_contact_author_phone       '+41 21 693 9302'
_publ_section_title
;
 Electronic Effects in 12-Metallacrown-3 Complexes. A Theoretical and
 Experimental Study
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3576
_journal_page_last               3581
_journal_paper_doi               10.1021/ic034042a
_journal_volume                  42
_journal_year                    2003
_chemical_formula_moiety         'C45 H48 Cl4 N3 Na O6 Ru3, C H Cl3, 2(H2 O)'
_chemical_formula_sum            'C46 H53 Cl7 N3 Na O8 Ru3'
_chemical_formula_weight         1350.26
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 105.586(15)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   19.957(5)
_cell_length_b                   16.444(4)
_cell_length_c                   32.834(4)
_cell_measurement_reflns_used    2201
_cell_measurement_temperature    140(2)
_cell_measurement_theta_max      20.0064
_cell_measurement_theta_min      1.63345
_cell_volume                     10379(4)
_computing_cell_refinement       'Oxford Diffraction CrysAlis RED'
_computing_data_collection       'marresearch mar345'
_computing_data_reduction        'Oxford Diffraction CrysAlis RED'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      140(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'marresearch mar345 IPDS'
_diffrn_measurement_method
'60 images with deltaphi = 3 deg. and exp. time = 180 sec.'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0598
_diffrn_reflns_av_sigmaI/netI    0.0521
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            27887
_diffrn_reflns_theta_full        24.41
_diffrn_reflns_theta_max         24.41
_diffrn_reflns_theta_min         3.21
_exptl_absorpt_coefficient_mu    1.284
_exptl_absorpt_correction_T_max  0.5720
_exptl_absorpt_correction_T_min  0.1070
_exptl_absorpt_correction_type   refdelf
_exptl_absorpt_process_details
; 
(See: Walker, N. & Stuart, D. (1983) Acta Cryst. A39, 158-166) 
;
_exptl_crystal_colour            'deep yellow'
_exptl_crystal_density_diffrn    1.728
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             5408
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.720
_refine_diff_density_min         -1.413
_refine_diff_density_rms         0.098
_refine_ls_extinction_coef       0.00019(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.151
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     628
_refine_ls_number_reflns         8436
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.151
_refine_ls_R_factor_all          0.0875
_refine_ls_R_factor_gt           0.0613
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0968P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1656
_refine_ls_wR_factor_ref         0.1858
_reflns_number_gt                5636
_reflns_number_total             8436
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic034042asi20030116_034304_3.cif
_cod_data_source_block           3_x_NaCl
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_database_code               4313718
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.12722(4) -0.09613(4) -0.13908(2) 0.0717(2) Uani 1 1 d . . .
Ru2 Ru 0.36775(4) -0.04452(6) -0.177865(19) 0.0801(3) Uani 1 1 d . . .
Ru3 Ru 0.31211(3) 0.11581(4) -0.047683(17) 0.0644(2) Uani 1 1 d . . .
Cl1 Cl 0.16176(14) 0.07295(17) -0.31997(7) 0.0909(7) Uani 1 1 d . . .
Cl2 Cl 0.34387(14) 0.36750(19) -0.15632(10) 0.1071(9) Uani 1 1 d . . .
Cl3 Cl 0.00440(10) 0.21007(14) -0.18763(6) 0.0728(5) Uani 1 1 d . . .
Cl4 Cl 0.35301(13) -0.17334(15) -0.03837(7) 0.0884(7) Uani 1 1 d . . .
Na1 Na 0.29744(16) -0.0686(2) -0.09534(9) 0.0678(8) Uani 1 1 d . . .
O1 O 0.2195(3) -0.0873(3) -0.15798(15) 0.0661(13) Uani 1 1 d . . .
O2 O 0.0888(3) -0.0710(4) -0.20218(17) 0.0744(15) Uani 1 1 d . . .
O3 O 0.3514(3) 0.0212(4) -0.12690(14) 0.0653(13) Uani 1 1 d . . .
O4 O 0.3814(3) 0.0736(5) -0.19596(17) 0.0887(19) Uani 1 1 d . . .
O5 O 0.2358(3) 0.0351(3) -0.08094(14) 0.0599(12) Uani 1 1 d . . .
O6 O 0.2283(3) 0.1932(3) -0.06770(14) 0.0655(13) Uani 1 1 d . . .
N1 N 0.2607(4) -0.0218(5) -0.20870(18) 0.0694(17) Uani 1 1 d . . .
N2 N 0.3277(3) 0.1506(4) -0.10766(18) 0.0647(16) Uani 1 1 d . . .
N3 N 0.1335(3) 0.0342(4) -0.13417(17) 0.0568(14) Uani 1 1 d . . .
C1 C 0.2091(4) -0.0494(5) -0.1944(2) 0.064(2) Uani 1 1 d . . .
C2 C 0.1368(4) -0.0421(5) -0.2185(2) 0.068(2) Uani 1 1 d . . .
C3 C 0.1229(5) -0.0028(5) -0.2581(2) 0.076(2) Uani 1 1 d . . .
H3 H 0.0767 0.0047 -0.2751 0.091 Uiso 1 1 calc R . .
C4 C 0.1793(5) 0.0244(6) -0.2710(2) 0.074(2) Uani 1 1 d . . .
C5 C 0.2452(5) 0.0165(6) -0.2475(2) 0.076(2) Uani 1 1 d . . .
H5 H 0.2819 0.0376 -0.2578 0.092 Uiso 1 1 calc R . .
C6 C 0.3462(4) 0.0981(6) -0.1346(2) 0.066(2) Uani 1 1 d . . .
C7 C 0.3640(4) 0.1292(7) -0.1714(3) 0.079(2) Uani 1 1 d . . .
C8 C 0.3640(4) 0.2116(8) -0.1784(3) 0.092(3) Uani 1 1 d . . .
H8 H 0.3766 0.2330 -0.2022 0.110 Uiso 1 1 calc R . .
C9 C 0.3448(5) 0.2632(6) -0.1495(3) 0.082(3) Uani 1 1 d . . .
C10 C 0.3269(4) 0.2320(6) -0.1155(3) 0.075(2) Uani 1 1 d . . .
H10 H 0.3134 0.2682 -0.0966 0.090 Uiso 1 1 calc R . .
C11 C 0.1827(4) 0.0745(5) -0.1050(2) 0.0591(17) Uani 1 1 d . . .
C12 C 0.1793(4) 0.1602(4) -0.0982(2) 0.0584(17) Uani 1 1 d . . .
C13 C 0.1234(4) 0.2024(5) -0.1234(2) 0.0582(17) Uani 1 1 d . . .
H13 H 0.1185 0.2592 -0.1196 0.070 Uiso 1 1 calc R . .
C14 C 0.0748(4) 0.1602(5) -0.1542(2) 0.0588(17) Uani 1 1 d . . .
C15 C 0.0793(4) 0.0770(5) -0.1590(2) 0.0650(19) Uani 1 1 d . . .
H15 H 0.0444 0.0495 -0.1799 0.078 Uiso 1 1 calc R . .
C16 C 0.0508(6) -0.1067(7) -0.1037(4) 0.098(3) Uani 1 1 d . . .
C17 C 0.0327(5) -0.1577(7) -0.1374(3) 0.093(3) Uani 1 1 d . . .
H17 H -0.0122 -0.1529 -0.1565 0.112 Uiso 1 1 calc R . .
C18 C 0.0776(7) -0.2157(8) -0.1445(5) 0.127(5) Uani 1 1 d . . .
H18 H 0.0595 -0.2516 -0.1675 0.153 Uiso 1 1 calc R . .
C19 C 0.1414(9) -0.2273(9) -0.1235(7) 0.154(7) Uani 1 1 d D . .
C20 C 0.1651(6) -0.1770(12) -0.0860(6) 0.145(7) Uani 1 1 d . . .
H20 H 0.2103 -0.1861 -0.0679 0.174 Uiso 1 1 calc R . .
C21 C 0.1210(9) -0.1111(9) -0.0745(4) 0.124(5) Uani 1 1 d . . .
H21 H 0.1369 -0.0760 -0.0508 0.149 Uiso 1 1 calc R . .
C22 C 0.0093(8) -0.0374(10) -0.0944(4) 0.134(5) Uani 1 1 d . . .
H22A H -0.0016 0.0002 -0.1185 0.201 Uiso 1 1 calc R . .
H22B H 0.0362 -0.0087 -0.0691 0.201 Uiso 1 1 calc R . .
H22C H -0.0340 -0.0578 -0.0895 0.201 Uiso 1 1 calc R . .
C23 C 0.1897(9) -0.2890(10) -0.1389(9) 0.190(10) Uani 1 1 d D . .
H23 H 0.2388 -0.2708 -0.1269 0.228 Uiso 1 1 calc R . .
C24 C 0.1755(12) -0.2891(14) -0.1869(9) 0.224(13) Uani 1 1 d . . .
H24A H 0.2131 -0.3178 -0.1948 0.336 Uiso 1 1 calc R . .
H24B H 0.1731 -0.2329 -0.1971 0.336 Uiso 1 1 calc R . .
H24C H 0.1312 -0.3166 -0.1995 0.336 Uiso 1 1 calc R . .
C25 C 0.1802(18) -0.3687(13) -0.1165(14) 0.35(2) Uani 1 1 d . . .
H25A H 0.1770 -0.4144 -0.1361 0.524 Uiso 1 1 calc R . .
H25B H 0.1374 -0.3656 -0.1073 0.524 Uiso 1 1 calc R . .
H25C H 0.2201 -0.3768 -0.0919 0.524 Uiso 1 1 calc R . .
C26 C 0.4571(6) -0.1108(9) -0.1374(3) 0.125(6) Uani 1 1 d . . .
C27 C 0.3957(7) -0.1586(8) -0.1435(3) 0.112(5) Uani 1 1 d . . .
H27 H 0.3827 -0.1790 -0.1197 0.135 Uiso 1 1 calc R . .
C28 C 0.3547(5) -0.1755(7) -0.1841(2) 0.086(3) Uani 1 1 d . . .
H28 H 0.3137 -0.2071 -0.1874 0.103 Uiso 1 1 calc R . .
C29 C 0.3723(5) -0.1470(6) -0.2209(2) 0.081(3) Uani 1 1 d . . .
C30 C 0.4323(5) -0.0987(8) -0.2146(3) 0.106(4) Uani 1 1 d . . .
H30 H 0.4456 -0.0773 -0.2381 0.127 Uiso 1 1 calc R . .
C31 C 0.4729(5) -0.0820(9) -0.1727(3) 0.117(5) Uani 1 1 d . . .
H31 H 0.5131 -0.0490 -0.1691 0.140 Uiso 1 1 calc R . .
C32 C 0.4995(7) -0.0881(11) -0.0927(3) 0.169(8) Uani 1 1 d . . .
H32A H 0.5167 -0.0323 -0.0927 0.254 Uiso 1 1 calc R . .
H32B H 0.5389 -0.1254 -0.0835 0.254 Uiso 1 1 calc R . .
H32C H 0.4699 -0.0920 -0.0733 0.254 Uiso 1 1 calc R . .
C33 C 0.3260(5) -0.1684(6) -0.2640(2) 0.079(2) Uani 1 1 d . . .
H33 H 0.2769 -0.1551 -0.2645 0.095 Uiso 1 1 calc R . .
C34 C 0.3310(5) -0.2598(6) -0.2705(3) 0.085(3) Uani 1 1 d . . .
H34A H 0.3794 -0.2746 -0.2680 0.127 Uiso 1 1 calc R . .
H34B H 0.3020 -0.2746 -0.2986 0.127 Uiso 1 1 calc R . .
H34C H 0.3146 -0.2888 -0.2489 0.127 Uiso 1 1 calc R . .
C35 C 0.3436(5) -0.1233(6) -0.3002(3) 0.083(2) Uani 1 1 d . . .
H35A H 0.3396 -0.0646 -0.2963 0.124 Uiso 1 1 calc R . .
H35B H 0.3114 -0.1398 -0.3270 0.124 Uiso 1 1 calc R . .
H35C H 0.3914 -0.1364 -0.3006 0.124 Uiso 1 1 calc R . .
C36 C 0.4247(5) 0.1260(6) -0.0207(2) 0.079(3) Uani 1 1 d . . .
C37 C 0.3901(5) 0.1884(6) -0.0039(2) 0.077(2) Uani 1 1 d . . .
H37 H 0.4032 0.2436 -0.0053 0.092 Uiso 1 1 calc R . .
C38 C 0.3367(5) 0.1683(6) 0.0148(2) 0.075(2) Uani 1 1 d . . .
H38 H 0.3137 0.2106 0.0255 0.090 Uiso 1 1 calc R . .
C39 C 0.3162(5) 0.0857(5) 0.0182(2) 0.076(3) Uani 1 1 d . . .
C40 C 0.3508(5) 0.0253(6) 0.0014(2) 0.079(3) Uani 1 1 d . . .
H40 H 0.3377 -0.0300 0.0028 0.095 Uiso 1 1 calc R . .
C41 C 0.4049(5) 0.0445(6) -0.0176(2) 0.083(3) Uani 1 1 d . . .
H41 H 0.4279 0.0022 -0.0283 0.099 Uiso 1 1 calc R . .
C42 C 0.4779(5) 0.1491(8) -0.0439(3) 0.098(3) Uani 1 1 d . . .
H42A H 0.5230 0.1586 -0.0234 0.148 Uiso 1 1 calc R . .
H42B H 0.4629 0.1987 -0.0603 0.148 Uiso 1 1 calc R . .
H42C H 0.4824 0.1048 -0.0629 0.148 Uiso 1 1 calc R . .
C43 C 0.2596(6) 0.0625(6) 0.0384(2) 0.083(3) Uani 1 1 d . . .
H43 H 0.2477 0.0041 0.0316 0.100 Uiso 1 1 calc R . .
C44 C 0.1942(6) 0.1120(7) 0.0220(3) 0.101(3) Uani 1 1 d . . .
H44A H 0.1578 0.0916 0.0343 0.152 Uiso 1 1 calc R . .
H44B H 0.1785 0.1074 -0.0089 0.152 Uiso 1 1 calc R . .
H44C H 0.2038 0.1692 0.0299 0.152 Uiso 1 1 calc R . .
C45 C 0.2853(7) 0.0701(7) 0.0851(3) 0.100(3) Uani 1 1 d . . .
H45A H 0.3228 0.0308 0.0959 0.150 Uiso 1 1 calc R . .
H45B H 0.2471 0.0593 0.0979 0.150 Uiso 1 1 calc R . .
H45C H 0.3030 0.1253 0.0925 0.150 Uiso 1 1 calc R . .
Cl5 Cl 0.4812(2) -0.3230(2) -0.08337(11) 0.1322(13) Uani 1 1 d . . .
Cl6 Cl 0.4909(3) -0.3798(3) -0.00111(10) 0.1451(15) Uani 1 1 d . . .
Cl7 Cl 0.3705(3) -0.4157(4) -0.06790(19) 0.198(3) Uani 1 1 d . . .
C46 C 0.4352(5) -0.3448(7) -0.0468(3) 0.084(2) Uani 1 1 d . . .
H46 H 0.4129 -0.2937 -0.0405 0.101 Uiso 1 1 calc R . .
O7 O 0.0000 -0.1825(7) -0.2500 0.169(8) Uani 1 2 d S . .
O8A O 0.4910(8) 0.1554(9) -0.2203(5) 0.107(5) Uani 0.50 1 d P A 1
O8B O 0.5104(14) 0.0555(15) -0.2138(10) 0.199(13) Uani 0.50 1 d P B 2
O9 O 0.2519(15) -0.1634(12) 0.0189(7) 0.168(9) Uani 0.50 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Ru1 O1 78.9(2) . . ?
O2 Ru1 N3 82.7(2) . . ?
O1 Ru1 N3 85.2(2) . . ?
O2 Ru1 C17 91.6(3) . . ?
O1 Ru1 C17 152.0(3) . . ?
N3 Ru1 C17 120.0(4) . . ?
O2 Ru1 C16 115.8(4) . . ?
O1 Ru1 C16 165.2(4) . . ?
N3 Ru1 C16 94.3(4) . . ?
C17 Ru1 C16 36.7(4) . . ?
O2 Ru1 C20 153.4(7) . . ?
O1 Ru1 C20 97.8(4) . . ?
N3 Ru1 C20 123.5(7) . . ?
C17 Ru1 C20 79.0(4) . . ?
C16 Ru1 C20 70.1(5) . . ?
O2 Ru1 C21 155.0(5) . . ?
O1 Ru1 C21 125.5(5) . . ?
N3 Ru1 C21 93.3(4) . . ?
C17 Ru1 C21 69.0(5) . . ?
C16 Ru1 C21 39.7(5) . . ?
C20 Ru1 C21 40.7(6) . . ?
O2 Ru1 C18 93.5(5) . . ?
O1 Ru1 C18 116.9(4) . . ?
N3 Ru1 C18 156.6(4) . . ?
C17 Ru1 C18 36.8(4) . . ?
C16 Ru1 C18 66.5(5) . . ?
C20 Ru1 C18 64.2(6) . . ?
C21 Ru1 C18 80.4(6) . . ?
O2 Ru1 C19 114.8(6) . . ?
O1 Ru1 C19 93.9(5) . . ?
N3 Ru1 C19 162.0(6) . . ?
C17 Ru1 C19 66.1(5) . . ?
C16 Ru1 C19 82.1(6) . . ?
C20 Ru1 C19 38.7(6) . . ?
C21 Ru1 C19 72.7(6) . . ?
C18 Ru1 C19 34.0(5) . . ?
O2 Ru1 Na1 117.89(19) . . ?
O1 Ru1 Na1 41.20(14) . . ?
N3 Ru1 Na1 78.51(16) . . ?
C17 Ru1 Na1 148.0(3) . . ?
C16 Ru1 Na1 124.2(4) . . ?
C20 Ru1 Na1 69.1(4) . . ?
C21 Ru1 Na1 85.0(4) . . ?
C18 Ru1 Na1 122.8(4) . . ?
C19 Ru1 Na1 88.9(5) . . ?
O4 Ru2 O3 78.8(2) . . ?
O4 Ru2 N1 83.8(3) . . ?
O3 Ru2 N1 86.4(2) . . ?
O4 Ru2 C31 95.2(5) . . ?
O3 Ru2 C31 116.4(3) . . ?
N1 Ru2 C31 156.6(3) . . ?
O4 Ru2 C28 157.6(3) . . ?
O3 Ru2 C28 123.2(3) . . ?
N1 Ru2 C28 92.8(3) . . ?
C31 Ru2 C28 79.2(5) . . ?
O4 Ru2 C30 94.7(4) . . ?
O3 Ru2 C30 153.9(3) . . ?
N1 Ru2 C30 118.3(3) . . ?
C31 Ru2 C30 38.4(3) . . ?
C28 Ru2 C30 67.4(4) . . ?
O4 Ru2 C27 156.8(4) . . ?
O3 Ru2 C27 96.0(3) . . ?
N1 Ru2 C27 118.7(4) . . ?
C31 Ru2 C27 66.7(6) . . ?
C28 Ru2 C27 37.3(3) . . ?
C30 Ru2 C27 80.1(5) . . ?
O4 Ru2 C26 119.3(5) . . ?
O3 Ru2 C26 92.8(3) . . ?
N1 Ru2 C26 156.3(5) . . ?
C31 Ru2 C26 36.5(5) . . ?
C28 Ru2 C26 67.9(5) . . ?
C30 Ru2 C26 68.2(4) . . ?
C27 Ru2 C26 37.9(5) . . ?
O4 Ru2 C29 119.9(3) . . ?
O3 Ru2 C29 161.0(3) . . ?
N1 Ru2 C29 92.2(3) . . ?
C31 Ru2 C29 68.0(4) . . ?
C28 Ru2 C29 37.9(3) . . ?
C30 Ru2 C29 37.3(4) . . ?
C27 Ru2 C29 68.2(3) . . ?
C26 Ru2 C29 80.9(3) . . ?
O4 Ru2 Na1 116.93(17) . . ?
O3 Ru2 Na1 39.99(17) . . ?
N1 Ru2 Na1 79.83(18) . . ?
C31 Ru2 Na1 120.5(3) . . ?
C28 Ru2 Na1 84.0(2) . . ?
C30 Ru2 Na1 145.9(4) . . ?
C27 Ru2 Na1 65.8(3) . . ?
C26 Ru2 Na1 84.4(4) . . ?
C29 Ru2 Na1 121.1(3) . . ?
O6 Ru3 O5 79.1(2) . . ?
O6 Ru3 N2 81.3(2) . . ?
O5 Ru3 N2 87.4(2) . . ?
O6 Ru3 C38 90.8(3) . . ?
O5 Ru3 C38 134.2(3) . . ?
N2 Ru3 C38 135.4(3) . . ?
O6 Ru3 C37 104.3(3) . . ?
O5 Ru3 C37 170.4(3) . . ?
N2 Ru3 C37 101.9(3) . . ?
C38 Ru3 C37 37.9(3) . . ?
O6 Ru3 C40 138.9(3) . . ?
O5 Ru3 C40 90.9(3) . . ?
N2 Ru3 C40 138.5(3) . . ?
C38 Ru3 C40 68.0(3) . . ?
C37 Ru3 C40 80.6(3) . . ?
O6 Ru3 C36 137.5(3) . . ?
O5 Ru3 C36 141.6(3) . . ?
N2 Ru3 C36 88.1(3) . . ?
C38 Ru3 C36 68.7(3) . . ?
C37 Ru3 C36 38.2(3) . . ?
C40 Ru3 C36 68.3(4) . . ?
O6 Ru3 C41 171.3(2) . . ?
O5 Ru3 C41 107.7(3) . . ?
N2 Ru3 C41 104.0(3) . . ?
C38 Ru3 C41 80.6(3) . . ?
C37 Ru3 C41 68.1(3) . . ?
C40 Ru3 C41 37.9(4) . . ?
C36 Ru3 C41 37.5(4) . . ?
O6 Ru3 C39 105.3(3) . . ?
O5 Ru3 C39 101.5(3) . . ?
N2 Ru3 C39 169.7(3) . . ?
C38 Ru3 C39 38.3(3) . . ?
C37 Ru3 C39 69.0(4) . . ?
C40 Ru3 C39 37.5(3) . . ?
C36 Ru3 C39 81.7(4) . . ?
C41 Ru3 C39 68.5(4) . . ?
O6 Ru3 Na1 116.28(14) . . ?
O5 Ru3 Na1 39.73(15) . . ?
N2 Ru3 Na1 80.25(19) . . ?
C38 Ru3 Na1 140.0(3) . . ?
C37 Ru3 Na1 139.1(2) . . ?
C40 Ru3 Na1 72.5(2) . . ?
C36 Ru3 Na1 102.0(2) . . ?
C41 Ru3 Na1 71.7(2) . . ?
C39 Ru3 Na1 103.2(2) . . ?
O5 Na1 O3 87.4(2) . . ?
O5 Na1 O1 90.8(2) . . ?
O3 Na1 O1 88.2(2) . . ?
O5 Na1 Cl4 120.96(18) . . ?
O3 Na1 Cl4 127.80(19) . . ?
O1 Na1 Cl4 129.3(2) . . ?
O5 Na1 Ru1 68.86(15) . . ?
O3 Na1 Ru1 116.73(16) . . ?
O1 Na1 Ru1 38.09(16) . . ?
Cl4 Na1 Ru1 114.35(13) . . ?
O5 Na1 Ru3 36.96(14) . . ?
O3 Na1 Ru3 68.34(16) . . ?
O1 Na1 Ru3 119.96(17) . . ?
Cl4 Na1 Ru3 107.30(10) . . ?
Ru1 Na1 Ru3 105.75(8) . . ?
O5 Na1 Ru2 116.83(17) . . ?
O3 Na1 Ru2 36.87(14) . . ?
O1 Na1 Ru2 67.51(17) . . ?
Cl4 Na1 Ru2 118.04(12) . . ?
Ru1 Na1 Ru2 105.26(7) . . ?
Ru3 Na1 Ru2 105.17(10) . . ?
C1 O1 Ru1 111.4(5) . . ?
C1 O1 Na1 132.1(5) . . ?
Ru1 O1 Na1 100.7(2) . . ?
C2 O2 Ru1 111.9(4) . . ?
C6 O3 Ru2 111.9(5) . . ?
C6 O3 Na1 135.6(5) . . ?
Ru2 O3 Na1 103.1(3) . . ?
C7 O4 Ru2 113.3(6) . . ?
C11 O5 Ru3 110.9(5) . . ?
C11 O5 Na1 130.9(4) . . ?
Ru3 O5 Na1 103.3(2) . . ?
C12 O6 Ru3 111.2(4) . . ?
C1 N1 C5 118.9(7) . . ?
C1 N1 Ru2 123.1(5) . . ?
C5 N1 Ru2 117.7(6) . . ?
C6 N2 C10 119.5(7) . . ?
C6 N2 Ru3 124.0(6) . . ?
C10 N2 Ru3 115.9(6) . . ?
C11 N3 C15 118.8(7) . . ?
C11 N3 Ru1 124.0(5) . . ?
C15 N3 Ru1 116.7(5) . . ?
O1 C1 N1 122.6(7) . . ?
O1 C1 C2 115.3(8) . . ?
N1 C1 C2 122.0(7) . . ?
O2 C2 C3 124.1(7) . . ?
O2 C2 C1 118.3(7) . . ?
C3 C2 C1 117.5(9) . . ?
C4 C3 C2 117.2(7) . . ?
C4 C3 H3 121.4 . . ?
C2 C3 H3 121.4 . . ?
C5 C4 C3 123.2(8) . . ?
C5 C4 Cl1 119.9(8) . . ?
C3 C4 Cl1 116.9(6) . . ?
C4 C5 N1 121.2(9) . . ?
C4 C5 H5 119.4 . . ?
N1 C5 H5 119.4 . . ?
O3 C6 N2 121.2(7) . . ?
O3 C6 C7 119.2(8) . . ?
N2 C6 C7 119.5(8) . . ?
O4 C7 C8 124.5(9) . . ?
O4 C7 C6 115.4(9) . . ?
C8 C7 C6 120.1(9) . . ?
C7 C8 C9 118.1(9) . . ?
C7 C8 H8 120.9 . . ?
C9 C8 H8 120.9 . . ?
C10 C9 C8 120.5(10) . . ?
C10 C9 Cl2 119.0(9) . . ?
C8 C9 Cl2 120.6(8) . . ?
C9 C10 N2 122.3(9) . . ?
C9 C10 H10 118.8 . . ?
N2 C10 H10 118.8 . . ?
O5 C11 N3 120.1(7) . . ?
O5 C11 C12 117.3(6) . . ?
N3 C11 C12 122.6(6) . . ?
O6 C12 C13 124.2(7) . . ?
O6 C12 C11 118.0(6) . . ?
C13 C12 C11 117.8(7) . . ?
C12 C13 C14 118.6(7) . . ?
C12 C13 H13 120.7 . . ?
C14 C13 H13 120.7 . . ?
C15 C14 C13 121.6(6) . . ?
C15 C14 Cl3 117.5(6) . . ?
C13 C14 Cl3 120.8(6) . . ?
N3 C15 C14 120.6(7) . . ?
N3 C15 H15 119.7 . . ?
C14 C15 H15 119.7 . . ?
C17 C16 C21 120.0(12) . . ?
C17 C16 C22 126.8(12) . . ?
C21 C16 C22 112.9(13) . . ?
C17 C16 Ru1 71.5(7) . . ?
C21 C16 Ru1 70.6(7) . . ?
C22 C16 Ru1 124.1(8) . . ?
C16 C17 C18 121.7(11) . . ?
C16 C17 Ru1 71.8(7) . . ?
C18 C17 Ru1 72.9(8) . . ?
C16 C17 H17 119.1 . . ?
C18 C17 H17 119.1 . . ?
Ru1 C17 H17 128.4 . . ?
C19 C18 C17 127.5(16) . . ?
C19 C18 Ru1 74.2(10) . . ?
C17 C18 Ru1 70.3(7) . . ?
C19 C18 H18 116.2 . . ?
C17 C18 H18 116.3 . . ?
Ru1 C18 H18 133.5 . . ?
C18 C19 C20 114.7(16) . . ?
C18 C19 C23 121.8(18) . . ?
C20 C19 C23 123.5(17) . . ?
C18 C19 Ru1 71.7(9) . . ?
C20 C19 Ru1 68.5(7) . . ?
C23 C19 Ru1 127.1(11) . . ?
C19 C20 C21 123.0(11) . . ?
C19 C20 Ru1 72.7(8) . . ?
C21 C20 Ru1 70.0(6) . . ?
C19 C20 H20 118.5 . . ?
C21 C20 H20 118.5 . . ?
Ru1 C20 H20 131.9 . . ?
C16 C21 C20 112.9(12) . . ?
C16 C21 Ru1 69.6(6) . . ?
C20 C21 Ru1 69.2(7) . . ?
C16 C21 H21 123.6 . . ?
C20 C21 H21 123.6 . . ?
Ru1 C21 H21 129.4 . . ?
C16 C22 H22A 109.5 . . ?
C16 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C16 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C24 C23 C25 119(3) . . ?
C24 C23 C19 111.9(16) . . ?
C25 C23 C19 103.3(17) . . ?
C24 C23 H23 107.4 . . ?
C25 C23 H23 107.4 . . ?
C19 C23 H23 107.4 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C23 C25 H25A 109.5 . . ?
C23 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C23 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C31 C26 C27 117.3(9) . . ?
C31 C26 C32 122.4(15) . . ?
C27 C26 C32 120.1(14) . . ?
C31 C26 Ru2 69.5(6) . . ?
C27 C26 Ru2 70.3(5) . . ?
C32 C26 Ru2 127.3(8) . . ?
C28 C27 C26 120.4(12) . . ?
C28 C27 Ru2 71.0(6) . . ?
C26 C27 Ru2 71.9(8) . . ?
C28 C27 H27 119.8 . . ?
C26 C27 H27 119.8 . . ?
Ru2 C27 H27 129.9 . . ?
C27 C28 C29 122.0(12) . . ?
C27 C28 Ru2 71.7(7) . . ?
C29 C28 Ru2 72.7(6) . . ?
C27 C28 H28 119.0 . . ?
C29 C28 H28 119.0 . . ?
Ru2 C28 H28 129.0 . . ?
C30 C29 C28 117.2(8) . . ?
C30 C29 C33 123.5(9) . . ?
C28 C29 C33 119.3(9) . . ?
C30 C29 Ru2 69.9(5) . . ?
C28 C29 Ru2 69.4(5) . . ?
C33 C29 Ru2 131.0(6) . . ?
C29 C30 C31 119.5(12) . . ?
C29 C30 Ru2 72.9(5) . . ?
C31 C30 Ru2 69.7(5) . . ?
C29 C30 H30 120.3 . . ?
C31 C30 H30 120.3 . . ?
Ru2 C30 H30 129.5 . . ?
C26 C31 C30 123.6(13) . . ?
C26 C31 Ru2 74.0(6) . . ?
C30 C31 Ru2 71.9(5) . . ?
C26 C31 H31 118.2 . . ?
C30 C31 H31 118.2 . . ?
Ru2 C31 H31 128.4 . . ?
C26 C32 H32A 109.5 . . ?
C26 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C26 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C29 C33 C35 114.0(9) . . ?
C29 C33 C34 108.3(7) . . ?
C35 C33 C34 109.6(7) . . ?
C29 C33 H33 108.3 . . ?
C35 C33 H33 108.3 . . ?
C34 C33 H33 108.3 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C41 C36 C37 118.8(10) . . ?
C41 C36 C42 121.5(9) . . ?
C37 C36 C42 119.5(10) . . ?
C41 C36 Ru3 71.3(5) . . ?
C37 C36 Ru3 70.2(5) . . ?
C42 C36 Ru3 126.7(6) . . ?
C38 C37 C36 120.2(9) . . ?
C38 C37 Ru3 70.6(5) . . ?
C36 C37 Ru3 71.6(5) . . ?
C38 C37 H37 119.9 . . ?
C36 C37 H37 119.9 . . ?
Ru3 C37 H37 130.5 . . ?
C37 C38 C39 121.6(8) . . ?
C37 C38 Ru3 71.5(4) . . ?
C39 C38 Ru3 72.4(4) . . ?
C37 C38 H38 119.2 . . ?
C39 C38 H38 119.2 . . ?
Ru3 C38 H38 129.3 . . ?
C40 C39 C38 117.3(9) . . ?
C40 C39 C43 120.0(9) . . ?
C38 C39 C43 122.7(8) . . ?
C40 C39 Ru3 70.4(5) . . ?
C38 C39 Ru3 69.3(4) . . ?
C43 C39 Ru3 131.1(6) . . ?
C39 C40 C41 121.9(9) . . ?
C39 C40 Ru3 72.2(5) . . ?
C41 C40 Ru3 71.6(5) . . ?
C39 C40 H40 119.1 . . ?
C41 C40 H40 119.1 . . ?
Ru3 C40 H40 129.9 . . ?
C36 C41 C40 120.2(8) . . ?
C36 C41 Ru3 71.2(5) . . ?
C40 C41 Ru3 70.5(5) . . ?
C36 C41 H41 119.9 . . ?
C40 C41 H41 119.9 . . ?
Ru3 C41 H41 131.2 . . ?
C36 C42 H42A 109.5 . . ?
C36 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C36 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C45 C43 C39 110.0(9) . . ?
C45 C43 C44 110.4(9) . . ?
C39 C43 C44 112.6(8) . . ?
C45 C43 H43 107.9 . . ?
C39 C43 H43 107.9 . . ?
C44 C43 H43 107.9 . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C43 C45 H45A 109.5 . . ?
C43 C45 H45B 109.5 . . ?
H45A C45 H45B 109.5 . . ?
C43 C45 H45C 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
Cl6 C46 Cl5 109.7(6) . . ?
Cl6 C46 Cl7 111.2(7) . . ?
Cl5 C46 Cl7 109.8(5) . . ?
Cl6 C46 H46 108.7 . . ?
Cl5 C46 H46 108.7 . . ?
Cl7 C46 H46 108.7 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 O2 2.049(6) . ?
Ru1 O1 2.100(6) . ?
Ru1 N3 2.151(6) . ?
Ru1 C17 2.154(11) . ?
Ru1 C16 2.159(12) . ?
Ru1 C20 2.161(10) . ?
Ru1 C21 2.172(12) . ?
Ru1 C18 2.188(14) . ?
Ru1 C19 2.218(14) . ?
Ru1 Na1 3.344(3) . ?
Ru2 O4 2.071(8) . ?
Ru2 O3 2.090(5) . ?
Ru2 N1 2.137(6) . ?
Ru2 C31 2.149(10) . ?
Ru2 C28 2.173(11) . ?
Ru2 C30 2.177(9) . ?
Ru2 C27 2.183(12) . ?
Ru2 C26 2.205(9) . ?
Ru2 C29 2.216(8) . ?
Ru2 Na1 3.393(3) . ?
Ru3 O6 2.064(5) . ?
Ru3 O5 2.093(5) . ?
Ru3 N2 2.152(6) . ?
Ru3 C38 2.158(7) . ?
Ru3 C37 2.171(8) . ?
Ru3 C40 2.177(8) . ?
Ru3 C36 2.190(9) . ?
Ru3 C41 2.191(8) . ?
Ru3 C39 2.200(8) . ?
Ru3 Na1 3.388(3) . ?
Cl1 C4 1.745(8) . ?
Cl2 C9 1.730(11) . ?
Cl3 C14 1.738(7) . ?
Cl4 Na1 2.566(4) . ?
Na1 O5 2.225(6) . ?
Na1 O3 2.239(7) . ?
Na1 O1 2.242(5) . ?
O1 C1 1.314(9) . ?
O2 C2 1.307(11) . ?
O3 C6 1.287(10) . ?
O4 C7 1.325(12) . ?
O5 C11 1.310(8) . ?
O6 C12 1.314(9) . ?
N1 C1 1.323(11) . ?
N1 C5 1.379(11) . ?
N2 C6 1.356(10) . ?
N2 C10 1.362(11) . ?
N3 C11 1.348(9) . ?
N3 C15 1.362(9) . ?
C1 C2 1.452(10) . ?
C2 C3 1.410(12) . ?
C3 C4 1.379(13) . ?
C3 H3 0.9500 . ?
C4 C5 1.340(12) . ?
C5 H5 0.9500 . ?
C6 C7 1.442(12) . ?
C7 C8 1.375(15) . ?
C8 C9 1.400(15) . ?
C8 H8 0.9500 . ?
C9 C10 1.360(13) . ?
C10 H10 0.9500 . ?
C11 C12 1.430(11) . ?
C12 C13 1.384(10) . ?
C13 C14 1.387(10) . ?
C13 H13 0.9500 . ?
C14 C15 1.381(11) . ?
C15 H15 0.9500 . ?
C16 C17 1.357(16) . ?
C16 C21 1.472(19) . ?
C16 C22 1.488(18) . ?
C17 C18 1.371(17) . ?
C17 H17 0.9500 . ?
C18 C19 1.29(2) . ?
C18 H18 0.9500 . ?
C19 C20 1.45(2) . ?
C19 C23 1.574(17) . ?
C20 C21 1.51(2) . ?
C20 H20 0.9500 . ?
C21 H21 0.9500 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C24 1.52(3) . ?
C23 C25 1.54(3) . ?
C23 H23 1.0000 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 C31 1.36(2) . ?
C26 C27 1.42(2) . ?
C26 C32 1.530(12) . ?
C27 C28 1.393(12) . ?
C27 H27 0.9500 . ?
C28 C29 1.426(13) . ?
C28 H28 0.9500 . ?
C29 C30 1.404(16) . ?
C29 C33 1.510(11) . ?
C30 C31 1.423(13) . ?
C30 H30 0.9500 . ?
C31 H31 0.9500 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C35 1.520(13) . ?
C33 C34 1.523(14) . ?
C33 H33 1.0000 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 C41 1.409(14) . ?
C36 C37 1.427(12) . ?
C36 C42 1.512(15) . ?
C37 C38 1.404(13) . ?
C37 H37 0.9500 . ?
C38 C39 1.431(13) . ?
C38 H38 0.9500 . ?
C39 C40 1.407(12) . ?
C39 C43 1.503(14) . ?
C40 C41 1.419(14) . ?
C40 H40 0.9500 . ?
C41 H41 0.9500 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C45 1.486(11) . ?
C43 C44 1.510(14) . ?
C43 H43 1.0000 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 H45C 0.9800 . ?
Cl5 C46 1.732(10) . ?
Cl6 C46 1.710(10) . ?
Cl7 C46 1.740(11) . ?
C46 H46 1.0000 . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
C46 H46 Cl4 1.00 2.32 3.312(11) 170.0 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O2 Ru1 Na1 O5 100.6(2) . . . . ?
O1 Ru1 Na1 O5 121.1(3) . . . . ?
N3 Ru1 Na1 O5 25.3(2) . . . . ?
C17 Ru1 Na1 O5 -104.3(6) . . . . ?
C16 Ru1 Na1 O5 -62.1(4) . . . . ?
C20 Ru1 Na1 O5 -107.7(7) . . . . ?
C21 Ru1 Na1 O5 -69.1(5) . . . . ?
C18 Ru1 Na1 O5 -144.3(5) . . . . ?
C19 Ru1 Na1 O5 -141.8(6) . . . . ?
O2 Ru1 Na1 O3 24.9(3) . . . . ?
O1 Ru1 Na1 O3 45.5(3) . . . . ?
N3 Ru1 Na1 O3 -50.3(2) . . . . ?
C17 Ru1 Na1 O3 -179.9(6) . . . . ?
C16 Ru1 Na1 O3 -137.7(4) . . . . ?
C20 Ru1 Na1 O3 176.7(8) . . . . ?
C21 Ru1 Na1 O3 -144.7(5) . . . . ?
C18 Ru1 Na1 O3 140.0(6) . . . . ?
C19 Ru1 Na1 O3 142.6(6) . . . . ?
O2 Ru1 Na1 O1 -20.5(3) . . . . ?
N3 Ru1 Na1 O1 -95.8(3) . . . . ?
C17 Ru1 Na1 O1 134.6(6) . . . . ?
C16 Ru1 Na1 O1 176.8(4) . . . . ?
C20 Ru1 Na1 O1 131.2(8) . . . . ?
C21 Ru1 Na1 O1 169.8(5) . . . . ?
C18 Ru1 Na1 O1 94.6(6) . . . . ?
C19 Ru1 Na1 O1 97.1(6) . . . . ?
O2 Ru1 Na1 Cl4 -143.9(2) . . . . ?
O1 Ru1 Na1 Cl4 -123.4(3) . . . . ?
N3 Ru1 Na1 Cl4 140.78(19) . . . . ?
C17 Ru1 Na1 Cl4 11.2(6) . . . . ?
C16 Ru1 Na1 Cl4 53.4(4) . . . . ?
C20 Ru1 Na1 Cl4 7.8(7) . . . . ?
C21 Ru1 Na1 Cl4 46.4(5) . . . . ?
C18 Ru1 Na1 Cl4 -28.8(5) . . . . ?
C19 Ru1 Na1 Cl4 -26.3(6) . . . . ?
O2 Ru1 Na1 Ru3 98.2(2) . . . . ?
O1 Ru1 Na1 Ru3 118.8(3) . . . . ?
N3 Ru1 Na1 Ru3 22.96(16) . . . . ?
C17 Ru1 Na1 Ru3 -106.6(6) . . . . ?
C16 Ru1 Na1 Ru3 -64.4(4) . . . . ?
C20 Ru1 Na1 Ru3 -110.0(7) . . . . ?
C21 Ru1 Na1 Ru3 -71.4(4) . . . . ?
C18 Ru1 Na1 Ru3 -146.7(5) . . . . ?
C19 Ru1 Na1 Ru3 -144.1(6) . . . . ?
O2 Ru1 Na1 Ru2 -12.8(2) . . . . ?
O1 Ru1 Na1 Ru2 7.8(2) . . . . ?
N3 Ru1 Na1 Ru2 -88.06(17) . . . . ?
C17 Ru1 Na1 Ru2 142.4(6) . . . . ?
C16 Ru1 Na1 Ru2 -175.5(4) . . . . ?
C20 Ru1 Na1 Ru2 139.0(7) . . . . ?
C21 Ru1 Na1 Ru2 177.6(4) . . . . ?
C18 Ru1 Na1 Ru2 102.3(5) . . . . ?
C19 Ru1 Na1 Ru2 104.9(6) . . . . ?
O6 Ru3 Na1 O5 -22.6(3) . . . . ?
N2 Ru3 Na1 O5 -97.7(3) . . . . ?
C38 Ru3 Na1 O5 105.3(4) . . . . ?
C37 Ru3 Na1 O5 165.2(5) . . . . ?
C40 Ru3 Na1 O5 113.9(4) . . . . ?
C36 Ru3 Na1 O5 176.4(3) . . . . ?
C41 Ru3 Na1 O5 153.9(4) . . . . ?
C39 Ru3 Na1 O5 92.2(3) . . . . ?
O6 Ru3 Na1 O3 94.0(2) . . . . ?
O5 Ru3 Na1 O3 116.6(3) . . . . ?
N2 Ru3 Na1 O3 18.9(2) . . . . ?
C38 Ru3 Na1 O3 -138.1(4) . . . . ?
C37 Ru3 Na1 O3 -78.2(4) . . . . ?
C40 Ru3 Na1 O3 -129.5(3) . . . . ?
C36 Ru3 Na1 O3 -67.0(3) . . . . ?
C41 Ru3 Na1 O3 -89.5(4) . . . . ?
C39 Ru3 Na1 O3 -151.2(3) . . . . ?
O6 Ru3 Na1 O1 19.6(3) . . . . ?
O5 Ru3 Na1 O1 42.2(3) . . . . ?
N2 Ru3 Na1 O1 -55.5(3) . . . . ?
C38 Ru3 Na1 O1 147.5(4) . . . . ?
C37 Ru3 Na1 O1 -152.5(5) . . . . ?
C40 Ru3 Na1 O1 156.2(4) . . . . ?
C36 Ru3 Na1 O1 -141.4(3) . . . . ?
C41 Ru3 Na1 O1 -163.9(4) . . . . ?
C39 Ru3 Na1 O1 134.4(3) . . . . ?
O6 Ru3 Na1 Cl4 -141.4(2) . . . . ?
O5 Ru3 Na1 Cl4 -118.8(3) . . . . ?
N2 Ru3 Na1 Cl4 143.4(2) . . . . ?
C38 Ru3 Na1 Cl4 -13.6(4) . . . . ?
C37 Ru3 Na1 Cl4 46.4(4) . . . . ?
C40 Ru3 Na1 Cl4 -4.9(3) . . . . ?
C36 Ru3 Na1 Cl4 57.5(3) . . . . ?
C41 Ru3 Na1 Cl4 35.0(3) . . . . ?
C39 Ru3 Na1 Cl4 -26.7(3) . . . . ?
O6 Ru3 Na1 Ru1 -19.0(2) . . . . ?
O5 Ru3 Na1 Ru1 3.6(2) . . . . ?
N2 Ru3 Na1 Ru1 -94.14(18) . . . . ?
C38 Ru3 Na1 Ru1 108.8(4) . . . . ?
C37 Ru3 Na1 Ru1 168.8(4) . . . . ?
C40 Ru3 Na1 Ru1 117.5(3) . . . . ?
C36 Ru3 Na1 Ru1 180.0(3) . . . . ?
C41 Ru3 Na1 Ru1 157.5(3) . . . . ?
C39 Ru3 Na1 Ru1 95.8(3) . . . . ?
O6 Ru3 Na1 Ru2 92.10(19) . . . . ?
O5 Ru3 Na1 Ru2 114.7(2) . . . . ?
N2 Ru3 Na1 Ru2 16.95(17) . . . . ?
C38 Ru3 Na1 Ru2 -140.1(4) . . . . ?
C37 Ru3 Na1 Ru2 -80.1(4) . . . . ?
C40 Ru3 Na1 Ru2 -131.4(3) . . . . ?
C36 Ru3 Na1 Ru2 -68.9(3) . . . . ?
C41 Ru3 Na1 Ru2 -91.5(3) . . . . ?
C39 Ru3 Na1 Ru2 -153.1(3) . . . . ?
O4 Ru2 Na1 O5 21.7(3) . . . . ?
O3 Ru2 Na1 O5 40.7(3) . . . . ?
N1 Ru2 Na1 O5 -55.9(3) . . . . ?
C31 Ru2 Na1 O5 136.5(5) . . . . ?
C28 Ru2 Na1 O5 -149.8(3) . . . . ?
C30 Ru2 Na1 O5 177.8(5) . . . . ?
C27 Ru2 Na1 O5 176.2(4) . . . . ?
C26 Ru2 Na1 O5 141.9(4) . . . . ?
C29 Ru2 Na1 O5 -142.2(3) . . . . ?
O4 Ru2 Na1 O3 -19.0(3) . . . . ?
N1 Ru2 Na1 O3 -96.6(3) . . . . ?
C31 Ru2 Na1 O3 95.7(5) . . . . ?
C28 Ru2 Na1 O3 169.4(3) . . . . ?
C30 Ru2 Na1 O3 137.0(5) . . . . ?
C27 Ru2 Na1 O3 135.5(4) . . . . ?
C26 Ru2 Na1 O3 101.1(4) . . . . ?
C29 Ru2 Na1 O3 177.0(3) . . . . ?
O4 Ru2 Na1 O1 100.6(2) . . . . ?
O3 Ru2 Na1 O1 119.6(3) . . . . ?
N1 Ru2 Na1 O1 23.0(3) . . . . ?
C31 Ru2 Na1 O1 -144.7(5) . . . . ?
C28 Ru2 Na1 O1 -71.0(3) . . . . ?
C30 Ru2 Na1 O1 -103.4(5) . . . . ?
C27 Ru2 Na1 O1 -104.9(4) . . . . ?
C26 Ru2 Na1 O1 -139.3(4) . . . . ?
C29 Ru2 Na1 O1 -63.4(3) . . . . ?
O4 Ru2 Na1 Cl4 -135.6(2) . . . . ?
O3 Ru2 Na1 Cl4 -116.6(3) . . . . ?
N1 Ru2 Na1 Cl4 146.8(2) . . . . ?
C31 Ru2 Na1 Cl4 -20.8(5) . . . . ?
C28 Ru2 Na1 Cl4 52.8(3) . . . . ?
C30 Ru2 Na1 Cl4 20.4(5) . . . . ?
C27 Ru2 Na1 Cl4 18.9(4) . . . . ?
C26 Ru2 Na1 Cl4 -15.4(4) . . . . ?
C29 Ru2 Na1 Cl4 60.5(3) . . . . ?
O4 Ru2 Na1 Ru1 95.4(2) . . . . ?
O3 Ru2 Na1 Ru1 114.4(2) . . . . ?
N1 Ru2 Na1 Ru1 17.8(2) . . . . ?
C31 Ru2 Na1 Ru1 -149.8(4) . . . . ?
C28 Ru2 Na1 Ru1 -76.2(2) . . . . ?
C30 Ru2 Na1 Ru1 -108.6(5) . . . . ?
C27 Ru2 Na1 Ru1 -110.1(4) . . . . ?
C26 Ru2 Na1 Ru1 -144.4(4) . . . . ?
C29 Ru2 Na1 Ru1 -68.6(3) . . . . ?
O4 Ru2 Na1 Ru3 -16.0(2) . . . . ?
O3 Ru2 Na1 Ru3 3.0(2) . . . . ?
N1 Ru2 Na1 Ru3 -93.6(2) . . . . ?
C31 Ru2 Na1 Ru3 98.7(4) . . . . ?
C28 Ru2 Na1 Ru3 172.4(2) . . . . ?
C30 Ru2 Na1 Ru3 140.0(5) . . . . ?
C27 Ru2 Na1 Ru3 138.4(4) . . . . ?
C26 Ru2 Na1 Ru3 104.1(4) . . . . ?
C29 Ru2 Na1 Ru3 -180.0(2) . . . . ?
O2 Ru1 O1 C1 17.9(5) . . . . ?
N3 Ru1 O1 C1 -65.6(5) . . . . ?
C17 Ru1 O1 C1 89.9(8) . . . . ?
C16 Ru1 O1 C1 -154.2(13) . . . . ?
C20 Ru1 O1 C1 171.1(8) . . . . ?
C21 Ru1 O1 C1 -156.2(7) . . . . ?
C18 Ru1 O1 C1 106.2(7) . . . . ?
C19 Ru1 O1 C1 132.4(7) . . . . ?
Na1 Ru1 O1 C1 -143.7(6) . . . . ?
O2 Ru1 O1 Na1 161.6(3) . . . . ?
N3 Ru1 O1 Na1 78.1(2) . . . . ?
C17 Ru1 O1 Na1 -126.4(6) . . . . ?
C16 Ru1 O1 Na1 -10.5(14) . . . . ?
C20 Ru1 O1 Na1 -45.1(7) . . . . ?
C21 Ru1 O1 Na1 -12.5(6) . . . . ?
C18 Ru1 O1 Na1 -110.1(5) . . . . ?
C19 Ru1 O1 Na1 -83.9(6) . . . . ?
O5 Na1 O1 C1 79.1(6) . . . . ?
O3 Na1 O1 C1 -8.4(6) . . . . ?
Cl4 Na1 O1 C1 -148.4(6) . . . . ?
Ru1 Na1 O1 C1 132.1(7) . . . . ?
Ru3 Na1 O1 C1 55.2(7) . . . . ?
Ru2 Na1 O1 C1 -39.8(6) . . . . ?
O5 Na1 O1 Ru1 -53.0(2) . . . . ?
O3 Na1 O1 Ru1 -140.4(2) . . . . ?
Cl4 Na1 O1 Ru1 79.5(3) . . . . ?
Ru3 Na1 O1 Ru1 -76.8(3) . . . . ?
Ru2 Na1 O1 Ru1 -171.9(2) . . . . ?
O1 Ru1 O2 C2 -16.7(5) . . . . ?
N3 Ru1 O2 C2 69.7(5) . . . . ?
C17 Ru1 O2 C2 -170.2(6) . . . . ?
C16 Ru1 O2 C2 161.0(6) . . . . ?
C20 Ru1 O2 C2 -102.0(10) . . . . ?
C21 Ru1 O2 C2 151.7(10) . . . . ?
C18 Ru1 O2 C2 -133.5(6) . . . . ?
C19 Ru1 O2 C2 -105.9(7) . . . . ?
Na1 Ru1 O2 C2 -3.1(6) . . . . ?
O4 Ru2 O3 C6 10.6(5) . . . . ?
N1 Ru2 O3 C6 -73.7(5) . . . . ?
C31 Ru2 O3 C6 100.9(7) . . . . ?
C28 Ru2 O3 C6 -164.8(5) . . . . ?
C30 Ru2 O3 C6 88.2(10) . . . . ?
C27 Ru2 O3 C6 167.8(6) . . . . ?
C26 Ru2 O3 C6 129.9(7) . . . . ?
C29 Ru2 O3 C6 -160.0(8) . . . . ?
Na1 Ru2 O3 C6 -152.2(6) . . . . ?
O4 Ru2 O3 Na1 162.8(3) . . . . ?
N1 Ru2 O3 Na1 78.4(3) . . . . ?
C31 Ru2 O3 Na1 -106.9(5) . . . . ?
C28 Ru2 O3 Na1 -12.6(4) . . . . ?
C30 Ru2 O3 Na1 -119.6(9) . . . . ?
C27 Ru2 O3 Na1 -40.0(4) . . . . ?
C26 Ru2 O3 Na1 -77.9(5) . . . . ?
C29 Ru2 O3 Na1 -7.8(8) . . . . ?
O5 Na1 O3 C6 -2.6(6) . . . . ?
O1 Na1 O3 C6 88.2(6) . . . . ?
Cl4 Na1 O3 C6 -130.7(6) . . . . ?
Ru1 Na1 O3 C6 62.1(6) . . . . ?
Ru3 Na1 O3 C6 -35.2(6) . . . . ?
Ru2 Na1 O3 C6 141.7(7) . . . . ?
O5 Na1 O3 Ru2 -144.4(2) . . . . ?
O1 Na1 O3 Ru2 -53.5(2) . . . . ?
Cl4 Na1 O3 Ru2 87.5(2) . . . . ?
Ru1 Na1 O3 Ru2 -79.6(2) . . . . ?
Ru3 Na1 O3 Ru2 -176.9(2) . . . . ?
O3 Ru2 O4 C7 -9.0(5) . . . . ?
N1 Ru2 O4 C7 78.5(6) . . . . ?
C31 Ru2 O4 C7 -125.0(6) . . . . ?
C28 Ru2 O4 C7 160.8(8) . . . . ?
C30 Ru2 O4 C7 -163.5(6) . . . . ?
C27 Ru2 O4 C7 -87.8(9) . . . . ?
C26 Ru2 O4 C7 -96.0(6) . . . . ?
C29 Ru2 O4 C7 167.5(5) . . . . ?
Na1 Ru2 O4 C7 3.3(6) . . . . ?
O6 Ru3 O5 C11 15.3(4) . . . . ?
N2 Ru3 O5 C11 -66.3(5) . . . . ?
C38 Ru3 O5 C11 95.6(5) . . . . ?
C37 Ru3 O5 C11 127.3(16) . . . . ?
C40 Ru3 O5 C11 155.1(5) . . . . ?
C36 Ru3 O5 C11 -149.9(5) . . . . ?
C41 Ru3 O5 C11 -170.2(5) . . . . ?
C39 Ru3 O5 C11 118.9(5) . . . . ?
Na1 Ru3 O5 C11 -144.2(5) . . . . ?
O6 Ru3 O5 Na1 159.5(2) . . . . ?
N2 Ru3 O5 Na1 77.9(3) . . . . ?
C38 Ru3 O5 Na1 -120.2(4) . . . . ?
C37 Ru3 O5 Na1 -88.5(16) . . . . ?
C40 Ru3 O5 Na1 -60.7(3) . . . . ?
C36 Ru3 O5 Na1 -5.7(5) . . . . ?
C41 Ru3 O5 Na1 -26.0(4) . . . . ?
C39 Ru3 O5 Na1 -96.9(3) . . . . ?
O3 Na1 O5 C11 77.4(7) . . . . ?
O1 Na1 O5 C11 -10.7(7) . . . . ?
Cl4 Na1 O5 C11 -149.1(6) . . . . ?
Ru1 Na1 O5 C11 -42.6(6) . . . . ?
Ru3 Na1 O5 C11 133.7(7) . . . . ?
Ru2 Na1 O5 C11 54.3(7) . . . . ?
O3 Na1 O5 Ru3 -56.3(2) . . . . ?
O1 Na1 O5 Ru3 -144.4(2) . . . . ?
Cl4 Na1 O5 Ru3 77.2(3) . . . . ?
Ru1 Na1 O5 Ru3 -176.3(2) . . . . ?
Ru2 Na1 O5 Ru3 -79.4(2) . . . . ?
O5 Ru3 O6 C12 -16.1(5) . . . . ?
N2 Ru3 O6 C12 72.9(5) . . . . ?
C38 Ru3 O6 C12 -151.2(5) . . . . ?
C37 Ru3 O6 C12 173.1(5) . . . . ?
C40 Ru3 O6 C12 -94.9(6) . . . . ?
C36 Ru3 O6 C12 150.3(5) . . . . ?
C41 Ru3 O6 C12 -159(2) . . . . ?
C39 Ru3 O6 C12 -115.2(5) . . . . ?
Na1 Ru3 O6 C12 -1.7(5) . . . . ?
O4 Ru2 N1 C1 -142.3(6) . . . . ?
O3 Ru2 N1 C1 -63.2(6) . . . . ?
C31 Ru2 N1 C1 129.0(12) . . . . ?
C28 Ru2 N1 C1 59.9(6) . . . . ?
C30 Ru2 N1 C1 125.8(7) . . . . ?
C27 Ru2 N1 C1 31.6(7) . . . . ?
C26 Ru2 N1 C1 25.6(11) . . . . ?
C29 Ru2 N1 C1 97.9(7) . . . . ?
Na1 Ru2 N1 C1 -23.4(6) . . . . ?
O4 Ru2 N1 C5 44.5(6) . . . . ?
O3 Ru2 N1 C5 123.5(6) . . . . ?
C31 Ru2 N1 C5 -44.3(15) . . . . ?
C28 Ru2 N1 C5 -113.4(6) . . . . ?
C30 Ru2 N1 C5 -47.5(8) . . . . ?
C27 Ru2 N1 C5 -141.6(6) . . . . ?
C26 Ru2 N1 C5 -147.7(8) . . . . ?
C29 Ru2 N1 C5 -75.4(7) . . . . ?
Na1 Ru2 N1 C5 163.3(6) . . . . ?
O6 Ru3 N2 C6 -138.0(6) . . . . ?
O5 Ru3 N2 C6 -58.6(6) . . . . ?
C38 Ru3 N2 C6 139.8(6) . . . . ?
C37 Ru3 N2 C6 119.1(6) . . . . ?
C40 Ru3 N2 C6 29.8(8) . . . . ?
C36 Ru3 N2 C6 83.2(6) . . . . ?
C41 Ru3 N2 C6 49.0(6) . . . . ?
C39 Ru3 N2 C6 91.4(16) . . . . ?
Na1 Ru3 N2 C6 -19.3(5) . . . . ?
O6 Ru3 N2 C10 50.4(5) . . . . ?
O5 Ru3 N2 C10 129.8(5) . . . . ?
C38 Ru3 N2 C10 -31.8(7) . . . . ?
C37 Ru3 N2 C10 -52.5(6) . . . . ?
C40 Ru3 N2 C10 -141.7(6) . . . . ?
C36 Ru3 N2 C10 -88.3(6) . . . . ?
C41 Ru3 N2 C10 -122.6(6) . . . . ?
C39 Ru3 N2 C10 -80.2(17) . . . . ?
Na1 Ru3 N2 C10 169.1(5) . . . . ?
O2 Ru1 N3 C11 -147.6(6) . . . . ?
O1 Ru1 N3 C11 -68.3(6) . . . . ?
C17 Ru1 N3 C11 124.7(6) . . . . ?
C16 Ru1 N3 C11 96.9(6) . . . . ?
C20 Ru1 N3 C11 27.9(8) . . . . ?
C21 Ru1 N3 C11 57.1(7) . . . . ?
C18 Ru1 N3 C11 130.4(12) . . . . ?
C19 Ru1 N3 C11 19.4(18) . . . . ?
Na1 Ru1 N3 C11 -27.2(5) . . . . ?
O2 Ru1 N3 C15 40.5(5) . . . . ?
O1 Ru1 N3 C15 119.8(5) . . . . ?
C17 Ru1 N3 C15 -47.2(6) . . . . ?
C16 Ru1 N3 C15 -75.0(6) . . . . ?
C20 Ru1 N3 C15 -144.0(6) . . . . ?
C21 Ru1 N3 C15 -114.8(7) . . . . ?
C18 Ru1 N3 C15 -41.5(13) . . . . ?
C19 Ru1 N3 C15 -152.5(16) . . . . ?
Na1 Ru1 N3 C15 160.9(5) . . . . ?
Ru1 O1 C1 N1 165.9(6) . . . . ?
Na1 O1 C1 N1 37.5(10) . . . . ?
Ru1 O1 C1 C2 -16.0(8) . . . . ?
Na1 O1 C1 C2 -144.5(6) . . . . ?
C5 N1 C1 O1 179.2(7) . . . . ?
Ru2 N1 C1 O1 5.9(10) . . . . ?
C5 N1 C1 C2 1.2(11) . . . . ?
Ru2 N1 C1 C2 -172.0(5) . . . . ?
Ru1 O2 C2 C3 -165.1(6) . . . . ?
Ru1 O2 C2 C1 13.8(8) . . . . ?
O1 C1 C2 O2 1.9(10) . . . . ?
N1 C1 C2 O2 179.9(7) . . . . ?
O1 C1 C2 C3 -179.2(7) . . . . ?
N1 C1 C2 C3 -1.1(11) . . . . ?
O2 C2 C3 C4 180.0(8) . . . . ?
C1 C2 C3 C4 1.1(11) . . . . ?
C2 C3 C4 C5 -1.3(13) . . . . ?
C2 C3 C4 Cl1 179.9(6) . . . . ?
C3 C4 C5 N1 1.5(14) . . . . ?
Cl1 C4 C5 N1 -179.8(6) . . . . ?
C1 N1 C5 C4 -1.4(12) . . . . ?
Ru2 N1 C5 C4 172.2(7) . . . . ?
Ru2 O3 C6 N2 172.5(5) . . . . ?
Na1 O3 C6 N2 33.0(10) . . . . ?
Ru2 O3 C6 C7 -10.9(8) . . . . ?
Na1 O3 C6 C7 -150.4(6) . . . . ?
C10 N2 C6 O3 175.9(7) . . . . ?
Ru3 N2 C6 O3 4.6(10) . . . . ?
C10 N2 C6 C7 -0.7(10) . . . . ?
Ru3 N2 C6 C7 -172.0(5) . . . . ?
Ru2 O4 C7 C8 -175.6(7) . . . . ?
Ru2 O4 C7 C6 6.3(9) . . . . ?
O3 C6 C7 O4 3.3(11) . . . . ?
N2 C6 C7 O4 180.0(7) . . . . ?
O3 C6 C7 C8 -174.9(7) . . . . ?
N2 C6 C7 C8 1.8(11) . . . . ?
O4 C7 C8 C9 -179.5(8) . . . . ?
C6 C7 C8 C9 -1.4(12) . . . . ?
C7 C8 C9 C10 0.1(13) . . . . ?
C7 C8 C9 Cl2 179.9(6) . . . . ?
C8 C9 C10 N2 1.0(13) . . . . ?
Cl2 C9 C10 N2 -178.8(6) . . . . ?
C6 N2 C10 C9 -0.6(11) . . . . ?
Ru3 N2 C10 C9 171.4(6) . . . . ?
Ru3 O5 C11 N3 168.8(5) . . . . ?
Na1 O5 C11 N3 37.7(10) . . . . ?
Ru3 O5 C11 C12 -12.3(8) . . . . ?
Na1 O5 C11 C12 -143.4(5) . . . . ?
C15 N3 C11 O5 -179.2(6) . . . . ?
Ru1 N3 C11 O5 9.0(9) . . . . ?
C15 N3 C11 C12 1.9(10) . . . . ?
Ru1 N3 C11 C12 -169.8(5) . . . . ?
Ru3 O6 C12 C13 -166.9(6) . . . . ?
Ru3 O6 C12 C11 15.0(8) . . . . ?
O5 C11 C12 O6 -1.8(10) . . . . ?
N3 C11 C12 O6 177.1(7) . . . . ?
O5 C11 C12 C13 -180.0(6) . . . . ?
N3 C11 C12 C13 -1.1(11) . . . . ?
O6 C12 C13 C14 -179.3(7) . . . . ?
C11 C12 C13 C14 -1.3(10) . . . . ?
C12 C13 C14 C15 2.8(11) . . . . ?
C12 C13 C14 Cl3 -178.7(6) . . . . ?
C11 N3 C15 C14 -0.3(11) . . . . ?
Ru1 N3 C15 C14 172.0(6) . . . . ?
C13 C14 C15 N3 -2.1(12) . . . . ?
Cl3 C14 C15 N3 179.4(6) . . . . ?
O2 Ru1 C16 C17 53.5(7) . . . . ?
O1 Ru1 C16 C17 -135.1(13) . . . . ?
N3 Ru1 C16 C17 137.5(6) . . . . ?
C20 Ru1 C16 C17 -98.3(9) . . . . ?
C21 Ru1 C16 C17 -132.6(11) . . . . ?
C18 Ru1 C16 C17 -28.7(7) . . . . ?
C19 Ru1 C16 C17 -60.2(8) . . . . ?
Na1 Ru1 C16 C17 -143.4(6) . . . . ?
O2 Ru1 C16 C21 -173.9(7) . . . . ?
O1 Ru1 C16 C21 -2.5(18) . . . . ?
N3 Ru1 C16 C21 -89.9(8) . . . . ?
C17 Ru1 C16 C21 132.6(11) . . . . ?
C20 Ru1 C16 C21 34.3(8) . . . . ?
C18 Ru1 C16 C21 103.9(9) . . . . ?
C19 Ru1 C16 C21 72.4(8) . . . . ?
Na1 Ru1 C16 C21 -10.9(9) . . . . ?
O2 Ru1 C16 C22 -68.9(12) . . . . ?
O1 Ru1 C16 C22 102.5(14) . . . . ?
N3 Ru1 C16 C22 15.1(12) . . . . ?
C17 Ru1 C16 C22 -122.4(14) . . . . ?
C20 Ru1 C16 C22 139.3(14) . . . . ?
C21 Ru1 C16 C22 105.0(15) . . . . ?
C18 Ru1 C16 C22 -151.1(13) . . . . ?
C19 Ru1 C16 C22 177.4(13) . . . . ?
Na1 Ru1 C16 C22 94.2(11) . . . . ?
C21 C16 C17 C18 2.3(17) . . . . ?
C22 C16 C17 C18 174.8(12) . . . . ?
Ru1 C16 C17 C18 55.6(11) . . . . ?
C21 C16 C17 Ru1 -53.3(9) . . . . ?
C22 C16 C17 Ru1 119.2(12) . . . . ?
O2 Ru1 C17 C16 -133.6(6) . . . . ?
O1 Ru1 C17 C16 157.4(6) . . . . ?
N3 Ru1 C17 C16 -51.0(7) . . . . ?
C20 Ru1 C17 C16 71.5(9) . . . . ?
C21 Ru1 C17 C16 30.3(7) . . . . ?
C18 Ru1 C17 C16 132.8(11) . . . . ?
C19 Ru1 C17 C16 110.0(9) . . . . ?
Na1 Ru1 C17 C16 68.2(9) . . . . ?
O2 Ru1 C17 C18 93.7(8) . . . . ?
O1 Ru1 C17 C18 24.7(12) . . . . ?
N3 Ru1 C17 C18 176.2(8) . . . . ?
C16 Ru1 C17 C18 -132.8(11) . . . . ?
C20 Ru1 C17 C18 -61.3(10) . . . . ?
C21 Ru1 C17 C18 -102.5(10) . . . . ?
C19 Ru1 C17 C18 -22.8(10) . . . . ?
Na1 Ru1 C17 C18 -64.5(11) . . . . ?
C16 C17 C18 C19 -5(2) . . . . ?
Ru1 C17 C18 C19 50.3(16) . . . . ?
C16 C17 C18 Ru1 -55.1(11) . . . . ?
O2 Ru1 C18 C19 131.3(12) . . . . ?
O1 Ru1 C18 C19 52.0(13) . . . . ?
N3 Ru1 C18 C19 -149.0(12) . . . . ?
C17 Ru1 C18 C19 -140.7(16) . . . . ?
C16 Ru1 C18 C19 -112.1(13) . . . . ?
C20 Ru1 C18 C19 -33.7(12) . . . . ?
C21 Ru1 C18 C19 -73.1(12) . . . . ?
Na1 Ru1 C18 C19 4.6(14) . . . . ?
O2 Ru1 C18 C17 -88.1(8) . . . . ?
O1 Ru1 C18 C17 -167.3(6) . . . . ?
N3 Ru1 C18 C17 -8.3(17) . . . . ?
C16 Ru1 C18 C17 28.6(7) . . . . ?
C20 Ru1 C18 C17 107.0(10) . . . . ?
C21 Ru1 C18 C17 67.6(9) . . . . ?
C19 Ru1 C18 C17 140.7(16) . . . . ?
Na1 Ru1 C18 C17 145.3(6) . . . . ?
C17 C18 C19 C20 6(2) . . . . ?
Ru1 C18 C19 C20 54.8(12) . . . . ?
C17 C18 C19 C23 -171.7(14) . . . . ?
Ru1 C18 C19 C23 -122.9(15) . . . . ?
C17 C18 C19 Ru1 -48.8(15) . . . . ?
O2 Ru1 C19 C18 -55.7(13) . . . . ?
O1 Ru1 C19 C18 -135.2(11) . . . . ?
N3 Ru1 C19 C18 138.5(13) . . . . ?
C17 Ru1 C19 C18 24.5(10) . . . . ?
C16 Ru1 C19 C18 59.1(12) . . . . ?
C20 Ru1 C19 C18 127.1(16) . . . . ?
C21 Ru1 C19 C18 98.7(12) . . . . ?
Na1 Ru1 C19 C18 -176.1(12) . . . . ?
O2 Ru1 C19 C20 177.2(7) . . . . ?
O1 Ru1 C19 C20 97.7(9) . . . . ?
N3 Ru1 C19 C20 11(2) . . . . ?
C17 Ru1 C19 C20 -102.5(10) . . . . ?
C16 Ru1 C19 C20 -68.0(9) . . . . ?
C21 Ru1 C19 C20 -28.4(8) . . . . ?
C18 Ru1 C19 C20 -127.1(16) . . . . ?
Na1 Ru1 C19 C20 56.8(8) . . . . ?
O2 Ru1 C19 C23 60.7(19) . . . . ?
O1 Ru1 C19 C23 -18.8(18) . . . . ?
N3 Ru1 C19 C23 -105(2) . . . . ?
C17 Ru1 C19 C23 141.0(19) . . . . ?
C16 Ru1 C19 C23 175.5(18) . . . . ?
C20 Ru1 C19 C23 -116(2) . . . . ?
C21 Ru1 C19 C23 -144.8(19) . . . . ?
C18 Ru1 C19 C23 116(2) . . . . ?
Na1 Ru1 C19 C23 -59.7(18) . . . . ?
C18 C19 C20 C21 -5(2) . . . . ?
C23 C19 C20 C21 172.3(12) . . . . ?
Ru1 C19 C20 C21 51.2(11) . . . . ?
C18 C19 C20 Ru1 -56.5(13) . . . . ?
C23 C19 C20 Ru1 121.2(15) . . . . ?
O2 Ru1 C20 C19 -5.6(15) . . . . ?
O1 Ru1 C20 C19 -86.4(9) . . . . ?
N3 Ru1 C20 C19 -175.8(8) . . . . ?
C17 Ru1 C20 C19 65.4(9) . . . . ?
C16 Ru1 C20 C19 102.5(9) . . . . ?
C21 Ru1 C20 C19 136.0(12) . . . . ?
C18 Ru1 C20 C19 29.7(9) . . . . ?
Na1 Ru1 C20 C19 -116.4(10) . . . . ?
O2 Ru1 C20 C21 -141.6(10) . . . . ?
O1 Ru1 C20 C21 137.6(7) . . . . ?
N3 Ru1 C20 C21 48.3(8) . . . . ?
C17 Ru1 C20 C21 -70.5(8) . . . . ?
C16 Ru1 C20 C21 -33.5(7) . . . . ?
C18 Ru1 C20 C21 -106.2(9) . . . . ?
C19 Ru1 C20 C21 -136.0(12) . . . . ?
Na1 Ru1 C20 C21 107.6(10) . . . . ?
C17 C16 C21 C20 -1.8(14) . . . . ?
C22 C16 C21 C20 -175.3(10) . . . . ?
Ru1 C16 C21 C20 -55.5(8) . . . . ?
C17 C16 C21 Ru1 53.7(9) . . . . ?
C22 C16 C21 Ru1 -119.8(9) . . . . ?
C19 C20 C21 C16 3.4(17) . . . . ?
Ru1 C20 C21 C16 55.7(8) . . . . ?
C19 C20 C21 Ru1 -52.3(12) . . . . ?
O2 Ru1 C21 C16 13.1(14) . . . . ?
O1 Ru1 C21 C16 179.2(6) . . . . ?
N3 Ru1 C21 C16 92.8(7) . . . . ?
C17 Ru1 C21 C16 -28.1(7) . . . . ?
C20 Ru1 C21 C16 -125.7(11) . . . . ?
C18 Ru1 C21 C16 -64.5(7) . . . . ?
C19 Ru1 C21 C16 -98.6(8) . . . . ?
Na1 Ru1 C21 C16 171.0(7) . . . . ?
O2 Ru1 C21 C20 138.8(11) . . . . ?
O1 Ru1 C21 C20 -55.1(9) . . . . ?
N3 Ru1 C21 C20 -141.5(8) . . . . ?
C17 Ru1 C21 C20 97.6(9) . . . . ?
C16 Ru1 C21 C20 125.7(11) . . . . ?
C18 Ru1 C21 C20 61.2(8) . . . . ?
C19 Ru1 C21 C20 27.1(8) . . . . ?
Na1 Ru1 C21 C20 -63.3(8) . . . . ?
C18 C19 C23 C24 37(2) . . . . ?
C20 C19 C23 C24 -140.6(19) . . . . ?
Ru1 C19 C23 C24 -54(3) . . . . ?
C18 C19 C23 C25 -92(3) . . . . ?
C20 C19 C23 C25 90(2) . . . . ?
Ru1 C19 C23 C25 178(2) . . . . ?
O4 Ru2 C26 C31 -54.3(8) . . . . ?
O3 Ru2 C26 C31 -133.0(8) . . . . ?
N1 Ru2 C26 C31 139.5(9) . . . . ?
C28 Ru2 C26 C31 102.1(8) . . . . ?
C30 Ru2 C26 C31 28.6(8) . . . . ?
C27 Ru2 C26 C31 130.9(10) . . . . ?
C29 Ru2 C26 C31 65.0(8) . . . . ?
Na1 Ru2 C26 C31 -172.2(8) . . . . ?
O4 Ru2 C26 C27 174.8(5) . . . . ?
O3 Ru2 C26 C27 96.1(6) . . . . ?
N1 Ru2 C26 C27 8.6(11) . . . . ?
C31 Ru2 C26 C27 -130.9(10) . . . . ?
C28 Ru2 C26 C27 -28.8(5) . . . . ?
C30 Ru2 C26 C27 -102.3(7) . . . . ?
C29 Ru2 C26 C27 -65.9(6) . . . . ?
Na1 Ru2 C26 C27 56.9(5) . . . . ?
O4 Ru2 C26 C32 61.5(17) . . . . ?
O3 Ru2 C26 C32 -17.2(16) . . . . ?
N1 Ru2 C26 C32 -104.7(16) . . . . ?
C31 Ru2 C26 C32 116(2) . . . . ?
C28 Ru2 C26 C32 -142.1(17) . . . . ?
C30 Ru2 C26 C32 144.4(17) . . . . ?
C27 Ru2 C26 C32 -113.3(18) . . . . ?
C29 Ru2 C26 C32 -179.2(16) . . . . ?
Na1 Ru2 C26 C32 -56.4(15) . . . . ?
C31 C26 C27 C28 1.0(15) . . . . ?
C32 C26 C27 C28 176.2(9) . . . . ?
Ru2 C26 C27 C28 53.8(8) . . . . ?
C31 C26 C27 Ru2 -52.9(9) . . . . ?
C32 C26 C27 Ru2 122.4(10) . . . . ?
O4 Ru2 C27 C28 -144.2(7) . . . . ?
O3 Ru2 C27 C28 140.5(6) . . . . ?
N1 Ru2 C27 C28 51.3(7) . . . . ?
C31 Ru2 C27 C28 -103.3(7) . . . . ?
C30 Ru2 C27 C28 -65.6(6) . . . . ?
C26 Ru2 C27 C28 -132.6(9) . . . . ?
C29 Ru2 C27 C28 -28.7(6) . . . . ?
Na1 Ru2 C27 C28 113.5(7) . . . . ?
O4 Ru2 C27 C26 -11.6(11) . . . . ?
O3 Ru2 C27 C26 -86.9(6) . . . . ?
N1 Ru2 C27 C26 -176.1(5) . . . . ?
C31 Ru2 C27 C26 29.3(5) . . . . ?
C28 Ru2 C27 C26 132.6(9) . . . . ?
C30 Ru2 C27 C26 67.0(6) . . . . ?
C29 Ru2 C27 C26 103.8(6) . . . . ?
Na1 Ru2 C27 C26 -113.9(6) . . . . ?
C26 C27 C28 C29 0.6(14) . . . . ?
Ru2 C27 C28 C29 54.9(8) . . . . ?
C26 C27 C28 Ru2 -54.3(9) . . . . ?
O4 Ru2 C28 C27 142.8(8) . . . . ?
O3 Ru2 C28 C27 -49.1(8) . . . . ?
N1 Ru2 C28 C27 -136.7(7) . . . . ?
C31 Ru2 C28 C27 65.5(7) . . . . ?
C30 Ru2 C28 C27 103.8(7) . . . . ?
C26 Ru2 C28 C27 29.2(7) . . . . ?
C29 Ru2 C28 C27 133.4(9) . . . . ?
Na1 Ru2 C28 C27 -57.2(7) . . . . ?
O4 Ru2 C28 C29 9.4(11) . . . . ?
O3 Ru2 C28 C29 177.5(4) . . . . ?
N1 Ru2 C28 C29 89.9(5) . . . . ?
C31 Ru2 C28 C29 -67.9(5) . . . . ?
C30 Ru2 C28 C29 -29.6(5) . . . . ?
C27 Ru2 C28 C29 -133.4(9) . . . . ?
C26 Ru2 C28 C29 -104.2(6) . . . . ?
Na1 Ru2 C28 C29 169.4(5) . . . . ?
C27 C28 C29 C30 -1.7(13) . . . . ?
Ru2 C28 C29 C30 52.7(8) . . . . ?
C27 C28 C29 C33 179.2(8) . . . . ?
Ru2 C28 C29 C33 -126.3(8) . . . . ?
C27 C28 C29 Ru2 -54.4(8) . . . . ?
O4 Ru2 C29 C30 53.0(7) . . . . ?
O3 Ru2 C29 C30 -137.6(8) . . . . ?
N1 Ru2 C29 C30 137.1(6) . . . . ?
C31 Ru2 C29 C30 -30.1(7) . . . . ?
C28 Ru2 C29 C30 -131.1(8) . . . . ?
C27 Ru2 C29 C30 -102.8(7) . . . . ?
C26 Ru2 C29 C30 -65.6(8) . . . . ?
Na1 Ru2 C29 C30 -143.4(6) . . . . ?
O4 Ru2 C29 C28 -175.9(5) . . . . ?
O3 Ru2 C29 C28 -6.5(10) . . . . ?
N1 Ru2 C29 C28 -91.8(5) . . . . ?
C31 Ru2 C29 C28 101.0(7) . . . . ?
C30 Ru2 C29 C28 131.1(8) . . . . ?
C27 Ru2 C29 C28 28.3(6) . . . . ?
C26 Ru2 C29 C28 65.4(7) . . . . ?
Na1 Ru2 C29 C28 -12.4(6) . . . . ?
O4 Ru2 C29 C33 -64.4(10) . . . . ?
O3 Ru2 C29 C33 105.0(11) . . . . ?
N1 Ru2 C29 C33 19.7(10) . . . . ?
C31 Ru2 C29 C33 -147.6(11) . . . . ?
C28 Ru2 C29 C33 111.5(12) . . . . ?
C30 Ru2 C29 C33 -117.5(13) . . . . ?
C27 Ru2 C29 C33 139.8(11) . . . . ?
C26 Ru2 C29 C33 176.9(11) . . . . ?
Na1 Ru2 C29 C33 99.1(9) . . . . ?
C28 C29 C30 C31 1.3(14) . . . . ?
C33 C29 C30 C31 -179.7(9) . . . . ?
Ru2 C29 C30 C31 53.8(9) . . . . ?
C28 C29 C30 Ru2 -52.5(7) . . . . ?
C33 C29 C30 Ru2 126.5(8) . . . . ?
O4 Ru2 C30 C29 -136.0(6) . . . . ?
O3 Ru2 C30 C29 150.1(7) . . . . ?
N1 Ru2 C30 C29 -50.5(8) . . . . ?
C31 Ru2 C30 C29 131.5(12) . . . . ?
C28 Ru2 C30 C29 30.1(5) . . . . ?
C27 Ru2 C30 C29 66.8(7) . . . . ?
C26 Ru2 C30 C29 104.3(8) . . . . ?
Na1 Ru2 C30 C29 65.3(7) . . . . ?
O4 Ru2 C30 C31 92.5(9) . . . . ?
O3 Ru2 C30 C31 18.5(15) . . . . ?
N1 Ru2 C30 C31 177.9(8) . . . . ?
C28 Ru2 C30 C31 -101.4(9) . . . . ?
C27 Ru2 C30 C31 -64.7(9) . . . . ?
C26 Ru2 C30 C31 -27.2(9) . . . . ?
C29 Ru2 C30 C31 -131.5(12) . . . . ?
Na1 Ru2 C30 C31 -66.2(11) . . . . ?
C27 C26 C31 C30 -1.4(17) . . . . ?
C32 C26 C31 C30 -176.5(11) . . . . ?
Ru2 C26 C31 C30 -54.6(10) . . . . ?
C27 C26 C31 Ru2 53.2(9) . . . . ?
C32 C26 C31 Ru2 -121.9(10) . . . . ?
C29 C30 C31 C26 0.3(17) . . . . ?
Ru2 C30 C31 C26 55.6(10) . . . . ?
C29 C30 C31 Ru2 -55.3(9) . . . . ?
O4 Ru2 C31 C26 134.7(8) . . . . ?
O3 Ru2 C31 C26 54.6(9) . . . . ?
N1 Ru2 C31 C26 -139.0(10) . . . . ?
C28 Ru2 C31 C26 -67.2(8) . . . . ?
C30 Ru2 C31 C26 -134.4(13) . . . . ?
C27 Ru2 C31 C26 -30.3(7) . . . . ?
C29 Ru2 C31 C26 -105.1(9) . . . . ?
Na1 Ru2 C31 C26 9.1(9) . . . . ?
O4 Ru2 C31 C30 -91.0(9) . . . . ?
O3 Ru2 C31 C30 -171.0(7) . . . . ?
N1 Ru2 C31 C30 -4.6(18) . . . . ?
C28 Ru2 C31 C30 67.1(8) . . . . ?
C27 Ru2 C31 C30 104.0(9) . . . . ?
C26 Ru2 C31 C30 134.4(13) . . . . ?
C29 Ru2 C31 C30 29.3(8) . . . . ?
Na1 Ru2 C31 C30 143.4(7) . . . . ?
C30 C29 C33 C35 -8.5(13) . . . . ?
C28 C29 C33 C35 170.5(8) . . . . ?
Ru2 C29 C33 C35 83.2(11) . . . . ?
C30 C29 C33 C34 113.8(11) . . . . ?
C28 C29 C33 C34 -67.2(10) . . . . ?
Ru2 C29 C33 C34 -154.5(8) . . . . ?
O6 Ru3 C36 C41 168.9(5) . . . . ?
O5 Ru3 C36 C41 -32.9(8) . . . . ?
N2 Ru3 C36 C41 -116.3(5) . . . . ?
C38 Ru3 C36 C41 102.7(6) . . . . ?
C37 Ru3 C36 C41 131.5(8) . . . . ?
C40 Ru3 C36 C41 28.8(5) . . . . ?
C39 Ru3 C36 C41 65.2(6) . . . . ?
Na1 Ru3 C36 C41 -36.7(5) . . . . ?
O6 Ru3 C36 C37 37.4(7) . . . . ?
O5 Ru3 C36 C37 -164.5(5) . . . . ?
N2 Ru3 C36 C37 112.2(6) . . . . ?
C38 Ru3 C36 C37 -28.9(6) . . . . ?
C40 Ru3 C36 C37 -102.7(6) . . . . ?
C41 Ru3 C36 C37 -131.5(8) . . . . ?
C39 Ru3 C36 C37 -66.3(6) . . . . ?
Na1 Ru3 C36 C37 -168.2(5) . . . . ?
O6 Ru3 C36 C42 -75.3(9) . . . . ?
O5 Ru3 C36 C42 82.9(10) . . . . ?
N2 Ru3 C36 C42 -0.4(9) . . . . ?
C38 Ru3 C36 C42 -141.5(10) . . . . ?
C37 Ru3 C36 C42 -112.6(11) . . . . ?
C40 Ru3 C36 C42 144.6(10) . . . . ?
C41 Ru3 C36 C42 115.8(11) . . . . ?
C39 Ru3 C36 C42 -179.0(9) . . . . ?
Na1 Ru3 C36 C42 79.2(9) . . . . ?
C41 C36 C37 C38 -0.8(10) . . . . ?
C42 C36 C37 C38 175.0(7) . . . . ?
Ru3 C36 C37 C38 53.2(6) . . . . ?
C41 C36 C37 Ru3 -54.0(6) . . . . ?
C42 C36 C37 Ru3 121.8(7) . . . . ?
O6 Ru3 C37 C38 72.2(5) . . . . ?
O5 Ru3 C37 C38 -37.8(18) . . . . ?
N2 Ru3 C37 C38 156.2(5) . . . . ?
C40 Ru3 C37 C38 -66.0(6) . . . . ?
C36 Ru3 C37 C38 -132.8(8) . . . . ?
C41 Ru3 C37 C38 -103.4(6) . . . . ?
C39 Ru3 C37 C38 -29.0(5) . . . . ?
Na1 Ru3 C37 C38 -115.0(5) . . . . ?
O6 Ru3 C37 C36 -155.0(5) . . . . ?
O5 Ru3 C37 C36 95.0(17) . . . . ?
N2 Ru3 C37 C36 -71.0(6) . . . . ?
C38 Ru3 C37 C36 132.8(8) . . . . ?
C40 Ru3 C37 C36 66.8(6) . . . . ?
C41 Ru3 C37 C36 29.4(6) . . . . ?
C39 Ru3 C37 C36 103.8(6) . . . . ?
Na1 Ru3 C37 C36 17.8(8) . . . . ?
C36 C37 C38 C39 1.0(11) . . . . ?
Ru3 C37 C38 C39 54.6(6) . . . . ?
C36 C37 C38 Ru3 -53.7(6) . . . . ?
O6 Ru3 C38 C37 -112.7(5) . . . . ?
O5 Ru3 C38 C37 171.8(4) . . . . ?
N2 Ru3 C38 C37 -34.3(7) . . . . ?
C40 Ru3 C38 C37 103.5(6) . . . . ?
C36 Ru3 C38 C37 29.1(5) . . . . ?
C41 Ru3 C38 C37 66.2(6) . . . . ?
C39 Ru3 C38 C37 133.2(8) . . . . ?
Na1 Ru3 C38 C37 112.4(5) . . . . ?
O6 Ru3 C38 C39 114.1(5) . . . . ?
O5 Ru3 C38 C39 38.6(7) . . . . ?
N2 Ru3 C38 C39 -167.5(5) . . . . ?
C37 Ru3 C38 C39 -133.2(8) . . . . ?
C40 Ru3 C38 C39 -29.7(6) . . . . ?
C36 Ru3 C38 C39 -104.1(6) . . . . ?
C41 Ru3 C38 C39 -67.0(6) . . . . ?
Na1 Ru3 C38 C39 -20.8(7) . . . . ?
C37 C38 C39 C40 -1.1(10) . . . . ?
Ru3 C38 C39 C40 53.2(6) . . . . ?
C37 C38 C39 C43 179.4(7) . . . . ?
Ru3 C38 C39 C43 -126.3(7) . . . . ?
C37 C38 C39 Ru3 -54.2(6) . . . . ?
O6 Ru3 C39 C40 157.9(6) . . . . ?
O5 Ru3 C39 C40 76.2(6) . . . . ?
N2 Ru3 C39 C40 -73.2(17) . . . . ?
C38 Ru3 C39 C40 -131.0(9) . . . . ?
C37 Ru3 C39 C40 -102.3(6) . . . . ?
C36 Ru3 C39 C40 -64.9(6) . . . . ?
C41 Ru3 C39 C40 -28.5(6) . . . . ?
Na1 Ru3 C39 C40 35.5(6) . . . . ?
O6 Ru3 C39 C38 -71.1(5) . . . . ?
O5 Ru3 C39 C38 -152.9(5) . . . . ?
N2 Ru3 C39 C38 57.8(17) . . . . ?
C37 Ru3 C39 C38 28.6(5) . . . . ?
C40 Ru3 C39 C38 131.0(9) . . . . ?
C36 Ru3 C39 C38 66.0(6) . . . . ?
C41 Ru3 C39 C38 102.5(6) . . . . ?
Na1 Ru3 C39 C38 166.5(5) . . . . ?
O6 Ru3 C39 C43 44.7(8) . . . . ?
O5 Ru3 C39 C43 -37.0(8) . . . . ?
N2 Ru3 C39 C43 173.6(13) . . . . ?
C38 Ru3 C39 C43 115.9(10) . . . . ?
C37 Ru3 C39 C43 144.5(9) . . . . ?
C40 Ru3 C39 C43 -113.2(11) . . . . ?
C36 Ru3 C39 C43 -178.1(8) . . . . ?
C41 Ru3 C39 C43 -141.7(9) . . . . ?
Na1 Ru3 C39 C43 -77.7(8) . . . . ?
C38 C39 C40 C41 1.1(10) . . . . ?
C43 C39 C40 C41 -179.4(7) . . . . ?
Ru3 C39 C40 C41 53.7(6) . . . . ?
C38 C39 C40 Ru3 -52.6(6) . . . . ?
C43 C39 C40 Ru3 126.9(7) . . . . ?
O6 Ru3 C40 C39 -33.5(8) . . . . ?
O5 Ru3 C40 C39 -107.9(6) . . . . ?
N2 Ru3 C40 C39 165.0(5) . . . . ?
C38 Ru3 C40 C39 30.3(6) . . . . ?
C37 Ru3 C40 C39 67.6(6) . . . . ?
C36 Ru3 C40 C39 105.3(6) . . . . ?
C41 Ru3 C40 C39 133.8(8) . . . . ?
Na1 Ru3 C40 C39 -143.6(6) . . . . ?
O6 Ru3 C40 C41 -167.3(4) . . . . ?
O5 Ru3 C40 C41 118.3(5) . . . . ?
N2 Ru3 C40 C41 31.2(7) . . . . ?
C38 Ru3 C40 C41 -103.5(6) . . . . ?
C37 Ru3 C40 C41 -66.3(5) . . . . ?
C36 Ru3 C40 C41 -28.5(5) . . . . ?
C39 Ru3 C40 C41 -133.8(8) . . . . ?
Na1 Ru3 C40 C41 82.5(5) . . . . ?
C37 C36 C41 C40 0.8(10) . . . . ?
C42 C36 C41 C40 -174.9(7) . . . . ?
Ru3 C36 C41 C40 -52.7(6) . . . . ?
C37 C36 C41 Ru3 53.5(6) . . . . ?
C42 C36 C41 Ru3 -122.2(7) . . . . ?
C39 C40 C41 C36 -1.0(11) . . . . ?
Ru3 C40 C41 C36 53.0(6) . . . . ?
C39 C40 C41 Ru3 -54.0(6) . . . . ?
O6 Ru3 C41 C36 -60(3) . . . . ?
O5 Ru3 C41 C36 159.2(5) . . . . ?
N2 Ru3 C41 C36 67.5(5) . . . . ?
C38 Ru3 C41 C36 -67.2(6) . . . . ?
C37 Ru3 C41 C36 -29.9(5) . . . . ?
C40 Ru3 C41 C36 -133.2(7) . . . . ?
C39 Ru3 C41 C36 -105.0(6) . . . . ?
Na1 Ru3 C41 C36 142.1(6) . . . . ?
O6 Ru3 C41 C40 74(3) . . . . ?
O5 Ru3 C41 C40 -67.6(5) . . . . ?
N2 Ru3 C41 C40 -159.3(5) . . . . ?
C38 Ru3 C41 C40 66.0(5) . . . . ?
C37 Ru3 C41 C40 103.3(6) . . . . ?
C36 Ru3 C41 C40 133.2(7) . . . . ?
C39 Ru3 C41 C40 28.2(5) . . . . ?
Na1 Ru3 C41 C40 -84.8(5) . . . . ?
C40 C39 C43 C45 106.0(9) . . . . ?
C38 C39 C43 C45 -74.5(10) . . . . ?
Ru3 C39 C43 C45 -164.6(7) . . . . ?
C40 C39 C43 C44 -130.4(8) . . . . ?
C38 C39 C43 C44 49.1(11) . . . . ?
Ru3 C39 C43 C44 -41.0(11) . . . . ?
