#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:28:27 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179247 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/67/4316749.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4316749
loop_
_publ_author_name
'Svetlana V. Eliseeva'
'Dmitry N. Pleshkov'
'Konstantin A. Lyssenko'
'Leonid S. Lepnev'
'Jean-Claude G. Bünzli'
'Natalia P. Kuzmina'
_publ_section_title
;
 Highly Luminescent and Triboluminescent Coordination Polymers Assembled
 from Lanthanide β-Diketonates and Aromatic Bidentate O-Donor Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9300
_journal_page_last               9311
_journal_paper_doi               10.1021/ic100974e
_journal_volume                  49
_journal_year                    2010
_chemical_formula_moiety         'C25 H13 F18 Gd O8'
_chemical_formula_sum            'C25 H13 F18 Gd O8'
_chemical_formula_weight         940.60
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.606(2)
_cell_angle_beta                 103.584(2)
_cell_angle_gamma                103.619(2)
_cell_formula_units_Z            2
_cell_length_a                   8.7100(10)
_cell_length_b                   11.9073(14)
_cell_length_c                   16.0528(19)
_cell_measurement_reflns_used    721
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      29
_cell_measurement_theta_min      3
_cell_volume                     1563.8(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX II'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'Bruker APEX II CCD area detector''
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0398
_diffrn_reflns_av_sigmaI/netI    0.0610
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            15435
_diffrn_reflns_theta_full        29.00
_diffrn_reflns_theta_max         29.00
_diffrn_reflns_theta_min         1.77
_exptl_absorpt_coefficient_mu    2.274
_exptl_absorpt_correction_T_max  0.727
_exptl_absorpt_correction_T_min  0.549
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.998
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             906
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.316
_refine_diff_density_min         -1.494
_refine_diff_density_rms         0.168
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.053
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     470
_refine_ls_number_reflns         8165
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.053
_refine_ls_R_factor_all          0.0420
_refine_ls_R_factor_gt           0.0387
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0596P)²+1.9462P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1050
_refine_ls_wR_factor_ref         0.1079
_reflns_number_gt                7524
_reflns_number_total             8165
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ic100974e_si_003_4.cif
_cod_data_source_block           gdhfa3_acbz
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_database_code               4316749
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Gd1 Gd 0.715298(17) 0.738789(13) 0.726740(10) 0.01101(6) Uani 1 1 d . . .
O1 O 0.9832(3) 0.7932(2) 0.82305(17) 0.0175(5) Uani 1 1 d . . .
C1 C 1.0242(4) 0.9068(3) 0.9535(2) 0.0142(6) Uani 1 1 d . . .
C2 C 1.0454(4) 0.9088(3) 1.0428(2) 0.0159(6) Uani 1 1 d . . .
H2A H 1.0763 0.8467 1.0718 0.019 Uiso 1 1 calc R . .
C3 C 1.0212(4) 1.0018(3) 1.0888(2) 0.0158(6) Uani 1 1 d . . .
H3A H 1.0355 1.0033 1.1494 0.019 Uiso 1 1 calc R . .
C4 C 1.0434(4) 0.8062(3) 0.9016(2) 0.0156(6) Uani 1 1 d . . .
C5 C 1.1295(5) 0.7210(3) 0.9439(3) 0.0228(7) Uani 1 1 d . . .
H5A H 1.1568 0.6745 0.9001 0.034 Uiso 1 1 calc R . .
H5B H 1.0583 0.6696 0.9730 0.034 Uiso 1 1 calc R . .
H5C H 1.2300 0.7629 0.9862 0.034 Uiso 1 1 calc R . .
O1A O 0.8776(3) 0.6983(2) 0.63377(17) 0.0171(5) Uani 1 1 d . . .
C1A C 1.0036(4) 0.5945(3) 0.5548(2) 0.0133(6) Uani 1 1 d . . .
C2A C 0.8598(4) 0.5072(3) 0.5256(2) 0.0159(6) Uani 1 1 d . . .
H2AA H 0.7652 0.5121 0.5438 0.019 Uiso 1 1 calc R . .
C3A C 0.8546(4) 0.4132(3) 0.4703(2) 0.0159(6) Uani 1 1 d . . .
H3AA H 0.7560 0.3542 0.4493 0.019 Uiso 1 1 calc R . .
C4A C 1.0055(4) 0.6933(3) 0.6150(2) 0.0136(6) Uani 1 1 d . . .
C5A C 1.1609(4) 0.7848(3) 0.6526(3) 0.0192(7) Uani 1 1 d . . .
H5AA H 1.1397 0.8442 0.6896 0.029 Uiso 1 1 calc R . .
H5AB H 1.2026 0.8209 0.6060 0.029 Uiso 1 1 calc R . .
H5AC H 1.2420 0.7493 0.6869 0.029 Uiso 1 1 calc R . .
O2 O 0.6951(3) 0.7090(2) 0.87119(16) 0.0156(5) Uani 1 1 d . . .
O3 O 0.5824(3) 0.8726(2) 0.77262(16) 0.0158(5) Uani 1 1 d . . .
O4 O 0.5700(3) 0.7594(2) 0.58890(17) 0.0178(5) Uani 1 1 d . . .
O5 O 0.8449(3) 0.9246(2) 0.69109(17) 0.0163(5) Uani 1 1 d . . .
O6 O 0.4599(3) 0.6040(2) 0.71196(17) 0.0170(5) Uani 1 1 d . . .
O7 O 0.7672(3) 0.5568(2) 0.74939(18) 0.0168(5) Uani 1 1 d . . .
F1 F 0.4986(4) 0.6234(3) 1.0059(2) 0.0482(8) Uani 1 1 d . . .
F2 F 0.6786(4) 0.7719(3) 1.07697(17) 0.0406(7) Uani 1 1 d . . .
F3 F 0.7529(4) 0.6333(3) 1.02152(18) 0.0416(7) Uani 1 1 d . . .
F4 F 0.4358(4) 1.0400(3) 0.76285(17) 0.0362(6) Uani 1 1 d . . .
F5 F 0.5605(3) 1.0877(2) 0.89628(18) 0.0279(5) Uani 1 1 d . . .
F6 F 0.3215(3) 0.9719(2) 0.8602(2) 0.0342(6) Uani 1 1 d . . .
F7 F 0.3457(6) 0.8047(9) 0.4518(5) 0.0386(6) Uani 0.50 1 d PD A 1
F8 F 0.4479(8) 0.6700(4) 0.4180(5) 0.0386(6) Uani 0.50 1 d PD A 1
F9 F 0.5523(7) 0.8232(6) 0.3778(3) 0.0386(6) Uani 0.50 1 d PD A 1
F10 F 0.9653(4) 1.1574(2) 0.6890(2) 0.0418(7) Uani 1 1 d . . .
F11 F 0.9576(3) 1.1307(2) 0.5548(2) 0.0389(7) Uani 1 1 d . . .
F12 F 1.1183(3) 1.0603(2) 0.6481(2) 0.0349(6) Uani 1 1 d . . .
F13 F 0.2191(3) 0.3935(3) 0.80119(18) 0.0334(6) Uani 1 1 d . . .
F14 F 0.1602(3) 0.4033(2) 0.66476(17) 0.0301(5) Uani 1 1 d . . .
F15 F 0.1727(3) 0.5504(2) 0.75059(19) 0.0316(6) Uani 1 1 d . . .
F16 F 0.7112(3) 0.2880(2) 0.8314(3) 0.0455(8) Uani 1 1 d . . .
F17 F 0.9200(3) 0.4335(2) 0.8701(2) 0.0363(6) Uani 1 1 d . . .
F18 F 0.8536(3) 0.3483(2) 0.7415(2) 0.0363(6) Uani 1 1 d . . .
C6 C 0.6347(4) 0.7514(3) 0.9242(2) 0.0159(6) Uani 1 1 d . . .
C7 C 0.5588(5) 0.8428(3) 0.9149(2) 0.0198(7) Uani 1 1 d . . .
H7A H 0.5189 0.8684 0.9607 0.024 Uiso 1 1 calc R . .
C8 C 0.5409(4) 0.8966(3) 0.8394(2) 0.0146(6) Uani 1 1 d . . .
C9 C 0.6427(5) 0.6941(3) 1.0086(3) 0.0213(7) Uani 1 1 d . . .
C10 C 0.4633(4) 1.0000(3) 0.8386(2) 0.0166(7) Uani 1 1 d . . .
C11 C 0.6052(4) 0.8242(3) 0.5325(2) 0.0198(7) Uani 1 1 d . A .
C12 C 0.7312(5) 0.9236(4) 0.5416(3) 0.0232(8) Uani 1 1 d . . .
H12A H 0.7444 0.9627 0.4925 0.028 Uiso 1 1 calc R . .
C13 C 0.8382(4) 0.9670(3) 0.6215(2) 0.0165(7) Uani 1 1 d . . .
C14 C 0.4877(4) 0.7844(3) 0.4427(3) 0.0343(10) Uani 1 1 d D . .
C15 C 0.9707(5) 1.0811(3) 0.6282(3) 0.0214(7) Uani 1 1 d . . .
C16 C 0.4237(4) 0.5097(3) 0.7430(2) 0.0163(6) Uani 1 1 d . . .
C17 C 0.5258(4) 0.4389(3) 0.7758(2) 0.0180(7) Uani 1 1 d . . .
H17A H 0.4832 0.3704 0.7997 0.022 Uiso 1 1 calc R . .
C18 C 0.6900(4) 0.4678(3) 0.7738(2) 0.0158(6) Uani 1 1 d . . .
C19 C 0.2418(4) 0.4637(3) 0.7405(3) 0.0206(7) Uani 1 1 d . . .
C20 C 0.7931(5) 0.3826(3) 0.8046(3) 0.0242(8) Uani 1 1 d . . .
F7' F 0.3343(6) 0.7923(9) 0.4351(5) 0.0386(6) Uani 0.50 1 d PD A 2
F8' F 0.4851(8) 0.6718(4) 0.4257(5) 0.0386(6) Uani 0.50 1 d PD A 2
F9' F 0.5195(8) 0.8565(5) 0.3832(4) 0.0386(6) Uani 0.50 1 d PD A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Gd Gd -0.1653 3.9035 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Gd1 O7 116.77(9) . . ?
O4 Gd1 O3 84.39(9) . . ?
O7 Gd1 O3 142.67(9) . . ?
O4 Gd1 O6 77.34(9) . . ?
O7 Gd1 O6 72.83(9) . . ?
O3 Gd1 O6 83.52(9) . . ?
O4 Gd1 O1A 75.14(9) . . ?
O7 Gd1 O1A 71.09(9) . . ?
O3 Gd1 O1A 146.24(9) . . ?
O6 Gd1 O1A 116.77(9) . . ?
O4 Gd1 O5 73.13(9) . . ?
O7 Gd1 O5 139.71(8) . . ?
O3 Gd1 O5 73.64(9) . . ?
O6 Gd1 O5 144.01(9) . . ?
O1A Gd1 O5 74.85(9) . . ?
O4 Gd1 O1 142.46(9) . . ?
O7 Gd1 O1 78.57(9) . . ?
O3 Gd1 O1 103.74(9) . . ?
O6 Gd1 O1 139.42(9) . . ?
O1A Gd1 O1 78.83(9) . . ?
O5 Gd1 O1 74.27(9) . . ?
O4 Gd1 O2 144.38(9) . . ?
O7 Gd1 O2 74.73(9) . . ?
O3 Gd1 O2 71.29(9) . . ?
O6 Gd1 O2 74.47(9) . . ?
O1A Gd1 O2 137.73(9) . . ?
O5 Gd1 O2 121.47(9) . . ?
O1 Gd1 O2 70.58(9) . . ?
C4 O1 Gd1 137.4(2) . . ?
C3 C1 C2 119.9(3) 2_777 . ?
C3 C1 C4 118.8(3) 2_777 . ?
C2 C1 C4 121.2(3) . . ?
C3 C2 C1 119.8(3) . . ?
C3 C2 H2A 120.1 . . ?
C1 C2 H2A 120.1 . . ?
C2 C3 C1 120.3(3) . 2_777 ?
C2 C3 H3A 119.8 . . ?
C1 C3 H3A 119.8 2_777 . ?
O1 C4 C1 118.6(3) . . ?
O1 C4 C5 120.5(3) . . ?
C1 C4 C5 120.9(3) . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C4A O1A Gd1 155.4(2) . . ?
C2A C1A C3A 120.4(3) . 2_766 ?
C2A C1A C4A 118.6(3) . . ?
C3A C1A C4A 120.9(3) 2_766 . ?
C3A C2A C1A 120.0(3) . . ?
C3A C2A H2AA 120.0 . . ?
C1A C2A H2AA 120.0 . . ?
C2A C3A C1A 119.5(3) . 2_766 ?
C2A C3A H3AA 120.3 . . ?
C1A C3A H3AA 120.3 2_766 . ?
O1A C4A C1A 118.9(3) . . ?
O1A C4A C5A 120.9(3) . . ?
C1A C4A C5A 120.2(3) . . ?
C4A C5A H5AA 109.5 . . ?
C4A C5A H5AB 109.5 . . ?
H5AA C5A H5AB 109.5 . . ?
C4A C5A H5AC 109.5 . . ?
H5AA C5A H5AC 109.5 . . ?
H5AB C5A H5AC 109.5 . . ?
C6 O2 Gd1 135.9(2) . . ?
C8 O3 Gd1 136.5(2) . . ?
C11 O4 Gd1 132.7(2) . . ?
C13 O5 Gd1 132.3(2) . . ?
C16 O6 Gd1 131.0(2) . . ?
C18 O7 Gd1 132.6(2) . . ?
O2 C6 C7 127.4(3) . . ?
O2 C6 C9 115.6(3) . . ?
C7 C6 C9 116.9(3) . . ?
C8 C7 C6 120.7(3) . . ?
C8 C7 H7A 119.7 . . ?
C6 C7 H7A 119.7 . . ?
O3 C8 C7 128.2(3) . . ?
O3 C8 C10 115.9(3) . . ?
C7 C8 C10 115.9(3) . . ?
F3 C9 F1 108.4(4) . . ?
F3 C9 F2 107.8(3) . . ?
F1 C9 F2 106.9(3) . . ?
F3 C9 C6 111.7(3) . . ?
F1 C9 C6 109.8(3) . . ?
F2 C9 C6 112.1(3) . . ?
F4 C10 F6 107.4(3) . . ?
F4 C10 F5 107.7(3) . . ?
F6 C10 F5 106.4(3) . . ?
F4 C10 C8 112.9(3) . . ?
F6 C10 C8 111.6(3) . . ?
F5 C10 C8 110.5(3) . . ?
O4 C11 C12 128.9(4) . . ?
O4 C11 C14 113.1(3) . . ?
C12 C11 C14 118.0(3) . . ?
C11 C12 C13 121.0(4) . . ?
C11 C12 H12A 119.5 . . ?
C13 C12 H12A 119.5 . . ?
O5 C13 C12 128.4(3) . . ?
O5 C13 C15 113.1(3) . . ?
C12 C13 C15 118.5(3) . . ?
F7' C14 F8 95.7(6) . . ?
F7' C14 F9 114.6(5) . . ?
F8 C14 F9 99.0(6) . . ?
F7' C14 F9' 96.1(6) . . ?
F8 C14 F9' 117.1(6) . . ?
F7' C14 F8' 108.6(6) . . ?
F9 C14 F8' 96.1(5) . . ?
F9' C14 F8' 117.5(6) . . ?
F8 C14 F7 103.5(6) . . ?
F9 C14 F7 121.3(6) . . ?
F9' C14 F7 100.2(6) . . ?
F8' C14 F7 115.6(6) . . ?
F7' C14 C11 115.8(4) . . ?
F8 C14 C11 115.7(4) . . ?
F9 C14 C11 113.6(4) . . ?
F9' C14 C11 113.4(4) . . ?
F8' C14 C11 105.6(4) . . ?
F7 C14 C11 103.9(4) . . ?
F10 C15 F12 108.0(3) . . ?
F10 C15 F11 107.9(3) . . ?
F12 C15 F11 106.7(3) . . ?
F10 C15 C13 110.8(3) . . ?
F12 C15 C13 109.9(3) . . ?
F11 C15 C13 113.3(3) . . ?
O6 C16 C17 128.2(3) . . ?
O6 C16 C19 115.5(3) . . ?
C17 C16 C19 116.3(3) . . ?
C16 C17 C18 120.7(3) . . ?
C16 C17 H17A 119.7 . . ?
C18 C17 H17A 119.7 . . ?
O7 C18 C17 128.0(3) . . ?
O7 C18 C20 113.6(3) . . ?
C17 C18 C20 118.4(3) . . ?
F13 C19 F15 108.1(3) . . ?
F13 C19 F14 107.1(3) . . ?
F15 C19 F14 107.1(3) . . ?
F13 C19 C16 112.3(3) . . ?
F15 C19 C16 111.4(3) . . ?
F14 C19 C16 110.5(3) . . ?
F17 C20 F16 107.0(4) . . ?
F17 C20 F18 106.9(3) . . ?
F16 C20 F18 107.9(4) . . ?
F17 C20 C18 110.6(3) . . ?
F16 C20 C18 113.7(3) . . ?
F18 C20 C18 110.4(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Gd1 O4 2.332(3) . ?
Gd1 O7 2.342(2) . ?
Gd1 O3 2.363(2) . ?
Gd1 O6 2.370(2) . ?
Gd1 O1A 2.388(2) . ?
Gd1 O5 2.396(2) . ?
Gd1 O1 2.400(3) . ?
Gd1 O2 2.402(3) . ?
O1 C4 1.234(4) . ?
C1 C3 1.395(5) 2_777 ?
C1 C2 1.400(5) . ?
C1 C4 1.491(5) . ?
C2 C3 1.387(5) . ?
C2 H2A 0.9500 . ?
C3 C1 1.395(5) 2_777 ?
C3 H3A 0.9500 . ?
C4 C5 1.496(5) . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
O1A C4A 1.234(4) . ?
C1A C2A 1.392(5) . ?
C1A C3A 1.407(4) 2_766 ?
C1A C4A 1.483(5) . ?
C2A C3A 1.382(5) . ?
C2A H2AA 0.9500 . ?
C3A C1A 1.407(4) 2_766 ?
C3A H3AA 0.9500 . ?
C4A C5A 1.498(5) . ?
C5A H5AA 0.9800 . ?
C5A H5AB 0.9800 . ?
C5A H5AC 0.9800 . ?
O2 C6 1.246(4) . ?
O3 C8 1.251(4) . ?
O4 C11 1.262(5) . ?
O5 C13 1.241(4) . ?
O6 C16 1.252(4) . ?
O7 C18 1.247(4) . ?
F1 C9 1.326(5) . ?
F2 C9 1.331(5) . ?
F3 C9 1.318(5) . ?
F4 C10 1.316(4) . ?
F5 C10 1.340(4) . ?
F6 C10 1.333(4) . ?
F7 C14 1.354(4) . ?
F8 C14 1.340(4) . ?
F9 C14 1.347(4) . ?
F10 C15 1.320(5) . ?
F11 C15 1.335(5) . ?
F12 C15 1.334(4) . ?
F13 C19 1.332(4) . ?
F14 C19 1.333(5) . ?
F15 C19 1.333(5) . ?
F16 C20 1.331(5) . ?
F17 C20 1.332(5) . ?
F18 C20 1.336(5) . ?
C6 C7 1.397(5) . ?
C6 C9 1.539(5) . ?
C7 C8 1.390(5) . ?
C7 H7A 0.9500 . ?
C8 C10 1.537(5) . ?
C11 C12 1.387(5) . ?
C11 C14 1.538(6) . ?
C12 C13 1.390(6) . ?
C12 H12A 0.9500 . ?
C13 C15 1.542(5) . ?
C14 F7' 1.339(4) . ?
C14 F9' 1.347(4) . ?
C14 F8' 1.350(4) . ?
C16 C17 1.397(5) . ?
C16 C19 1.539(5) . ?
C17 C18 1.398(5) . ?
C17 H17A 0.9500 . ?
C18 C20 1.533(5) . ?
