#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:06:48 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179231 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/51/4315160.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4315160
loop_
_publ_author_name
'Fuyan Han'
'Jie Zhang'
'Weiyin Yi'
'Zhengxing Zhang'
'Jingyi Yu'
'Linhong Weng'
'Xigeng Zhou'
_publ_section_title
;
 γ-Deprotonation of Anionic Bis(trimethylsilyl)amidolanthanide Complexes
 with a Countered [(TpMe2)2Ln]+ Cation
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2793
_journal_page_last               2798
_journal_paper_doi               10.1021/ic902296d
_journal_volume                  49
_journal_year                    2010
_chemical_formula_sum            'C48 H98 B2 Cl Er2 N15 Si6'
_chemical_formula_weight         1445.54
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           146
_symmetry_cell_setting           rhombohedral
_symmetry_space_group_name_Hall  'R 3'
_symmetry_space_group_name_H-M   'R 3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   16.712
_cell_length_b                   16.712
_cell_length_c                   22.056
_cell_measurement_reflns_used    927
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      20.198
_cell_measurement_theta_min      2.438
_cell_volume                     5334.752
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0973
_diffrn_reflns_av_sigmaI/netI    0.1153
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            7409
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.68
_exptl_absorpt_coefficient_mu    2.523
_exptl_absorpt_correction_T_max  0.7865
_exptl_absorpt_correction_T_min  0.7034
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.350
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2214
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         5.717
_refine_diff_density_min         -0.898
_refine_diff_density_rms         0.224
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.43(3)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     226
_refine_ls_number_reflns         4108
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.007
_refine_ls_R_factor_all          0.1018
_refine_ls_R_factor_gt           0.0772
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1018P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1714
_refine_ls_wR_factor_ref         0.1854
_reflns_number_gt                2954
_reflns_number_total             4108
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic902296d_si_001_3.cif
_cod_data_source_block           f80718a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Rhombohedral' changed to
'rhombohedral' according to the built-in table from CIF Core
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        5334.8
_cod_original_sg_symbol_H-M      'R 3'
_cod_database_code               4315160
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Er1 Er 0.0000 0.0000 0.06521(2) 0.0515(4) Uani 1 3 d S . .
B1 B 0.0000 0.0000 -0.0893(17) 0.066(8) Uani 1 3 d SD . .
H1B H 0.0000 0.0000 -0.139(2) 0.079 Uiso 1 3 d SD . .
B2 B 0.0000 0.0000 0.2225(10) 0.045(6) Uani 1 3 d SD . .
H2B H 0.0000 0.0000 0.2721(14) 0.054 Uiso 1 3 d SD . .
N1 N 0.0776(8) 0.0941(8) -0.0648(6) 0.055(3) Uani 1 1 d . . .
N2 N 0.0906(9) 0.1179(9) -0.0056(6) 0.061(3) Uani 1 1 d . . .
N3 N 0.0995(8) 0.0317(8) 0.1961(5) 0.054(3) Uani 1 1 d . . .
N4 N 0.1151(8) 0.0283(8) 0.1347(6) 0.054(3) Uani 1 1 d . . .
C1 C 0.1971(12) 0.2510(11) 0.0597(9) 0.077(5) Uani 1 1 d . . .
H1A H 0.1594 0.2102 0.0915 0.115 Uiso 1 1 calc R . .
H1C H 0.1929 0.3062 0.0605 0.115 Uiso 1 1 calc R . .
H1D H 0.2601 0.2666 0.0657 0.115 Uiso 1 1 calc R . .
C2 C 0.1641(11) 0.2044(12) 0.0002(8) 0.062(4) Uani 1 1 d . . .
C3 C 0.1945(16) 0.2340(15) -0.0566(9) 0.073(5) Uani 1 1 d . . .
H3A H 0.2429 0.2923 -0.0666 0.088 Uiso 1 1 calc R . .
C4 C 0.1433(12) 0.1655(11) -0.0972(9) 0.068(4) Uani 1 1 d . . .
C5 C 0.1501(17) 0.1671(14) -0.1651(10) 0.111(8) Uani 1 1 d . . .
H5A H 0.1042 0.1084 -0.1811 0.167 Uiso 1 1 calc R . .
H5B H 0.2104 0.1790 -0.1767 0.167 Uiso 1 1 calc R . .
H5C H 0.1400 0.2148 -0.1809 0.167 Uiso 1 1 calc R . .
C6 C 0.1830(15) 0.0720(16) 0.2947(10) 0.100(7) Uani 1 1 d . . .
H6A H 0.1230 0.0524 0.3116 0.150 Uiso 1 1 calc R . .
H6B H 0.2239 0.1357 0.3046 0.150 Uiso 1 1 calc R . .
H6C H 0.2068 0.0349 0.3112 0.150 Uiso 1 1 calc R . .
C7 C 0.1758(12) 0.0614(11) 0.2307(10) 0.074(5) Uani 1 1 d . . .
C8 C 0.2478(13) 0.0827(12) 0.1874(12) 0.083(6) Uani 1 1 d . . .
H8A H 0.3101 0.1065 0.1960 0.100 Uiso 1 1 calc R . .
C9 C 0.2100(11) 0.0625(12) 0.1336(10) 0.067(5) Uani 1 1 d . . .
C10 C 0.2535(12) 0.0683(13) 0.0723(10) 0.081(5) Uani 1 1 d . . .
H10A H 0.3187 0.0928 0.0772 0.122 Uiso 1 1 calc R . .
H10B H 0.2431 0.1082 0.0462 0.122 Uiso 1 1 calc R . .
H10C H 0.2262 0.0078 0.0547 0.122 Uiso 1 1 calc R . .
Er2 Er 0.6667 0.3333 0.93517(6) 0.0544(4) Uani 1 3 d S . .
Si1 Si 0.5567(3) 0.1045(3) 0.9605(3) 0.0818(15) Uani 1 1 d . . .
Si2 Si 0.4713(4) 0.1573(3) 0.8616(3) 0.0838(15) Uani 1 1 d . . .
Cl1 Cl 0.6667 0.3333 1.0508(5) 0.119(4) Uani 1 3 d S . .
N5 N 0.5565(8) 0.1859(8) 0.9143(6) 0.061(3) Uani 1 1 d . . .
C11 C 0.5210(18) -0.0101(14) 0.9218(16) 0.141(11) Uani 1 1 d . . .
H11A H 0.4887 -0.0596 0.9502 0.212 Uiso 1 1 calc R . .
H11B H 0.5750 -0.0105 0.9075 0.212 Uiso 1 1 calc R . .
H11C H 0.4813 -0.0180 0.8882 0.212 Uiso 1 1 calc R . .
C12 C 0.474(2) 0.074(2) 1.0312(15) 0.145(13) Uani 1 1 d . . .
H12A H 0.4424 0.0090 1.0384 0.217 Uiso 1 1 calc R . .
H12B H 0.4290 0.0932 1.0233 0.217 Uiso 1 1 calc R . .
H12C H 0.5093 0.1063 1.0664 0.217 Uiso 1 1 calc R . .
C13 C 0.6742(15) 0.1394(17) 0.9925(12) 0.110(7) Uani 1 1 d . . .
H13A H 0.6745 0.0857 1.0076 0.164 Uiso 1 1 calc R . .
H13B H 0.6879 0.1827 1.0250 0.164 Uiso 1 1 calc R . .
H13C H 0.7199 0.1677 0.9612 0.164 Uiso 1 1 calc R . .
C14 C 0.488(3) 0.2611(17) 0.8184(17) 0.146(13) Uani 1 1 d . . .
H14A H 0.4882 0.3056 0.8461 0.218 Uiso 1 1 calc R . .
H14B H 0.4382 0.2428 0.7899 0.218 Uiso 1 1 calc R . .
H14C H 0.5456 0.2881 0.7970 0.218 Uiso 1 1 calc R . .
C15 C 0.4725(17) 0.0815(16) 0.8001(12) 0.120(8) Uani 1 1 d . . .
H15A H 0.4632 0.0247 0.8173 0.180 Uiso 1 1 calc R . .
H15B H 0.5310 0.1123 0.7796 0.180 Uiso 1 1 calc R . .
H15C H 0.4240 0.0685 0.7718 0.180 Uiso 1 1 calc R . .
C16 C 0.3545(14) 0.0927(18) 0.8969(12) 0.114(8) Uani 1 1 d . . .
H16A H 0.3495 0.0414 0.9195 0.171 Uiso 1 1 calc R . .
H16B H 0.3082 0.0705 0.8657 0.171 Uiso 1 1 calc R . .
H16C H 0.3457 0.1330 0.9236 0.171 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Er Er -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N4 Er1 N4 81.0(5) 3 . ?
N4 Er1 N4 81.0(5) 3 2 ?
N4 Er1 N4 81.0(5) . 2 ?
N4 Er1 N2 99.3(4) 3 2 ?
N4 Er1 N2 179.3(4) . 2 ?
N4 Er1 N2 98.4(4) 2 2 ?
N4 Er1 N2 98.4(4) 3 3 ?
N4 Er1 N2 99.3(4) . 3 ?
N4 Er1 N2 179.3(5) 2 3 ?
N2 Er1 N2 81.4(5) 2 3 ?
N4 Er1 N2 179.3(4) 3 . ?
N4 Er1 N2 98.4(4) . . ?
N4 Er1 N2 99.3(4) 2 . ?
N2 Er1 N2 81.4(5) 2 . ?
N2 Er1 N2 81.4(5) 3 . ?
N1 B1 N1 108.6(15) 3 . ?
N1 B1 N1 108.6(15) 3 2 ?
N1 B1 N1 108.6(15) . 2 ?
N1 B1 H1B 110.4(14) 3 . ?
N1 B1 H1B 110.4(14) . . ?
N1 B1 H1B 110.4(14) 2 . ?
N3 B2 N3 107.3(10) 2 . ?
N3 B2 N3 107.3(10) 2 3 ?
N3 B2 N3 107.3(10) . 3 ?
N3 B2 H2B 111.6(9) 2 . ?
N3 B2 H2B 111.6(9) . . ?
N3 B2 H2B 111.6(9) 3 . ?
C4 N1 N2 108.1(12) . . ?
C4 N1 B1 127.5(18) . . ?
N2 N1 B1 124.4(17) . . ?
N1 N2 C2 109.3(12) . . ?
N1 N2 Er1 116.8(9) . . ?
C2 N2 Er1 133.2(11) . . ?
C7 N3 N4 113.8(14) . . ?
C7 N3 B2 123.9(15) . . ?
N4 N3 B2 122.3(12) . . ?
N3 N4 C9 101.5(13) . . ?
N3 N4 Er1 120.1(8) . . ?
C9 N4 Er1 137.1(12) . . ?
C2 C1 H1A 109.5 . . ?
C2 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
C2 C1 H1D 109.5 . . ?
H1A C1 H1D 109.5 . . ?
H1C C1 H1D 109.5 . . ?
C3 C2 N2 106.1(16) . . ?
C3 C2 C1 131.0(18) . . ?
N2 C2 C1 122.9(16) . . ?
C2 C3 C4 109.7(19) . . ?
C2 C3 H3A 125.1 . . ?
C4 C3 H3A 125.1 . . ?
N1 C4 C3 106.6(17) . . ?
N1 C4 C5 124.3(16) . . ?
C3 C4 C5 128.9(17) . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C7 C6 H6A 109.5 . . ?
C7 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C7 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
N3 C7 C6 127.8(18) . . ?
N3 C7 C8 103.7(19) . . ?
C6 C7 C8 128.5(18) . . ?
C9 C8 C7 107.6(17) . . ?
C9 C8 H8A 126.2 . . ?
C7 C8 H8A 126.2 . . ?
C8 C9 N4 113.3(18) . . ?
C8 C9 C10 129.8(19) . . ?
N4 C9 C10 117.0(18) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
N5 Er2 N5 116.0(2) . 2_655 ?
N5 Er2 N5 116.0(2) . 3_665 ?
N5 Er2 N5 116.0(2) 2_655 3_665 ?
N5 Er2 Cl1 101.7(4) . . ?
N5 Er2 Cl1 101.7(4) 2_655 . ?
N5 Er2 Cl1 101.7(4) 3_665 . ?
N5 Er2 Si1 104.3(3) . 3_665 ?
N5 Er2 Si1 137.9(3) 2_655 3_665 ?
N5 Er2 Si1 27.3(4) 3_665 3_665 ?
Cl1 Er2 Si1 80.42(12) . 3_665 ?
N5 Er2 Si1 137.9(3) . 2_655 ?
N5 Er2 Si1 27.3(4) 2_655 2_655 ?
N5 Er2 Si1 104.3(3) 3_665 2_655 ?
Cl1 Er2 Si1 80.42(12) . 2_655 ?
Si1 Er2 Si1 117.28(7) 3_665 2_655 ?
N5 Er2 Si1 27.3(4) . . ?
N5 Er2 Si1 104.3(3) 2_655 . ?
N5 Er2 Si1 137.9(3) 3_665 . ?
Cl1 Er2 Si1 80.42(12) . . ?
Si1 Er2 Si1 117.29(7) 3_665 . ?
Si1 Er2 Si1 117.29(6) 2_655 . ?
N5 Si1 C13 113.3(10) . . ?
N5 Si1 C11 114.3(11) . . ?
C13 Si1 C11 103.6(11) . . ?
N5 Si1 C12 113.2(11) . . ?
C13 Si1 C12 105.9(14) . . ?
C11 Si1 C12 105.7(14) . . ?
N5 Si1 Er2 37.7(4) . . ?
C13 Si1 Er2 79.5(8) . . ?
C11 Si1 Er2 142.2(11) . . ?
C12 Si1 Er2 109.6(10) . . ?
N5 Si2 C16 111.3(10) . . ?
N5 Si2 C15 113.1(9) . . ?
C16 Si2 C15 105.9(11) . . ?
N5 Si2 C14 111.7(11) . . ?
C16 Si2 C14 112.1(15) . . ?
C15 Si2 C14 102.2(14) . . ?
Si1 N5 Si2 121.2(8) . . ?
Si1 N5 Er2 114.9(7) . . ?
Si2 N5 Er2 123.5(7) . . ?
Si1 C11 H11A 109.5 . . ?
Si1 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
Si1 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
Si1 C12 H12A 109.5 . . ?
Si1 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
Si1 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
Si1 C13 H13A 109.5 . . ?
Si1 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
Si1 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
Si2 C14 H14A 109.5 . . ?
Si2 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
Si2 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
Si2 C15 H15A 109.5 . . ?
Si2 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
Si2 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
Si2 C16 H16A 109.5 . . ?
Si2 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
Si2 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Er1 N4 2.316(12) 3 ?
Er1 N4 2.316(12) . ?
Er1 N4 2.316(12) 2 ?
Er1 N2 2.372(12) 2 ?
Er1 N2 2.372(12) 3 ?
Er1 N2 2.372(12) . ?
B1 N1 1.552(17) 3 ?
B1 N1 1.552(17) . ?
B1 N1 1.552(17) 2 ?
B1 H1B 1.10(2) . ?
B2 N3 1.582(14) 2 ?
B2 N3 1.582(14) . ?
B2 N3 1.582(14) 3 ?
B2 H2B 1.09(2) . ?
N1 C4 1.35(2) . ?
N1 N2 1.352(18) . ?
N2 C2 1.36(2) . ?
N3 C7 1.35(2) . ?
N3 N4 1.386(16) . ?
N4 C9 1.39(2) . ?
C1 C2 1.48(3) . ?
C1 H1A 0.9600 . ?
C1 H1C 0.9600 . ?
C1 H1D 0.9600 . ?
C2 C3 1.35(3) . ?
C3 C4 1.37(3) . ?
C3 H3A 0.9300 . ?
C4 C5 1.50(3) . ?
C5 H5A 0.9600 . ?
C5 H5B 0.9600 . ?
C5 H5C 0.9600 . ?
C6 C7 1.42(3) . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C7 C8 1.43(3) . ?
C8 C9 1.31(3) . ?
C8 H8A 0.9300 . ?
C9 C10 1.52(3) . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
Er2 N5 2.267(12) . ?
Er2 N5 2.267(12) 2_655 ?
Er2 N5 2.267(12) 3_665 ?
Er2 Cl1 2.551(12) . ?
Er2 Si1 3.360(5) 3_665 ?
Er2 Si1 3.360(5) 2_655 ?
Er2 Si1 3.360(5) . ?
Si1 N5 1.702(15) . ?
Si1 C13 1.882(19) . ?
Si1 C11 1.90(2) . ?
Si1 C12 1.98(3) . ?
Si2 N5 1.710(14) . ?
Si2 C16 1.86(2) . ?
Si2 C15 1.86(2) . ?
Si2 C14 1.87(3) . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C15 H15A 0.9600 . ?
C15 H15B 0.9600 . ?
C15 H15C 0.9600 . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
