#------------------------------------------------------------------------------
#$Date: 2016-03-23 02:57:22 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179221 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/45/4314518.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4314518
loop_
_publ_author_name
'C. W. Liu'
'Hao-Wei Chang'
'Bijay Sarkar'
'Jean-Yves Saillard'
'Samia Kahlal'
'Ying-Yann Wu'
_publ_section_title
;
 Stable Silver(I) Hydride Complexes Supported by Diselenophosphate Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              468
_journal_page_last               475
_journal_paper_doi               10.1021/ic901408n
_journal_volume                  49
_journal_year                    2010
_chemical_formula_sum            'C36 H85 Ag8 F6 O12 P7 Se12'
_chemical_formula_weight         2851.31
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                116.883(2)
_cell_angle_beta                 99.052(2)
_cell_angle_gamma                95.746(2)
_cell_formula_units_Z            1
_cell_length_a                   13.048(2)
_cell_length_b                   13.1199(12)
_cell_length_c                   13.8959(13)
_cell_measurement_reflns_used    7251
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.33
_cell_measurement_theta_min      2.37
_cell_volume                     2055.3(4)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.968
_diffrn_measured_fraction_theta_max 0.968
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0489
_diffrn_reflns_av_sigmaI/netI    0.0738
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            21308
_diffrn_reflns_theta_full        28.48
_diffrn_reflns_theta_max         28.48
_diffrn_reflns_theta_min         1.61
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    7.368
_exptl_absorpt_correction_T_max  0.6662
_exptl_absorpt_correction_T_min  0.1260
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.304
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1340
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.185
_refine_diff_density_min         -1.255
_refine_diff_density_rms         0.207
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.025
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     416
_refine_ls_number_reflns         10080
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.1067
_refine_ls_R_factor_gt           0.0565
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0818P)²+5.2510P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1441
_refine_ls_wR_factor_ref         0.1793
_reflns_number_gt                6202
_reflns_number_total             10080
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic901408n_si_001_1.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        2055.4(5)
_cod_database_code               4314518
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.41458(11) 0.36898(12) -0.12749(11) 0.0529(3) Uani 0.50 1 d P . .
Ag5 Ag 0.35442(11) 0.29030(12) -0.21272(11) 0.0538(3) Uani 0.50 1 d P . .
Ag2 Ag 0.49947(11) 0.35447(14) 0.01752(10) 0.0551(3) Uani 0.50 1 d P . .
Ag6 Ag 0.50552(10) 0.28248(12) 0.02941(10) 0.0480(3) Uani 0.50 1 d P . .
Ag3 Ag 0.35469(13) 0.52394(12) -0.02301(10) 0.0529(3) Uani 0.50 1 d P . .
Ag7 Ag 0.27430(12) 0.53919(13) -0.03176(11) 0.0547(3) Uani 0.50 1 d P . .
Ag4 Ag 0.44901(11) 0.52182(11) 0.12525(10) 0.0508(3) Uani 0.50 1 d P . .
Ag8 Ag 0.40997(12) 0.53826(11) 0.20038(10) 0.0534(3) Uani 0.50 1 d P . .
Se1 Se 0.19926(7) 0.32493(9) -0.12944(8) 0.0585(3) Uani 1 1 d . . .
Se2 Se 0.35001(7) 0.32195(7) 0.12335(6) 0.0472(2) Uani 1 1 d . . .
Se3 Se 0.46404(7) 0.15374(7) -0.17988(7) 0.0507(2) Uani 1 1 d . . .
Se5 Se 0.40868(9) 0.37446(9) -0.32734(7) 0.0627(3) Uani 1 1 d . . .
Se4 Se 0.29104(8) 0.65919(8) 0.16995(8) 0.0624(3) Uani 1 1 d . . .
Se6 Se 0.69110(8) 0.36080(9) 0.14396(7) 0.0600(3) Uani 1 1 d . . .
P1 P 0.21584(16) 0.25187(18) -0.01687(16) 0.0419(4) Uani 1 1 d . . .
P2 P 0.62043(17) 0.17246(17) -0.21004(15) 0.0419(4) Uani 1 1 d . . .
P3 P 0.6759(2) 0.4864(2) 0.30589(18) 0.0658(7) Uani 1 1 d . . .
P4 P 1.0000 0.0000 0.5000 0.158(3) Uani 1 2 d S . .
F1 F 0.9023(10) -0.0929(14) 0.4210(11) 0.209(6) Uani 1 1 d . . .
F2 F 0.9556(12) 0.005(2) 0.5980(12) 0.283(11) Uani 1 1 d . . .
F3 F 0.9328(15) 0.0909(17) 0.498(2) 0.309(13) Uani 1 1 d . . .
O1 O 0.2185(4) 0.1187(4) -0.0807(4) 0.0493(13) Uani 1 1 d . . .
O2 O 0.6020(5) 0.0848(5) -0.3378(4) 0.0580(15) Uani 1 1 d . . .
O3 O 0.6967(5) 0.1289(5) -0.1441(5) 0.0544(14) Uani 1 1 d . . .
O4 O 0.1105(5) 0.2524(6) 0.0261(5) 0.0627(16) Uani 1 1 d . . .
O5 O 0.7836(9) 0.5361(9) 0.3860(10) 0.158(6) Uani 1 1 d . . .
O6 O 0.6130(11) 0.4173(10) 0.3530(8) 0.138(4) Uani 1 1 d . . .
C1 C 0.1436(9) 0.0344(9) -0.1863(8) 0.073(3) Uani 1 1 d . . .
H1 H 0.1184 0.0740 -0.2280 0.088 Uiso 1 1 calc R . .
C2 C 0.6863(9) 0.0618(9) -0.3996(8) 0.072(3) Uani 1 1 d . . .
H2 H 0.7560 0.0918 -0.3485 0.086 Uiso 1 1 calc R . .
C3 C 0.2007(11) -0.0542(13) -0.2495(11) 0.119(5) Uani 1 1 d . . .
H3A H 0.2039 -0.1093 -0.2219 0.178 Uiso 1 1 calc R . .
H3B H 0.2712 -0.0177 -0.2418 0.178 Uiso 1 1 calc R . .
H3C H 0.1646 -0.0939 -0.3263 0.178 Uiso 1 1 calc R . .
C4 C 0.7708(12) -0.0361(14) -0.1685(14) 0.116(5) Uani 1 1 d . . .
H4A H 0.7964 -0.0245 -0.2246 0.174 Uiso 1 1 calc R . .
H4B H 0.7541 -0.1180 -0.1920 0.174 Uiso 1 1 calc R . .
H4C H 0.8243 0.0016 -0.1007 0.174 Uiso 1 1 calc R . .
C5 C 0.6744(8) 0.0143(9) -0.1501(9) 0.069(3) Uani 1 1 d . . .
H5 H 0.6158 -0.0354 -0.2140 0.083 Uiso 1 1 calc R . .
C6 C 0.6425(13) 0.0270(12) -0.0472(11) 0.106(5) Uani 1 1 d . . .
H6A H 0.7001 0.0737 0.0157 0.160 Uiso 1 1 calc R . .
H6B H 0.6245 -0.0485 -0.0528 0.160 Uiso 1 1 calc R . .
H6C H 0.5822 0.0641 -0.0385 0.160 Uiso 1 1 calc R . .
C7 C 0.6743(15) 0.1211(13) -0.4696(11) 0.123(6) Uani 1 1 d . . .
H7A H 0.6137 0.0790 -0.5303 0.185 Uiso 1 1 calc R . .
H7B H 0.7365 0.1232 -0.4979 0.185 Uiso 1 1 calc R . .
H7C H 0.6648 0.1992 -0.4256 0.185 Uiso 1 1 calc R . .
C8 C 0.0566(15) -0.0149(19) -0.1595(16) 0.226(15) Uani 1 1 d . . .
H8A H 0.0823 -0.0519 -0.1172 0.339 Uiso 1 1 calc R . .
H8B H 0.0075 -0.0714 -0.2265 0.339 Uiso 1 1 calc R . .
H8C H 0.0218 0.0457 -0.1167 0.339 Uiso 1 1 calc R . .
C9 C 0.0731(10) 0.3576(12) 0.0890(11) 0.090(4) Uani 1 1 d . . .
H9 H 0.1223 0.4250 0.0989 0.108 Uiso 1 1 calc R . .
C10 C -0.0298(12) 0.3528(19) 0.0305(17) 0.161(8) Uani 1 1 d . . .
H10A H -0.0260 0.3438 -0.0413 0.241 Uiso 1 1 calc R . .
H10B H -0.0538 0.4236 0.0716 0.241 Uiso 1 1 calc R . .
H10C H -0.0784 0.2878 0.0221 0.241 Uiso 1 1 calc R . .
C11 C 0.8573(11) 0.6478(11) 0.4270(10) 0.095(4) Uani 1 1 d . . .
H11 H 0.8245 0.6967 0.3999 0.114 Uiso 1 1 calc R . .
C12 C 0.8736(18) 0.7006(18) 0.5439(12) 0.176(9) Uani 1 1 d . . .
H12A H 0.8788 0.6423 0.5672 0.264 Uiso 1 1 calc R . .
H12B H 0.8153 0.7373 0.5663 0.264 Uiso 1 1 calc R . .
H12C H 0.9379 0.7580 0.5773 0.264 Uiso 1 1 calc R . .
C13 C 0.074(2) 0.364(2) 0.2009(16) 0.223(14) Uani 1 1 d . . .
H13A H 0.0574 0.4376 0.2495 0.334 Uiso 1 1 calc R . .
H13B H 0.1421 0.3581 0.2321 0.334 Uiso 1 1 calc R . .
H13C H 0.0213 0.3019 0.1920 0.334 Uiso 1 1 calc R . .
C14 C 0.6685(12) -0.0677(11) -0.4674(12) 0.119(6) Uani 1 1 d . . .
H14A H 0.6787 -0.1018 -0.4191 0.179 Uiso 1 1 calc R . .
H14B H 0.7178 -0.0881 -0.5144 0.179 Uiso 1 1 calc R . .
H14C H 0.5976 -0.0966 -0.5121 0.179 Uiso 1 1 calc R . .
C15 C 0.614(3) 0.367(3) 0.398(2) 0.41(3) Uani 1 1 d . . .
H15 H 0.6688 0.3274 0.3646 0.490 Uiso 1 1 calc R . .
C16 C 0.676(3) 0.404(3) 0.512(2) 0.34(3) Uani 1 1 d . . .
H16A H 0.7497 0.4088 0.5122 0.508 Uiso 1 1 calc R . .
H16B H 0.6539 0.3481 0.5353 0.508 Uiso 1 1 calc R . .
H16C H 0.6638 0.4788 0.5622 0.508 Uiso 1 1 calc R . .
C17 C 0.9543(19) 0.625(3) 0.389(2) 0.243(15) Uani 1 1 d . . .
H17A H 0.9738 0.6762 0.3600 0.365 Uiso 1 1 calc R . .
H17B H 0.9433 0.5457 0.3320 0.365 Uiso 1 1 calc R . .
H17C H 1.0099 0.6383 0.4500 0.365 Uiso 1 1 calc R . .
C18 C 0.545(3) 0.262(2) 0.359(2) 0.29(2) Uani 1 1 d . . .
H18A H 0.4796 0.2767 0.3802 0.429 Uiso 1 1 calc R . .
H18B H 0.5759 0.2165 0.3893 0.429 Uiso 1 1 calc R . .
H18C H 0.5328 0.2205 0.2795 0.429 Uiso 1 1 calc R . .
H0 H 0.5000 0.5000 0.0000 0.02(2) Uiso 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag5 Ag1 Ag4 124.26(10) . 2_665 ?
Ag5 Ag1 Ag3 119.16(12) . . ?
Ag4 Ag1 Ag3 90.66(7) 2_665 . ?
Ag5 Ag1 Ag2 127.07(11) . . ?
Ag4 Ag1 Ag2 92.80(8) 2_665 . ?
Ag3 Ag1 Ag2 93.49(7) . . ?
Ag5 Ag1 Se3 67.62(9) . . ?
Ag4 Ag1 Se3 107.62(6) 2_665 . ?
Ag3 Ag1 Se3 152.26(6) . . ?
Ag2 Ag1 Se3 65.61(5) . . ?
Ag5 Ag1 Se5 61.34(8) . . ?
Ag4 Ag1 Se5 66.03(5) 2_665 . ?
Ag3 Ag1 Se5 105.24(6) . . ?
Ag2 Ag1 Se5 151.37(7) . . ?
Se3 Ag1 Se5 101.28(5) . . ?
Ag5 Ag1 Se1 61.55(9) . . ?
Ag4 Ag1 Se1 150.72(7) 2_665 . ?
Ag3 Ag1 Se1 65.63(6) . . ?
Ag2 Ag1 Se1 105.01(6) . . ?
Se3 Ag1 Se1 100.92(5) . . ?
Se5 Ag1 Se1 102.41(5) . . ?
Ag5 Ag1 Ag7 102.75(10) . . ?
Ag4 Ag1 Ag7 102.57(7) 2_665 . ?
Ag3 Ag1 Ag7 16.49(5) . . ?
Ag2 Ag1 Ag7 104.01(6) . . ?
Se3 Ag1 Ag7 148.33(6) . . ?
Se5 Ag1 Ag7 99.49(5) . . ?
Se1 Ag1 Ag7 51.02(4) . . ?
Ag5 Ag1 Ag8 106.29(9) . 2_665 ?
Ag4 Ag1 Ag8 18.38(4) 2_665 2_665 ?
Ag3 Ag1 Ag8 104.61(7) . 2_665 ?
Ag2 Ag1 Ag8 103.53(7) . 2_665 ?
Se3 Ag1 Ag8 98.21(5) . 2_665 ?
Se5 Ag1 Ag8 51.26(4) . 2_665 ?
Se1 Ag1 Ag8 150.28(6) . 2_665 ?
Ag7 Ag1 Ag8 113.45(6) . 2_665 ?
Ag5 Ag1 Ag6 112.16(10) . . ?
Ag4 Ag1 Ag6 102.63(7) 2_665 . ?
Ag3 Ag1 Ag6 104.44(6) . . ?
Ag2 Ag1 Ag6 14.99(5) . . ?
Se3 Ag1 Ag6 52.05(4) . . ?
Se5 Ag1 Ag6 148.22(6) . . ?
Se1 Ag1 Ag6 99.93(5) . . ?
Ag7 Ag1 Ag6 112.13(5) . . ?
Ag8 Ag1 Ag6 109.76(6) 2_665 . ?
Ag5 Ag1 Ag4 145.76(10) . . ?
Ag4 Ag1 Ag4 89.39(6) 2_665 . ?
Ag3 Ag1 Ag4 46.56(5) . . ?
Ag2 Ag1 Ag4 47.09(5) . . ?
Se3 Ag1 Ag4 111.37(5) . . ?
Se5 Ag1 Ag4 144.04(6) . . ?
Se1 Ag1 Ag4 86.22(5) . . ?
Ag7 Ag1 Ag4 59.05(4) . . ?
Ag8 Ag1 Ag4 107.65(6) 2_665 . ?
Ag6 Ag1 Ag4 59.43(4) . . ?
Ag5 Ag1 Ag3 148.63(11) . 2_665 ?
Ag4 Ag1 Ag3 45.31(5) 2_665 2_665 ?
Ag3 Ag1 Ag3 91.97(7) . 2_665 ?
Ag2 Ag1 Ag3 47.50(5) . 2_665 ?
Se3 Ag1 Ag3 86.83(5) . 2_665 ?
Se5 Ag1 Ag3 109.28(5) . 2_665 ?
Se1 Ag1 Ag3 145.21(5) . 2_665 ?
Ag7 Ag1 Ag3 108.45(6) . 2_665 ?
Ag8 Ag1 Ag3 58.03(4) 2_665 2_665 ?
Ag6 Ag1 Ag3 58.50(4) . 2_665 ?
Ag4 Ag1 Ag3 59.66(4) . 2_665 ?
Ag5 Ag1 H0 174.33(12) . . ?
Ag4 Ag1 H0 54.62(5) 2_665 . ?
Ag3 Ag1 H0 56.35(5) . . ?
Ag2 Ag1 H0 58.18(5) . . ?
Se3 Ag1 H0 118.01(6) . . ?
Se5 Ag1 H0 115.36(6) . . ?
Se1 Ag1 H0 116.34(6) . . ?
Ag7 Ag1 H0 72.83(5) . . ?
Ag8 Ag1 H0 72.90(5) 2_665 . ?
Ag6 Ag1 H0 73.14(5) . . ?
Ag4 Ag1 H0 34.77(3) . . ?
Ag3 Ag1 H0 35.62(4) 2_665 . ?
Ag1 Ag5 Se5 92.52(10) . . ?
Ag1 Ag5 Se1 92.35(9) . . ?
Se5 Ag5 Se1 124.87(6) . . ?
Ag1 Ag5 Se3 85.81(10) . . ?
Se5 Ag5 Se3 117.88(6) . . ?
Se1 Ag5 Se3 117.23(6) . . ?
Ag1 Ag5 Ag3 39.82(8) . . ?
Se5 Ag5 Ag3 93.34(5) . . ?
Se1 Ag5 Ag3 59.62(5) . . ?
Se3 Ag5 Ag3 119.81(6) . . ?
Ag1 Ag5 Ag4 36.05(8) . 2_665 ?
Se5 Ag5 Ag4 59.15(4) . 2_665 ?
Se1 Ag5 Ag4 121.47(6) . 2_665 ?
Se3 Ag5 Ag4 90.50(5) . 2_665 ?
Ag3 Ag5 Ag4 61.86(5) . 2_665 ?
Ag1 Ag5 Ag2 34.65(8) . . ?
Se5 Ag5 Ag2 120.92(6) . . ?
Se1 Ag5 Ag2 90.63(5) . . ?
Se3 Ag5 Ag2 56.36(4) . . ?
Ag3 Ag5 Ag2 63.48(5) . . ?
Ag4 Ag5 Ag2 62.09(5) 2_665 . ?
Ag6 Ag2 Ag1 131.10(13) . . ?
Ag6 Ag2 Ag4 129.18(12) . . ?
Ag1 Ag2 Ag4 86.48(7) . . ?
Ag6 Ag2 Ag3 122.96(13) . 2_665 ?
Ag1 Ag2 Ag3 87.29(7) . 2_665 ?
Ag4 Ag2 Ag3 85.04(7) . 2_665 ?
Ag6 Ag2 Se2 69.26(10) . . ?
Ag1 Ag2 Se2 106.86(7) . . ?
Ag4 Ag2 Se2 67.25(5) . . ?
Ag3 Ag2 Se2 147.43(7) 2_665 . ?
Ag6 Ag2 Se3 68.41(10) . . ?
Ag1 Ag2 Se3 66.27(5) . . ?
Ag4 Ag2 Se3 149.24(7) . . ?
Ag3 Ag2 Se3 106.59(6) 2_665 . ?
Se2 Ag2 Se3 105.96(6) . . ?
Ag6 Ag2 Se6 63.29(11) . . ?
Ag1 Ag2 Se6 148.19(7) . . ?
Ag4 Ag2 Se6 104.53(6) . . ?
Ag3 Ag2 Se6 64.60(5) 2_665 . ?
Se2 Ag2 Se6 104.92(5) . . ?
Se3 Ag2 Se6 106.17(6) . . ?
Ag6 Ag2 Ag7 106.07(12) . 2_665 ?
Ag1 Ag2 Ag7 99.03(7) . 2_665 ?
Ag4 Ag2 Ag7 97.90(7) . 2_665 ?
Ag3 Ag2 Ag7 16.95(4) 2_665 2_665 ?
Se2 Ag2 Ag7 148.80(6) . 2_665 ?
Se3 Ag2 Ag7 100.16(5) . 2_665 ?
Se6 Ag2 Ag7 50.44(4) . 2_665 ?
Ag6 Ag2 Ag8 111.45(11) . . ?
Ag1 Ag2 Ag8 98.52(7) . . ?
Ag4 Ag2 Ag8 18.01(4) . . ?
Ag3 Ag2 Ag8 98.93(7) 2_665 . ?
Se2 Ag2 Ag8 50.80(4) . . ?
Se3 Ag2 Ag8 149.14(6) . . ?
Se6 Ag2 Ag8 100.24(5) . . ?
Ag7 Ag2 Ag8 108.96(6) 2_665 . ?
Ag6 Ag2 Ag5 112.92(12) . . ?
Ag1 Ag2 Ag5 18.27(5) . . ?
Ag4 Ag2 Ag5 99.48(7) . . ?
Ag3 Ag2 Ag5 101.12(6) 2_665 . ?
Se2 Ag2 Ag5 100.08(5) . . ?
Se3 Ag2 Ag5 50.88(4) . . ?
Se6 Ag2 Ag5 150.44(6) . . ?
Ag7 Ag2 Ag5 109.63(5) 2_665 . ?
Ag8 Ag2 Ag5 107.76(6) . . ?
Ag6 Ag2 Ag4 145.34(12) . 2_665 ?
Ag1 Ag2 Ag4 42.59(5) . 2_665 ?
Ag4 Ag2 Ag4 85.08(6) . 2_665 ?
Ag3 Ag2 Ag4 44.71(5) 2_665 2_665 ?
Se2 Ag2 Ag4 141.51(6) . 2_665 ?
Se3 Ag2 Ag4 84.04(5) . 2_665 ?
Se6 Ag2 Ag4 107.70(5) . 2_665 ?
Ag7 Ag2 Ag4 57.27(4) 2_665 2_665 ?
Ag8 Ag2 Ag4 103.01(6) . 2_665 ?
Ag5 Ag2 Ag4 57.23(4) . 2_665 ?
Ag6 Ag2 Ag1 143.08(12) . 2_665 ?
Ag1 Ag2 Ag1 85.66(7) . 2_665 ?
Ag4 Ag2 Ag1 41.90(5) . 2_665 ?
Ag3 Ag2 Ag1 43.14(5) 2_665 2_665 ?
Se2 Ag2 Ag1 107.46(5) . 2_665 ?
Se3 Ag2 Ag1 141.29(6) . 2_665 ?
Se6 Ag2 Ag1 83.48(5) . 2_665 ?
Ag7 Ag2 Ag1 56.87(4) 2_665 2_665 ?
Ag8 Ag2 Ag1 56.75(4) . 2_665 ?
Ag5 Ag2 Ag1 103.91(6) . 2_665 ?
Ag4 Ag2 Ag1 57.55(4) 2_665 2_665 ?
Ag6 Ag2 H0 175.47(14) . . ?
Ag1 Ag2 H0 52.32(5) . . ?
Ag4 Ag2 H0 51.35(5) . . ?
Ag3 Ag2 H0 52.75(5) 2_665 . ?
Se2 Ag2 H0 113.45(6) . . ?
Se3 Ag2 H0 113.42(6) . . ?
Se6 Ag2 H0 112.22(6) . . ?
Ag7 Ag2 H0 69.68(5) 2_665 . ?
Ag8 Ag2 H0 69.30(5) . . ?
Ag5 Ag2 H0 70.58(5) . . ?
Ag4 Ag2 H0 33.73(3) 2_665 . ?
Ag1 Ag2 H0 33.34(3) 2_665 . ?
Ag2 Ag6 Se6 94.97(12) . . ?
Ag2 Ag6 Se3 89.32(10) . . ?
Se6 Ag6 Se3 122.24(6) . . ?
Ag2 Ag6 Se2 88.39(11) . . ?
Se6 Ag6 Se2 119.93(6) . . ?
Se3 Ag6 Se2 117.75(6) . . ?
Ag2 Ag6 Ag3 40.27(10) . 2_665 ?
Se6 Ag6 Ag3 59.16(5) . 2_665 ?
Se3 Ag6 Ag3 93.53(5) . 2_665 ?
Se2 Ag6 Ag3 120.92(6) . 2_665 ?
Ag2 Ag6 Ag1 33.91(10) . . ?
Se6 Ag6 Ag1 121.97(6) . . ?
Se3 Ag6 Ag1 58.48(4) . . ?
Se2 Ag6 Ag1 91.26(5) . . ?
Ag3 Ag6 Ag1 62.85(5) 2_665 . ?
Ag2 Ag6 Ag4 35.41(9) . . ?
Se6 Ag6 Ag4 92.47(5) . . ?
Se3 Ag6 Ag4 119.62(6) . . ?
Se2 Ag6 Ag4 59.30(4) . . ?
Ag3 Ag6 Ag4 61.72(5) 2_665 . ?
Ag1 Ag6 Ag4 61.28(4) . . ?
Ag7 Ag3 Ag1 128.33(13) . . ?
Ag7 Ag3 Ag4 125.10(12) . . ?
Ag1 Ag3 Ag4 87.87(7) . . ?
Ag7 Ag3 Ag2 124.41(13) . 2_665 ?
Ag1 Ag3 Ag2 90.69(7) . 2_665 ?
Ag4 Ag3 Ag2 88.38(7) . 2_665 ?
Ag7 Ag3 Se1 65.17(11) . . ?
Ag1 Ag3 Se1 67.72(6) . . ?
Ag4 Ag3 Se1 106.89(6) . . ?
Ag2 Ag3 Se1 152.45(7) 2_665 . ?
Ag7 Ag3 Se6 65.35(10) . 2_665 ?
Ag1 Ag3 Se6 107.43(6) . 2_665 ?
Ag4 Ag3 Se6 149.59(7) . 2_665 ?
Ag2 Ag3 Se6 65.89(5) 2_665 2_665 ?
Se1 Ag3 Se6 103.25(5) . 2_665 ?
Ag7 Ag3 Se4 62.68(10) . . ?
Ag1 Ag3 Se4 150.82(7) . . ?
Ag4 Ag3 Se4 67.70(5) . . ?
Ag2 Ag3 Se4 103.78(6) 2_665 . ?
Se1 Ag3 Se4 103.23(5) . . ?
Se6 Ag3 Se4 101.63(6) 2_665 . ?
Ag7 Ag3 Ag8 104.92(11) . . ?
Ag1 Ag3 Ag8 102.56(7) . . ?
Ag4 Ag3 Ag8 20.18(5) . . ?
Ag2 Ag3 Ag8 101.83(7) 2_665 . ?
Se1 Ag3 Ag8 99.55(5) . . ?
Se6 Ag3 Ag8 147.44(6) 2_665 . ?
Se4 Ag3 Ag8 50.09(4) . . ?
Ag7 Ag3 Ag5 107.40(12) . . ?
Ag1 Ag3 Ag5 21.02(5) . . ?
Ag4 Ag3 Ag5 104.08(7) . . ?
Ag2 Ag3 Ag5 104.22(6) 2_665 . ?
Se1 Ag3 Ag5 50.46(4) . . ?
Se6 Ag3 Ag5 98.04(5) 2_665 . ?
Se4 Ag3 Ag5 150.52(6) . . ?
Ag8 Ag3 Ag5 114.41(6) . . ?
Ag7 Ag3 Ag6 107.70(12) . 2_665 ?
Ag1 Ag3 Ag6 102.35(7) . 2_665 ?
Ag4 Ag3 Ag6 100.72(7) . 2_665 ?
Ag2 Ag3 Ag6 16.77(4) 2_665 2_665 ?
Se1 Ag3 Ag6 150.00(5) . 2_665 ?
Se6 Ag3 Ag6 51.07(4) 2_665 2_665 ?
Se4 Ag3 Ag6 97.87(5) . 2_665 ?
Ag8 Ag3 Ag6 110.36(6) . 2_665 ?
Ag5 Ag3 Ag6 111.57(5) . 2_665 ?
Ag7 Ag3 Ag4 147.43(11) . 2_665 ?
Ag1 Ag3 Ag4 44.06(5) . 2_665 ?
Ag4 Ag3 Ag4 87.45(7) . 2_665 ?
Ag2 Ag3 Ag4 46.63(5) 2_665 2_665 ?
Se1 Ag3 Ag4 109.90(5) . 2_665 ?
Se6 Ag3 Ag4 86.09(5) 2_665 2_665 ?
Se4 Ag3 Ag4 143.24(6) . 2_665 ?
Ag8 Ag3 Ag4 107.62(6) . 2_665 ?
Ag5 Ag3 Ag4 59.45(4) . 2_665 ?
Ag6 Ag3 Ag4 59.28(4) 2_665 2_665 ?
Ag7 Ag3 Ag1 143.59(12) . 2_665 ?
Ag1 Ag3 Ag1 88.03(7) . 2_665 ?
Ag4 Ag3 Ag1 43.19(5) . 2_665 ?
Ag2 Ag3 Ag1 45.21(5) 2_665 2_665 ?
Se1 Ag3 Ag1 143.79(6) . 2_665 ?
Se6 Ag3 Ag1 109.68(5) 2_665 2_665 ?
Se4 Ag3 Ag1 84.73(5) . 2_665 ?
Ag8 Ag3 Ag1 58.56(4) . 2_665 ?
Ag5 Ag3 Ag1 109.00(6) . 2_665 ?
Ag6 Ag3 Ag1 58.65(4) 2_665 2_665 ?
Ag4 Ag3 Ag1 59.11(4) 2_665 2_665 ?
Ag7 Ag3 H0 177.40(12) . . ?
Ag1 Ag3 H0 53.71(5) . . ?
Ag4 Ag3 H0 52.49(5) . . ?
Ag2 Ag3 H0 55.85(6) 2_665 . ?
Se1 Ag3 H0 115.90(6) . . ?
Se6 Ag3 H0 116.14(6) 2_665 . ?
Se4 Ag3 H0 114.74(6) . . ?
Ag8 Ag3 H0 72.66(5) . . ?
Ag5 Ag3 H0 74.69(5) . . ?
Ag6 Ag3 H0 72.61(5) 2_665 . ?
Ag4 Ag3 H0 34.96(3) 2_665 . ?
Ag1 Ag3 H0 34.32(4) 2_665 . ?
Ag3 Ag7 Se4 94.39(11) . . ?
Ag3 Ag7 Se1 91.68(12) . . ?
Se4 Ag7 Se1 121.26(6) . . ?
Ag3 Ag7 Se6 91.51(11) . 2_665 ?
Se4 Ag7 Se6 118.88(6) . 2_665 ?
Se1 Ag7 Se6 119.28(6) . 2_665 ?
Ag3 Ag7 Ag4 37.67(9) . . ?
Se4 Ag7 Ag4 61.40(5) . . ?
Se1 Ag7 Ag4 93.64(5) . . ?
Se6 Ag7 Ag4 122.17(7) 2_665 . ?
Ag3 Ag7 Ag1 35.18(9) . . ?
Se4 Ag7 Ag1 123.20(6) . . ?
Se1 Ag7 Ag1 60.44(5) . . ?
Se6 Ag7 Ag1 93.13(5) 2_665 . ?
Ag4 Ag7 Ag1 61.86(5) . . ?
Ag3 Ag7 Ag2 38.64(10) . 2_665 ?
Se4 Ag7 Ag2 92.39(6) . 2_665 ?
Se1 Ag7 Ag2 124.34(7) . 2_665 ?
Se6 Ag7 Ag2 58.96(5) 2_665 2_665 ?
Ag4 Ag7 Ag2 63.23(5) . 2_665 ?
Ag1 Ag7 Ag2 64.09(5) . 2_665 ?
Ag8 Ag4 Ag1 126.27(11) . 2_665 ?
Ag8 Ag4 Ag3 118.70(12) . . ?
Ag1 Ag4 Ag3 91.50(7) 2_665 . ?
Ag8 Ag4 Ag2 125.46(11) . . ?
Ag1 Ag4 Ag2 93.61(7) 2_665 . ?
Ag3 Ag4 Ag2 91.84(7) . . ?
Ag8 Ag4 Se5 66.08(9) . 2_665 ?
Ag1 Ag4 Se5 68.27(5) 2_665 2_665 ?
Ag3 Ag4 Se5 152.89(7) . 2_665 ?
Ag2 Ag4 Se5 106.74(6) . 2_665 ?
Ag8 Ag4 Se2 64.56(9) . . ?
Ag1 Ag4 Se2 152.39(7) 2_665 . ?
Ag3 Ag4 Se2 104.96(6) . . ?
Ag2 Ag4 Se2 64.37(5) . . ?
Se5 Ag4 Se2 100.90(5) 2_665 . ?
Ag8 Ag4 Se4 59.27(9) . . ?
Ag1 Ag4 Se4 106.01(6) 2_665 . ?
Ag3 Ag4 Se4 65.23(5) . . ?
Ag2 Ag4 Se4 149.63(7) . . ?
Se5 Ag4 Se4 102.04(5) 2_665 . ?
Se2 Ag4 Se4 101.03(5) . . ?
Ag8 Ag4 Ag7 101.48(11) . . ?
Ag1 Ag4 Ag7 103.23(6) 2_665 . ?
Ag3 Ag4 Ag7 17.23(4) . . ?
Ag2 Ag4 Ag7 103.40(6) . . ?
Se5 Ag4 Ag7 149.05(6) 2_665 . ?
Se2 Ag4 Ag7 98.25(5) . . ?
Se4 Ag4 Ag7 50.15(4) . . ?
Ag8 Ag4 Ag6 110.30(10) . . ?
Ag1 Ag4 Ag6 103.26(7) 2_665 . ?
Ag3 Ag4 Ag6 103.36(6) . . ?
Ag2 Ag4 Ag6 15.41(4) . . ?
Se5 Ag4 Ag6 98.90(5) 2_665 . ?
Se2 Ag4 Ag6 51.86(4) . . ?
Se4 Ag4 Ag6 148.68(6) . . ?
Ag7 Ag4 Ag6 112.05(5) . . ?
Ag8 Ag4 Ag5 107.02(10) . 2_665 ?
Ag1 Ag4 Ag5 19.68(4) 2_665 2_665 ?
Ag3 Ag4 Ag5 106.68(6) . 2_665 ?
Ag2 Ag4 Ag5 105.12(7) . 2_665 ?
Se5 Ag4 Ag5 50.05(4) 2_665 2_665 ?
Se2 Ag4 Ag5 146.96(6) . 2_665 ?
Se4 Ag4 Ag5 100.64(5) . 2_665 ?
Ag7 Ag4 Ag5 114.79(6) . 2_665 ?
Ag6 Ag4 Ag5 110.67(6) . 2_665 ?
Ag8 Ag4 Ag1 142.63(11) . . ?
Ag1 Ag4 Ag1 90.61(6) 2_665 . ?
Ag3 Ag4 Ag1 45.57(5) . . ?
Ag2 Ag4 Ag1 46.42(5) . . ?
Se5 Ag4 Ag1 146.23(6) 2_665 . ?
Se2 Ag4 Ag1 85.67(5) . . ?
Se4 Ag4 Ag1 109.20(5) . . ?
Ag7 Ag4 Ag1 59.09(4) . . ?
Ag6 Ag4 Ag1 59.29(4) . . ?
Ag5 Ag4 Ag1 110.15(5) 2_665 . ?
Ag8 Ag4 Ag3 148.72(11) . 2_665 ?
Ag1 Ag4 Ag3 45.28(5) 2_665 2_665 ?
Ag3 Ag4 Ag3 92.55(7) . 2_665 ?
Ag2 Ag4 Ag3 48.33(5) . 2_665 ?
Se5 Ag4 Ag3 85.75(5) 2_665 2_665 ?
Se2 Ag4 Ag3 110.78(5) . 2_665 ?
Se4 Ag4 Ag3 145.24(6) . 2_665 ?
Ag7 Ag4 Ag3 109.78(6) . 2_665 ?
Ag6 Ag4 Ag3 58.99(4) . 2_665 ?
Ag5 Ag4 Ag3 58.70(4) 2_665 2_665 ?
Ag1 Ag4 Ag3 61.24(4) . 2_665 ?
Ag8 Ag4 H0 174.46(12) . . ?
Ag1 Ag4 H0 55.44(5) 2_665 . ?
Ag3 Ag4 H0 55.84(5) . . ?
Ag2 Ag4 H0 57.89(5) . . ?
Se5 Ag4 H0 118.12(6) 2_665 . ?
Se2 Ag4 H0 116.63(6) . . ?
Se4 Ag4 H0 115.45(6) . . ?
Ag7 Ag4 H0 73.06(5) . . ?
Ag6 Ag4 H0 73.23(5) . . ?
Ag5 Ag4 H0 75.01(5) 2_665 . ?
Ag1 Ag4 H0 35.17(4) . . ?
Ag3 Ag4 H0 36.71(4) 2_665 . ?
Ag4 Ag8 Se4 96.36(10) . . ?
Ag4 Ag8 Se5 88.65(10) . 2_665 ?
Se4 Ag8 Se5 121.89(6) . 2_665 ?
Ag4 Ag8 Se2 90.54(10) . . ?
Se4 Ag8 Se2 121.66(7) . . ?
Se5 Ag8 Se2 116.11(6) 2_665 . ?
Ag4 Ag8 Ag3 41.12(9) . . ?
Se4 Ag8 Ag3 60.50(5) . . ?
Se5 Ag8 Ag3 123.54(6) 2_665 . ?
Se2 Ag8 Ag3 92.87(5) . . ?
Ag4 Ag8 Ag1 35.35(8) . 2_665 ?
Se4 Ag8 Ag1 93.92(5) . 2_665 ?
Se5 Ag8 Ag1 60.13(5) 2_665 2_665 ?
Se2 Ag8 Ag1 120.66(6) . 2_665 ?
Ag3 Ag8 Ag1 63.41(5) . 2_665 ?
Ag4 Ag8 Ag2 36.53(8) . . ?
Se4 Ag8 Ag2 124.58(6) . . ?
Se5 Ag8 Ag2 91.34(5) 2_665 . ?
Se2 Ag8 Ag2 57.04(4) . . ?
Ag3 Ag8 Ag2 64.20(5) . . ?
Ag1 Ag8 Ag2 63.74(5) 2_665 . ?
P1 Se1 Ag5 104.85(7) . . ?
P1 Se1 Ag7 111.74(7) . . ?
Ag5 Se1 Ag7 89.03(5) . . ?
P1 Se1 Ag3 103.21(7) . . ?
Ag5 Se1 Ag3 69.92(5) . . ?
Ag7 Se1 Ag3 23.15(4) . . ?
P1 Se1 Ag1 96.95(7) . . ?
Ag5 Se1 Ag1 26.09(4) . . ?
Ag7 Se1 Ag1 68.54(5) . . ?
Ag3 Se1 Ag1 46.65(4) . . ?
P1 Se2 Ag8 111.66(7) . . ?
P1 Se2 Ag6 102.25(7) . . ?
Ag8 Se2 Ag6 90.63(5) . . ?
P1 Se2 Ag2 97.09(6) . . ?
Ag8 Se2 Ag2 72.17(5) . . ?
Ag6 Se2 Ag2 22.34(4) . . ?
P1 Se2 Ag4 103.59(7) . . ?
Ag8 Se2 Ag4 24.90(4) . . ?
Ag6 Se2 Ag4 68.84(5) . . ?
Ag2 Se2 Ag4 48.38(4) . . ?
P2 Se3 Ag6 100.05(7) . . ?
P2 Se3 Ag5 113.26(7) . . ?
Ag6 Se3 Ag5 92.16(5) . . ?
P2 Se3 Ag2 97.43(7) . . ?
Ag6 Se3 Ag2 22.28(4) . . ?
Ag5 Se3 Ag2 72.75(5) . . ?
P2 Se3 Ag1 102.75(7) . . ?
Ag6 Se3 Ag1 69.47(5) . . ?
Ag5 Se3 Ag1 26.57(4) . . ?
Ag2 Se3 Ag1 48.12(5) . . ?
P3 Se5 Ag5 107.65(9) 2_665 . ?
P3 Se5 Ag8 108.42(9) 2_665 2_665 ?
Ag5 Se5 Ag8 91.18(5) . 2_665 ?
P3 Se5 Ag4 99.86(8) 2_665 2_665 ?
Ag5 Se5 Ag4 70.80(5) . 2_665 ?
Ag8 Se5 Ag4 25.26(4) 2_665 2_665 ?
P3 Se5 Ag1 101.60(7) 2_665 . ?
Ag5 Se5 Ag1 26.14(4) . . ?
Ag8 Se5 Ag1 68.61(5) 2_665 . ?
Ag4 Se5 Ag1 45.71(4) 2_665 . ?
P2 Se4 Ag8 110.65(8) 2_665 . ?
P2 Se4 Ag7 104.42(7) 2_665 . ?
Ag8 Se4 Ag7 88.37(5) . . ?
P2 Se4 Ag3 98.52(6) 2_665 . ?
Ag8 Se4 Ag3 69.41(5) . . ?
Ag7 Se4 Ag3 22.93(4) . . ?
P2 Se4 Ag4 101.15(7) 2_665 . ?
Ag8 Se4 Ag4 24.37(4) . . ?
Ag7 Se4 Ag4 68.45(5) . . ?
Ag3 Se4 Ag4 47.07(4) . . ?
P3 Se6 Ag6 104.74(9) . . ?
P3 Se6 Ag7 110.11(8) . 2_665 ?
Ag6 Se6 Ag7 88.69(5) . 2_665 ?
P3 Se6 Ag3 101.31(7) . 2_665 ?
Ag6 Se6 Ag3 69.77(5) . 2_665 ?
Ag7 Se6 Ag3 23.13(4) 2_665 2_665 ?
P3 Se6 Ag2 99.15(9) . . ?
Ag6 Se6 Ag2 21.75(4) . . ?
Ag7 Se6 Ag2 70.60(5) 2_665 . ?
Ag3 Se6 Ag2 49.51(5) 2_665 . ?
O1 P1 O4 102.8(3) . . ?
O1 P1 Se2 104.1(2) . . ?
O4 P1 Se2 108.9(3) . . ?
O1 P1 Se1 110.8(2) . . ?
O4 P1 Se1 108.2(3) . . ?
Se2 P1 Se1 120.59(10) . . ?
O3 P2 O2 108.3(3) . . ?
O3 P2 Se3 110.1(2) . . ?
O2 P2 Se3 102.6(3) . . ?
O3 P2 Se4 103.3(2) . 2_665 ?
O2 P2 Se4 110.8(3) . 2_665 ?
Se3 P2 Se4 121.44(9) . 2_665 ?
O5 P3 O6 103.9(8) . . ?
O5 P3 Se5 109.5(4) . 2_665 ?
O6 P3 Se5 103.1(5) . 2_665 ?
O5 P3 Se6 110.1(6) . . ?
O6 P3 Se6 107.2(4) . . ?
Se5 P3 Se6 121.50(10) 2_665 . ?
F1 P4 F1 179.998(1) . 2_756 ?
F1 P4 F2 91.5(8) . 2_756 ?
F1 P4 F2 88.5(8) 2_756 2_756 ?
F1 P4 F2 88.5(8) . . ?
F1 P4 F2 91.5(8) 2_756 . ?
F2 P4 F2 179.997(5) 2_756 . ?
F1 P4 F3 86.2(9) . . ?
F1 P4 F3 93.8(9) 2_756 . ?
F2 P4 F3 91.7(11) 2_756 . ?
F2 P4 F3 88.3(11) . . ?
F1 P4 F3 93.8(9) . 2_756 ?
F1 P4 F3 86.2(9) 2_756 2_756 ?
F2 P4 F3 88.3(11) 2_756 2_756 ?
F2 P4 F3 91.7(11) . 2_756 ?
F3 P4 F3 179.998(4) . 2_756 ?
C1 O1 P1 124.1(6) . . ?
C2 O2 P2 124.4(6) . . ?
C5 O3 P2 124.0(6) . . ?
C9 O4 P1 123.2(7) . . ?
C11 O5 P3 131.0(9) . . ?
C15 O6 P3 149(3) . . ?
C8 C1 C3 111.5(14) . . ?
C8 C1 O1 107.7(10) . . ?
C3 C1 O1 107.2(9) . . ?
C8 C1 H1 110.1 . . ?
C3 C1 H1 110.1 . . ?
O1 C1 H1 110.1 . . ?
O2 C2 C14 105.5(9) . . ?
O2 C2 C7 107.3(10) . . ?
C14 C2 C7 112.5(11) . . ?
O2 C2 H2 110.5 . . ?
C14 C2 H2 110.5 . . ?
C7 C2 H2 110.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C5 C4 H4A 109.5 . . ?
C5 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C5 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
O3 C5 C4 106.7(9) . . ?
O3 C5 C6 109.5(9) . . ?
C4 C5 C6 114.0(10) . . ?
O3 C5 H5 108.8 . . ?
C4 C5 H5 108.8 . . ?
C6 C5 H5 108.8 . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C2 C7 H7A 109.5 . . ?
C2 C7 H7B 109.5 . . ?
H7A C7 H7B 109.5 . . ?
C2 C7 H7C 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C1 C8 H8A 109.5 . . ?
C1 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C1 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C10 C9 O4 109.6(13) . . ?
C10 C9 C13 113.2(14) . . ?
O4 C9 C13 105.8(12) . . ?
C10 C9 H9 109.4 . . ?
O4 C9 H9 109.4 . . ?
C13 C9 H9 109.4 . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C12 C11 C17 112.7(16) . . ?
C12 C11 O5 104.7(14) . . ?
C17 C11 O5 109.4(17) . . ?
C12 C11 H11 109.9 . . ?
C17 C11 H11 109.9 . . ?
O5 C11 H11 109.9 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C9 C13 H13A 109.5 . . ?
C9 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C9 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C2 C14 H14A 109.5 . . ?
C2 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C2 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
O6 C15 C18 122(2) . . ?
O6 C15 C16 127(2) . . ?
C18 C15 C16 110.4(18) . . ?
O6 C15 H15 92.1 . . ?
C18 C15 H15 92.1 . . ?
C16 C15 H15 92.1 . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C11 C17 H17A 109.5 . . ?
C11 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C11 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag5 1.2345(19) . ?
Ag1 Ag4 2.1572(19) 2_665 ?
Ag1 Ag3 2.2040(19) . ?
Ag1 Ag2 2.2384(19) . ?
Ag1 Se3 2.7523(16) . ?
Ag1 Se5 2.7995(15) . ?
Ag1 Se1 2.8045(17) . ?
Ag1 Ag7 3.001(2) . ?
Ag1 Ag8 3.0059(19) 2_665 ?
Ag1 Ag6 3.0238(18) . ?
Ag1 Ag4 3.0841(18) . ?
Ag1 Ag3 3.151(2) 2_665 ?
Ag1 H0 1.8912(15) . ?
Ag5 Se5 2.4589(16) . ?
Ag5 Se1 2.4680(17) . ?
Ag5 Se3 2.5517(16) . ?
Ag5 Ag3 3.0055(19) . ?
Ag5 Ag4 3.029(2) 2_665 ?
Ag5 Ag2 3.1411(19) . ?
Ag2 Ag6 1.0381(18) . ?
Ag2 Ag4 2.263(2) . ?
Ag2 Ag3 2.326(2) 2_665 ?
Ag2 Se2 2.7296(16) . ?
Ag2 Se3 2.7382(16) . ?
Ag2 Se6 2.7911(17) . ?
Ag2 Ag7 3.073(2) 2_665 ?
Ag2 Ag8 3.0970(19) . ?
Ag2 Ag4 3.184(2) 2_665 ?
Ag2 Ag1 3.223(2) 2_665 ?
Ag2 H0 2.0306(17) . ?
Ag6 Se6 2.5026(17) . ?
Ag6 Se3 2.5462(15) . ?
Ag6 Se2 2.5538(15) . ?
Ag6 Ag3 3.0188(19) 2_665 ?
Ag6 Ag4 3.0280(19) . ?
Ag3 Ag7 1.0858(19) . ?
Ag3 Ag4 2.2407(19) . ?
Ag3 Ag2 2.326(2) 2_665 ?
Ag3 Se1 2.7607(17) . ?
Ag3 Se6 2.7625(16) 2_665 ?
Ag3 Se4 2.7787(15) . ?
Ag3 Ag8 2.9888(17) . ?
Ag3 Ag6 3.0188(19) 2_665 ?
Ag3 Ag4 3.102(2) 2_665 ?
Ag3 Ag1 3.151(2) 2_665 ?
Ag3 H0 1.9533(17) . ?
Ag7 Se4 2.4760(16) . ?
Ag7 Se1 2.5066(18) . ?
Ag7 Se6 2.5117(16) 2_665 ?
Ag7 Ag4 3.000(2) . ?
Ag7 Ag2 3.073(2) 2_665 ?
Ag4 Ag8 1.1755(17) . ?
Ag4 Ag1 2.1571(19) 2_665 ?
Ag4 Se5 2.7538(16) 2_665 ?
Ag4 Se2 2.7918(15) . ?
Ag4 Se4 2.8315(17) . ?
Ag4 Ag5 3.029(2) 2_665 ?
Ag4 Ag3 3.102(2) 2_665 ?
Ag4 H0 1.8723(13) . ?
Ag8 Se4 2.4490(17) . ?
Ag8 Se5 2.5181(18) 2_665 ?
Ag8 Se2 2.5212(16) . ?
Ag8 Ag1 3.0058(19) 2_665 ?
Se1 P1 2.169(2) . ?
Se2 P1 2.166(2) . ?
Se3 P2 2.159(2) . ?
Se5 P3 2.158(3) 2_665 ?
Se5 Ag8 2.5180(18) 2_665 ?
Se5 Ag4 2.7538(16) 2_665 ?
Se4 P2 2.167(2) 2_665 ?
Se6 P3 2.161(3) . ?
Se6 Ag7 2.5117(16) 2_665 ?
Se6 Ag3 2.7625(16) 2_665 ?
P1 O1 1.568(6) . ?
P1 O4 1.582(6) . ?
P2 O3 1.568(6) . ?
P2 O2 1.579(6) . ?
P2 Se4 2.167(2) 2_665 ?
P3 O5 1.519(9) . ?
P3 O6 1.576(10) . ?
P3 Se5 2.157(3) 2_665 ?
P4 F1 1.535(11) . ?
P4 F1 1.535(11) 2_756 ?
P4 F2 1.541(14) 2_756 ?
P4 F2 1.541(14) . ?
P4 F3 1.556(17) . ?
P4 F3 1.556(17) 2_756 ?
O1 C1 1.482(11) . ?
O2 C2 1.473(11) . ?
O3 C5 1.465(11) . ?
O4 C9 1.444(13) . ?
O5 C11 1.478(18) . ?
O6 C15 1.10(2) . ?
C1 C8 1.43(2) . ?
C1 C3 1.462(17) . ?
C1 H1 0.9800 . ?
C2 C14 1.494(15) . ?
C2 C7 1.495(16) . ?
C2 H2 0.9800 . ?
C3 H3A 0.9600 . ?
C3 H3B 0.9600 . ?
C3 H3C 0.9600 . ?
C4 C5 1.483(15) . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C4 H4C 0.9600 . ?
C5 C6 1.493(15) . ?
C5 H5 0.9800 . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C7 H7A 0.9600 . ?
C7 H7B 0.9600 . ?
C7 H7C 0.9600 . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
C9 C10 1.436(19) . ?
C9 C13 1.52(2) . ?
C9 H9 0.9800 . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C11 C12 1.416(18) . ?
C11 C17 1.45(2) . ?
C11 H11 0.9800 . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C15 C18 1.38(3) . ?
C15 C16 1.49(3) . ?
C15 H15 0.9800 . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
C17 H17A 0.9600 . ?
C17 H17B 0.9600 . ?
C17 H17C 0.9600 . ?
C18 H18A 0.9600 . ?
C18 H18B 0.9600 . ?
C18 H18C 0.9600 . ?
