#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/44/4314443.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4314443
loop_
_publ_author_name
'Hari Pada Nayek'
'Werner Massa'
'Stefanie Dehnen'
_publ_contact_author
;
Dehnen, S.

Fachbereich Chemie der Philipps-Universitaet
Hans-Meerwein-Str.
D-35043 Marburg, Germany
;
_publ_contact_author_email       dehnen@chemie.uni-marburg.de
_publ_contact_author_fax         +6421-2825653
_publ_contact_author_phone       +6421-2825751
_publ_section_title
;
 Presence or Absence of a Central Se Atom in Silver Selenide/Selenolate
 Clusters with Halite Topology: Syntheses and Properties of
 [(Ph3PAg)8Ag6(μ6-Se)1-x/2(SePh)12]x+ (x= 0, 1)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              144
_journal_page_last               149
_journal_paper_doi               10.1021/ic901629k
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety
'C216 H180 Ag14 P8 Se12.5, C18 H33 Cl2 Sn, 5(C4 H8 O)'
_chemical_formula_sum            'C254 H253 Ag14 Cl2 O5 P8 Se12.5 Sn'
_chemical_formula_weight         6320.09
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           148
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            6
_cell_length_a                   20.3517(4)
_cell_length_b                   20.3517(4)
_cell_length_c                   99.087(3)
_cell_measurement_reflns_used    27007
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      23.82
_cell_measurement_theta_min      1.225
_cell_volume                     35542.6(15)
_computing_cell_refinement       'XAREA 1.43 (Stoe 2007)'
_computing_data_collection       'XAREA 1.43 (Stoe 2007)'
_computing_data_reduction        'XAREA 1.43 (Stoe 2007)'
_computing_molecular_graphics    'DIAMOND 3.1f (Brandenburg 2007)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR 2004 (Burla et al. 2004)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 6.7
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'IPDS-II (Stoe)'
_diffrn_measurement_method       omega-scans
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1371
_diffrn_reflns_av_sigmaI/netI    0.2491
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       109
_diffrn_reflns_limit_l_min       -121
_diffrn_reflns_number            59101
_diffrn_reflns_theta_full        25.94
_diffrn_reflns_theta_max         25.94
_diffrn_reflns_theta_min         1.23
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.283
_exptl_absorpt_correction_T_max  0.821
_exptl_absorpt_correction_T_min  0.627
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details   'Coppens et al. (1965)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.772
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             18624
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.305
_refine_diff_density_min         -1.228
_refine_diff_density_rms         0.181
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.978
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     632
_refine_ls_number_reflns         15185
_refine_ls_number_restraints     62
_refine_ls_restrained_S_all      0.981
_refine_ls_R_factor_all          0.1930
_refine_ls_R_factor_gt           0.0956
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2247
_refine_ls_wR_factor_ref         0.2484
_reflns_number_gt                6064
_reflns_number_total             15185
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic901629k_si_004.cif
_cod_data_source_block           2b
_cod_original_cell_volume        35542.5(15)
_cod_original_sg_symbol_H-M      'R -3'
_cod_original_formula_sum        'C254 H253 Ag14 Cl2 O5 P8 Se12.50 Sn'
_cod_database_code               4314443
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.44064(7) 0.15379(7) 0.847797(14) 0.0367(3) Uani 1 1 d . . .
Ag2 Ag 0.6667 0.3333 0.87504(2) 0.0349(7) Uani 0.9536(18) 3 d SP . .
Ag2A Ag 0.6667 0.3333 0.8805(7) 0.0349(7) Uani 0.0464(18) 3 d SP . .
Ag3 Ag 0.53379(7) 0.20280(7) 0.821146(14) 0.0376(4) Uani 0.9536(18) 1 d P . .
Ag3A Ag 0.6249(16) 0.2167(15) 0.8533(3) 0.0376(4) Uani 0.0464(18) 1 d P . .
Ag4 Ag 0.0000 0.0000 0.95802(2) 0.0455(6) Uani 1 3 d S . .
Ag5 Ag -0.12827(9) 0.11655(9) 1.013700(16) 0.0605(5) Uani 1 1 d . . .
Ag6 Ag -0.04550(15) 0.07321(13) 0.98171(2) 0.0539(6) Uani 0.6684(18) 1 d P . .
Ag6A Ag -0.0961(3) 0.0456(3) 0.98825(5) 0.0539(6) Uani 0.3316(18) 1 d P . .
Se1 Se 0.40921(10) 0.24993(10) 0.834517(18) 0.0338(4) Uani 0.9536(18) 1 d P . .
Se1A Se 0.460(2) 0.283(2) 0.8423(4) 0.0338(4) Uani 0.0464(18) 1 d P . .
Se2 Se 0.56988(10) 0.20592(10) 0.861638(18) 0.0344(5) Uani 0.9536(18) 1 d P . .
Se2A Se 0.533(2) 0.213(2) 0.8713(4) 0.0344(5) Uani 0.0464(18) 1 d P . .
Se3 Se 0.6667 0.3333 0.8333 0.042(2) Uani 0.50 6 d SP . .
Se4 Se -0.1768(2) 0.02122(19) 0.99211(3) 0.0534(8) Uani 0.6684(18) 1 d PD . .
Se4A Se -0.2282(4) 0.0016(4) 0.99725(6) 0.0534(8) Uani 0.3316(18) 1 d P . .
Se5 Se 0.09516(17) -0.05727(18) 0.96497(3) 0.0502(8) Uani 0.6684(18) 1 d P . .
Se5A Se 0.1067(3) -0.0101(4) 0.97113(7) 0.0502(8) Uani 0.3316(18) 1 d P . .
Se6 Se 0.0000 0.0000 1.0000 0.0271(17) Uani 0.50 6 d SP . .
P1 P 0.3163(2) 0.0513(2) 0.85592(5) 0.0371(11) Uani 1 1 d . . .
P2 P 0.2075(4) -0.1692(4) 0.97901(8) 0.0786(19) Uani 1 1 d . . .
P3 P 0.0000 0.0000 0.93286(8) 0.0370(19) Uani 1 3 d S . .
P4 P 0.6667 0.3333 0.89967(8) 0.0365(19) Uani 1 3 d S . .
Sn1 Sn 0.3333 0.6667 0.89923(2) 0.0417(5) Uani 1 3 d S . .
Cl1 Cl 0.3333 0.6667 0.87334(9) 0.058(2) Uani 1 3 d S . .
Cl2 Cl 0.356(3) 0.662(4) 0.9271(4) 0.24(3) Uani 0.33 1 d PU . .
C31 C 0.0120(9) -0.0811(9) 0.92541(17) 0.043(5) Uani 1 1 d . . .
C32 C 0.0488(12) -0.0696(11) 0.91365(19) 0.057(6) Uani 1 1 d . . .
H32A H 0.0692 -0.0218 0.9093 0.069 Uiso 1 1 calc R . .
C33 C 0.0572(13) -0.1256(14) 0.9080(2) 0.069(6) Uani 1 1 d . . .
H33A H 0.0847 -0.1180 0.8998 0.083 Uiso 1 1 calc R . .
C34 C 0.0224(12) -0.1965(13) 0.9149(2) 0.060(6) Uani 1 1 d . . .
H34A H 0.0257 -0.2380 0.9113 0.072 Uiso 1 1 calc R . .
C35 C -0.0157(13) -0.2048(13) 0.9267(2) 0.072(7) Uani 1 1 d . . .
H35A H -0.0395 -0.2526 0.9312 0.087 Uiso 1 1 calc R . .
C36 C -0.0201(11) -0.1447(12) 0.9324(2) 0.064(6) Uani 1 1 d . . .
H36A H -0.0448 -0.1491 0.9408 0.077 Uiso 1 1 calc R . .
C41 C 0.5660(8) 0.2965(9) 0.9068(2) 0.047(5) Uani 1 1 d . . .
C42 C 0.5217(12) 0.3180(17) 0.8993(3) 0.116(11) Uani 1 1 d U . .
H42A H 0.5387 0.3506 0.8917 0.139 Uiso 1 1 calc R . .
C43 C 0.453(2) 0.287(2) 0.9044(5) 0.166(15) Uani 1 1 d U . .
H43A H 0.4148 0.2896 0.8994 0.199 Uiso 1 1 calc R . .
C44 C 0.432(2) 0.245(2) 0.9183(5) 0.151(14) Uani 1 1 d U . .
H44A H 0.3849 0.2320 0.9225 0.181 Uiso 1 1 calc R . .
C45 C 0.4775(16) 0.230(2) 0.9236(3) 0.126(13) Uani 1 1 d . . .
H45A H 0.4651 0.2029 0.9318 0.151 Uiso 1 1 calc R . .
C46 C 0.5450(11) 0.2532(13) 0.9176(2) 0.076(7) Uani 1 1 d . . .
H46A H 0.5782 0.2376 0.9213 0.092 Uiso 1 1 calc R . .
C51 C 0.3357(9) 0.2564(9) 0.84648(19) 0.037(4) Uani 1 1 d . . .
C52 C 0.2641(12) 0.2265(10) 0.84208(19) 0.048(5) Uani 1 1 d . . .
H52A H 0.2494 0.2023 0.8335 0.058 Uiso 1 1 calc R . .
C53 C 0.2114(12) 0.2319(12) 0.8504(2) 0.058(6) Uani 1 1 d . . .
H53A H 0.1603 0.2114 0.8475 0.069 Uiso 1 1 calc R . .
C54 C 0.2323(15) 0.2653(13) 0.8622(3) 0.073(7) Uani 1 1 d . . .
H54A H 0.1958 0.2689 0.8676 0.087 Uiso 1 1 calc R . .
C55 C 0.3049(15) 0.2951(16) 0.8669(2) 0.092(9) Uani 1 1 d . . .
H55A H 0.3186 0.3197 0.8755 0.111 Uiso 1 1 calc R . .
C56 C 0.3558(11) 0.2891(12) 0.8595(2) 0.064(6) Uani 1 1 d . . .
H56A H 0.4055 0.3067 0.8629 0.076 Uiso 1 1 calc R . .
C61 C 0.5314(9) 0.1216(9) 0.8741(2) 0.043(5) Uani 1 1 d . . .
C62 C 0.5509(11) 0.0637(12) 0.8727(3) 0.073(7) Uani 1 1 d . . .
H62A H 0.5825 0.0649 0.8656 0.087 Uiso 1 1 calc R . .
C63 C 0.5229(12) 0.0058(12) 0.8821(2) 0.064(6) Uani 1 1 d . . .
H63A H 0.5315 -0.0356 0.8808 0.077 Uiso 1 1 calc R . .
C64 C 0.4822(13) 0.0061(14) 0.8934(3) 0.075(7) Uani 1 1 d . . .
H64A H 0.4671 -0.0324 0.9001 0.089 Uiso 1 1 calc R . .
C65 C 0.4633(14) 0.0648(12) 0.8950(2) 0.076(7) Uani 1 1 d . . .
H65A H 0.4328 0.0642 0.9023 0.091 Uiso 1 1 calc R . .
C66 C 0.4925(12) 0.1246(11) 0.8851(2) 0.063(6) Uani 1 1 d . . .
H66A H 0.4846 0.1665 0.8862 0.075 Uiso 1 1 calc R . .
C71 C -0.236(3) 0.047(4) 0.9809(3) 0.258(13) Uiso 1 1 d GD . .
C72 C -0.1961(17) 0.122(3) 0.9764(5) 0.309(15) Uiso 1 1 d G . .
H72A H -0.1436 0.1520 0.9784 0.371 Uiso 1 1 calc R . .
C73 C -0.233(4) 0.152(2) 0.9689(5) 0.361(18) Uiso 1 1 d G . .
H73A H -0.2051 0.2026 0.9657 0.433 Uiso 1 1 calc R . .
C74 C -0.309(4) 0.107(4) 0.9659(4) 0.41(2) Uiso 1 1 d G . .
H74A H -0.3344 0.1278 0.9608 0.495 Uiso 1 1 calc R . .
C75 C -0.3497(17) 0.033(4) 0.9705(4) 0.361(18) Uiso 1 1 d G . .
H75A H -0.4022 0.0023 0.9685 0.433 Uiso 1 1 calc R . .
C76 C -0.313(3) 0.003(2) 0.9780(4) 0.309(15) Uiso 1 1 d G . .
H76A H -0.3408 -0.0482 0.9811 0.371 Uiso 1 1 calc R . .
C81 C 0.1815(10) -0.0524(9) 0.9416(2) 0.108(4) Uiso 1 1 d G . .
C82 C 0.2450(11) -0.0160(13) 0.93338(18) 0.129(5) Uiso 1 1 d G . .
H82A H 0.2509 -0.0423 0.9260 0.155 Uiso 1 1 calc R . .
C83 C 0.2998(10) 0.0590(13) 0.9359(2) 0.172(7) Uiso 1 1 d G . .
H83A H 0.3432 0.0838 0.9303 0.207 Uiso 1 1 calc R . .
C84 C 0.2912(10) 0.0975(9) 0.9467(3) 0.151(6) Uiso 1 1 d G . .
H84A H 0.3287 0.1487 0.9485 0.181 Uiso 1 1 calc R . .
C85 C 0.2277(11) 0.0611(13) 0.9550(2) 0.151(6) Uiso 1 1 d G . .
H85A H 0.2218 0.0874 0.9624 0.181 Uiso 1 1 calc R . .
C86 C 0.1729(10) -0.0138(12) 0.95246(19) 0.129(5) Uiso 1 1 d G . .
H86A H 0.1295 -0.0387 0.9581 0.155 Uiso 1 1 calc R . .
C91 C 0.2642(10) 0.7185(11) 0.9008(2) 0.054(5) Uani 1 1 d . . .
H91A H 0.2429 0.7065 0.9102 0.065 Uiso 1 1 calc R . .
C92 C 0.1954(13) 0.6852(13) 0.8915(3) 0.083(8) Uani 1 1 d . . .
H92A H 0.1646 0.6299 0.8932 0.099 Uiso 1 1 calc R . .
H92B H 0.2129 0.6927 0.8820 0.099 Uiso 1 1 calc R . .
C93 C 0.1448(15) 0.7214(15) 0.8936(3) 0.104(10) Uani 1 1 d . . .
H93A H 0.1029 0.7008 0.8869 0.125 Uiso 1 1 calc R . .
H93B H 0.1225 0.7100 0.9028 0.125 Uiso 1 1 calc R . .
C94 C 0.1944(12) 0.8058(13) 0.8917(3) 0.073(7) Uani 1 1 d . . .
H94A H 0.2141 0.8162 0.8824 0.088 Uiso 1 1 calc R . .
H94B H 0.1634 0.8303 0.8930 0.088 Uiso 1 1 calc R . .
C95 C 0.2588(13) 0.8398(12) 0.9012(3) 0.076(7) Uani 1 1 d . . .
H95A H 0.2392 0.8335 0.9105 0.092 Uiso 1 1 calc R . .
H95B H 0.2896 0.8949 0.8993 0.092 Uiso 1 1 calc R . .
C96 C 0.3096(11) 0.8046(10) 0.9002(2) 0.059(6) Uani 1 1 d . . .
H96A H 0.3381 0.8203 0.8916 0.071 Uiso 1 1 calc R . .
H96B H 0.3469 0.8238 0.9076 0.071 Uiso 1 1 calc R . .
C111 C 0.3028(10) -0.0445(8) 0.85642(17) 0.035(4) Uani 1 1 d . . .
C112 C 0.3539(9) -0.0588(10) 0.86303(19) 0.045(5) Uani 1 1 d . . .
H11B H 0.3954 -0.0181 0.8676 0.054 Uiso 1 1 calc R . .
C113 C 0.3478(11) -0.1281(11) 0.86340(18) 0.045(5) Uani 1 1 d . . .
H11A H 0.3866 -0.1347 0.8674 0.054 Uiso 1 1 calc R . .
C114 C 0.2858(10) -0.1876(10) 0.85800(19) 0.046(5) Uani 1 1 d . . .
H11E H 0.2798 -0.2368 0.8588 0.056 Uiso 1 1 calc R . .
C115 C 0.2308(11) -0.1792(12) 0.85136(18) 0.053(5) Uani 1 1 d . . .
H11C H 0.1892 -0.2216 0.8472 0.064 Uiso 1 1 calc R . .
C116 C 0.2368(10) -0.1075(9) 0.85087(16) 0.035(4) Uani 1 1 d . . .
H11D H 0.1978 -0.1012 0.8469 0.042 Uiso 1 1 calc R . .
C121 C 0.2424(9) 0.0406(8) 0.84423(18) 0.035(4) Uani 1 1 d . . .
C122 C 0.1713(11) 0.0263(10) 0.8489(2) 0.065(6) Uani 1 1 d . . .
H12D H 0.1596 0.0212 0.8582 0.078 Uiso 1 1 calc R . .
C123 C 0.1203(13) 0.0200(14) 0.8395(3) 0.084(8) Uani 1 1 d . . .
H12B H 0.0705 0.0062 0.8424 0.101 Uiso 1 1 calc R . .
C124 C 0.1362(17) 0.0323(12) 0.8261(4) 0.100(11) Uani 1 1 d . . .
H12C H 0.1006 0.0334 0.8200 0.120 Uiso 1 1 calc R . .
C125 C 0.2056(13) 0.0435(11) 0.8214(2) 0.060(6) Uani 1 1 d . . .
H12E H 0.2151 0.0449 0.8120 0.072 Uiso 1 1 calc R . .
C126 C 0.2593(10) 0.0522(8) 0.83050(18) 0.039(4) Uani 1 1 d . . .
H12A H 0.3089 0.0664 0.8275 0.047 Uiso 1 1 calc R . .
C131 C 0.2878(11) 0.0614(10) 0.87231(19) 0.051(5) Uani 1 1 d . . .
C132 C 0.2623(12) 0.0065(13) 0.8825(3) 0.074(7) Uani 1 1 d . . .
H13B H 0.2579 -0.0414 0.8806 0.089 Uiso 1 1 calc R . .
C133 C 0.2429(13) 0.0207(14) 0.8955(2) 0.066(6) Uani 1 1 d . . .
H13A H 0.2268 -0.0178 0.9022 0.080 Uiso 1 1 calc R . .
C134 C 0.2463(16) 0.0843(14) 0.8986(2) 0.100(10) Uani 1 1 d . . .
H13C H 0.2329 0.0930 0.9073 0.119 Uiso 1 1 calc R . .
C135 C 0.270(2) 0.1380(16) 0.8888(3) 0.158(15) Uani 1 1 d U . .
H13D H 0.2734 0.1855 0.8906 0.189 Uiso 1 1 calc R . .
C136 C 0.289(2) 0.1234(16) 0.8760(3) 0.158(15) Uani 1 1 d U . .
H13E H 0.3044 0.1623 0.8694 0.190 Uiso 1 1 calc R . .
C211 C 0.370(3) -0.1071(18) 0.9787(3) 0.202(9) Uiso 1 1 d G . .
C212 C 0.442(2) -0.052(3) 0.9746(4) 0.243(11) Uiso 1 1 d G . .
H21A H 0.4837 -0.0614 0.9754 0.291 Uiso 1 1 calc R . .
C213 C 0.4542(19) 0.016(2) 0.9692(4) 0.283(13) Uiso 1 1 d G . .
H21B H 0.5036 0.0534 0.9664 0.340 Uiso 1 1 calc R . .
C214 C 0.394(3) 0.0294(17) 0.9680(4) 0.324(15) Uiso 1 1 d G . .
H21C H 0.4020 0.0760 0.9644 0.389 Uiso 1 1 calc R . .
C215 C 0.322(2) -0.025(2) 0.9722(4) 0.283(13) Uiso 1 1 d G . .
H21D H 0.2805 -0.0163 0.9713 0.340 Uiso 1 1 calc R . .
C216 C 0.3099(19) -0.0937(18) 0.9775(4) 0.243(11) Uiso 1 1 d G . .
H21E H 0.2606 -0.1312 0.9804 0.291 Uiso 1 1 calc R . .
C221 C 0.2318(19) -0.324(2) 0.9848(4) 0.273(13) Uiso 1 1 d G . .
C222 C 0.213(2) -0.268(2) 0.9834(3) 0.327(16) Uiso 1 1 d G . .
H22A H 0.2181 -0.2445 0.9749 0.393 Uiso 1 1 calc R . .
C223 C 0.1880(17) -0.2447(18) 0.9945(3) 0.382(18) Uiso 1 1 d G . .
H22B H 0.1754 -0.2059 0.9935 0.458 Uiso 1 1 calc R . .
C224 C 0.181(2) -0.279(3) 1.0070(3) 0.44(2) Uiso 1 1 d G . .
H22C H 0.1638 -0.2629 1.0146 0.524 Uiso 1 1 calc R . .
C225 C 0.200(3) -0.335(2) 1.0084(4) 0.382(18) Uiso 1 1 d G . .
H22D H 0.1948 -0.3586 1.0169 0.458 Uiso 1 1 calc R . .
C226 C 0.225(2) -0.358(2) 0.9973(5) 0.327(16) Uiso 1 1 d G . .
H22E H 0.2374 -0.3972 0.9983 0.393 Uiso 1 1 calc R . .
C231 C 0.1936(19) -0.2029(15) 0.9613(2) 0.171(7) Uiso 1 1 d G . .
C232 C 0.1262(17) -0.2181(15) 0.9550(3) 0.206(9) Uiso 1 1 d G . .
H23A H 0.0907 -0.2092 0.9597 0.247 Uiso 1 1 calc R . .
C233 C 0.1109(15) -0.2465(18) 0.9419(3) 0.240(10) Uiso 1 1 d G . .
H23B H 0.0649 -0.2569 0.9377 0.288 Uiso 1 1 calc R . .
C234 C 0.163(2) -0.2596(18) 0.9351(3) 0.274(12) Uiso 1 1 d G . .
H23C H 0.1524 -0.2790 0.9262 0.329 Uiso 1 1 calc R . .
C235 C 0.230(2) -0.2444(17) 0.9414(3) 0.240(10) Uiso 1 1 d G . .
H23D H 0.2658 -0.2533 0.9367 0.288 Uiso 1 1 calc R . .
C236 C 0.2456(14) -0.2160(17) 0.9544(3) 0.206(9) Uiso 1 1 d G . .
H23E H 0.2916 -0.2055 0.9587 0.247 Uiso 1 1 calc R . .
O10 O 0.040(2) 0.077(2) 0.8761(4) 0.091(10) Uiso 0.33 1 d PG . .
C10A C 0.0985(17) 0.062(2) 0.8795(4) 0.091(10) Uiso 0.33 1 d PG . .
H10C H 0.1208 0.0852 0.8880 0.109 Uiso 0.33 1 d PG . .
H10D H 0.1374 0.0828 0.8727 0.109 Uiso 0.33 1 d PG . .
C10B C 0.066(2) -0.018(2) 0.8803(3) 0.091(10) Uiso 0.33 1 d PG . .
H10E H 0.0739 -0.0318 0.8891 0.109 Uiso 0.33 1 d PG . .
H10F H 0.0905 -0.0342 0.8738 0.109 Uiso 0.33 1 d PG . .
C10C C -0.012(2) -0.052(2) 0.8774(4) 0.091(10) Uiso 0.33 1 d PG . .
H10G H -0.0414 -0.0819 0.8849 0.109 Uiso 0.33 1 d PG . .
H10H H -0.0248 -0.0843 0.8697 0.109 Uiso 0.33 1 d PG . .
C10D C -0.0289(18) 0.007(3) 0.8749(4) 0.091(10) Uiso 0.33 1 d PG . .
H10I H -0.0492 0.0018 0.8659 0.109 Uiso 0.33 1 d PG . .
H10J H -0.0658 0.0042 0.8812 0.109 Uiso 0.33 1 d PG . .
O11 O 0.476(2) 0.048(2) 0.9325(3) 0.259(12) Uiso 1 1 d GD . .
C11A C 0.4187(17) -0.034(3) 0.9325(4) 0.259(12) Uiso 1 1 d GD . .
H11F H 0.3850 -0.0482 0.9245 0.310 Uiso 1 1 calc R . .
H11G H 0.3880 -0.0495 0.9409 0.310 Uiso 1 1 calc R . .
C11B C 0.472(3) -0.0637(17) 0.9318(4) 0.259(12) Uiso 1 1 d GD . .
H11H H 0.4752 -0.0841 0.9407 0.310 Uiso 1 1 calc R . .
H11I H 0.4537 -0.1055 0.9251 0.310 Uiso 1 1 calc R . .
C11C C 0.549(2) -0.002(3) 0.9277(4) 0.259(12) Uiso 1 1 d GD . .
H11J H 0.5581 -0.0077 0.9181 0.310 Uiso 1 1 calc R . .
H11K H 0.5883 -0.0055 0.9331 0.310 Uiso 1 1 calc R . .
C11D C 0.557(2) 0.0747(19) 0.9299(4) 0.259(12) Uiso 1 1 d GD . .
H11L H 0.5893 0.1017 0.9377 0.310 Uiso 1 1 calc R . .
H11M H 0.5755 0.1071 0.9218 0.310 Uiso 1 1 calc R . .
O12 O 0.666(10) 0.295(7) 0.9562(10) 0.23(3) Uiso 0.33 1 d PG . .
C12A C 0.594(9) 0.292(6) 0.957(3) 0.23(3) Uiso 0.33 1 d PG . .
H12F H 0.5693 0.2675 0.9656 0.273 Uiso 0.33 1 d PG . .
H12G H 0.5614 0.2625 0.9499 0.273 Uiso 0.33 1 d PG . .
C12B C 0.607(8) 0.368(8) 0.9569(16) 0.23(3) Uiso 0.33 1 d PG . .
H12H H 0.5887 0.3795 0.9650 0.273 Uiso 0.33 1 d PG . .
H12I H 0.5808 0.3745 0.9493 0.273 Uiso 0.33 1 d PG . .
C12C C 0.688(9) 0.420(6) 0.956(2) 0.23(3) Uiso 0.33 1 d PG . .
H12J H 0.7066 0.4538 0.9631 0.273 Uiso 0.33 1 d PG . .
H12K H 0.6987 0.4488 0.9474 0.273 Uiso 0.33 1 d PG . .
C12D C 0.725(8) 0.374(8) 0.955(2) 0.23(3) Uiso 0.33 1 d PG . .
H12L H 0.7521 0.3828 0.9468 0.273 Uiso 0.33 1 d PG . .
H12M H 0.7600 0.3878 0.9625 0.273 Uiso 0.33 1 d PG . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Ag1 Se1A 120.6(8) . . ?
P1 Ag1 Se2 123.83(13) . . ?
Se1A Ag1 Se2 95.1(9) . . ?
P1 Ag1 Se1 104.92(12) . . ?
Se1A Ag1 Se1 26.2(9) . . ?
Se2 Ag1 Se1 120.52(7) . . ?
P1 Ag1 Se1 102.77(12) . 18_546 ?
Se1A Ag1 Se1 124.9(8) . 18_546 ?
Se2 Ag1 Se1 86.16(6) . 18_546 ?
Se1 Ag1 Se1 116.08(6) . 18_546 ?
P1 Ag1 Se2A 105.7(8) . . ?
Se1A Ag1 Se2A 90.4(11) . . ?
Se2 Ag1 Se2A 26.3(7) . . ?
Se1 Ag1 Se2A 115.9(7) . . ?
Se1 Ag1 Se2A 109.8(7) 18_546 . ?
P1 Ag1 Se1A 119.2(8) . 18_546 ?
Se1A Ag1 Se1A 101.1(11) . 18_546 ?
Se2 Ag1 Se1A 90.5(7) . 18_546 ?
Se1 Ag1 Se1A 93.7(7) . 18_546 ?
Se1 Ag1 Se1A 24.0(7) 18_546 18_546 ?
Se2A Ag1 Se1A 116.8(10) . 18_546 ?
P1 Ag1 Ag3 138.49(12) . . ?
Se1A Ag1 Ag3 74.4(8) . . ?
Se2 Ag1 Ag3 89.27(6) . . ?
Se1 Ag1 Ag3 71.31(5) . . ?
Se1 Ag1 Ag3 50.50(5) 18_546 . ?
Se2A Ag1 Ag3 113.0(8) . . ?
Se1A Ag1 Ag3 26.9(7) 18_546 . ?
P1 Ag1 Ag3 140.18(12) . 17_556 ?
Se1A Ag1 Ag3 24.9(9) . 17_556 ?
Se2 Ag1 Ag3 70.76(5) . 17_556 ?
Se1 Ag1 Ag3 49.77(5) . 17_556 ?
Se1 Ag1 Ag3 115.76(6) 18_546 17_556 ?
Se2A Ag1 Ag3 71.2(7) . 17_556 ?
Se1A Ag1 Ag3 95.3(8) 18_546 17_556 ?
Ag3 Ag1 Ag3 69.54(5) . 17_556 ?
P1 Ag1 Ag3A 138.3(5) . . ?
Se1A Ag1 Ag3A 94.4(10) . . ?
Se2 Ag1 Ag3A 21.8(5) . . ?
Se1 Ag1 Ag3A 115.5(5) . . ?
Se1 Ag1 Ag3A 68.7(5) 18_546 . ?
Se2A Ag1 Ag3A 47.9(9) . . ?
Se1A Ag1 Ag3A 69.2(9) 18_546 . ?
Ag3 Ag1 Ag3A 68.3(5) . . ?
Ag3 Ag1 Ag3A 69.8(5) 17_556 . ?
Ag2A Ag2 P4 0.00(5) . . ?
Ag2A Ag2 Se2A 98.2(9) . 2_655 ?
P4 Ag2 Se2A 98.2(8) . 2_655 ?
Ag2A Ag2 Se2A 98.2(9) . . ?
P4 Ag2 Se2A 98.2(8) . . ?
Se2A Ag2 Se2A 118.0(4) 2_655 . ?
Ag2A Ag2 Se2A 98.2(9) . 3_665 ?
P4 Ag2 Se2A 98.2(8) . 3_665 ?
Se2A Ag2 Se2A 118.0(4) 2_655 3_665 ?
Se2A Ag2 Se2A 118.0(4) . 3_665 ?
Ag2A Ag2 Se2 119.52(7) . 2_655 ?
P4 Ag2 Se2 119.52(6) . 2_655 ?
Se2A Ag2 Se2 27.6(8) 2_655 2_655 ?
Se2A Ag2 Se2 125.2(8) . 2_655 ?
Se2A Ag2 Se2 95.8(8) 3_665 2_655 ?
Ag2A Ag2 Se2 119.52(7) . . ?
P4 Ag2 Se2 119.52(6) . . ?
Se2A Ag2 Se2 95.8(8) 2_655 . ?
Se2A Ag2 Se2 27.6(8) . . ?
Se2A Ag2 Se2 125.2(8) 3_665 . ?
Se2 Ag2 Se2 97.80(8) 2_655 . ?
Ag2A Ag2 Se2 119.52(6) . 3_665 ?
P4 Ag2 Se2 119.52(6) . 3_665 ?
Se2A Ag2 Se2 125.2(8) 2_655 3_665 ?
Se2A Ag2 Se2 95.8(8) . 3_665 ?
Se2A Ag2 Se2 27.6(8) 3_665 3_665 ?
Se2 Ag2 Se2 97.80(8) 2_655 3_665 ?
Se2 Ag2 Se2 97.80(8) . 3_665 ?
Ag2A Ag2 Ag3A 135.9(6) . . ?
P4 Ag2 Ag3A 135.9(6) . . ?
Se2A Ag2 Ag3A 74.0(10) 2_655 . ?
Se2A Ag2 Ag3A 53.7(10) . . ?
Se2A Ag2 Ag3A 124.2(10) 3_665 . ?
Se2 Ag2 Ag3A 71.8(6) 2_655 . ?
Se2 Ag2 Ag3A 26.1(6) . . ?
Se2 Ag2 Ag3A 98.5(6) 3_665 . ?
Ag2A Ag2 Ag3A 135.9(7) . 2_655 ?
P4 Ag2 Ag3A 135.9(6) . 2_655 ?
Se2A Ag2 Ag3A 53.7(10) 2_655 2_655 ?
Se2A Ag2 Ag3A 124.2(10) . 2_655 ?
Se2A Ag2 Ag3A 74.0(10) 3_665 2_655 ?
Se2 Ag2 Ag3A 26.1(5) 2_655 2_655 ?
Se2 Ag2 Ag3A 98.5(6) . 2_655 ?
Se2 Ag2 Ag3A 71.8(6) 3_665 2_655 ?
Ag3A Ag2 Ag3A 74.1(9) . 2_655 ?
Ag2A Ag2 Ag3A 135.9(6) . 3_665 ?
P4 Ag2 Ag3A 135.9(5) . 3_665 ?
Se2A Ag2 Ag3A 124.2(10) 2_655 3_665 ?
Se2A Ag2 Ag3A 74.0(10) . 3_665 ?
Se2A Ag2 Ag3A 53.7(10) 3_665 3_665 ?
Se2 Ag2 Ag3A 98.5(6) 2_655 3_665 ?
Se2 Ag2 Ag3A 71.8(6) . 3_665 ?
Se2 Ag2 Ag3A 26.1(5) 3_665 3_665 ?
Ag3A Ag2 Ag3A 74.1(9) . 3_665 ?
Ag3A Ag2 Ag3A 74.1(9) 2_655 3_665 ?
Ag2 Ag2A Se2A 70.6(15) . 2_655 ?
P4 Ag2A Se2A 109.4(15) . 2_655 ?
Ag2 Ag2A Se2A 70.6(16) . . ?
P4 Ag2A Se2A 109.4(15) . . ?
Se2A Ag2A Se2A 109.6(15) 2_655 . ?
Ag2 Ag2A Se2A 70.6(15) . 3_665 ?
P4 Ag2A Se2A 109.4(15) . 3_665 ?
Se2A Ag2A Se2A 109.6(15) 2_655 3_665 ?
Se2A Ag2A Se2A 109.6(15) . 3_665 ?
Ag2 Ag2A Se2 51.5(10) . 2_655 ?
P4 Ag2A Se2 128.5(10) . 2_655 ?
Se2A Ag2A Se2 25.1(9) 2_655 2_655 ?
Se2A Ag2A Se2 110.3(19) . 2_655 ?
Se2A Ag2A Se2 86.5(14) 3_665 2_655 ?
Ag2 Ag2A Se2 51.5(10) . . ?
P4 Ag2A Se2 128.5(10) . . ?
Se2A Ag2A Se2 86.5(14) 2_655 . ?
Se2A Ag2A Se2 25.1(9) . . ?
Se2A Ag2A Se2 110(2) 3_665 . ?
Se2 Ag2A Se2 85.3(14) 2_655 . ?
Ag2 Ag2A Se2 51.5(10) . 3_665 ?
P4 Ag2A Se2 128.5(10) . 3_665 ?
Se2A Ag2A Se2 110.3(19) 2_655 3_665 ?
Se2A Ag2A Se2 86.5(14) . 3_665 ?
Se2A Ag2A Se2 25.1(9) 3_665 3_665 ?
Se2 Ag2A Se2 85.3(14) 2_655 3_665 ?
Se2 Ag2A Se2 85.3(14) . 3_665 ?
Ag3A Ag3 Se1A 155(2) 17_556 18_546 ?
Ag3A Ag3 Se1 167.9(13) 17_556 18_546 ?
Se1A Ag3 Se1 12.7(15) 18_546 18_546 ?
Ag3A Ag3 Se2 10.8(12) 17_556 17_556 ?
Se1A Ag3 Se2 150.9(15) 18_546 17_556 ?
Se1 Ag3 Se2 161.18(8) 18_546 17_556 ?
Ag3A Ag3 Se3 74.5(13) 17_556 . ?
Se1A Ag3 Se3 123.7(15) 18_546 . ?
Se1 Ag3 Se3 115.54(6) 18_546 . ?
Se2 Ag3 Se3 83.27(6) 17_556 . ?
Ag3A Ag3 Ag1 130.3(13) 17_556 . ?
Se1A Ag3 Ag1 69.0(15) 18_546 . ?
Se1 Ag3 Ag1 57.93(5) 18_546 . ?
Se2 Ag3 Ag1 124.44(6) 17_556 . ?
Se3 Ag3 Ag1 94.52(5) . . ?
Ag3A Ag3 Ag1 121.3(13) 17_556 18_546 ?
Se1A Ag3 Ag1 48.5(14) 18_546 18_546 ?
Se1 Ag3 Ag1 54.20(5) 18_546 18_546 ?
Se2 Ag3 Ag1 128.35(7) 17_556 18_546 ?
Se3 Ag3 Ag1 92.36(4) . 18_546 ?
Ag1 Ag3 Ag1 107.20(5) . 18_546 ?
Ag3 Ag3A Se2 159(2) 18_546 . ?
Ag3 Ag3A Se2A 165(2) 18_546 . ?
Se2 Ag3A Se2A 8.4(10) . . ?
Ag3 Ag3A Se1A 13.0(11) 18_546 2_655 ?
Se2 Ag3A Se1A 152.6(19) . 2_655 ?
Se2A Ag3A Se1A 155.0(17) . 2_655 ?
Ag3 Ag3A Se3 80.3(13) 18_546 . ?
Se2 Ag3A Se3 116.4(15) . . ?
Se2A Ag3A Se3 114.4(13) . . ?
Se1A Ag3A Se3 90.4(12) 2_655 . ?
Ag3 Ag3A Ag2 132.6(17) 18_546 . ?
Se2 Ag3A Ag2 64.1(11) . . ?
Se2A Ag3A Ag2 55.7(10) . . ?
Se1A Ag3A Ag2 125.3(13) 2_655 . ?
Se3 Ag3A Ag2 89.5(7) . . ?
Ag3 Ag3A Ag1 122.3(16) 18_546 . ?
Se2 Ag3A Ag1 48.9(10) . . ?
Se2A Ag3A Ag1 55.9(10) . . ?
Se1A Ag3A Ag1 130.7(13) 2_655 . ?
Se3 Ag3A Ag1 90.9(8) . . ?
Ag2 Ag3A Ag1 103.9(8) . . ?
P3 Ag4 Se5A 119.66(16) . 3 ?
P3 Ag4 Se5A 119.66(15) . 2 ?
Se5A Ag4 Se5A 97.6(2) 3 2 ?
P3 Ag4 Se5A 119.66(15) . . ?
Se5A Ag4 Se5A 97.6(2) 3 . ?
Se5A Ag4 Se5A 97.6(2) 2 . ?
P3 Ag4 Se5 104.23(8) . 3 ?
Se5A Ag4 Se5 22.24(16) 3 3 ?
Se5A Ag4 Se5 93.59(18) 2 3 ?
Se5A Ag4 Se5 119.87(16) . 3 ?
P3 Ag4 Se5 104.23(8) . 2 ?
Se5A Ag4 Se5 119.87(16) 3 2 ?
Se5A Ag4 Se5 22.24(16) 2 2 ?
Se5A Ag4 Se5 93.59(18) . 2 ?
Se5 Ag4 Se5 114.16(6) 3 2 ?
P3 Ag4 Se5 104.23(8) . . ?
Se5A Ag4 Se5 93.59(18) 3 . ?
Se5A Ag4 Se5 119.87(16) 2 . ?
Se5A Ag4 Se5 22.24(16) . . ?
Se5 Ag4 Se5 114.16(6) 3 . ?
Se5 Ag4 Se5 114.16(6) 2 . ?
P3 Ag4 Ag6 138.03(5) . 3 ?
Se5A Ag4 Ag6 96.80(17) 3 3 ?
Se5A Ag4 Ag6 70.40(15) 2 3 ?
Se5A Ag4 Ag6 27.55(17) . 3 ?
Se5 Ag4 Ag6 116.16(11) 3 3 ?
Se5 Ag4 Ag6 70.04(8) 2 3 ?
Se5 Ag4 Ag6 49.62(9) . 3 ?
P3 Ag4 Ag6 138.03(5) . . ?
Se5A Ag4 Ag6 70.40(15) 3 . ?
Se5A Ag4 Ag6 27.55(18) 2 . ?
Se5A Ag4 Ag6 96.80(17) . . ?
Se5 Ag4 Ag6 70.04(8) 3 . ?
Se5 Ag4 Ag6 49.62(9) 2 . ?
Se5 Ag4 Ag6 116.16(11) . . ?
Ag6 Ag4 Ag6 70.79(8) 3 . ?
P3 Ag4 Ag6 138.03(5) . 2 ?
Se5A Ag4 Ag6 27.55(17) 3 2 ?
Se5A Ag4 Ag6 96.80(18) 2 2 ?
Se5A Ag4 Ag6 70.40(15) . 2 ?
Se5 Ag4 Ag6 49.62(9) 3 2 ?
Se5 Ag4 Ag6 116.16(11) 2 2 ?
Se5 Ag4 Ag6 70.04(8) . 2 ?
Ag6 Ag4 Ag6 70.79(8) 3 2 ?
Ag6 Ag4 Ag6 70.79(8) . 2 ?
P2 Ag5 Se5 109.44(19) 10_557 10_557 ?
P2 Ag5 Se4 125.46(19) 10_557 11_557 ?
Se5 Ag5 Se4 89.15(11) 10_557 11_557 ?
P2 Ag5 Se4A 108.7(2) 10_557 11_557 ?
Se5 Ag5 Se4A 109.85(19) 10_557 11_557 ?
Se4 Ag5 Se4A 22.24(15) 11_557 11_557 ?
P2 Ag5 Se4 117.39(19) 10_557 . ?
Se5 Ag5 Se4 112.49(12) 10_557 . ?
Se4 Ag5 Se4 99.59(11) 11_557 . ?
Se4A Ag5 Se4 98.23(16) 11_557 . ?
P2 Ag5 Se4A 100.3(2) 10_557 . ?
Se5 Ag5 Se4A 109.31(17) 10_557 . ?
Se4 Ag5 Se4A 121.65(18) 11_557 . ?
Se4A Ag5 Se4A 118.57(13) 11_557 . ?
Se4 Ag5 Se4A 22.06(14) . . ?
P2 Ag5 Se5A 124.3(2) 10_557 10_557 ?
Se5 Ag5 Se5A 21.86(14) 10_557 10_557 ?
Se4 Ag5 Se5A 91.44(16) 11_557 10_557 ?
Se4A Ag5 Se5A 113.7(2) 11_557 10_557 ?
Se4 Ag5 Se5A 90.68(18) . 10_557 ?
Se4A Ag5 Se5A 89.7(2) . 10_557 ?
P2 Ag5 Ag6A 140.7(2) 10_557 . ?
Se5 Ag5 Ag6A 105.64(12) 10_557 . ?
Se4 Ag5 Ag6A 71.39(13) 11_557 . ?
Se4A Ag5 Ag6A 74.37(17) 11_557 . ?
Se4 Ag5 Ag6A 28.78(12) . . ?
Se4A Ag5 Ag6A 50.53(18) . . ?
Se5A Ag5 Ag6A 85.81(17) 10_557 . ?
P2 Ag5 Ag6A 146.55(19) 10_557 11_557 ?
Se5 Ag5 Ag6A 68.09(12) 10_557 11_557 ?
Se4 Ag5 Ag6A 26.59(11) 11_557 11_557 ?
Se4A Ag5 Ag6A 48.36(18) 11_557 11_557 ?
Se4 Ag5 Ag6A 92.49(12) . 11_557 ?
Se4A Ag5 Ag6A 112.07(17) . 11_557 ?
Se5A Ag5 Ag6A 65.78(16) 10_557 11_557 ?
Ag6A Ag5 Ag6A 64.65(16) . 11_557 ?
Ag6A Ag6 Se5A 165.2(4) . 2 ?
Ag6A Ag6 Se5 167.7(3) . 2 ?
Se5A Ag6 Se5 4.3(3) 2 2 ?
Ag6A Ag6 Se4 14.8(3) . . ?
Se5A Ag6 Se4 150.4(3) 2 . ?
Se5 Ag6 Se4 153.40(14) 2 . ?
Ag6A Ag6 Se6 79.6(3) . . ?
Se5A Ag6 Se6 115.2(3) 2 . ?
Se5 Ag6 Se6 112.29(11) 2 . ?
Se4 Ag6 Se6 94.30(10) . . ?
Ag6A Ag6 Ag4 128.0(3) . . ?
Se5A Ag6 Ag4 55.7(2) 2 . ?
Se5 Ag6 Ag4 57.81(9) 2 . ?
Se4 Ag6 Ag4 126.79(11) . . ?
Se6 Ag6 Ag4 88.68(7) . . ?
Ag6 Ag6A Se4 154.4(5) . . ?
Ag6 Ag6A Se4A 160.4(4) . . ?
Se4 Ag6A Se4A 6.2(2) . . ?
Ag6 Ag6A Se5A 8.5(2) . 2 ?
Se4 Ag6A Se5A 146.0(3) . 2 ?
Se4A Ag6A Se5A 151.9(3) . 2 ?
Ag6 Ag6A Se6 77.6(3) . . ?
Se4 Ag6A Se6 127.7(3) . . ?
Se4A Ag6A Se6 122.0(2) . . ?
Se5A Ag6A Se6 86.0(2) 2 . ?
Ag6 Ag6A Ag5 126.5(3) . . ?
Se4 Ag6A Ag5 60.2(2) . . ?
Se4A Ag6A Ag5 56.67(18) . . ?
Se5A Ag6A Ag5 125.9(2) 2 . ?
Se6 Ag6A Ag5 99.17(14) . . ?
Ag6 Ag6A Ag5 129.1(3) . 12_557 ?
Se4 Ag6A Ag5 53.2(2) . 12_557 ?
Se4A Ag6A Ag5 53.31(18) . 12_557 ?
Se5A Ag6A Ag5 128.9(2) 2 12_557 ?
Se6 Ag6A Ag5 94.97(14) . 12_557 ?
Ag5 Ag6A Ag5 104.43(17) . 12_557 ?
Se1A Se1 C51 92.4(18) . . ?
Se1A Se1 Ag3 15.2(18) . 17_556 ?
C51 Se1 Ag3 104.1(5) . 17_556 ?
Se1A Se1 Ag1 68.7(17) . . ?
C51 Se1 Ag1 102.7(5) . . ?
Ag3 Se1 Ag1 76.02(6) 17_556 . ?
Se1A Se1 Ag1 84.7(18) . 17_556 ?
C51 Se1 Ag1 111.4(5) . 17_556 ?
Ag3 Se1 Ag1 71.57(6) 17_556 17_556 ?
Ag1 Se1 Ag1 137.38(9) . 17_556 ?
Se1 Se1A Ag3 152(3) . 17_556 ?
Se1 Se1A C51 57.0(15) . . ?
Ag3 Se1A C51 142(2) 17_556 . ?
Se1 Se1A Ag1 85.1(18) . . ?
Ag3 Se1A Ag1 106.5(19) 17_556 . ?
C51 Se1A Ag1 97.9(13) . . ?
Se1 Se1A Ag3A 164(3) . 3_665 ?
Ag3 Se1A Ag3A 11.7(10) 17_556 3_665 ?
C51 Se1A Ag3A 133.9(17) . 3_665 ?
Ag1 Se1A Ag3A 103.2(14) . 3_665 ?
Se1 Se1A Ag1 71.3(17) . 17_556 ?
Ag3 Se1A Ag1 84.1(15) 17_556 17_556 ?
C51 Se1A Ag1 96.5(13) . 17_556 ?
Ag1 Se1A Ag1 139.1(15) . 17_556 ?
Ag3A Se1A Ag1 93.7(12) 3_665 17_556 ?
Se2A Se2 Ag3A 163(2) . . ?
Se2A Se2 C61 67.8(17) . . ?
Ag3A Se2 C61 118.7(13) . . ?
Se2A Se2 Ag3 169.2(16) . 18_546 ?
Ag3A Se2 Ag3 10.4(12) . 18_546 ?
C61 Se2 Ag3 109.9(6) . 18_546 ?
Se2A Se2 Ag1 84.8(16) . . ?
Ag3A Se2 Ag1 109.3(13) . . ?
C61 Se2 Ag1 95.3(5) . . ?
Ag3 Se2 Ag1 106.01(8) 18_546 . ?
Se2A Se2 Ag2 73.0(17) . . ?
Ag3A Se2 Ag2 89.8(13) . . ?
C61 Se2 Ag2 108.5(5) . . ?
Ag3 Se2 Ag2 98.43(7) 18_546 . ?
Ag1 Se2 Ag2 137.41(8) . . ?
Se2A Se2 Ag2A 66.5(18) . . ?
Ag3A Se2 Ag2A 96.3(15) . . ?
C61 Se2 Ag2A 99.8(11) . . ?
Ag3 Se2 Ag2A 104.2(6) 18_546 . ?
Ag1 Se2 Ag2A 138.96(11) . . ?
Ag2 Se2 Ag2A 9.0(10) . . ?
Se2 Se2A C61 73.2(18) . . ?
Se2 Se2A C66 113(2) . . ?
C61 Se2A C66 40.2(11) . . ?
Se2 Se2A Ag3A 8.8(10) . . ?
C61 Se2A Ag3A 77.1(15) . . ?
C66 Se2A Ag3A 116.7(18) . . ?
Se2 Se2A Ag2 79.4(17) . . ?
C61 Se2A Ag2 113.7(16) . . ?
C66 Se2A Ag2 119.5(17) . . ?
Ag3A Se2A Ag2 70.7(11) . . ?
Se2 Se2A Ag2A 88(2) . . ?
C61 Se2A Ag2A 110.7(16) . . ?
C66 Se2A Ag2A 109.8(19) . . ?
Ag3A Se2A Ag2A 79.7(16) . . ?
Ag2 Se2A Ag2A 11.2(13) . . ?
Se2 Se2A Ag1 68.9(16) . . ?
C61 Se2A Ag1 91.1(14) . . ?
C66 Se2A Ag1 106.2(15) . . ?
Ag3A Se2A Ag1 76.2(12) . . ?
Ag2 Se2A Ag1 131.9(14) . . ?
Ag2A Se2A Ag1 142.8(19) . . ?
Ag3A Se3 Ag3A 77.8(9) 2_655 . ?
Ag3A Se3 Ag3A 77.8(9) 2_655 3_665 ?
Ag3A Se3 Ag3A 77.8(9) . 3_665 ?
Ag3A Se3 Ag3A 102.2(9) 2_655 16_656 ?
Ag3A Se3 Ag3A 102.2(9) 3_665 16_656 ?
Ag3A Se3 Ag3A 102.2(9) . 17_556 ?
Ag3A Se3 Ag3A 102.2(9) 3_665 17_556 ?
Ag3A Se3 Ag3A 77.8(9) 16_656 17_556 ?
Ag3A Se3 Ag3A 102.2(9) 2_655 18_546 ?
Ag3A Se3 Ag3A 102.2(9) . 18_546 ?
Ag3A Se3 Ag3A 77.8(9) 16_656 18_546 ?
Ag3A Se3 Ag3A 77.8(9) 17_556 18_546 ?
Ag3A Se3 Ag3 102.8(6) 2_655 17_556 ?
Ag3A Se3 Ag3 80.4(6) . 17_556 ?
Ag3A Se3 Ag3 25.2(6) 3_665 17_556 ?
Ag3A Se3 Ag3 99.6(6) 16_656 17_556 ?
Ag3A Se3 Ag3 77.2(6) 17_556 17_556 ?
Ag3A Se3 Ag3 154.8(6) 18_546 17_556 ?
Ag3A Se3 Ag3 25.2(6) 2_655 16_656 ?
Ag3A Se3 Ag3 102.8(6) . 16_656 ?
Ag3A Se3 Ag3 80.4(6) 3_665 16_656 ?
Ag3A Se3 Ag3 77.2(6) 16_656 16_656 ?
Ag3A Se3 Ag3 154.8(6) 17_556 16_656 ?
Ag3A Se3 Ag3 99.6(6) 18_546 16_656 ?
Ag3A Se3 Ag3 80.4(6) 2_655 18_546 ?
Ag3A Se3 Ag3 25.2(6) . 18_546 ?
Ag3A Se3 Ag3 102.8(6) 3_665 18_546 ?
Ag3A Se3 Ag3 154.8(6) 16_656 18_546 ?
Ag3A Se3 Ag3 99.6(6) 17_556 18_546 ?
Ag3A Se3 Ag3 77.2(6) 18_546 18_546 ?
Ag3A Se3 Ag3 77.2(6) 2_655 2_655 ?
Ag3A Se3 Ag3 99.6(6) . 2_655 ?
Ag3A Se3 Ag3 154.8(6) 3_665 2_655 ?
Ag3A Se3 Ag3 80.4(6) 16_656 2_655 ?
Ag3A Se3 Ag3 102.8(6) 17_556 2_655 ?
Ag3A Se3 Ag3 25.2(6) 18_546 2_655 ?
Ag3 Se3 Ag3 75.70(3) 16_656 2_655 ?
Ag3 Se3 Ag3 75.70(3) 18_546 2_655 ?
Ag3A Se3 Ag3 154.8(6) 2_655 . ?
Ag3A Se3 Ag3 77.2(6) . . ?
Ag3A Se3 Ag3 99.6(6) 3_665 . ?
Ag3A Se3 Ag3 102.8(6) 16_656 . ?
Ag3A Se3 Ag3 25.2(6) 17_556 . ?
Ag3A Se3 Ag3 80.4(6) 18_546 . ?
Ag3 Se3 Ag3 75.70(3) 17_556 . ?
Ag3 Se3 Ag3 75.70(3) 18_546 . ?
Ag3A Se3 Ag3 99.6(6) 2_655 3_665 ?
Ag3A Se3 Ag3 154.8(6) . 3_665 ?
Ag3A Se3 Ag3 77.2(6) 3_665 3_665 ?
Ag3A Se3 Ag3 25.2(6) 16_656 3_665 ?
Ag3A Se3 Ag3 80.4(6) 17_556 3_665 ?
Ag3A Se3 Ag3 102.8(6) 18_546 3_665 ?
Ag3 Se3 Ag3 75.70(3) 17_556 3_665 ?
Ag3 Se3 Ag3 75.70(3) 16_656 3_665 ?
Se4A Se4 Ag6A 164.7(5) . . ?
Se4A Se4 C71 74.7(17) . . ?
Ag6A Se4 C71 120.1(18) . . ?
Se4A Se4 Ag6 174.6(4) . . ?
Ag6A Se4 Ag6 10.8(2) . . ?
C71 Se4 Ag6 109.3(17) . . ?
Se4A Se4 Ag5 79.7(4) . 12_557 ?
Ag6A Se4 Ag5 100.2(2) . 12_557 ?
C71 Se4 Ag5 99(2) . 12_557 ?
Ag6 Se4 Ag5 102.80(12) . 12_557 ?
Se4A Se4 Ag5 80.0(4) . . ?
Ag6A Se4 Ag5 91.0(2) . . ?
C71 Se4 Ag5 108.4(14) . . ?
Ag6 Se4 Ag5 95.18(12) . . ?
Ag5 Se4 Ag5 140.35(14) 12_557 . ?
Se4 Se4A C71 73.5(14) . . ?
Se4 Se4A Ag6A 9.0(3) . . ?
C71 Se4A Ag6A 82.3(14) . . ?
Se4 Se4A Ag5 78.0(4) . 12_557 ?
C71 Se4A Ag5 97.8(15) . 12_557 ?
Ag6A Se4A Ag5 78.3(2) . 12_557 ?
Se4 Se4A Ag5 77.9(4) . . ?
C71 Se4A Ag5 107(2) . . ?
Ag6A Se4A Ag5 72.8(2) . . ?
Ag5 Se4A Ag5 138.3(3) 12_557 . ?
Se5A Se5 C86 101.8(8) . . ?
Se5A Se5 Ag6 6.0(4) . 3 ?
C86 Se5 Ag6 106.4(7) . 3 ?
Se5A Se5 Ag5 87.8(4) . 10_557 ?
C86 Se5 Ag5 113.3(6) . 10_557 ?
Ag6 Se5 Ag5 82.44(11) 3 10_557 ?
Se5A Se5 Ag4 69.6(4) . . ?
C86 Se5 Ag4 103.9(6) . . ?
Ag6 Se5 Ag4 72.57(10) 3 . ?
Ag5 Se5 Ag4 139.71(13) 10_557 . ?
Se5 Se5A Ag6 169.6(6) . 3 ?
Se5 Se5A C86 51.6(6) . . ?
Ag6 Se5A C86 136.1(7) 3 . ?
Se5 Se5A Ag6A 172.3(5) . 3 ?
Ag6 Se5A Ag6A 6.36(18) 3 3 ?
C86 Se5A Ag6A 129.7(6) . 3 ?
Se5 Se5A Ag4 88.2(4) . . ?
Ag6 Se5A Ag4 96.8(3) 3 . ?
C86 Se5A Ag4 97.2(5) . . ?
Ag6A Se5A Ag4 98.9(3) 3 . ?
Se5 Se5A Ag5 70.3(4) . 10_557 ?
Ag6 Se5A Ag5 100.4(3) 3 10_557 ?
C86 Se5A Ag5 94.8(6) . 10_557 ?
Ag6A Se5A Ag5 102.1(2) 3 10_557 ?
Ag4 Se5A Ag5 140.3(3) . 10_557 ?
Ag6 Se6 Ag6 82.15(7) 11_557 12_557 ?
Ag6 Se6 Ag6 97.85(7) 2 12_557 ?
Ag6 Se6 Ag6 97.85(7) 11_557 . ?
Ag6 Se6 Ag6 82.15(7) 2 . ?
Ag6 Se6 Ag6 97.85(7) 12_557 . ?
Ag6 Se6 Ag6 82.15(7) 11_557 10_557 ?
Ag6 Se6 Ag6 97.85(7) 2 10_557 ?
Ag6 Se6 Ag6 82.15(7) 12_557 10_557 ?
Ag6 Se6 Ag6 97.85(8) 11_557 3 ?
Ag6 Se6 Ag6 82.15(7) 2 3 ?
Ag6 Se6 Ag6 82.15(7) . 3 ?
Ag6 Se6 Ag6 97.85(7) 10_557 3 ?
Ag6 Se6 Ag6A 22.80(11) 11_557 11_557 ?
Ag6 Se6 Ag6A 157.20(11) 2 11_557 ?
Ag6 Se6 Ag6A 81.81(11) 12_557 11_557 ?
Ag6 Se6 Ag6A 75.35(13) . 11_557 ?
Ag6 Se6 Ag6A 104.65(13) 10_557 11_557 ?
Ag6 Se6 Ag6A 98.19(12) 3 11_557 ?
Ag6 Se6 Ag6A 157.20(11) 11_557 2 ?
Ag6 Se6 Ag6A 22.80(11) 2 2 ?
Ag6 Se6 Ag6A 98.19(12) 12_557 2 ?
Ag6 Se6 Ag6A 104.65(13) . 2 ?
Ag6 Se6 Ag6A 75.35(13) 10_557 2 ?
Ag6 Se6 Ag6A 81.81(11) 3 2 ?
Ag6 Se6 Ag6A 104.65(12) 11_557 12_557 ?
Ag6 Se6 Ag6A 75.35(13) 2 12_557 ?
Ag6 Se6 Ag6A 22.80(11) 12_557 12_557 ?
Ag6 Se6 Ag6A 98.19(12) . 12_557 ?
Ag6 Se6 Ag6A 81.81(12) 10_557 12_557 ?
Ag6 Se6 Ag6A 157.20(11) 3 12_557 ?
Ag6A Se6 Ag6A 103.97(12) 11_557 12_557 ?
Ag6A Se6 Ag6A 76.03(12) 2 12_557 ?
Ag6 Se6 Ag6A 98.19(11) 11_557 . ?
Ag6 Se6 Ag6A 81.81(11) 2 . ?
Ag6 Se6 Ag6A 75.35(13) 12_557 . ?
Ag6 Se6 Ag6A 22.80(11) . . ?
Ag6 Se6 Ag6A 157.20(12) 10_557 . ?
Ag6 Se6 Ag6A 104.65(13) 3 . ?
Ag6A Se6 Ag6A 76.03(12) 11_557 . ?
Ag6A Se6 Ag6A 103.97(12) 2 . ?
Ag6A Se6 Ag6A 76.03(12) 12_557 . ?
Ag6 Se6 Ag6A 75.35(13) 11_557 3 ?
Ag6 Se6 Ag6A 104.65(12) 2 3 ?
Ag6 Se6 Ag6A 157.20(11) 12_557 3 ?
Ag6 Se6 Ag6A 81.81(12) . 3 ?
Ag6 Se6 Ag6A 98.19(12) 10_557 3 ?
Ag6 Se6 Ag6A 22.80(11) 3 3 ?
Ag6A Se6 Ag6A 76.03(12) 11_557 3 ?
Ag6A Se6 Ag6A 103.97(12) 2 3 ?
Ag6A Se6 Ag6A 103.97(12) . 3 ?
Ag6 Se6 Ag6A 81.81(11) 11_557 10_557 ?
Ag6 Se6 Ag6A 98.19(11) 2 10_557 ?
Ag6 Se6 Ag6A 104.65(13) 12_557 10_557 ?
Ag6 Se6 Ag6A 157.20(12) . 10_557 ?
Ag6 Se6 Ag6A 22.80(11) 10_557 10_557 ?
Ag6 Se6 Ag6A 75.35(13) 3 10_557 ?
Ag6A Se6 Ag6A 103.97(12) 11_557 10_557 ?
Ag6A Se6 Ag6A 76.03(12) 2 10_557 ?
Ag6A Se6 Ag6A 103.97(12) 12_557 10_557 ?
Ag6A Se6 Ag6A 76.03(12) 3 10_557 ?
C131 P1 C121 107.4(9) . . ?
C131 P1 C111 102.5(8) . . ?
C121 P1 C111 102.4(8) . . ?
C131 P1 Ag1 117.1(7) . . ?
C121 P1 Ag1 109.2(6) . . ?
C111 P1 Ag1 116.9(6) . . ?
C231 P2 C216 97.5(15) . . ?
C231 P2 C223 119.5(12) . . ?
C216 P2 C223 112.9(15) . . ?
C231 P2 C222 85.2(14) . . ?
C216 P2 C222 103.2(15) . . ?
C223 P2 C222 38.9(7) . . ?
C231 P2 Ag5 115.3(11) . 10_557 ?
C216 P2 Ag5 111.6(13) . 10_557 ?
C223 P2 Ag5 100.5(10) . 10_557 ?
C222 P2 Ag5 135.7(9) . 10_557 ?
C31 P3 C31 106.3(6) 3 2 ?
C31 P3 C31 106.3(6) 3 . ?
C31 P3 C31 106.3(6) 2 . ?
C31 P3 Ag4 112.5(5) 3 . ?
C31 P3 Ag4 112.5(6) 2 . ?
C31 P3 Ag4 112.5(5) . . ?
Ag2A P4 C41 111.5(6) . 2_655 ?
Ag2A P4 C41 111.5(6) . 3_665 ?
C41 P4 C41 107.4(7) 2_655 3_665 ?
Ag2A P4 C41 111.5(6) . . ?
C41 P4 C41 107.4(7) 2_655 . ?
C41 P4 C41 107.4(7) 3_665 . ?
Ag2A P4 Ag2 0.000(12) . . ?
C41 P4 Ag2 111.5(6) 2_655 . ?
C41 P4 Ag2 111.5(6) 3_665 . ?
C41 P4 Ag2 111.5(6) . . ?
C91 Sn1 C91 119.47(16) . 3_565 ?
C91 Sn1 C91 119.47(15) . 2_665 ?
C91 Sn1 C91 119.47(15) 3_565 2_665 ?
C91 Sn1 Cl1 94.2(6) . . ?
C91 Sn1 Cl1 94.2(6) 3_565 . ?
C91 Sn1 Cl1 94.2(6) 2_665 . ?
C91 Sn1 Cl2 78.1(12) . 2_665 ?
C91 Sn1 Cl2 83.3(16) 3_565 2_665 ?
C91 Sn1 Cl2 96.2(14) 2_665 2_665 ?
Cl1 Sn1 Cl2 169.2(12) . 2_665 ?
C91 Sn1 Cl2 83.3(15) . 3_565 ?
C91 Sn1 Cl2 96.2(15) 3_565 3_565 ?
C91 Sn1 Cl2 78.1(12) 2_665 3_565 ?
Cl1 Sn1 Cl2 169.2(13) . 3_565 ?
Cl2 Sn1 Cl2 19(2) 2_665 3_565 ?
C91 Sn1 Cl2 96.2(14) . . ?
C91 Sn1 Cl2 78.1(12) 3_565 . ?
C91 Sn1 Cl2 83.3(16) 2_665 . ?
Cl1 Sn1 Cl2 169.2(12) . . ?
Cl2 Sn1 Cl2 19(2) 2_665 . ?
Cl2 Sn1 Cl2 19(2) 3_565 . ?
Cl2 Cl2 Cl2 60.00(4) 3_565 2_665 ?
Cl2 Cl2 Sn1 80.7(10) 3_565 . ?
Cl2 Cl2 Sn1 80.7(10) 2_665 . ?
C36 C31 C32 126.0(17) . . ?
C36 C31 P3 115.2(14) . . ?
C32 C31 P3 118.7(13) . . ?
C31 C32 C33 120.4(19) . . ?
C31 C32 H32A 119.8 . . ?
C33 C32 H32A 119.8 . . ?
C32 C33 C34 116(2) . . ?
C32 C33 H33A 121.8 . . ?
C34 C33 H33A 121.8 . . ?
C35 C34 C33 120.1(19) . . ?
C35 C34 H34A 120.0 . . ?
C33 C34 H34A 120.0 . . ?
C34 C35 C36 121(2) . . ?
C34 C35 H35A 119.4 . . ?
C36 C35 H35A 119.4 . . ?
C31 C36 C35 116(2) . . ?
C31 C36 H36A 122.2 . . ?
C35 C36 H36A 122.2 . . ?
C46 C41 C42 126.8(18) . . ?
C46 C41 P4 119.0(14) . . ?
C42 C41 P4 114.2(15) . . ?
C43 C42 C41 110(3) . . ?
C43 C42 H42A 125.0 . . ?
C41 C42 H42A 125.0 . . ?
C42 C43 C44 123(3) . . ?
C42 C43 H43A 118.6 . . ?
C44 C43 H43A 118.6 . . ?
C45 C44 C43 118(3) . . ?
C45 C44 H44A 120.9 . . ?
C43 C44 H44A 120.9 . . ?
C44 C45 C46 119(3) . . ?
C44 C45 H45A 120.3 . . ?
C46 C45 H45A 120.3 . . ?
C41 C46 C45 121(2) . . ?
C41 C46 H46A 119.3 . . ?
C45 C46 H46A 119.3 . . ?
C52 C51 C56 120.2(17) . . ?
C52 C51 Se1 117.7(14) . . ?
C56 C51 Se1 122.1(13) . . ?
C52 C51 Se1A 148.3(17) . . ?
C56 C51 Se1A 91.5(15) . . ?
Se1 C51 Se1A 30.6(10) . . ?
C51 C52 C53 118.3(19) . . ?
C51 C52 H52A 120.9 . . ?
C53 C52 H52A 120.9 . . ?
C54 C53 C52 120(2) . . ?
C54 C53 H53A 119.9 . . ?
C52 C53 H53A 119.9 . . ?
C53 C54 C55 122(2) . . ?
C53 C54 H54A 118.8 . . ?
C55 C54 H54A 118.8 . . ?
C56 C55 C54 119(2) . . ?
C56 C55 H55A 120.4 . . ?
C54 C55 H55A 120.4 . . ?
C55 C56 C51 119.7(19) . . ?
C55 C56 H56A 120.2 . . ?
C51 C56 H56A 120.2 . . ?
C66 C61 C62 121.1(19) . . ?
C66 C61 Se2A 78.2(17) . . ?
C62 C61 Se2A 160(2) . . ?
C66 C61 Se2 117.1(14) . . ?
C62 C61 Se2 121.3(16) . . ?
Se2A C61 Se2 39.0(12) . . ?
C63 C62 C61 119(2) . . ?
C63 C62 H62A 120.7 . . ?
C61 C62 H62A 120.7 . . ?
C62 C63 C64 122(2) . . ?
C62 C63 H63A 119.0 . . ?
C64 C63 H63A 119.0 . . ?
C63 C64 C65 120(2) . . ?
C63 C64 H64A 120.1 . . ?
C65 C64 H64A 120.1 . . ?
C64 C65 C66 118(2) . . ?
C64 C65 H65A 121.2 . . ?
C66 C65 H65A 121.2 . . ?
C61 C66 C65 121(2) . . ?
C61 C66 Se2A 61.6(15) . . ?
C65 C66 Se2A 178(2) . . ?
C61 C66 H66A 119.7 . . ?
C65 C66 H66A 119.7 . . ?
Se2A C66 H66A 58.1 . . ?
C72 C71 C76 120.0 . . ?
C72 C71 Se4 112(5) . . ?
C76 C71 Se4 127(4) . . ?
C72 C71 Se4A 131(4) . . ?
C76 C71 Se4A 102(4) . . ?
Se4 C71 Se4A 31.8(3) . . ?
C73 C72 C71 120.00(15) . . ?
C73 C72 H72A 120.0 . . ?
C71 C72 H72A 120.0 . . ?
C72 C73 C74 120.00(14) . . ?
C72 C73 H73A 120.0 . . ?
C74 C73 H73A 120.0 . . ?
C75 C74 C73 120.0 . . ?
C75 C74 H74A 120.0 . . ?
C73 C74 H74A 120.0 . . ?
C74 C75 C76 120.00(17) . . ?
C74 C75 H75A 120.0 . . ?
C76 C75 H75A 120.0 . . ?
C75 C76 C71 120.00(13) . . ?
C75 C76 H76A 120.0 . . ?
C71 C76 H76A 120.0 . . ?
C82 C81 C86 120.00(7) . . ?
C83 C82 C81 120.0 . . ?
C83 C82 H82A 120.0 . . ?
C81 C82 H82A 120.0 . . ?
C84 C83 C82 120.00(6) . . ?
C84 C83 H83A 120.0 . . ?
C82 C83 H83A 120.0 . . ?
C83 C84 C85 120.00(6) . . ?
C83 C84 H84A 120.0 . . ?
C85 C84 H84A 120.0 . . ?
C86 C85 C84 120.0 . . ?
C86 C85 H85A 120.0 . . ?
C84 C85 H85A 120.0 . . ?
C85 C86 C81 120.00(5) . . ?
C85 C86 Se5 115.3(13) . . ?
C81 C86 Se5 124.5(13) . . ?
C85 C86 Se5A 88.8(11) . . ?
C81 C86 Se5A 151.1(12) . . ?
Se5 C86 Se5A 26.7(3) . . ?
C85 C86 H86A 120.0 . . ?
C81 C86 H86A 120.0 . . ?
Se5 C86 H86A 6.0 . . ?
Se5A C86 H86A 31.2 . . ?
C96 C91 C92 112.4(18) . . ?
C96 C91 Sn1 113.2(12) . . ?
C92 C91 Sn1 114.9(13) . . ?
C96 C91 H91A 105.0 . . ?
C92 C91 H91A 105.0 . . ?
Sn1 C91 H91A 105.0 . . ?
C91 C92 C93 113(2) . . ?
C91 C92 H92A 109.0 . . ?
C93 C92 H92A 109.0 . . ?
C91 C92 H92B 109.0 . . ?
C93 C92 H92B 109.0 . . ?
H92A C92 H92B 107.8 . . ?
C94 C93 C92 107(2) . . ?
C94 C93 H93A 110.2 . . ?
C92 C93 H93A 110.2 . . ?
C94 C93 H93B 110.2 . . ?
C92 C93 H93B 110.2 . . ?
H93A C93 H93B 108.5 . . ?
C95 C94 C93 113(2) . . ?
C95 C94 H94A 109.0 . . ?
C93 C94 H94A 109.0 . . ?
C95 C94 H94B 109.0 . . ?
C93 C94 H94B 109.0 . . ?
H94A C94 H94B 107.8 . . ?
C94 C95 C96 113.0(19) . . ?
C94 C95 H95A 109.0 . . ?
C96 C95 H95A 109.0 . . ?
C94 C95 H95B 109.0 . . ?
C96 C95 H95B 109.0 . . ?
H95A C95 H95B 107.8 . . ?
C91 C96 C95 112.0(16) . . ?
C91 C96 H96A 109.2 . . ?
C95 C96 H96A 109.2 . . ?
C91 C96 H96B 109.2 . . ?
C95 C96 H96B 109.2 . . ?
H96A C96 H96B 107.9 . . ?
C112 C111 C116 117.7(14) . . ?
C112 C111 P1 120.8(14) . . ?
C116 C111 P1 121.4(13) . . ?
C113 C112 C111 123.2(17) . . ?
C113 C112 H11B 118.4 . . ?
C111 C112 H11B 118.4 . . ?
C114 C113 C112 118.8(17) . . ?
C114 C113 H11A 120.6 . . ?
C112 C113 H11A 120.6 . . ?
C113 C114 C115 122.1(18) . . ?
C113 C114 H11E 118.9 . . ?
C115 C114 H11E 118.9 . . ?
C114 C115 C116 119.3(18) . . ?
C114 C115 H11C 120.3 . . ?
C116 C115 H11C 120.3 . . ?
C115 C116 C111 118.5(15) . . ?
C115 C116 H11D 120.8 . . ?
C111 C116 H11D 120.8 . . ?
C126 C121 C122 119.8(17) . . ?
C126 C121 P1 118.7(13) . . ?
C122 C121 P1 121.3(16) . . ?
C123 C122 C121 117(2) . . ?
C123 C122 H12D 121.3 . . ?
C121 C122 H12D 121.3 . . ?
C122 C123 C124 123(3) . . ?
C122 C123 H12B 118.3 . . ?
C124 C123 H12B 118.3 . . ?
C123 C124 C125 119(2) . . ?
C123 C124 H12C 120.5 . . ?
C125 C124 H12C 120.5 . . ?
C126 C125 C124 119(2) . . ?
C126 C125 H12E 120.6 . . ?
C124 C125 H12E 120.6 . . ?
C125 C126 C121 120.8(19) . . ?
C125 C126 H12A 119.6 . . ?
C121 C126 H12A 119.6 . . ?
C136 C131 C132 113(2) . . ?
C136 C131 P1 121.2(17) . . ?
C132 C131 P1 125.4(17) . . ?
C131 C132 C133 121(2) . . ?
C131 C132 H13B 119.3 . . ?
C133 C132 H13B 119.3 . . ?
C134 C133 C132 122(2) . . ?
C134 C133 H13A 118.8 . . ?
C132 C133 H13A 118.8 . . ?
C133 C134 C135 117(2) . . ?
C133 C134 H13C 121.4 . . ?
C135 C134 H13C 121.4 . . ?
C134 C135 C136 120(3) . . ?
C134 C135 H13D 120.0 . . ?
C136 C135 H13D 120.0 . . ?
C131 C136 C135 126(3) . . ?
C131 C136 H13E 117.1 . . ?
C135 C136 H13E 117.1 . . ?
C212 C211 C216 120.00(7) . . ?
C211 C212 C213 120.00(5) . . ?
C211 C212 H21A 120.0 . . ?
C213 C212 H21A 120.0 . . ?
C214 C213 C212 120.00(16) . . ?
C214 C213 H21B 120.0 . . ?
C212 C213 H21B 120.0 . . ?
C213 C214 C215 120.00(9) . . ?
C213 C214 H21C 120.0 . . ?
C215 C214 H21C 120.0 . . ?
C216 C215 C214 120.00(7) . . ?
C216 C215 H21D 120.0 . . ?
C214 C215 H21D 120.0 . . ?
C215 C216 C211 120.0(2) . . ?
C215 C216 P2 115(3) . . ?
C211 C216 P2 124(3) . . ?
C215 C216 H21E 120.0 . . ?
C211 C216 H21E 120.0 . . ?
P2 C216 H21E 12.7 . . ?
C222 C221 C226 120.0 . . ?
C221 C222 C223 120.0 . . ?
C221 C222 P2 167.7(17) . . ?
C223 C222 P2 68.8(13) . . ?
C221 C222 H22A 120.0 . . ?
C223 C222 H22A 120.0 . . ?
P2 C222 H22A 52.0 . . ?
C222 C223 C224 120.0 . . ?
C222 C223 P2 72.3(15) . . ?
C224 C223 P2 164.9(13) . . ?
C222 C223 H22B 120.0 . . ?
C224 C223 H22B 120.0 . . ?
P2 C223 H22B 48.5 . . ?
C225 C224 C223 120.0 . . ?
C225 C224 H22C 120.0 . . ?
C223 C224 H22C 120.0 . . ?
C224 C225 C226 120.0 . . ?
C224 C225 H22D 120.0 . . ?
C226 C225 H22D 120.0 . . ?
C225 C226 C221 120.00(5) . . ?
C225 C226 H22E 120.0 . . ?
C221 C226 H22E 120.0 . . ?
C232 C231 C236 120.0 . . ?
C232 C231 P2 117(2) . . ?
C236 C231 P2 123(2) . . ?
C231 C232 C233 120.0 . . ?
C231 C232 H23A 120.0 . . ?
C233 C232 H23A 120.0 . . ?
C234 C233 C232 120.00(7) . . ?
C234 C233 H23B 120.0 . . ?
C232 C233 H23B 120.0 . . ?
C235 C234 C233 120.0 . . ?
C235 C234 H23C 120.0 . . ?
C233 C234 H23C 120.0 . . ?
C234 C235 C236 120.0 . . ?
C234 C235 H23D 120.0 . . ?
C236 C235 H23D 120.0 . . ?
C235 C236 C231 120.00(9) . . ?
C235 C236 H23E 120.0 . . ?
C231 C236 H23E 120.0 . . ?
C10B O10 C10C 125(5) 2 2 ?
C10B O10 C10D 125(5) 2 3 ?
C10B O10 C10A 129(4) 2 . ?
C10B O10 C10D 81(7) 2 . ?
C10A O10 C10D 108.00(10) . . ?
C10C O10 C10C 82(7) 2 3 ?
C10A O10 C10C 116(3) . 3 ?
C10C O10 C10A 108(5) 2 2 ?
C10D O10 C10A 94(3) 3 2 ?
C10A O10 C10A 137.9(16) . 2 ?
O10 C10A C10B 108.01(10) . . ?
O10 C10A O10 92(2) . 3 ?
C10B C10A C10B 108(2) . 2 ?
O10 C10A C10B 95.8(11) 3 2 ?
C10C C10A H10C 127.2 2 . ?
C10D C10A H10C 136.2 3 . ?
O10 C10A H10C 110.1 . . ?
C10B C10A H10C 110.1 . . ?
O10 C10A H10C 126.5 3 . ?
C10B C10A H10C 95.9 2 . ?
C10C C10A H10D 121.6 2 . ?
C10D C10A H10D 113.1 3 . ?
O10 C10A H10D 110.1 . . ?
C10B C10A H10D 110.1 . . ?
O10 C10A H10D 107.9 3 . ?
C10B C10A H10D 123.1 2 . ?
H10C C10A H10D 108.4 . . ?
O10 C10B C10C 87(4) 3 2 ?
O10 C10B C10A 119(5) 3 . ?
C10C C10B C10A 108.0 . . ?
C10A C10B C10D 96(3) . 2 ?
C10C C10B C10A 96.6(15) 2 3 ?
C10A C10B C10A 131(2) . 3 ?
C10D C10B C10A 85(3) 3 3 ?
O10 C10B H10E 125.2 3 . ?
C10C C10B H10E 125.4 2 . ?
C10C C10B H10E 110.1 . . ?
C10A C10B H10E 110.1 . . ?
C10D C10B H10E 123.9 2 . ?
C10D C10B H10E 135.1 3 . ?
C10A C10B H10E 92.7 3 . ?
C10C C10B H10F 121.8 2 . ?
C10C C10B H10F 110.1 . . ?
C10A C10B H10F 110.1 . . ?
C10D C10B H10F 107.8 2 . ?
C10D C10B H10F 116.0 3 . ?
C10A C10B H10F 101.6 3 . ?
H10E C10B H10F 108.5 . . ?
C10D C10C C10A 151(7) 2 3 ?
C10D C10C O10 83(10) 2 3 ?
C10A C10C O10 106(9) 3 3 ?
C10D C10C C10B 98(8) 2 3 ?
O10 C10C C10B 175(5) 3 3 ?
C10D C10C C10B 87(8) 2 . ?
C10A C10C C10B 112(6) 3 . ?
C10B C10C C10B 152.5(15) 3 . ?
C10A C10C C10D 138(6) 3 . ?
O10 C10C C10D 116(4) 3 . ?
C10B C10C C10D 107.99(16) . . ?
C10B C10C C10D 109(5) 3 3 ?
C10A C10C O10 99(4) 3 2 ?
O10 C10C O10 154(6) 3 2 ?
C10B C10C O10 145(3) . 2 ?
C10D C10C O10 86(4) 3 2 ?
C10A C10C C10C 162(5) 3 2 ?
C10B C10C C10C 114(3) 3 2 ?
O10 C10C C10C 94(3) 2 2 ?
C10A C10C C10C 131(6) 3 3 ?
O10 C10C C10C 123(5) 3 3 ?
C10B C10C C10C 110.8(18) . 3 ?
C10D C10C H10G 151.4 2 . ?
O10 C10C H10G 121.5 3 . ?
C10B C10C H10G 110.1 . . ?
C10D C10C H10G 110.1 . . ?
C10D C10C H10G 135.1 3 . ?
O10 C10C H10G 82.1 2 . ?
C10C C10C H10G 127.3 2 . ?
C10C C10C H10G 99.1 3 . ?
C10D C10C H10H 85.4 2 . ?
O10 C10C H10H 87.4 3 . ?
C10B C10C H10H 97.3 3 . ?
C10B C10C H10H 110.1 . . ?
C10D C10C H10H 110.1 . . ?
C10D C10C H10H 115.8 3 . ?
O10 C10C H10H 96.1 2 . ?
C10C C10C H10H 124.2 2 . ?
C10C C10C H10H 117.6 3 . ?
H10G C10C H10H 108.4 . . ?
C10C C10D C10D 126(8) 3 3 ?
O10 C10D C10D 143(4) 2 3 ?
C10C C10D C10D 134(10) 3 2 ?
O10 C10D C10D 83(4) 2 2 ?
O10 C10D C10A 82(5) 2 2 ?
C10D C10D C10A 129(7) 3 2 ?
C10D C10D C10A 154(4) 2 2 ?
C10C C10D O10 94(9) 3 . ?
O10 C10D O10 166(4) 2 . ?
C10D C10D O10 102(3) 2 . ?
C10A C10D O10 89(5) 2 . ?
C10C C10D C10C 122(10) 3 . ?
C10A C10D C10C 142(3) 2 . ?
O10 C10D C10C 108.01(8) . . ?
C10D C10D C10B 123(6) 3 3 ?
C10A C10D C10B 91.8(11) 2 3 ?
O10 C10D C10B 150.6(18) . 3 ?
C10C C10D C10C 115(5) 3 2 ?
O10 C10D C10C 143(4) 2 2 ?
C10A C10D C10C 120(5) 2 2 ?
C10B C10D C10C 122(5) 3 2 ?
O10 C10D C10B 141(4) 2 2 ?
C10D C10D C10B 121(5) 2 2 ?
C10C C10D C10B 122(2) . 2 ?
C10B C10D C10B 135.95(9) 3 2 ?
C10C C10D H10I 111.5 3 . ?
C10D C10D H10I 112.7 3 . ?
C10D C10D H10I 103.0 2 . ?
C10A C10D H10I 94.9 2 . ?
O10 C10D H10I 110.1 . . ?
C10C C10D H10I 110.1 . . ?
C10B C10D H10I 99.1 3 . ?
C10C C10D H10I 122.5 2 . ?
C10B C10D H10I 117.7 2 . ?
C10D C10D H10J 136.7 3 . ?
C10D C10D H10J 122.7 2 . ?
O10 C10D H10J 110.1 . . ?
C10C C10D H10J 110.1 . . ?
C10C C10D H10J 125.8 2 . ?
C10B C10D H10J 83.7 2 . ?
H10I C10D H10J 108.4 . . ?
C11D O11 C11A 121.98(5) . . ?
O11 C11A C11B 97.36(12) . . ?
O11 C11A H11F 112.3 . . ?
C11B C11A H11F 112.3 . . ?
O11 C11A H11G 112.3 . . ?
C11B C11A H11G 112.3 . . ?
H11F C11A H11G 109.9 . . ?
C11C C11B C11A 109.88(9) . . ?
C11C C11B H11H 109.7 . . ?
C11A C11B H11H 109.7 . . ?
C11C C11B H11I 109.7 . . ?
C11A C11B H11I 109.7 . . ?
H11H C11B H11I 108.2 . . ?
C11B C11C C11D 110.9 . . ?
C11B C11C H11J 109.5 . . ?
C11D C11C H11J 109.5 . . ?
C11B C11C H11K 109.5 . . ?
C11D C11C H11K 109.5 . . ?
H11J C11C H11K 108.1 . . ?
O11 C11D C11C 97.0 . . ?
O11 C11D H11L 112.3 . . ?
C11C C11D H11L 112.3 . . ?
O11 C11D H11M 112.3 . . ?
C11C C11D H11M 112.3 . . ?
H11L C11D H11M 109.9 . . ?
C12D O12 C12A 123(10) 3_665 2_655 ?
C12A O12 C12B 106(10) 2_655 2_655 ?
C12D O12 C12C 124(10) 3_665 3_665 ?
C12B O12 C12C 112(8) 2_655 3_665 ?
C12D O12 O12 153(10) 3_665 2_655 ?
C12A O12 O12 81(10) 2_655 2_655 ?
C12B O12 O12 172(10) 2_655 2_655 ?
C12D O12 O12 97(10) 3_665 3_665 ?
C12A O12 O12 140(10) 2_655 3_665 ?
C12B O12 O12 112(10) 2_655 3_665 ?
C12C O12 O12 135(10) 3_665 3_665 ?
C12B O12 C12A 80(10) 2_655 . ?
C12C O12 C12A 168(10) 3_665 . ?
O12 O12 C12A 93(10) 2_655 . ?
C12D O12 C12D 159(10) 3_665 . ?
C12B O12 C12D 172(10) 2_655 . ?
C12A O12 C12D 108.0(3) . . ?
C12A O12 C12C 170(10) 2_655 2_655 ?
O12 O12 C12C 108(10) 2_655 2_655 ?
C12D O12 C12C 122(9) . 2_655 ?
C12D O12 C12D 101(10) 3_665 2_655 ?
C12A O12 C12D 136(10) 2_655 2_655 ?
C12B O12 C12D 117(10) 2_655 2_655 ?
C12C O12 C12D 130(10) 3_665 2_655 ?
C12C C12A C12D 80(10) 2_655 3_665 ?
O12 C12A C12D 81(10) 3_665 3_665 ?
C12D C12A C12D 97(10) 2_655 3_665 ?
C12D C12A C12B 122(10) 3_665 . ?
C12C C12A O12 95(10) 2_655 . ?
C12D C12A O12 84(10) 2_655 . ?
C12B C12A O12 108.0(2) . . ?
O12 C12A C12B 104(9) 3_665 2_655 ?
C12D C12A C12B 121(10) 2_655 2_655 ?
C12B C12A C12B 146(8) . 2_655 ?
O12 C12A H12F 127.9 3_665 . ?
C12D C12A H12F 128.0 2_655 . ?
C12D C12A H12F 107.2 3_665 . ?
C12B C12A H12F 110.1 . . ?
O12 C12A H12F 110.1 . . ?
C12B C12A H12F 88.9 2_655 . ?
C12D C12A H12G 97.5 3_665 . ?
C12B C12A H12G 110.1 . . ?
O12 C12A H12G 110.1 . . ?
C12B C12A H12G 88.8 2_655 . ?
H12F C12A H12G 108.4 . . ?
C12A C12B C12C 108.0(2) . . ?
C12A C12B C12A 94(7) . 3_665 ?
C12C C12B C12C 113(8) . 2_655 ?
C12A C12B C12C 100(4) 3_665 2_655 ?
O12 C12B H12H 125.2 3_665 . ?
C12A C12B H12H 110.1 . . ?
C12A C12B H12H 110.7 3_665 . ?
C12C C12B H12H 112.8 2_655 . ?
C12D C12B H12I 112.0 2_655 . ?
O12 C12B H12I 120.4 3_665 . ?
C12A C12B H12I 110.1 . . ?
C12C C12B H12I 110.1 . . ?
C12A C12B H12I 122.5 3_665 . ?
C12C C12B H12I 102.2 2_655 . ?
H12H C12B H12I 108.4 . . ?
C12A C12C C12D 81(10) 3_665 2_655 ?
C12D C12C C12D 81(9) 2_655 . ?
C12A C12C C12B 103(10) 3_665 . ?
O12 C12C C12B 96(10) 2_655 . ?
C12D C12C C12B 108.0(4) . . ?
C12D C12C C12B 100(5) 2_655 3_665 ?
C12B C12C C12B 126(9) . 3_665 ?
O12 C12C C12B 87(9) 3_665 3_665 ?
C12B C12C H12J 94.4 3_665 . ?
H12J C12C H12K 108.4 . . ?
C12B C12D C12A 112(10) 3_665 3_665 ?
O12 C12D C12C 116(10) 2_655 3_665 ?
C12B C12D C12C 86(10) 3_665 3_665 ?
C12A C12D C12C 154(10) 3_665 3_665 ?
O12 C12D C12A 97(10) 2_655 2_655 ?
C12B C12D C12A 100(10) 3_665 2_655 ?
C12A C12D C12A 136(10) 3_665 2_655 ?
C12B C12D C12C 114(10) 3_665 . ?
C12C C12D C12C 158(10) 3_665 . ?
C12A C12D C12C 140(10) 2_655 . ?
C12B C12D O12 133(10) 3_665 . ?
C12A C12D O12 106(10) 3_665 . ?
C12C C12D O12 108.0(5) . . ?
C12C C12D O12 100(10) 3_665 3_665 ?
C12A C12D O12 82(10) 2_655 3_665 ?
C12B C12D C12D 157(10) 3_665 2_655 ?
C12C C12D C12D 112(9) 3_665 2_655 ?
C12A C12D C12D 94(10) 2_655 2_655 ?
C12B C12D C12D 136(10) 3_665 3_665 ?
C12A C12D C12D 106(10) 3_665 3_665 ?
C12C C12D C12D 107(5) . 3_665 ?
O12 C12D H12L 136.0 2_655 . ?
C12A C12D H12L 119.3 3_665 . ?
C12A C12D H12L 98.0 2_655 . ?
C12C C12D H12L 110.1 . . ?
O12 C12D H12L 110.1 . . ?
O12 C12D H12L 124.2 3_665 . ?
C12D C12D H12L 120.8 2_655 . ?
C12D C12D H12L 107.0 3_665 . ?
C12A C12D H12M 102.2 3_665 . ?
C12C C12D H12M 80.5 3_665 . ?
C12A C12D H12M 86.3 2_655 . ?
O12 C12D H12M 110.1 . . ?
O12 C12D H12M 127.1 3_665 . ?
C12D C12D H12M 130.1 2_655 . ?
C12D C12D H12M 114.4 3_665 . ?
H12L C12D H12M 108.4 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 P1 2.475(5) . ?
Ag1 Se1A 2.51(4) . ?
Ag1 Se2 2.671(2) . ?
Ag1 Se1 2.687(2) . ?
Ag1 Se1 2.778(2) 18_546 ?
Ag1 Se2A 2.85(4) . ?
Ag1 Se1A 2.92(4) 18_546 ?
Ag1 Ag3 3.1099(19) . ?
Ag1 Ag3 3.2149(18) 17_556 ?
Ag1 Ag3A 3.35(3) . ?
Ag2 Ag2A 0.54(6) . ?
Ag2 P4 2.441(9) . ?
Ag2 Se2A 2.62(4) 2_655 ?
Ag2 Se2A 2.62(4) . ?
Ag2 Se2A 2.62(4) 3_665 ?
Ag2 Se2 2.694(2) 2_655 ?
Ag2 Se2 2.694(2) . ?
Ag2 Se2 2.694(2) 3_665 ?
Ag2 Ag3A 3.00(3) . ?
Ag2 Ag3A 3.00(3) 2_655 ?
Ag2 Ag3A 3.00(3) 3_665 ?
Ag2A P4 1.90(7) . ?
Ag2A Se2A 2.75(4) 2_655 ?
Ag2A Se2A 2.75(4) . ?
Ag2A Se2A 2.75(4) 3_665 ?
Ag2A Se2 3.00(4) 2_655 ?
Ag2A Se2 3.00(4) . ?
Ag2A Se2 3.00(4) 3_665 ?
Ag3 Ag3A 1.27(3) 17_556 ?
Ag3 Se1A 1.41(4) 18_546 ?
Ag3 Se1 2.530(2) 18_546 ?
Ag3 Se2 2.544(2) 17_556 ?
Ag3 Se3 2.9402(14) . ?
Ag3 Ag1 3.2150(18) 18_546 ?
Ag3A Ag3 1.27(3) 18_546 ?
Ag3A Se2 1.32(3) . ?
Ag3A Se2A 2.56(5) . ?
Ag3A Se1A 2.62(5) 2_655 ?
Ag3A Se3 2.87(3) . ?
Ag4 P3 2.493(8) . ?
Ag4 Se5A 2.625(6) 3 ?
Ag4 Se5A 2.625(6) 2 ?
Ag4 Se5A 2.625(6) . ?
Ag4 Se5 2.800(3) 3 ?
Ag4 Se5 2.800(3) 2 ?
Ag4 Se5 2.800(3) . ?
Ag4 Ag6 3.157(3) 3 ?
Ag4 Ag6 3.157(3) . ?
Ag4 Ag6 3.157(3) 2 ?
Ag5 P2 2.450(7) 10_557 ?
Ag5 Se5 2.681(3) 10_557 ?
Ag5 Se4 2.700(4) 11_557 ?
Ag5 Se4A 2.716(7) 11_557 ?
Ag5 Se4 2.720(3) . ?
Ag5 Se4A 2.740(7) . ?
Ag5 Se5A 2.845(7) 10_557 ?
Ag5 Ag6A 3.133(5) . ?
Ag5 Ag6A 3.317(6) 11_557 ?
Ag6 Ag6A 1.104(6) . ?
Ag6 Se5A 1.470(8) 2 ?
Ag6 Se5 2.520(4) 2 ?
Ag6 Se4 2.549(4) . ?
Ag6 Se6 2.783(2) . ?
Ag6A Se4 1.509(6) . ?
Ag6A Se4A 2.532(9) . ?
Ag6A Se5A 2.553(10) 2 ?
Ag6A Se6 2.803(5) . ?
Ag6A Ag5 3.317(6) 12_557 ?
Se1 Se1A 1.19(4) . ?
Se1 C51 1.964(18) . ?
Se1 Ag3 2.529(2) 17_556 ?
Se1 Ag1 2.778(2) 17_556 ?
Se1A Ag3 1.41(4) 17_556 ?
Se1A C51 2.34(4) . ?
Se1A Ag3A 2.62(5) 3_665 ?
Se1A Ag1 2.92(4) 17_556 ?
Se2 Se2A 1.27(4) . ?
Se2 C61 1.931(19) . ?
Se2 Ag3 2.544(2) 18_546 ?
Se2A C61 1.87(4) . ?
Se2A C66 2.08(4) . ?
Se3 Ag3A 2.87(3) 2_655 ?
Se3 Ag3A 2.87(3) 3_665 ?
Se3 Ag3A 2.87(3) 16_656 ?
Se3 Ag3A 2.88(3) 17_556 ?
Se3 Ag3A 2.88(3) 18_546 ?
Se3 Ag3 2.9400(14) 17_556 ?
Se3 Ag3 2.9401(14) 16_656 ?
Se3 Ag3 2.9401(14) 18_546 ?
Se3 Ag3 2.9402(14) 2_655 ?
Se3 Ag3 2.9402(14) 3_665 ?
Se4 Se4A 1.045(7) . ?
Se4 C71 1.901(5) . ?
Se4 Ag5 2.700(4) 12_557 ?
Se4A C71 1.91(3) . ?
Se4A Ag5 2.716(6) 12_557 ?
Se5 Se5A 1.060(7) . ?
Se5 C86 1.849(17) . ?
Se5 Ag6 2.520(4) 3 ?
Se5 Ag5 2.681(3) 10_557 ?
Se5A Ag6 1.470(8) 3 ?
Se5A C86 2.312(19) . ?
Se5A Ag6A 2.553(10) 3 ?
Se5A Ag5 2.845(6) 10_557 ?
Se6 Ag6 2.783(2) 11_557 ?
Se6 Ag6 2.783(2) 2 ?
Se6 Ag6 2.783(2) 12_557 ?
Se6 Ag6 2.783(2) 10_557 ?
Se6 Ag6 2.783(2) 3 ?
Se6 Ag6A 2.803(5) 11_557 ?
Se6 Ag6A 2.803(5) 2 ?
Se6 Ag6A 2.803(5) 12_557 ?
Se6 Ag6A 2.803(5) 3 ?
Se6 Ag6A 2.803(5) 10_557 ?
P1 C131 1.77(2) . ?
P1 C121 1.823(17) . ?
P1 C111 1.828(16) . ?
P2 C231 1.86(3) . ?
P2 C216 1.88(3) . ?
P2 C223 2.06(4) . ?
P2 C222 2.11(4) . ?
P2 Ag5 2.450(7) 10_557 ?
P3 C31 1.932(15) 3 ?
P3 C31 1.932(15) 2 ?
P3 C31 1.932(15) . ?
P4 C41 1.930(15) 2_655 ?
P4 C41 1.930(15) 3_665 ?
P4 C41 1.930(15) . ?
Sn1 C91 2.145(18) . ?
Sn1 C91 2.145(18) 3_565 ?
Sn1 C91 2.145(18) 2_665 ?
Sn1 Cl1 2.565(9) . ?
Sn1 Cl2 2.81(4) 2_665 ?
Sn1 Cl2 2.81(4) 3_565 ?
Sn1 Cl2 2.81(4) . ?
Cl2 Cl2 0.91(10) 3_565 ?
Cl2 Cl2 0.91(10) 2_665 ?
C31 C36 1.32(2) . ?
C31 C32 1.34(2) . ?
C32 C33 1.36(3) . ?
C32 H32A 0.9500 . ?
C33 C34 1.42(3) . ?
C33 H33A 0.9500 . ?
C34 C35 1.37(3) . ?
C34 H34A 0.9500 . ?
C35 C36 1.39(3) . ?
C35 H35A 0.9500 . ?
C36 H36A 0.9500 . ?
C41 C46 1.31(3) . ?
C41 C42 1.40(3) . ?
C42 C43 1.31(4) . ?
C42 H42A 0.9500 . ?
C43 C44 1.56(5) . ?
C43 H43A 0.9500 . ?
C44 C45 1.23(4) . ?
C44 H44A 0.9500 . ?
C45 C46 1.35(3) . ?
C45 H45A 0.9500 . ?
C46 H46A 0.9500 . ?
C51 C52 1.34(2) . ?
C51 C56 1.41(2) . ?
C52 C53 1.40(2) . ?
C52 H52A 0.9500 . ?
C53 C54 1.31(3) . ?
C53 H53A 0.9500 . ?
C54 C55 1.37(3) . ?
C54 H54A 0.9500 . ?
C55 C56 1.33(3) . ?
C55 H55A 0.9500 . ?
C56 H56A 0.9500 . ?
C61 C66 1.37(3) . ?
C61 C62 1.43(3) . ?
C62 C63 1.38(3) . ?
C62 H62A 0.9500 . ?
C63 C64 1.40(3) . ?
C63 H63A 0.9500 . ?
C64 C65 1.43(3) . ?
C64 H64A 0.9500 . ?
C65 C66 1.44(3) . ?
C65 H65A 0.9500 . ?
C66 H66A 0.9500 . ?
C71 C72 1.390(3) . ?
C71 C76 1.390(2) . ?
C72 C73 1.3900 . ?
C72 H72A 0.9500 . ?
C73 C74 1.390(4) . ?
C73 H73A 0.9500 . ?
C74 C75 1.390(3) . ?
C74 H74A 0.9500 . ?
C75 C76 1.3900 . ?
C75 H75A 0.9500 . ?
C76 H76A 0.9500 . ?
C81 C82 1.3900(10) . ?
C81 C86 1.3900 . ?
C82 C83 1.3900(13) . ?
C82 H82A 0.9500 . ?
C83 C84 1.3900 . ?
C83 H83A 0.9500 . ?
C84 C85 1.3900 . ?
C84 H84A 0.9500 . ?
C85 C86 1.3900(12) . ?
C85 H85A 0.9500 . ?
C86 H86A 0.9500 . ?
C91 C96 1.52(2) . ?
C91 C92 1.52(3) . ?
C91 H91A 1.0000 . ?
C92 C93 1.55(3) . ?
C92 H92A 0.9900 . ?
C92 H92B 0.9900 . ?
C93 C94 1.51(3) . ?
C93 H93A 0.9900 . ?
C93 H93B 0.9900 . ?
C94 C95 1.47(3) . ?
C94 H94A 0.9900 . ?
C94 H94B 0.9900 . ?
C95 C96 1.53(3) . ?
C95 H95A 0.9900 . ?
C95 H95B 0.9900 . ?
C96 H96A 0.9900 . ?
C96 H96B 0.9900 . ?
C111 C112 1.38(2) . ?
C111 C116 1.42(2) . ?
C112 C113 1.35(2) . ?
C112 H11B 0.9500 . ?
C113 C114 1.35(2) . ?
C113 H11A 0.9500 . ?
C114 C115 1.38(2) . ?
C114 H11E 0.9500 . ?
C115 C116 1.40(2) . ?
C115 H11C 0.9500 . ?
C116 H11D 0.9500 . ?
C121 C126 1.39(2) . ?
C121 C122 1.40(2) . ?
C122 C123 1.35(3) . ?
C122 H12D 0.9500 . ?
C123 C124 1.36(4) . ?
C123 H12B 0.9500 . ?
C124 C125 1.39(4) . ?
C124 H12C 0.9500 . ?
C125 C126 1.36(3) . ?
C125 H12E 0.9500 . ?
C126 H12A 0.9500 . ?
C131 C136 1.30(3) . ?
C131 C132 1.40(3) . ?
C132 C133 1.42(3) . ?
C132 H13B 0.9500 . ?
C133 C134 1.30(3) . ?
C133 H13A 0.9500 . ?
C134 C135 1.36(3) . ?
C134 H13C 0.9500 . ?
C135 C136 1.40(4) . ?
C135 H13D 0.9500 . ?
C136 H13E 0.9500 . ?
C211 C212 1.390(3) . ?
C211 C216 1.3900 . ?
C212 C213 1.3900(13) . ?
C212 H21A 0.9500 . ?
C213 C214 1.3900 . ?
C213 H21B 0.9500 . ?
C214 C215 1.390(2) . ?
C214 H21C 0.9500 . ?
C215 C216 1.3900 . ?
C215 H21D 0.9500 . ?
C216 H21E 0.9500 . ?
C221 C222 1.3900 . ?
C221 C226 1.3900 . ?
C222 C223 1.3900 . ?
C222 H22A 0.9500 . ?
C223 C224 1.3900 . ?
C223 H22B 0.9500 . ?
C224 C225 1.3900 . ?
C224 H22C 0.9500 . ?
C225 C226 1.3900 . ?
C225 H22D 0.9500 . ?
C226 H22E 0.9500 . ?
C231 C232 1.3900 . ?
C231 C236 1.3900 . ?
C232 C233 1.3900 . ?
C232 H23A 0.9500 . ?
C233 C234 1.3900 . ?
C233 H23B 0.9500 . ?
C234 C235 1.3900 . ?
C234 H23C 0.9500 . ?
C235 C236 1.3900 . ?
C235 H23D 0.9500 . ?
C236 H23E 0.9500 . ?
O10 C10B 0.67(6) 2 ?
O10 C10D 0.96(6) 3 ?
O10 C10A 1.4199 . ?
O10 C10D 1.420(2) . ?
O10 C10C 1.49(5) 3 ?
O10 C10A 1.83(9) 2 ?
C10A C10C 0.85(6) 2 ?
C10A C10D 1.20(5) 3 ?
C10A C10B 1.4202 . ?
C10A H10C 0.9605 . ?
C10A H10D 0.9600 . ?
C10B C10C 1.37(5) 2 ?
C10B C10C 1.4200(11) . ?
C10B C10D 1.45(5) 2 ?
C10B C10D 1.47(6) 3 ?
C10B H10E 0.9600 . ?
C10B H10F 0.9603 . ?
C10C C10B 1.37(9) 3 ?
C10C C10D 1.4202 . ?
C10C C10D 1.45(6) 3 ?
C10C O10 1.49(5) 2 ?
C10C C10C 1.65(6) 2 ?
C10C C10C 1.65(9) 3 ?
C10C H10G 0.9595 . ?
C10C H10H 0.9601 . ?
C10D C10B 1.45(5) 3 ?
C10D C10C 1.45(6) 2 ?
C10D C10B 1.47(7) 2 ?
C10D H10I 0.9600 . ?
C10D H10J 0.9599 . ?
O11 C11D 1.4698(15) . ?
O11 C11A 1.473(2) . ?
C11A C11B 1.4960 . ?
C11A H11F 0.9900 . ?
C11A H11G 0.9900 . ?
C11B C11C 1.492(3) . ?
C11B H11H 0.9900 . ?
C11B H11I 0.9900 . ?
C11C C11D 1.5010(11) . ?
C11C H11J 0.9900 . ?
C11C H11K 0.9900 . ?
C11D H11L 0.9900 . ?
C11D H11M 0.9900 . ?
O12 O12 1.35(14) 2_655 ?
O12 O12 1.35(13) 3_665 ?
O12 C12A 1.450(3) . ?
O12 C12D 1.450(10) . ?
C12A C12D 1.35(15) 3_665 ?
C12A C12B 1.450(3) . ?
C12A C12B 1.6(3) 2_655 ?
C12A H12G 0.9604 . ?
C12B C12C 1.450(9) . ?
C12B C12A 1.6(2) 3_665 ?
C12B H12H 0.9599 . ?
C12B H12I 0.9605 . ?
C12C C12D 1.4499 . ?
C12D C12A 1.35(14) 2_655 ?
C12D H12L 0.9598 . ?
C12D H12M 0.9604 . ?
