#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:52:50 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179267 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/87/4318759.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4318759
loop_
_publ_author_name
'Franck Gascoin'
'Slavi C. Sevov'
_publ_section_title
;
 Synthesis and Characterization of K38Nb7As24 and Cs9Nb2As6: The First
 Mixed-Valence Transition-Metal Zintl Phases
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5920
_journal_page_last               5924
_journal_paper_doi               10.1021/ic020250b
_journal_volume                  41
_journal_year                    2002
_chemical_formula_moiety         K38Nb7As24
_chemical_formula_sum            'As24 K38 Nb7'
_chemical_formula_weight         3934.25
_chemical_name_common            K38Nb7As24
_chemical_name_systematic
;
   ?
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.4974(7)
_cell_length_b                   23.915(2)
_cell_length_c                   36.047(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      19.743
_cell_measurement_theta_min      11.698
_cell_volume                     9049.4(11)
_computing_cell_refinement       CAD4_(Enraf-Nonius,_1977)
_computing_data_collection       CAD4_(Enraf-Nonius,_1977)
_computing_data_reduction        SDS_Package_(Enraf-Nonius,_1985)
_computing_molecular_graphics    'SHELXTL (Siemens, 1994)'
_computing_publication_material  'SHELXTL (Siemens, 1994)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  Enraf_Nonius_Cad4
_diffrn_measurement_method       omega-2theta
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0808
_diffrn_reflns_av_sigmaI/netI    0.0951
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            8439
_diffrn_reflns_theta_full        24.99
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         2.04
_diffrn_standards_interval_count 200
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    11.329
_exptl_absorpt_correction_T_max  0.31929
_exptl_absorpt_correction_T_min  0.19819
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   'average of 4 psi-scans reflections'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.888
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             7204
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.08
_refine_diff_density_max         2.712
_refine_diff_density_min         -1.207
_refine_diff_density_rms         0.298
_refine_ls_extinction_coef       0.000004(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.008
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     194
_refine_ls_number_reflns         4295
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.008
_refine_ls_R_factor_all          0.1118
_refine_ls_R_factor_gt           0.0598
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0825P)²+6.2925P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1340
_refine_ls_wR_factor_ref         0.1570
_reflns_number_gt                2772
_reflns_number_total             4295
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic020250b_1.cif
_cod_data_source_block           k38nb7as24
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' tag value 'psi-scans' was replaced
with 'psi-scan' value.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        9049.2(11)
_cod_database_code               4318759
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Nb1 Nb 0.0000 -0.20461(6) 0.29376(5) 0.0177(4) Uani 1 2 d S . .
Nb2 Nb 0.5000 0.52333(6) 0.45359(5) 0.0184(4) Uani 1 2 d S . .
Nb3 Nb 0.0000 0.09695(9) 0.2500 0.0157(5) Uani 1 4 d S . .
Nb4 Nb 0.0000 0.32181(7) 0.42644(5) 0.0205(4) Uani 1 2 d S . .
As1 As 0.0000 -0.13068(8) 0.34058(6) 0.0261(5) Uani 1 2 d S . .
As2 As 0.0000 -0.30192(8) 0.31892(7) 0.0299(5) Uani 1 2 d S . .
As3 As -0.18799(18) -0.18473(7) 0.2500 0.0195(4) Uani 1 2 d S . .
As4 As 0.69290(14) 0.54296(5) 0.41730(4) 0.0261(3) Uani 1 1 d . . .
As5 As 0.5000 0.42657(7) 0.48407(6) 0.0232(5) Uani 1 2 d S . .
As6 As 0.20143(18) 0.03697(7) 0.2500 0.0236(4) Uani 1 2 d S . .
As7 As 0.0000 0.15914(8) 0.30541(5) 0.0226(5) Uani 1 2 d S . .
As8 As 0.0000 0.37165(8) 0.36453(6) 0.0249(5) Uani 1 2 d S . .
As9 As 0.0000 0.39381(9) 0.47567(6) 0.0316(5) Uani 1 2 d S . .
As10 As 0.20017(14) 0.26434(5) 0.43460(4) 0.0267(3) Uani 1 1 d . . .
K1 K 0.0000 -0.0678(2) 0.2500 0.0248(13) Uani 1 4 d S . .
K2 K 0.2512(4) 0.35065(14) 0.51587(12) 0.0557(11) Uani 1 1 d . . .
K3 K 0.2013(3) 0.26864(12) 0.34159(9) 0.0319(7) Uani 1 1 d . . .
K4 K 0.0000 0.16220(16) 0.40280(12) 0.0293(10) Uani 1 2 d S . .
K5 K 0.2812(3) -0.08028(13) 0.19281(9) 0.0350(8) Uani 1 1 d . . .
K6 K 0.2918(3) 0.39852(12) 0.41331(8) 0.0304(7) Uani 1 1 d . . .
K7 K 0.1927(4) 0.5000 0.5000 0.0266(9) Uani 1 2 d S . .
K8 K 0.2762(4) 0.18155(16) 0.2500 0.0272(10) Uani 1 2 d S . .
K9 K 0.0000 0.2752(3) 0.2500 0.0430(19) Uani 1 4 d S . .
K10 K 0.5000 0.0750(4) 0.2500 0.063(3) Uani 1 4 d S . .
K11 K 0.0000 0.01565(17) 0.34244(13) 0.0333(11) Uani 1 2 d S . .
K12 K 0.0000 0.4906(2) 0.41034(16) 0.0465(13) Uani 1 2 d S . .
K13 K 0.2698(3) 0.10574(14) 0.33685(10) 0.0446(9) Uani 1 1 d . . .
K14 K 0.0000 0.2400(3) 0.50788(15) 0.0583(16) Uani 1 2 d S . .
K15 K 0.0000 -0.2380(4) 0.39764(19) 0.080(2) Uani 1 2 d S . .
K16 K 0.0000 0.6345(8) 0.4221(5) 0.195(15) Uani 0.50 2 d SP . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nb Nb -2.0727 0.6215 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
As1 Nb1 As2 115.04(10) . . ?
As1 Nb1 As3 106.85(6) . 3 ?
As2 Nb1 As3 113.27(6) . 3 ?
As1 Nb1 As3 106.85(6) . . ?
As2 Nb1 As3 113.27(6) . . ?
As3 Nb1 As3 100.29(8) 3 . ?
As1 Nb1 Nb1 133.67(6) . 10_556 ?
As2 Nb1 Nb1 111.29(7) . 10_556 ?
As3 Nb1 Nb1 52.15(4) 3 10_556 ?
As3 Nb1 Nb1 52.15(4) . 10_556 ?
As1 Nb1 K1 69.41(7) . . ?
As2 Nb1 K1 175.55(9) . . ?
As3 Nb1 K1 64.34(5) 3 . ?
As3 Nb1 K1 64.34(5) . . ?
Nb1 Nb1 K1 64.26(4) 10_556 . ?
As1 Nb1 K3 78.46(6) . 16_545 ?
As2 Nb1 K3 70.36(6) . 16_545 ?
As3 Nb1 K3 70.20(6) 3 16_545 ?
As3 Nb1 K3 170.31(8) . 16_545 ?
Nb1 Nb1 K3 118.31(6) 10_556 16_545 ?
K1 Nb1 K3 111.38(6) . 16_545 ?
As1 Nb1 K3 78.46(6) . 5_445 ?
As2 Nb1 K3 70.36(6) . 5_445 ?
As3 Nb1 K3 170.31(8) 3 5_445 ?
As3 Nb1 K3 70.20(6) . 5_445 ?
Nb1 Nb1 K3 118.31(6) 10_556 5_445 ?
K1 Nb1 K3 111.38(6) . 5_445 ?
K3 Nb1 K3 119.23(11) 16_545 5_445 ?
As1 Nb1 K15 58.36(14) . . ?
As2 Nb1 K15 56.68(14) . . ?
As3 Nb1 K15 129.69(4) 3 . ?
As3 Nb1 K15 129.69(4) . . ?
Nb1 Nb1 K15 167.97(13) 10_556 . ?
K1 Nb1 K15 127.77(14) . . ?
K3 Nb1 K15 59.97(6) 16_545 . ?
K3 Nb1 K15 59.97(6) 5_445 . ?
As1 Nb1 K8 141.16(6) . 7_545 ?
As2 Nb1 K8 59.99(6) . 7_545 ?
As3 Nb1 K8 54.72(7) 3 7_545 ?
As3 Nb1 K8 109.93(7) . 7_545 ?
Nb1 Nb1 K8 66.31(3) 10_556 7_545 ?
K1 Nb1 K8 116.75(6) . 7_545 ?
K3 Nb1 K8 63.41(7) 16_545 7_545 ?
K3 Nb1 K8 125.77(8) 5_445 7_545 ?
K15 Nb1 K8 104.39(11) . 7_545 ?
As1 Nb1 K8 141.16(6) . 5_445 ?
As2 Nb1 K8 59.99(7) . 5_445 ?
As3 Nb1 K8 109.93(7) 3 5_445 ?
As3 Nb1 K8 54.73(7) . 5_445 ?
Nb1 Nb1 K8 66.31(3) 10_556 5_445 ?
K1 Nb1 K8 116.75(6) . 5_445 ?
K3 Nb1 K8 125.77(8) 16_545 5_445 ?
K3 Nb1 K8 63.41(7) 5_445 5_445 ?
K15 Nb1 K8 104.39(11) . 5_445 ?
K8 Nb1 K8 73.48(12) 7_545 5_445 ?
As4 Nb2 As4 111.07(9) . 12_655 ?
As4 Nb2 As5 112.34(6) . 9_666 ?
As4 Nb2 As5 112.34(6) 12_655 9_666 ?
As4 Nb2 As5 113.65(5) . . ?
As4 Nb2 As5 113.64(5) 12_655 . ?
As5 Nb2 As5 92.67(8) 9_666 . ?
As4 Nb2 K7 174.16(7) . . ?
As4 Nb2 K7 63.12(5) 12_655 . ?
As5 Nb2 K7 70.72(4) 9_666 . ?
As5 Nb2 K7 70.60(4) . . ?
As4 Nb2 K7 63.12(5) . 9_666 ?
As4 Nb2 K7 174.16(7) 12_655 9_666 ?
As5 Nb2 K7 70.72(4) 9_666 9_666 ?
As5 Nb2 K7 70.59(4) . 9_666 ?
K7 Nb2 K7 122.67(8) . 9_666 ?
As4 Nb2 K4 64.88(5) . 5 ?
As4 Nb2 K4 64.88(5) 12_655 5 ?
As5 Nb2 K4 90.80(9) 9_666 5 ?
As5 Nb2 K4 176.53(10) . 5 ?
K7 Nb2 K4 110.64(4) . 5 ?
K7 Nb2 K4 110.65(4) 9_666 5 ?
As4 Nb2 K6 59.70(6) . 12_655 ?
As4 Nb2 K6 113.72(8) 12_655 12_655 ?
As5 Nb2 K6 132.52(6) 9_666 12_655 ?
As5 Nb2 K6 58.55(6) . 12_655 ?
K7 Nb2 K6 122.33(6) . 12_655 ?
K7 Nb2 K6 64.52(5) 9_666 12_655 ?
K4 Nb2 K6 118.77(8) 5 12_655 ?
As4 Nb2 K6 113.72(8) . . ?
As4 Nb2 K6 59.70(6) 12_655 . ?
As5 Nb2 K6 132.52(6) 9_666 . ?
As5 Nb2 K6 58.55(6) . . ?
K7 Nb2 K6 64.52(5) . . ?
K7 Nb2 K6 122.33(6) 9_666 . ?
K4 Nb2 K6 118.77(8) 5 . ?
K6 Nb2 K6 66.72(10) 12_655 . ?
As4 Nb2 K11 58.45(5) . 5 ?
As4 Nb2 K11 58.44(5) 12_655 5 ?
As5 Nb2 K11 154.56(9) 9_666 5 ?
As5 Nb2 K11 112.77(9) . 5 ?
K7 Nb2 K11 116.59(4) . 5 ?
K7 Nb2 K11 116.59(4) 9_666 5 ?
K4 Nb2 K11 63.76(9) 5 5 ?
K6 Nb2 K11 66.46(7) 12_655 5 ?
K6 Nb2 K11 66.46(7) . 5 ?
As4 Nb2 K2 58.80(8) . 9_666 ?
As4 Nb2 K2 121.53(8) 12_655 9_666 ?
As5 Nb2 K2 54.72(7) 9_666 9_666 ?
As5 Nb2 K2 122.95(7) . 9_666 ?
K7 Nb2 K2 122.91(8) . 9_666 ?
K7 Nb2 K2 55.64(5) 9_666 9_666 ?
K4 Nb2 K2 59.37(7) 5 9_666 ?
K6 Nb2 K2 107.29(8) 12_655 9_666 ?
K6 Nb2 K2 172.53(9) . 9_666 ?
K11 Nb2 K2 107.41(8) 5 9_666 ?
As4 Nb2 K2 121.53(8) . 4_566 ?
As4 Nb2 K2 58.81(8) 12_655 4_566 ?
As5 Nb2 K2 54.72(7) 9_666 4_566 ?
As5 Nb2 K2 122.95(7) . 4_566 ?
K7 Nb2 K2 55.64(5) . 4_566 ?
K7 Nb2 K2 122.91(8) 9_666 4_566 ?
K4 Nb2 K2 59.37(7) 5 4_566 ?
K6 Nb2 K2 172.52(9) 12_655 4_566 ?
K6 Nb2 K2 107.29(8) . 4_566 ?
K11 Nb2 K2 107.41(8) 5 4_566 ?
K2 Nb2 K2 78.29(12) 9_666 4_566 ?
Nb3 Nb3 As7 0(10) 10_556 10_556 ?
Nb3 Nb3 As7 0(10) 10_556 . ?
As7 Nb3 As7 106.65(12) 10_556 . ?
Nb3 Nb3 As6 0(10) 10_556 . ?
As7 Nb3 As6 109.59(3) 10_556 . ?
As7 Nb3 As6 109.59(3) . . ?
Nb3 Nb3 As6 0(10) 10_556 3 ?
As7 Nb3 As6 109.59(3) 10_556 3 ?
As7 Nb3 As6 109.59(3) . 3 ?
As6 Nb3 As6 111.70(11) . 3 ?
Nb3 Nb3 K8 0(10) 10_556 3 ?
As7 Nb3 K8 70.02(5) 10_556 3 ?
As7 Nb3 K8 70.01(5) . 3 ?
As6 Nb3 K8 179.25(10) . 3 ?
As6 Nb3 K8 69.05(8) 3 3 ?
Nb3 Nb3 K8 0(6) 10_556 . ?
As7 Nb3 K8 70.01(5) 10_556 . ?
As7 Nb3 K8 70.02(5) . . ?
As6 Nb3 K8 69.05(8) . . ?
As6 Nb3 K8 179.25(10) 3 . ?
K8 Nb3 K8 110.19(14) 3 . ?
Nb3 Nb3 K11 0(10) 10_556 . ?
As7 Nb3 K11 173.58(10) 10_556 . ?
As7 Nb3 K11 66.93(8) . . ?
As6 Nb3 K11 73.57(5) . . ?
As6 Nb3 K11 73.56(5) 3 . ?
K8 Nb3 K11 106.76(4) 3 . ?
K8 Nb3 K11 106.76(4) . . ?
Nb3 Nb3 K11 0(10) 10_556 10_556 ?
As7 Nb3 K11 66.94(8) 10_556 10_556 ?
As7 Nb3 K11 173.59(10) . 10_556 ?
As6 Nb3 K11 73.57(5) . 10_556 ?
As6 Nb3 K11 73.57(5) 3 10_556 ?
K8 Nb3 K11 106.76(4) 3 10_556 ?
K8 Nb3 K11 106.76(4) . 10_556 ?
K11 Nb3 K11 119.48(14) . 10_556 ?
Nb3 Nb3 K1 0(10) 10_556 . ?
As7 Nb3 K1 126.68(6) 10_556 . ?
As7 Nb3 K1 126.67(6) . . ?
As6 Nb3 K1 55.85(6) . . ?
As6 Nb3 K1 55.85(6) 3 . ?
K8 Nb3 K1 124.90(7) 3 . ?
K8 Nb3 K1 124.90(7) . . ?
K11 Nb3 K1 59.74(7) . . ?
K11 Nb3 K1 59.74(7) 10_556 . ?
As9 Nb4 As10 107.16(6) . . ?
As9 Nb4 As10 107.16(6) . 12 ?
As10 Nb4 As10 112.44(9) . 12 ?
As9 Nb4 As8 107.76(9) . . ?
As10 Nb4 As8 111.03(6) . . ?
As10 Nb4 As8 111.03(6) 12 . ?
As9 Nb4 K14 77.82(12) . . ?
As10 Nb4 K14 66.52(6) . . ?
As10 Nb4 K14 66.52(6) 12 . ?
As8 Nb4 K14 174.43(13) . . ?
As9 Nb4 K6 74.91(6) . . ?
As10 Nb4 K6 65.50(6) . . ?
As10 Nb4 K6 177.58(8) 12 . ?
As8 Nb4 K6 69.15(6) . . ?
K14 Nb4 K6 113.07(7) . . ?
As9 Nb4 K6 74.91(6) . 12 ?
As10 Nb4 K6 177.58(8) . 12 ?
As10 Nb4 K6 65.50(6) 12 12 ?
As8 Nb4 K6 69.15(6) . 12 ?
K14 Nb4 K6 113.07(7) . 12 ?
K6 Nb4 K6 116.53(11) . 12 ?
As9 Nb4 K4 146.72(10) . . ?
As10 Nb4 K4 59.65(5) . . ?
As10 Nb4 K4 59.65(5) 12 . ?
As8 Nb4 K4 105.53(9) . . ?
K14 Nb4 K4 68.90(12) . . ?
K6 Nb4 K4 117.93(6) . . ?
K6 Nb4 K4 117.93(6) 12 . ?
As9 Nb4 K3 141.64(6) . . ?
As10 Nb4 K3 57.84(6) . . ?
As10 Nb4 K3 111.20(8) 12 . ?
As8 Nb4 K3 57.71(6) . . ?
K14 Nb4 K3 117.93(10) . . ?
K6 Nb4 K3 66.75(7) . . ?
K6 Nb4 K3 121.32(8) 12 . ?
K4 Nb4 K3 60.96(7) . . ?
As9 Nb4 K3 141.64(6) . 12 ?
As10 Nb4 K3 111.20(8) . 12 ?
As10 Nb4 K3 57.84(6) 12 12 ?
As8 Nb4 K3 57.71(6) . 12 ?
K14 Nb4 K3 117.92(10) . 12 ?
K6 Nb4 K3 121.32(8) . 12 ?
K6 Nb4 K3 66.75(7) 12 12 ?
K4 Nb4 K3 60.95(7) . 12 ?
K3 Nb4 K3 65.06(10) . 12 ?
As9 Nb4 K12 54.05(10) . . ?
As10 Nb4 K12 123.69(4) . . ?
As10 Nb4 K12 123.69(4) 12 . ?
As8 Nb4 K12 53.71(10) . . ?
K14 Nb4 K12 131.87(14) . . ?
K6 Nb4 K12 58.48(5) . . ?
K6 Nb4 K12 58.48(5) 12 . ?
K4 Nb4 K12 159.23(11) . . ?
K3 Nb4 K12 102.10(9) . . ?
K3 Nb4 K12 102.10(9) 12 . ?
Nb1 As1 K15 82.38(15) . . ?
Nb1 As1 K5 90.69(7) . 10_556 ?
K15 As1 K5 119.79(6) . 10_556 ?
Nb1 As1 K5 90.69(7) . 3 ?
K15 As1 K5 119.79(6) . 3 ?
K5 As1 K5 120.03(12) 10_556 3 ?
Nb1 As1 K6 131.65(7) . 16_545 ?
K15 As1 K6 71.68(12) . 16_545 ?
K5 As1 K6 69.60(8) 10_556 16_545 ?
K5 As1 K6 137.57(9) 3 16_545 ?
Nb1 As1 K6 131.65(7) . 5_445 ?
K15 As1 K6 71.68(12) . 5_445 ?
K5 As1 K6 137.57(9) 10_556 5_445 ?
K5 As1 K6 69.60(8) 3 5_445 ?
K6 As1 K6 77.70(11) 16_545 5_445 ?
Nb1 As1 K11 137.43(12) . . ?
K15 As1 K11 140.18(17) . . ?
K5 As1 K11 69.71(7) 10_556 . ?
K5 As1 K11 69.71(7) 3 . ?
K6 As1 K11 77.59(8) 16_545 . ?
K6 As1 K11 77.59(8) 5_445 . ?
Nb1 As1 K1 71.06(10) . . ?
K15 As1 K1 153.44(17) . . ?
K5 As1 K1 62.05(6) 10_556 . ?
K5 As1 K1 62.05(6) 3 . ?
K6 As1 K1 126.85(8) 16_545 . ?
K6 As1 K1 126.85(8) 5_445 . ?
K11 As1 K1 66.38(12) . . ?
Nb1 As1 K3 64.27(6) . 16_545 ?
K15 As1 K3 61.26(8) . 16_545 ?
K5 As1 K3 62.07(7) 10_556 16_545 ?
K5 As1 K3 154.90(9) 3 16_545 ?
K6 As1 K3 67.52(7) 16_545 16_545 ?
K6 As1 K3 127.79(9) 5_445 16_545 ?
K11 As1 K3 127.49(5) . 16_545 ?
K1 As1 K3 105.25(7) . 16_545 ?
Nb1 As1 K3 64.27(6) . 5_445 ?
K15 As1 K3 61.26(8) . 5_445 ?
K5 As1 K3 154.90(9) 10_556 5_445 ?
K5 As1 K3 62.07(7) 3 5_445 ?
K6 As1 K3 127.79(9) 16_545 5_445 ?
K6 As1 K3 67.52(7) 5_445 5_445 ?
K11 As1 K3 127.49(5) . 5_445 ?
K1 As1 K3 105.25(7) . 5_445 ?
K3 As1 K3 104.96(10) 16_545 5_445 ?
Nb1 As2 K15 82.96(16) . . ?
Nb1 As2 K13 133.40(6) . 16_545 ?
K15 As2 K13 98.26(13) . 16_545 ?
Nb1 As2 K13 133.40(6) . 5_445 ?
K15 As2 K13 98.26(13) . 5_445 ?
K13 As2 K13 92.80(13) 16_545 5_445 ?
Nb1 As2 K8 81.08(8) . 7_545 ?
K15 As2 K8 133.62(8) . 7_545 ?
K13 As2 K8 64.50(8) 16_545 7_545 ?
K13 As2 K8 123.91(11) 5_445 7_545 ?
Nb1 As2 K8 81.08(8) . 5_445 ?
K15 As2 K8 133.62(8) . 5_445 ?
K13 As2 K8 123.91(11) 16_545 5_445 ?
K13 As2 K8 64.50(8) 5_445 5_445 ?
K8 As2 K8 86.08(12) 7_545 5_445 ?
Nb1 As2 K3 69.57(6) . 16_545 ?
K15 As2 K3 65.42(7) . 16_545 ?
K13 As2 K3 68.95(8) 16_545 16_545 ?
K13 As2 K3 152.12(10) 5_445 16_545 ?
K8 As2 K3 68.20(8) 7_545 16_545 ?
K8 As2 K3 143.15(10) 5_445 16_545 ?
Nb1 As2 K3 69.57(6) . 5_445 ?
K15 As2 K3 65.42(7) . 5_445 ?
K13 As2 K3 152.12(10) 16_545 5_445 ?
K13 As2 K3 68.95(8) 5_445 5_445 ?
K8 As2 K3 143.15(10) 7_545 5_445 ?
K8 As2 K3 68.20(8) 5_445 5_445 ?
K3 As2 K3 118.26(11) 16_545 5_445 ?
Nb1 As2 K10 118.54(12) . 5_445 ?
K15 As2 K10 158.50(18) . 5_445 ?
K13 As2 K10 67.61(9) 16_545 5_445 ?
K13 As2 K10 67.61(9) 5_445 5_445 ?
K8 As2 K10 56.40(9) 7_545 5_445 ?
K8 As2 K10 56.40(9) 5_445 5_445 ?
K3 As2 K10 119.81(6) 16_545 5_445 ?
K3 As2 K10 119.81(6) 5_445 5_445 ?
Nb1 As3 Nb1 75.70(8) 10_556 . ?
Nb1 As3 K8 84.60(8) 10_556 5_445 ?
Nb1 As3 K8 84.60(8) . 5_445 ?
Nb1 As3 K5 89.13(7) 10_556 12 ?
Nb1 As3 K5 137.09(9) . 12 ?
K8 As3 K5 134.39(8) 5_445 12 ?
Nb1 As3 K5 137.10(9) 10_556 3 ?
Nb1 As3 K5 89.12(7) . 3 ?
K8 As3 K5 134.39(8) 5_445 3 ?
K5 As3 K5 75.08(11) 12 3 ?
Nb1 As3 K9 133.23(8) 10_556 5_445 ?
Nb1 As3 K9 133.22(8) . 5_445 ?
K8 As3 K9 67.00(14) 5_445 5_445 ?
K5 As3 K9 85.96(11) 12 5_445 ?
K5 As3 K9 85.96(11) 3 5_445 ?
Nb1 As3 K1 73.05(7) 10_556 . ?
Nb1 As3 K1 73.05(7) . . ?
K8 As3 K1 151.48(11) 5_445 . ?
K5 As3 K1 64.13(7) 12 . ?
K5 As3 K1 64.13(7) 3 . ?
K9 As3 K1 141.51(13) 5_445 . ?
Nb1 As3 K3 68.62(6) 10_556 14_446 ?
Nb1 As3 K3 137.59(8) . 14_446 ?
K8 As3 K3 70.22(6) 5_445 14_446 ?
K5 As3 K3 65.48(7) 12 14_446 ?
K5 As3 K3 132.86(9) 3 14_446 ?
K9 As3 K3 67.11(6) 5_445 14_446 ?
K1 As3 K3 115.50(5) . 14_446 ?
Nb1 As3 K3 137.58(8) 10_556 5_445 ?
Nb1 As3 K3 68.61(6) . 5_445 ?
K8 As3 K3 70.22(6) 5_445 5_445 ?
K5 As3 K3 132.85(9) 12 5_445 ?
K5 As3 K3 65.48(7) 3 5_445 ?
K9 As3 K3 67.11(6) 5_445 5_445 ?
K1 As3 K3 115.50(5) . 5_445 ?
K3 As3 K3 127.97(11) 14_446 5_445 ?
Nb2 As4 K13 137.94(9) . 5 ?
Nb2 As4 K7 76.39(8) . 9_666 ?
K13 As4 K7 144.31(10) 5 9_666 ?
Nb2 As4 K11 84.04(7) . 5 ?
K13 As4 K11 63.21(9) 5 5 ?
K7 As4 K11 147.74(9) 9_666 5 ?
Nb2 As4 K6 82.51(7) . 12_655 ?
K13 As4 K6 113.48(9) 5 12_655 ?
K7 As4 K6 73.53(6) 9_666 12_655 ?
K11 As4 K6 78.75(9) 5 12_655 ?
Nb2 As4 K12 137.40(10) . 1_655 ?
K13 As4 K12 82.85(11) 5 1_655 ?
K7 As4 K12 67.86(12) 9_666 1_655 ?
K11 As4 K12 114.99(11) 5 1_655 ?
K6 As4 K12 66.02(10) 12_655 1_655 ?
Nb2 As4 K4 76.16(7) . 5 ?
K13 As4 K4 69.53(9) 5 5 ?
K7 As4 K4 125.44(9) 9_666 5 ?
K11 As4 K4 72.53(9) 5 5 ?
K6 As4 K4 145.61(8) 12_655 5 ?
K12 As4 K4 144.38(10) 1_655 5 ?
Nb2 As4 K2 84.94(9) . 9_666 ?
K13 As4 K2 103.03(10) 5 9_666 ?
K7 As4 K2 63.91(6) 9_666 9_666 ?
K11 As4 K2 139.98(10) 5 9_666 ?
K6 As4 K2 137.34(9) 12_655 9_666 ?
K12 As4 K2 98.87(12) 1_655 9_666 ?
K4 As4 K2 67.49(9) 5 9_666 ?
Nb2 As4 K16 139.9(3) . 1_655 ?
K13 As4 K16 65.8(3) 5 1_655 ?
K7 As4 K16 80.7(3) 9_666 1_655 ?
K11 As4 K16 128.9(3) 5 1_655 ?
K6 As4 K16 121.6(3) 12_655 1_655 ?
K12 As4 K16 55.8(3) 1_655 1_655 ?
K4 As4 K16 91.6(3) 5 1_655 ?
K2 As4 K16 55.4(3) 9_666 1_655 ?
Nb2 As5 Nb2 87.33(8) 9_666 . ?
Nb2 As5 K2 87.33(9) 9_666 . ?
Nb2 As5 K2 129.09(7) . . ?
Nb2 As5 K2 87.33(9) 9_666 12_655 ?
Nb2 As5 K2 129.09(7) . 12_655 ?
K2 As5 K2 101.15(13) . 12_655 ?
Nb2 As5 K6 138.53(6) 9_666 . ?
Nb2 As5 K6 81.81(7) . . ?
K2 As5 K6 69.79(9) . . ?
K2 As5 K6 129.81(11) 12_655 . ?
Nb2 As5 K6 138.53(6) 9_666 12_655 ?
Nb2 As5 K6 81.81(7) . 12_655 ?
K2 As5 K6 129.80(11) . 12_655 ?
K2 As5 K6 69.79(9) 12_655 12_655 ?
K6 As5 K6 79.28(11) . 12_655 ?
Nb2 As5 K7 68.99(4) 9_666 . ?
Nb2 As5 K7 68.87(4) . . ?
K2 As5 K7 62.03(7) . . ?
K2 As5 K7 150.64(9) 12_655 . ?
K6 As5 K7 69.75(6) . . ?
K6 As5 K7 139.57(8) 12_655 . ?
Nb2 As5 K7 68.99(4) 9_666 9_666 ?
Nb2 As5 K7 68.87(4) . 9_666 ?
K2 As5 K7 150.64(9) . 9_666 ?
K2 As5 K7 62.03(7) 12_655 9_666 ?
K6 As5 K7 139.57(8) . 9_666 ?
K6 As5 K7 69.76(6) 12_655 9_666 ?
K7 As5 K7 120.39(8) . 9_666 ?
Nb3 As6 Nb3 0.0 10_556 . ?
Nb3 As6 K10 129.67(16) 10_556 . ?
Nb3 As6 K10 129.67(16) . . ?
Nb3 As6 K1 83.99(9) 10_556 . ?
Nb3 As6 K1 83.99(9) . . ?
K10 As6 K1 146.34(17) . . ?
Nb3 As6 K8 68.65(9) 10_556 . ?
Nb3 As6 K8 68.65(9) . . ?
K10 As6 K8 61.02(17) . . ?
K1 As6 K8 152.64(11) . . ?
Nb3 As6 K5 129.30(8) 10_556 . ?
Nb3 As6 K5 129.30(8) . . ?
K10 As6 K5 89.63(14) . . ?
K1 As6 K5 63.40(7) . . ?
K8 As6 K5 135.40(8) . . ?
Nb3 As6 K5 129.30(8) 10_556 10_556 ?
Nb3 As6 K5 129.30(8) . 10_556 ?
K10 As6 K5 89.63(14) . 10_556 ?
K1 As6 K5 63.40(7) . 10_556 ?
K8 As6 K5 135.40(8) . 10_556 ?
K5 As6 K5 70.33(11) . 10_556 ?
Nb3 As6 K13 84.77(7) 10_556 10_556 ?
Nb3 As6 K13 84.77(7) . 10_556 ?
K10 As6 K13 71.45(9) . 10_556 ?
K1 As6 K13 118.47(6) . 10_556 ?
K8 As6 K13 60.76(6) . 10_556 ?
K5 As6 K13 79.09(7) . 10_556 ?
K5 As6 K13 144.10(9) 10_556 10_556 ?
Nb3 As6 K13 84.77(7) 10_556 . ?
Nb3 As6 K13 84.77(7) . . ?
K10 As6 K13 71.45(9) . . ?
K1 As6 K13 118.47(6) . . ?
K8 As6 K13 60.76(6) . . ?
K5 As6 K13 144.10(9) . . ?
K5 As6 K13 79.09(7) 10_556 . ?
K13 As6 K13 120.36(11) 10_556 . ?
Nb3 As6 K11 68.42(6) 10_556 . ?
Nb3 As6 K11 68.42(6) . . ?
K10 As6 K11 123.09(5) . . ?
K1 As6 K11 63.86(6) . . ?
K8 As6 K11 104.04(8) . . ?
K5 As6 K11 120.41(9) . . ?
K5 As6 K11 62.72(8) 10_556 . ?
K13 As6 K11 152.96(9) 10_556 . ?
K13 As6 K11 55.78(7) . . ?
Nb3 As6 K11 68.42(6) 10_556 10_556 ?
Nb3 As6 K11 68.42(6) . 10_556 ?
K10 As6 K11 123.09(5) . 10_556 ?
K1 As6 K11 63.86(6) . 10_556 ?
K8 As6 K11 104.04(8) . 10_556 ?
K5 As6 K11 62.72(8) . 10_556 ?
K5 As6 K11 120.42(9) 10_556 10_556 ?
K13 As6 K11 55.78(7) 10_556 10_556 ?
K13 As6 K11 152.96(9) . 10_556 ?
K11 As6 K11 113.73(9) . 10_556 ?
Nb3 As7 Nb3 0.00(8) 10_556 . ?
Nb3 As7 K13 92.53(8) 10_556 12 ?
Nb3 As7 K13 92.53(8) . 12 ?
Nb3 As7 K13 92.53(8) 10_556 . ?
Nb3 As7 K13 92.53(8) . . ?
K13 As7 K13 117.84(13) 12 . ?
Nb3 As7 K9 90.94(10) 10_556 . ?
Nb3 As7 K9 90.94(10) . . ?
K13 As7 K9 120.90(6) 12 . ?
K13 As7 K9 120.90(6) . . ?
Nb3 As7 K4 144.52(10) 10_556 . ?
Nb3 As7 K4 144.52(10) . . ?
K13 As7 K4 70.46(8) 12 . ?
K13 As7 K4 70.46(8) . . ?
K9 As7 K4 124.54(11) . . ?
Nb3 As7 K8 68.91(6) 10_556 3 ?
Nb3 As7 K8 68.91(6) . 3 ?
K13 As7 K8 63.44(8) 12 3 ?
K13 As7 K8 161.36(10) . 3 ?
K9 As7 K8 63.28(7) . 3 ?
K4 As7 K8 123.88(5) . 3 ?
Nb3 As7 K8 68.91(6) 10_556 . ?
Nb3 As7 K8 68.91(6) . . ?
K13 As7 K8 161.36(10) 12 . ?
K13 As7 K8 63.45(8) . . ?
K9 As7 K8 63.28(7) . . ?
K4 As7 K8 123.88(5) . . ?
K8 As7 K8 109.02(10) 3 . ?
Nb3 As7 K3 136.33(7) 10_556 12 ?
Nb3 As7 K3 136.33(7) . 12 ?
K13 As7 K3 69.82(8) 12 12 ?
K13 As7 K3 131.13(10) . 12 ?
K9 As7 K3 67.79(8) . 12 ?
K4 As7 K3 67.88(8) . 12 ?
K8 As7 K3 67.47(7) 3 12 ?
K8 As7 K3 124.76(9) . 12 ?
Nb3 As7 K3 136.33(7) 10_556 . ?
Nb3 As7 K3 136.33(7) . . ?
K13 As7 K3 131.13(10) 12 . ?
K13 As7 K3 69.82(8) . . ?
K9 As7 K3 67.79(8) . . ?
K4 As7 K3 67.89(8) . . ?
K8 As7 K3 124.76(9) 3 . ?
K8 As7 K3 67.47(7) . . ?
K3 As7 K3 71.67(10) 12 . ?
Nb3 As7 K11 74.58(9) 10_556 . ?
Nb3 As7 K11 74.58(9) . . ?
K13 As7 K11 61.05(6) 12 . ?
K13 As7 K11 61.05(6) . . ?
K9 As7 K11 165.53(11) . . ?
K4 As7 K11 69.94(10) . . ?
K8 As7 K11 110.09(8) 3 . ?
K8 As7 K11 110.09(8) . . ?
K3 As7 K11 123.04(8) 12 . ?
K3 As7 K11 123.04(8) . . ?
Nb4 As8 K12 87.98(12) . . ?
Nb4 As8 K5 135.83(6) . 7 ?
K12 As8 K5 90.76(10) . 7 ?
Nb4 As8 K5 135.83(6) . 14_456 ?
K12 As8 K5 90.76(10) . 14_456 ?
K5 As8 K5 88.32(13) 7 14_456 ?
Nb4 As8 K3 82.61(7) . . ?
K12 As8 K3 139.48(7) . . ?
K5 As8 K3 70.26(8) 7 . ?
K5 As8 K3 122.76(10) 14_456 . ?
Nb4 As8 K3 82.60(8) . 12 ?
K12 As8 K3 139.48(7) . 12 ?
K5 As8 K3 122.76(10) 7 12 ?
K5 As8 K3 70.26(8) 14_456 12 ?
K3 As8 K3 78.22(12) . 12 ?
Nb4 As8 K6 69.66(6) . . ?
K12 As8 K6 66.38(7) . . ?
K5 As8 K6 69.52(8) 7 . ?
K5 As8 K6 147.04(9) 14_456 . ?
K3 As8 K6 73.40(7) . . ?
K3 As8 K6 142.27(9) 12 . ?
Nb4 As8 K6 69.66(6) . 12 ?
K12 As8 K6 66.38(7) . 12 ?
K5 As8 K6 147.04(9) 7 12 ?
K5 As8 K6 69.52(8) 14_456 12 ?
K3 As8 K6 142.27(9) . 12 ?
K3 As8 K6 73.40(7) 12 12 ?
K6 As8 K6 117.15(11) . 12 ?
Nb4 As9 K2 95.80(9) . . ?
Nb4 As9 K2 95.80(9) . 12 ?
K2 As9 K2 111.99(16) . 12 ?
Nb4 As9 K12 88.64(13) . . ?
K2 As9 K12 123.52(8) . . ?
K2 As9 K12 123.53(8) 12 . ?
Nb4 As9 K7 135.48(7) . 9_566 ?
K2 As9 K7 128.67(11) . 9_566 ?
K2 As9 K7 68.13(8) 12 9_566 ?
K12 As9 K7 69.93(9) . 9_566 ?
Nb4 As9 K7 135.48(7) . . ?
K2 As9 K7 68.13(8) . . ?
K2 As9 K7 128.67(11) 12 . ?
K12 As9 K7 69.92(9) . . ?
K7 As9 K7 73.96(13) 9_566 . ?
Nb4 As9 K16 125.4(3) . 9_566 ?
K2 As9 K16 59.56(12) . 9_566 ?
K2 As9 K16 59.55(12) 12 9_566 ?
K12 As9 K16 145.9(3) . 9_566 ?
K7 As9 K16 83.1(2) 9_566 9_566 ?
K7 As9 K16 83.1(2) . 9_566 ?
Nb4 As9 K6 66.19(6) . . ?
K2 As9 K6 67.10(9) . . ?
K2 As9 K6 161.28(11) 12 . ?
K12 As9 K6 63.73(7) . . ?
K7 As9 K6 128.07(9) 9_566 . ?
K7 As9 K6 69.33(7) . . ?
K16 As9 K6 125.94(6) 9_566 . ?
Nb4 As9 K6 66.19(6) . 12 ?
K2 As9 K6 161.27(11) . 12 ?
K2 As9 K6 67.10(9) 12 12 ?
K12 As9 K6 63.73(7) . 12 ?
K7 As9 K6 69.33(7) 9_566 12 ?
K7 As9 K6 128.07(9) . 12 ?
K16 As9 K6 125.94(6) 9_566 12 ?
K6 As9 K6 107.39(11) . 12 ?
Nb4 As9 K14 63.38(10) . . ?
K2 As9 K14 63.48(8) . . ?
K2 As9 K14 63.48(8) 12 . ?
K12 As9 K14 152.02(15) . . ?
K7 As9 K14 129.91(8) 9_566 . ?
K7 As9 K14 129.91(8) . . ?
K16 As9 K14 62.1(3) 9_566 . ?
K6 As9 K14 101.91(8) . . ?
K6 As9 K14 101.91(8) 12 . ?
Nb4 As10 K2 129.86(10) . 13_556 ?
Nb4 As10 K3 82.52(8) . . ?
K2 As10 K3 124.24(10) 13_556 . ?
Nb4 As10 K15 136.78(14) . 5 ?
K2 As10 K15 93.14(15) 13_556 5 ?
K3 As10 K15 66.90(12) . 5 ?
Nb4 As10 K4 80.71(7) . . ?
K2 As10 K4 71.51(10) 13_556 . ?
K3 As10 K4 71.88(10) . . ?
K15 As10 K4 115.06(15) 5 . ?
Nb4 As10 K14 70.87(9) . . ?
K2 As10 K14 62.52(12) 13_556 . ?
K3 As10 K14 141.09(10) . . ?
K15 As10 K14 149.63(13) 5 . ?
K4 As10 K14 76.12(12) . . ?
Nb4 As10 K6 72.49(7) . . ?
K2 As10 K6 148.31(10) 13_556 . ?
K3 As10 K6 75.36(8) . . ?
K15 As10 K6 70.74(15) 5 . ?
K4 As10 K6 139.82(10) . . ?
K14 As10 K6 120.18(12) . . ?
Nb4 As10 K2 84.68(8) . . ?
K2 As10 K2 90.82(9) 13_556 . ?
K3 As10 K2 142.20(9) . . ?
K15 As10 K2 100.84(14) 5 . ?
K4 As10 K2 140.24(10) . . ?
K14 As10 K2 64.16(12) . . ?
K6 As10 K2 66.88(8) . . ?
Nb4 As10 K14 140.61(11) . 13_556 ?
K2 As10 K14 63.44(11) 13_556 13_556 ?
K3 As10 K14 123.20(10) . 13_556 ?
K15 As10 K14 56.31(13) 5 13_556 ?
K4 As10 K14 132.65(12) . 13_556 ?
K14 As10 K14 94.78(4) . 13_556 ?
K6 As10 K14 85.12(11) . 13_556 ?
K2 As10 K14 56.47(11) . 13_556 ?
As6 K1 As6 80.31(13) 3 . ?
As6 K1 As3 104.63(5) 3 . ?
As6 K1 As3 175.06(12) . . ?
As6 K1 As3 175.06(12) 3 3 ?
As6 K1 As3 104.63(5) . 3 ?
As3 K1 As3 70.43(12) . 3 ?
As6 K1 As1 108.64(5) 3 10_556 ?
As6 K1 As1 108.64(5) . 10_556 ?
As3 K1 As1 70.02(8) . 10_556 ?
As3 K1 As1 70.02(8) 3 10_556 ?
As6 K1 As1 108.64(5) 3 . ?
As6 K1 As1 108.64(5) . . ?
As3 K1 As1 70.02(8) . . ?
As3 K1 As1 70.02(8) 3 . ?
As1 K1 As1 130.56(16) 10_556 . ?
As6 K1 K5 126.16(13) 3 . ?
As6 K1 K5 62.36(6) . . ?
As3 K1 K5 113.82(13) . . ?
As3 K1 K5 57.42(7) 3 . ?
As1 K1 K5 56.45(6) 10_556 . ?
As1 K1 K5 118.93(9) . . ?
As6 K1 K5 62.36(6) 3 12 ?
As6 K1 K5 126.15(13) . 12 ?
As3 K1 K5 57.41(7) . 12 ?
As3 K1 K5 113.82(13) 3 12 ?
As1 K1 K5 56.44(6) 10_556 12 ?
As1 K1 K5 118.93(9) . 12 ?
K5 K1 K5 109.59(11) . 12 ?
As6 K1 K5 126.15(13) 3 10_556 ?
As6 K1 K5 62.36(6) . 10_556 ?
As3 K1 K5 113.82(13) . 10_556 ?
As3 K1 K5 57.41(7) 3 10_556 ?
As1 K1 K5 118.93(9) 10_556 10_556 ?
As1 K1 K5 56.44(6) . 10_556 ?
K5 K1 K5 69.58(11) . 10_556 ?
K5 K1 K5 170.54(19) 12 10_556 ?
As6 K1 K5 62.36(6) 3 3 ?
As6 K1 K5 126.15(13) . 3 ?
As3 K1 K5 57.42(7) . 3 ?
As3 K1 K5 113.81(13) 3 3 ?
As1 K1 K5 118.93(9) 10_556 3 ?
As1 K1 K5 56.44(6) . 3 ?
K5 K1 K5 170.54(19) . 3 ?
K5 K1 K5 69.58(11) 12 3 ?
K5 K1 K5 109.59(11) 10_556 3 ?
As6 K1 Nb1 133.50(4) 3 . ?
As6 K1 Nb1 133.51(4) . . ?
As3 K1 Nb1 42.62(6) . . ?
As3 K1 Nb1 42.62(6) 3 . ?
As1 K1 Nb1 91.02(12) 10_556 . ?
As1 K1 Nb1 39.53(6) . . ?
K5 K1 Nb1 100.00(11) . . ?
K5 K1 Nb1 99.99(11) 12 . ?
K5 K1 Nb1 71.21(8) 10_556 . ?
K5 K1 Nb1 71.21(8) 3 . ?
As6 K1 Nb1 133.51(4) 3 10_556 ?
As6 K1 Nb1 133.51(4) . 10_556 ?
As3 K1 Nb1 42.62(6) . 10_556 ?
As3 K1 Nb1 42.62(6) 3 10_556 ?
As1 K1 Nb1 39.54(6) 10_556 10_556 ?
As1 K1 Nb1 91.02(12) . 10_556 ?
K5 K1 Nb1 71.21(8) . 10_556 ?
K5 K1 Nb1 71.21(8) 12 10_556 ?
K5 K1 Nb1 99.99(11) 10_556 10_556 ?
K5 K1 Nb1 99.99(11) 3 10_556 ?
Nb1 K1 Nb1 51.49(9) . 10_556 ?
As9 K2 As10 129.90(13) . 13_556 ?
As9 K2 As5 108.16(11) . . ?
As10 K2 As5 120.58(12) 13_556 . ?
As9 K2 K16 68.3(3) . 9_566 ?
As10 K2 K16 81.7(3) 13_556 9_566 ?
As5 K2 K16 138.5(3) . 9_566 ?
As9 K2 K14 135.07(17) . 13_556 ?
As10 K2 K14 60.24(11) 13_556 13_556 ?
As5 K2 K14 70.94(12) . 13_556 ?
K16 K2 K14 141.9(4) 9_566 13_556 ?
As9 K2 As4 102.32(12) . 9_666 ?
As10 K2 As4 101.73(11) 13_556 9_666 ?
As5 K2 As4 73.61(8) . 9_666 ?
K16 K2 As4 67.4(3) 9_566 9_666 ?
K14 K2 As4 119.10(14) 13_556 9_666 ?
As9 K2 As10 72.18(9) . . ?
As10 K2 As10 89.18(9) 13_556 . ?
As5 K2 As10 98.40(12) . . ?
K16 K2 As10 117.8(3) 9_566 . ?
K14 K2 As10 63.88(11) 13_556 . ?
As4 K2 As10 168.70(12) 9_666 . ?
As9 K2 K7 58.29(9) . . ?
As10 K2 K7 156.40(14) 13_556 . ?
As5 K2 K7 63.49(9) . . ?
K16 K2 K7 82.8(4) 9_566 . ?
K14 K2 K7 133.61(16) 13_556 . ?
As4 K2 K7 55.67(6) 9_666 . ?
As10 K2 K7 113.81(10) . . ?
As9 K2 K14 67.08(10) . . ?
As10 K2 K14 64.17(10) 13_556 . ?
As5 K2 K14 153.75(17) . . ?
K16 K2 K14 65.6(3) 9_566 . ?
K14 K2 K14 93.95(9) 13_556 . ?
As4 K2 K14 132.38(16) 9_666 . ?
As10 K2 K14 55.35(10) . . ?
K7 K2 K14 123.89(14) . . ?
As9 K2 K6 64.08(9) . . ?
As10 K2 K6 137.54(14) 13_556 . ?
As5 K2 K6 55.64(8) . . ?
K16 K2 K6 131.6(3) 9_566 . ?
K14 K2 K6 82.43(14) 13_556 . ?
As4 K2 K6 114.53(10) 9_666 . ?
As10 K2 K6 54.27(7) . . ?
K7 K2 K6 65.42(7) . . ?
K14 K2 K6 102.22(13) . . ?
As9 K2 K4 156.08(16) . 13_556 ?
As10 K2 K4 55.44(8) 13_556 13_556 ?
As5 K2 K4 77.42(10) . 13_556 ?
K16 K2 K4 91.8(3) 9_566 13_556 ?
K14 K2 K4 68.84(12) 13_556 13_556 ?
As4 K2 K4 56.06(8) 9_666 13_556 ?
As10 K2 K4 130.96(13) . 13_556 ?
K7 K2 K4 107.64(12) . 13_556 ?
K14 K2 K4 117.96(13) . 13_556 ?
K6 K2 K4 131.09(13) . 13_556 ?
As9 K2 Nb2 114.09(10) . 9_666 ?
As10 K2 Nb2 111.32(10) 13_556 9_666 ?
As5 K2 Nb2 37.94(5) . 9_666 ?
K16 K2 Nb2 103.5(3) 9_566 9_666 ?
K14 K2 Nb2 92.60(12) 13_556 9_666 ?
As4 K2 Nb2 36.25(5) 9_666 9_666 ?
As10 K2 Nb2 136.35(13) . 9_666 ?
K7 K2 Nb2 55.80(8) . 9_666 ?
K14 K2 Nb2 168.29(16) . 9_666 ?
K6 K2 Nb2 88.24(9) . 9_666 ?
K4 K2 Nb2 55.96(8) 13_556 9_666 ?
As8 K3 As10 76.91(8) . . ?
As8 K3 As7 104.70(9) . . ?
As10 K3 As7 109.69(9) . . ?
As8 K3 Nb1 122.13(9) . 5 ?
As10 K3 Nb1 118.83(10) . 5 ?
As7 K3 Nb1 117.47(9) . 5 ?
As8 K3 As2 159.45(11) . 5 ?
As10 K3 As2 102.25(9) . 5 ?
As7 K3 As2 94.96(8) . 5 ?
Nb1 K3 As2 40.08(5) 5 5 ?
As8 K3 As3 101.44(9) . 5 ?
As10 K3 As3 155.32(11) . 5 ?
As7 K3 As3 94.63(8) . 5 ?
Nb1 K3 As3 41.18(5) 5 5 ?
As2 K3 As3 70.59(7) 5 5 ?
As8 K3 K15 115.30(15) . 5 ?
As10 K3 K15 57.37(11) . 5 ?
As7 K3 K15 131.04(16) . 5 ?
Nb1 K3 K15 62.58(11) 5 5 ?
As2 K3 K15 51.72(12) 5 5 ?
As3 K3 K15 103.49(12) 5 5 ?
As8 K3 K5 54.23(7) . 7 ?
As10 K3 K5 110.68(10) . 7 ?
As7 K3 K5 126.63(11) . 7 ?
Nb1 K3 K5 68.81(8) 5 7 ?
As2 K3 K5 108.82(10) 5 7 ?
As3 K3 K5 53.61(7) 5 7 ?
K15 K3 K5 100.08(15) 5 7 ?
As8 K3 K9 80.71(10) . . ?
As10 K3 K9 147.21(10) . . ?
As7 K3 K9 53.82(10) . . ?
Nb1 K3 K9 93.35(7) 5 . ?
As2 K3 K9 107.02(9) 5 . ?
As3 K3 K9 53.27(6) 5 . ?
K15 K3 K9 155.43(13) 5 . ?
K5 K3 K9 73.45(12) 7 . ?
As8 K3 Nb4 39.68(5) . . ?
As10 K3 Nb4 39.64(5) . . ?
As7 K3 Nb4 101.62(8) . . ?
Nb1 K3 Nb4 140.90(9) 5 . ?
As2 K3 Nb4 141.73(10) 5 . ?
As3 K3 Nb4 140.50(9) 5 . ?
K15 K3 Nb4 92.53(12) 5 . ?
K5 K3 Nb4 88.42(8) 7 . ?
K9 K3 Nb4 110.65(9) . . ?
As8 K3 As1 93.13(8) . 5 ?
As10 K3 As1 91.75(8) . 5 ?
As7 K3 As1 154.55(10) . 5 ?
Nb1 K3 As1 37.28(5) 5 5 ?
As2 K3 As1 66.32(6) 5 5 ?
As3 K3 As1 63.63(6) 5 5 ?
K15 K3 As1 50.55(13) 5 5 ?
K5 K3 As1 51.94(7) 7 5 ?
K9 K3 As1 113.27(10) . 5 ?
Nb4 K3 As1 103.68(8) . 5 ?
As8 K3 K13 147.98(11) . . ?
As10 K3 K13 90.78(9) . . ?
As7 K3 K13 51.52(7) . . ?
Nb1 K3 K13 89.76(9) 5 . ?
As2 K3 K13 51.74(7) 5 . ?
As3 K3 K13 101.66(9) 5 . ?
K15 K3 K13 80.17(15) 5 . ?
K5 K3 K13 154.89(11) 7 . ?
K9 K3 K13 95.79(13) . . ?
Nb4 K3 K13 116.69(10) . . ?
As1 K3 K13 116.99(10) 5 . ?
As10 K4 As10 75.82(10) . 12 ?
As10 K4 As7 110.49(10) . . ?
As10 K4 As7 110.49(10) 12 . ?
As10 K4 As4 100.06(5) . 5_445 ?
As10 K4 As4 151.43(15) 12 5_445 ?
As7 K4 As4 97.52(10) . 5_445 ?
As10 K4 As4 151.43(15) . 16_545 ?
As10 K4 As4 100.06(5) 12 16_545 ?
As7 K4 As4 97.52(10) . 16_545 ?
As4 K4 As4 69.86(9) 5_445 16_545 ?
As10 K4 Nb2 117.63(10) . 5_445 ?
As10 K4 Nb2 117.63(10) 12 5_445 ?
As7 K4 Nb2 117.67(12) . 5_445 ?
As4 K4 Nb2 38.96(5) 5_445 5_445 ?
As4 K4 Nb2 38.96(5) 16_545 5_445 ?
As10 K4 Nb4 39.64(5) . . ?
As10 K4 Nb4 39.64(5) 12 . ?
As7 K4 Nb4 103.78(11) . . ?
As4 K4 Nb4 139.01(8) 5_445 . ?
As4 K4 Nb4 139.01(8) 16_545 . ?
Nb2 K4 Nb4 138.55(13) 5_445 . ?
As10 K4 K13 90.30(6) . . ?
As10 K4 K13 152.81(13) 12 . ?
As7 K4 K13 52.35(7) . . ?
As4 K4 K13 53.18(6) 5_445 . ?
As4 K4 K13 102.98(11) 16_545 . ?
Nb2 K4 K13 89.49(9) 5_445 . ?
Nb4 K4 K13 117.79(9) . . ?
As10 K4 K13 152.80(13) . 12 ?
As10 K4 K13 90.31(6) 12 12 ?
As7 K4 K13 52.34(7) . 12 ?
As4 K4 K13 102.98(11) 5_445 12 ?
As4 K4 K13 53.18(6) 16_545 12 ?
Nb2 K4 K13 89.49(9) 5_445 12 ?
Nb4 K4 K13 117.80(9) . 12 ?
K13 K4 K13 92.03(14) . 12 ?
As10 K4 K2 53.05(7) . 13_556 ?
As10 K4 K2 102.34(13) 12 13_556 ?
As7 K4 K2 137.96(8) . 13_556 ?
As4 K4 K2 56.45(8) 5_445 13_556 ?
As4 K4 K2 101.93(12) 16_545 13_556 ?
Nb2 K4 K2 64.68(8) 5_445 13_556 ?
Nb4 K4 K2 85.07(9) . 13_556 ?
K13 K4 K2 86.89(9) . 13_556 ?
K13 K4 K2 154.14(13) 12 13_556 ?
As10 K4 K2 102.34(13) . 8_456 ?
As10 K4 K2 53.04(7) 12 8_456 ?
As7 K4 K2 137.96(8) . 8_456 ?
As4 K4 K2 101.93(12) 5_445 8_456 ?
As4 K4 K2 56.45(8) 16_545 8_456 ?
Nb2 K4 K2 64.68(8) 5_445 8_456 ?
Nb4 K4 K2 85.07(9) . 8_456 ?
K13 K4 K2 154.14(13) . 8_456 ?
K13 K4 K2 86.89(9) 12 8_456 ?
K2 K4 K2 83.07(16) 13_556 8_456 ?
As10 K4 K3 93.17(10) . 12 ?
As10 K4 K3 53.30(7) 12 12 ?
As7 K4 K3 57.22(8) . 12 ?
As4 K4 K3 154.48(14) 5_445 12 ?
As4 K4 K3 107.10(7) 16_545 12 ?
Nb2 K4 K3 145.94(7) 5_445 12 ?
Nb4 K4 K3 59.74(7) . 12 ?
K13 K4 K3 105.47(12) . 12 ?
K13 K4 K3 60.14(8) 12 12 ?
K2 K4 K3 144.63(13) 13_556 12 ?
K2 K4 K3 96.36(8) 8_456 12 ?
As8 K5 As3 109.03(10) 14_546 3 ?
As8 K5 As1 104.99(9) 14_546 10_556 ?
As3 K5 As1 72.75(8) 3 10_556 ?
As8 K5 As6 142.87(11) 14_546 . ?
As3 K5 As6 99.19(9) 3 . ?
As1 K5 As6 106.12(10) 10_556 . ?
As8 K5 K1 162.88(13) 14_546 . ?
As3 K5 K1 58.46(10) 3 . ?
As1 K5 K1 61.50(7) 10_556 . ?
As6 K5 K1 54.24(9) . . ?
As8 K5 K3 55.51(7) 14_546 7_545 ?
As3 K5 K3 60.91(7) 3 7_545 ?
As1 K5 K3 65.99(8) 10_556 7_545 ?
As6 K5 K3 159.72(11) . 7_545 ?
K1 K5 K3 107.59(12) . 7_545 ?
As8 K5 K6 58.75(7) 14_546 7_545 ?
As3 K5 K6 116.16(10) 3 7_545 ?
As1 K5 K6 56.10(8) 10_556 7_545 ?
As6 K5 K6 127.97(10) . 7_545 ?
K1 K5 K6 113.96(10) . 7_545 ?
K3 K5 K6 64.69(8) 7_545 7_545 ?
As8 K5 K11 121.44(12) 14_546 10_556 ?
As3 K5 K11 114.13(11) 3 10_556 ?
As1 K5 K11 56.24(8) 10_556 10_556 ?
As6 K5 K11 63.60(9) . 10_556 ?
K1 K5 K11 61.63(9) . 10_556 ?
K3 K5 K11 118.72(12) 7_545 10_556 ?
K6 K5 K11 67.43(10) 7_545 10_556 ?
As8 K5 K5 128.83(7) 14_546 10_556 ?
As3 K5 K5 52.46(6) 3 10_556 ?
As1 K5 K5 110.68(6) 10_556 10_556 ?
As6 K5 K5 54.84(6) . 10_556 ?
K1 K5 K5 55.21(5) . 10_556 ?
K3 K5 K5 108.91(7) 7_545 10_556 ?
K6 K5 K5 166.49(7) 7_545 10_556 ?
K11 K5 K5 108.78(8) 10_556 10_556 ?
As8 K5 K13 102.16(9) 14_546 10_556 ?
As3 K5 K13 148.48(10) 3 10_556 ?
As1 K5 K13 103.81(9) 10_556 10_556 ?
As6 K5 K13 50.73(6) . 10_556 ?
K1 K5 K13 91.82(11) . 10_556 ?
K3 K5 K13 147.55(10) 7_545 10_556 ?
K6 K5 K13 83.86(8) 7_545 10_556 ?
K11 K5 K13 48.75(7) 10_556 10_556 ?
K5 K5 K13 103.51(6) 10_556 10_556 ?
As8 K5 K5 45.84(6) 14_546 12_655 ?
As3 K5 K5 106.81(7) 3 12_655 ?
As1 K5 K5 150.02(6) 10_556 12_655 ?
As6 K5 K5 103.53(6) . 12_655 ?
K1 K5 K5 144.80(5) . 12_655 ?
K3 K5 K5 87.24(7) 7_545 12_655 ?
K6 K5 K5 101.24(7) 7_545 12_655 ?
K11 K5 K5 138.38(7) 10_556 12_655 ?
K5 K5 K5 90.0 10_556 12_655 ?
K13 K5 K5 91.50(6) 10_556 12_655 ?
As8 K5 K9 70.95(7) 14_546 5_545 ?
As3 K5 K9 47.28(6) 3 5_545 ?
As1 K5 K9 108.82(10) 10_556 5_545 ?
As6 K5 K9 116.36(9) . 5_545 ?
K1 K5 K9 102.28(9) . 5_545 ?
K3 K5 K9 54.25(8) 7_545 5_545 ?
K6 K5 K9 115.67(9) 7_545 5_545 ?
K11 K5 K9 161.28(10) 10_556 5_545 ?
K5 K5 K9 63.58(5) 10_556 5_545 ?
K13 K5 K9 147.34(10) 10_556 5_545 ?
K5 K5 K9 60.28(5) 12_655 5_545 ?
As5 K6 As10 101.25(9) . . ?
As5 K6 As4 75.17(7) . 12_655 ?
As10 K6 As4 159.31(11) . 12_655 ?
As5 K6 As1 101.51(9) . 5 ?
As10 K6 As1 99.00(8) . 5 ?
As4 K6 As1 101.68(9) 12_655 5 ?
As5 K6 As8 160.76(11) . . ?
As10 K6 As8 72.74(7) . . ?
As4 K6 As8 103.80(9) 12_655 . ?
As1 K6 As8 97.52(8) 5 . ?
As5 K6 Nb4 122.99(9) . . ?
As10 K6 Nb4 42.01(5) . . ?
As4 K6 Nb4 122.83(10) 12_655 . ?
As1 K6 Nb4 122.03(9) 5 . ?
As8 K6 Nb4 41.19(5) . . ?
As5 K6 K12 115.14(12) . . ?
As10 K6 K12 108.89(11) . . ?
As4 K6 K12 57.08(8) 12_655 . ?
As1 K6 K12 127.21(12) 5 . ?
As8 K6 K12 52.98(9) . . ?
Nb4 K6 K12 67.08(9) . . ?
As5 K6 As9 94.56(8) . . ?
As10 K6 As9 67.33(7) . . ?
As4 K6 As9 92.43(8) 12_655 . ?
As1 K6 As9 160.83(10) 5 . ?
As8 K6 As9 66.21(7) . . ?
Nb4 K6 As9 38.90(5) . . ?
K12 K6 As9 51.68(9) . . ?
As5 K6 K2 54.57(8) . . ?
As10 K6 K2 58.85(7) . . ?
As4 K6 K2 105.01(9) 12_655 . ?
As1 K6 K2 136.41(11) 5 . ?
As8 K6 K2 108.60(10) . . ?
Nb4 K6 K2 68.43(8) . . ?
K12 K6 K2 96.29(12) . . ?
As9 K6 K2 48.82(8) . . ?
As5 K6 K5 145.41(11) . 7 ?
As10 K6 K5 106.43(9) . 7 ?
As4 K6 K5 85.46(8) 12_655 7 ?
As1 K6 K5 54.30(7) 5 7 ?
As8 K6 K5 51.72(7) . 7 ?
Nb4 K6 K5 91.58(9) . 7 ?
K12 K6 K5 74.87(12) . 7 ?
As9 K6 K5 114.94(10) . 7 ?
K2 K6 K5 160.01(12) . 7 ?
As5 K6 K15 85.17(11) . 5 ?
As10 K6 K15 54.41(9) . 5 ?
As4 K6 K15 143.26(12) 12_655 5 ?
As1 K6 K15 51.87(11) 5 5 ?
As8 K6 K15 104.65(10) . 5 ?
Nb4 K6 K15 93.91(9) . 5 ?
K12 K6 K15 157.33(13) . 5 ?
As9 K6 K15 120.23(12) . 5 ?
K2 K6 K15 87.34(13) . 5 ?
K5 K6 K15 94.30(13) 7 5 ?
As5 K6 Nb2 39.64(5) . . ?
As10 K6 Nb2 140.68(9) . . ?
As4 K6 Nb2 37.79(4) 12_655 . ?
As1 K6 Nb2 94.63(8) 5 . ?
As8 K6 Nb2 141.50(9) . . ?
Nb4 K6 Nb2 143.34(9) . . ?
K12 K6 Nb2 91.06(9) . . ?
As9 K6 Nb2 104.44(8) . . ?
K2 K6 Nb2 86.22(8) . . ?
K5 K6 Nb2 111.45(9) 7 . ?
K15 K6 Nb2 111.53(11) 5 . ?
As9 K7 As9 106.04(13) 9_566 . ?
As9 K7 As4 102.34(5) 9_566 9_666 ?
As9 K7 As4 102.39(5) . 9_666 ?
As9 K7 As4 102.39(5) 9_566 12_655 ?
As9 K7 As4 102.33(5) . 12_655 ?
As4 K7 As4 138.31(15) 9_666 12_655 ?
As9 K7 K2 53.58(7) 9_566 4_566 ?
As9 K7 K2 142.67(12) . 4_566 ?
As4 K7 K2 112.00(9) 9_666 4_566 ?
As4 K7 K2 60.42(7) 12_655 4_566 ?
As9 K7 K2 142.67(12) 9_566 . ?
As9 K7 K2 53.58(7) . . ?
As4 K7 K2 60.41(7) 9_666 . ?
As4 K7 K2 111.99(9) 12_655 . ?
K2 K7 K2 160.73(19) 4_566 . ?
As9 K7 Nb2 121.59(5) 9_566 9_666 ?
As9 K7 Nb2 122.13(5) . 9_666 ?
As4 K7 Nb2 40.49(5) 9_666 9_666 ?
As4 K7 Nb2 97.82(11) 12_655 9_666 ?
K2 K7 Nb2 94.12(11) 4_566 9_666 ?
K2 K7 Nb2 68.56(8) . 9_666 ?
As9 K7 Nb2 122.13(5) 9_566 . ?
As9 K7 Nb2 121.58(5) . . ?
As4 K7 Nb2 97.82(11) 9_666 . ?
As4 K7 Nb2 40.49(5) 12_655 . ?
K2 K7 Nb2 68.56(8) 4_566 . ?
K2 K7 Nb2 94.12(11) . . ?
Nb2 K7 Nb2 57.33(8) 9_666 . ?
As9 K7 As5 97.18(4) 9_566 9_666 ?
As9 K7 As5 156.78(10) . 9_666 ?
As4 K7 As5 72.45(8) 9_666 9_666 ?
As4 K7 As5 71.57(8) 12_655 9_666 ?
K2 K7 As5 54.47(8) 4_566 9_666 ?
K2 K7 As5 106.89(12) . 9_666 ?
Nb2 K7 As5 40.54(6) 9_666 9_666 ?
Nb2 K7 As5 40.29(6) . 9_666 ?
As9 K7 As5 156.78(10) 9_566 . ?
As9 K7 As5 97.18(4) . . ?
As4 K7 As5 71.57(8) 9_666 . ?
As4 K7 As5 72.45(8) 12_655 . ?
K2 K7 As5 106.89(12) 4_566 . ?
K2 K7 As5 54.47(8) . . ?
Nb2 K7 As5 40.29(6) 9_666 . ?
Nb2 K7 As5 40.54(6) . . ?
As5 K7 As5 59.61(8) 9_666 . ?
As9 K7 K12 86.93(11) 9_566 . ?
As9 K7 K12 54.28(9) . . ?
As4 K7 K12 156.66(10) 9_666 . ?
As4 K7 K12 57.23(6) 12_655 . ?
K2 K7 K12 90.81(11) 4_566 . ?
K2 K7 K12 99.39(10) . . ?
Nb2 K7 K12 147.23(10) 9_666 . ?
Nb2 K7 K12 95.09(6) . . ?
As5 K7 K12 128.18(8) 9_666 . ?
As5 K7 K12 107.52(7) . . ?
As9 K7 K12 54.29(9) 9_566 9_566 ?
As9 K7 K12 86.94(11) . 9_566 ?
As4 K7 K12 57.24(6) 9_666 9_566 ?
As4 K7 K12 156.66(10) 12_655 9_566 ?
K2 K7 K12 99.40(10) 4_566 9_566 ?
K2 K7 K12 90.81(11) . 9_566 ?
Nb2 K7 K12 95.09(6) 9_666 9_566 ?
Nb2 K7 K12 147.23(10) . 9_566 ?
As5 K7 K12 107.52(7) 9_666 9_566 ?
As5 K7 K12 128.18(8) . 9_566 ?
K12 K7 K12 116.04(14) . 9_566 ?
As3 K8 As2 78.84(8) 5 14_556 ?
As3 K8 As2 78.83(8) 5 5 ?
As2 K8 As2 92.41(12) 14_556 5 ?
As3 K8 K10 130.63(17) 5 . ?
As2 K8 K10 67.78(10) 14_556 . ?
As2 K8 K10 67.78(10) 5 . ?
As3 K8 Nb3 131.60(14) 5 . ?
As2 K8 Nb3 128.71(7) 14_556 . ?
As2 K8 Nb3 128.71(7) 5 . ?
K10 K8 Nb3 97.77(14) . . ?
As3 K8 Nb3 131.60(14) 5 10_556 ?
As2 K8 Nb3 128.71(7) 14_556 10_556 ?
As2 K8 Nb3 128.71(7) 5 10_556 ?
K10 K8 Nb3 97.77(14) . 10_556 ?
Nb3 K8 Nb3 0.00(6) . 10_556 ?
As3 K8 As6 173.90(16) 5 . ?
As2 K8 As6 105.26(9) 14_556 . ?
As2 K8 As6 105.26(9) 5 . ?
K10 K8 As6 55.47(12) . . ?
Nb3 K8 As6 42.30(6) . . ?
Nb3 K8 As6 42.30(6) 10_556 . ?
As3 K8 As7 104.15(11) 5 10_556 ?
As2 K8 As7 99.68(4) 14_556 10_556 ?
As2 K8 As7 167.88(10) 5 10_556 ?
K10 K8 As7 116.18(12) . 10_556 ?
Nb3 K8 As7 41.07(6) . 10_556 ?
Nb3 K8 As7 41.07(6) 10_556 10_556 ?
As6 K8 As7 70.91(8) . 10_556 ?
As3 K8 As7 104.14(11) 5 . ?
As2 K8 As7 167.88(10) 14_556 . ?
As2 K8 As7 99.68(4) 5 . ?
K10 K8 As7 116.18(12) . . ?
Nb3 K8 As7 41.08(6) . . ?
Nb3 K8 As7 41.08(6) 10_556 . ?
As6 K8 As7 70.91(8) . . ?
As7 K8 As7 68.21(9) 10_556 . ?
As3 K8 K13 119.99(8) 5 . ?
As2 K8 K13 134.01(14) 14_556 . ?
As2 K8 K13 56.33(7) 5 . ?
K10 K8 K13 69.15(9) . . ?
Nb3 K8 K13 72.43(8) . . ?
Nb3 K8 K13 72.43(8) 10_556 . ?
As6 K8 K13 60.48(8) . . ?
As7 K8 K13 113.24(12) 10_556 . ?
As7 K8 K13 54.85(7) . . ?
As3 K8 K13 119.99(8) 5 10_556 ?
As2 K8 K13 56.34(7) 14_556 10_556 ?
As2 K8 K13 134.01(14) 5 10_556 ?
K10 K8 K13 69.15(9) . 10_556 ?
Nb3 K8 K13 72.43(8) . 10_556 ?
Nb3 K8 K13 72.43(8) 10_556 10_556 ?
As6 K8 K13 60.48(8) . 10_556 ?
As7 K8 K13 54.85(7) 10_556 10_556 ?
As7 K8 K13 113.24(12) . 10_556 ?
K13 K8 K13 119.81(16) . 10_556 ?
As3 K8 K9 59.01(11) 5 . ?
As2 K8 K9 118.03(9) 14_556 . ?
As2 K8 K9 118.02(9) 5 . ?
K10 K8 K9 170.36(18) . . ?
Nb3 K8 K9 72.59(12) . . ?
Nb3 K8 K9 72.59(12) 10_556 . ?
As6 K8 K9 114.89(14) . . ?
As7 K8 K9 56.47(9) 10_556 . ?
As7 K8 K9 56.47(9) . . ?
K13 K8 K9 106.96(10) . . ?
K13 K8 K9 106.96(10) 10_556 . ?
As3 K9 As3 147.4(2) 5 7_455 ?
As3 K9 As7 103.17(8) 5 10_556 ?
As3 K9 As7 103.17(8) 7_455 10_556 ?
As3 K9 As7 103.17(8) 5 . ?
As3 K9 As7 103.17(8) 7_455 . ?
As7 K9 As7 71.46(14) 10_556 . ?
As3 K9 K8 53.98(7) 5 . ?
As3 K9 K8 158.6(2) 7_455 . ?
As7 K9 K8 60.25(10) 10_556 . ?
As7 K9 K8 60.25(10) . . ?
As3 K9 K8 158.6(2) 5 3 ?
As3 K9 K8 53.99(7) 7_455 3 ?
As7 K9 K8 60.25(10) 10_556 3 ?
As7 K9 K8 60.24(10) . 3 ?
K8 K9 K8 104.6(2) . 3 ?
As3 K9 K3 59.63(5) 5 10_556 ?
As3 K9 K3 121.89(6) 7_455 10_556 ?
As7 K9 K3 58.39(6) 10_556 10_556 ?
As7 K9 K3 117.32(15) . 10_556 ?
K8 K9 K3 63.21(6) . 10_556 ?
K8 K9 K3 113.68(11) 3 10_556 ?
As3 K9 K3 121.89(6) 5 3 ?
As3 K9 K3 59.63(5) 7_455 3 ?
As7 K9 K3 58.39(6) 10_556 3 ?
As7 K9 K3 117.32(15) . 3 ?
K8 K9 K3 113.68(11) . 3 ?
K8 K9 K3 63.21(6) 3 3 ?
K3 K9 K3 65.18(9) 10_556 3 ?
As3 K9 K3 59.62(5) 5 . ?
As3 K9 K3 121.88(6) 7_455 . ?
As7 K9 K3 117.32(15) 10_556 . ?
As7 K9 K3 58.39(6) . . ?
K8 K9 K3 63.21(6) . . ?
K8 K9 K3 113.68(11) 3 . ?
K3 K9 K3 114.62(9) 10_556 . ?
K3 K9 K3 175.4(2) 3 . ?
As3 K9 K3 121.88(6) 5 12 ?
As3 K9 K3 59.62(5) 7_455 12 ?
As7 K9 K3 117.31(15) 10_556 12 ?
As7 K9 K3 58.39(6) . 12 ?
K8 K9 K3 113.68(11) . 12 ?
K8 K9 K3 63.21(6) 3 12 ?
K3 K9 K3 175.4(2) 10_556 12 ?
K3 K9 K3 114.62(9) 3 12 ?
K3 K9 K3 65.17(9) . 12 ?
As3 K9 K5 46.76(7) 5 16 ?
As3 K9 K5 105.45(14) 7_455 16 ?
As7 K9 K5 110.22(5) 10_556 16 ?
As7 K9 K5 149.92(4) . 16 ?
K8 K9 K5 93.65(7) . 16 ?
K8 K9 K5 148.03(7) 3 16 ?
K3 K9 K5 52.30(7) 10_556 16 ?
K3 K9 K5 85.55(9) 3 16 ?
K3 K9 K5 97.90(10) . 16 ?
K3 K9 K5 132.17(16) 12 16 ?
As3 K9 K5 105.45(14) 5 5_455 ?
As3 K9 K5 46.76(7) 7_455 5_455 ?
As7 K9 K5 110.22(5) 10_556 5_455 ?
As7 K9 K5 149.92(4) . 5_455 ?
K8 K9 K5 148.02(7) . 5_455 ?
K8 K9 K5 93.66(7) 3 5_455 ?
K3 K9 K5 85.55(9) 10_556 5_455 ?
K3 K9 K5 52.30(7) 3 5_455 ?
K3 K9 K5 132.17(16) . 5_455 ?
K3 K9 K5 97.90(10) 12 5_455 ?
K5 K9 K5 59.43(11) 16 5_455 ?
As6 K10 As6 147.6(3) 3_655 . ?
As6 K10 K8 63.51(9) 3_655 3_655 ?
As6 K10 K8 148.9(3) . 3_655 ?
As6 K10 K8 148.9(3) 3_655 . ?
As6 K10 K8 63.51(9) . . ?
K8 K10 K8 85.3(2) 3_655 . ?
As6 K10 As2 102.30(10) 3_655 14_556 ?
As6 K10 As2 102.30(10) . 14_556 ?
K8 K10 As2 55.82(12) 3_655 14_556 ?
K8 K10 As2 55.82(12) . 14_556 ?
As6 K10 As2 102.30(10) 3_655 5 ?
As6 K10 As2 102.30(10) . 5 ?
K8 K10 As2 55.82(12) 3_655 5 ?
K8 K10 As2 55.82(12) . 5 ?
As2 K10 As2 80.34(18) 14_556 5 ?
As6 K10 K13 58.26(5) 3_655 12_655 ?
As6 K10 K13 128.89(6) . 12_655 ?
K8 K10 K13 57.21(8) 3_655 12_655 ?
K8 K10 K13 105.83(17) . 12_655 ?
As2 K10 K13 111.25(18) 14_556 12_655 ?
As2 K10 K13 50.08(7) 5 12_655 ?
As6 K10 K13 128.89(6) 3_655 . ?
As6 K10 K13 58.27(5) . . ?
K8 K10 K13 105.83(17) 3_655 . ?
K8 K10 K13 57.22(8) . . ?
As2 K10 K13 111.25(18) 14_556 . ?
As2 K10 K13 50.08(7) 5 . ?
K13 K10 K13 73.84(11) 12_655 . ?
As6 K10 K13 58.27(5) 3_655 3_655 ?
As6 K10 K13 128.89(6) . 3_655 ?
K8 K10 K13 57.22(8) 3_655 3_655 ?
K8 K10 K13 105.83(17) . 3_655 ?
As2 K10 K13 50.08(7) 14_556 3_655 ?
As2 K10 K13 111.25(18) 5 3_655 ?
K13 K10 K13 102.21(11) 12_655 3_655 ?
K13 K10 K13 158.9(3) . 3_655 ?
As6 K10 K13 128.89(6) 3_655 10_556 ?
As6 K10 K13 58.27(5) . 10_556 ?
K8 K10 K13 105.83(17) 3_655 10_556 ?
K8 K10 K13 57.22(8) . 10_556 ?
As2 K10 K13 50.08(7) 14_556 10_556 ?
As2 K10 K13 111.25(18) 5 10_556 ?
K13 K10 K13 158.9(3) 12_655 10_556 ?
K13 K10 K13 102.22(11) . 10_556 ?
K13 K10 K13 73.84(11) 3_655 10_556 ?
As6 K10 K5 104.03(19) 3_655 . ?
As6 K10 K5 47.84(10) . . ?
K8 K10 K5 152.61(5) 3_655 . ?
K8 K10 K5 104.07(8) . . ?
As2 K10 K5 108.20(5) 14_556 . ?
As2 K10 K5 149.66(4) 5 . ?
K13 K10 K5 139.33(19) 12_655 . ?
K13 K10 K5 100.78(11) . . ?
K13 K10 K5 95.39(10) 3_655 . ?
K13 K10 K5 61.48(8) 10_556 . ?
As6 K10 K5 47.85(10) 3_655 12_655 ?
As6 K10 K5 104.03(19) . 12_655 ?
K8 K10 K5 104.07(8) 3_655 12_655 ?
K8 K10 K5 152.61(5) . 12_655 ?
As2 K10 K5 108.20(5) 14_556 12_655 ?
As2 K10 K5 149.67(4) 5 12_655 ?
K13 K10 K5 100.78(11) 12_655 12_655 ?
K13 K10 K5 139.33(19) . 12_655 ?
K13 K10 K5 61.48(8) 3_655 12_655 ?
K13 K10 K5 95.39(10) 10_556 12_655 ?
K5 K10 K5 56.80(11) . 12_655 ?
As4 K11 As4 72.21(10) 5_445 16_545 ?
As4 K11 As1 101.83(11) 5_445 . ?
As4 K11 As1 101.83(11) 16_545 . ?
As4 K11 K13 113.45(13) 5_445 12 ?
As4 K11 K13 57.41(7) 16_545 12 ?
As1 K11 K13 127.10(8) . 12 ?
As4 K11 K13 57.41(7) 5_445 . ?
As4 K11 K13 113.45(13) 16_545 . ?
As1 K11 K13 127.10(8) . . ?
K13 K11 K13 105.25(15) 12 . ?
As4 K11 As7 96.18(10) 5_445 . ?
As4 K11 As7 96.18(10) 16_545 . ?
As1 K11 As7 157.64(16) . . ?
K13 K11 As7 54.28(8) 12 . ?
K13 K11 As7 54.28(8) . . ?
As4 K11 Nb3 125.63(10) 5_445 . ?
As4 K11 Nb3 125.63(10) 16_545 . ?
As1 K11 Nb3 119.16(13) . . ?
K13 K11 Nb3 69.30(9) 12 . ?
K13 K11 Nb3 69.30(9) . . ?
As7 K11 Nb3 38.48(6) . . ?
As4 K11 Nb3 125.63(10) 5_445 10_556 ?
As4 K11 Nb3 125.63(10) 16_545 10_556 ?
As1 K11 Nb3 119.16(13) . 10_556 ?
K13 K11 Nb3 69.30(9) 12 10_556 ?
K13 K11 Nb3 69.30(9) . 10_556 ?
As7 K11 Nb3 38.48(6) . 10_556 ?
Nb3 K11 Nb3 0.0 . 10_556 ?
As4 K11 K1 140.47(7) 5_445 . ?
As4 K11 K1 140.47(7) 16_545 . ?
As1 K11 K1 57.98(10) . . ?
K13 K11 K1 105.19(12) 12 . ?
K13 K11 K1 105.19(12) . . ?
As7 K11 K1 99.67(13) . . ?
Nb3 K11 K1 61.19(10) . . ?
Nb3 K11 K1 61.19(10) 10_556 . ?
As4 K11 K5 85.55(7) 5_445 10_556 ?
As4 K11 K5 143.48(14) 16_545 10_556 ?
As1 K11 K5 54.05(7) . 10_556 ?
K13 K11 K5 157.97(16) 12 10_556 ?
K13 K11 K5 74.86(8) . 10_556 ?
As7 K11 K5 115.14(10) . 10_556 ?
Nb3 K11 K5 90.85(10) . 10_556 ?
Nb3 K11 K5 90.85(10) 10_556 10_556 ?
K1 K11 K5 54.93(8) . 10_556 ?
As4 K11 K5 143.48(14) 5_445 3 ?
As4 K11 K5 85.55(7) 16_545 3 ?
As1 K11 K5 54.05(7) . 3 ?
K13 K11 K5 74.86(8) 12 3 ?
K13 K11 K5 157.98(16) . 3 ?
As7 K11 K5 115.14(10) . 3 ?
Nb3 K11 K5 90.85(10) . 3 ?
Nb3 K11 K5 90.85(10) 10_556 3 ?
K1 K11 K5 54.93(8) . 3 ?
K5 K11 K5 96.77(13) 10_556 3 ?
As4 K11 As6 161.15(13) 5_445 3 ?
As4 K11 As6 108.67(5) 16_545 3 ?
As1 K11 As6 96.43(10) . 3 ?
K13 K11 As6 56.83(8) 12 3 ?
K13 K11 As6 107.31(13) . 3 ?
As7 K11 As6 64.98(8) . 3 ?
Nb3 K11 As6 38.02(5) . 3 ?
Nb3 K11 As6 38.02(5) 10_556 3 ?
K1 K11 As6 49.27(8) . 3 ?
K5 K11 As6 101.67(12) 10_556 3 ?
K5 K11 As6 53.68(7) 3 3 ?
As8 K12 As9 75.63(12) . . ?
As8 K12 As4 110.41(9) . 12_655 ?
As9 K12 As4 101.62(10) . 12_655 ?
As8 K12 As4 110.41(9) . 1_455 ?
As9 K12 As4 101.62(10) . 1_455 ?
As4 K12 As4 136.78(17) 12_655 1_455 ?
As8 K12 K16 156.9(4) . . ?
As9 K12 K16 127.5(4) . . ?
As4 K12 K16 68.45(9) 12_655 . ?
As4 K12 K16 68.45(9) 1_455 . ?
As8 K12 K6 60.64(9) . . ?
As9 K12 K6 64.59(9) . . ?
As4 K12 K6 56.90(5) 12_655 . ?
As4 K12 K6 164.42(16) 1_455 . ?
K16 K12 K6 125.14(9) . . ?
As8 K12 K6 60.64(9) . 12 ?
As9 K12 K6 64.59(9) . 12 ?
As4 K12 K6 164.42(16) 12_655 12 ?
As4 K12 K6 56.90(5) 1_455 12 ?
K16 K12 K6 125.14(9) . 12 ?
K6 K12 K6 108.53(16) . 12 ?
As8 K12 K7 118.41(13) . . ?
As9 K12 K7 55.79(9) . . ?
As4 K12 K7 54.90(8) 12_655 . ?
As4 K12 K7 114.20(15) 1_455 . ?
K16 K12 K7 80.7(3) . . ?
K6 K12 K7 65.19(8) . . ?
K6 K12 K7 116.12(15) 12 . ?
As8 K12 K7 118.41(13) . 9_566 ?
As9 K12 K7 55.79(9) . 9_566 ?
As4 K12 K7 114.20(15) 12_655 9_566 ?
As4 K12 K7 54.91(8) 1_455 9_566 ?
K16 K12 K7 80.7(3) . 9_566 ?
K6 K12 K7 116.12(15) . 9_566 ?
K6 K12 K7 65.19(8) 12 9_566 ?
K7 K12 K7 63.96(14) . 9_566 ?
As8 K12 Nb4 38.32(7) . . ?
As9 K12 Nb4 37.31(7) . . ?
As4 K12 Nb4 110.31(8) 12_655 . ?
As4 K12 Nb4 110.31(8) 1_455 . ?
K16 K12 Nb4 164.8(4) . . ?
K6 K12 Nb4 54.45(8) . . ?
K6 K12 Nb4 54.45(8) 12 . ?
K7 K12 Nb4 86.44(10) . . ?
K7 K12 Nb4 86.44(10) 9_566 . ?
As8 K12 K13 103.45(13) . 16 ?
As9 K12 K13 147.66(6) . 16 ?
As4 K12 K13 47.59(7) 12_655 16 ?
As4 K12 K13 108.62(13) 1_455 16 ?
K16 K12 K13 57.8(3) . 16 ?
K6 K12 K13 86.45(8) . 16 ?
K6 K12 K13 143.68(15) 12 16 ?
K7 K12 K13 100.19(9) . 16 ?
K7 K12 K13 137.99(15) 9_566 16 ?
Nb4 K12 K13 133.34(11) . 16 ?
As8 K12 K13 103.45(13) . 5_455 ?
As9 K12 K13 147.66(6) . 5_455 ?
As4 K12 K13 108.62(13) 12_655 5_455 ?
As4 K12 K13 47.59(7) 1_455 5_455 ?
K16 K12 K13 57.8(3) . 5_455 ?
K6 K12 K13 143.68(15) . 5_455 ?
K6 K12 K13 86.45(8) 12 5_455 ?
K7 K12 K13 137.99(15) . 5_455 ?
K7 K12 K13 100.19(9) 9_566 5_455 ?
Nb4 K12 K13 133.34(11) . 5_455 ?
K13 K12 K13 64.61(11) 16 5_455 ?
As7 K13 As2 107.35(10) . 5 ?
As7 K13 As4 105.19(10) . 5_445 ?
As2 K13 As4 129.51(12) 5 5_445 ?
As7 K13 K11 64.67(9) . . ?
As2 K13 K11 170.56(14) 5 . ?
As4 K13 K11 59.38(10) 5_445 . ?
As7 K13 As6 73.04(8) . . ?
As2 K13 As6 106.13(11) 5 . ?
As4 K13 As6 119.78(10) 5_445 . ?
K11 K13 As6 67.39(10) . . ?
As7 K13 K8 61.70(10) . . ?
As2 K13 K8 59.16(9) 5 . ?
As4 K13 K8 166.90(14) 5_445 . ?
K11 K13 K8 111.50(14) . . ?
As6 K13 K8 58.76(8) . . ?
As7 K13 K4 57.20(8) . . ?
As2 K13 K4 114.26(12) 5 . ?
As4 K13 K4 57.30(9) 5_445 . ?
K11 K13 K4 66.51(10) . . ?
As6 K13 K4 122.48(11) . . ?
K8 K13 K4 111.34(12) . . ?
As7 K13 K3 58.66(8) . . ?
As2 K13 K3 59.31(8) 5 . ?
As4 K13 K3 110.96(11) 5_445 . ?
K11 K13 K3 116.55(12) . . ?
As6 K13 K3 116.68(10) . . ?
K8 K13 K3 63.15(9) . . ?
K4 K13 K3 60.42(9) . . ?
As7 K13 K16 136.0(2) . 5_545 ?
As2 K13 K16 66.1(3) 5 5_545 ?
As4 K13 K16 63.6(3) 5_445 5_545 ?
K11 K13 K16 123.0(3) . 5_545 ?
As6 K13 K16 150.7(2) . 5_545 ?
K8 K13 K16 124.9(3) . 5_545 ?
K4 K13 K16 84.89(18) . 5_545 ?
K3 K13 K16 84.7(3) . 5_545 ?
As7 K13 K10 108.56(11) . . ?
As2 K13 K10 62.31(12) 5 . ?
As4 K13 K10 137.19(15) 5_445 . ?
K11 K13 K10 114.26(15) . . ?
As6 K13 K10 50.28(8) . . ?
K8 K13 K10 53.63(12) . . ?
K4 K13 K10 164.77(14) . . ?
K3 K13 K10 108.79(15) . . ?
K16 K13 K10 105.59(18) 5_545 . ?
As7 K13 K12 153.34(11) . 5_545 ?
As2 K13 K12 97.45(9) 5 5_545 ?
As4 K13 K12 49.55(7) 5_445 5_545 ?
K11 K13 K12 91.34(10) . 5_545 ?
As6 K13 K12 109.70(11) . 5_545 ?
K8 K13 K12 143.35(13) . 5_545 ?
K4 K13 K12 103.86(11) . 5_545 ?
K3 K13 K12 132.08(13) . 5_545 ?
K16 K13 K12 47.7(3) 5_545 5_545 ?
K10 K13 K12 91.36(12) . 5_545 ?
As7 K13 K5 108.52(10) . 10_556 ?
As2 K13 K5 125.40(11) 5 10_556 ?
As4 K13 K5 76.93(8) 5_445 10_556 ?
K11 K13 K5 56.39(9) . 10_556 ?
As6 K13 K5 50.18(6) . 10_556 ?
K8 K13 K5 106.53(11) . 10_556 ?
K4 K13 K5 119.55(10) . 10_556 ?
K3 K13 K5 165.86(11) . 10_556 ?
K16 K13 K5 109.5(3) 5_545 10_556 ?
K10 K13 K5 67.97(14) . 10_556 ?
K12 K13 K5 62.02(9) 5_545 10_556 ?
K15 K14 As10 140.67(9) 9_556 12 ?
K15 K14 As10 140.67(9) 9_556 . ?
As10 K14 As10 75.69(12) 12 . ?
K15 K14 K2 103.63(16) 9_556 13_556 ?
As10 K14 K2 111.99(18) 12 13_556 ?
As10 K14 K2 57.25(9) . 13_556 ?
K15 K14 K2 103.63(16) 9_556 8_456 ?
As10 K14 K2 57.25(9) 12 8_456 ?
As10 K14 K2 111.99(18) . 8_456 ?
K2 K14 K2 96.5(2) 13_556 8_456 ?
K15 K14 Nb4 147.1(3) 9_556 . ?
As10 K14 Nb4 42.61(7) 12 . ?
As10 K14 Nb4 42.61(7) . . ?
K2 K14 Nb4 98.05(13) 13_556 . ?
K2 K14 Nb4 98.05(13) 8_456 . ?
K15 K14 K2 86.18(17) 9_556 . ?
As10 K14 K2 111.78(16) 12 . ?
As10 K14 K2 60.49(9) . . ?
K2 K14 K2 86.05(9) 13_556 . ?
K2 K14 K2 168.90(17) 8_456 . ?
Nb4 K14 K2 70.87(11) . . ?
K15 K14 K2 86.17(17) 9_556 12 ?
As10 K14 K2 60.49(9) 12 12 ?
As10 K14 K2 111.78(16) . 12 ?
K2 K14 K2 168.90(17) 13_556 12 ?
K2 K14 K2 86.05(9) 8_456 12 ?
Nb4 K14 K2 70.87(11) . 12 ?
K2 K14 K2 89.47(19) . 12 ?
K15 K14 As10 56.61(7) 9_556 13_556 ?
As10 K14 As10 160.21(13) 12 13_556 ?
As10 K14 As10 85.22(4) . 13_556 ?
K2 K14 As10 59.64(8) 13_556 13_556 ?
K2 K14 As10 137.74(18) 8_456 13_556 ?
Nb4 K14 As10 118.22(9) . 13_556 ?
K2 K14 As10 52.39(7) . 13_556 ?
K2 K14 As10 124.38(18) 12 13_556 ?
K15 K14 As10 56.61(7) 9_556 8_456 ?
As10 K14 As10 85.22(4) 12 8_456 ?
As10 K14 As10 160.21(13) . 8_456 ?
K2 K14 As10 137.74(18) 13_556 8_456 ?
K2 K14 As10 59.64(8) 8_456 8_456 ?
Nb4 K14 As10 118.22(9) . 8_456 ?
K2 K14 As10 124.38(18) . 8_456 ?
K2 K14 As10 52.39(7) 12 8_456 ?
As10 K14 As10 113.18(14) 13_556 8_456 ?
K15 K14 As9 108.3(2) 9_556 . ?
As10 K14 As9 66.78(10) 12 . ?
As10 K14 As9 66.78(10) . . ?
K2 K14 As9 121.14(12) 13_556 . ?
K2 K14 As9 121.13(12) 8_456 . ?
Nb4 K14 As9 38.80(7) . . ?
K2 K14 As9 49.44(9) . . ?
K2 K14 As9 49.44(9) 12 . ?
As10 K14 As9 101.06(11) 13_556 . ?
As10 K14 As9 101.06(11) 8_456 . ?
K15 K14 K16 50.8(3) 9_556 9_566 ?
As10 K14 K16 111.5(3) 12 9_566 ?
As10 K14 K16 111.5(3) . 9_566 ?
K2 K14 K16 129.15(14) 13_556 9_566 ?
K2 K14 K16 129.15(13) 8_456 9_566 ?
Nb4 K14 K16 96.4(3) . 9_566 ?
K2 K14 K16 53.85(18) . 9_566 ?
K2 K14 K16 53.84(18) 12 9_566 ?
As10 K14 K16 70.56(17) 13_556 9_566 ?
As10 K14 K16 70.56(17) 8_456 9_566 ?
As9 K14 K16 57.6(3) . 9_566 ?
K16 K15 As2 77.8(4) 1_545 . ?
K16 K15 As1 157.4(4) 1_545 . ?
As2 K15 As1 79.61(16) . . ?
K16 K15 K14 73.0(4) 1_545 9_556 ?
As2 K15 K14 150.8(3) . 9_556 ?
As1 K15 K14 129.5(3) . 9_556 ?
K16 K15 As10 84.67(19) 1_545 16_545 ?
As2 K15 As10 110.53(13) . 16_545 ?
As1 K15 As10 103.37(15) . 16_545 ?
K14 K15 As10 67.07(11) 9_556 16_545 ?
K16 K15 As10 84.67(19) 1_545 5_445 ?
As2 K15 As10 110.53(13) . 5_445 ?
As1 K15 As10 103.37(15) . 5_445 ?
K14 K15 As10 67.07(11) 9_556 5_445 ?
As10 K15 As10 134.1(2) 16_545 5_445 ?
K16 K15 K3 101.0(2) 1_545 16_545 ?
As2 K15 K3 62.85(11) . 16_545 ?
As1 K15 K3 68.20(12) . 16_545 ?
K14 K15 K3 122.80(10) 9_556 16_545 ?
As10 K15 K3 55.73(6) 16_545 16_545 ?
As10 K15 K3 169.6(2) 5_445 16_545 ?
K16 K15 K3 101.0(2) 1_545 5_445 ?
As2 K15 K3 62.85(11) . 5_445 ?
As1 K15 K3 68.20(12) . 5_445 ?
K14 K15 K3 122.80(10) 9_556 5_445 ?
As10 K15 K3 169.6(2) 16_545 5_445 ?
As10 K15 K3 55.73(6) 5_445 5_445 ?
K3 K15 K3 114.3(2) 16_545 5_445 ?
K16 K15 Nb1 118.2(4) 1_545 . ?
As2 K15 Nb1 40.35(9) . . ?
As1 K15 Nb1 39.26(9) . . ?
K14 K15 Nb1 168.8(3) 9_556 . ?
As10 K15 Nb1 112.21(11) 16_545 . ?
As10 K15 Nb1 112.21(11) 5_445 . ?
K3 K15 Nb1 57.45(10) 16_545 . ?
K3 K15 Nb1 57.45(10) 5_445 . ?
K16 K15 K6 138.6(2) 1_545 16_545 ?
As2 K15 K6 121.04(17) . 16_545 ?
As1 K15 K6 56.44(13) . 16_545 ?
K14 K15 K6 82.50(18) 9_556 16_545 ?
As10 K15 K6 54.85(9) 16_545 16_545 ?
As10 K15 K6 116.0(2) 5_445 16_545 ?
K3 K15 K6 65.15(10) 16_545 16_545 ?
K3 K15 K6 120.3(2) 5_445 16_545 ?
Nb1 K15 K6 88.16(15) . 16_545 ?
K16 K15 K6 138.6(2) 1_545 5_445 ?
As2 K15 K6 121.04(17) . 5_445 ?
As1 K15 K6 56.44(13) . 5_445 ?
K14 K15 K6 82.50(18) 9_556 5_445 ?
As10 K15 K6 116.0(2) 16_545 5_445 ?
As10 K15 K6 54.85(9) 5_445 5_445 ?
K3 K15 K6 120.3(2) 16_545 5_445 ?
K3 K15 K6 65.15(10) 5_445 5_445 ?
Nb1 K15 K6 88.16(15) . 5_445 ?
K6 K15 K6 66.82(16) 16_545 5_445 ?
K16 K15 K2 45.1(2) 1_545 4_556 ?
As2 K15 K2 107.43(18) . 4_556 ?
As1 K15 K2 145.93(10) . 4_556 ?
K14 K15 K2 49.83(12) 9_556 4_556 ?
As10 K15 K2 42.62(9) 16_545 4_556 ?
As10 K15 K2 104.88(17) 5_445 4_556 ?
K3 K15 K2 85.15(9) 16_545 4_556 ?
K3 K15 K2 145.2(2) 5_445 4_556 ?
Nb1 K15 K2 137.56(14) . 4_556 ?
K6 K15 K2 93.76(11) 16_545 4_556 ?
K6 K15 K2 131.24(18) 5_445 4_556 ?
K15 K16 K12 156.8(6) 1_565 . ?
K15 K16 K2 94.6(4) 1_565 4_566 ?
K12 K16 K2 100.4(4) . 4_566 ?
K15 K16 K2 94.6(4) 1_565 9_566 ?
K12 K16 K2 100.4(4) . 9_566 ?
K2 K16 K2 98.7(5) 4_566 9_566 ?
K15 K16 As9 116.6(5) 1_565 9_566 ?
K12 K16 As9 86.6(5) . 9_566 ?
K2 K16 As9 52.1(3) 4_566 9_566 ?
K2 K16 As9 52.1(3) 9_566 9_566 ?
K15 K16 As4 121.8(3) 1_565 12_655 ?
K12 K16 As4 55.8(2) . 12_655 ?
K2 K16 As4 57.23(15) 4_566 12_655 ?
K2 K16 As4 135.5(6) 9_566 12_655 ?
As9 K16 As4 86.7(3) 9_566 12_655 ?
K15 K16 As4 121.8(3) 1_565 1_455 ?
K12 K16 As4 55.8(2) . 1_455 ?
K2 K16 As4 135.5(6) 4_566 1_455 ?
K2 K16 As4 57.23(15) 9_566 1_455 ?
As9 K16 As4 86.7(3) 9_566 1_455 ?
As4 K16 As4 111.5(5) 12_655 1_455 ?
K15 K16 K14 56.2(3) 1_565 9_566 ?
K12 K16 K14 147.0(6) . 9_566 ?
K2 K16 K14 60.5(3) 4_566 9_566 ?
K2 K16 K14 60.5(3) 9_566 9_566 ?
As9 K16 K14 60.4(3) 9_566 9_566 ?
As4 K16 K14 117.3(3) 12_655 9_566 ?
As4 K16 K14 117.3(3) 1_455 9_566 ?
K15 K16 K13 87.2(4) 1_565 16 ?
K12 K16 K13 74.5(3) . 16 ?
K2 K16 K13 93.09(11) 4_566 16 ?
K2 K16 K13 167.8(4) 9_566 16 ?
As9 K16 K13 136.9(3) 9_566 16 ?
As4 K16 K13 50.60(15) 12_655 16 ?
As4 K16 K13 111.8(4) 1_455 16 ?
K14 K16 K13 129.1(4) 9_566 16 ?
K15 K16 K13 87.2(4) 1_565 5_455 ?
K12 K16 K13 74.5(3) . 5_455 ?
K2 K16 K13 167.8(4) 4_566 5_455 ?
K2 K16 K13 93.09(11) 9_566 5_455 ?
As9 K16 K13 136.9(3) 9_566 5_455 ?
As4 K16 K13 111.8(4) 12_655 5_455 ?
As4 K16 K13 50.60(15) 1_455 5_455 ?
K14 K16 K13 129.1(4) 9_566 5_455 ?
K13 K16 K13 75.0(3) 16 5_455 ?
K15 K16 K7 145.0(4) 1_565 . ?
K12 K16 K7 52.9(3) . . ?
K2 K16 K7 50.4(2) 4_566 . ?
K2 K16 K7 90.7(4) 9_566 . ?
As9 K16 K7 45.0(2) 9_566 . ?
As4 K16 K7 44.80(19) 12_655 . ?
As4 K16 K7 89.9(4) 1_455 . ?
K14 K16 K7 98.0(4) 9_566 . ?
K13 K16 K7 94.7(3) 16 . ?
K13 K16 K7 127.1(5) 5_455 . ?
K15 K16 K7 145.0(4) 1_565 9_566 ?
K12 K16 K7 52.9(3) . 9_566 ?
K2 K16 K7 90.7(4) 4_566 9_566 ?
K2 K16 K7 50.4(2) 9_566 9_566 ?
As9 K16 K7 45.0(2) 9_566 9_566 ?
As4 K16 K7 89.9(4) 12_655 9_566 ?
As4 K16 K7 44.80(19) 1_455 9_566 ?
K14 K16 K7 98.0(4) 9_566 9_566 ?
K13 K16 K7 127.1(5) 16 9_566 ?
K13 K16 K7 94.7(3) 5_455 9_566 ?
K7 K16 K7 50.7(2) . 9_566 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Nb1 As1 2.444(2) . ?
Nb1 As2 2.498(2) . ?
Nb1 As3 2.5707(18) 3 ?
Nb1 As3 2.5708(18) . ?
Nb1 Nb1 3.155(3) 10_556 ?
Nb1 K1 3.632(5) . ?
Nb1 K3 3.635(3) 16_545 ?
Nb1 K3 3.635(3) 5_445 ?
Nb1 K15 3.828(7) . ?
Nb1 K8 3.927(4) 7_545 ?
Nb1 K8 3.927(4) 5_445 ?
Nb2 As4 2.4560(17) . ?
Nb2 As4 2.4560(17) 12_655 ?
Nb2 As5 2.547(3) 9_666 ?
Nb2 As5 2.562(2) . ?
Nb2 K7 3.676(4) . ?
Nb2 K7 3.676(4) 9_666 ?
Nb2 K4 3.792(4) 5 ?
Nb2 K6 3.974(3) 12_655 ?
Nb2 K6 3.974(3) . ?
Nb2 K11 4.011(5) 5 ?
Nb2 K2 4.137(4) 9_666 ?
Nb2 K2 4.137(4) 4_566 ?
Nb3 Nb3 0.000(4) 10_556 ?
Nb3 As7 2.490(2) 10_556 ?
Nb3 As7 2.490(2) . ?
Nb3 As6 2.555(2) . ?
Nb3 As6 2.555(2) 3 ?
Nb3 K8 3.536(4) 3 ?
Nb3 K8 3.536(4) . ?
Nb3 K11 3.858(5) . ?
Nb3 K11 3.858(5) 10_556 ?
Nb3 K1 3.940(6) . ?
Nb4 As9 2.472(3) . ?
Nb4 As10 2.5280(17) . ?
Nb4 As10 2.5281(17) 12 ?
Nb4 As8 2.530(3) . ?
Nb4 K14 3.528(6) . ?
Nb4 K6 3.602(3) . ?
Nb4 K6 3.602(3) 12 ?
Nb4 K4 3.911(4) . ?
Nb4 K3 3.929(3) . ?
Nb4 K3 3.929(3) 12 ?
Nb4 K12 4.078(5) . ?
As1 K15 3.288(8) . ?
As1 K5 3.408(4) 10_556 ?
As1 K5 3.408(4) 3 ?
As1 K6 3.483(3) 16_545 ?
As1 K6 3.483(3) 5_445 ?
As1 K11 3.500(5) . ?
As1 K1 3.595(3) . ?
As1 K3 3.954(3) 16_545 ?
As1 K3 3.954(3) 5_445 ?
As2 K15 3.223(8) . ?
As2 K13 3.336(4) 16_545 ?
As2 K13 3.336(4) 5_445 ?
As2 K8 3.442(4) 7_545 ?
As2 K8 3.442(4) 5_445 ?
As2 K3 3.654(3) 16_545 ?
As2 K3 3.654(3) 5_445 ?
As2 K10 3.852(7) 5_445 ?
As3 Nb1 2.5707(18) 10_556 ?
As3 K8 3.220(4) 5_445 ?
As3 K5 3.383(3) 12 ?
As3 K5 3.384(3) 3 ?
As3 K9 3.412(3) 5_445 ?
As3 K1 3.422(5) . ?
As3 K3 3.673(3) 14_446 ?
As3 K3 3.674(3) 5_445 ?
As4 K13 3.364(4) 5 ?
As4 K7 3.374(2) 9_666 ?
As4 K11 3.436(4) 5 ?
As4 K6 3.461(3) 12_655 ?
As4 K12 3.468(2) 1_655 ?
As4 K4 3.536(4) 5 ?
As4 K2 3.553(4) 9_666 ?
As4 K16 3.901(11) 1_655 ?
As5 Nb2 2.546(3) 9_666 ?
As5 K2 3.381(4) . ?
As5 K2 3.381(4) 12_655 ?
As5 K6 3.425(3) . ?
As5 K6 3.425(3) 12_655 ?
As5 K7 3.717(4) . ?
As5 K7 3.717(4) 9_666 ?
As6 Nb3 2.555(2) 10_556 ?
As6 K10 3.264(3) . ?
As6 K1 3.279(4) . ?
As6 K8 3.546(4) . ?
As6 K5 3.579(3) . ?
As6 K5 3.580(3) 10_556 ?
As6 K13 3.608(4) 10_556 ?
As6 K13 3.608(4) . ?
As6 K11 3.979(4) . ?
As6 K11 3.980(4) 10_556 ?
As7 Nb3 2.490(2) 10_556 ?
As7 K13 3.307(4) 12 ?
As7 K13 3.307(4) . ?
As7 K9 3.420(6) . ?
As7 K4 3.512(5) . ?
As7 K8 3.562(4) 3 ?
As7 K8 3.562(4) . ?
As7 K3 3.608(3) 12 ?
As7 K3 3.609(3) . ?
As7 K11 3.682(5) . ?
As8 K12 3.289(6) . ?
As8 K5 3.297(3) 7 ?
As8 K5 3.297(3) 14_456 ?
As8 K3 3.349(3) . ?
As8 K3 3.349(3) 12 ?
As8 K6 3.590(3) . ?
As8 K6 3.590(3) 12 ?
As9 K2 3.181(4) . ?
As9 K2 3.181(4) 12 ?
As9 K12 3.302(6) . ?
As9 K7 3.363(3) 9_566 ?
As9 K7 3.363(3) . ?
As9 K16 3.746(19) 9_566 ?
As9 K6 3.801(3) . ?
As9 K6 3.801(3) 12 ?
As9 K14 3.857(6) . ?
As10 K2 3.318(4) 13_556 ?
As10 K3 3.354(3) . ?
As10 K15 3.418(3) 5 ?
As10 K4 3.420(3) . ?
As10 K14 3.425(5) . ?
As10 K6 3.437(3) . ?
As10 K2 3.623(4) . ?
As10 K14 3.770(3) 13_556 ?
K1 As6 3.279(4) 3 ?
K1 As3 3.422(5) 3 ?
K1 As1 3.594(3) 10_556 ?
K1 K5 3.613(3) . ?
K1 K5 3.613(3) 12 ?
K1 K5 3.613(3) 10_556 ?
K1 K5 3.613(3) 3 ?
K1 Nb1 3.632(5) 10_556 ?
K2 As10 3.318(4) 13_556 ?
K2 K16 3.475(13) 9_566 ?
K2 K14 3.500(6) 13_556 ?
K2 As4 3.552(4) 9_666 ?
K2 K7 3.669(4) . ?
K2 K14 3.747(6) . ?
K2 K6 3.894(5) . ?
K2 K4 3.938(5) 13_556 ?
K2 Nb2 4.137(4) 9_666 ?
K3 Nb1 3.635(3) 5 ?
K3 As2 3.654(3) 5 ?
K3 As3 3.673(3) 5 ?
K3 K15 3.734(5) 5 ?
K3 K5 3.824(4) 7 ?
K3 K9 3.923(3) . ?
K3 As1 3.954(3) 5 ?
K3 K13 3.966(5) . ?
K4 As10 3.420(3) 12 ?
K4 As4 3.536(4) 5_445 ?
K4 As4 3.536(4) 16_545 ?
K4 Nb2 3.792(4) 5_445 ?
K4 K13 3.937(5) . ?
K4 K13 3.937(5) 12 ?
K4 K2 3.938(5) 13_556 ?
K4 K2 3.938(5) 8_456 ?
K4 K3 3.976(5) 12 ?
K5 As8 3.297(3) 14_546 ?
K5 As3 3.384(3) 3 ?
K5 As1 3.408(4) 10_556 ?
K5 K3 3.824(4) 7_545 ?
K5 K6 3.934(4) 7_545 ?
K5 K11 3.949(4) 10_556 ?
K5 K5 4.123(6) 10_556 ?
K5 K13 4.577(5) 10_556 ?
K5 K5 4.593(7) 12_655 ?
K5 K9 4.633(6) 5_545 ?
K6 As4 3.461(3) 12_655 ?
K6 As1 3.484(3) 5 ?
K6 K12 3.774(4) . ?
K6 K5 3.934(4) 7 ?
K6 K15 3.968(7) 5 ?
K7 As9 3.363(3) 9_566 ?
K7 As4 3.374(2) 9_666 ?
K7 As4 3.374(2) 12_655 ?
K7 K2 3.669(4) 4_566 ?
K7 Nb2 3.676(4) 9_666 ?
K7 As5 3.717(4) 9_666 ?
K7 K12 3.820(5) . ?
K7 K12 3.820(5) 9_566 ?
K8 As3 3.220(4) 5 ?
K8 As2 3.442(4) 14_556 ?
K8 As2 3.442(4) 5 ?
K8 K10 3.465(8) . ?
K8 Nb3 3.536(4) 10_556 ?
K8 As7 3.562(4) 10_556 ?
K8 K13 3.618(4) . ?
K8 K13 3.618(4) 10_556 ?
K8 K9 3.664(6) . ?
K9 As3 3.412(3) 5 ?
K9 As3 3.412(3) 7_455 ?
K9 As7 3.420(6) 10_556 ?
K9 K8 3.664(6) 3 ?
K9 K3 3.922(3) 10_556 ?
K9 K3 3.922(3) 3 ?
K9 K3 3.923(3) 12 ?
K9 K5 4.633(6) 16 ?
K9 K5 4.633(6) 5_455 ?
K10 As6 3.263(3) 3_655 ?
K10 K8 3.465(8) 3_655 ?
K10 As2 3.852(7) 14_556 ?
K10 As2 3.852(7) 5 ?
K10 K13 4.022(4) 12_655 ?
K10 K13 4.022(4) . ?
K10 K13 4.022(4) 3_655 ?
K10 K13 4.022(4) 10_556 ?
K10 K5 4.828(7) 12_655 ?
K11 As4 3.436(4) 5_445 ?
K11 As4 3.436(4) 16_545 ?
K11 K13 3.564(4) 12 ?
K11 K13 3.565(4) . ?
K11 Nb3 3.858(5) 10_556 ?
K11 K5 3.949(4) 10_556 ?
K11 K5 3.949(4) 3 ?
K11 As6 3.979(4) 3 ?
K12 As4 3.467(2) 12_655 ?
K12 As4 3.467(2) 1_455 ?
K12 K16 3.47(2) . ?
K12 K6 3.774(4) 12 ?
K12 K7 3.820(5) 9_566 ?
K12 K13 4.521(6) 16 ?
K12 K13 4.521(6) 5_455 ?
K13 As2 3.336(4) 5 ?
K13 As4 3.364(4) 5_445 ?
K13 K16 3.969(15) 5_545 ?
K13 K12 4.521(6) 5_545 ?
K13 K5 4.577(5) 10_556 ?
K14 K15 3.406(9) 9_556 ?
K14 As10 3.425(5) 12 ?
K14 K2 3.500(6) 13_556 ?
K14 K2 3.500(6) 8_456 ?
K14 K2 3.747(6) 12 ?
K14 As10 3.770(3) 13_556 ?
K14 As10 3.771(3) 8_456 ?
K14 K16 3.921(19) 9_566 ?
K15 K16 3.17(2) 1_545 ?
K15 K14 3.406(9) 9_556 ?
K15 As10 3.418(3) 16_545 ?
K15 As10 3.418(3) 5_445 ?
K15 K3 3.734(5) 16_545 ?
K15 K3 3.734(5) 5_445 ?
K15 K6 3.968(7) 16_545 ?
K15 K6 3.968(7) 5_445 ?
K15 K2 4.893(7) 4_556 ?
K16 K15 3.17(2) 1_565 ?
K16 K2 3.476(13) 4_566 ?
K16 K2 3.476(13) 9_566 ?
K16 As9 3.746(19) 9_566 ?
K16 As4 3.901(11) 12_655 ?
K16 As4 3.901(11) 1_455 ?
K16 K14 3.921(19) 9_566 ?
K16 K13 3.970(15) 16 ?
K16 K13 3.970(15) 5_455 ?
K16 K7 4.725(19) 9_566 ?
