#------------------------------------------------------------------------------
#$Date: 2018-10-05 15:19:55 +0300 (Fri, 05 Oct 2018) $
#$Revision: 211332 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/31/48/4314867.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4314867
loop_
_publ_author_name
'John E. Bercaw'
'Alec C. Durrell'
'Harry B. Gray'
'Jennifer C. Green'
'Nilay Hazari'
'Jay A. Labinger'
'Jay R. Winkler'
_publ_section_title
;
 Electronic Structures of PdII Dimers
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1801
_journal_page_last               1810
_journal_paper_doi               10.1021/ic902189g
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C26 H16 F6 N2 O4 Pd2'
_chemical_formula_sum            'C26 H16 F6 N2 O4 Pd2'
_chemical_formula_weight         747.21
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 104.9510(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            12
_cell_length_a                   26.4337(10)
_cell_length_b                   17.4055(7)
_cell_length_c                   17.2538(7)
_cell_measurement_reflns_used    9936
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      29.21
_cell_measurement_theta_min      2.37
_cell_volume                     7669.6(5)
_computing_cell_refinement       'Bruker SAINT-Plus v7.34A'
_computing_data_collection       'Bruker APEX2 v2.1-0'
_computing_data_reduction        'Bruker SAINT-Plus v7.34A'
_computing_molecular_graphics    'Bruker XP v5.1'
_computing_publication_material  'Bruker XCIF 2008'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.845
_diffrn_measured_fraction_theta_max 0.845
_diffrn_measurement_device_type  'Bruker KAPPA APEX II'
_diffrn_measurement_method       'ω scans; 5 settings'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0499
_diffrn_reflns_av_sigmaI/netI    0.0441
_diffrn_reflns_limit_h_max       34
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            56449
_diffrn_reflns_theta_full        29.32
_diffrn_reflns_theta_max         29.32
_diffrn_reflns_theta_min         1.59
_exptl_absorpt_coefficient_mu    1.488
_exptl_absorpt_correction_T_max  0.9293
_exptl_absorpt_correction_T_min  0.7260
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.941
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Plate
_exptl_crystal_F_000             4368
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.320
_refine_diff_density_min         -1.119
_refine_diff_density_rms         0.097
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.740
_refine_ls_hydrogen_treatment    Unrestrained
_refine_ls_matrix_type           'Full matrix'
_refine_ls_number_parameters     1273
_refine_ls_number_reflns         17747
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.740
_refine_ls_R_factor_all          0.0589
_refine_ls_R_factor_gt           0.0411
_refine_ls_shift/su_max          0.007
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/s²(Fo²)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0622
_refine_ls_wR_factor_ref         0.0635
_reflns_number_gt                13988
_reflns_number_total             17747
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic902189g_si_002_3.cif
_cod_data_source_block           COMPOUND_3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_weighting_scheme' value 'Sigma' changed to
'sigma' according to the built-in table from CIF Core dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'Direct methods' was changed to
'direct'.

'_atom_sites_solution_secondary' value 'Difference Fourier map' was
changed to 'difmap'.

'_atom_sites_solution_hydrogens' value 'Difference Fourier map' was
changed to 'difmap'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_database_code               4314867
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1 Pd 1.060974(10) 0.582285(16) 0.341757(16) 0.02468(7) Uani 1 1 d . . .
Pd2 Pd 1.010976(10) 0.696601(19) 0.227678(18) 0.03224(8) Uani 1 1 d . . .
F1A F 1.05262(8) 0.51515(16) 0.04326(14) 0.0517(7) Uani 1 1 d . . .
F2A F 1.12417(8) 0.48507(17) 0.12703(15) 0.0597(8) Uani 1 1 d . . .
F3A F 1.11619(9) 0.59463(17) 0.07118(16) 0.0640(8) Uani 1 1 d . . .
F4A F 1.21689(8) 0.72625(15) 0.37658(18) 0.0642(8) Uani 1 1 d . . .
F5A F 1.17003(10) 0.8087(2) 0.4146(2) 0.0955(12) Uani 1 1 d . . .
F6A F 1.17987(9) 0.81381(18) 0.2969(2) 0.0811(10) Uani 1 1 d . . .
O1A O 1.07867(8) 0.53944(15) 0.23350(15) 0.0310(6) Uani 1 1 d . . .
O2A O 1.04422(9) 0.63665(16) 0.14912(16) 0.0370(7) Uani 1 1 d . . .
O3A O 1.12734(8) 0.65207(15) 0.35789(15) 0.0305(6) Uani 1 1 d . . .
O4A O 1.08665(9) 0.74855(15) 0.27816(17) 0.0391(7) Uani 1 1 d . . .
N1A N 0.99502(10) 0.52167(18) 0.33226(18) 0.0295(7) Uani 1 1 d . . .
N2A N 0.97424(11) 0.7498(2) 0.3004(2) 0.0380(9) Uani 1 1 d . . .
C1A C 0.97464(14) 0.4722(2) 0.2721(2) 0.0343(9) Uani 1 1 d . . .
C2A C 0.92691(15) 0.4386(3) 0.2637(3) 0.0425(11) Uani 1 1 d . . .
C3A C 0.89859(16) 0.4561(3) 0.3189(3) 0.0406(11) Uani 1 1 d . . .
C4A C 0.91899(14) 0.5064(2) 0.3806(3) 0.0342(10) Uani 1 1 d . . .
C5A C 0.96818(12) 0.5392(2) 0.3873(2) 0.0258(8) Uani 1 1 d . . .
C6A C 0.99436(13) 0.5929(2) 0.4479(2) 0.0281(8) Uani 1 1 d . . .
C7A C 0.97618(15) 0.6192(2) 0.5118(2) 0.0321(9) Uani 1 1 d . . .
C8A C 1.00508(16) 0.6694(3) 0.5664(3) 0.0434(11) Uani 1 1 d . . .
C9A C 1.05347(16) 0.6954(3) 0.5582(3) 0.0428(11) Uani 1 1 d . . .
C10A C 1.07164(15) 0.6704(2) 0.4949(2) 0.0352(10) Uani 1 1 d . . .
C11A C 1.04337(12) 0.6196(2) 0.4393(2) 0.0250(8) Uani 1 1 d . . .
C12A C 0.99711(18) 0.7989(3) 0.3598(3) 0.0518(13) Uani 1 1 d . . .
C13A C 0.97196(19) 0.8291(3) 0.4129(3) 0.0581(14) Uani 1 1 d . . .
C14A C 0.9198(2) 0.8073(3) 0.4030(4) 0.0611(15) Uani 1 1 d . . .
C15A C 0.89604(16) 0.7583(3) 0.3453(3) 0.0477(12) Uani 1 1 d . . .
C16A C 0.92354(14) 0.7275(2) 0.2930(2) 0.0382(10) Uani 1 1 d . . .
C17A C 0.90448(13) 0.6739(3) 0.2276(2) 0.0393(11) Uani 1 1 d . . .
C18A C 0.85395(15) 0.6454(3) 0.2041(3) 0.0472(13) Uani 1 1 d . . .
C19A C 0.83854(17) 0.5992(4) 0.1386(3) 0.0597(15) Uani 1 1 d . . .
C20A C 0.87402(17) 0.5797(3) 0.0936(3) 0.0554(14) Uani 1 1 d . . .
C21A C 0.92479(16) 0.6069(3) 0.1174(3) 0.0493(13) Uani 1 1 d . . .
C22A C 0.94062(13) 0.6545(2) 0.1839(2) 0.0348(10) Uani 1 1 d . . .
C23A C 1.06963(12) 0.5757(2) 0.1701(2) 0.0292(9) Uani 1 1 d . . .
C24A C 1.09125(13) 0.5419(3) 0.1029(2) 0.0356(10) Uani 1 1 d . . .
C25A C 1.12457(13) 0.7168(2) 0.3266(2) 0.0314(9) Uani 1 1 d . . .
C26A C 1.17354(15) 0.7666(3) 0.3531(3) 0.0435(11) Uani 1 1 d . . .
H1A H 0.9939(10) 0.4628(18) 0.2335(17) 0.009(8) Uiso 1 1 d . . .
H2A H 0.9149(12) 0.403(2) 0.227(2) 0.019(9) Uiso 1 1 d . . .
H3A H 0.8728(17) 0.436(3) 0.322(3) 0.074(18) Uiso 1 1 d . . .
H4A H 0.9028(11) 0.5172(18) 0.4170(18) 0.009(8) Uiso 1 1 d . . .
H7A H 0.9424(12) 0.6030(19) 0.5167(19) 0.021(9) Uiso 1 1 d . . .
H8A H 0.9939(16) 0.691(3) 0.612(3) 0.076(16) Uiso 1 1 d . . .
H9A H 1.0696(15) 0.729(3) 0.599(3) 0.064(15) Uiso 1 1 d . . .
H10A H 1.1028(15) 0.688(3) 0.487(3) 0.061(14) Uiso 1 1 d . . .
H12A H 1.0272(13) 0.810(2) 0.362(2) 0.038(12) Uiso 1 1 d . . .
H13A H 0.9927(19) 0.864(3) 0.461(3) 0.10(2) Uiso 1 1 d . . .
H14A H 0.9065(14) 0.823(2) 0.442(2) 0.046(13) Uiso 1 1 d . . .
H15A H 0.8564(15) 0.739(3) 0.328(3) 0.064(14) Uiso 1 1 d . . .
H18A H 0.8269(13) 0.658(2) 0.233(2) 0.033(10) Uiso 1 1 d . . .
H19A H 0.8086(15) 0.579(2) 0.122(2) 0.043(12) Uiso 1 1 d . . .
H20A H 0.8614(16) 0.546(3) 0.050(3) 0.072(16) Uiso 1 1 d . . .
H21A H 0.9478(13) 0.597(2) 0.094(2) 0.031(11) Uiso 1 1 d . . .
Pd3 Pd 0.228194(9) 0.372096(17) 0.646594(17) 0.02632(7) Uani 1 1 d . . .
Pd4 Pd 0.332692(10) 0.348086(18) 0.627342(18) 0.03098(7) Uani 1 1 d . . .
F1B F 0.38193(10) 0.43460(19) 0.89284(16) 0.0735(9) Uani 1 1 d . . .
F2B F 0.37252(10) 0.31616(18) 0.91464(16) 0.0783(9) Uani 1 1 d . . .
F3B F 0.31338(9) 0.39469(18) 0.92281(14) 0.0621(8) Uani 1 1 d . . .
F4B F 0.21126(9) 0.10404(15) 0.64117(17) 0.0602(8) Uani 1 1 d . . .
F5B F 0.29222(8) 0.08261(14) 0.66384(18) 0.0627(8) Uani 1 1 d . . .
F6B F 0.24740(12) 0.10761(16) 0.54487(16) 0.0746(9) Uani 1 1 d . . .
O1B O 0.27401(8) 0.37685(15) 0.76925(14) 0.0307(6) Uani 1 1 d . . .
O2B O 0.35438(8) 0.34730(15) 0.75311(15) 0.0335(6) Uani 1 1 d . . .
O3B O 0.23007(9) 0.25086(15) 0.64932(16) 0.0348(6) Uani 1 1 d . . .
O4B O 0.30927(9) 0.23064(15) 0.62448(17) 0.0424(7) Uani 1 1 d . . .
N1B N 0.22457(10) 0.48672(19) 0.6324(2) 0.0337(8) Uani 1 1 d . . .
N2B N 0.30892(11) 0.3620(2) 0.5088(2) 0.0437(9) Uani 1 1 d . . .
C1B C 0.24639(13) 0.5385(3) 0.6902(3) 0.0327(10) Uani 1 1 d . . .
C2B C 0.24675(15) 0.6155(3) 0.6720(3) 0.0418(12) Uani 1 1 d . . .
C3B C 0.22514(15) 0.6403(3) 0.5962(3) 0.0425(11) Uani 1 1 d . . .
C4B C 0.20265(14) 0.5882(3) 0.5373(3) 0.0366(10) Uani 1 1 d . . .
C5B C 0.20230(12) 0.5109(2) 0.5559(2) 0.0299(9) Uani 1 1 d . . .
C6B C 0.17989(12) 0.4491(2) 0.5010(2) 0.0304(9) Uani 1 1 d . . .
C7B C 0.15384(15) 0.4584(3) 0.4202(2) 0.0355(10) Uani 1 1 d . . .
C8B C 0.13155(15) 0.3958(3) 0.3754(3) 0.0416(11) Uani 1 1 d . . .
C9B C 0.13431(16) 0.3248(3) 0.4102(3) 0.0415(11) Uani 1 1 d . . .
C10B C 0.16156(14) 0.3138(3) 0.4897(2) 0.0358(10) Uani 1 1 d . . .
C11B C 0.18451(11) 0.3766(2) 0.5362(2) 0.0250(8) Uani 1 1 d . . .
C12B C 0.28789(17) 0.3059(4) 0.4551(3) 0.0572(15) Uani 1 1 d . . .
C13B C 0.2655(2) 0.3221(5) 0.3764(3) 0.0712(19) Uani 1 1 d . . .
C14B C 0.2640(2) 0.3968(5) 0.3503(3) 0.078(2) Uani 1 1 d . . .
C15B C 0.28509(18) 0.4543(4) 0.4032(3) 0.0540(15) Uani 1 1 d . . .
C16B C 0.30796(13) 0.4364(3) 0.4833(2) 0.0407(11) Uani 1 1 d . . .
C17B C 0.33213(12) 0.4904(2) 0.5479(2) 0.0336(9) Uani 1 1 d . . .
C18B C 0.33632(17) 0.5693(3) 0.5384(3) 0.0434(12) Uani 1 1 d . . .
C19B C 0.36230(18) 0.6135(3) 0.6015(3) 0.0482(12) Uani 1 1 d . . .
C20B C 0.38392(14) 0.5795(3) 0.6755(3) 0.0431(11) Uani 1 1 d . . .
C21B C 0.37741(14) 0.5021(3) 0.6846(3) 0.0364(10) Uani 1 1 d . . .
C22B C 0.35145(11) 0.4567(2) 0.6217(2) 0.0255(8) Uani 1 1 d . . .
C23B C 0.32212(13) 0.3656(2) 0.7918(2) 0.0282(8) Uani 1 1 d . . .
C24B C 0.34727(15) 0.3779(3) 0.8817(3) 0.0427(11) Uani 1 1 d . . .
C25B C 0.26541(14) 0.2114(2) 0.6339(2) 0.0314(9) Uani 1 1 d . . .
C26B C 0.25426(14) 0.1254(2) 0.6210(2) 0.0356(9) Uani 1 1 d . . .
H1B H 0.2582(13) 0.521(2) 0.739(2) 0.036(12) Uiso 1 1 d . . .
H2B H 0.2562(13) 0.643(2) 0.708(2) 0.031(12) Uiso 1 1 d . . .
H3B H 0.2294(13) 0.687(2) 0.579(2) 0.036(11) Uiso 1 1 d . . .
H4B H 0.1900(12) 0.600(2) 0.489(2) 0.023(10) Uiso 1 1 d . . .
H7B H 0.1535(13) 0.505(2) 0.397(2) 0.035(11) Uiso 1 1 d . . .
H8B H 0.1137(13) 0.396(2) 0.323(2) 0.036(11) Uiso 1 1 d . . .
H9B H 0.1191(13) 0.289(2) 0.385(2) 0.033(12) Uiso 1 1 d . . .
H10B H 0.1602(12) 0.265(2) 0.519(2) 0.032(10) Uiso 1 1 d . . .
H12B H 0.2901(13) 0.252(2) 0.478(2) 0.039(12) Uiso 1 1 d . . .
H13B H 0.2505(17) 0.281(3) 0.346(3) 0.076(17) Uiso 1 1 d . . .
H14B H 0.2489(15) 0.410(3) 0.297(3) 0.053(13) Uiso 1 1 d . . .
H15B H 0.2873(14) 0.496(2) 0.391(2) 0.024(13) Uiso 1 1 d . . .
H18B H 0.3216(13) 0.583(2) 0.498(2) 0.018(11) Uiso 1 1 d . . .
H19B H 0.3651(13) 0.666(2) 0.592(2) 0.040(11) Uiso 1 1 d . . .
H20B H 0.4039(12) 0.621(2) 0.724(2) 0.036(10) Uiso 1 1 d . . .
H21B H 0.3903(11) 0.480(2) 0.732(2) 0.016(9) Uiso 1 1 d . . .
Pd5 Pd 0.385491(9) 0.640952(17) 0.401327(17) 0.02668(7) Uani 1 1 d . . .
Pd6 Pd 0.388635(10) 0.75779(2) 0.285647(19) 0.03807(9) Uani 1 1 d . . .
F1C F 0.34845(10) 0.91773(16) 0.48695(18) 0.0719(8) Uani 1 1 d . . .
F2C F 0.29780(10) 0.83208(16) 0.51552(16) 0.0600(7) Uani 1 1 d . . .
F3C F 0.27430(9) 0.89413(16) 0.40470(17) 0.0640(8) Uani 1 1 d . . .
F4C F 0.21534(9) 0.5840(2) 0.25026(18) 0.0904(12) Uani 1 1 d . . .
F5C F 0.24442(9) 0.5877(2) 0.14915(18) 0.0818(11) Uani 1 1 d . . .
F6C F 0.20874(9) 0.68541(17) 0.1838(2) 0.1138(15) Uani 1 1 d . . .
O1C O 0.35507(9) 0.74068(16) 0.45151(16) 0.0365(7) Uani 1 1 d . . .
O2C O 0.34831(9) 0.82462(16) 0.34931(16) 0.0400(7) Uani 1 1 d . . .
O3C O 0.31021(8) 0.62358(15) 0.32641(16) 0.0334(6) Uani 1 1 d . . .
O4C O 0.31496(8) 0.70528(16) 0.22635(16) 0.0381(7) Uani 1 1 d . . .
N1C N 0.45952(10) 0.65024(18) 0.46817(18) 0.0302(7) Uani 1 1 d . . .
N2C N 0.43223(11) 0.6954(2) 0.2302(2) 0.0453(10) Uani 1 1 d . . .
C1C C 0.47685(14) 0.7048(2) 0.5241(2) 0.0319(9) Uani 1 1 d . . .
C2C C 0.52903(16) 0.7118(3) 0.5632(3) 0.0384(10) Uani 1 1 d . . .
C3C C 0.56480(15) 0.6610(3) 0.5436(3) 0.0380(10) Uani 1 1 d . . .
C4C C 0.54740(13) 0.6056(2) 0.4872(2) 0.0308(9) Uani 1 1 d . . .
C5C C 0.49376(12) 0.5991(2) 0.4486(2) 0.0268(8) Uani 1 1 d . . .
C6C C 0.46959(12) 0.5439(2) 0.3885(2) 0.0273(8) Uani 1 1 d . . .
C7C C 0.49575(14) 0.4856(2) 0.3599(2) 0.0339(10) Uani 1 1 d . . .
C8C C 0.46862(15) 0.4350(3) 0.3022(3) 0.0390(10) Uani 1 1 d . . .
C9C C 0.41466(15) 0.4417(3) 0.2744(3) 0.0387(10) Uani 1 1 d . . .
C10C C 0.38858(15) 0.4999(2) 0.3034(2) 0.0362(10) Uani 1 1 d . . .
C11C C 0.41492(12) 0.5514(2) 0.3596(2) 0.0251(8) Uani 1 1 d . . .
C12C C 0.41339(17) 0.6415(3) 0.1748(3) 0.0495(13) Uani 1 1 d . . .
C13C C 0.44512(19) 0.5933(3) 0.1441(3) 0.0639(16) Uani 1 1 d . . .
C14C C 0.4997(2) 0.6032(5) 0.1747(4) 0.075(2) Uani 1 1 d . . .
C15C C 0.5186(2) 0.6569(4) 0.2302(4) 0.071(2) Uani 1 1 d . . .
C16C C 0.48529(14) 0.7060(3) 0.2597(3) 0.0522(14) Uani 1 1 d . . .
C17C C 0.49946(15) 0.7656(3) 0.3167(3) 0.0582(15) Uani 1 1 d . . .
C18C C 0.55077(18) 0.7910(5) 0.3533(4) 0.073(2) Uani 1 1 d . . .
C19C C 0.5601(2) 0.8496(5) 0.4044(4) 0.093(3) Uani 1 1 d . . .
C20C C 0.5190(3) 0.8871(5) 0.4240(4) 0.088(3) Uani 1 1 d . . .
C21C C 0.46677(19) 0.8641(4) 0.3896(3) 0.0644(18) Uani 1 1 d . . .
C22C C 0.45789(15) 0.8023(3) 0.3373(3) 0.0518(14) Uani 1 1 d . . .
C23C C 0.29444(12) 0.6560(2) 0.2609(2) 0.0310(9) Uani 1 1 d . . .
C24C C 0.23945(14) 0.6287(3) 0.2102(3) 0.0409(10) Uani 1 1 d . . .
C25C C 0.34241(13) 0.8018(2) 0.4148(2) 0.0336(9) Uani 1 1 d . . .
C26C C 0.31512(16) 0.8615(3) 0.4561(3) 0.0490(12) Uani 1 1 d . . .
H1C H 0.4523(13) 0.741(2) 0.537(2) 0.042(11) Uiso 1 1 d . . .
H2C H 0.5367(13) 0.745(2) 0.597(2) 0.024(11) Uiso 1 1 d . . .
H3C H 0.5980(14) 0.666(2) 0.571(2) 0.045(12) Uiso 1 1 d . . .
H4C H 0.5695(11) 0.566(2) 0.4721(19) 0.020(9) Uiso 1 1 d . . .
H7C H 0.5297(13) 0.479(2) 0.374(2) 0.035(11) Uiso 1 1 d . . .
H8C H 0.4848(15) 0.397(3) 0.281(2) 0.052(13) Uiso 1 1 d . . .
H9C H 0.3983(12) 0.409(2) 0.237(2) 0.026(10) Uiso 1 1 d . . .
H10C H 0.3554(13) 0.501(2) 0.283(2) 0.030(10) Uiso 1 1 d . . .
H12C H 0.3828(15) 0.635(2) 0.151(3) 0.046(13) Uiso 1 1 d . . .
H13C H 0.4335(15) 0.551(3) 0.100(3) 0.060(15) Uiso 1 1 d . . .
H14C H 0.516(2) 0.564(3) 0.162(3) 0.10(2) Uiso 1 1 d . . .
H15C H 0.549(2) 0.667(3) 0.246(3) 0.10(2) Uiso 1 1 d . . .
H18C H 0.5733(19) 0.766(3) 0.338(3) 0.08(2) Uiso 1 1 d . . .
H19C H 0.5920(18) 0.865(3) 0.428(3) 0.078(16) Uiso 1 1 d . . .
H20C H 0.5238(16) 0.925(2) 0.454(2) 0.036(14) Uiso 1 1 d . . .
H21C H 0.4400(19) 0.885(3) 0.399(4) 0.10(2) Uiso 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11A Pd1 N1A 81.45(13) . . yes
C11A Pd1 O3A 94.01(12) . . yes
N1A Pd1 O3A 175.09(11) . . yes
C11A Pd1 O1A 178.60(12) . . yes
N1A Pd1 O1A 97.16(11) . . yes
O3A Pd1 O1A 87.39(9) . . yes
C11A Pd1 Pd2 100.90(10) . . yes
N1A Pd1 Pd2 94.11(9) . . yes
O3A Pd1 Pd2 84.88(7) . . yes
O1A Pd1 Pd2 79.13(7) . . yes
C22A Pd2 N2A 81.32(15) . . yes
C22A Pd2 O2A 94.58(14) . . yes
N2A Pd2 O2A 175.84(12) . . yes
C22A Pd2 O4A 176.83(14) . . yes
N2A Pd2 O4A 95.85(12) . . yes
O2A Pd2 O4A 88.27(10) . . yes
C22A Pd2 Pd1 103.22(11) . . yes
N2A Pd2 Pd1 95.93(9) . . yes
O2A Pd2 Pd1 84.36(7) . . yes
O4A Pd2 Pd1 78.42(7) . . yes
C23A O1A Pd1 123.6(2) . . ?
C23A O2A Pd2 121.4(2) . . ?
C25A O3A Pd1 121.0(2) . . ?
C25A O4A Pd2 125.5(2) . . ?
C1A N1A C5A 120.3(3) . . ?
C1A N1A Pd1 124.3(2) . . ?
C5A N1A Pd1 115.1(2) . . ?
C12A N2A C16A 119.0(4) . . ?
C12A N2A Pd2 125.0(3) . . ?
C16A N2A Pd2 115.6(3) . . ?
N1A C1A C2A 121.9(4) . . ?
N1A C1A H1A 117.9(18) . . ?
C2A C1A H1A 120.1(18) . . ?
C1A C2A C3A 118.8(4) . . ?
C1A C2A H2A 122(2) . . ?
C3A C2A H2A 119(2) . . ?
C4A C3A C2A 119.8(4) . . ?
C4A C3A H3A 114(4) . . ?
C2A C3A H3A 125(4) . . ?
C3A C4A C5A 119.6(4) . . ?
C3A C4A H4A 122(2) . . ?
C5A C4A H4A 118(2) . . ?
N1A C5A C4A 119.5(3) . . ?
N1A C5A C6A 114.4(3) . . ?
C4A C5A C6A 126.0(3) . . ?
C7A C6A C11A 119.1(3) . . ?
C7A C6A C5A 126.2(3) . . ?
C11A C6A C5A 114.7(3) . . ?
C8A C7A C6A 120.8(4) . . ?
C8A C7A H7A 120(2) . . ?
C6A C7A H7A 120(2) . . ?
C7A C8A C9A 120.0(4) . . ?
C7A C8A H8A 125(3) . . ?
C9A C8A H8A 115(3) . . ?
C10A C9A C8A 119.7(4) . . ?
C10A C9A H9A 128(3) . . ?
C8A C9A H9A 112(3) . . ?
C11A C10A C9A 121.3(4) . . ?
C11A C10A H10A 117(3) . . ?
C9A C10A H10A 122(3) . . ?
C10A C11A C6A 119.0(3) . . ?
C10A C11A Pd1 127.1(3) . . ?
C6A C11A Pd1 113.9(3) . . ?
N2A C12A C13A 123.5(4) . . ?
N2A C12A H12A 116(3) . . ?
C13A C12A H12A 121(3) . . ?
C12A C13A C14A 116.7(5) . . ?
C12A C13A H13A 120(3) . . ?
C14A C13A H13A 123(3) . . ?
C15A C14A C13A 121.5(5) . . ?
C15A C14A H14A 124(3) . . ?
C13A C14A H14A 114(3) . . ?
C14A C15A C16A 120.0(4) . . ?
C14A C15A H15A 130(2) . . ?
C16A C15A H15A 109(2) . . ?
N2A C16A C15A 119.3(4) . . ?
N2A C16A C17A 112.9(3) . . ?
C15A C16A C17A 127.8(4) . . ?
C18A C17A C22A 119.7(4) . . ?
C18A C17A C16A 125.0(4) . . ?
C22A C17A C16A 115.1(3) . . ?
C19A C18A C17A 121.0(4) . . ?
C19A C18A H18A 116(2) . . ?
C17A C18A H18A 123(2) . . ?
C18A C19A C20A 120.2(4) . . ?
C18A C19A H19A 125(3) . . ?
C20A C19A H19A 115(3) . . ?
C21A C20A C19A 119.2(5) . . ?
C21A C20A H20A 124(3) . . ?
C19A C20A H20A 116(3) . . ?
C22A C21A C20A 120.9(4) . . ?
C22A C21A H21A 115(3) . . ?
C20A C21A H21A 125(3) . . ?
C21A C22A C17A 119.0(4) . . ?
C21A C22A Pd2 126.5(3) . . ?
C17A C22A Pd2 114.4(3) . . ?
O1A C23A O2A 130.8(4) . . ?
O1A C23A C24A 116.7(3) . . ?
O2A C23A C24A 112.4(3) . . ?
F2A C24A F3A 107.0(3) . . ?
F2A C24A F1A 107.1(3) . . ?
F3A C24A F1A 106.6(3) . . ?
F2A C24A C23A 113.3(3) . . ?
F3A C24A C23A 111.6(3) . . ?
F1A C24A C23A 110.9(3) . . ?
O3A C25A O4A 129.5(3) . . ?
O3A C25A C26A 115.7(3) . . ?
O4A C25A C26A 114.8(4) . . ?
F5A C26A F6A 107.2(4) . . ?
F5A C26A F4A 106.7(4) . . ?
F6A C26A F4A 107.1(3) . . ?
F5A C26A C25A 109.2(3) . . ?
F6A C26A C25A 113.1(4) . . ?
F4A C26A C25A 113.2(4) . . ?
C11B Pd3 N1B 81.05(14) . . yes
C11B Pd3 O3B 93.79(13) . . yes
N1B Pd3 O3B 174.48(12) . . yes
C11B Pd3 O1B 175.17(13) . . yes
N1B Pd3 O1B 94.51(11) . . yes
O3B Pd3 O1B 90.71(10) . . yes
C11B Pd3 Pd4 103.58(9) . . yes
N1B Pd3 Pd4 98.41(7) . . yes
O3B Pd3 Pd4 80.84(6) . . yes
O1B Pd3 Pd4 78.86(6) . . yes
C22B Pd4 N2B 81.32(15) . . yes
C22B Pd4 O2B 93.01(13) . . yes
N2B Pd4 O2B 172.92(13) . . yes
C22B Pd4 O4B 175.82(13) . . yes
N2B Pd4 O4B 94.58(14) . . yes
O2B Pd4 O4B 91.02(11) . . yes
C22B Pd4 Pd3 97.31(9) . . yes
N2B Pd4 Pd3 92.44(8) . . yes
O2B Pd4 Pd3 84.05(6) . . yes
O4B Pd4 Pd3 82.02(6) . . yes
C23B O1B Pd3 124.8(2) . . ?
C23B O2B Pd4 120.5(2) . . ?
C25B O3B Pd3 124.2(2) . . ?
C25B O4B Pd4 121.6(3) . . ?
C1B N1B C5B 120.1(4) . . ?
C1B N1B Pd3 124.9(3) . . ?
C5B N1B Pd3 114.7(3) . . ?
C12B N2B C16B 119.3(4) . . ?
C12B N2B Pd4 125.2(4) . . ?
C16B N2B Pd4 114.9(3) . . ?
N1B C1B C2B 120.4(4) . . ?
N1B C1B H1B 117(3) . . ?
C2B C1B H1B 122(3) . . ?
C3B C2B C1B 120.2(4) . . ?
C3B C2B H2B 123(3) . . ?
C1B C2B H2B 116(3) . . ?
C2B C3B C4B 119.8(4) . . ?
C2B C3B H3B 124(3) . . ?
C4B C3B H3B 115(3) . . ?
C3B C4B C5B 119.7(4) . . ?
C3B C4B H4B 124(3) . . ?
C5B C4B H4B 117(3) . . ?
N1B C5B C4B 119.8(4) . . ?
N1B C5B C6B 113.8(3) . . ?
C4B C5B C6B 126.4(4) . . ?
C11B C6B C7B 120.5(4) . . ?
C11B C6B C5B 114.2(3) . . ?
C7B C6B C5B 125.3(4) . . ?
C8B C7B C6B 119.8(4) . . ?
C8B C7B H7B 121(2) . . ?
C6B C7B H7B 119(3) . . ?
C9B C8B C7B 120.2(4) . . ?
C9B C8B H8B 114(3) . . ?
C7B C8B H8B 126(3) . . ?
C8B C9B C10B 120.8(4) . . ?
C8B C9B H9B 120(3) . . ?
C10B C9B H9B 119(3) . . ?
C9B C10B C11B 119.8(4) . . ?
C9B C10B H10B 123(2) . . ?
C11B C10B H10B 116(2) . . ?
C6B C11B C10B 118.8(3) . . ?
C6B C11B Pd3 115.1(3) . . ?
C10B C11B Pd3 125.9(3) . . ?
N2B C12B C13B 121.7(6) . . ?
N2B C12B H12B 115(2) . . ?
C13B C12B H12B 123(2) . . ?
C12B C13B C14B 119.4(6) . . ?
C12B C13B H13B 115(3) . . ?
C14B C13B H13B 125(3) . . ?
C15B C14B C13B 120.0(6) . . ?
C15B C14B H14B 118(3) . . ?
C13B C14B H14B 122(3) . . ?
C14B C15B C16B 119.6(6) . . ?
C14B C15B H15B 124(3) . . ?
C16B C15B H15B 116(3) . . ?
N2B C16B C15B 120.0(5) . . ?
N2B C16B C17B 113.1(4) . . ?
C15B C16B C17B 126.9(5) . . ?
C22B C17B C18B 120.5(4) . . ?
C22B C17B C16B 114.5(4) . . ?
C18B C17B C16B 125.0(4) . . ?
C19B C18B C17B 120.1(5) . . ?
C19B C18B H18B 127(3) . . ?
C17B C18B H18B 113(3) . . ?
C18B C19B C20B 119.7(5) . . ?
C18B C19B H19B 117(2) . . ?
C20B C19B H19B 123(2) . . ?
C21B C20B C19B 119.3(5) . . ?
C21B C20B H20B 125.8(19) . . ?
C19B C20B H20B 114.8(19) . . ?
C22B C21B C20B 121.7(4) . . ?
C22B C21B H21B 118(2) . . ?
C20B C21B H21B 121(2) . . ?
C21B C22B C17B 118.5(4) . . ?
C21B C22B Pd4 126.5(3) . . ?
C17B C22B Pd4 114.7(3) . . ?
O1B C23B O2B 130.9(3) . . ?
O1B C23B C24B 115.7(3) . . ?
O2B C23B C24B 113.4(3) . . ?
F3B C24B F2B 106.8(4) . . ?
F3B C24B F1B 107.4(4) . . ?
F2B C24B F1B 106.9(3) . . ?
F3B C24B C23B 113.5(3) . . ?
F2B C24B C23B 111.2(4) . . ?
F1B C24B C23B 110.7(4) . . ?
O3B C25B O4B 130.5(4) . . ?
O3B C25B C26B 116.4(3) . . ?
O4B C25B C26B 113.0(3) . . ?
F6B C26B F5B 108.5(4) . . ?
F6B C26B F4B 106.8(3) . . ?
F5B C26B F4B 106.0(3) . . ?
F6B C26B C25B 110.3(3) . . ?
F5B C26B C25B 112.4(3) . . ?
F4B C26B C25B 112.4(3) . . ?
C11C Pd5 N1C 81.63(13) . . yes
C11C Pd5 O3C 93.57(12) . . yes
N1C Pd5 O3C 175.19(12) . . yes
C11C Pd5 O1C 177.98(12) . . yes
N1C Pd5 O1C 96.46(11) . . yes
O3C Pd5 O1C 88.34(9) . . yes
C11C Pd5 Pd6 102.88(10) . . yes
N1C Pd5 Pd6 98.28(9) . . yes
O3C Pd5 Pd6 82.32(7) . . yes
O1C Pd5 Pd6 77.99(7) . . yes
C22C Pd6 N2C 81.2(2) . . yes
C22C Pd6 O2C 94.83(18) . . yes
N2C Pd6 O2C 175.88(12) . . yes
C22C Pd6 O4C 177.20(19) . . yes
N2C Pd6 O4C 95.98(13) . . yes
O2C Pd6 O4C 87.95(10) . . yes
C22C Pd6 Pd5 98.88(11) . . yes
N2C Pd6 Pd5 94.10(9) . . yes
O2C Pd6 Pd5 85.29(8) . . yes
O4C Pd6 Pd5 81.07(7) . . yes
C25C O1C Pd5 124.0(3) . . ?
C25C O2C Pd6 120.3(3) . . ?
C23C O3C Pd5 122.7(2) . . ?
C23C O4C Pd6 121.1(2) . . ?
C1C N1C C5C 120.6(3) . . ?
C1C N1C Pd5 124.7(2) . . ?
C5C N1C Pd5 114.5(2) . . ?
C12C N2C C16C 121.0(4) . . ?
C12C N2C Pd6 124.6(3) . . ?
C16C N2C Pd6 114.1(4) . . ?
N1C C1C C2C 121.7(4) . . ?
N1C C1C H1C 119(2) . . ?
C2C C1C H1C 119(2) . . ?
C1C C2C C3C 118.8(4) . . ?
C1C C2C H2C 117(2) . . ?
C3C C2C H2C 125(2) . . ?
C4C C3C C2C 119.7(4) . . ?
C4C C3C H3C 124(3) . . ?
C2C C3C H3C 116(3) . . ?
C3C C4C C5C 120.5(4) . . ?
C3C C4C H4C 124.7(19) . . ?
C5C C4C H4C 114.7(19) . . ?
N1C C5C C4C 118.7(3) . . ?
N1C C5C C6C 114.4(3) . . ?
C4C C5C C6C 127.0(3) . . ?
C7C C6C C11C 120.1(3) . . ?
C7C C6C C5C 125.1(3) . . ?
C11C C6C C5C 114.7(3) . . ?
C8C C7C C6C 120.6(3) . . ?
C8C C7C H7C 114(2) . . ?
C6C C7C H7C 125(3) . . ?
C7C C8C C9C 119.4(4) . . ?
C7C C8C H8C 123(3) . . ?
C9C C8C H8C 118(3) . . ?
C8C C9C C10C 119.9(4) . . ?
C8C C9C H9C 117(2) . . ?
C10C C9C H9C 123(2) . . ?
C11C C10C C9C 121.5(4) . . ?
C11C C10C H10C 123(3) . . ?
C9C C10C H10C 115(3) . . ?
C10C C11C C6C 118.5(3) . . ?
C10C C11C Pd5 127.1(3) . . ?
C6C C11C Pd5 114.3(3) . . ?
N2C C12C C13C 123.1(5) . . ?
N2C C12C H12C 127(3) . . ?
C13C C12C H12C 110(3) . . ?
C12C C13C C14C 116.3(6) . . ?
C12C C13C H13C 128(2) . . ?
C14C C13C H13C 116(2) . . ?
C15C C14C C13C 120.5(6) . . ?
C15C C14C H14C 128(4) . . ?
C13C C14C H14C 110(4) . . ?
C14C C15C C16C 121.9(5) . . ?
C14C C15C H15C 124(5) . . ?
C16C C15C H15C 113(5) . . ?
N2C C16C C15C 117.1(5) . . ?
N2C C16C C17C 114.8(4) . . ?
C15C C16C C17C 128.2(5) . . ?
C22C C17C C18C 118.2(6) . . ?
C22C C17C C16C 115.4(4) . . ?
C18C C17C C16C 126.4(6) . . ?
C19C C18C C17C 122.0(7) . . ?
C19C C18C H18C 126(4) . . ?
C17C C18C H18C 112(4) . . ?
C18C C19C C20C 120.1(6) . . ?
C18C C19C H19C 122(3) . . ?
C20C C19C H19C 117(3) . . ?
C19C C20C C21C 120.5(7) . . ?
C19C C20C H20C 122(3) . . ?
C21C C20C H20C 118(3) . . ?
C22C C21C C20C 118.5(7) . . ?
C22C C21C H21C 117(4) . . ?
C20C C21C H21C 124(4) . . ?
C21C C22C C17C 120.6(4) . . ?
C21C C22C Pd6 125.5(4) . . ?
C17C C22C Pd6 113.9(4) . . ?
O3C C23C O4C 131.8(3) . . ?
O3C C23C C24C 114.7(3) . . ?
O4C C23C C24C 113.4(3) . . ?
F6C C24C F5C 108.7(4) . . ?
F6C C24C F4C 107.1(4) . . ?
F5C C24C F4C 105.3(4) . . ?
F6C C24C C23C 112.1(4) . . ?
F5C C24C C23C 110.2(3) . . ?
F4C C24C C23C 113.1(4) . . ?
O1C C25C O2C 131.0(4) . . ?
O1C C25C C26C 116.1(4) . . ?
O2C C25C C26C 112.9(4) . . ?
F1C C26C F3C 106.9(4) . . ?
F1C C26C F2C 107.4(4) . . ?
F3C C26C F2C 107.2(3) . . ?
F1C C26C C25C 109.9(3) . . ?
F3C C26C C25C 112.0(4) . . ?
F2C C26C C25C 113.1(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd1 C11A 1.969(3) . yes
Pd1 N1A 2.008(3) . yes
Pd1 O3A 2.093(2) . yes
Pd1 O1A 2.171(2) . yes
Pd1 Pd2 2.8701(4) . yes
Pd2 C22A 1.960(4) . yes
Pd2 N2A 2.000(3) . yes
Pd2 O2A 2.077(3) . yes
Pd2 O4A 2.163(2) . yes
F1A C24A 1.333(4) . ?
F2A C24A 1.313(5) . ?
F3A C24A 1.328(4) . ?
F4A C26A 1.315(4) . ?
F5A C26A 1.313(5) . ?
F6A C26A 1.315(5) . ?
O1A C23A 1.232(4) . ?
O2A C23A 1.258(4) . ?
O3A C25A 1.243(4) . ?
O4A C25A 1.255(4) . ?
N1A C1A 1.350(5) . ?
N1A C5A 1.359(4) . ?
N2A C12A 1.351(6) . ?
N2A C16A 1.369(5) . ?
C1A C2A 1.364(5) . ?
C1A H1A 0.95(3) . ?
C2A C3A 1.388(6) . ?
C2A H2A 0.88(3) . ?
C3A C4A 1.376(6) . ?
C3A H3A 0.78(4) . ?
C4A C5A 1.398(5) . ?
C4A H4A 0.87(3) . ?
C5A C6A 1.439(5) . ?
C6A C7A 1.388(5) . ?
C6A C11A 1.420(5) . ?
C7A C8A 1.366(6) . ?
C7A H7A 0.96(3) . ?
C8A C9A 1.398(6) . ?
C8A H8A 0.98(5) . ?
C9A C10A 1.373(6) . ?
C9A H9A 0.93(5) . ?
C10A C11A 1.375(5) . ?
C10A H10A 0.92(4) . ?
C12A C13A 1.368(6) . ?
C12A H12A 0.81(3) . ?
C13A C14A 1.398(7) . ?
C13A H13A 1.07(5) . ?
C14A C15A 1.337(7) . ?
C14A H14A 0.88(4) . ?
C15A C16A 1.403(6) . ?
C15A H15A 1.07(4) . ?
C16A C17A 1.452(6) . ?
C17A C18A 1.384(5) . ?
C17A C22A 1.403(5) . ?
C18A C19A 1.360(7) . ?
C18A H18A 0.99(3) . ?
C19A C20A 1.405(6) . ?
C19A H19A 0.84(4) . ?
C20A C21A 1.382(6) . ?
C20A H20A 0.95(5) . ?
C21A C22A 1.389(6) . ?
C21A H21A 0.83(3) . ?
C23A C24A 1.535(5) . ?
C25A C26A 1.527(5) . ?
Pd3 C11B 1.958(3) . yes
Pd3 N1B 2.009(3) . yes
Pd3 O3B 2.111(3) . yes
Pd3 O1B 2.152(2) . yes
Pd3 Pd4 2.8963(4) . yes
Pd4 C22B 1.964(4) . yes
Pd4 N2B 1.993(3) . yes
Pd4 O2B 2.097(3) . yes
Pd4 O4B 2.133(3) . yes
F1B C24B 1.326(5) . ?
F2B C24B 1.315(5) . ?
F3B C24B 1.312(4) . ?
F4B C26B 1.325(4) . ?
F5B C26B 1.313(4) . ?
F6B C26B 1.316(5) . ?
O1B C23B 1.246(4) . ?
O2B C23B 1.252(4) . ?
O3B C25B 1.243(4) . ?
O4B C25B 1.257(4) . ?
N1B C1B 1.357(5) . ?
N1B C5B 1.366(5) . ?
N2B C12B 1.362(6) . ?
N2B C16B 1.365(6) . ?
C1B C2B 1.377(6) . ?
C1B H1B 0.88(4) . ?
C2B C3B 1.356(7) . ?
C2B H2B 0.77(4) . ?
C3B C4B 1.379(6) . ?
C3B H3B 0.87(4) . ?
C4B C5B 1.383(6) . ?
C4B H4B 0.85(3) . ?
C5B C6B 1.455(5) . ?
C6B C11B 1.392(5) . ?
C6B C7B 1.395(5) . ?
C7B C8B 1.377(6) . ?
C7B H7B 0.90(4) . ?
C8B C9B 1.368(6) . ?
C8B H8B 0.91(4) . ?
C9B C10B 1.389(6) . ?
C9B H9B 0.81(4) . ?
C10B C11B 1.397(5) . ?
C10B H10B 0.99(4) . ?
C12B C13B 1.364(7) . ?
C12B H12B 1.01(4) . ?
C13B C14B 1.373(9) . ?
C13B H13B 0.92(5) . ?
C14B C15B 1.372(8) . ?
C14B H14B 0.93(4) . ?
C15B C16B 1.395(6) . ?
C15B H15B 0.77(4) . ?
C16B C17B 1.472(6) . ?
C17B C22B 1.374(5) . ?
C17B C18B 1.392(6) . ?
C18B C19B 1.364(7) . ?
C18B H18B 0.74(3) . ?
C19B C20B 1.390(6) . ?
C19B H19B 0.94(4) . ?
C20B C21B 1.372(6) . ?
C20B H20B 1.13(4) . ?
C21B C22B 1.374(5) . ?
C21B H21B 0.88(3) . ?
C23B C24B 1.537(5) . ?
C25B C26B 1.531(5) . ?
Pd5 C11C 1.960(4) . yes
Pd5 N1C 2.005(3) . yes
Pd5 O3C 2.096(2) . yes
Pd5 O1C 2.184(3) . yes
Pd5 Pd6 2.8656(4) . yes
Pd6 C22C 1.976(4) . yes
Pd6 N2C 1.998(4) . yes
Pd6 O2C 2.074(3) . yes
Pd6 O4C 2.156(2) . yes
F1C C26C 1.332(5) . ?
F2C C26C 1.329(5) . ?
F3C C26C 1.334(5) . ?
F4C C24C 1.311(5) . ?
F5C C24C 1.306(5) . ?
F6C C24C 1.284(5) . ?
O1C C25C 1.240(5) . ?
O2C C25C 1.245(5) . ?
O3C C23C 1.236(5) . ?
O4C C23C 1.245(4) . ?
N1C C1C 1.348(5) . ?
N1C C5C 1.372(4) . ?
N2C C12C 1.340(6) . ?
N2C C16C 1.376(5) . ?
C1C C2C 1.375(5) . ?
C1C H1C 0.96(4) . ?
C2C C3C 1.398(6) . ?
C2C H2C 0.81(3) . ?
C3C C4C 1.363(6) . ?
C3C H3C 0.89(4) . ?
C4C C5C 1.407(5) . ?
C4C H4C 0.98(3) . ?
C5C C6C 1.437(5) . ?
C6C C7C 1.389(5) . ?
C6C C11C 1.408(4) . ?
C7C C8C 1.384(6) . ?
C7C H7C 0.88(3) . ?
C8C C9C 1.387(5) . ?
C8C H8C 0.91(4) . ?
C9C C10C 1.389(6) . ?
C9C H9C 0.89(4) . ?
C10C C11C 1.372(5) . ?
C10C H10C 0.86(3) . ?
C12C C13C 1.385(7) . ?
C12C H12C 0.82(4) . ?
C13C C14C 1.414(8) . ?
C13C H13C 1.04(4) . ?
C14C C15C 1.339(9) . ?
C14C H14C 0.86(5) . ?
C15C C16C 1.413(8) . ?
C15C H15C 0.80(5) . ?
C16C C17C 1.412(7) . ?
C17C C22C 1.394(7) . ?
C17C C18C 1.412(6) . ?
C18C C19C 1.329(10) . ?
C18C H18C 0.83(5) . ?
C19C C20C 1.381(10) . ?
C19C H19C 0.88(5) . ?
C20C C21C 1.413(7) . ?
C20C H20C 0.83(4) . ?
C21C C22C 1.385(8) . ?
C21C H21C 0.85(5) . ?
C23C C24C 1.565(5) . ?
C25C C26C 1.540(6) . ?
