#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/58/4315847.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4315847
loop_
_publ_author_name
'Karunesh Keshav'
'Nem Singh'
'Anil J. Elias'
_publ_contact_author_address
;DEPARTMENT OF CHEMISTRY
INDIAN INSTITUTE OF TECHNOLOGY DELHI
HAUZ KHAS, NEW DELHI 110016
INDIA
;
_publ_contact_author_email       elias@chemistry.iitd.ac.in
_publ_contact_author_fax         +91-11-2658????
_publ_contact_author_name        'Dr.Anil J. Elias'
_publ_contact_author_phone       +91-11-2659????
_publ_section_title
;
 Synthesis and Reactions of Ethynylferrocene-Derived Fluoro- and
 Chlorocyclotriphosphazenes
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5753
_journal_page_last               5765
_journal_paper_doi               10.1021/ic100703h
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C29 H23 Cl10 Co Fe2 N6 P6, C2, C'
_chemical_formula_sum            'C32 H23 Cl10 Co Fe2 N6 P6'
_chemical_formula_weight         1202.52
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                105.160(3)
_cell_angle_beta                 100.969(3)
_cell_angle_gamma                91.629(3)
_cell_formula_units_Z            2
_cell_length_a                   12.276(2)
_cell_length_b                   12.859(2)
_cell_length_c                   16.920(3)
_cell_measurement_temperature    293(2)
_cell_volume                     2522.3(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0338
_diffrn_reflns_av_sigmaI/netI    0.0413
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            24859
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
_diffrn_reflns_theta_min         1.65
_exptl_absorpt_coefficient_mu    1.644
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.583
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1192.0
_exptl_crystal_size_max          0.214
_exptl_crystal_size_mid          0.118
_exptl_crystal_size_min          0.083
_refine_diff_density_max         0.967
_refine_diff_density_min         -0.450
_refine_diff_density_rms         0.121
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.125
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     514
_refine_ls_number_reflns         9306
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.125
_refine_ls_R_factor_all          0.0756
_refine_ls_R_factor_gt           0.0630
_refine_ls_shift/su_max          0.162
_refine_ls_shift/su_mean         0.010
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0974P)²+1.3451P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1682
_refine_ls_wR_factor_ref         0.1764
_reflns_number_gt                7708
_reflns_number_total             9306
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic100703h_si_002_07.cif
_cod_data_source_block           7
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        2522.4(7)
_cod_original_sg_symbol_Hall     -P1
_cod_database_code               4315847
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.07518(4) 0.08430(4) 0.24821(4) 0.03724(17) Uani 1 1 d . . .
Fe1 Fe 0.43911(6) 0.12627(6) 0.15307(4) 0.0518(2) Uani 1 1 d . . .
Fe2 Fe 0.22375(6) 0.40666(5) 0.49266(4) 0.0464(2) Uani 1 1 d . . .
Cl1 Cl 0.43548(11) 0.09461(13) 0.43532(10) 0.0673(4) Uani 1 1 d . . .
Cl2 Cl 0.03378(14) -0.13514(17) 0.45521(14) 0.0973(6) Uani 1 1 d . . .
Cl3 Cl 0.26765(16) -0.12628(18) 0.55763(11) 0.0942(6) Uani 1 1 d . . .
Cl4 Cl 0.2249(2) -0.30420(15) 0.20283(12) 0.1005(6) Uani 1 1 d . . .
Cl5 Cl 0.4299(2) -0.27742(18) 0.34558(14) 0.1126(7) Uani 1 1 d . . .
Cl6 Cl 0.24546(13) 0.41151(12) 0.20850(10) 0.0727(4) Uani 1 1 d . . .
Cl7 Cl 0.01754(15) 0.35735(13) -0.03328(9) 0.0753(4) Uani 1 1 d . . .
Cl8 Cl -0.15267(15) 0.19276(15) -0.00971(10) 0.0861(5) Uani 1 1 d . . .
Cl9 Cl -0.03710(15) 0.59948(11) 0.24691(10) 0.0744(4) Uani 1 1 d . . .
Cl10 Cl -0.20357(14) 0.41568(16) 0.24758(13) 0.0917(5) Uani 1 1 d . . .
P1 P 0.28866(10) 0.01398(9) 0.36826(8) 0.0415(3) Uani 1 1 d . . .
P2 P 0.19029(12) -0.11730(11) 0.44497(9) 0.0545(3) Uani 1 1 d . . .
P3 P 0.29030(14) -0.20809(11) 0.31586(9) 0.0595(4) Uani 1 1 d . . .
P4 P 0.11005(10) 0.31292(9) 0.20292(7) 0.0414(3) Uani 1 1 d . . .
P5 P -0.03493(12) 0.30949(11) 0.05707(8) 0.0522(3) Uani 1 1 d . . .
P6 P -0.06564(11) 0.43921(11) 0.20663(8) 0.0504(3) Uani 1 1 d . . .
N1 N 0.2159(4) -0.0027(3) 0.4332(3) 0.0523(10) Uani 1 1 d . . .
N2 N 0.2109(5) -0.2200(4) 0.3763(3) 0.0816(16) Uani 1 1 d . . .
N3 N 0.3180(4) -0.0931(3) 0.3062(3) 0.0572(11) Uani 1 1 d . . .
N4 N 0.0605(4) 0.2579(3) 0.1059(2) 0.0510(10) Uani 1 1 d . . .
N5 N -0.0916(4) 0.4058(4) 0.1076(3) 0.0732(15) Uani 1 1 d . . .
N6 N 0.0303(4) 0.3853(3) 0.2534(2) 0.0534(10) Uani 1 1 d . . .
C1 C -0.0842(6) 0.0738(8) 0.1816(7) 0.097(3) Uani 1 1 d . . .
H1 H -0.1136 0.1276 0.1534 0.116 Uiso 1 1 calc R . .
C2 C -0.0875(6) 0.0779(8) 0.2576(7) 0.099(3) Uani 1 1 d . . .
H2 H -0.1215 0.1333 0.2949 0.119 Uiso 1 1 calc R . .
C3 C -0.0393(8) -0.0058(12) 0.2777(6) 0.131(5) Uani 1 1 d . . .
H3 H -0.0346 -0.0254 0.3304 0.157 Uiso 1 1 calc R . .
C4 C -0.0026(6) -0.0647(5) 0.2053(13) 0.152(6) Uani 1 1 d . . .
H4 H 0.0311 -0.1340 0.1967 0.182 Uiso 1 1 calc R . .
C5 C -0.0366(7) -0.0086(12) 0.1472(5) 0.123(4) Uani 1 1 d . . .
H5 H -0.0266 -0.0284 0.0892 0.147 Uiso 1 1 calc R . .
C6 C 0.2300(3) 0.1051(3) 0.3129(3) 0.0363(9) Uani 1 1 d . . .
C7 C 0.2268(3) 0.1223(3) 0.2301(3) 0.0354(9) Uani 1 1 d . . .
C8 C 0.1641(3) 0.2178(3) 0.2546(3) 0.0352(9) Uani 1 1 d . . .
C9 C 0.1700(3) 0.2018(3) 0.3384(3) 0.0346(9) Uani 1 1 d . . .
C10 C 0.2811(4) 0.0790(4) 0.1601(3) 0.0428(10) Uani 1 1 d . . .
C11 C 0.3484(4) -0.0113(4) 0.1498(3) 0.0509(12) Uani 1 1 d . . .
H11 H 0.3657 -0.0561 0.1886 0.061 Uiso 1 1 calc R . .
C12 C 0.3863(4) -0.0238(5) 0.0735(3) 0.0600(14) Uani 1 1 d . . .
H12 H 0.4343 -0.0787 0.0509 0.072 Uiso 1 1 calc R . .
C13 C 0.3430(4) 0.0563(5) 0.0364(3) 0.0613(14) Uani 1 1 d . . .
H13 H 0.3564 0.0671 -0.0163 0.074 Uiso 1 1 calc R . .
C14 C 0.2781(4) 0.1203(4) 0.0888(3) 0.0516(12) Uani 1 1 d . . .
H14 H 0.2388 0.1823 0.0784 0.062 Uiso 1 1 calc R . .
C15 C 0.5672(7) 0.1543(9) 0.2529(5) 0.109(3) Uani 1 1 d . . .
H15 H 0.5807 0.1100 0.2923 0.131 Uiso 1 1 calc R . .
C16 C 0.6082(6) 0.1375(9) 0.1785(7) 0.112(3) Uani 1 1 d . . .
H16 H 0.6555 0.0806 0.1579 0.135 Uiso 1 1 calc R . .
C17 C 0.5721(7) 0.2163(9) 0.1412(6) 0.110(3) Uani 1 1 d . . .
H17 H 0.5882 0.2259 0.0889 0.132 Uiso 1 1 calc R . .
C18 C 0.5060(6) 0.2827(6) 0.1935(7) 0.113(3) Uani 1 1 d . . .
H18 H 0.4694 0.3464 0.1839 0.135 Uiso 1 1 calc R . .
C19 C 0.5066(7) 0.2398(9) 0.2613(5) 0.111(3) Uani 1 1 d . . .
H19 H 0.4688 0.2679 0.3076 0.133 Uiso 1 1 calc R . .
C20 C 0.1459(3) 0.2623(3) 0.4187(3) 0.0362(9) Uani 1 1 d . . .
C21 C 0.0671(4) 0.3407(4) 0.4327(3) 0.0438(10) Uani 1 1 d . . .
H21 H 0.0179 0.3652 0.3895 0.053 Uiso 1 1 calc R . .
C22 C 0.0730(4) 0.3781(4) 0.5211(3) 0.0518(12) Uani 1 1 d . . .
H22 H 0.0288 0.4330 0.5490 0.062 Uiso 1 1 calc R . .
C23 C 0.1544(4) 0.3242(4) 0.5607(3) 0.0489(11) Uani 1 1 d . . .
H23 H 0.1767 0.3349 0.6212 0.059 Uiso 1 1 calc R . .
C24 C 0.2000(4) 0.2521(3) 0.4988(3) 0.0419(10) Uani 1 1 d . . .
H24 H 0.2586 0.2042 0.5091 0.050 Uiso 1 1 calc R . .
C25 C 0.3397(5) 0.4541(5) 0.4341(4) 0.0727(17) Uani 1 1 d . . .
H25 H 0.3531 0.4153 0.3792 0.087 Uiso 1 1 calc R . .
C26 C 0.2647(7) 0.5326(5) 0.4489(5) 0.093(2) Uani 1 1 d . . .
H26 H 0.2171 0.5598 0.4065 0.112 Uiso 1 1 calc R . .
C27 C 0.2717(10) 0.5680(6) 0.5374(6) 0.112(3) Uani 1 1 d . . .
H27 H 0.2295 0.6237 0.5667 0.135 Uiso 1 1 calc R . .
C28 C 0.3494(8) 0.5094(8) 0.5739(5) 0.104(3) Uani 1 1 d . . .
H28 H 0.3709 0.5163 0.6340 0.125 Uiso 1 1 calc R . .
C29 C 0.3920(6) 0.4385(6) 0.5111(5) 0.086(2) Uani 1 1 d . . .
H29 H 0.4485 0.3880 0.5195 0.103 Uiso 1 1 calc R . .
C30 C 0.3140(19) 0.196(3) 0.743(2) 0.40(2) Uani 1 1 d . . .
C32 C 0.325(2) 0.327(4) 0.918(3) 0.50(3) Uani 1 1 d . . .
C31 C 0.399(4) 0.232(4) 0.843(3) 0.51(3) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C8 Co1 C6 62.80(17) . . ?
C8 Co1 C9 43.59(17) . . ?
C6 Co1 C9 43.52(17) . . ?
C8 Co1 C4 161.5(6) . . ?
C6 Co1 C4 119.5(3) . . ?
C9 Co1 C4 151.6(6) . . ?
C8 Co1 C7 43.51(16) . . ?
C6 Co1 C7 43.15(17) . . ?
C9 Co1 C7 63.44(17) . . ?
C4 Co1 C7 123.7(4) . . ?
C8 Co1 C3 156.1(5) . . ?
C6 Co1 C3 119.4(3) . . ?
C9 Co1 C3 119.3(4) . . ?
C4 Co1 C3 41.5(5) . . ?
C7 Co1 C3 155.2(5) . . ?
C8 Co1 C2 124.3(3) . . ?
C6 Co1 C2 144.0(3) . . ?
C9 Co1 C2 113.2(2) . . ?
C4 Co1 C2 66.0(3) . . ?
C7 Co1 C2 166.4(4) . . ?
C3 Co1 C2 38.4(4) . . ?
C8 Co1 C5 127.2(4) . . ?
C6 Co1 C5 146.2(4) . . ?
C9 Co1 C5 167.5(5) . . ?
C4 Co1 C5 39.8(5) . . ?
C7 Co1 C5 117.3(3) . . ?
C3 Co1 C5 65.9(4) . . ?
C2 Co1 C5 62.8(3) . . ?
C8 Co1 C1 113.4(3) . . ?
C6 Co1 C1 176.1(3) . . ?
C9 Co1 C1 133.2(3) . . ?
C4 Co1 C1 64.4(4) . . ?
C7 Co1 C1 135.1(3) . . ?
C3 Co1 C1 63.5(3) . . ?
C2 Co1 C1 36.7(3) . . ?
C5 Co1 C1 36.5(4) . . ?
C15 Fe1 C16 40.7(4) . . ?
C15 Fe1 C19 38.5(4) . . ?
C16 Fe1 C19 67.1(3) . . ?
C15 Fe1 C18 66.4(4) . . ?
C16 Fe1 C18 67.6(4) . . ?
C19 Fe1 C18 40.1(4) . . ?
C15 Fe1 C17 67.0(4) . . ?
C16 Fe1 C17 39.3(4) . . ?
C19 Fe1 C17 67.9(3) . . ?
C18 Fe1 C17 41.4(4) . . ?
C15 Fe1 C11 107.3(3) . . ?
C16 Fe1 C11 121.4(4) . . ?
C19 Fe1 C11 122.8(3) . . ?
C18 Fe1 C11 159.4(3) . . ?
C17 Fe1 C11 156.5(4) . . ?
C15 Fe1 C12 123.8(4) . . ?
C16 Fe1 C12 107.2(3) . . ?
C19 Fe1 C12 158.5(4) . . ?
C18 Fe1 C12 159.2(4) . . ?
C17 Fe1 C12 121.9(3) . . ?
C11 Fe1 C12 40.8(2) . . ?
C15 Fe1 C10 121.6(3) . . ?
C16 Fe1 C10 157.3(4) . . ?
C19 Fe1 C10 107.9(2) . . ?
C18 Fe1 C10 123.8(3) . . ?
C17 Fe1 C10 161.6(4) . . ?
C11 Fe1 C10 41.09(18) . . ?
C12 Fe1 C10 68.86(19) . . ?
C15 Fe1 C13 160.1(4) . . ?
C16 Fe1 C13 123.7(3) . . ?
C19 Fe1 C13 160.2(4) . . ?
C18 Fe1 C13 124.6(4) . . ?
C17 Fe1 C13 109.0(3) . . ?
C11 Fe1 C13 68.1(2) . . ?
C12 Fe1 C13 40.1(2) . . ?
C10 Fe1 C13 68.55(19) . . ?
C15 Fe1 C14 157.8(3) . . ?
C16 Fe1 C14 160.2(4) . . ?
C19 Fe1 C14 124.1(3) . . ?
C18 Fe1 C14 109.4(3) . . ?
C17 Fe1 C14 125.5(4) . . ?
C11 Fe1 C14 68.5(2) . . ?
C12 Fe1 C14 68.2(2) . . ?
C10 Fe1 C14 40.89(19) . . ?
C13 Fe1 C14 40.5(2) . . ?
C23 Fe2 C24 40.86(18) . . ?
C23 Fe2 C28 106.6(3) . . ?
C24 Fe2 C28 120.7(3) . . ?
C23 Fe2 C26 159.0(3) . . ?
C24 Fe2 C26 159.6(3) . . ?
C28 Fe2 C26 67.8(3) . . ?
C23 Fe2 C20 69.01(18) . . ?
C24 Fe2 C20 41.22(17) . . ?
C28 Fe2 C20 156.8(4) . . ?
C26 Fe2 C20 124.2(3) . . ?
C23 Fe2 C27 121.8(3) . . ?
C24 Fe2 C27 156.3(3) . . ?
C28 Fe2 C27 39.7(3) . . ?
C26 Fe2 C27 41.1(3) . . ?
C20 Fe2 C27 161.7(4) . . ?
C23 Fe2 C21 68.49(19) . . ?
C24 Fe2 C21 68.76(18) . . ?
C28 Fe2 C21 160.6(3) . . ?
C26 Fe2 C21 109.7(3) . . ?
C20 Fe2 C21 40.84(17) . . ?
C27 Fe2 C21 125.6(4) . . ?
C23 Fe2 C29 122.0(3) . . ?
C24 Fe2 C29 105.9(3) . . ?
C28 Fe2 C29 40.2(3) . . ?
C26 Fe2 C29 67.7(3) . . ?
C20 Fe2 C29 121.4(3) . . ?
C27 Fe2 C29 67.6(4) . . ?
C21 Fe2 C29 158.4(3) . . ?
C23 Fe2 C25 158.6(3) . . ?
C24 Fe2 C25 122.9(2) . . ?
C28 Fe2 C25 67.4(3) . . ?
C26 Fe2 C25 39.9(3) . . ?
C20 Fe2 C25 107.9(2) . . ?
C27 Fe2 C25 67.7(3) . . ?
C21 Fe2 C25 123.9(2) . . ?
C29 Fe2 C25 40.2(3) . . ?
C23 Fe2 C22 40.1(2) . . ?
C24 Fe2 C22 68.34(19) . . ?
C28 Fe2 C22 123.3(3) . . ?
C26 Fe2 C22 124.7(3) . . ?
C20 Fe2 C22 68.92(18) . . ?
C27 Fe2 C22 108.8(3) . . ?
C21 Fe2 C22 41.09(19) . . ?
C29 Fe2 C22 158.2(3) . . ?
C25 Fe2 C22 160.3(3) . . ?
N1 P1 N3 116.4(2) . . ?
N1 P1 C6 111.0(2) . . ?
N3 P1 C6 111.3(2) . . ?
N1 P1 Cl1 107.43(18) . . ?
N3 P1 Cl1 106.77(18) . . ?
C6 P1 Cl1 102.90(15) . . ?
N1 P2 N2 118.4(2) . . ?
N1 P2 Cl2 109.92(18) . . ?
N2 P2 Cl2 106.7(2) . . ?
N1 P2 Cl3 110.75(19) . . ?
N2 P2 Cl3 109.4(2) . . ?
Cl2 P2 Cl3 99.99(10) . . ?
N3 P3 N2 118.7(2) . . ?
N3 P3 Cl4 107.93(19) . . ?
N2 P3 Cl4 108.0(2) . . ?
N3 P3 Cl5 110.5(2) . . ?
N2 P3 Cl5 109.0(2) . . ?
Cl4 P3 Cl5 101.32(12) . . ?
N6 P4 N4 116.2(2) . . ?
N6 P4 C8 110.5(2) . . ?
N4 P4 C8 111.6(2) . . ?
N6 P4 Cl6 106.88(18) . . ?
N4 P4 Cl6 106.38(18) . . ?
C8 P4 Cl6 104.26(15) . . ?
N4 P5 N5 118.7(2) . . ?
N4 P5 Cl7 110.30(18) . . ?
N5 P5 Cl7 107.7(2) . . ?
N4 P5 Cl8 108.64(18) . . ?
N5 P5 Cl8 108.8(2) . . ?
Cl7 P5 Cl8 101.23(9) . . ?
N6 P6 N5 118.5(2) . . ?
N6 P6 Cl10 108.05(19) . . ?
N5 P6 Cl10 109.8(2) . . ?
N6 P6 Cl9 109.55(18) . . ?
N5 P6 Cl9 108.2(2) . . ?
Cl10 P6 Cl9 101.46(9) . . ?
P2 N1 P1 121.6(3) . . ?
P3 N2 P2 119.6(3) . . ?
P3 N3 P1 121.9(3) . . ?
P5 N4 P4 120.1(2) . . ?
P5 N5 P6 120.7(3) . . ?
P6 N6 P4 120.2(2) . . ?
C5 C1 C2 112.0(9) . . ?
C5 C1 Co1 71.7(4) . . ?
C2 C1 Co1 71.2(4) . . ?
C5 C1 H1 124.0 . . ?
C2 C1 H1 124.0 . . ?
Co1 C1 H1 124.0 . . ?
C1 C2 C3 109.4(9) . . ?
C1 C2 Co1 72.1(4) . . ?
C3 C2 Co1 69.8(4) . . ?
C1 C2 H2 125.3 . . ?
C3 C2 H2 125.3 . . ?
Co1 C2 H2 125.3 . . ?
C2 C3 C4 106.1(8) . . ?
C2 C3 Co1 71.7(4) . . ?
C4 C3 Co1 69.0(4) . . ?
C2 C3 H3 127.0 . . ?
C4 C3 H3 126.9 . . ?
Co1 C3 H3 126.9 . . ?
C5 C4 C3 104.0(7) . . ?
C5 C4 Co1 71.7(5) . . ?
C3 C4 Co1 69.5(4) . . ?
C5 C4 H4 127.7 . . ?
C3 C4 H4 127.9 . . ?
Co1 C4 H4 127.8 . . ?
C1 C5 C4 108.5(9) . . ?
C1 C5 Co1 71.8(4) . . ?
C4 C5 Co1 68.6(4) . . ?
C1 C5 H5 125.7 . . ?
C4 C5 H5 125.8 . . ?
Co1 C5 H5 125.8 . . ?
C7 C6 C9 91.5(3) . . ?
C7 C6 P1 136.7(3) . . ?
C9 C6 P1 131.6(3) . . ?
C7 C6 Co1 69.6(2) . . ?
C9 C6 Co1 68.9(2) . . ?
P1 C6 Co1 123.2(2) . . ?
C10 C7 C6 135.9(4) . . ?
C10 C7 C8 134.3(4) . . ?
C6 C7 C8 88.8(3) . . ?
C10 C7 Co1 130.7(3) . . ?
C6 C7 Co1 67.2(2) . . ?
C8 C7 Co1 67.0(2) . . ?
C9 C8 C7 91.0(3) . . ?
C9 C8 P4 135.8(3) . . ?
C7 C8 P4 133.2(3) . . ?
C9 C8 Co1 69.0(2) . . ?
C7 C8 Co1 69.5(2) . . ?
P4 C8 Co1 121.8(2) . . ?
C20 C9 C6 133.4(4) . . ?
C20 C9 C8 137.2(4) . . ?
C6 C9 C8 88.6(3) . . ?
C20 C9 Co1 128.7(3) . . ?
C6 C9 Co1 67.6(2) . . ?
C8 C9 Co1 67.5(2) . . ?
C14 C10 C11 107.0(4) . . ?
C14 C10 C7 126.0(4) . . ?
C11 C10 C7 126.9(4) . . ?
C14 C10 Fe1 69.7(3) . . ?
C11 C10 Fe1 69.3(3) . . ?
C7 C10 Fe1 125.5(3) . . ?
C12 C11 C10 108.0(5) . . ?
C12 C11 Fe1 69.7(3) . . ?
C10 C11 Fe1 69.6(3) . . ?
C12 C11 H11 126.0 . . ?
C10 C11 H11 126.0 . . ?
Fe1 C11 H11 126.0 . . ?
C13 C12 C11 108.2(4) . . ?
C13 C12 Fe1 70.2(3) . . ?
C11 C12 Fe1 69.5(3) . . ?
C13 C12 H12 125.9 . . ?
C11 C12 H12 125.9 . . ?
Fe1 C12 H12 125.9 . . ?
C12 C13 C14 108.6(5) . . ?
C12 C13 Fe1 69.7(3) . . ?
C14 C13 Fe1 69.8(3) . . ?
C12 C13 H13 125.7 . . ?
C14 C13 H13 125.7 . . ?
Fe1 C13 H13 125.7 . . ?
C13 C14 C10 108.0(5) . . ?
C13 C14 Fe1 69.7(3) . . ?
C10 C14 Fe1 69.4(3) . . ?
C13 C14 H14 126.0 . . ?
C10 C14 H14 126.0 . . ?
Fe1 C14 H14 126.0 . . ?
C19 C15 C16 109.7(9) . . ?
C19 C15 Fe1 71.1(5) . . ?
C16 C15 Fe1 70.0(4) . . ?
C19 C15 H15 125.2 . . ?
C16 C15 H15 125.2 . . ?
Fe1 C15 H15 125.2 . . ?
C17 C16 C15 107.6(9) . . ?
C17 C16 Fe1 70.9(4) . . ?
C15 C16 Fe1 69.3(4) . . ?
C17 C16 H16 126.2 . . ?
C15 C16 H16 126.2 . . ?
Fe1 C16 H16 126.2 . . ?
C16 C17 C18 107.2(9) . . ?
C16 C17 Fe1 69.8(4) . . ?
C18 C17 Fe1 69.1(4) . . ?
C16 C17 H17 126.4 . . ?
C18 C17 H17 126.4 . . ?
Fe1 C17 H17 126.4 . . ?
C19 C18 C17 106.5(9) . . ?
C19 C18 Fe1 69.6(4) . . ?
C17 C18 Fe1 69.5(4) . . ?
C19 C18 H18 126.8 . . ?
C17 C18 H18 126.8 . . ?
Fe1 C18 H18 126.8 . . ?
C15 C19 C18 109.0(8) . . ?
C15 C19 Fe1 70.4(4) . . ?
C18 C19 Fe1 70.3(4) . . ?
C15 C19 H19 125.5 . . ?
C18 C19 H19 125.5 . . ?
Fe1 C19 H19 125.5 . . ?
C21 C20 C24 107.3(4) . . ?
C21 C20 C9 127.8(4) . . ?
C24 C20 C9 124.9(4) . . ?
C21 C20 Fe2 69.6(2) . . ?
C24 C20 Fe2 69.2(2) . . ?
C9 C20 Fe2 126.2(3) . . ?
C20 C21 C22 108.0(4) . . ?
C20 C21 Fe2 69.5(2) . . ?
C22 C21 Fe2 69.7(3) . . ?
C20 C21 H21 126.0 . . ?
C22 C21 H21 126.0 . . ?
Fe2 C21 H21 126.0 . . ?
C23 C22 C21 108.1(4) . . ?
C23 C22 Fe2 69.5(3) . . ?
C21 C22 Fe2 69.3(3) . . ?
C23 C22 H22 126.0 . . ?
C21 C22 H22 126.0 . . ?
Fe2 C22 H22 126.0 . . ?
C22 C23 C24 108.8(4) . . ?
C22 C23 Fe2 70.5(3) . . ?
C24 C23 Fe2 69.6(3) . . ?
C22 C23 H23 125.6 . . ?
C24 C23 H23 125.6 . . ?
Fe2 C23 H23 125.6 . . ?
C23 C24 C20 107.9(4) . . ?
C23 C24 Fe2 69.6(3) . . ?
C20 C24 Fe2 69.6(2) . . ?
C23 C24 H24 126.1 . . ?
C20 C24 H24 126.1 . . ?
Fe2 C24 H24 126.1 . . ?
C26 C25 C29 108.6(7) . . ?
C26 C25 Fe2 69.7(3) . . ?
C29 C25 Fe2 69.8(3) . . ?
C26 C25 H25 125.7 . . ?
C29 C25 H25 125.7 . . ?
Fe2 C25 H25 125.7 . . ?
C25 C26 C27 107.4(8) . . ?
C25 C26 Fe2 70.4(4) . . ?
C27 C26 Fe2 69.6(4) . . ?
C25 C26 H26 126.3 . . ?
C27 C26 H26 126.3 . . ?
Fe2 C26 H26 126.3 . . ?
C28 C27 C26 107.4(8) . . ?
C28 C27 Fe2 69.9(4) . . ?
C26 C27 Fe2 69.3(3) . . ?
C28 C27 H27 126.3 . . ?
C26 C27 H27 126.3 . . ?
Fe2 C27 H27 126.3 . . ?
C27 C28 C29 109.1(7) . . ?
C27 C28 Fe2 70.3(4) . . ?
C29 C28 Fe2 70.2(4) . . ?
C27 C28 H28 125.5 . . ?
C29 C28 H28 125.4 . . ?
Fe2 C28 H28 125.5 . . ?
C28 C29 C25 107.5(8) . . ?
C28 C29 Fe2 69.6(4) . . ?
C25 C29 Fe2 70.0(4) . . ?
C28 C29 H29 126.3 . . ?
C25 C29 H29 126.3 . . ?
Fe2 C29 H29 126.3 . . ?
C30 C31 C32 109(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 C8 1.975(4) . ?
Co1 C6 1.977(4) . ?
Co1 C9 1.996(4) . ?
Co1 C4 2.004(6) . ?
Co1 C7 2.010(4) . ?
Co1 C3 2.011(6) . ?
Co1 C2 2.035(6) . ?
Co1 C5 2.044(7) . ?
Co1 C1 2.045(6) . ?
Fe1 C15 2.023(7) . ?
Fe1 C16 2.031(7) . ?
Fe1 C19 2.031(7) . ?
Fe1 C18 2.040(7) . ?
Fe1 C17 2.045(7) . ?
Fe1 C11 2.046(5) . ?
Fe1 C12 2.048(5) . ?
Fe1 C10 2.051(4) . ?
Fe1 C13 2.055(5) . ?
Fe1 C14 2.056(5) . ?
Fe2 C23 2.033(5) . ?
Fe2 C24 2.033(4) . ?
Fe2 C28 2.035(7) . ?
Fe2 C26 2.037(6) . ?
Fe2 C20 2.038(4) . ?
Fe2 C27 2.040(6) . ?
Fe2 C21 2.040(5) . ?
Fe2 C29 2.042(6) . ?
Fe2 C25 2.045(6) . ?
Fe2 C22 2.045(5) . ?
Cl1 P1 2.0277(18) . ?
Cl2 P2 1.974(2) . ?
Cl3 P2 1.995(2) . ?
Cl4 P3 1.988(2) . ?
Cl5 P3 1.995(2) . ?
Cl6 P4 2.0340(19) . ?
Cl7 P5 1.994(2) . ?
Cl8 P5 1.997(2) . ?
Cl9 P6 1.992(2) . ?
Cl10 P6 1.991(2) . ?
P1 N1 1.593(4) . ?
P1 N3 1.595(4) . ?
P1 C6 1.770(4) . ?
P2 N1 1.568(4) . ?
P2 N2 1.576(5) . ?
P3 N3 1.565(4) . ?
P3 N2 1.573(5) . ?
P4 N6 1.584(4) . ?
P4 N4 1.598(4) . ?
P4 C8 1.756(4) . ?
P5 N4 1.568(4) . ?
P5 N5 1.571(5) . ?
P6 N6 1.573(4) . ?
P6 N5 1.583(4) . ?
C1 C5 1.282(13) . ?
C1 C2 1.283(11) . ?
C1 H1 0.9800 . ?
C2 C3 1.332(14) . ?
C2 H2 0.9800 . ?
C3 C4 1.422(15) . ?
C3 H3 0.9800 . ?
C4 C5 1.377(15) . ?
C4 H4 0.9800 . ?
C5 H5 0.9800 . ?
C6 C7 1.467(6) . ?
C6 C9 1.473(6) . ?
C7 C10 1.460(6) . ?
C7 C8 1.478(6) . ?
C8 C9 1.475(6) . ?
C9 C20 1.466(6) . ?
C10 C14 1.434(7) . ?
C10 C11 1.438(6) . ?
C11 C12 1.426(7) . ?
C11 H11 0.9800 . ?
C12 C13 1.408(8) . ?
C12 H12 0.9800 . ?
C13 C14 1.423(7) . ?
C13 H13 0.9800 . ?
C14 H14 0.9800 . ?
C15 C19 1.336(13) . ?
C15 C16 1.410(12) . ?
C15 H15 0.9800 . ?
C16 C17 1.370(13) . ?
C16 H16 0.9800 . ?
C17 C18 1.445(12) . ?
C17 H17 0.9800 . ?
C18 C19 1.396(13) . ?
C18 H18 0.9800 . ?
C19 H19 0.9800 . ?
C20 C21 1.423(6) . ?
C20 C24 1.433(6) . ?
C21 C22 1.434(7) . ?
C21 H21 0.9800 . ?
C22 C23 1.398(7) . ?
C22 H22 0.9800 . ?
C23 C24 1.419(6) . ?
C23 H23 0.9800 . ?
C24 H24 0.9800 . ?
C25 C26 1.393(10) . ?
C25 C29 1.405(9) . ?
C25 H25 0.9800 . ?
C26 C27 1.431(11) . ?
C26 H26 0.9800 . ?
C27 C28 1.385(12) . ?
C27 H27 0.9800 . ?
C28 C29 1.401(11) . ?
C28 H28 0.9800 . ?
C29 H29 0.9800 . ?
C30 C31 1.75(5) . ?
C32 C31 1.91(5) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N2 P2 N1 P1 -15.4(5) . . . . ?
Cl2 P2 N1 P1 -138.4(3) . . . . ?
Cl3 P2 N1 P1 112.0(3) . . . . ?
N3 P1 N1 P2 9.2(4) . . . . ?
C6 P1 N1 P2 137.8(3) . . . . ?
Cl1 P1 N1 P2 -110.4(3) . . . . ?
N3 P3 N2 P2 -18.4(6) . . . . ?
Cl4 P3 N2 P2 -141.6(4) . . . . ?
Cl5 P3 N2 P2 109.2(4) . . . . ?
N1 P2 N2 P3 19.9(6) . . . . ?
Cl2 P2 N2 P3 144.5(4) . . . . ?
Cl3 P2 N2 P3 -108.2(4) . . . . ?
N2 P3 N3 P1 12.3(5) . . . . ?
Cl4 P3 N3 P1 135.5(3) . . . . ?
Cl5 P3 N3 P1 -114.5(3) . . . . ?
N1 P1 N3 P3 -7.6(5) . . . . ?
C6 P1 N3 P3 -136.1(3) . . . . ?
Cl1 P1 N3 P3 112.3(3) . . . . ?
N5 P5 N4 P4 -8.4(5) . . . . ?
Cl7 P5 N4 P4 116.6(3) . . . . ?
Cl8 P5 N4 P4 -133.3(3) . . . . ?
N6 P4 N4 P5 24.9(4) . . . . ?
C8 P4 N4 P5 152.9(3) . . . . ?
Cl6 P4 N4 P5 -93.9(3) . . . . ?
N4 P5 N5 P6 -8.7(6) . . . . ?
Cl7 P5 N5 P6 -134.9(4) . . . . ?
Cl8 P5 N5 P6 116.1(4) . . . . ?
N6 P6 N5 P5 8.5(6) . . . . ?
Cl10 P6 N5 P5 -116.2(4) . . . . ?
Cl9 P6 N5 P5 133.9(4) . . . . ?
N5 P6 N6 P4 8.9(5) . . . . ?
Cl10 P6 N6 P4 134.5(3) . . . . ?
Cl9 P6 N6 P4 -115.8(3) . . . . ?
N4 P4 N6 P6 -25.1(4) . . . . ?
C8 P4 N6 P6 -153.7(3) . . . . ?
Cl6 P4 N6 P6 93.4(3) . . . . ?
C8 Co1 C1 C5 121.6(7) . . . . ?
C6 Co1 C1 C5 136(5) . . . . ?
C9 Co1 C1 C5 169.0(6) . . . . ?
C4 Co1 C1 C5 -38.2(7) . . . . ?
C7 Co1 C1 C5 74.8(7) . . . . ?
C3 Co1 C1 C5 -84.7(8) . . . . ?
C2 Co1 C1 C5 -121.9(9) . . . . ?
C8 Co1 C1 C2 -116.5(6) . . . . ?
C6 Co1 C1 C2 -102(5) . . . . ?
C9 Co1 C1 C2 -69.1(7) . . . . ?
C4 Co1 C1 C2 83.7(7) . . . . ?
C7 Co1 C1 C2 -163.3(5) . . . . ?
C3 Co1 C1 C2 37.2(6) . . . . ?
C5 Co1 C1 C2 121.9(9) . . . . ?
C5 C1 C2 C3 0.3(9) . . . . ?
Co1 C1 C2 C3 -60.1(5) . . . . ?
C5 C1 C2 Co1 60.4(6) . . . . ?
C8 Co1 C2 C1 83.6(6) . . . . ?
C6 Co1 C2 C1 173.5(5) . . . . ?
C9 Co1 C2 C1 132.2(6) . . . . ?
C4 Co1 C2 C1 -78.8(7) . . . . ?
C7 Co1 C2 C1 59.4(13) . . . . ?
C3 Co1 C2 C1 -119.4(8) . . . . ?
C5 Co1 C2 C1 -34.6(6) . . . . ?
C8 Co1 C2 C3 -157.0(6) . . . . ?
C6 Co1 C2 C3 -67.1(7) . . . . ?
C9 Co1 C2 C3 -108.4(6) . . . . ?
C4 Co1 C2 C3 40.7(7) . . . . ?
C7 Co1 C2 C3 178.8(9) . . . . ?
C5 Co1 C2 C3 84.8(7) . . . . ?
C1 Co1 C2 C3 119.4(8) . . . . ?
C1 C2 C3 C4 0.7(8) . . . . ?
Co1 C2 C3 C4 -60.8(5) . . . . ?
C1 C2 C3 Co1 61.5(5) . . . . ?
C8 Co1 C3 C2 52.9(8) . . . . ?
C6 Co1 C3 C2 141.6(5) . . . . ?
C9 Co1 C3 C2 91.2(6) . . . . ?
C4 Co1 C3 C2 -116.0(8) . . . . ?
C7 Co1 C3 C2 -179.3(5) . . . . ?
C5 Co1 C3 C2 -76.0(6) . . . . ?
C1 Co1 C3 C2 -35.5(5) . . . . ?
C8 Co1 C3 C4 168.9(7) . . . . ?
C6 Co1 C3 C4 -102.4(7) . . . . ?
C9 Co1 C3 C4 -152.8(6) . . . . ?
C7 Co1 C3 C4 -63.3(8) . . . . ?
C2 Co1 C3 C4 116.0(8) . . . . ?
C5 Co1 C3 C4 40.0(6) . . . . ?
C1 Co1 C3 C4 80.5(7) . . . . ?
C2 C3 C4 C5 -1.3(8) . . . . ?
Co1 C3 C4 C5 -63.9(5) . . . . ?
C2 C3 C4 Co1 62.6(5) . . . . ?
C8 Co1 C4 C5 -52.4(10) . . . . ?
C6 Co1 C4 C5 -144.4(5) . . . . ?
C9 Co1 C4 C5 170.6(5) . . . . ?
C7 Co1 C4 C5 -93.4(5) . . . . ?
C3 Co1 C4 C5 113.4(7) . . . . ?
C2 Co1 C4 C5 75.7(6) . . . . ?
C1 Co1 C4 C5 35.2(5) . . . . ?
C8 Co1 C4 C3 -165.7(7) . . . . ?
C6 Co1 C4 C3 102.3(6) . . . . ?
C9 Co1 C4 C3 57.2(8) . . . . ?
C7 Co1 C4 C3 153.2(5) . . . . ?
C2 Co1 C4 C3 -37.7(5) . . . . ?
C5 Co1 C4 C3 -113.4(7) . . . . ?
C1 Co1 C4 C3 -78.2(6) . . . . ?
C2 C1 C5 C4 -1.2(9) . . . . ?
Co1 C1 C5 C4 58.9(5) . . . . ?
C2 C1 C5 Co1 -60.1(6) . . . . ?
C3 C4 C5 C1 1.5(9) . . . . ?
Co1 C4 C5 C1 -60.9(6) . . . . ?
C3 C4 C5 Co1 62.4(5) . . . . ?
C8 Co1 C5 C1 -79.2(6) . . . . ?
C6 Co1 C5 C1 -175.1(4) . . . . ?
C9 Co1 C5 C1 -39.8(15) . . . . ?
C4 Co1 C5 C1 119.2(9) . . . . ?
C7 Co1 C5 C1 -129.9(5) . . . . ?
C3 Co1 C5 C1 77.4(7) . . . . ?
C2 Co1 C5 C1 34.7(6) . . . . ?
C8 Co1 C5 C4 161.6(6) . . . . ?
C6 Co1 C5 C4 65.7(8) . . . . ?
C9 Co1 C5 C4 -159.0(11) . . . . ?
C7 Co1 C5 C4 110.9(7) . . . . ?
C3 Co1 C5 C4 -41.8(6) . . . . ?
C2 Co1 C5 C4 -84.5(7) . . . . ?
C1 Co1 C5 C4 -119.2(9) . . . . ?
N1 P1 C6 C7 -150.9(4) . . . . ?
N3 P1 C6 C7 -19.6(5) . . . . ?
Cl1 P1 C6 C7 94.4(4) . . . . ?
N1 P1 C6 C9 34.6(5) . . . . ?
N3 P1 C6 C9 166.0(4) . . . . ?
Cl1 P1 C6 C9 -80.0(4) . . . . ?
N1 P1 C6 Co1 -55.8(3) . . . . ?
N3 P1 C6 Co1 75.5(3) . . . . ?
Cl1 P1 C6 Co1 -170.5(2) . . . . ?
C8 Co1 C6 C7 -49.9(2) . . . . ?
C9 Co1 C6 C7 -100.0(3) . . . . ?
C4 Co1 C6 C7 109.2(7) . . . . ?
C3 Co1 C6 C7 157.2(6) . . . . ?
C2 Co1 C6 C7 -161.7(5) . . . . ?
C5 Co1 C6 C7 67.2(7) . . . . ?
C1 Co1 C6 C7 -65(5) . . . . ?
C8 Co1 C6 C9 50.1(2) . . . . ?
C4 Co1 C6 C9 -150.8(7) . . . . ?
C7 Co1 C6 C9 100.0(3) . . . . ?
C3 Co1 C6 C9 -102.8(6) . . . . ?
C2 Co1 C6 C9 -61.7(6) . . . . ?
C5 Co1 C6 C9 167.2(7) . . . . ?
C1 Co1 C6 C9 35(5) . . . . ?
C8 Co1 C6 P1 176.9(3) . . . . ?
C9 Co1 C6 P1 126.8(4) . . . . ?
C4 Co1 C6 P1 -24.0(7) . . . . ?
C7 Co1 C6 P1 -133.2(4) . . . . ?
C3 Co1 C6 P1 24.0(6) . . . . ?
C2 Co1 C6 P1 65.1(6) . . . . ?
C5 Co1 C6 P1 -66.0(8) . . . . ?
C1 Co1 C6 P1 162(5) . . . . ?
C9 C6 C7 C10 167.5(5) . . . . ?
P1 C6 C7 C10 -8.4(8) . . . . ?
Co1 C6 C7 C10 -125.7(5) . . . . ?
C9 C6 C7 C8 -1.3(3) . . . . ?
P1 C6 C7 C8 -177.2(4) . . . . ?
Co1 C6 C7 C8 65.5(2) . . . . ?
C9 C6 C7 Co1 -66.8(2) . . . . ?
P1 C6 C7 Co1 117.3(4) . . . . ?
C8 Co1 C7 C10 -129.4(5) . . . . ?
C6 Co1 C7 C10 131.8(5) . . . . ?
C9 Co1 C7 C10 -178.9(5) . . . . ?
C4 Co1 C7 C10 32.9(8) . . . . ?
C3 Co1 C7 C10 78.3(10) . . . . ?
C2 Co1 C7 C10 -99.9(12) . . . . ?
C5 Co1 C7 C10 -13.0(7) . . . . ?
C1 Co1 C7 C10 -53.3(7) . . . . ?
C8 Co1 C7 C6 98.8(3) . . . . ?
C9 Co1 C7 C6 49.3(2) . . . . ?
C4 Co1 C7 C6 -98.8(7) . . . . ?
C3 Co1 C7 C6 -53.5(9) . . . . ?
C2 Co1 C7 C6 128.3(12) . . . . ?
C5 Co1 C7 C6 -144.7(6) . . . . ?
C1 Co1 C7 C6 175.0(5) . . . . ?
C6 Co1 C7 C8 -98.8(3) . . . . ?
C9 Co1 C7 C8 -49.5(2) . . . . ?
C4 Co1 C7 C8 162.4(7) . . . . ?
C3 Co1 C7 C8 -152.3(8) . . . . ?
C2 Co1 C7 C8 29.5(12) . . . . ?
C5 Co1 C7 C8 116.5(6) . . . . ?
C1 Co1 C7 C8 76.2(5) . . . . ?
C10 C7 C8 C9 -167.8(5) . . . . ?
C6 C7 C8 C9 1.3(3) . . . . ?
Co1 C7 C8 C9 67.0(2) . . . . ?
C10 C7 C8 P4 10.3(8) . . . . ?
C6 C7 C8 P4 179.4(4) . . . . ?
Co1 C7 C8 P4 -114.9(4) . . . . ?
C10 C7 C8 Co1 125.2(5) . . . . ?
C6 C7 C8 Co1 -65.7(2) . . . . ?
N6 P4 C8 C9 -13.6(5) . . . . ?
N4 P4 C8 C9 -144.6(4) . . . . ?
Cl6 P4 C8 C9 101.0(4) . . . . ?
N6 P4 C8 C7 169.2(4) . . . . ?
N4 P4 C8 C7 38.2(5) . . . . ?
Cl6 P4 C8 C7 -76.2(4) . . . . ?
N6 P4 C8 Co1 78.2(3) . . . . ?
N4 P4 C8 Co1 -52.8(3) . . . . ?
Cl6 P4 C8 Co1 -167.2(2) . . . . ?
C6 Co1 C8 C9 -50.0(2) . . . . ?
C4 Co1 C8 C9 -152.0(10) . . . . ?
C7 Co1 C8 C9 -99.5(3) . . . . ?
C3 Co1 C8 C9 51.7(7) . . . . ?
C2 Co1 C8 C9 88.6(4) . . . . ?
C5 Co1 C8 C9 168.5(5) . . . . ?
C1 Co1 C8 C9 128.9(4) . . . . ?
C6 Co1 C8 C7 49.5(2) . . . . ?
C9 Co1 C8 C7 99.5(3) . . . . ?
C4 Co1 C8 C7 -52.5(10) . . . . ?
C3 Co1 C8 C7 151.2(7) . . . . ?
C2 Co1 C8 C7 -171.9(4) . . . . ?
C5 Co1 C8 C7 -92.1(5) . . . . ?
C1 Co1 C8 C7 -131.6(4) . . . . ?
C6 Co1 C8 P4 178.3(3) . . . . ?
C9 Co1 C8 P4 -131.7(4) . . . . ?
C4 Co1 C8 P4 76.3(10) . . . . ?
C7 Co1 C8 P4 128.9(4) . . . . ?
C3 Co1 C8 P4 -79.9(7) . . . . ?
C2 Co1 C8 P4 -43.1(5) . . . . ?
C5 Co1 C8 P4 36.8(5) . . . . ?
C1 Co1 C8 P4 -2.8(5) . . . . ?
C7 C6 C9 C20 -169.8(4) . . . . ?
P1 C6 C9 C20 6.4(7) . . . . ?
Co1 C6 C9 C20 122.7(5) . . . . ?
C7 C6 C9 C8 1.3(3) . . . . ?
P1 C6 C9 C8 177.6(4) . . . . ?
Co1 C6 C9 C8 -66.1(2) . . . . ?
C7 C6 C9 Co1 67.4(2) . . . . ?
P1 C6 C9 Co1 -116.3(4) . . . . ?
C7 C8 C9 C20 169.2(5) . . . . ?
P4 C8 C9 C20 -8.7(8) . . . . ?
Co1 C8 C9 C20 -123.2(5) . . . . ?
C7 C8 C9 C6 -1.3(3) . . . . ?
P4 C8 C9 C6 -179.3(4) . . . . ?
Co1 C8 C9 C6 66.2(2) . . . . ?
C7 C8 C9 Co1 -67.5(2) . . . . ?
P4 C8 C9 Co1 114.5(4) . . . . ?
C8 Co1 C9 C20 133.3(5) . . . . ?
C6 Co1 C9 C20 -128.5(5) . . . . ?
C4 Co1 C9 C20 -65.0(8) . . . . ?
C7 Co1 C9 C20 -177.3(4) . . . . ?
C3 Co1 C9 C20 -25.3(7) . . . . ?
C2 Co1 C9 C20 17.2(6) . . . . ?
C5 Co1 C9 C20 86.1(12) . . . . ?
C1 Co1 C9 C20 54.6(6) . . . . ?
C8 Co1 C9 C6 -98.2(3) . . . . ?
C4 Co1 C9 C6 63.5(8) . . . . ?
C7 Co1 C9 C6 -48.8(2) . . . . ?
C3 Co1 C9 C6 103.2(6) . . . . ?
C2 Co1 C9 C6 145.7(4) . . . . ?
C5 Co1 C9 C6 -145.4(11) . . . . ?
C1 Co1 C9 C6 -176.9(4) . . . . ?
C6 Co1 C9 C8 98.2(3) . . . . ?
C4 Co1 C9 C8 161.7(7) . . . . ?
C7 Co1 C9 C8 49.4(2) . . . . ?
C3 Co1 C9 C8 -158.6(5) . . . . ?
C2 Co1 C9 C8 -116.0(4) . . . . ?
C5 Co1 C9 C8 -47.2(12) . . . . ?
C1 Co1 C9 C8 -78.7(4) . . . . ?
C6 C7 C10 C14 -169.6(5) . . . . ?
C8 C7 C10 C14 -5.4(8) . . . . ?
Co1 C7 C10 C14 91.5(5) . . . . ?
C6 C7 C10 C11 9.5(8) . . . . ?
C8 C7 C10 C11 173.7(4) . . . . ?
Co1 C7 C10 C11 -89.4(6) . . . . ?
C6 C7 C10 Fe1 -80.0(6) . . . . ?
C8 C7 C10 Fe1 84.2(6) . . . . ?
Co1 C7 C10 Fe1 -178.9(2) . . . . ?
C15 Fe1 C10 C14 161.8(5) . . . . ?
C16 Fe1 C10 C14 -164.8(7) . . . . ?
C19 Fe1 C10 C14 121.9(5) . . . . ?
C18 Fe1 C10 C14 80.6(5) . . . . ?
C17 Fe1 C10 C14 48.5(9) . . . . ?
C11 Fe1 C10 C14 -118.3(4) . . . . ?
C12 Fe1 C10 C14 -80.6(3) . . . . ?
C13 Fe1 C10 C14 -37.4(3) . . . . ?
C15 Fe1 C10 C11 -79.9(5) . . . . ?
C16 Fe1 C10 C11 -46.5(8) . . . . ?
C19 Fe1 C10 C11 -119.8(5) . . . . ?
C18 Fe1 C10 C11 -161.1(5) . . . . ?
C17 Fe1 C10 C11 166.7(9) . . . . ?
C12 Fe1 C10 C11 37.6(3) . . . . ?
C13 Fe1 C10 C11 80.8(3) . . . . ?
C14 Fe1 C10 C11 118.3(4) . . . . ?
C15 Fe1 C10 C7 41.3(6) . . . . ?
C16 Fe1 C10 C7 74.7(8) . . . . ?
C19 Fe1 C10 C7 1.4(6) . . . . ?
C18 Fe1 C10 C7 -39.8(6) . . . . ?
C17 Fe1 C10 C7 -72.0(10) . . . . ?
C11 Fe1 C10 C7 121.3(5) . . . . ?
C12 Fe1 C10 C7 158.9(5) . . . . ?
C13 Fe1 C10 C7 -157.9(5) . . . . ?
C14 Fe1 C10 C7 -120.5(5) . . . . ?
C14 C10 C11 C12 0.4(5) . . . . ?
C7 C10 C11 C12 -178.8(4) . . . . ?
Fe1 C10 C11 C12 -59.3(4) . . . . ?
C14 C10 C11 Fe1 59.8(3) . . . . ?
C7 C10 C11 Fe1 -119.5(5) . . . . ?
C15 Fe1 C11 C12 -122.1(4) . . . . ?
C16 Fe1 C11 C12 -79.8(5) . . . . ?
C19 Fe1 C11 C12 -161.3(5) . . . . ?
C18 Fe1 C11 C12 169.2(9) . . . . ?
C17 Fe1 C11 C12 -50.3(9) . . . . ?
C10 Fe1 C11 C12 119.3(4) . . . . ?
C13 Fe1 C11 C12 37.3(3) . . . . ?
C14 Fe1 C11 C12 81.0(3) . . . . ?
C15 Fe1 C11 C10 118.6(4) . . . . ?
C16 Fe1 C11 C10 160.9(4) . . . . ?
C19 Fe1 C11 C10 79.4(5) . . . . ?
C18 Fe1 C11 C10 49.9(10) . . . . ?
C17 Fe1 C11 C10 -169.6(8) . . . . ?
C12 Fe1 C11 C10 -119.3(4) . . . . ?
C13 Fe1 C11 C10 -82.0(3) . . . . ?
C14 Fe1 C11 C10 -38.3(3) . . . . ?
C10 C11 C12 C13 -0.4(6) . . . . ?
Fe1 C11 C12 C13 -59.7(4) . . . . ?
C10 C11 C12 Fe1 59.3(3) . . . . ?
C15 Fe1 C12 C13 -163.9(4) . . . . ?
C16 Fe1 C12 C13 -122.3(5) . . . . ?
C19 Fe1 C12 C13 166.6(7) . . . . ?
C18 Fe1 C12 C13 -50.0(9) . . . . ?
C17 Fe1 C12 C13 -81.9(5) . . . . ?
C11 Fe1 C12 C13 119.3(4) . . . . ?
C10 Fe1 C12 C13 81.4(3) . . . . ?
C14 Fe1 C12 C13 37.3(3) . . . . ?
C15 Fe1 C12 C11 76.8(5) . . . . ?
C16 Fe1 C12 C11 118.4(5) . . . . ?
C19 Fe1 C12 C11 47.2(8) . . . . ?
C18 Fe1 C12 C11 -169.3(8) . . . . ?
C17 Fe1 C12 C11 158.8(5) . . . . ?
C10 Fe1 C12 C11 -37.9(3) . . . . ?
C13 Fe1 C12 C11 -119.3(4) . . . . ?
C14 Fe1 C12 C11 -82.0(3) . . . . ?
C11 C12 C13 C14 0.3(6) . . . . ?
Fe1 C12 C13 C14 -59.1(4) . . . . ?
C11 C12 C13 Fe1 59.3(4) . . . . ?
C15 Fe1 C13 C12 42.5(10) . . . . ?
C16 Fe1 C13 C12 76.2(5) . . . . ?
C19 Fe1 C13 C12 -165.4(8) . . . . ?
C18 Fe1 C13 C12 160.7(4) . . . . ?
C17 Fe1 C13 C12 117.2(5) . . . . ?
C11 Fe1 C13 C12 -37.9(3) . . . . ?
C10 Fe1 C13 C12 -82.2(3) . . . . ?
C14 Fe1 C13 C12 -120.0(5) . . . . ?
C15 Fe1 C13 C14 162.5(9) . . . . ?
C16 Fe1 C13 C14 -163.8(5) . . . . ?
C19 Fe1 C13 C14 -45.4(9) . . . . ?
C18 Fe1 C13 C14 -79.3(5) . . . . ?
C17 Fe1 C13 C14 -122.8(5) . . . . ?
C11 Fe1 C13 C14 82.1(3) . . . . ?
C12 Fe1 C13 C14 120.0(5) . . . . ?
C10 Fe1 C13 C14 37.8(3) . . . . ?
C12 C13 C14 C10 0.0(6) . . . . ?
Fe1 C13 C14 C10 -59.0(3) . . . . ?
C12 C13 C14 Fe1 59.0(4) . . . . ?
C11 C10 C14 C13 -0.3(5) . . . . ?
C7 C10 C14 C13 179.0(4) . . . . ?
Fe1 C10 C14 C13 59.2(3) . . . . ?
C11 C10 C14 Fe1 -59.5(3) . . . . ?
C7 C10 C14 Fe1 119.8(4) . . . . ?
C15 Fe1 C14 C13 -164.2(9) . . . . ?
C16 Fe1 C14 C13 43.2(11) . . . . ?
C19 Fe1 C14 C13 163.1(5) . . . . ?
C18 Fe1 C14 C13 120.9(5) . . . . ?
C17 Fe1 C14 C13 77.4(5) . . . . ?
C11 Fe1 C14 C13 -81.0(4) . . . . ?
C12 Fe1 C14 C13 -37.0(3) . . . . ?
C10 Fe1 C14 C13 -119.5(5) . . . . ?
C15 Fe1 C14 C10 -44.8(10) . . . . ?
C16 Fe1 C14 C10 162.6(9) . . . . ?
C19 Fe1 C14 C10 -77.5(5) . . . . ?
C18 Fe1 C14 C10 -119.6(4) . . . . ?
C17 Fe1 C14 C10 -163.2(4) . . . . ?
C11 Fe1 C14 C10 38.5(3) . . . . ?
C12 Fe1 C14 C10 82.5(3) . . . . ?
C13 Fe1 C14 C10 119.5(5) . . . . ?
C16 Fe1 C15 C19 120.2(9) . . . . ?
C18 Fe1 C15 C19 37.6(5) . . . . ?
C17 Fe1 C15 C19 83.0(6) . . . . ?
C11 Fe1 C15 C19 -121.4(6) . . . . ?
C12 Fe1 C15 C19 -163.1(5) . . . . ?
C10 Fe1 C15 C19 -78.7(6) . . . . ?
C13 Fe1 C15 C19 165.3(8) . . . . ?
C14 Fe1 C15 C19 -45.9(12) . . . . ?
C19 Fe1 C15 C16 -120.2(9) . . . . ?
C18 Fe1 C15 C16 -82.6(7) . . . . ?
C17 Fe1 C15 C16 -37.3(6) . . . . ?
C11 Fe1 C15 C16 118.4(6) . . . . ?
C12 Fe1 C15 C16 76.6(7) . . . . ?
C10 Fe1 C15 C16 161.0(6) . . . . ?
C13 Fe1 C15 C16 45.0(13) . . . . ?
C14 Fe1 C15 C16 -166.2(7) . . . . ?
C19 C15 C16 C17 0.7(9) . . . . ?
Fe1 C15 C16 C17 60.9(6) . . . . ?
C19 C15 C16 Fe1 -60.2(5) . . . . ?
C15 Fe1 C16 C17 -118.2(9) . . . . ?
C19 Fe1 C16 C17 -82.5(6) . . . . ?
C18 Fe1 C16 C17 -38.9(6) . . . . ?
C11 Fe1 C16 C17 161.9(5) . . . . ?
C12 Fe1 C16 C17 119.6(5) . . . . ?
C10 Fe1 C16 C17 -164.1(6) . . . . ?
C13 Fe1 C16 C17 78.6(6) . . . . ?
C14 Fe1 C16 C17 46.3(12) . . . . ?
C19 Fe1 C16 C15 35.7(6) . . . . ?
C18 Fe1 C16 C15 79.3(7) . . . . ?
C17 Fe1 C16 C15 118.2(9) . . . . ?
C11 Fe1 C16 C15 -79.9(7) . . . . ?
C12 Fe1 C16 C15 -122.2(6) . . . . ?
C10 Fe1 C16 C15 -45.9(11) . . . . ?
C13 Fe1 C16 C15 -163.1(6) . . . . ?
C14 Fe1 C16 C15 164.5(8) . . . . ?
C15 C16 C17 C18 -0.6(9) . . . . ?
Fe1 C16 C17 C18 59.2(5) . . . . ?
C15 C16 C17 Fe1 -59.9(5) . . . . ?
C15 Fe1 C17 C16 38.6(6) . . . . ?
C19 Fe1 C17 C16 80.5(6) . . . . ?
C18 Fe1 C17 C16 118.5(9) . . . . ?
C11 Fe1 C17 C16 -41.7(10) . . . . ?
C12 Fe1 C17 C16 -78.0(6) . . . . ?
C10 Fe1 C17 C16 160.5(7) . . . . ?
C13 Fe1 C17 C16 -120.4(5) . . . . ?
C14 Fe1 C17 C16 -162.5(5) . . . . ?
C15 Fe1 C17 C18 -79.9(6) . . . . ?
C16 Fe1 C17 C18 -118.5(9) . . . . ?
C19 Fe1 C17 C18 -38.1(6) . . . . ?
C11 Fe1 C17 C18 -160.2(7) . . . . ?
C12 Fe1 C17 C18 163.5(6) . . . . ?
C10 Fe1 C17 C18 41.9(12) . . . . ?
C13 Fe1 C17 C18 121.1(6) . . . . ?
C14 Fe1 C17 C18 78.9(7) . . . . ?
C16 C17 C18 C19 0.4(8) . . . . ?
Fe1 C17 C18 C19 60.1(5) . . . . ?
C16 C17 C18 Fe1 -59.7(6) . . . . ?
C15 Fe1 C18 C19 -36.2(5) . . . . ?
C16 Fe1 C18 C19 -80.6(6) . . . . ?
C17 Fe1 C18 C19 -117.5(8) . . . . ?
C11 Fe1 C18 C19 39.9(12) . . . . ?
C12 Fe1 C18 C19 -160.2(8) . . . . ?
C10 Fe1 C18 C19 77.2(6) . . . . ?
C13 Fe1 C18 C19 163.0(5) . . . . ?
C14 Fe1 C18 C19 120.4(5) . . . . ?
C15 Fe1 C18 C17 81.3(6) . . . . ?
C16 Fe1 C18 C17 37.0(6) . . . . ?
C19 Fe1 C18 C17 117.5(8) . . . . ?
C11 Fe1 C18 C17 157.5(8) . . . . ?
C12 Fe1 C18 C17 -42.7(12) . . . . ?
C10 Fe1 C18 C17 -165.3(5) . . . . ?
C13 Fe1 C18 C17 -79.5(7) . . . . ?
C14 Fe1 C18 C17 -122.1(6) . . . . ?
C16 C15 C19 C18 -0.4(9) . . . . ?
Fe1 C15 C19 C18 -59.9(5) . . . . ?
C16 C15 C19 Fe1 59.5(5) . . . . ?
C17 C18 C19 C15 0.0(8) . . . . ?
Fe1 C18 C19 C15 60.0(5) . . . . ?
C17 C18 C19 Fe1 -60.0(5) . . . . ?
C16 Fe1 C19 C15 -37.7(6) . . . . ?
C18 Fe1 C19 C15 -119.7(8) . . . . ?
C17 Fe1 C19 C15 -80.3(6) . . . . ?
C11 Fe1 C19 C15 75.9(6) . . . . ?
C12 Fe1 C19 C15 41.1(10) . . . . ?
C10 Fe1 C19 C15 118.7(6) . . . . ?
C13 Fe1 C19 C15 -165.1(7) . . . . ?
C14 Fe1 C19 C15 160.9(5) . . . . ?
C15 Fe1 C19 C18 119.7(8) . . . . ?
C16 Fe1 C19 C18 81.9(6) . . . . ?
C17 Fe1 C19 C18 39.3(6) . . . . ?
C11 Fe1 C19 C18 -164.4(4) . . . . ?
C12 Fe1 C19 C18 160.8(6) . . . . ?
C10 Fe1 C19 C18 -121.7(5) . . . . ?
C13 Fe1 C19 C18 -45.5(10) . . . . ?
C14 Fe1 C19 C18 -79.5(5) . . . . ?
C6 C9 C20 C21 -165.2(4) . . . . ?
C8 C9 C20 C21 27.8(8) . . . . ?
Co1 C9 C20 C21 -70.3(6) . . . . ?
C6 C9 C20 C24 15.0(7) . . . . ?
C8 C9 C20 C24 -152.0(5) . . . . ?
Co1 C9 C20 C24 109.8(4) . . . . ?
C6 C9 C20 Fe2 103.5(5) . . . . ?
C8 C9 C20 Fe2 -63.5(6) . . . . ?
Co1 C9 C20 Fe2 -161.7(2) . . . . ?
C23 Fe2 C20 C21 81.0(3) . . . . ?
C24 Fe2 C20 C21 118.7(4) . . . . ?
C28 Fe2 C20 C21 164.3(6) . . . . ?
C26 Fe2 C20 C21 -80.5(4) . . . . ?
C27 Fe2 C20 C21 -48.4(10) . . . . ?
C29 Fe2 C20 C21 -163.5(3) . . . . ?
C25 Fe2 C20 C21 -121.5(3) . . . . ?
C22 Fe2 C20 C21 37.9(3) . . . . ?
C23 Fe2 C20 C24 -37.7(3) . . . . ?
C28 Fe2 C20 C24 45.6(7) . . . . ?
C26 Fe2 C20 C24 160.8(4) . . . . ?
C27 Fe2 C20 C24 -167.1(9) . . . . ?
C21 Fe2 C20 C24 -118.7(4) . . . . ?
C29 Fe2 C20 C24 77.8(4) . . . . ?
C25 Fe2 C20 C24 119.8(3) . . . . ?
C22 Fe2 C20 C24 -80.8(3) . . . . ?
C23 Fe2 C20 C9 -156.4(4) . . . . ?
C24 Fe2 C20 C9 -118.7(5) . . . . ?
C28 Fe2 C20 C9 -73.1(8) . . . . ?
C26 Fe2 C20 C9 42.1(5) . . . . ?
C27 Fe2 C20 C9 74.2(10) . . . . ?
C21 Fe2 C20 C9 122.6(5) . . . . ?
C29 Fe2 C20 C9 -40.9(5) . . . . ?
C25 Fe2 C20 C9 1.1(5) . . . . ?
C22 Fe2 C20 C9 160.5(4) . . . . ?
C24 C20 C21 C22 -0.1(5) . . . . ?
C9 C20 C21 C22 -179.9(4) . . . . ?
Fe2 C20 C21 C22 -59.3(3) . . . . ?
C24 C20 C21 Fe2 59.2(3) . . . . ?
C9 C20 C21 Fe2 -120.7(4) . . . . ?
C23 Fe2 C21 C20 -82.4(3) . . . . ?
C24 Fe2 C21 C20 -38.3(2) . . . . ?
C28 Fe2 C21 C20 -161.3(9) . . . . ?
C26 Fe2 C21 C20 120.0(3) . . . . ?
C27 Fe2 C21 C20 163.2(4) . . . . ?
C29 Fe2 C21 C20 41.0(8) . . . . ?
C25 Fe2 C21 C20 77.8(4) . . . . ?
C22 Fe2 C21 C20 -119.3(4) . . . . ?
C23 Fe2 C21 C22 37.0(3) . . . . ?
C24 Fe2 C21 C22 81.0(3) . . . . ?
C28 Fe2 C21 C22 -42.0(10) . . . . ?
C26 Fe2 C21 C22 -120.7(4) . . . . ?
C20 Fe2 C21 C22 119.3(4) . . . . ?
C27 Fe2 C21 C22 -77.5(4) . . . . ?
C29 Fe2 C21 C22 160.3(7) . . . . ?
C25 Fe2 C21 C22 -162.9(3) . . . . ?
C20 C21 C22 C23 0.4(5) . . . . ?
Fe2 C21 C22 C23 -58.8(3) . . . . ?
C20 C21 C22 Fe2 59.2(3) . . . . ?
C24 Fe2 C22 C23 37.6(3) . . . . ?
C28 Fe2 C22 C23 -75.7(5) . . . . ?
C26 Fe2 C22 C23 -160.2(4) . . . . ?
C20 Fe2 C22 C23 82.1(3) . . . . ?
C27 Fe2 C22 C23 -117.3(4) . . . . ?
C21 Fe2 C22 C23 119.7(4) . . . . ?
C29 Fe2 C22 C23 -40.8(8) . . . . ?
C25 Fe2 C22 C23 166.4(7) . . . . ?
C23 Fe2 C22 C21 -119.7(4) . . . . ?
C24 Fe2 C22 C21 -82.1(3) . . . . ?
C28 Fe2 C22 C21 164.6(4) . . . . ?
C26 Fe2 C22 C21 80.1(4) . . . . ?
C20 Fe2 C22 C21 -37.7(3) . . . . ?
C27 Fe2 C22 C21 123.0(4) . . . . ?
C29 Fe2 C22 C21 -160.5(7) . . . . ?
C25 Fe2 C22 C21 46.7(8) . . . . ?
C21 C22 C23 C24 -0.5(6) . . . . ?
Fe2 C22 C23 C24 -59.2(3) . . . . ?
C21 C22 C23 Fe2 58.7(3) . . . . ?
C24 Fe2 C23 C22 -119.8(4) . . . . ?
C28 Fe2 C23 C22 122.3(4) . . . . ?
C26 Fe2 C23 C22 51.1(8) . . . . ?
C20 Fe2 C23 C22 -81.8(3) . . . . ?
C27 Fe2 C23 C22 81.6(5) . . . . ?
C21 Fe2 C23 C22 -37.8(3) . . . . ?
C29 Fe2 C23 C22 163.4(4) . . . . ?
C25 Fe2 C23 C22 -167.5(6) . . . . ?
C28 Fe2 C23 C24 -117.9(4) . . . . ?
C26 Fe2 C23 C24 170.9(7) . . . . ?
C20 Fe2 C23 C24 38.0(3) . . . . ?
C27 Fe2 C23 C24 -158.6(5) . . . . ?
C21 Fe2 C23 C24 82.0(3) . . . . ?
C29 Fe2 C23 C24 -76.8(4) . . . . ?
C25 Fe2 C23 C24 -47.6(7) . . . . ?
C22 Fe2 C23 C24 119.8(4) . . . . ?
C22 C23 C24 C20 0.5(5) . . . . ?
Fe2 C23 C24 C20 -59.2(3) . . . . ?
C22 C23 C24 Fe2 59.7(3) . . . . ?
C21 C20 C24 C23 -0.3(5) . . . . ?
C9 C20 C24 C23 179.6(4) . . . . ?
Fe2 C20 C24 C23 59.2(3) . . . . ?
C21 C20 C24 Fe2 -59.5(3) . . . . ?
C9 C20 C24 Fe2 120.4(4) . . . . ?
C28 Fe2 C24 C23 79.8(4) . . . . ?
C26 Fe2 C24 C23 -170.7(8) . . . . ?
C20 Fe2 C24 C23 -119.2(4) . . . . ?
C27 Fe2 C24 C23 50.7(9) . . . . ?
C21 Fe2 C24 C23 -81.3(3) . . . . ?
C29 Fe2 C24 C23 120.9(3) . . . . ?
C25 Fe2 C24 C23 161.3(3) . . . . ?
C22 Fe2 C24 C23 -37.0(3) . . . . ?
C23 Fe2 C24 C20 119.2(4) . . . . ?
C28 Fe2 C24 C20 -160.9(4) . . . . ?
C26 Fe2 C24 C20 -51.4(9) . . . . ?
C27 Fe2 C24 C20 170.0(8) . . . . ?
C21 Fe2 C24 C20 38.0(2) . . . . ?
C29 Fe2 C24 C20 -119.9(3) . . . . ?
C25 Fe2 C24 C20 -79.5(3) . . . . ?
C22 Fe2 C24 C20 82.3(3) . . . . ?
C23 Fe2 C25 C26 -159.6(6) . . . . ?
C24 Fe2 C25 C26 165.2(4) . . . . ?
C28 Fe2 C25 C26 -82.0(5) . . . . ?
C20 Fe2 C25 C26 122.3(4) . . . . ?
C27 Fe2 C25 C26 -38.8(5) . . . . ?
C21 Fe2 C25 C26 80.1(5) . . . . ?
C29 Fe2 C25 C26 -119.9(6) . . . . ?
C22 Fe2 C25 C26 44.9(9) . . . . ?
C23 Fe2 C25 C29 -39.7(8) . . . . ?
C24 Fe2 C25 C29 -74.9(5) . . . . ?
C28 Fe2 C25 C29 38.0(5) . . . . ?
C26 Fe2 C25 C29 119.9(6) . . . . ?
C20 Fe2 C25 C29 -117.8(4) . . . . ?
C27 Fe2 C25 C29 81.1(6) . . . . ?
C21 Fe2 C25 C29 -160.0(4) . . . . ?
C22 Fe2 C25 C29 164.8(6) . . . . ?
C29 C25 C26 C27 0.9(7) . . . . ?
Fe2 C25 C26 C27 60.0(4) . . . . ?
C29 C25 C26 Fe2 -59.1(4) . . . . ?
C23 Fe2 C26 C25 159.2(6) . . . . ?
C24 Fe2 C26 C25 -38.0(10) . . . . ?
C28 Fe2 C26 C25 80.8(5) . . . . ?
C20 Fe2 C26 C25 -76.5(5) . . . . ?
C27 Fe2 C26 C25 118.1(8) . . . . ?
C21 Fe2 C26 C25 -119.8(4) . . . . ?
C29 Fe2 C26 C25 37.2(4) . . . . ?
C22 Fe2 C26 C25 -163.2(4) . . . . ?
C23 Fe2 C26 C27 41.1(11) . . . . ?
C24 Fe2 C26 C27 -156.2(8) . . . . ?
C28 Fe2 C26 C27 -37.3(6) . . . . ?
C20 Fe2 C26 C27 165.3(6) . . . . ?
C21 Fe2 C26 C27 122.1(6) . . . . ?
C29 Fe2 C26 C27 -80.9(6) . . . . ?
C25 Fe2 C26 C27 -118.1(8) . . . . ?
C22 Fe2 C26 C27 78.6(7) . . . . ?
C25 C26 C27 C28 -0.7(8) . . . . ?
Fe2 C26 C27 C28 59.8(5) . . . . ?
C25 C26 C27 Fe2 -60.5(4) . . . . ?
C23 Fe2 C27 C28 77.4(6) . . . . ?
C24 Fe2 C27 C28 40.9(11) . . . . ?
C26 Fe2 C27 C28 -118.6(8) . . . . ?
C20 Fe2 C27 C28 -160.6(8) . . . . ?
C21 Fe2 C27 C28 162.4(4) . . . . ?
C29 Fe2 C27 C28 -37.3(5) . . . . ?
C25 Fe2 C27 C28 -80.9(5) . . . . ?
C22 Fe2 C27 C28 119.8(5) . . . . ?
C23 Fe2 C27 C26 -164.0(5) . . . . ?
C24 Fe2 C27 C26 159.5(6) . . . . ?
C28 Fe2 C27 C26 118.6(8) . . . . ?
C20 Fe2 C27 C26 -42.0(13) . . . . ?
C21 Fe2 C27 C26 -79.0(6) . . . . ?
C29 Fe2 C27 C26 81.3(6) . . . . ?
C25 Fe2 C27 C26 37.7(5) . . . . ?
C22 Fe2 C27 C26 -121.6(5) . . . . ?
C26 C27 C28 C29 0.3(8) . . . . ?
Fe2 C27 C28 C29 59.7(5) . . . . ?
C26 C27 C28 Fe2 -59.4(5) . . . . ?
C23 Fe2 C28 C27 -120.0(5) . . . . ?
C24 Fe2 C28 C27 -162.2(4) . . . . ?
C26 Fe2 C28 C27 38.6(5) . . . . ?
C20 Fe2 C28 C27 164.6(5) . . . . ?
C21 Fe2 C28 C27 -47.6(11) . . . . ?
C29 Fe2 C28 C27 119.9(7) . . . . ?
C25 Fe2 C28 C27 81.9(5) . . . . ?
C22 Fe2 C28 C27 -79.3(6) . . . . ?
C23 Fe2 C28 C29 120.2(5) . . . . ?
C24 Fe2 C28 C29 77.9(5) . . . . ?
C26 Fe2 C28 C29 -81.3(5) . . . . ?
C20 Fe2 C28 C29 44.7(9) . . . . ?
C27 Fe2 C28 C29 -119.9(7) . . . . ?
C21 Fe2 C28 C29 -167.5(7) . . . . ?
C25 Fe2 C28 C29 -38.0(5) . . . . ?
C22 Fe2 C28 C29 160.8(4) . . . . ?
C27 C28 C29 C25 0.3(8) . . . . ?
Fe2 C28 C29 C25 60.1(4) . . . . ?
C27 C28 C29 Fe2 -59.8(5) . . . . ?
C26 C25 C29 C28 -0.7(7) . . . . ?
Fe2 C25 C29 C28 -59.8(4) . . . . ?
C26 C25 C29 Fe2 59.1(4) . . . . ?
C23 Fe2 C29 C28 -77.6(6) . . . . ?
C24 Fe2 C29 C28 -119.0(5) . . . . ?
C26 Fe2 C29 C28 81.5(6) . . . . ?
C20 Fe2 C29 C28 -161.1(5) . . . . ?
C27 Fe2 C29 C28 36.9(5) . . . . ?
C21 Fe2 C29 C28 168.7(7) . . . . ?
C25 Fe2 C29 C28 118.4(7) . . . . ?
C22 Fe2 C29 C28 -47.9(10) . . . . ?
C23 Fe2 C29 C25 164.0(4) . . . . ?
C24 Fe2 C29 C25 122.6(4) . . . . ?
C28 Fe2 C29 C25 -118.4(7) . . . . ?
C26 Fe2 C29 C25 -36.9(4) . . . . ?
C20 Fe2 C29 C25 80.5(5) . . . . ?
C27 Fe2 C29 C25 -81.5(5) . . . . ?
C21 Fe2 C29 C25 50.3(9) . . . . ?
C22 Fe2 C29 C25 -166.3(6) . . . . ?
