#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:24:00 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179244 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/64/4316499.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4316499
loop_
_publ_author_name
'Daniel E. Bugaris'
'Daniel M. Wells'
'Jiyong Yao'
'S. Skanthakumar'
'Richard G. Haire'
'L. Soderholm'
'James A. Ibers'
_publ_contact_author_address
;
Department of Chemistry
Northwestern University
Evanston, IL 60208-3113
;
_publ_contact_author_email       ibers@chem.northwestern.edu
_publ_contact_author_fax         '1 847 491 3976'
_publ_contact_author_name        'James A. Ibers'
_publ_contact_author_phone       '1 847 491 5449'
_publ_section_title
;
 Dichalcogenide Bonding in Seven Alkali-Metal Actinide Chalcogenides of
 the KTh2Se6 Structure Type
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8381
_journal_page_last               8388
_journal_paper_doi               10.1021/ic1008895
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         '2(Se3 U), (Rb)'
_chemical_formula_sum            'Rb Se6 U2'
_chemical_formula_weight         1035.29
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.066(3)
_cell_length_b                   5.552(5)
_cell_length_c                   22.444(18)
_cell_measurement_reflns_used    2578
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      28.50
_cell_measurement_theta_min      3.63
_cell_volume                     506.7(7)
_computing_cell_refinement       'APEX2 version 2009.5-1 (Bruker, 2009)'
_computing_data_collection       'SMART version 5.054 (Bruker, 2000)'
_computing_data_reduction        'SAINT version 7.34a (Bruker, 2009)'
_computing_molecular_graphics    'CrystalMaker version 2.2.1 (Palmer, 2009)'
_computing_publication_material  'SHELXTL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      153(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.944
_diffrn_measurement_device_type  'Bruker SMART 1000 CCD'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0458
_diffrn_reflns_av_sigmaI/netI    0.0266
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            2888
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         28.50
_diffrn_reflns_theta_min         3.63
_exptl_absorpt_coefficient_mu    58.172
_exptl_absorpt_correction_T_max  0.0718
_exptl_absorpt_correction_T_min  0.0036
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
;
'face indexed; SADABS version 2008/1 (Sheldrick, 2008)' 
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    6.786
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             850
_exptl_crystal_size_max          0.994
_exptl_crystal_size_mid          0.110
_exptl_crystal_size_min          0.064
_refine_diff_density_max         5.022
_refine_diff_density_min         -2.682
_refine_diff_density_rms         0.526
_refine_ls_extinction_coef       0.0013(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.593
_refine_ls_matrix_type           full
_refine_ls_number_parameters     23
_refine_ls_number_reflns         391
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.593
_refine_ls_R_factor_all          0.0298
_refine_ls_R_factor_gt           0.0292
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
; calc 
 [1.00000+0.00000exp(0.00(sinθ/λ)²)]/ 
   [σ²(Fo²)+0.0000+0.0000*P+(0.0400P)²+0.0000sinθ/λ] 
 where P = 1.00000Fo² + 0.00000Fc² 
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0812
_refine_ls_wR_factor_ref         0.0813
_reflns_number_gt                384
_reflns_number_total             391
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic1008895_si_001_4.cif
_cod_data_source_block           RbUSe
_cod_original_cell_volume        506.6(7)
_cod_database_code               4316499
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.0000 0.0000 0.181247(18) 0.0074(3) Uani 1 4 d S . .
Se1 Se 0.5000 0.0000 0.27280(5) 0.0062(3) Uani 1 4 d S . .
Se2 Se 0.0000 0.25699(18) 0.39076(4) 0.0140(3) Uani 1 2 d S . .
Rb1 Rb 0.5000 0.0000 0.5000 0.0191(7) Uani 0.865(7) 8 d SP . .
Rb2 Rb 0.0000 0.0000 0.0000 0.025(4) Uani 0.135(7) 8 d SP . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Se1 U1 Se1 89.38(7) . 1_455 ?
Se1 U1 Se2 151.78(3) . 14_445 ?
Se1 U1 Se2 84.50(6) 1_455 14_445 ?
Se1 U1 Se2 151.78(3) . 13_455 ?
Se1 U1 Se2 84.50(6) 1_455 13_455 ?
Se2 U1 Se2 54.90(6) 14_445 13_455 ?
Se1 U1 Se2 84.49(6) . 13 ?
Se1 U1 Se2 151.78(3) 1_455 13 ?
Se2 U1 Se2 112.96(6) 14_445 13 ?
Se2 U1 Se2 87.99(6) 13_455 13 ?
Se1 U1 Se2 84.49(6) . 14_545 ?
Se1 U1 Se2 151.78(3) 1_455 14_545 ?
Se2 U1 Se2 87.99(6) 14_445 14_545 ?
Se2 U1 Se2 112.96(7) 13_455 14_545 ?
Se2 U1 Se2 54.90(6) 13 14_545 ?
Se1 U1 Se1 75.67(2) . 13 ?
Se1 U1 Se1 75.67(2) 1_455 13 ?
Se2 U1 Se1 128.64(3) 14_445 13 ?
Se2 U1 Se1 76.12(4) 13_455 13 ?
Se2 U1 Se1 76.12(4) 13 13 ?
Se2 U1 Se1 128.64(3) 14_545 13 ?
Se1 U1 Se1 75.67(2) . 13_545 ?
Se1 U1 Se1 75.67(2) 1_455 13_545 ?
Se2 U1 Se1 76.12(4) 14_445 13_545 ?
Se2 U1 Se1 128.64(3) 13_455 13_545 ?
Se2 U1 Se1 128.64(3) 13 13_545 ?
Se2 U1 Se1 76.12(4) 14_545 13_545 ?
Se1 U1 Se1 139.24(6) 13 13_545 ?
Se1 U1 U1 45.31(4) . 1_655 ?
Se1 U1 U1 134.69(4) 1_455 1_655 ?
Se2 U1 U1 134.00(3) 14_445 1_655 ?
Se2 U1 U1 134.00(3) 13_455 1_655 ?
Se2 U1 U1 46.00(3) 13 1_655 ?
Se2 U1 U1 46.00(3) 14_545 1_655 ?
Se1 U1 U1 90.0 13 1_655 ?
Se1 U1 U1 90.0 13_545 1_655 ?
Se1 U1 U1 134.69(4) . 1_455 ?
Se1 U1 U1 45.31(4) 1_455 1_455 ?
Se2 U1 U1 46.00(3) 14_445 1_455 ?
Se2 U1 U1 46.00(3) 13_455 1_455 ?
Se2 U1 U1 134.00(3) 13 1_455 ?
Se2 U1 U1 134.00(3) 14_545 1_455 ?
Se1 U1 U1 90.0 13 1_455 ?
Se1 U1 U1 90.0 13_545 1_455 ?
U1 U1 U1 180.0 1_655 1_455 ?
Se1 U1 Rb2 135.31(4) . . ?
Se1 U1 Rb2 135.31(4) 1_455 . ?
Se2 U1 Rb2 56.48(3) 14_445 . ?
Se2 U1 Rb2 56.48(3) 13_455 . ?
Se2 U1 Rb2 56.48(3) 13 . ?
Se2 U1 Rb2 56.48(3) 14_545 . ?
Se1 U1 Rb2 110.38(3) 13 . ?
Se1 U1 Rb2 110.38(3) 13_545 . ?
U1 U1 Rb2 90.0 1_655 . ?
U1 U1 Rb2 90.0 1_455 . ?
U1 Se1 U1 89.38(7) . 1_655 ?
U1 Se1 U1 104.34(2) . 13 ?
U1 Se1 U1 104.34(2) 1_655 13 ?
U1 Se1 U1 104.34(2) . 13_545 ?
U1 Se1 U1 104.34(2) 1_655 13_545 ?
U1 Se1 U1 139.23(6) 13 13_545 ?
Se2 Se2 U1 62.55(3) 2_565 13_455 ?
Se2 Se2 U1 62.55(3) 2_565 13 ?
U1 Se2 U1 88.00(6) 13_455 13 ?
Se2 Se2 Rb2 67.04(3) 2_565 5 ?
U1 Se2 Rb2 128.31(5) 13_455 5 ?
U1 Se2 Rb2 78.66(6) 13 5 ?
Se2 Se2 Rb2 67.04(3) 2_565 5_455 ?
U1 Se2 Rb2 78.66(6) 13_455 5_455 ?
U1 Se2 Rb2 128.31(5) 13 5_455 ?
Rb2 Se2 Rb2 71.99(6) 5 5_455 ?
Se2 Se2 Rb1 114.13(3) 2_565 . ?
U1 Se2 Rb1 168.83(3) 13_455 . ?
U1 Se2 Rb1 99.89(6) 13 . ?
Rb2 Se2 Rb1 47.09(4) 5 . ?
Rb2 Se2 Rb1 90.22(6) 5_455 . ?
Se2 Se2 Rb1 114.13(3) 2_565 1_455 ?
U1 Se2 Rb1 99.89(6) 13_455 1_455 ?
U1 Se2 Rb1 168.83(3) 13 1_455 ?
Rb2 Se2 Rb1 90.22(6) 5 1_455 ?
Rb2 Se2 Rb1 47.09(4) 5_455 1_455 ?
Rb1 Se2 Rb1 71.25(6) . 1_455 ?
Rb2 Rb1 Rb2 180.0 5 5_545 ?
Rb2 Rb1 Se2 65.87(3) 5 . ?
Rb2 Rb1 Se2 114.13(3) 5_545 . ?
Rb2 Rb1 Se2 65.87(3) 5 10_656 ?
Rb2 Rb1 Se2 114.13(3) 5_545 10_656 ?
Se2 Rb1 Se2 131.74(5) . 10_656 ?
Rb2 Rb1 Se2 114.13(3) 5 2 ?
Rb2 Rb1 Se2 65.87(3) 5_545 2 ?
Se2 Rb1 Se2 48.26(5) . 2 ?
Se2 Rb1 Se2 180.0 10_656 2 ?
Rb2 Rb1 Se2 114.13(3) 5 9_656 ?
Rb2 Rb1 Se2 65.87(3) 5_545 9_656 ?
Se2 Rb1 Se2 180.00(2) . 9_656 ?
Se2 Rb1 Se2 48.26(5) 10_656 9_656 ?
Se2 Rb1 Se2 131.74(5) 2 9_656 ?
Rb2 Rb1 Se2 114.13(3) 5 2_655 ?
Rb2 Rb1 Se2 65.87(3) 5_545 2_655 ?
Se2 Rb1 Se2 90.74(6) . 2_655 ?
Se2 Rb1 Se2 108.75(6) 10_656 2_655 ?
Se2 Rb1 Se2 71.25(6) 2 2_655 ?
Se2 Rb1 Se2 89.26(6) 9_656 2_655 ?
Rb2 Rb1 Se2 65.87(3) 5 10_556 ?
Rb2 Rb1 Se2 114.13(3) 5_545 10_556 ?
Se2 Rb1 Se2 89.26(6) . 10_556 ?
Se2 Rb1 Se2 71.25(6) 10_656 10_556 ?
Se2 Rb1 Se2 108.75(6) 2 10_556 ?
Se2 Rb1 Se2 90.74(6) 9_656 10_556 ?
Se2 Rb1 Se2 180.00(2) 2_655 10_556 ?
Rb2 Rb1 Se2 114.13(3) 5 9_556 ?
Rb2 Rb1 Se2 65.87(3) 5_545 9_556 ?
Se2 Rb1 Se2 108.75(6) . 9_556 ?
Se2 Rb1 Se2 90.74(6) 10_656 9_556 ?
Se2 Rb1 Se2 89.26(6) 2 9_556 ?
Se2 Rb1 Se2 71.25(6) 9_656 9_556 ?
Se2 Rb1 Se2 131.74(5) 2_655 9_556 ?
Se2 Rb1 Se2 48.26(5) 10_556 9_556 ?
Rb2 Rb1 Se2 65.87(3) 5 1_655 ?
Rb2 Rb1 Se2 114.13(3) 5_545 1_655 ?
Se2 Rb1 Se2 71.25(6) . 1_655 ?
Se2 Rb1 Se2 89.26(6) 10_656 1_655 ?
Se2 Rb1 Se2 90.74(6) 2 1_655 ?
Se2 Rb1 Se2 108.75(6) 9_656 1_655 ?
Se2 Rb1 Se2 48.26(5) 2_655 1_655 ?
Se2 Rb1 Se2 131.74(5) 10_556 1_655 ?
Se2 Rb1 Se2 180.0 9_556 1_655 ?
Rb2 Rb1 Rb1 90.0 5 1_455 ?
Rb2 Rb1 Rb1 90.0 5_545 1_455 ?
Se2 Rb1 Rb1 54.37(3) . 1_455 ?
Se2 Rb1 Rb1 125.63(3) 10_656 1_455 ?
Se2 Rb1 Rb1 54.37(3) 2 1_455 ?
Se2 Rb1 Rb1 125.63(3) 9_656 1_455 ?
Se2 Rb1 Rb1 125.63(3) 2_655 1_455 ?
Se2 Rb1 Rb1 54.37(3) 10_556 1_455 ?
Se2 Rb1 Rb1 54.37(3) 9_556 1_455 ?
Se2 Rb1 Rb1 125.63(3) 1_655 1_455 ?
Rb2 Rb1 Rb1 90.0 5 1_655 ?
Rb2 Rb1 Rb1 90.0 5_545 1_655 ?
Se2 Rb1 Rb1 125.63(3) . 1_655 ?
Se2 Rb1 Rb1 54.37(3) 10_656 1_655 ?
Se2 Rb1 Rb1 125.63(3) 2 1_655 ?
Se2 Rb1 Rb1 54.37(3) 9_656 1_655 ?
Se2 Rb1 Rb1 54.37(3) 2_655 1_655 ?
Se2 Rb1 Rb1 125.63(3) 10_556 1_655 ?
Se2 Rb1 Rb1 125.63(3) 9_556 1_655 ?
Se2 Rb1 Rb1 54.37(3) 1_655 1_655 ?
Rb1 Rb1 Rb1 180.0 1_455 1_655 ?
Rb1 Rb2 Rb1 180.0 5_454 5_444 ?
Rb1 Rb2 Se2 67.04(3) 5_454 13 ?
Rb1 Rb2 Se2 112.96(3) 5_444 13 ?
Rb1 Rb2 Se2 112.96(3) 5_454 5_444 ?
Rb1 Rb2 Se2 67.04(3) 5_444 5_444 ?
Se2 Rb2 Se2 180.00(2) 13 5_444 ?
Rb1 Rb2 Se2 112.96(3) 5_454 14_545 ?
Rb1 Rb2 Se2 67.04(3) 5_444 14_545 ?
Se2 Rb2 Se2 45.92(5) 13 14_545 ?
Se2 Rb2 Se2 134.08(5) 5_444 14_545 ?
Rb1 Rb2 Se2 67.04(3) 5_454 6_454 ?
Rb1 Rb2 Se2 112.96(3) 5_444 6_454 ?
Se2 Rb2 Se2 134.08(5) 13 6_454 ?
Se2 Rb2 Se2 45.92(5) 5_444 6_454 ?
Se2 Rb2 Se2 180.00(2) 14_545 6_454 ?
Rb1 Rb2 Se2 67.04(3) 5_454 13_455 ?
Rb1 Rb2 Se2 112.96(3) 5_444 13_455 ?
Se2 Rb2 Se2 71.99(6) 13 13_455 ?
Se2 Rb2 Se2 108.01(6) 5_444 13_455 ?
Se2 Rb2 Se2 89.72(6) 14_545 13_455 ?
Se2 Rb2 Se2 90.28(6) 6_454 13_455 ?
Rb1 Rb2 Se2 112.96(3) 5_454 5_544 ?
Rb1 Rb2 Se2 67.04(3) 5_444 5_544 ?
Se2 Rb2 Se2 108.01(6) 13 5_544 ?
Se2 Rb2 Se2 71.99(6) 5_444 5_544 ?
Se2 Rb2 Se2 90.28(6) 14_545 5_544 ?
Se2 Rb2 Se2 89.72(6) 6_454 5_544 ?
Se2 Rb2 Se2 180.00(2) 13_455 5_544 ?
Rb1 Rb2 Se2 67.04(3) 5_454 6_554 ?
Rb1 Rb2 Se2 112.96(3) 5_444 6_554 ?
Se2 Rb2 Se2 90.28(6) 13 6_554 ?
Se2 Rb2 Se2 89.72(6) 5_444 6_554 ?
Se2 Rb2 Se2 108.01(6) 14_545 6_554 ?
Se2 Rb2 Se2 71.99(6) 6_454 6_554 ?
Se2 Rb2 Se2 134.08(5) 13_455 6_554 ?
Se2 Rb2 Se2 45.92(5) 5_544 6_554 ?
Rb1 Rb2 Se2 112.96(3) 5_454 14_445 ?
Rb1 Rb2 Se2 67.04(3) 5_444 14_445 ?
Se2 Rb2 Se2 89.72(6) 13 14_445 ?
Se2 Rb2 Se2 90.28(6) 5_444 14_445 ?
Se2 Rb2 Se2 71.99(6) 14_545 14_445 ?
Se2 Rb2 Se2 108.01(6) 6_454 14_445 ?
Se2 Rb2 Se2 45.92(5) 13_455 14_445 ?
Se2 Rb2 Se2 134.08(5) 5_544 14_445 ?
Se2 Rb2 Se2 180.00(4) 6_554 14_445 ?
Rb1 Rb2 Rb2 90.0 5_454 1_655 ?
Rb1 Rb2 Rb2 90.0 5_444 1_655 ?
Se2 Rb2 Rb2 54.00(3) 13 1_655 ?
Se2 Rb2 Rb2 126.00(3) 5_444 1_655 ?
Se2 Rb2 Rb2 54.00(3) 14_545 1_655 ?
Se2 Rb2 Rb2 126.00(3) 6_454 1_655 ?
Se2 Rb2 Rb2 126.00(3) 13_455 1_655 ?
Se2 Rb2 Rb2 54.00(3) 5_544 1_655 ?
Se2 Rb2 Rb2 54.00(3) 6_554 1_655 ?
Se2 Rb2 Rb2 126.00(3) 14_445 1_655 ?
Rb1 Rb2 Rb2 90.0 5_454 1_455 ?
Rb1 Rb2 Rb2 90.0 5_444 1_455 ?
Se2 Rb2 Rb2 126.00(3) 13 1_455 ?
Se2 Rb2 Rb2 54.00(3) 5_444 1_455 ?
Se2 Rb2 Rb2 126.00(3) 14_545 1_455 ?
Se2 Rb2 Rb2 54.00(3) 6_454 1_455 ?
Se2 Rb2 Rb2 54.00(3) 13_455 1_455 ?
Se2 Rb2 Rb2 126.00(3) 5_544 1_455 ?
Se2 Rb2 Rb2 126.00(3) 6_554 1_455 ?
Se2 Rb2 Rb2 54.00(3) 14_445 1_455 ?
Rb2 Rb2 Rb2 180.0 1_655 1_455 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 Se1 2.8905(19) . ?
U1 Se1 2.8906(19) 1_455 ?
U1 Se2 2.9266(16) 14_445 ?
U1 Se2 2.9266(16) 13_455 ?
U1 Se2 2.9266(16) 13 ?
U1 Se2 2.9266(16) 14_545 ?
U1 Se1 2.961(2) 13 ?
U1 Se1 2.961(2) 13_545 ?
U1 U1 4.066(3) 1_655 ?
U1 U1 4.066(3) 1_455 ?
U1 Rb2 4.068(3) . ?
Se1 U1 2.8906(19) 1_655 ?
Se1 U1 2.961(2) 13 ?
Se1 U1 2.961(2) 13_545 ?
Se2 Se2 2.698(3) 2_565 ?
Se2 U1 2.9266(16) 13_455 ?
Se2 U1 2.9266(16) 13 ?
Se2 Rb2 3.4589(19) 5 ?
Se2 Rb2 3.4589(19) 5_455 ?
Se2 Rb1 3.4899(19) . ?
Se2 Rb1 3.4899(19) 1_455 ?
Rb1 Rb2 2.776(2) 5 ?
Rb1 Rb2 2.776(2) 5_545 ?
Rb1 Se2 3.4899(19) 10_656 ?
Rb1 Se2 3.4899(19) 2 ?
Rb1 Se2 3.4899(19) 9_656 ?
Rb1 Se2 3.4899(19) 2_655 ?
Rb1 Se2 3.4899(19) 10_556 ?
Rb1 Se2 3.4899(19) 9_556 ?
Rb1 Se2 3.4899(19) 1_655 ?
Rb1 Rb1 4.066(3) 1_455 ?
Rb1 Rb1 4.066(3) 1_655 ?
Rb2 Rb1 2.776(2) 5_454 ?
Rb2 Rb1 2.776(2) 5_444 ?
Rb2 Se2 3.4589(19) 13 ?
Rb2 Se2 3.4589(19) 5_444 ?
Rb2 Se2 3.4589(19) 14_545 ?
Rb2 Se2 3.4589(19) 6_454 ?
Rb2 Se2 3.4589(19) 13_455 ?
Rb2 Se2 3.4589(19) 5_544 ?
Rb2 Se2 3.4589(19) 6_554 ?
Rb2 Se2 3.4589(19) 14_445 ?
Rb2 Rb2 4.066(3) 1_655 ?
Rb2 Rb2 4.066(3) 1_455 ?
