#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:13:37 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179236 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/56/4315645.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4315645
loop_
_publ_author_name
'Mathias Kessler'
'Carsten Knapp'
'Vanessa Sagawe'
'Harald Scherer'
'Rabiya Uzun'
_publ_section_title
;
 Synthesis, Characterization, and Crystal Structures of Silylium Compounds
 of the Weakly Coordinating Dianion [B12Cl12]2-
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5223
_journal_page_last               5230
_journal_paper_doi               10.1021/ic100337k
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C18 H42 B12 Cl12 Si2'
_chemical_formula_sum            'C18 H42 B12 Cl12 Si2'
_chemical_formula_weight         869.82
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 96.40(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.652(2)
_cell_length_b                   15.584(3)
_cell_length_c                   24.034(5)
_cell_measurement_reflns_used    1000
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.01
_cell_volume                     3964.8(14)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2007)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2007)'
_computing_molecular_graphics    Diamond
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean 10.000
_diffrn_measured_fraction_theta_full 0.882
_diffrn_measured_fraction_theta_max 0.882
_diffrn_measurement_details
;
scan:
    Number of images: 21
               Slice: 20.0000 - 125.0000
         Image width: 5.0000
            Exp time: 60.0000
       Rotation axis: Omega
               Omega: 0.0000
                 Chi: 54.0000
                 Phi: 90.0000
                 XTD: 127.4000
              2theta: -0.4187
;
_diffrn_measurement_device_type  'Rigaku R-AXIS Spider'
_diffrn_measurement_method       dtprofit.ref
_diffrn_radiation_detector       RX
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0314
_diffrn_reflns_av_sigmaI/netI    0.0284
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            28809
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.01
_exptl_absorpt_coefficient_mu    0.915
_exptl_absorpt_correction_T_max  0.660
_exptl_absorpt_correction_T_min  0.516
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
March 2001 T Higashi
;
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.457
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             1768
_exptl_crystal_size_max          0.53
_exptl_crystal_size_mid          0.50
_exptl_crystal_size_min          0.45
_refine_diff_density_max         0.767
_refine_diff_density_min         -0.776
_refine_diff_density_rms         0.205
_refine_ls_extinction_coef       0.0033(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.128
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     418
_refine_ls_number_reflns         8022
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.128
_refine_ls_R_factor_all          0.0480
_refine_ls_R_factor_gt           0.0361
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0761P)²+4.5801P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1076
_refine_ls_wR_factor_ref         0.1372
_reflns_number_gt                6832
_reflns_number_total             8022
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic100337k_si_002_2.cif
_cod_data_source_block           ck013
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        3964.9(14)
_cod_database_code               4315645
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
B1 B 0.4516(3) 0.17607(19) 0.15678(14) 0.0165(6) Uani 1 1 d . . .
Cl1 Cl 0.53345(7) 0.07639(5) 0.16662(3) 0.02449(18) Uani 1 1 d . . .
B2 B 0.4295(3) 0.23117(19) 0.09232(14) 0.0159(6) Uani 1 1 d . . .
Cl2 Cl 0.47092(7) 0.18233(4) 0.02651(3) 0.01964(16) Uani 1 1 d . . .
B3 B 0.2976(3) 0.18293(19) 0.11887(14) 0.0153(6) Uani 1 1 d . . .
Cl3 Cl 0.22137(7) 0.09016(4) 0.08764(3) 0.02270(17) Uani 1 1 d . . .
B4 B 0.3175(3) 0.2009(2) 0.19209(13) 0.0158(6) Uani 1 1 d . . .
Cl4 Cl 0.27620(7) 0.11440(5) 0.23953(3) 0.02301(17) Uani 1 1 d . . .
B5 B 0.4629(3) 0.2555(2) 0.21102(14) 0.0193(7) Uani 1 1 d . . .
Cl5 Cl 0.55605(8) 0.23595(6) 0.27548(3) 0.0328(2) Uani 1 1 d . . .
B6 B 0.5329(3) 0.2754(2) 0.14771(14) 0.0180(6) Uani 1 1 d . . .
Cl6 Cl 0.70048(7) 0.28016(5) 0.14810(3) 0.02558(18) Uani 1 1 d . . .
B7 B 0.2813(3) 0.2863(2) 0.08551(14) 0.0181(6) Uani 1 1 d . . .
Cl7 Cl 0.19000(8) 0.30001(6) 0.01981(3) 0.0296(2) Uani 1 1 d . . .
B8 B 0.2110(3) 0.2670(2) 0.14906(14) 0.0168(6) Uani 1 1 d . . .
Cl8 Cl 0.04402(7) 0.26274(5) 0.14948(3) 0.02137(17) Uani 1 1 d . . .
B9 B 0.3147(3) 0.3122(2) 0.20625(14) 0.0191(7) Uani 1 1 d . . .
Cl9 Cl 0.25533(7) 0.35672(5) 0.26643(3) 0.02561(18) Uani 1 1 d . . .
B10 B 0.4466(3) 0.3593(2) 0.17786(16) 0.0218(7) Uani 1 1 d . . .
Cl10 Cl 0.52267(8) 0.45077(5) 0.21021(4) 0.0371(2) Uani 1 1 d . . .
B11 B 0.4272(3) 0.3435(2) 0.10399(15) 0.0192(7) Uani 1 1 d . . .
Cl11 Cl 0.48143(8) 0.41911(5) 0.05612(4) 0.0313(2) Uani 1 1 d . . .
B12 B 0.2924(3) 0.3655(2) 0.13998(15) 0.0204(7) Uani 1 1 d . . .
Cl12 Cl 0.21078(8) 0.46516(5) 0.13069(4) 0.0333(2) Uani 1 1 d . . .
Si1 Si 0.66912(8) 0.17752(5) -0.00468(3) 0.01745(18) Uani 1 1 d . . .
C1 C 0.7144(3) 0.29355(19) -0.00570(13) 0.0218(6) Uani 1 1 d . . .
H1 H 0.6927 0.3192 0.0302 0.022(4) Uiso 1 1 calc R . .
C2 C 0.8567(3) 0.3064(2) -0.00710(17) 0.0334(8) Uani 1 1 d . . .
H2A H 0.8843 0.2746 -0.0387 0.0404(19) Uiso 1 1 calc R . .
H2B H 0.9023 0.2853 0.0279 0.0404(19) Uiso 1 1 calc R . .
H2C H 0.8745 0.3676 -0.0113 0.0404(19) Uiso 1 1 calc R . .
C3 C 0.6388(3) 0.3432(2) -0.05343(15) 0.0296(7) Uani 1 1 d . . .
H3A H 0.6599 0.4043 -0.0502 0.0404(19) Uiso 1 1 calc R . .
H3B H 0.5482 0.3355 -0.0511 0.0404(19) Uiso 1 1 calc R . .
H3C H 0.6600 0.3215 -0.0895 0.0404(19) Uiso 1 1 calc R . .
C4 C 0.6156(3) 0.12276(19) -0.07274(12) 0.0207(6) Uani 1 1 d . . .
H4 H 0.6076 0.0603 -0.0643 0.022(4) Uiso 1 1 calc R . .
C5 C 0.7226(3) 0.1315(2) -0.11051(14) 0.0282(7) Uani 1 1 d . . .
H5A H 0.7024 0.0970 -0.1444 0.0404(19) Uiso 1 1 calc R . .
H5B H 0.8020 0.1113 -0.0903 0.0404(19) Uiso 1 1 calc R . .
H5C H 0.7314 0.1919 -0.1209 0.0404(19) Uiso 1 1 calc R . .
C6 C 0.4890(3) 0.1513(2) -0.10422(13) 0.0259(7) Uani 1 1 d . . .
H6A H 0.4925 0.2128 -0.1126 0.0404(19) Uiso 1 1 calc R . .
H6B H 0.4209 0.1405 -0.0809 0.0404(19) Uiso 1 1 calc R . .
H6C H 0.4729 0.1189 -0.1392 0.0404(19) Uiso 1 1 calc R . .
C7 C 0.7600(3) 0.10509(19) 0.04734(13) 0.0227(6) Uani 1 1 d . . .
H7 H 0.7664 0.1337 0.0848 0.022(4) Uiso 1 1 calc R . .
C8 C 0.8950(3) 0.0892(2) 0.03246(18) 0.0365(8) Uani 1 1 d . . .
H8A H 0.9404 0.0523 0.0610 0.0404(19) Uiso 1 1 calc R . .
H8B H 0.9393 0.1441 0.0311 0.0404(19) Uiso 1 1 calc R . .
H8C H 0.8911 0.0610 -0.0042 0.0404(19) Uiso 1 1 calc R . .
C9 C 0.6960(3) 0.0177(2) 0.05243(14) 0.0271(7) Uani 1 1 d . . .
H9A H 0.7003 -0.0151 0.0179 0.0404(19) Uiso 1 1 calc R . .
H9B H 0.6074 0.0264 0.0585 0.0404(19) Uiso 1 1 calc R . .
H9C H 0.7394 -0.0139 0.0842 0.0404(19) Uiso 1 1 calc R . .
Si2 Si 0.11089(8) 0.09385(5) 0.29558(3) 0.01762(18) Uani 1 1 d . . .
C10 C 0.0192(3) 0.01141(19) 0.25201(13) 0.0225(6) Uani 1 1 d . . .
H10 H -0.0549 -0.0030 0.2724 0.022(4) Uiso 1 1 calc R . .
C11 C -0.0362(4) 0.0422(2) 0.19345(15) 0.0328(8) Uani 1 1 d . . .
H11A H 0.0326 0.0530 0.1705 0.0404(19) Uiso 1 1 calc R . .
H11B H -0.0841 0.0953 0.1970 0.0404(19) Uiso 1 1 calc R . .
H11C H -0.0924 -0.0021 0.1756 0.0404(19) Uiso 1 1 calc R . .
C12 C 0.0924(3) -0.0729(2) 0.24794(16) 0.0308(7) Uani 1 1 d . . .
H12A H 0.0381 -0.1151 0.2268 0.0404(19) Uiso 1 1 calc R . .
H12B H 0.1182 -0.0950 0.2857 0.0404(19) Uiso 1 1 calc R . .
H12C H 0.1675 -0.0624 0.2288 0.0404(19) Uiso 1 1 calc R . .
C13 C 0.0284(3) 0.19787(19) 0.30422(14) 0.0225(6) Uani 1 1 d . . .
H13 H 0.0387 0.2340 0.2706 0.022(4) Uiso 1 1 calc R . .
C14 C 0.0796(4) 0.2492(2) 0.35624(14) 0.0311(8) Uani 1 1 d . . .
H14A H 0.0351 0.3042 0.3565 0.0404(19) Uiso 1 1 calc R . .
H14B H 0.1701 0.2596 0.3555 0.0404(19) Uiso 1 1 calc R . .
H14C H 0.0663 0.2166 0.3900 0.0404(19) Uiso 1 1 calc R . .
C15 C -0.1139(3) 0.1821(2) 0.30549(19) 0.0387(9) Uani 1 1 d . . .
H15A H -0.1268 0.1456 0.3376 0.0404(19) Uiso 1 1 calc R . .
H15B H -0.1484 0.1535 0.2708 0.0404(19) Uiso 1 1 calc R . .
H15C H -0.1570 0.2370 0.3089 0.0404(19) Uiso 1 1 calc R . .
C16 C 0.2153(3) 0.04732(19) 0.35552(12) 0.0195(6) Uani 1 1 d . . .
H16 H 0.2589 -0.0029 0.3403 0.022(4) Uiso 1 1 calc R . .
C17 C 0.3195(3) 0.1056(2) 0.38398(14) 0.0277(7) Uani 1 1 d . . .
H17A H 0.2812 0.1519 0.4039 0.0404(19) Uiso 1 1 calc R . .
H17B H 0.3681 0.1302 0.3556 0.0404(19) Uiso 1 1 calc R . .
H17C H 0.3758 0.0718 0.4106 0.0404(19) Uiso 1 1 calc R . .
C18 C 0.1333(3) 0.0111(2) 0.39874(15) 0.0332(8) Uani 1 1 d . . .
H18A H 0.1875 -0.0171 0.4290 0.0404(19) Uiso 1 1 calc R . .
H18B H 0.0734 -0.0307 0.3806 0.0404(19) Uiso 1 1 calc R . .
H18C H 0.0867 0.0580 0.4143 0.0404(19) Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B2 B1 B4 106.1(2) . . ?
B2 B1 Cl1 123.8(2) . . ?
B4 B1 Cl1 122.1(2) . . ?
B2 B1 B3 59.88(18) . . ?
B4 B1 B3 59.46(18) . . ?
Cl1 B1 B3 121.8(2) . . ?
B2 B1 B5 107.1(2) . . ?
B4 B1 B5 59.77(18) . . ?
Cl1 B1 B5 120.9(2) . . ?
B3 B1 B5 108.2(2) . . ?
B2 B1 B6 59.58(18) . . ?
B4 B1 B6 107.0(2) . . ?
Cl1 B1 B6 122.0(2) . . ?
B3 B1 B6 108.3(2) . . ?
B5 B1 B6 59.95(18) . . ?
B1 B2 B6 61.18(19) . . ?
B1 B2 B11 110.1(2) . . ?
B6 B2 B11 61.00(19) . . ?
B1 B2 B3 60.74(18) . . ?
B6 B2 B3 110.2(2) . . ?
B11 B2 B3 109.6(2) . . ?
B1 B2 B7 110.1(2) . . ?
B6 B2 B7 110.5(2) . . ?
B11 B2 B7 60.83(18) . . ?
B3 B2 B7 60.67(18) . . ?
B1 B2 Cl2 121.9(2) . . ?
B6 B2 Cl2 127.9(2) . . ?
B11 B2 Cl2 123.3(2) . . ?
B3 B2 Cl2 114.00(19) . . ?
B7 B2 Cl2 114.3(2) . . ?
B2 Cl2 Si1 126.97(11) . . ?
B4 B3 B2 106.2(2) . . ?
B4 B3 Cl3 123.0(2) . . ?
B2 B3 Cl3 122.3(2) . . ?
B4 B3 B1 60.12(18) . . ?
B2 B3 B1 59.37(18) . . ?
Cl3 B3 B1 121.0(2) . . ?
B4 B3 B7 107.2(2) . . ?
B2 B3 B7 60.10(18) . . ?
Cl3 B3 B7 121.4(2) . . ?
B1 B3 B7 108.6(2) . . ?
B4 B3 B8 59.65(18) . . ?
B2 B3 B8 107.4(2) . . ?
Cl3 B3 B8 122.0(2) . . ?
B1 B3 B8 108.7(2) . . ?
B7 B3 B8 59.96(17) . . ?
B9 B4 B3 110.1(2) . . ?
B9 B4 B8 61.30(18) . . ?
B3 B4 B8 61.02(18) . . ?
B9 B4 B5 60.98(19) . . ?
B3 B4 B5 109.5(2) . . ?
B8 B4 B5 110.6(2) . . ?
B9 B4 B1 109.6(2) . . ?
B3 B4 B1 60.42(18) . . ?
B8 B4 B1 110.0(2) . . ?
B5 B4 B1 60.37(18) . . ?
B9 B4 Cl4 125.9(2) . . ?
B3 B4 Cl4 119.1(2) . . ?
B8 B4 Cl4 126.9(2) . . ?
B5 B4 Cl4 116.8(2) . . ?
B1 B4 Cl4 113.17(19) . . ?
B4 Cl4 Si2 134.11(11) . . ?
Cl5 B5 B4 121.8(2) . . ?
Cl5 B5 B1 120.2(2) . . ?
B4 B5 B1 59.87(18) . . ?
Cl5 B5 B6 121.8(2) . . ?
B4 B5 B6 107.3(2) . . ?
B1 B5 B6 60.20(18) . . ?
Cl5 B5 B9 122.8(2) . . ?
B4 B5 B9 59.14(18) . . ?
B1 B5 B9 107.8(2) . . ?
B6 B5 B9 107.8(2) . . ?
Cl5 B5 B10 124.0(2) . . ?
B4 B5 B10 106.1(2) . . ?
B1 B5 B10 107.6(2) . . ?
B6 B5 B10 59.95(19) . . ?
B9 B5 B10 59.43(19) . . ?
B2 B6 Cl6 123.9(2) . . ?
B2 B6 B5 106.7(2) . . ?
Cl6 B6 B5 120.8(2) . . ?
B2 B6 B10 106.4(2) . . ?
Cl6 B6 B10 121.6(2) . . ?
B5 B6 B10 60.27(19) . . ?
B2 B6 B11 59.57(18) . . ?
Cl6 B6 B11 122.6(2) . . ?
B5 B6 B11 107.7(2) . . ?
B10 B6 B11 59.39(19) . . ?
B2 B6 B1 59.23(17) . . ?
Cl6 B6 B1 122.0(2) . . ?
B5 B6 B1 59.84(18) . . ?
B10 B6 B1 107.6(2) . . ?
B11 B6 B1 107.4(2) . . ?
Cl7 B7 B2 122.0(2) . . ?
Cl7 B7 B12 123.5(2) . . ?
B2 B7 B12 106.1(2) . . ?
Cl7 B7 B3 121.4(2) . . ?
B2 B7 B3 59.23(17) . . ?
B12 B7 B3 107.2(2) . . ?
Cl7 B7 B8 122.5(2) . . ?
B2 B7 B8 106.8(2) . . ?
B12 B7 B8 59.70(18) . . ?
B3 B7 B8 60.08(18) . . ?
Cl7 B7 B11 122.1(2) . . ?
B2 B7 B11 59.15(18) . . ?
B12 B7 B11 59.69(19) . . ?
B3 B7 B11 107.1(2) . . ?
B8 B7 B11 107.6(2) . . ?
B4 B8 Cl8 123.3(2) . . ?
B4 B8 B12 106.4(2) . . ?
Cl8 B8 B12 122.1(2) . . ?
B4 B8 B7 106.9(2) . . ?
Cl8 B8 B7 121.4(2) . . ?
B12 B8 B7 59.99(18) . . ?
B4 B8 B3 59.32(17) . . ?
Cl8 B8 B3 122.1(2) . . ?
B12 B8 B3 107.3(2) . . ?
B7 B8 B3 59.95(17) . . ?
B4 B8 B9 59.10(18) . . ?
Cl8 B8 B9 122.5(2) . . ?
B12 B8 B9 59.66(19) . . ?
B7 B8 B9 107.7(2) . . ?
B3 B8 B9 107.0(2) . . ?
B4 B9 Cl9 123.6(2) . . ?
B4 B9 B10 107.4(2) . . ?
Cl9 B9 B10 121.0(2) . . ?
B4 B9 B12 106.7(2) . . ?
Cl9 B9 B12 121.1(2) . . ?
B10 B9 B12 60.1(2) . . ?
B4 B9 B5 59.88(18) . . ?
Cl9 B9 B5 121.8(2) . . ?
B10 B9 B5 60.34(19) . . ?
B12 B9 B5 108.3(2) . . ?
B4 B9 B8 59.60(18) . . ?
Cl9 B9 B8 121.8(2) . . ?
B10 B9 B8 108.1(2) . . ?
B12 B9 B8 59.64(19) . . ?
B5 B9 B8 108.4(2) . . ?
Cl10 B10 B11 123.0(2) . . ?
Cl10 B10 B9 120.2(2) . . ?
B11 B10 B9 108.3(2) . . ?
Cl10 B10 B12 121.9(2) . . ?
B11 B10 B12 60.2(2) . . ?
B9 B10 B12 60.03(19) . . ?
Cl10 B10 B6 122.1(2) . . ?
B11 B10 B6 60.34(19) . . ?
B9 B10 B6 108.3(2) . . ?
B12 B10 B6 108.4(2) . . ?
Cl10 B10 B5 120.6(2) . . ?
B11 B10 B5 108.1(2) . . ?
B9 B10 B5 60.24(19) . . ?
B12 B10 B5 108.1(2) . . ?
B6 B10 B5 59.79(19) . . ?
B2 B11 B10 107.0(2) . . ?
B2 B11 Cl11 122.5(2) . . ?
B10 B11 Cl11 122.7(2) . . ?
B2 B11 B12 107.0(2) . . ?
B10 B11 B12 60.15(19) . . ?
Cl11 B11 B12 121.2(2) . . ?
B2 B11 B6 59.42(18) . . ?
B10 B11 B6 60.26(19) . . ?
Cl11 B11 B6 122.6(2) . . ?
B12 B11 B6 108.4(2) . . ?
B2 B11 B7 60.02(18) . . ?
B10 B11 B7 108.4(2) . . ?
Cl11 B11 B7 119.9(2) . . ?
B12 B11 B7 59.88(19) . . ?
B6 B11 B7 108.6(2) . . ?
Cl12 B12 B8 121.8(2) . . ?
Cl12 B12 B9 122.1(2) . . ?
B8 B12 B9 60.70(18) . . ?
Cl12 B12 B10 121.2(2) . . ?
B8 B12 B10 108.8(2) . . ?
B9 B12 B10 59.9(2) . . ?
Cl12 B12 B11 120.9(2) . . ?
B8 B12 B11 108.7(2) . . ?
B9 B12 B11 107.8(2) . . ?
B10 B12 B11 59.68(19) . . ?
Cl12 B12 B7 121.1(2) . . ?
B8 B12 B7 60.31(18) . . ?
B9 B12 B7 108.7(2) . . ?
B10 B12 B7 108.4(2) . . ?
B11 B12 B7 60.43(19) . . ?
C1 Si1 C7 118.43(14) . . ?
C1 Si1 C4 118.78(14) . . ?
C7 Si1 C4 113.09(14) . . ?
C1 Si1 Cl2 102.59(10) . . ?
C7 Si1 Cl2 103.03(11) . . ?
C4 Si1 Cl2 95.60(10) . . ?
C2 C1 C3 110.8(3) . . ?
C2 C1 Si1 112.5(2) . . ?
C3 C1 Si1 112.5(2) . . ?
C2 C1 H1 106.9 . . ?
C3 C1 H1 106.9 . . ?
Si1 C1 H1 106.9 . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C6 C4 C5 110.5(3) . . ?
C6 C4 Si1 117.5(2) . . ?
C5 C4 Si1 107.5(2) . . ?
C6 C4 H4 106.9 . . ?
C5 C4 H4 106.9 . . ?
Si1 C4 H4 106.9 . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C4 C6 H6A 109.5 . . ?
C4 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C4 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C9 C7 C8 108.1(3) . . ?
C9 C7 Si1 112.8(2) . . ?
C8 C7 Si1 111.6(2) . . ?
C9 C7 H7 108.1 . . ?
C8 C7 H7 108.1 . . ?
Si1 C7 H7 108.1 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C7 C9 H9A 109.5 . . ?
C7 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C7 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C10 Si2 C16 113.32(14) . . ?
C10 Si2 C13 115.95(15) . . ?
C16 Si2 C13 119.94(14) . . ?
C10 Si2 Cl4 98.67(11) . . ?
C16 Si2 Cl4 94.32(10) . . ?
C13 Si2 Cl4 109.69(10) . . ?
C12 C10 C11 110.7(3) . . ?
C12 C10 Si2 112.8(2) . . ?
C11 C10 Si2 115.0(2) . . ?
C12 C10 H10 105.9 . . ?
C11 C10 H10 105.9 . . ?
Si2 C10 H10 105.9 . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 C15 109.2(3) . . ?
C14 C13 Si2 114.5(2) . . ?
C15 C13 Si2 109.9(2) . . ?
C14 C13 H13 107.7 . . ?
C15 C13 H13 107.7 . . ?
Si2 C13 H13 107.7 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C13 C15 H15A 109.5 . . ?
C13 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C13 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C17 C16 C18 110.7(3) . . ?
C17 C16 Si2 117.0(2) . . ?
C18 C16 Si2 109.3(2) . . ?
C17 C16 H16 106.4 . . ?
C18 C16 H16 106.4 . . ?
Si2 C16 H16 106.4 . . ?
C16 C17 H17A 109.5 . . ?
C16 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C16 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C16 C18 H18A 109.5 . . ?
C16 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C16 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B1 B2 1.764(5) . ?
B1 B4 1.783(4) . ?
B1 Cl1 1.784(3) . ?
B1 B3 1.789(5) . ?
B1 B5 1.792(4) . ?
B1 B6 1.799(4) . ?
B2 B6 1.770(5) . ?
B2 B11 1.773(4) . ?
B2 B3 1.773(4) . ?
B2 B7 1.789(5) . ?
B2 Cl2 1.852(3) . ?
Cl2 Si1 2.3190(12) . ?
B3 B4 1.771(5) . ?
B3 Cl3 1.782(3) . ?
B3 B7 1.799(4) . ?
B3 B8 1.802(4) . ?
B4 B9 1.768(4) . ?
B4 B8 1.777(5) . ?
B4 B5 1.782(5) . ?
B4 Cl4 1.850(3) . ?
Cl4 Si2 2.3550(12) . ?
B5 Cl5 1.771(4) . ?
B5 B6 1.794(5) . ?
B5 B9 1.801(5) . ?
B5 B10 1.803(5) . ?
B6 Cl6 1.785(3) . ?
B6 B10 1.797(5) . ?
B6 B11 1.799(5) . ?
B7 Cl7 1.773(3) . ?
B7 B12 1.794(5) . ?
B7 B8 1.800(5) . ?
B7 B11 1.804(5) . ?
B8 Cl8 1.781(3) . ?
B8 B12 1.788(5) . ?
B8 B9 1.808(5) . ?
B9 Cl9 1.783(3) . ?
B9 B10 1.786(5) . ?
B9 B12 1.789(5) . ?
B10 Cl10 1.775(3) . ?
B10 B11 1.781(5) . ?
B10 B12 1.790(5) . ?
B11 Cl11 1.787(3) . ?
B11 B12 1.790(5) . ?
B12 Cl12 1.781(3) . ?
Si1 C1 1.872(3) . ?
Si1 C7 1.872(3) . ?
Si1 C4 1.876(3) . ?
C1 C2 1.534(4) . ?
C1 C3 1.535(4) . ?
C1 H1 1.0000 . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C4 C6 1.537(4) . ?
C4 C5 1.540(4) . ?
C4 H4 1.0000 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C9 1.534(4) . ?
C7 C8 1.539(5) . ?
C7 H7 1.0000 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
Si2 C10 1.863(3) . ?
Si2 C16 1.866(3) . ?
Si2 C13 1.867(3) . ?
C10 C12 1.536(4) . ?
C10 C11 1.541(5) . ?
C10 H10 1.0000 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.532(5) . ?
C13 C15 1.539(5) . ?
C13 H13 1.0000 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 C17 1.535(4) . ?
C16 C18 1.537(4) . ?
C16 H16 1.0000 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
B4 B1 B2 B6 100.6(2) . . . . ?
Cl1 B1 B2 B6 -110.3(3) . . . . ?
B3 B1 B2 B6 139.5(2) . . . . ?
B5 B1 B2 B6 38.0(2) . . . . ?
B4 B1 B2 B11 62.9(3) . . . . ?
Cl1 B1 B2 B11 -148.0(2) . . . . ?
B3 B1 B2 B11 101.8(2) . . . . ?
B5 B1 B2 B11 0.3(3) . . . . ?
B6 B1 B2 B11 -37.7(2) . . . . ?
B4 B1 B2 B3 -38.9(2) . . . . ?
Cl1 B1 B2 B3 110.1(3) . . . . ?
B5 B1 B2 B3 -101.5(2) . . . . ?
B6 B1 B2 B3 -139.5(2) . . . . ?
B4 B1 B2 B7 -2.3(3) . . . . ?
Cl1 B1 B2 B7 146.7(2) . . . . ?
B3 B1 B2 B7 36.5(2) . . . . ?
B5 B1 B2 B7 -65.0(3) . . . . ?
B6 B1 B2 B7 -103.0(2) . . . . ?
B4 B1 B2 Cl2 -140.4(2) . . . . ?
Cl1 B1 B2 Cl2 8.6(4) . . . . ?
B3 B1 B2 Cl2 -101.6(2) . . . . ?
B5 B1 B2 Cl2 156.9(2) . . . . ?
B6 B1 B2 Cl2 118.9(3) . . . . ?
B1 B2 Cl2 Si1 -82.6(2) . . . . ?
B6 B2 Cl2 Si1 -6.2(3) . . . . ?
B11 B2 Cl2 Si1 70.9(3) . . . . ?
B3 B2 Cl2 Si1 -151.94(15) . . . . ?
B7 B2 Cl2 Si1 140.85(16) . . . . ?
B1 B2 B3 B4 39.2(2) . . . . ?
B6 B2 B3 B4 1.9(3) . . . . ?
B11 B2 B3 B4 -63.4(3) . . . . ?
B7 B2 B3 B4 -100.9(2) . . . . ?
Cl2 B2 B3 B4 153.69(19) . . . . ?
B1 B2 B3 Cl3 -109.5(2) . . . . ?
B6 B2 B3 Cl3 -146.8(2) . . . . ?
B11 B2 B3 Cl3 147.8(2) . . . . ?
B7 B2 B3 Cl3 110.4(3) . . . . ?
Cl2 B2 B3 Cl3 4.9(3) . . . . ?
B6 B2 B3 B1 -37.3(2) . . . . ?
B11 B2 B3 B1 -102.7(2) . . . . ?
B7 B2 B3 B1 -140.1(2) . . . . ?
Cl2 B2 B3 B1 114.5(2) . . . . ?
B1 B2 B3 B7 140.1(2) . . . . ?
B6 B2 B3 B7 102.8(2) . . . . ?
B11 B2 B3 B7 37.4(2) . . . . ?
Cl2 B2 B3 B7 -105.4(2) . . . . ?
B1 B2 B3 B8 101.8(2) . . . . ?
B6 B2 B3 B8 64.5(3) . . . . ?
B11 B2 B3 B8 -0.8(3) . . . . ?
B7 B2 B3 B8 -38.3(2) . . . . ?
Cl2 B2 B3 B8 -143.7(2) . . . . ?
B2 B1 B3 B4 -135.5(2) . . . . ?
Cl1 B1 B3 B4 111.1(3) . . . . ?
B5 B1 B3 B4 -35.9(2) . . . . ?
B6 B1 B3 B4 -99.4(2) . . . . ?
B4 B1 B3 B2 135.5(2) . . . . ?
Cl1 B1 B3 B2 -113.4(3) . . . . ?
B5 B1 B3 B2 99.6(2) . . . . ?
B6 B1 B3 B2 36.1(2) . . . . ?
B2 B1 B3 Cl3 111.6(3) . . . . ?
B4 B1 B3 Cl3 -112.8(2) . . . . ?
Cl1 B1 B3 Cl3 -1.7(4) . . . . ?
B5 B1 B3 Cl3 -148.8(2) . . . . ?
B6 B1 B3 Cl3 147.8(2) . . . . ?
B2 B1 B3 B7 -35.9(2) . . . . ?
B4 B1 B3 B7 99.6(2) . . . . ?
Cl1 B1 B3 B7 -149.3(2) . . . . ?
B5 B1 B3 B7 63.7(3) . . . . ?
B6 B1 B3 B7 0.2(3) . . . . ?
B2 B1 B3 B8 -99.6(2) . . . . ?
B4 B1 B3 B8 36.0(2) . . . . ?
Cl1 B1 B3 B8 147.1(2) . . . . ?
B5 B1 B3 B8 0.0(3) . . . . ?
B6 B1 B3 B8 -63.4(3) . . . . ?
B2 B3 B4 B9 62.9(3) . . . . ?
Cl3 B3 B4 B9 -148.7(2) . . . . ?
B1 B3 B4 B9 101.8(2) . . . . ?
B7 B3 B4 B9 -0.2(3) . . . . ?
B8 B3 B4 B9 -38.1(2) . . . . ?
B2 B3 B4 B8 101.0(2) . . . . ?
Cl3 B3 B4 B8 -110.6(3) . . . . ?
B1 B3 B4 B8 139.9(2) . . . . ?
B7 B3 B4 B8 37.9(2) . . . . ?
B2 B3 B4 B5 -2.4(3) . . . . ?
Cl3 B3 B4 B5 146.1(2) . . . . ?
B1 B3 B4 B5 36.5(2) . . . . ?
B7 B3 B4 B5 -65.4(3) . . . . ?
B8 B3 B4 B5 -103.4(2) . . . . ?
B2 B3 B4 B1 -38.9(2) . . . . ?
Cl3 B3 B4 B1 109.6(3) . . . . ?
B7 B3 B4 B1 -101.9(2) . . . . ?
B8 B3 B4 B1 -139.9(2) . . . . ?
B2 B3 B4 Cl4 -140.5(2) . . . . ?
Cl3 B3 B4 Cl4 8.0(3) . . . . ?
B1 B3 B4 Cl4 -101.6(2) . . . . ?
B7 B3 B4 Cl4 156.5(2) . . . . ?
B8 B3 B4 Cl4 118.5(2) . . . . ?
B2 B1 B4 B9 -63.4(3) . . . . ?
Cl1 B1 B4 B9 146.9(2) . . . . ?
B3 B1 B4 B9 -102.5(2) . . . . ?
B5 B1 B4 B9 37.3(2) . . . . ?
B6 B1 B4 B9 -1.0(3) . . . . ?
B2 B1 B4 B3 39.1(2) . . . . ?
Cl1 B1 B4 B3 -110.6(3) . . . . ?
B5 B1 B4 B3 139.8(2) . . . . ?
B6 B1 B4 B3 101.5(2) . . . . ?
B2 B1 B4 B8 2.2(3) . . . . ?
Cl1 B1 B4 B8 -147.5(2) . . . . ?
B3 B1 B4 B8 -36.9(2) . . . . ?
B5 B1 B4 B8 102.9(2) . . . . ?
B6 B1 B4 B8 64.6(3) . . . . ?
B2 B1 B4 B5 -100.7(2) . . . . ?
Cl1 B1 B4 B5 109.6(3) . . . . ?
B3 B1 B4 B5 -139.8(2) . . . . ?
B6 B1 B4 B5 -38.3(2) . . . . ?
B2 B1 B4 Cl4 150.6(2) . . . . ?
Cl1 B1 B4 Cl4 0.9(3) . . . . ?
B3 B1 B4 Cl4 111.5(2) . . . . ?
B5 B1 B4 Cl4 -108.7(2) . . . . ?
B6 B1 B4 Cl4 -147.0(2) . . . . ?
B9 B4 Cl4 Si2 44.6(3) . . . . ?
B3 B4 Cl4 Si2 -108.0(2) . . . . ?
B8 B4 Cl4 Si2 -33.9(3) . . . . ?
B5 B4 Cl4 Si2 116.9(2) . . . . ?
B1 B4 Cl4 Si2 -175.88(14) . . . . ?
B9 B4 B5 Cl5 111.8(3) . . . . ?
B3 B4 B5 Cl5 -145.4(2) . . . . ?
B8 B4 B5 Cl5 149.2(2) . . . . ?
B1 B4 B5 Cl5 -108.9(3) . . . . ?
Cl4 B4 B5 Cl5 -6.2(3) . . . . ?
B9 B4 B5 B1 -139.2(2) . . . . ?
B3 B4 B5 B1 -36.5(2) . . . . ?
B8 B4 B5 B1 -101.9(2) . . . . ?
Cl4 B4 B5 B1 102.7(2) . . . . ?
B9 B4 B5 B6 -100.8(3) . . . . ?
B3 B4 B5 B6 2.0(3) . . . . ?
B8 B4 B5 B6 -63.4(3) . . . . ?
B1 B4 B5 B6 38.5(2) . . . . ?
Cl4 B4 B5 B6 141.2(2) . . . . ?
B3 B4 B5 B9 102.7(2) . . . . ?
B8 B4 B5 B9 37.3(2) . . . . ?
B1 B4 B5 B9 139.2(2) . . . . ?
Cl4 B4 B5 B9 -118.1(2) . . . . ?
B9 B4 B5 B10 -37.9(2) . . . . ?
B3 B4 B5 B10 64.9(3) . . . . ?
B8 B4 B5 B10 -0.6(3) . . . . ?
B1 B4 B5 B10 101.4(2) . . . . ?
Cl4 B4 B5 B10 -155.9(2) . . . . ?
B2 B1 B5 Cl5 -149.5(2) . . . . ?
B4 B1 B5 Cl5 111.6(3) . . . . ?
Cl1 B1 B5 Cl5 0.0(4) . . . . ?
B3 B1 B5 Cl5 147.4(2) . . . . ?
B6 B1 B5 Cl5 -111.6(3) . . . . ?
B2 B1 B5 B4 99.0(2) . . . . ?
Cl1 B1 B5 B4 -111.6(3) . . . . ?
B3 B1 B5 B4 35.8(2) . . . . ?
B6 B1 B5 B4 136.8(2) . . . . ?
B2 B1 B5 B6 -37.8(2) . . . . ?
B4 B1 B5 B6 -136.8(2) . . . . ?
Cl1 B1 B5 B6 111.6(3) . . . . ?
B3 B1 B5 B6 -101.0(2) . . . . ?
B2 B1 B5 B9 62.9(3) . . . . ?
B4 B1 B5 B9 -36.0(2) . . . . ?
Cl1 B1 B5 B9 -147.6(2) . . . . ?
B3 B1 B5 B9 -0.3(3) . . . . ?
B6 B1 B5 B9 100.7(3) . . . . ?
B2 B1 B5 B10 0.2(3) . . . . ?
B4 B1 B5 B10 -98.7(2) . . . . ?
Cl1 B1 B5 B10 149.7(2) . . . . ?
B3 B1 B5 B10 -63.0(3) . . . . ?
B6 B1 B5 B10 38.0(2) . . . . ?
B1 B2 B6 Cl6 110.0(3) . . . . ?
B11 B2 B6 Cl6 -111.0(3) . . . . ?
B3 B2 B6 Cl6 147.2(2) . . . . ?
B7 B2 B6 Cl6 -147.6(2) . . . . ?
Cl2 B2 B6 Cl6 0.4(4) . . . . ?
B1 B2 B6 B5 -37.9(2) . . . . ?
B11 B2 B6 B5 101.1(2) . . . . ?
B3 B2 B6 B5 -0.7(3) . . . . ?
B7 B2 B6 B5 64.5(3) . . . . ?
Cl2 B2 B6 B5 -147.5(2) . . . . ?
B1 B2 B6 B10 -101.0(2) . . . . ?
B11 B2 B6 B10 37.9(2) . . . . ?
B3 B2 B6 B10 -63.9(3) . . . . ?
B7 B2 B6 B10 1.3(3) . . . . ?
Cl2 B2 B6 B10 149.3(2) . . . . ?
B1 B2 B6 B11 -139.0(2) . . . . ?
B3 B2 B6 B11 -101.8(2) . . . . ?
B7 B2 B6 B11 -36.6(2) . . . . ?
Cl2 B2 B6 B11 111.4(3) . . . . ?
B11 B2 B6 B1 139.0(2) . . . . ?
B3 B2 B6 B1 37.1(2) . . . . ?
B7 B2 B6 B1 102.3(2) . . . . ?
Cl2 B2 B6 B1 -109.7(3) . . . . ?
Cl5 B5 B6 B2 146.7(2) . . . . ?
B4 B5 B6 B2 -0.8(3) . . . . ?
B1 B5 B6 B2 37.6(2) . . . . ?
B9 B5 B6 B2 -63.1(3) . . . . ?
B10 B5 B6 B2 -99.7(2) . . . . ?
Cl5 B5 B6 Cl6 -2.4(4) . . . . ?
B4 B5 B6 Cl6 -149.8(2) . . . . ?
B1 B5 B6 Cl6 -111.5(3) . . . . ?
B9 B5 B6 Cl6 147.8(2) . . . . ?
B10 B5 B6 Cl6 111.2(2) . . . . ?
Cl5 B5 B6 B10 -113.6(3) . . . . ?
B4 B5 B6 B10 98.9(2) . . . . ?
B1 B5 B6 B10 137.3(2) . . . . ?
B9 B5 B6 B10 36.6(2) . . . . ?
Cl5 B5 B6 B11 -150.6(2) . . . . ?
B4 B5 B6 B11 61.9(3) . . . . ?
B1 B5 B6 B11 100.3(2) . . . . ?
B9 B5 B6 B11 -0.4(3) . . . . ?
B10 B5 B6 B11 -37.0(2) . . . . ?
Cl5 B5 B6 B1 109.1(3) . . . . ?
B4 B5 B6 B1 -38.3(2) . . . . ?
B9 B5 B6 B1 -100.7(2) . . . . ?
B10 B5 B6 B1 -137.3(2) . . . . ?
B4 B1 B6 B2 -99.0(2) . . . . ?
Cl1 B1 B6 B2 113.1(3) . . . . ?
B3 B1 B6 B2 -36.2(2) . . . . ?
B5 B1 B6 B2 -137.2(2) . . . . ?
B2 B1 B6 Cl6 -113.2(3) . . . . ?
B4 B1 B6 Cl6 147.8(2) . . . . ?
Cl1 B1 B6 Cl6 -0.1(4) . . . . ?
B3 B1 B6 Cl6 -149.4(2) . . . . ?
B5 B1 B6 Cl6 109.6(3) . . . . ?
B2 B1 B6 B5 137.2(2) . . . . ?
B4 B1 B6 B5 38.2(2) . . . . ?
Cl1 B1 B6 B5 -109.7(3) . . . . ?
B3 B1 B6 B5 100.9(2) . . . . ?
B2 B1 B6 B10 99.0(3) . . . . ?
B4 B1 B6 B10 0.1(3) . . . . ?
Cl1 B1 B6 B10 -147.9(2) . . . . ?
B3 B1 B6 B10 62.8(3) . . . . ?
B5 B1 B6 B10 -38.2(2) . . . . ?
B2 B1 B6 B11 36.4(2) . . . . ?
B4 B1 B6 B11 -62.5(3) . . . . ?
Cl1 B1 B6 B11 149.5(2) . . . . ?
B3 B1 B6 B11 0.2(3) . . . . ?
B5 B1 B6 B11 -100.8(2) . . . . ?
B1 B2 B7 Cl7 -146.6(2) . . . . ?
B6 B2 B7 Cl7 147.6(2) . . . . ?
B11 B2 B7 Cl7 110.9(3) . . . . ?
B3 B2 B7 Cl7 -110.1(3) . . . . ?
Cl2 B2 B7 Cl7 -5.1(3) . . . . ?
B1 B2 B7 B12 64.2(3) . . . . ?
B6 B2 B7 B12 -1.6(3) . . . . ?
B11 B2 B7 B12 -38.3(2) . . . . ?
B3 B2 B7 B12 100.7(2) . . . . ?
Cl2 B2 B7 B12 -154.30(19) . . . . ?
B1 B2 B7 B3 -36.6(2) . . . . ?
B6 B2 B7 B3 -102.3(2) . . . . ?
B11 B2 B7 B3 -139.0(2) . . . . ?
Cl2 B2 B7 B3 105.0(2) . . . . ?
B1 B2 B7 B8 1.6(3) . . . . ?
B6 B2 B7 B8 -64.1(3) . . . . ?
B11 B2 B7 B8 -100.8(2) . . . . ?
B3 B2 B7 B8 38.2(2) . . . . ?
Cl2 B2 B7 B8 143.2(2) . . . . ?
B1 B2 B7 B11 102.4(2) . . . . ?
B6 B2 B7 B11 36.7(2) . . . . ?
B3 B2 B7 B11 139.0(2) . . . . ?
Cl2 B2 B7 B11 -116.0(2) . . . . ?
B4 B3 B7 Cl7 -149.8(2) . . . . ?
B2 B3 B7 Cl7 111.1(3) . . . . ?
Cl3 B3 B7 Cl7 -0.7(3) . . . . ?
B1 B3 B7 Cl7 146.7(2) . . . . ?
B8 B3 B7 Cl7 -112.0(3) . . . . ?
B4 B3 B7 B2 99.1(2) . . . . ?
Cl3 B3 B7 B2 -111.8(3) . . . . ?
B1 B3 B7 B2 35.6(2) . . . . ?
B8 B3 B7 B2 136.9(2) . . . . ?
B4 B3 B7 B12 0.2(3) . . . . ?
B2 B3 B7 B12 -98.9(2) . . . . ?
Cl3 B3 B7 B12 149.3(2) . . . . ?
B1 B3 B7 B12 -63.3(3) . . . . ?
B8 B3 B7 B12 38.0(2) . . . . ?
B4 B3 B7 B8 -37.8(2) . . . . ?
B2 B3 B7 B8 -136.9(2) . . . . ?
Cl3 B3 B7 B8 111.3(3) . . . . ?
B1 B3 B7 B8 -101.3(2) . . . . ?
B4 B3 B7 B11 63.0(3) . . . . ?
B2 B3 B7 B11 -36.1(2) . . . . ?
Cl3 B3 B7 B11 -147.9(2) . . . . ?
B1 B3 B7 B11 -0.5(3) . . . . ?
B8 B3 B7 B11 100.8(2) . . . . ?
B9 B4 B8 Cl8 -110.8(3) . . . . ?
B3 B4 B8 Cl8 110.5(3) . . . . ?
B5 B4 B8 Cl8 -148.0(2) . . . . ?
B1 B4 B8 Cl8 147.2(2) . . . . ?
Cl4 B4 B8 Cl8 4.3(4) . . . . ?
B9 B4 B8 B12 37.9(2) . . . . ?
B3 B4 B8 B12 -100.8(2) . . . . ?
B5 B4 B8 B12 0.7(3) . . . . ?
B1 B4 B8 B12 -64.1(3) . . . . ?
Cl4 B4 B8 B12 153.0(2) . . . . ?
B9 B4 B8 B7 100.8(2) . . . . ?
B3 B4 B8 B7 -37.9(2) . . . . ?
B5 B4 B8 B7 63.6(3) . . . . ?
B1 B4 B8 B7 -1.2(3) . . . . ?
Cl4 B4 B8 B7 -144.1(2) . . . . ?
B9 B4 B8 B3 138.7(2) . . . . ?
B5 B4 B8 B3 101.5(2) . . . . ?
B1 B4 B8 B3 36.6(2) . . . . ?
Cl4 B4 B8 B3 -106.3(3) . . . . ?
B3 B4 B8 B9 -138.7(2) . . . . ?
B5 B4 B8 B9 -37.2(2) . . . . ?
B1 B4 B8 B9 -102.0(2) . . . . ?
Cl4 B4 B8 B9 115.1(3) . . . . ?
Cl7 B7 B8 B4 147.8(2) . . . . ?
B2 B7 B8 B4 -0.2(3) . . . . ?
B12 B7 B8 B4 -99.5(2) . . . . ?
B3 B7 B8 B4 37.6(2) . . . . ?
B11 B7 B8 B4 -62.4(3) . . . . ?
Cl7 B7 B8 Cl8 -1.3(3) . . . . ?
B2 B7 B8 Cl8 -149.3(2) . . . . ?
B12 B7 B8 Cl8 111.5(3) . . . . ?
B3 B7 B8 Cl8 -111.5(2) . . . . ?
B11 B7 B8 Cl8 148.5(2) . . . . ?
Cl7 B7 B8 B12 -112.7(3) . . . . ?
B2 B7 B8 B12 99.2(2) . . . . ?
B3 B7 B8 B12 137.0(2) . . . . ?
B11 B7 B8 B12 37.0(2) . . . . ?
Cl7 B7 B8 B3 110.2(3) . . . . ?
B2 B7 B8 B3 -37.8(2) . . . . ?
B12 B7 B8 B3 -137.0(2) . . . . ?
B11 B7 B8 B3 -100.0(2) . . . . ?
Cl7 B7 B8 B9 -150.0(2) . . . . ?
B2 B7 B8 B9 62.0(3) . . . . ?
B12 B7 B8 B9 -37.3(2) . . . . ?
B3 B7 B8 B9 99.8(2) . . . . ?
B11 B7 B8 B9 -0.2(3) . . . . ?
B2 B3 B8 B4 -98.9(2) . . . . ?
Cl3 B3 B8 B4 112.3(3) . . . . ?
B1 B3 B8 B4 -36.2(2) . . . . ?
B7 B3 B8 B4 -137.3(2) . . . . ?
B4 B3 B8 Cl8 -112.4(3) . . . . ?
B2 B3 B8 Cl8 148.7(2) . . . . ?
Cl3 B3 B8 Cl8 -0.1(4) . . . . ?
B1 B3 B8 Cl8 -148.5(2) . . . . ?
B7 B3 B8 Cl8 110.4(3) . . . . ?
B4 B3 B8 B12 99.1(2) . . . . ?
B2 B3 B8 B12 0.2(3) . . . . ?
Cl3 B3 B8 B12 -148.6(2) . . . . ?
B1 B3 B8 B12 62.9(3) . . . . ?
B7 B3 B8 B12 -38.2(2) . . . . ?
B4 B3 B8 B7 137.3(2) . . . . ?
B2 B3 B8 B7 38.4(2) . . . . ?
Cl3 B3 B8 B7 -110.4(3) . . . . ?
B1 B3 B8 B7 101.1(2) . . . . ?
B4 B3 B8 B9 36.3(2) . . . . ?
B2 B3 B8 B9 -62.6(3) . . . . ?
Cl3 B3 B8 B9 148.6(2) . . . . ?
B1 B3 B8 B9 0.2(3) . . . . ?
B7 B3 B8 B9 -100.9(2) . . . . ?
B3 B4 B9 Cl9 148.0(2) . . . . ?
B8 B4 B9 Cl9 110.0(3) . . . . ?
B5 B4 B9 Cl9 -110.2(3) . . . . ?
B1 B4 B9 Cl9 -147.3(2) . . . . ?
Cl4 B4 B9 Cl9 -6.7(4) . . . . ?
B3 B4 B9 B10 -63.1(3) . . . . ?
B8 B4 B9 B10 -101.1(3) . . . . ?
B5 B4 B9 B10 38.6(2) . . . . ?
B1 B4 B9 B10 1.6(3) . . . . ?
Cl4 B4 B9 B10 142.2(2) . . . . ?
B3 B4 B9 B12 0.0(3) . . . . ?
B8 B4 B9 B12 -38.0(2) . . . . ?
B5 B4 B9 B12 101.8(2) . . . . ?
B1 B4 B9 B12 64.7(3) . . . . ?
Cl4 B4 B9 B12 -154.7(2) . . . . ?
B3 B4 B9 B5 -101.7(3) . . . . ?
B8 B4 B9 B5 -139.7(2) . . . . ?
B1 B4 B9 B5 -37.0(2) . . . . ?
Cl4 B4 B9 B5 103.6(3) . . . . ?
B3 B4 B9 B8 38.0(2) . . . . ?
B5 B4 B9 B8 139.7(2) . . . . ?
B1 B4 B9 B8 102.7(2) . . . . ?
Cl4 B4 B9 B8 -116.7(3) . . . . ?
Cl5 B5 B9 B4 -110.2(3) . . . . ?
B1 B5 B9 B4 36.4(2) . . . . ?
B6 B5 B9 B4 99.9(2) . . . . ?
B10 B5 B9 B4 136.8(2) . . . . ?
Cl5 B5 B9 Cl9 2.9(4) . . . . ?
B4 B5 B9 Cl9 113.1(3) . . . . ?
B1 B5 B9 Cl9 149.5(2) . . . . ?
B6 B5 B9 Cl9 -147.0(2) . . . . ?
B10 B5 B9 Cl9 -110.1(3) . . . . ?
Cl5 B5 B9 B10 113.0(3) . . . . ?
B4 B5 B9 B10 -136.8(2) . . . . ?
B1 B5 B9 B10 -100.4(3) . . . . ?
B6 B5 B9 B10 -36.8(2) . . . . ?
Cl5 B5 B9 B12 150.6(2) . . . . ?
B4 B5 B9 B12 -99.2(2) . . . . ?
B1 B5 B9 B12 -62.8(3) . . . . ?
B6 B5 B9 B12 0.8(3) . . . . ?
B10 B5 B9 B12 37.6(2) . . . . ?
Cl5 B5 B9 B8 -146.2(2) . . . . ?
B4 B5 B9 B8 -36.0(2) . . . . ?
B1 B5 B9 B8 0.4(3) . . . . ?
B6 B5 B9 B8 63.9(3) . . . . ?
B10 B5 B9 B8 100.8(2) . . . . ?
Cl8 B8 B9 B4 112.1(3) . . . . ?
B12 B8 B9 B4 -137.0(2) . . . . ?
B7 B8 B9 B4 -99.6(2) . . . . ?
B3 B8 B9 B4 -36.4(2) . . . . ?
B4 B8 B9 Cl9 -113.0(3) . . . . ?
Cl8 B8 B9 Cl9 -0.9(4) . . . . ?
B12 B8 B9 Cl9 110.0(3) . . . . ?
B7 B8 B9 Cl9 147.4(2) . . . . ?
B3 B8 B9 Cl9 -149.5(2) . . . . ?
B4 B8 B9 B10 100.0(2) . . . . ?
Cl8 B8 B9 B10 -147.9(2) . . . . ?
B12 B8 B9 B10 -37.0(2) . . . . ?
B7 B8 B9 B10 0.4(3) . . . . ?
B3 B8 B9 B10 63.5(3) . . . . ?
B4 B8 B9 B12 137.0(2) . . . . ?
Cl8 B8 B9 B12 -110.9(3) . . . . ?
B7 B8 B9 B12 37.4(2) . . . . ?
B3 B8 B9 B12 100.5(2) . . . . ?
B4 B8 B9 B5 36.1(2) . . . . ?
Cl8 B8 B9 B5 148.2(2) . . . . ?
B12 B8 B9 B5 -100.8(3) . . . . ?
B7 B8 B9 B5 -63.4(3) . . . . ?
B3 B8 B9 B5 -0.3(3) . . . . ?
B4 B9 B10 Cl10 -148.7(2) . . . . ?
Cl9 B9 B10 Cl10 1.2(4) . . . . ?
B12 B9 B10 Cl10 111.7(3) . . . . ?
B5 B9 B10 Cl10 -110.3(3) . . . . ?
B8 B9 B10 Cl10 148.4(2) . . . . ?
B4 B9 B10 B11 62.4(3) . . . . ?
Cl9 B9 B10 B11 -147.8(2) . . . . ?
B12 B9 B10 B11 -37.2(2) . . . . ?
B5 B9 B10 B11 100.8(2) . . . . ?
B8 B9 B10 B11 -0.5(3) . . . . ?
B4 B9 B10 B12 99.7(2) . . . . ?
Cl9 B9 B10 B12 -110.5(3) . . . . ?
B5 B9 B10 B12 138.1(2) . . . . ?
B8 B9 B10 B12 36.8(2) . . . . ?
B4 B9 B10 B6 -1.5(3) . . . . ?
Cl9 B9 B10 B6 148.3(2) . . . . ?
B12 B9 B10 B6 -101.2(3) . . . . ?
B5 B9 B10 B6 36.9(2) . . . . ?
B8 B9 B10 B6 -64.4(3) . . . . ?
B4 B9 B10 B5 -38.4(2) . . . . ?
Cl9 B9 B10 B5 111.4(3) . . . . ?
B12 B9 B10 B5 -138.1(2) . . . . ?
B8 B9 B10 B5 -101.3(2) . . . . ?
B2 B6 B10 Cl10 -150.5(2) . . . . ?
Cl6 B6 B10 Cl10 -0.7(4) . . . . ?
B5 B6 B10 Cl10 109.3(3) . . . . ?
B11 B6 B10 Cl10 -112.5(3) . . . . ?
B1 B6 B10 Cl10 147.3(2) . . . . ?
B2 B6 B10 B11 -38.0(2) . . . . ?
Cl6 B6 B10 B11 111.8(3) . . . . ?
B5 B6 B10 B11 -138.2(2) . . . . ?
B1 B6 B10 B11 -100.2(2) . . . . ?
B2 B6 B10 B9 63.1(3) . . . . ?
Cl6 B6 B10 B9 -147.1(2) . . . . ?
B5 B6 B10 B9 -37.1(2) . . . . ?
B11 B6 B10 B9 101.1(3) . . . . ?
B1 B6 B10 B9 0.9(3) . . . . ?
B2 B6 B10 B12 -0.5(3) . . . . ?
Cl6 B6 B10 B12 149.3(2) . . . . ?
B5 B6 B10 B12 -100.7(2) . . . . ?
B11 B6 B10 B12 37.5(2) . . . . ?
B1 B6 B10 B12 -62.7(3) . . . . ?
B2 B6 B10 B5 100.2(2) . . . . ?
Cl6 B6 B10 B5 -110.0(3) . . . . ?
B11 B6 B10 B5 138.2(2) . . . . ?
B1 B6 B10 B5 38.0(2) . . . . ?
Cl5 B5 B10 Cl10 -1.6(4) . . . . ?
B4 B5 B10 Cl10 147.3(2) . . . . ?
B1 B5 B10 Cl10 -149.9(2) . . . . ?
B6 B5 B10 Cl10 -111.7(3) . . . . ?
B9 B5 B10 Cl10 109.6(3) . . . . ?
Cl5 B5 B10 B11 147.6(2) . . . . ?
B4 B5 B10 B11 -63.5(3) . . . . ?
B1 B5 B10 B11 -0.6(3) . . . . ?
B6 B5 B10 B11 37.5(2) . . . . ?
B9 B5 B10 B11 -101.2(2) . . . . ?
Cl5 B5 B10 B9 -111.2(3) . . . . ?
B4 B5 B10 B9 37.7(2) . . . . ?
B1 B5 B10 B9 100.6(2) . . . . ?
B6 B5 B10 B9 138.7(2) . . . . ?
Cl5 B5 B10 B12 -148.7(2) . . . . ?
B4 B5 B10 B12 0.2(3) . . . . ?
B1 B5 B10 B12 63.1(3) . . . . ?
B6 B5 B10 B12 101.2(3) . . . . ?
B9 B5 B10 B12 -37.5(2) . . . . ?
Cl5 B5 B10 B6 110.1(3) . . . . ?
B4 B5 B10 B6 -101.0(2) . . . . ?
B1 B5 B10 B6 -38.2(2) . . . . ?
B9 B5 B10 B6 -138.7(2) . . . . ?
B1 B2 B11 B10 -0.7(3) . . . . ?
B6 B2 B11 B10 -38.5(2) . . . . ?
B3 B2 B11 B10 64.4(3) . . . . ?
B7 B2 B11 B10 101.8(2) . . . . ?
Cl2 B2 B11 B10 -156.9(2) . . . . ?
B1 B2 B11 Cl11 149.2(2) . . . . ?
B6 B2 B11 Cl11 111.4(3) . . . . ?
B3 B2 B11 Cl11 -145.7(2) . . . . ?
B7 B2 B11 Cl11 -108.4(3) . . . . ?
Cl2 B2 B11 Cl11 -7.0(4) . . . . ?
B1 B2 B11 B12 -63.9(3) . . . . ?
B6 B2 B11 B12 -101.7(3) . . . . ?
B3 B2 B11 B12 1.2(3) . . . . ?
B7 B2 B11 B12 38.6(2) . . . . ?
Cl2 B2 B11 B12 139.9(2) . . . . ?
B1 B2 B11 B6 37.8(2) . . . . ?
B3 B2 B11 B6 102.8(2) . . . . ?
B7 B2 B11 B6 140.2(2) . . . . ?
Cl2 B2 B11 B6 -118.4(3) . . . . ?
B1 B2 B11 B7 -102.4(2) . . . . ?
B6 B2 B11 B7 -140.2(2) . . . . ?
B3 B2 B11 B7 -37.4(2) . . . . ?
Cl2 B2 B11 B7 101.3(3) . . . . ?
Cl10 B10 B11 B2 149.1(2) . . . . ?
B9 B10 B11 B2 -63.0(3) . . . . ?
B12 B10 B11 B2 -100.2(2) . . . . ?
B6 B10 B11 B2 38.1(2) . . . . ?
B5 B10 B11 B2 0.8(3) . . . . ?
Cl10 B10 B11 Cl11 -0.7(4) . . . . ?
B9 B10 B11 Cl11 147.2(2) . . . . ?
B12 B10 B11 Cl11 110.0(3) . . . . ?
B6 B10 B11 Cl11 -111.7(3) . . . . ?
B5 B10 B11 Cl11 -149.0(2) . . . . ?
Cl10 B10 B11 B12 -110.7(3) . . . . ?
B9 B10 B11 B12 37.2(2) . . . . ?
B6 B10 B11 B12 138.2(2) . . . . ?
B5 B10 B11 B12 101.0(2) . . . . ?
Cl10 B10 B11 B6 111.1(3) . . . . ?
B9 B10 B11 B6 -101.1(2) . . . . ?
B12 B10 B11 B6 -138.2(2) . . . . ?
B5 B10 B11 B6 -37.3(2) . . . . ?
Cl10 B10 B11 B7 -147.5(2) . . . . ?
B9 B10 B11 B7 0.3(3) . . . . ?
B12 B10 B11 B7 -36.9(2) . . . . ?
B6 B10 B11 B7 101.4(2) . . . . ?
B5 B10 B11 B7 64.1(3) . . . . ?
Cl6 B6 B11 B2 113.1(3) . . . . ?
B5 B6 B11 B2 -99.4(2) . . . . ?
B10 B6 B11 B2 -136.8(2) . . . . ?
B1 B6 B11 B2 -36.3(2) . . . . ?
B2 B6 B11 B10 136.8(2) . . . . ?
Cl6 B6 B11 B10 -110.1(3) . . . . ?
B5 B6 B11 B10 37.4(2) . . . . ?
B1 B6 B11 B10 100.5(2) . . . . ?
B2 B6 B11 Cl11 -111.3(3) . . . . ?
Cl6 B6 B11 Cl11 1.8(4) . . . . ?
B5 B6 B11 Cl11 149.3(2) . . . . ?
B10 B6 B11 Cl11 111.9(3) . . . . ?
B1 B6 B11 Cl11 -147.6(2) . . . . ?
B2 B6 B11 B12 99.3(2) . . . . ?
Cl6 B6 B11 B12 -147.6(2) . . . . ?
B5 B6 B11 B12 -0.1(3) . . . . ?
B10 B6 B11 B12 -37.5(2) . . . . ?
B1 B6 B11 B12 63.0(3) . . . . ?
B2 B6 B11 B7 35.8(2) . . . . ?
Cl6 B6 B11 B7 148.9(2) . . . . ?
B5 B6 B11 B7 -63.6(3) . . . . ?
B10 B6 B11 B7 -101.0(2) . . . . ?
B1 B6 B11 B7 -0.5(3) . . . . ?
Cl7 B7 B11 B2 -110.7(3) . . . . ?
B12 B7 B11 B2 136.4(2) . . . . ?
B3 B7 B11 B2 36.1(2) . . . . ?
B8 B7 B11 B2 99.4(2) . . . . ?
Cl7 B7 B11 B10 149.8(2) . . . . ?
B2 B7 B11 B10 -99.4(2) . . . . ?
B12 B7 B11 B10 37.0(2) . . . . ?
B3 B7 B11 B10 -63.3(3) . . . . ?
B8 B7 B11 B10 0.0(3) . . . . ?
Cl7 B7 B11 Cl11 1.9(3) . . . . ?
B2 B7 B11 Cl11 112.6(3) . . . . ?
B12 B7 B11 Cl11 -111.0(3) . . . . ?
B3 B7 B11 Cl11 148.7(2) . . . . ?
B8 B7 B11 Cl11 -148.0(2) . . . . ?
Cl7 B7 B11 B12 112.9(3) . . . . ?
B2 B7 B11 B12 -136.4(2) . . . . ?
B3 B7 B11 B12 -100.3(2) . . . . ?
B8 B7 B11 B12 -37.0(2) . . . . ?
Cl7 B7 B11 B6 -146.3(2) . . . . ?
B2 B7 B11 B6 -35.5(2) . . . . ?
B12 B7 B11 B6 100.9(3) . . . . ?
B3 B7 B11 B6 0.6(3) . . . . ?
B8 B7 B11 B6 63.9(3) . . . . ?
B4 B8 B12 Cl12 -149.3(2) . . . . ?
Cl8 B8 B12 Cl12 -0.1(4) . . . . ?
B7 B8 B12 Cl12 110.3(3) . . . . ?
B3 B8 B12 Cl12 148.5(2) . . . . ?
B9 B8 B12 Cl12 -111.7(3) . . . . ?
B4 B8 B12 B9 -37.6(2) . . . . ?
Cl8 B8 B12 B9 111.5(3) . . . . ?
B7 B8 B12 B9 -138.1(2) . . . . ?
B3 B8 B12 B9 -99.9(2) . . . . ?
B4 B8 B12 B10 -0.6(3) . . . . ?
Cl8 B8 B12 B10 148.6(2) . . . . ?
B7 B8 B12 B10 -101.0(3) . . . . ?
B3 B8 B12 B10 -62.8(3) . . . . ?
B9 B8 B12 B10 37.1(2) . . . . ?
B4 B8 B12 B11 62.8(3) . . . . ?
Cl8 B8 B12 B11 -148.0(2) . . . . ?
B7 B8 B12 B11 -37.6(2) . . . . ?
B3 B8 B12 B11 0.6(3) . . . . ?
B9 B8 B12 B11 100.4(3) . . . . ?
B4 B8 B12 B7 100.4(2) . . . . ?
Cl8 B8 B12 B7 -110.4(3) . . . . ?
B3 B8 B12 B7 38.2(2) . . . . ?
B9 B8 B12 B7 138.1(2) . . . . ?
B4 B9 B12 Cl12 149.1(2) . . . . ?
Cl9 B9 B12 Cl12 0.2(4) . . . . ?
B10 B9 B12 Cl12 -110.1(3) . . . . ?
B5 B9 B12 Cl12 -147.8(2) . . . . ?
B8 B9 B12 Cl12 111.2(3) . . . . ?
B4 B9 B12 B8 37.9(2) . . . . ?
Cl9 B9 B12 B8 -111.0(3) . . . . ?
B10 B9 B12 B8 138.7(2) . . . . ?
B5 B9 B12 B8 101.0(2) . . . . ?
B4 B9 B12 B10 -100.8(2) . . . . ?
Cl9 B9 B12 B10 110.3(3) . . . . ?
B5 B9 B12 B10 -37.7(2) . . . . ?
B8 B9 B12 B10 -138.7(2) . . . . ?
B4 B9 B12 B11 -63.9(3) . . . . ?
Cl9 B9 B12 B11 147.2(2) . . . . ?
B10 B9 B12 B11 36.9(2) . . . . ?
B5 B9 B12 B11 -0.8(3) . . . . ?
B8 B9 B12 B11 -101.8(2) . . . . ?
B4 B9 B12 B7 0.1(3) . . . . ?
Cl9 B9 B12 B7 -148.8(2) . . . . ?
B10 B9 B12 B7 100.9(2) . . . . ?
B5 B9 B12 B7 63.2(3) . . . . ?
B8 B9 B12 B7 -37.8(2) . . . . ?
Cl10 B10 B12 Cl12 2.6(4) . . . . ?
B11 B10 B12 Cl12 -109.9(3) . . . . ?
B9 B10 B12 Cl12 111.5(3) . . . . ?
B6 B10 B12 Cl12 -147.5(2) . . . . ?
B5 B10 B12 Cl12 149.2(2) . . . . ?
Cl10 B10 B12 B8 -146.4(2) . . . . ?
B11 B10 B12 B8 101.1(2) . . . . ?
B9 B10 B12 B8 -37.4(2) . . . . ?
B6 B10 B12 B8 63.5(3) . . . . ?
B5 B10 B12 B8 0.2(3) . . . . ?
Cl10 B10 B12 B9 -109.0(3) . . . . ?
B11 B10 B12 B9 138.5(2) . . . . ?
B6 B10 B12 B9 100.9(3) . . . . ?
B5 B10 B12 B9 37.6(2) . . . . ?
Cl10 B10 B12 B11 112.5(3) . . . . ?
B9 B10 B12 B11 -138.5(2) . . . . ?
B6 B10 B12 B11 -37.6(2) . . . . ?
B5 B10 B12 B11 -100.9(2) . . . . ?
Cl10 B10 B12 B7 149.6(2) . . . . ?
B11 B10 B12 B7 37.1(2) . . . . ?
B9 B10 B12 B7 -101.4(2) . . . . ?
B6 B10 B12 B7 -0.5(3) . . . . ?
B5 B10 B12 B7 -63.8(3) . . . . ?
B2 B11 B12 Cl12 -149.3(2) . . . . ?
B10 B11 B12 Cl12 110.5(3) . . . . ?
Cl11 B11 B12 Cl12 -1.9(4) . . . . ?
B6 B11 B12 Cl12 148.0(2) . . . . ?
B7 B11 B12 Cl12 -110.7(3) . . . . ?
B2 B11 B12 B8 -1.1(3) . . . . ?
B10 B11 B12 B8 -101.3(3) . . . . ?
Cl11 B11 B12 B8 146.4(2) . . . . ?
B6 B11 B12 B8 -63.7(3) . . . . ?
B7 B11 B12 B8 37.6(2) . . . . ?
B2 B11 B12 B9 63.2(3) . . . . ?
B10 B11 B12 B9 -37.0(2) . . . . ?
Cl11 B11 B12 B9 -149.3(2) . . . . ?
B6 B11 B12 B9 0.5(3) . . . . ?
B7 B11 B12 B9 101.8(2) . . . . ?
B2 B11 B12 B10 100.2(2) . . . . ?
Cl11 B11 B12 B10 -112.3(3) . . . . ?
B6 B11 B12 B10 37.5(2) . . . . ?
B7 B11 B12 B10 138.8(2) . . . . ?
B2 B11 B12 B7 -38.6(2) . . . . ?
B10 B11 B12 B7 -138.8(2) . . . . ?
Cl11 B11 B12 B7 108.8(3) . . . . ?
B6 B11 B12 B7 -101.3(2) . . . . ?
Cl7 B7 B12 Cl12 -0.3(4) . . . . ?
B2 B7 B12 Cl12 148.3(2) . . . . ?
B3 B7 B12 Cl12 -149.6(2) . . . . ?
B8 B7 B12 Cl12 -111.4(3) . . . . ?
B11 B7 B12 Cl12 110.3(3) . . . . ?
Cl7 B7 B12 B8 111.1(3) . . . . ?
B2 B7 B12 B8 -100.3(2) . . . . ?
B3 B7 B12 B8 -38.2(2) . . . . ?
B11 B7 B12 B8 -138.3(2) . . . . ?
Cl7 B7 B12 B9 149.1(2) . . . . ?
B2 B7 B12 B9 -62.3(3) . . . . ?
B3 B7 B12 B9 -0.2(3) . . . . ?
B8 B7 B12 B9 38.0(2) . . . . ?
B11 B7 B12 B9 -100.3(3) . . . . ?
Cl7 B7 B12 B10 -147.4(2) . . . . ?
B2 B7 B12 B10 1.2(3) . . . . ?
B3 B7 B12 B10 63.3(3) . . . . ?
B8 B7 B12 B10 101.5(3) . . . . ?
B11 B7 B12 B10 -36.8(2) . . . . ?
Cl7 B7 B12 B11 -110.6(3) . . . . ?
B2 B7 B12 B11 38.0(2) . . . . ?
B3 B7 B12 B11 100.1(2) . . . . ?
B8 B7 B12 B11 138.3(2) . . . . ?
B2 Cl2 Si1 C1 -56.48(17) . . . . ?
B2 Cl2 Si1 C7 67.06(17) . . . . ?
B2 Cl2 Si1 C4 -177.65(16) . . . . ?
C7 Si1 C1 C2 49.4(3) . . . . ?
C4 Si1 C1 C2 -94.3(3) . . . . ?
Cl2 Si1 C1 C2 162.0(2) . . . . ?
C7 Si1 C1 C3 175.4(2) . . . . ?
C4 Si1 C1 C3 31.7(3) . . . . ?
Cl2 Si1 C1 C3 -72.0(2) . . . . ?
C1 Si1 C4 C6 -67.7(3) . . . . ?
C7 Si1 C4 C6 146.8(2) . . . . ?
Cl2 Si1 C4 C6 40.0(2) . . . . ?
C1 Si1 C4 C5 57.7(2) . . . . ?
C7 Si1 C4 C5 -87.9(2) . . . . ?
Cl2 Si1 C4 C5 165.37(19) . . . . ?
C1 Si1 C7 C9 167.5(2) . . . . ?
C4 Si1 C7 C9 -46.8(3) . . . . ?
Cl2 Si1 C7 C9 55.2(2) . . . . ?
C1 Si1 C7 C8 -70.6(3) . . . . ?
C4 Si1 C7 C8 75.1(3) . . . . ?
Cl2 Si1 C7 C8 177.1(2) . . . . ?
B4 Cl4 Si2 C10 106.10(18) . . . . ?
B4 Cl4 Si2 C16 -139.50(18) . . . . ?
B4 Cl4 Si2 C13 -15.54(19) . . . . ?
C16 Si2 C10 C12 -34.3(3) . . . . ?
C13 Si2 C10 C12 -178.8(2) . . . . ?
Cl4 Si2 C10 C12 64.3(2) . . . . ?
C16 Si2 C10 C11 -162.5(2) . . . . ?
C13 Si2 C10 C11 53.0(3) . . . . ?
Cl4 Si2 C10 C11 -64.0(3) . . . . ?
C10 Si2 C13 C14 157.0(2) . . . . ?
C16 Si2 C13 C14 15.0(3) . . . . ?
Cl4 Si2 C13 C14 -92.3(2) . . . . ?
C10 Si2 C13 C15 33.7(3) . . . . ?
C16 Si2 C13 C15 -108.3(3) . . . . ?
Cl4 Si2 C13 C15 144.3(2) . . . . ?
C10 Si2 C16 C17 163.9(2) . . . . ?
C13 Si2 C16 C17 -53.1(3) . . . . ?
Cl4 Si2 C16 C17 62.5(2) . . . . ?
C10 Si2 C16 C18 -69.4(3) . . . . ?
C13 Si2 C16 C18 73.6(3) . . . . ?
Cl4 Si2 C16 C18 -170.7(2) . . . . ?
