#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:28:27 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179247 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/67/4316747.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4316747
loop_
_publ_author_name
'Svetlana V. Eliseeva'
'Dmitry N. Pleshkov'
'Konstantin A. Lyssenko'
'Leonid S. Lepnev'
'Jean-Claude G. Bünzli'
'Natalia P. Kuzmina'
_publ_section_title
;
 Highly Luminescent and Triboluminescent Coordination Polymers Assembled
 from Lanthanide β-Diketonates and Aromatic Bidentate O-Donor Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9300
_journal_page_last               9311
_journal_paper_doi               10.1021/ic100974e
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C25 H13 Eu F18 O8'
_chemical_formula_sum            'C25 H13 Eu F18 O8'
_chemical_formula_weight         935.31
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.6420(10)
_cell_angle_beta                 103.6320(10)
_cell_angle_gamma                103.6060(10)
_cell_formula_units_Z            2
_cell_length_a                   8.7081(3)
_cell_length_b                   11.9363(5)
_cell_length_c                   16.0984(6)
_cell_measurement_reflns_used    983
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      29
_cell_measurement_theta_min      3
_cell_volume                     1571.37(10)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX II'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX II CCD area detector''
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0211
_diffrn_reflns_av_sigmaI/netI    0.0276
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            19180
_diffrn_reflns_theta_full        29.00
_diffrn_reflns_theta_max         29.00
_diffrn_reflns_theta_min         1.31
_exptl_absorpt_coefficient_mu    2.149
_exptl_absorpt_correction_T_max  0.673
_exptl_absorpt_correction_T_min  0.480
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorles
_exptl_crystal_density_diffrn    1.977
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             904
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.991
_refine_diff_density_min         -1.094
_refine_diff_density_rms         0.090
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     470
_refine_ls_number_reflns         8338
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0250
_refine_ls_R_factor_gt           0.0228
_refine_ls_shift/su_max          0.048
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0217P)²+1.8625P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0526
_refine_ls_wR_factor_ref         0.0537
_reflns_number_gt                7852
_reflns_number_total             8338
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ic100974e_si_003_2.cif
_cod_data_source_block           euhfa3_acbz
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_database_code               4316747
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Eu1 Eu 0.714544(12) 0.738982(8) 0.726433(6) 0.01031(3) Uani 1 1 d . . .
O1 O 0.98452(18) 0.79292(13) 0.82364(9) 0.0164(3) Uani 1 1 d . . .
C1 C 1.0243(2) 0.90687(18) 0.95373(13) 0.0140(4) Uani 1 1 d . . .
C2 C 1.0456(3) 0.90922(18) 1.04283(13) 0.0162(4) Uani 1 1 d . . .
H2A H 1.0770 0.8475 1.0719 0.019 Uiso 1 1 calc R . .
C3 C 1.0207(3) 1.00185(18) 1.08868(13) 0.0159(4) Uani 1 1 d . . .
H3A H 1.0344 1.0032 1.1491 0.019 Uiso 1 1 calc R . .
C4 C 1.0432(2) 0.80637(18) 0.90199(13) 0.0152(4) Uani 1 1 d . . .
C5 C 1.1288(3) 0.7213(2) 0.94440(15) 0.0231(5) Uani 1 1 d . . .
H5A H 1.1548 0.6740 0.9008 0.035 Uiso 1 1 calc R . .
H5B H 1.0578 0.6710 0.9740 0.035 Uiso 1 1 calc R . .
H5C H 1.2300 0.7630 0.9862 0.035 Uiso 1 1 calc R . .
O1A O 0.87798(18) 0.69830(13) 0.63335(9) 0.0164(3) Uani 1 1 d . . .
C1A C 1.0043(2) 0.59468(17) 0.55472(12) 0.0124(4) Uani 1 1 d . . .
C2A C 0.8600(2) 0.50721(18) 0.52536(13) 0.0151(4) Uani 1 1 d . . .
H2AA H 0.7650 0.5124 0.5430 0.018 Uiso 1 1 calc R . .
C3A C 0.8553(2) 0.41288(18) 0.47042(13) 0.0153(4) Uani 1 1 d . . .
H3AA H 0.7570 0.3536 0.4500 0.018 Uiso 1 1 calc R . .
C4A C 1.0055(3) 0.69318(17) 0.61507(12) 0.0134(4) Uani 1 1 d . . .
C5A C 1.1608(3) 0.78448(19) 0.65285(14) 0.0194(4) Uani 1 1 d . . .
H5AA H 1.1417 0.8397 0.6938 0.029 Uiso 1 1 calc R . .
H5AB H 1.1974 0.8254 0.6068 0.029 Uiso 1 1 calc R . .
H5AC H 1.2450 0.7480 0.6827 0.029 Uiso 1 1 calc R . .
O2 O 0.69447(18) 0.70918(13) 0.87120(9) 0.0149(3) Uani 1 1 d . . .
O3 O 0.58133(18) 0.87289(13) 0.77307(9) 0.0153(3) Uani 1 1 d . . .
O4 O 0.56829(18) 0.76043(13) 0.58771(9) 0.0170(3) Uani 1 1 d . . .
O5 O 0.84396(18) 0.92509(12) 0.69077(9) 0.0158(3) Uani 1 1 d . . .
O6 O 0.45829(18) 0.60371(13) 0.71228(10) 0.0165(3) Uani 1 1 d . . .
O7 O 0.76565(18) 0.55616(13) 0.74918(10) 0.0165(3) Uani 1 1 d . . .
F1 F 0.4982(2) 0.62308(17) 1.00569(12) 0.0475(5) Uani 1 1 d . . .
F2 F 0.6781(3) 0.77140(15) 1.07669(9) 0.0410(4) Uani 1 1 d . . .
F3 F 0.7521(2) 0.63326(16) 1.02110(10) 0.0415(4) Uani 1 1 d . . .
F4 F 0.4343(2) 1.04011(14) 0.76369(9) 0.0364(4) Uani 1 1 d . . .
F5 F 0.56076(17) 1.08778(12) 0.89666(10) 0.0273(3) Uani 1 1 d . . .
F6 F 0.32131(18) 0.97224(13) 0.86141(12) 0.0347(4) Uani 1 1 d . . .
F7 F 0.3432(4) 0.8051(5) 0.4508(3) 0.0382(4) Uani 0.50 1 d PD A 1
F8 F 0.4474(5) 0.6712(3) 0.4173(3) 0.0382(4) Uani 0.50 1 d PD A 1
F9 F 0.5510(4) 0.8241(3) 0.3771(2) 0.0382(4) Uani 0.50 1 d PD A 1
F10 F 0.9659(2) 1.15747(13) 0.68838(12) 0.0410(4) Uani 1 1 d . . .
F11 F 0.9581(2) 1.13107(15) 0.55462(11) 0.0391(4) Uani 1 1 d . . .
F12 F 1.11801(17) 1.06002(14) 0.64719(12) 0.0352(4) Uani 1 1 d . . .
F13 F 0.21765(17) 0.39307(15) 0.80085(10) 0.0330(4) Uani 1 1 d . . .
F14 F 0.15844(17) 0.40303(13) 0.66475(10) 0.0303(3) Uani 1 1 d . . .
F15 F 0.17209(17) 0.55029(13) 0.75105(11) 0.0306(3) Uani 1 1 d . . .
F16 F 0.7101(2) 0.28774(14) 0.83111(14) 0.0446(5) Uani 1 1 d . . .
F17 F 0.91905(19) 0.43318(14) 0.87009(10) 0.0351(4) Uani 1 1 d . . .
F18 F 0.8525(2) 0.34831(14) 0.74170(11) 0.0356(4) Uani 1 1 d . . .
C6 C 0.6340(3) 0.75155(18) 0.92411(13) 0.0148(4) Uani 1 1 d . . .
C7 C 0.5589(3) 0.8432(2) 0.91513(14) 0.0188(4) Uani 1 1 d . . .
H7A H 0.5199 0.8691 0.9610 0.023 Uiso 1 1 calc R . .
C8 C 0.5405(2) 0.89689(17) 0.83993(13) 0.0134(4) Uani 1 1 d . . .
C9 C 0.6418(3) 0.6941(2) 1.00821(14) 0.0217(4) Uani 1 1 d . . .
C10 C 0.4629(3) 1.00035(18) 0.83926(14) 0.0163(4) Uani 1 1 d . . .
C11 C 0.6042(3) 0.8244(2) 0.53174(14) 0.0191(4) Uani 1 1 d . A .
C12 C 0.7300(3) 0.9242(2) 0.54089(15) 0.0223(5) Uani 1 1 d . . .
H12A H 0.7430 0.9631 0.4919 0.027 Uiso 1 1 calc R . .
C13 C 0.8379(3) 0.96816(18) 0.62120(14) 0.0161(4) Uani 1 1 d . . .
C14 C 0.4870(3) 0.7850(2) 0.44179(15) 0.0336(6) Uani 1 1 d D . .
C15 C 0.9707(3) 1.0811(2) 0.62780(16) 0.0224(5) Uani 1 1 d . . .
C16 C 0.4224(2) 0.50904(18) 0.74314(13) 0.0151(4) Uani 1 1 d . . .
C17 C 0.5245(3) 0.43862(19) 0.77583(14) 0.0177(4) Uani 1 1 d . . .
H17A H 0.4819 0.3702 0.7995 0.021 Uiso 1 1 calc R . .
C18 C 0.6883(3) 0.46739(18) 0.77411(13) 0.0158(4) Uani 1 1 d . . .
C19 C 0.2407(3) 0.4633(2) 0.74046(15) 0.0206(4) Uani 1 1 d . . .
C20 C 0.7919(3) 0.3822(2) 0.80429(17) 0.0232(5) Uani 1 1 d . . .
F7' F 0.3339(4) 0.7916(5) 0.4341(3) 0.0382(4) Uani 0.50 1 d PD A 2
F8' F 0.4861(5) 0.6725(3) 0.4241(3) 0.0382(4) Uani 0.50 1 d PD A 2
F9' F 0.5185(5) 0.8583(3) 0.3833(2) 0.0382(4) Uani 0.50 1 d PD A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Eu1 O7 116.90(5) . . ?
O4 Eu1 O3 84.56(5) . . ?
O7 Eu1 O3 142.26(5) . . ?
O4 Eu1 O6 77.83(5) . . ?
O7 Eu1 O6 72.45(5) . . ?
O3 Eu1 O6 83.49(5) . . ?
O4 Eu1 O1A 75.19(5) . . ?
O7 Eu1 O1A 71.26(5) . . ?
O3 Eu1 O1A 146.47(5) . . ?
O6 Eu1 O1A 116.96(5) . . ?
O4 Eu1 O5 72.84(5) . . ?
O7 Eu1 O5 140.08(5) . . ?
O3 Eu1 O5 73.68(5) . . ?
O6 Eu1 O5 144.11(5) . . ?
O1A Eu1 O5 74.93(5) . . ?
O4 Eu1 O2 144.49(5) . . ?
O7 Eu1 O2 74.60(5) . . ?
O3 Eu1 O2 71.05(5) . . ?
O6 Eu1 O2 74.19(5) . . ?
O1A Eu1 O2 137.64(5) . . ?
O5 Eu1 O2 121.48(5) . . ?
O4 Eu1 O1 142.51(5) . . ?
O7 Eu1 O1 78.53(5) . . ?
O3 Eu1 O1 103.67(5) . . ?
O6 Eu1 O1 138.88(5) . . ?
O1A Eu1 O1 78.82(5) . . ?
O5 Eu1 O1 74.63(5) . . ?
O2 Eu1 O1 70.39(5) . . ?
C4 O1 Eu1 136.90(14) . . ?
C3 C1 C2 119.90(19) 2_777 . ?
C3 C1 C4 118.76(18) 2_777 . ?
C2 C1 C4 121.31(19) . . ?
C3 C2 C1 119.92(19) . . ?
C3 C2 H2A 120.0 . . ?
C1 C2 H2A 120.0 . . ?
C2 C3 C1 120.18(19) . 2_777 ?
C2 C3 H3A 119.9 . . ?
C1 C3 H3A 119.9 2_777 . ?
O1 C4 C1 119.13(19) . . ?
O1 C4 C5 120.08(19) . . ?
C1 C4 C5 120.77(18) . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C4A O1A Eu1 155.24(14) . . ?
C3A C1A C2A 120.26(18) 2_766 . ?
C3A C1A C4A 121.30(18) 2_766 . ?
C2A C1A C4A 118.42(18) . . ?
C3A C2A C1A 120.04(18) . . ?
C3A C2A H2AA 120.0 . . ?
C1A C2A H2AA 120.0 . . ?
C2A C3A C1A 119.70(19) . 2_766 ?
C2A C3A H3AA 120.1 . . ?
C1A C3A H3AA 120.1 2_766 . ?
O1A C4A C1A 119.12(18) . . ?
O1A C4A C5A 120.81(18) . . ?
C1A C4A C5A 120.07(18) . . ?
C4A C5A H5AA 109.5 . . ?
C4A C5A H5AB 109.5 . . ?
H5AA C5A H5AB 109.5 . . ?
C4A C5A H5AC 109.5 . . ?
H5AA C5A H5AC 109.5 . . ?
H5AB C5A H5AC 109.5 . . ?
C6 O2 Eu1 135.79(13) . . ?
C8 O3 Eu1 136.57(13) . . ?
C11 O4 Eu1 132.65(14) . . ?
C13 O5 Eu1 132.68(14) . . ?
C16 O6 Eu1 131.05(13) . . ?
C18 O7 Eu1 132.65(14) . . ?
O2 C6 C7 127.53(19) . . ?
O2 C6 C9 115.50(18) . . ?
C7 C6 C9 116.96(18) . . ?
C8 C7 C6 120.80(19) . . ?
C8 C7 H7A 119.6 . . ?
C6 C7 H7A 119.6 . . ?
O3 C8 C7 128.16(19) . . ?
O3 C8 C10 115.85(18) . . ?
C7 C8 C10 115.98(18) . . ?
F3 C9 F1 108.0(2) . . ?
F3 C9 F2 107.6(2) . . ?
F1 C9 F2 106.9(2) . . ?
F3 C9 C6 111.76(18) . . ?
F1 C9 C6 110.17(19) . . ?
F2 C9 C6 112.23(18) . . ?
F4 C10 F6 107.43(19) . . ?
F4 C10 F5 107.79(18) . . ?
F6 C10 F5 106.49(17) . . ?
F4 C10 C8 112.95(17) . . ?
F6 C10 C8 111.48(17) . . ?
F5 C10 C8 110.41(17) . . ?
O4 C11 C12 129.1(2) . . ?
O4 C11 C14 113.29(19) . . ?
C12 C11 C14 117.60(19) . . ?
C11 C12 C13 121.1(2) . . ?
C11 C12 H12A 119.5 . . ?
C13 C12 H12A 119.5 . . ?
O5 C13 C12 127.9(2) . . ?
O5 C13 C15 113.44(19) . . ?
C12 C13 C15 118.65(19) . . ?
F7' C14 F8 95.1(3) . . ?
F7' C14 F9' 96.1(3) . . ?
F8 C14 F9' 118.1(3) . . ?
F7' C14 F9 114.6(3) . . ?
F8 C14 F9 99.3(3) . . ?
F7' C14 F8' 108.7(3) . . ?
F9' C14 F8' 117.7(3) . . ?
F9 C14 F8' 95.6(3) . . ?
F8 C14 F7 103.4(3) . . ?
F9' C14 F7 99.7(3) . . ?
F9 C14 F7 121.1(3) . . ?
F8' C14 F7 116.2(4) . . ?
F7' C14 C11 115.8(2) . . ?
F8 C14 C11 115.5(3) . . ?
F9' C14 C11 113.2(2) . . ?
F9 C14 C11 113.9(2) . . ?
F8' C14 C11 105.6(2) . . ?
F7 C14 C11 103.8(2) . . ?
F10 C15 F12 108.2(2) . . ?
F10 C15 F11 107.6(2) . . ?
F12 C15 F11 106.39(19) . . ?
F10 C15 C13 110.78(19) . . ?
F12 C15 C13 110.13(18) . . ?
F11 C15 C13 113.5(2) . . ?
O6 C16 C17 128.42(19) . . ?
O6 C16 C19 115.14(18) . . ?
C17 C16 C19 116.38(19) . . ?
C18 C17 C16 120.77(19) . . ?
C18 C17 H17A 119.6 . . ?
C16 C17 H17A 119.6 . . ?
O7 C18 C17 127.9(2) . . ?
O7 C18 C20 113.38(18) . . ?
C17 C18 C20 118.68(19) . . ?
F13 C19 F14 107.04(19) . . ?
F13 C19 F15 107.92(19) . . ?
F14 C19 F15 107.34(18) . . ?
F13 C19 C16 112.34(18) . . ?
F14 C19 C16 110.69(19) . . ?
F15 C19 C16 111.26(18) . . ?
F18 C20 F16 108.0(2) . . ?
F18 C20 F17 106.97(19) . . ?
F16 C20 F17 106.7(2) . . ?
F18 C20 C18 110.84(19) . . ?
F16 C20 C18 113.59(19) . . ?
F17 C20 C18 110.40(19) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Eu1 O4 2.3538(15) . ?
Eu1 O7 2.3554(15) . ?
Eu1 O3 2.3741(14) . ?
Eu1 O6 2.3811(15) . ?
Eu1 O1A 2.4021(14) . ?
Eu1 O5 2.4040(15) . ?
Eu1 O2 2.4140(14) . ?
Eu1 O1 2.4189(15) . ?
O1 C4 1.232(3) . ?
C1 C3 1.397(3) 2_777 ?
C1 C2 1.401(3) . ?
C1 C4 1.491(3) . ?
C2 C3 1.388(3) . ?
C2 H2A 0.9500 . ?
C3 C1 1.397(3) 2_777 ?
C3 H3A 0.9500 . ?
C4 C5 1.495(3) . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
O1A C4A 1.228(2) . ?
C1A C3A 1.395(3) 2_766 ?
C1A C2A 1.396(3) . ?
C1A C4A 1.487(3) . ?
C2A C3A 1.386(3) . ?
C2A H2AA 0.9500 . ?
C3A C1A 1.395(3) 2_766 ?
C3A H3AA 0.9500 . ?
C4A C5A 1.498(3) . ?
C5A H5AA 0.9800 . ?
C5A H5AB 0.9800 . ?
C5A H5AC 0.9800 . ?
O2 C6 1.247(2) . ?
O3 C8 1.252(2) . ?
O4 C11 1.256(3) . ?
O5 C13 1.249(3) . ?
O6 C16 1.257(3) . ?
O7 C18 1.252(3) . ?
F1 C9 1.326(3) . ?
F2 C9 1.331(3) . ?
F3 C9 1.319(3) . ?
F4 C10 1.317(3) . ?
F5 C10 1.338(2) . ?
F6 C10 1.336(2) . ?
F7 C14 1.368(4) . ?
F8 C14 1.335(4) . ?
F9 C14 1.345(3) . ?
F10 C15 1.319(3) . ?
F11 C15 1.338(3) . ?
F12 C15 1.333(3) . ?
F13 C19 1.333(2) . ?
F14 C19 1.335(3) . ?
F15 C19 1.337(3) . ?
F16 C20 1.333(3) . ?
F17 C20 1.338(3) . ?
F18 C20 1.331(3) . ?
C6 C7 1.397(3) . ?
C6 C9 1.540(3) . ?
C7 C8 1.389(3) . ?
C7 H7A 0.9500 . ?
C8 C10 1.540(3) . ?
C11 C12 1.391(3) . ?
C11 C14 1.541(3) . ?
C12 C13 1.401(3) . ?
C12 H12A 0.9500 . ?
C13 C15 1.536(3) . ?
C14 F7' 1.331(4) . ?
C14 F9' 1.346(3) . ?
C14 F8' 1.357(4) . ?
C16 C17 1.395(3) . ?
C16 C19 1.537(3) . ?
C17 C18 1.393(3) . ?
C17 H17A 0.9500 . ?
C18 C20 1.534(3) . ?
