#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:44:19 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179260 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/80/4318030.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4318030
loop_
_publ_author_name
'Jean-Pierre Costes'
'Juan Modesto Clemente-Juan'
'Françoise Dahan'
'Frédéric Dumestre'
'Jean-Pierre Tuchagues'
_publ_contact_author
;
        Dr Jean-Pierre Costes
        Laboratoire de Chimie de Coordination du CNRS
        205 Route de Narbonne
        31077 Toulouse Cedex 4
        France
;
_publ_contact_author_email       costes@lcc-toulouse.fr
_publ_contact_author_fax         '(33) 0561553003'
_publ_contact_author_phone       '(33) 0561333152'
_publ_section_title
;
 Dinuclear (FeII, GdIII) Complexes Deriving from Hexadentate Schiff Bases:
 Synthesis, Structure, and Mössbauer and Magnetic Properties
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2886
_journal_page_last               2891
_journal_paper_doi               10.1021/ic0112793
_journal_volume                  41
_journal_year                    2002
_chemical_formula_sum            'C24 H30 Fe Gd N5 O14'
_chemical_formula_weight         825.63
_chemical_name_systematic
;
  ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.15(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.6264(17)
_cell_length_b                   19.662(3)
_cell_length_c                   16.039(3)
_cell_measurement_temperature    160(2)
_cell_volume                     3023.5(9)
_computing_cell_refinement       'STOE-IPDS software (Stoe, 2.93, 1997)'
_computing_data_collection       'STOE-IPDS software (Stoe, 2.93, 1997)'
_computing_data_reduction        'XRED (Stoe, 1.08, 1996)'
_computing_molecular_graphics    'ZORTEP (Zsolnai, 1996)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      160(2)
_diffrn_measured_fraction_theta_full 0.970
_diffrn_measured_fraction_theta_max 0.970
_diffrn_measurement_device_type  STOE-IPDS
_diffrn_measurement_method       'Imaging Plate Detector System'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0311
_diffrn_reflns_av_sigmaI/netI    0.0187
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            20456
_diffrn_reflns_theta_full        24.07
_diffrn_reflns_theta_max         24.07
_diffrn_reflns_theta_min         2.07
_exptl_absorpt_coefficient_mu    2.730
_exptl_absorpt_correction_T_max  0.8210
_exptl_absorpt_correction_T_min  0.5756
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'X-SHAPE (Stoe & Cie, 1996)'
_exptl_crystal_colour            Light-brown
_exptl_crystal_density_diffrn    1.814
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Parallelepiped
_exptl_crystal_F_000             1644
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.804
_refine_diff_density_min         -0.508
_refine_diff_density_rms         0.072
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     406
_refine_ls_number_reflns         4656
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0213
_refine_ls_R_factor_gt           0.0193
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0228P)²+2.5711P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0445
_refine_ls_wR_factor_ref         0.0452
_reflns_number_gt                4357
_reflns_number_total             4656
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0112793_2.cif
_cod_data_source_block           (1')
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Numerical'
changed to 'numerical' according to the built-in table from CIF Core
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0228P)^2^+2.5711P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0228P)^2^+2.5711P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3023.6(9)
_cod_database_code               4318030
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y+1/2, z+1/2'
'-x, -y, -z'
'-x, y-1/2, -z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Gd Gd 0.204294(12) 0.424084(5) 0.242871(7) 0.01887(5) Uani 1 d . . .
Fe Fe 0.32252(3) 0.262099(16) 0.30970(2) 0.01872(8) Uani 1 d . . .
O1 O 0.29655(18) 0.35614(8) 0.35827(10) 0.0237(4) Uani 1 d . . .
C1 C 0.3344(3) 0.37931(12) 0.43472(15) 0.0226(5) Uani 1 d . . .
C2 C 0.3103(3) 0.44832(13) 0.45178(15) 0.0252(5) Uani 1 d . . .
C3 C 0.3509(3) 0.47679(13) 0.52819(16) 0.0301(6) Uani 1 d . . .
H3 H 0.3338 0.5236 0.5378 0.033 Uiso 1 calc R . .
C4 C 0.4169(3) 0.43697(14) 0.59145(16) 0.0336(6) Uani 1 d . . .
H4 H 0.4480 0.4568 0.6439 0.037 Uiso 1 calc R . .
C5 C 0.4370(3) 0.36903(14) 0.57788(16) 0.0308(6) Uani 1 d . . .
H5 H 0.4795 0.3418 0.6220 0.034 Uiso 1 calc R . .
C6 C 0.3961(3) 0.33877(13) 0.49997(15) 0.0247(5) Uani 1 d . . .
O3 O 0.24456(19) 0.48391(8) 0.38477(11) 0.0276(4) Uani 1 d . . .
C20 C 0.1961(3) 0.55122(13) 0.40400(19) 0.0366(7) Uani 1 d . . .
H20A H 0.1514 0.5722 0.3530 0.040 Uiso 1 calc R . .
H20B H 0.2754 0.5791 0.4260 0.040 Uiso 1 calc R . .
H20C H 0.1285 0.5479 0.4460 0.040 Uiso 1 calc R . .
C7 C 0.4180(3) 0.26636(13) 0.49359(15) 0.0265(6) Uani 1 d . . .
H7 H 0.4500 0.2436 0.5439 0.029 Uiso 1 calc R . .
N1 N 0.3992(2) 0.22934(10) 0.42789(12) 0.0238(4) Uani 1 d . . .
C8 C 0.4392(3) 0.15707(13) 0.43850(16) 0.0285(6) Uani 1 d . . .
H8A H 0.4496 0.1464 0.4991 0.031 Uiso 1 calc R . .
H8B H 0.5313 0.1504 0.4168 0.031 Uiso 1 calc R . .
C9 C 0.3358(3) 0.10660(12) 0.39460(16) 0.0252(5) Uani 1 d . . .
C10 C 0.3395(3) 0.10776(12) 0.30008(16) 0.0262(5) Uani 1 d . . .
H10A H 0.4380 0.1065 0.2869 0.029 Uiso 1 calc R . .
H10B H 0.2932 0.0662 0.2763 0.029 Uiso 1 calc R . .
C18 C 0.3875(3) 0.03572(13) 0.42316(18) 0.0356(7) Uani 1 d . . .
H18A H 0.4822 0.0287 0.4070 0.039 Uiso 1 calc R . .
H18B H 0.3253 0.0010 0.3966 0.039 Uiso 1 calc R . .
H18C H 0.3879 0.0323 0.4841 0.039 Uiso 1 calc R . .
C19 C 0.1886(3) 0.11782(13) 0.41936(19) 0.0342(6) Uani 1 d . . .
H19A H 0.1560 0.1630 0.4008 0.038 Uiso 1 calc R . .
H19B H 0.1888 0.1146 0.4803 0.038 Uiso 1 calc R . .
H19C H 0.1264 0.0831 0.3929 0.038 Uiso 1 calc R . .
N2 N 0.2714(2) 0.16771(10) 0.25937(12) 0.0212(4) Uani 1 d . . .
O2 O 0.18190(17) 0.30443(8) 0.22300(10) 0.0228(4) Uani 1 d . . .
C11 C 0.1142(2) 0.27487(12) 0.15658(14) 0.0204(5) Uani 1 d . . .
C12 C 0.0316(2) 0.31666(12) 0.10074(15) 0.0219(5) Uani 1 d . . .
C13 C -0.0369(3) 0.29132(14) 0.02866(17) 0.0321(6) Uani 1 d . . .
H13 H -0.0923 0.3205 -0.0080 0.035 Uiso 1 calc R . .
C14 C -0.0250(3) 0.22290(14) 0.00966(18) 0.0371(7) Uani 1 d . . .
H14 H -0.0688 0.2055 -0.0413 0.041 Uiso 1 calc R . .
C15 C 0.0497(3) 0.18056(14) 0.06424(17) 0.0324(6) Uani 1 d . . .
H15 H 0.0551 0.1335 0.0514 0.036 Uiso 1 calc R . .
C16 C 0.1188(3) 0.20530(12) 0.13920(16) 0.0238(5) Uani 1 d . . .
O4 O 0.02925(17) 0.38427(8) 0.12510(10) 0.0254(4) Uani 1 d . . .
C21 C -0.0774(3) 0.42569(13) 0.08049(19) 0.0344(7) Uani 1 d . . .
H21A H -0.0711 0.4723 0.1020 0.038 Uiso 1 calc R . .
H21B H -0.1696 0.4070 0.0885 0.038 Uiso 1 calc R . .
H21C H -0.0637 0.4258 0.0207 0.038 Uiso 1 calc R . .
C17 C 0.1918(3) 0.15557(12) 0.19315(16) 0.0239(5) Uani 1 d . . .
H17 H 0.1792 0.1092 0.1777 0.026 Uiso 1 calc R . .
O5 O 0.51373(18) 0.25233(9) 0.25431(11) 0.0299(4) Uani 1 d . . .
C22 C 0.6356(3) 0.26768(14) 0.27380(19) 0.0360(7) Uani 1 d . . .
C23 C 0.7476(4) 0.2443(2) 0.2227(3) 0.0671(11) Uani 1 d . . .
H23A H 0.7064 0.2179 0.1749 0.074 Uiso 1 calc R . .
H23B H 0.8137 0.2158 0.2570 0.074 Uiso 1 calc R . .
H23C H 0.7966 0.2838 0.2023 0.074 Uiso 1 calc R . .
C24 C 0.6758(3) 0.3082(2) 0.3496(2) 0.0567(10) Uani 1 d . . .
H24A H 0.5922 0.3194 0.3775 0.062 Uiso 1 calc R . .
H24B H 0.7214 0.3502 0.3338 0.062 Uiso 1 calc R . .
H24C H 0.7403 0.2818 0.3877 0.062 Uiso 1 calc R . .
O6 O -0.0031(2) 0.39552(9) 0.31871(12) 0.0337(4) Uani 1 d . . .
O7 O -0.00335(19) 0.49365(9) 0.25890(12) 0.0316(4) Uani 1 d . . .
N3 N -0.0615(2) 0.45277(11) 0.30697(15) 0.0334(5) Uani 1 d . . .
O8 O -0.1651(3) 0.46891(12) 0.33934(18) 0.0614(7) Uani 1 d . . .
O9 O 0.2840(2) 0.54713(10) 0.23305(12) 0.0409(5) Uani 1 d . . .
O10 O 0.1769(2) 0.50756(10) 0.12228(12) 0.0440(5) Uani 1 d . . .
N4 N 0.2330(2) 0.55783(11) 0.15958(14) 0.0272(5) Uani 1 d . . .
O11 O 0.2387(2) 0.61344(10) 0.12692(14) 0.0441(5) Uani 1 d . . .
O12 O 0.3637(2) 0.38957(14) 0.13859(14) 0.0559(6) Uani 1 d . . .
O13 O 0.4636(2) 0.42796(13) 0.25138(15) 0.0520(6) Uani 1 d . . .
N5 N 0.4761(3) 0.40010(11) 0.18204(15) 0.0340(6) Uani 1 d . . .
O14 O 0.5888(2) 0.38394(11) 0.15934(16) 0.0544(6) Uani 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Gd Gd -0.1653 3.9035 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Gd O1 64.79(5) . . ?
O2 Gd O7 119.98(6) . . ?
O1 Gd O7 118.70(6) . . ?
O2 Gd O12 72.03(8) . . ?
O1 Gd O12 99.27(8) . . ?
O7 Gd O12 141.91(8) . . ?
O2 Gd O13 96.66(7) . . ?
O1 Gd O13 70.93(7) . . ?
O7 Gd O13 143.07(7) . . ?
O12 Gd O13 50.45(8) . . ?
O2 Gd O6 77.05(6) . . ?
O1 Gd O6 75.78(6) . . ?
O7 Gd O6 51.62(6) . . ?
O12 Gd O6 147.53(7) . . ?
O13 Gd O6 145.41(7) . . ?
O2 Gd O10 122.42(6) . . ?
O1 Gd O10 163.83(7) . . ?
O7 Gd O10 71.87(7) . . ?
O12 Gd O10 71.85(9) . . ?
O13 Gd O10 93.28(8) . . ?
O6 Gd O10 119.04(7) . . ?
O2 Gd O4 63.24(5) . . ?
O1 Gd O4 125.43(5) . . ?
O7 Gd O4 75.96(6) . . ?
O12 Gd O4 79.76(7) . . ?
O13 Gd O4 130.20(7) . . ?
O6 Gd O4 77.67(6) . . ?
O10 Gd O4 67.36(6) . . ?
O2 Gd O9 162.60(7) . . ?
O1 Gd O9 119.09(6) . . ?
O7 Gd O9 74.32(7) . . ?
O12 Gd O9 90.59(8) . . ?
O13 Gd O9 70.62(8) . . ?
O6 Gd O9 120.19(7) . . ?
O10 Gd O9 49.34(6) . . ?
O4 Gd O9 115.48(6) . . ?
O2 Gd O3 125.28(5) . . ?
O1 Gd O3 63.39(5) . . ?
O7 Gd O3 73.18(6) . . ?
O12 Gd O3 132.54(7) . . ?
O13 Gd O3 82.30(7) . . ?
O6 Gd O3 74.56(6) . . ?
O10 Gd O3 112.23(6) . . ?
O4 Gd O3 147.17(6) . . ?
O9 Gd O3 66.18(6) . . ?
O2 Fe O1 77.99(6) . . ?
O2 Fe N2 88.84(7) . . ?
O1 Fe N2 159.20(8) . . ?
O2 Fe N1 156.09(8) . . ?
O1 Fe N1 88.75(7) . . ?
N2 Fe N1 97.52(8) . . ?
O2 Fe O5 107.47(7) . . ?
O1 Fe O5 112.59(7) . . ?
N2 Fe O5 86.58(8) . . ?
N1 Fe O5 95.94(8) . . ?
O2 Fe Gd 40.74(4) . . ?
O1 Fe Gd 40.95(4) . . ?
N2 Fe Gd 129.44(6) . . ?
N1 Fe Gd 129.69(6) . . ?
O5 Fe Gd 102.90(5) . . ?
C1 O1 Fe 129.31(14) . . ?
C1 O1 Gd 125.15(14) . . ?
Fe O1 Gd 105.19(7) . . ?
O1 C1 C6 123.8(2) . . ?
O1 C1 C2 118.3(2) . . ?
C6 C1 C2 117.9(2) . . ?
C3 C2 O3 124.1(2) . . ?
C3 C2 C1 121.9(2) . . ?
O3 C2 C1 114.0(2) . . ?
C2 C3 C4 119.8(2) . . ?
C5 C4 C3 119.7(2) . . ?
C4 C5 C6 121.4(2) . . ?
C1 C6 C5 119.2(2) . . ?
C1 C6 C7 124.2(2) . . ?
C5 C6 C7 116.7(2) . . ?
C2 O3 C20 115.48(19) . . ?
C2 O3 Gd 118.63(14) . . ?
C20 O3 Gd 125.74(15) . . ?
N1 C7 C6 127.4(2) . . ?
C7 N1 C8 115.8(2) . . ?
C7 N1 Fe 126.03(17) . . ?
C8 N1 Fe 118.13(15) . . ?
N1 C8 C9 114.7(2) . . ?
C10 C9 C19 111.3(2) . . ?
C10 C9 C8 112.1(2) . . ?
C19 C9 C8 111.6(2) . . ?
C10 C9 C18 106.0(2) . . ?
C19 C9 C18 109.8(2) . . ?
C8 C9 C18 105.7(2) . . ?
N2 C10 C9 113.9(2) . . ?
C17 N2 C10 115.5(2) . . ?
C17 N2 Fe 126.72(17) . . ?
C10 N2 Fe 117.71(15) . . ?
C11 O2 Fe 128.13(14) . . ?
C11 O2 Gd 124.78(14) . . ?
Fe O2 Gd 105.46(7) . . ?
O2 C11 C16 124.4(2) . . ?
O2 C11 C12 117.5(2) . . ?
C16 C11 C12 118.1(2) . . ?
C13 C12 O4 124.5(2) . . ?
C13 C12 C11 121.7(2) . . ?
O4 C12 C11 113.8(2) . . ?
C12 C13 C14 119.6(2) . . ?
C15 C14 C13 120.0(2) . . ?
C14 C15 C16 121.2(2) . . ?
C11 C16 C15 119.2(2) . . ?
C11 C16 C17 124.4(2) . . ?
C15 C16 C17 116.4(2) . . ?
C12 O4 C21 115.39(18) . . ?
C12 O4 Gd 118.60(13) . . ?
C21 O4 Gd 126.00(15) . . ?
N2 C17 C16 126.5(2) . . ?
C22 O5 Fe 135.9(2) . . ?
O5 C22 C24 121.2(3) . . ?
O5 C22 C23 120.6(3) . . ?
C24 C22 C23 118.2(3) . . ?
N3 O6 Gd 95.22(15) . . ?
N3 O7 Gd 96.75(14) . . ?
O8 N3 O6 122.9(2) . . ?
O8 N3 O7 121.2(2) . . ?
O6 N3 O7 115.9(2) . . ?
N4 O9 Gd 97.07(14) . . ?
N4 O10 Gd 97.80(14) . . ?
O11 N4 O10 122.5(2) . . ?
O11 N4 O9 121.8(2) . . ?
O10 N4 O9 115.6(2) . . ?
N5 O12 Gd 97.84(16) . . ?
N5 O13 Gd 96.50(16) . . ?
O14 N5 O12 122.7(3) . . ?
O14 N5 O13 122.5(3) . . ?
O12 N5 O13 114.8(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Gd O2 2.3813(16) . ?
Gd O1 2.3884(16) . ?
Gd O7 2.4545(18) . ?
Gd O12 2.464(2) . ?
Gd O13 2.489(2) . ?
Gd O6 2.494(2) . ?
Gd O10 2.5324(19) . ?
Gd O4 2.5394(17) . ?
Gd O9 2.5472(19) . ?
Gd O3 2.5605(17) . ?
Fe O2 2.0301(16) . ?
Fe O1 2.0305(16) . ?
Fe N2 2.066(2) . ?
Fe N1 2.074(2) . ?
Fe O5 2.1233(19) . ?
O1 C1 1.328(3) . ?
C1 C6 1.404(3) . ?
C1 C2 1.408(4) . ?
C2 C3 1.372(4) . ?
C2 O3 1.387(3) . ?
C3 C4 1.389(4) . ?
C4 C5 1.370(4) . ?
C5 C6 1.408(3) . ?
C6 C7 1.444(4) . ?
O3 C20 1.446(3) . ?
C7 N1 1.280(3) . ?
N1 C8 1.478(3) . ?
C8 C9 1.532(4) . ?
C9 C10 1.520(4) . ?
C9 C19 1.521(4) . ?
C9 C18 1.536(3) . ?
C10 N2 1.473(3) . ?
N2 C17 1.275(3) . ?
O2 C11 1.331(3) . ?
C11 C16 1.397(3) . ?
C11 C12 1.408(3) . ?
C12 C13 1.372(4) . ?
C12 O4 1.386(3) . ?
C13 C14 1.386(4) . ?
C14 C15 1.365(4) . ?
C15 C16 1.408(4) . ?
C16 C17 1.445(3) . ?
O4 C21 1.448(3) . ?
O5 C22 1.225(3) . ?
C22 C24 1.475(5) . ?
C22 C23 1.485(5) . ?
O6 N3 1.265(3) . ?
O7 N3 1.277(3) . ?
N3 O8 1.208(3) . ?
O9 N4 1.253(3) . ?
O10 N4 1.253(3) . ?
N4 O11 1.216(3) . ?
O12 N5 1.250(3) . ?
O13 N5 1.255(3) . ?
N5 O14 1.218(3) . ?
