#------------------------------------------------------------------------------
#$Date: 2020-10-19 10:35:42 +0300 (Mon, 19 Oct 2020) $
#$Revision: 258458 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/31/87/4318795.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4318795
loop_
_publ_author_name
'Oleg Volkov'
'Ramón Macías'
'Nigam P. Rath'
'Lawrence Barton'
_publ_section_title
;
 Phosphine-Boranes as Bidentate Ligands: Formation of
 [8,8-η2-{η2-(BH3).dppm}-nido-8,7-RhSB9H10] and
 [9,9-η2-{η2-(BH3).dppm}-nido-9,7,8-RhC2B8H11] from
 [8,8-(η2-dppm)-8-(η1-dppm)-nido-8,7-RhSB9H10] and
 [9,9-(η2-dppm)-9-(η1-dppm)-nido-9,7,8-RhC2B8H11], Respectively
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5837
_journal_page_last               5843
_journal_paper_doi               10.1021/ic0258375
_journal_volume                  41
_journal_year                    2002
_chemical_formula_sum            'C27 H36 B9 P2 Rh'
_chemical_formula_weight         622.70
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                91.269(6)
_cell_angle_beta                 91.546(6)
_cell_angle_gamma                106.672(6)
_cell_formula_units_Z            4
_cell_length_a                   10.8504(9)
_cell_length_b                   16.1632(14)
_cell_length_c                   18.1727(15)
_cell_measurement_reflns_used    6712
_cell_measurement_temperature    140(2)
_cell_measurement_theta_max      27.6
_cell_measurement_theta_min      2.2
_cell_volume                     3050.5(5)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker-SHELXTL (Sheldrick, 2001)'
_computing_publication_material  'Bruker-SHELXTL (Sheldrick, 2001)'
_computing_structure_refinement  'Bruker-SHELXTL (Sheldrick, 2001)'
_computing_structure_solution    'Bruker-SHELXTL (Sheldrick, 2001)'
_diffrn_ambient_temperature      140(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'normal-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0807
_diffrn_reflns_av_sigmaI/netI    0.1184
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            45520
_diffrn_reflns_theta_full        29.00
_diffrn_reflns_theta_max         29.00
_diffrn_reflns_theta_min         1.12
_exptl_absorpt_coefficient_mu    0.682
_exptl_absorpt_correction_T_max  0.9226
_exptl_absorpt_correction_T_min  0.8215
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.356
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       rod
_exptl_crystal_F_000             1272
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.696
_refine_diff_density_min         -1.411
_refine_diff_density_rms         0.142
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     814
_refine_ls_number_reflns         16095
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.1281
_refine_ls_R_factor_gt           0.0633
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0528P)²+12.6681P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1461
_refine_ls_wR_factor_ref         0.1736
_reflns_number_gt                9563
_reflns_number_total             16095
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0258375_s1_2.cif
_cod_data_source_block           Compd4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'no' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

;
_cod_original_cell_volume        3050.5(4)
_cod_database_code               4318795
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh9 Rh 0.54691(4) 0.81071(3) 0.56198(2) 0.02012(11) Uani 1 1 d . . .
Rh9' Rh 0.94659(4) 0.71166(3) 0.05794(2) 0.02198(12) Uani 1 1 d . . .
P1 P 0.53493(14) 0.80601(10) 0.75579(8) 0.0216(3) Uani 1 1 d . . .
P2 P 0.67339(13) 0.74894(10) 0.63149(8) 0.0202(3) Uani 1 1 d . . .
P1' P 0.98318(14) 0.71923(10) 0.25022(8) 0.0216(3) Uani 1 1 d . . .
P2' P 0.80122(13) 0.74436(9) 0.13239(8) 0.0195(3) Uani 1 1 d . . .
B1 B 0.4744(8) 0.7632(6) 0.3813(4) 0.040(2) Uani 1 1 d . . .
B2 B 0.5144(8) 0.8720(6) 0.3577(4) 0.042(2) Uani 1 1 d . . .
B3 B 0.3756(7) 0.8282(5) 0.4057(4) 0.0301(15) Uani 1 1 d . . .
B4 B 0.4128(7) 0.7596(5) 0.4711(4) 0.0304(16) Uani 1 1 d . . .
B5 B 0.5765(7) 0.7532(5) 0.4564(4) 0.0291(15) Uani 1 1 d . . .
B6 B 0.6352(8) 0.8278(6) 0.3869(4) 0.039(2) Uani 1 1 d . . .
B10 B 0.6883(6) 0.8566(5) 0.4809(4) 0.0299(16) Uani 1 1 d . . .
B11 B 0.6377(7) 0.9344(5) 0.4228(4) 0.0359(18) Uani 1 1 d . . .
B' B 0.4562(6) 0.8399(5) 0.6703(4) 0.0232(13) Uani 1 1 d . . .
B1' B 0.9343(7) 0.7408(6) -0.1248(4) 0.0366(18) Uani 1 1 d . . .
B2' B 0.9640(8) 0.6404(6) -0.1464(4) 0.0402(19) Uani 1 1 d . . .
B3' B 1.0889(7) 0.7264(6) -0.1096(4) 0.0366(18) Uani 1 1 d . . .
B4' B 1.0215(7) 0.7792(5) -0.0399(4) 0.0299(16) Uani 1 1 d . . .
B5' B 0.8470(7) 0.7306(5) -0.0428(4) 0.0294(16) Uani 1 1 d . . .
B6' B 0.8171(7) 0.6420(5) -0.1093(4) 0.0314(16) Uani 1 1 d . . .
B10' B 0.8078(7) 0.6219(5) -0.0133(4) 0.0288(15) Uani 1 1 d . . .
B11' B 0.8989(8) 0.5678(5) -0.0757(4) 0.0354(17) Uani 1 1 d . . .
H13' H 0.873(6) 0.568(4) -0.013(4) 0.042 Uiso 1 1 d . . .
B'' B 1.0716(7) 0.7077(5) 0.1612(4) 0.0289(16) Uani 1 1 d . . .
C1 C 0.6870(5) 0.7913(4) 0.7274(3) 0.0248(12) Uani 1 1 d . . .
H1A H 0.7121 0.7505 0.7604 0.030 Uiso 1 1 calc R . .
H1B H 0.7550 0.8473 0.7317 0.030 Uiso 1 1 calc R . .
C7 C 0.4816(6) 0.9235(4) 0.4331(3) 0.0297(13) Uani 1 1 d . . .
C8 C 0.4212(6) 0.8603(4) 0.4925(3) 0.0251(12) Uani 1 1 d . . .
C1' C 0.8154(5) 0.7036(4) 0.2258(3) 0.0213(12) Uani 1 1 d . . .
H1'1 H 0.7772 0.7351 0.2619 0.026 Uiso 1 1 calc R . .
H1'2 H 0.7679 0.6414 0.2268 0.026 Uiso 1 1 calc R . .
C7' C 1.0538(7) 0.6268(5) -0.0749(4) 0.0377(16) Uani 1 1 d . . .
C8' C 1.0891(6) 0.7030(4) -0.0203(3) 0.0315(14) Uani 1 1 d . . .
C1A C 0.4447(5) 0.7059(4) 0.7943(3) 0.0241(12) Uani 1 1 d . . .
C2A C 0.4902(6) 0.6743(4) 0.8559(3) 0.0337(14) Uani 1 1 d . . .
H2A H 0.5691 0.7066 0.8795 0.040 Uiso 1 1 calc R . .
C3A C 0.4227(7) 0.5962(4) 0.8838(4) 0.0396(16) Uani 1 1 d . . .
H3A H 0.4562 0.5739 0.9253 0.048 Uiso 1 1 calc R . .
C4A C 0.3068(6) 0.5511(4) 0.8511(4) 0.0348(15) Uani 1 1 d . . .
H4A H 0.2590 0.4979 0.8706 0.042 Uiso 1 1 calc R . .
C5A C 0.2592(7) 0.5821(5) 0.7904(4) 0.0395(16) Uani 1 1 d . . .
H5A H 0.1788 0.5502 0.7682 0.047 Uiso 1 1 calc R . .
C6A C 0.3269(6) 0.6592(4) 0.7611(3) 0.0309(14) Uani 1 1 d . . .
H6A H 0.2939 0.6803 0.7188 0.037 Uiso 1 1 calc R . .
C7A C 0.5756(6) 0.8901(4) 0.8285(3) 0.0281(13) Uani 1 1 d . . .
C8A C 0.6805(6) 0.9002(4) 0.8761(3) 0.0331(14) Uani 1 1 d . . .
H8A H 0.7325 0.8621 0.8721 0.040 Uiso 1 1 calc R . .
C9A C 0.7102(7) 0.9660(5) 0.9300(4) 0.0430(17) Uani 1 1 d . . .
H9A H 0.7812 0.9721 0.9635 0.052 Uiso 1 1 calc R . .
C10A C 0.6376(10) 1.0213(6) 0.9344(5) 0.076(3) Uani 1 1 d . . .
H10A H 0.6596 1.0675 0.9701 0.091 Uiso 1 1 calc R . .
C11A C 0.5318(12) 1.0112(8) 0.8875(6) 0.111(5) Uani 1 1 d . . .
H11A H 0.4815 1.0503 0.8910 0.133 Uiso 1 1 calc R . .
C12A C 0.4988(9) 0.9437(6) 0.8352(5) 0.075(3) Uani 1 1 d . . .
H12A H 0.4237 0.9348 0.8045 0.089 Uiso 1 1 calc R . .
C13A C 0.8395(5) 0.7574(4) 0.6101(3) 0.0248(12) Uani 1 1 d . . .
C14A C 0.9429(6) 0.8119(5) 0.6489(4) 0.048(2) Uani 1 1 d . . .
H14A H 0.9296 0.8460 0.6895 0.058 Uiso 1 1 calc R . .
C15A C 1.0666(7) 0.8164(6) 0.6282(5) 0.071(3) Uani 1 1 d . . .
H15A H 1.1380 0.8549 0.6543 0.085 Uiso 1 1 calc R . .
C16A C 1.0877(7) 0.7665(5) 0.5709(4) 0.050(2) Uani 1 1 d . . .
H16A H 1.1730 0.7684 0.5585 0.060 Uiso 1 1 calc R . .
C17A C 0.9871(7) 0.7149(4) 0.5324(4) 0.0367(15) Uani 1 1 d . . .
H17A H 1.0017 0.6824 0.4910 0.044 Uiso 1 1 calc R . .
C18A C 0.8624(6) 0.7081(4) 0.5516(3) 0.0332(14) Uani 1 1 d . . .
H18A H 0.7922 0.6694 0.5247 0.040 Uiso 1 1 calc R . .
C19A C 0.6032(5) 0.6337(4) 0.6408(3) 0.0249(12) Uani 1 1 d . . .
C20A C 0.4977(6) 0.5885(4) 0.5967(3) 0.0306(14) Uani 1 1 d . . .
H20A H 0.4622 0.6185 0.5614 0.037 Uiso 1 1 calc R . .
C21A C 0.4438(7) 0.5006(4) 0.6033(4) 0.0391(16) Uani 1 1 d . . .
H21A H 0.3729 0.4702 0.5721 0.047 Uiso 1 1 calc R . .
C22A C 0.4934(7) 0.4576(5) 0.6554(4) 0.0397(16) Uani 1 1 d . . .
H22A H 0.4547 0.3975 0.6612 0.048 Uiso 1 1 calc R . .
C23A C 0.5974(7) 0.5002(4) 0.6989(4) 0.0380(16) Uani 1 1 d . . .
H23A H 0.6310 0.4695 0.7345 0.046 Uiso 1 1 calc R . .
C24A C 0.6549(6) 0.5883(4) 0.6919(3) 0.0317(14) Uani 1 1 d . . .
H24A H 0.7287 0.6174 0.7216 0.038 Uiso 1 1 calc R . .
C1B C 0.9937(6) 0.6380(4) 0.3144(3) 0.0272(13) Uani 1 1 d . . .
C2B C 0.8884(7) 0.5833(5) 0.3452(4) 0.0411(17) Uani 1 1 d . . .
H2B H 0.8055 0.5903 0.3360 0.049 Uiso 1 1 calc R . .
C3B C 0.9022(8) 0.5174(5) 0.3900(4) 0.050(2) Uani 1 1 d . . .
H3B H 0.8289 0.4792 0.4108 0.060 Uiso 1 1 calc R . .
C4B C 1.0213(9) 0.5081(5) 0.4035(4) 0.052(2) Uani 1 1 d . . .
H4B H 1.0303 0.4615 0.4321 0.062 Uiso 1 1 calc R . .
C5B C 1.1313(8) 0.5664(5) 0.3759(4) 0.053(2) Uani 1 1 d . . .
H5B H 1.2145 0.5617 0.3884 0.063 Uiso 1 1 calc R . .
C6B C 1.1173(7) 0.6308(5) 0.3301(4) 0.0404(16) Uani 1 1 d . . .
H6B H 1.1905 0.6696 0.3097 0.048 Uiso 1 1 calc R . .
C7B C 1.0457(5) 0.8230(4) 0.2969(3) 0.0235(12) Uani 1 1 d . . .
C8B C 1.1468(6) 0.8840(4) 0.2670(3) 0.0349(15) Uani 1 1 d . . .
H8B H 1.1803 0.8719 0.2215 0.042 Uiso 1 1 calc R . .
C9B C 1.1994(7) 0.9631(4) 0.3037(4) 0.0438(18) Uani 1 1 d . . .
H9B H 1.2690 1.0051 0.2832 0.053 Uiso 1 1 calc R . .
C10B C 1.1518(7) 0.9807(4) 0.3688(4) 0.0419(17) Uani 1 1 d . . .
H10B H 1.1896 1.0346 0.3940 0.050 Uiso 1 1 calc R . .
C11B C 1.0495(7) 0.9213(5) 0.3984(4) 0.0455(18) Uani 1 1 d . . .
H11B H 1.0154 0.9348 0.4432 0.055 Uiso 1 1 calc R . .
C12B C 0.9961(6) 0.8416(4) 0.3629(3) 0.0328(14) Uani 1 1 d . . .
H12B H 0.9260 0.8001 0.3835 0.039 Uiso 1 1 calc R . .
C13B C 0.8306(5) 0.8602(4) 0.1506(3) 0.0224(12) Uani 1 1 d . . .
C14B C 0.9263(6) 0.9196(4) 0.1153(4) 0.0344(15) Uani 1 1 d . . .
H14B H 0.9772 0.9005 0.0807 0.041 Uiso 1 1 calc R . .
C15B C 0.9479(7) 1.0065(4) 0.1303(5) 0.0464(19) Uani 1 1 d . . .
H15B H 1.0131 1.0473 0.1053 0.056 Uiso 1 1 calc R . .
C16B C 0.8756(6) 1.0353(4) 0.1814(4) 0.0387(16) Uani 1 1 d . . .
H16B H 0.8913 1.0954 0.1915 0.046 Uiso 1 1 calc R . .
C17B C 0.7816(7) 0.9766(4) 0.2173(3) 0.0343(15) Uani 1 1 d . . .
H17B H 0.7336 0.9959 0.2535 0.041 Uiso 1 1 calc R . .
C18B C 0.7563(6) 0.8894(4) 0.2011(3) 0.0281(13) Uani 1 1 d . . .
H18B H 0.6882 0.8490 0.2243 0.034 Uiso 1 1 calc R . .
C19B C 0.6300(5) 0.7077(4) 0.1115(3) 0.0209(11) Uani 1 1 d . . .
C20B C 0.5749(6) 0.7597(4) 0.0686(3) 0.0304(14) Uani 1 1 d . . .
H20B H 0.6256 0.8147 0.0539 0.036 Uiso 1 1 calc R . .
C21B C 0.4454(6) 0.7297(4) 0.0477(4) 0.0350(15) Uani 1 1 d . . .
H21B H 0.4077 0.7649 0.0188 0.042 Uiso 1 1 calc R . .
C22B C 0.3715(6) 0.6512(4) 0.0676(4) 0.0349(15) Uani 1 1 d . . .
H22B H 0.2830 0.6320 0.0528 0.042 Uiso 1 1 calc R . .
C23B C 0.4248(6) 0.5991(4) 0.1092(4) 0.0340(15) Uani 1 1 d . . .
H23B H 0.3734 0.5437 0.1227 0.041 Uiso 1 1 calc R . .
C24B C 0.5529(5) 0.6277(4) 0.1312(3) 0.0274(13) Uani 1 1 d . . .
H24B H 0.5889 0.5918 0.1605 0.033 Uiso 1 1 calc R . .
H1 H 0.442(7) 0.718(5) 0.339(4) 0.05(2) Uiso 1 1 d . . .
H2 H 0.517(7) 0.909(5) 0.301(4) 0.06(2) Uiso 1 1 d . . .
H3 H 0.285(6) 0.826(4) 0.389(3) 0.024(15) Uiso 1 1 d . . .
H4 H 0.325(6) 0.694(4) 0.484(3) 0.034(17) Uiso 1 1 d . . .
H5 H 0.600(6) 0.684(4) 0.460(3) 0.027(16) Uiso 1 1 d . . .
H6 H 0.715(7) 0.824(5) 0.349(4) 0.05(2) Uiso 1 1 d . . .
H7 H 0.445(5) 0.972(3) 0.427(3) 0.011(13) Uiso 1 1 d . . .
H8 H 0.344(5) 0.873(3) 0.520(3) 0.012(13) Uiso 1 1 d . . .
H10 H 0.784(6) 0.863(4) 0.494(3) 0.028(16) Uiso 1 1 d . . .
H11 H 0.704(5) 1.000(3) 0.401(3) 0.016(14) Uiso 1 1 d . . .
H12B H 0.427(5) 0.783(4) 0.632(3) 0.016(14) Uiso 1 1 d . . .
H12C H 0.384(6) 0.866(4) 0.681(3) 0.024(15) Uiso 1 1 d . . .
H12D H 0.538(6) 0.902(4) 0.643(3) 0.039(19) Uiso 1 1 d . . .
H13 H 0.654(6) 0.928(4) 0.495(3) 0.025(16) Uiso 1 1 d . . .
H1' H 0.912(5) 0.779(4) -0.170(3) 0.022(15) Uiso 1 1 d . . .
H2' H 0.969(5) 0.609(4) -0.203(3) 0.022(15) Uiso 1 1 d . . .
H3' H 1.181(6) 0.754(4) -0.137(3) 0.038(18) Uiso 1 1 d . . .
H4' H 1.070(5) 0.849(4) -0.027(3) 0.021(15) Uiso 1 1 d . . .
H5' H 0.774(5) 0.765(3) -0.038(3) 0.015(14) Uiso 1 1 d . . .
H7' H 1.108(7) 0.589(5) -0.084(4) 0.05(2) Uiso 1 1 d . . .
H6' H 0.728(6) 0.619(4) -0.143(3) 0.023(15) Uiso 1 1 d . . .
H8' H 1.188(8) 0.719(5) 0.003(4) 0.08(3) Uiso 1 1 d . . .
H10' H 0.711(6) 0.587(4) 0.011(3) 0.026(16) Uiso 1 1 d . . .
H11' H 0.876(6) 0.499(4) -0.094(3) 0.036(18) Uiso 1 1 d . . .
H12E H 1.173(6) 0.702(4) 0.174(3) 0.034(17) Uiso 1 1 d . . .
H12F H 0.977(5) 0.657(3) 0.123(3) 0.014(14) Uiso 1 1 d . . .
H12G H 1.084(6) 0.776(4) 0.127(3) 0.033(17) Uiso 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B10 Rh9 B4 86.6(3) . . ?
B10 Rh9 C8 85.7(3) . . ?
B4 Rh9 C8 44.7(3) . . ?
B10 Rh9 B5 49.1(3) . . ?
B4 Rh9 B5 50.0(3) . . ?
C8 Rh9 B5 80.8(2) . . ?
B10 Rh9 P2 94.7(2) . . ?
B4 Rh9 P2 131.3(2) . . ?
C8 Rh9 P2 175.94(16) . . ?
B5 Rh9 P2 96.37(19) . . ?
B10 Rh9 B' 147.4(3) . . ?
B4 Rh9 B' 115.5(3) . . ?
C8 Rh9 B' 93.9(2) . . ?
B5 Rh9 B' 162.7(3) . . ?
P2 Rh9 B' 87.97(16) . . ?
B10 Rh9 H12B 174.1(18) . . ?
B4 Rh9 H12B 95.0(17) . . ?
C8 Rh9 H12B 91.4(17) . . ?
B5 Rh9 H12B 135.5(18) . . ?
P2 Rh9 H12B 88.5(17) . . ?
B' Rh9 H12B 27.5(17) . . ?
B10 Rh9 H12D 115.2(18) . . ?
B4 Rh9 H12D 128.3(18) . . ?
C8 Rh9 H12D 88.6(18) . . ?
B5 Rh9 H12D 161.4(18) . . ?
P2 Rh9 H12D 94.9(18) . . ?
B' Rh9 H12D 32.4(18) . . ?
H12B Rh9 H12D 59(2) . . ?
B10' Rh9' C8' 87.0(3) . . ?
B10' Rh9' B4' 87.1(3) . . ?
C8' Rh9' B4' 44.8(3) . . ?
B10' Rh9' B5' 48.8(3) . . ?
C8' Rh9' B5' 80.8(2) . . ?
B4' Rh9' B5' 49.9(3) . . ?
B10' Rh9' P2' 96.03(19) . . ?
C8' Rh9' P2' 169.90(19) . . ?
B4' Rh9' P2' 125.6(2) . . ?
B5' Rh9' P2' 93.89(18) . . ?
B10' Rh9' B'' 137.9(3) . . ?
C8' Rh9' B'' 95.8(2) . . ?
B4' Rh9' B'' 123.5(3) . . ?
B5' Rh9' B'' 172.7(3) . . ?
P2' Rh9' B'' 88.45(17) . . ?
B10' Rh9' H12F 105.7(19) . . ?
C8' Rh9' H12F 101.9(19) . . ?
B4' Rh9' H12F 144.5(19) . . ?
B5' Rh9' H12F 154.4(19) . . ?
P2' Rh9' H12F 86.6(19) . . ?
B'' Rh9' H12F 32.6(19) . . ?
B10' Rh9' H12G 169.7(19) . . ?
C8' Rh9' H12G 89.5(18) . . ?
B4' Rh9' H12G 97.2(18) . . ?
B5' Rh9' H12G 140.0(19) . . ?
P2' Rh9' H12G 89.1(18) . . ?
B'' Rh9' H12G 33.0(18) . . ?
H12F Rh9' H12G 66(3) . . ?
C1A P1 C1 106.9(3) . . ?
C1A P1 C7A 109.0(3) . . ?
C1 P1 C7A 106.1(3) . . ?
C1A P1 B' 115.2(3) . . ?
C1 P1 B' 106.7(3) . . ?
C7A P1 B' 112.5(3) . . ?
C19A P2 C13A 102.8(3) . . ?
C19A P2 C1 103.1(3) . . ?
C13A P2 C1 103.1(3) . . ?
C19A P2 Rh9 113.01(19) . . ?
C13A P2 Rh9 122.72(19) . . ?
C1 P2 Rh9 110.02(19) . . ?
C1B P1' C7B 107.5(3) . . ?
C1B P1' C1' 108.3(3) . . ?
C7B P1' C1' 108.6(3) . . ?
C1B P1' B'' 110.7(3) . . ?
C7B P1' B'' 113.5(3) . . ?
C1' P1' B'' 108.2(3) . . ?
C19B P2' C13B 102.8(3) . . ?
C19B P2' C1' 103.1(2) . . ?
C13B P2' C1' 102.3(3) . . ?
C19B P2' Rh9' 122.27(19) . . ?
C13B P2' Rh9' 113.82(19) . . ?
C1' P2' Rh9' 110.19(19) . . ?
B2 B1 B6 59.5(5) . . ?
B2 B1 B3 59.3(5) . . ?
B6 B1 B3 108.2(6) . . ?
B2 B1 B5 108.5(6) . . ?
B6 B1 B5 60.1(4) . . ?
B3 B1 B5 111.4(5) . . ?
B2 B1 B4 105.6(5) . . ?
B6 B1 B4 107.6(5) . . ?
B3 B1 B4 59.6(4) . . ?
B5 B1 B4 62.2(4) . . ?
B2 B1 H1 117(4) . . ?
B6 B1 H1 121(4) . . ?
B3 B1 H1 118(4) . . ?
B5 B1 H1 125(4) . . ?
B4 B1 H1 127(4) . . ?
C7 B2 B3 59.2(4) . . ?
C7 B2 B6 104.8(5) . . ?
B3 B2 B6 110.1(6) . . ?
C7 B2 B1 104.4(5) . . ?
B3 B2 B1 60.6(5) . . ?
B6 B2 B1 60.4(5) . . ?
C7 B2 B11 56.7(4) . . ?
B3 B2 B11 108.0(5) . . ?
B6 B2 B11 61.6(5) . . ?
B1 B2 B11 108.6(5) . . ?
C7 B2 H2 116(4) . . ?
B3 B2 H2 124(4) . . ?
B6 B2 H2 123(4) . . ?
B1 B2 H2 135(4) . . ?
B11 B2 H2 111(4) . . ?
C8 B3 C7 54.2(4) . . ?
C8 B3 B2 103.1(5) . . ?
C7 B3 B2 58.9(4) . . ?
C8 B3 B4 57.2(4) . . ?
C7 B3 B4 100.3(5) . . ?
B2 B3 B4 107.0(5) . . ?
C8 B3 B1 104.2(5) . . ?
C7 B3 B1 103.7(5) . . ?
B2 B3 B1 60.1(5) . . ?
B4 B3 B1 60.6(4) . . ?
C8 B3 H3 118(3) . . ?
C7 B3 H3 120(3) . . ?
B2 B3 H3 126(3) . . ?
B4 B3 H3 125(3) . . ?
B1 B3 H3 131(3) . . ?
C8 B4 B3 58.5(4) . . ?
C8 B4 B1 104.6(5) . . ?
B3 B4 B1 59.7(4) . . ?
C8 B4 B5 108.2(5) . . ?
B3 B4 B5 108.7(5) . . ?
B1 B4 B5 58.8(4) . . ?
C8 B4 Rh9 67.9(3) . . ?
B3 B4 Rh9 121.0(4) . . ?
B1 B4 Rh9 118.0(4) . . ?
B5 B4 Rh9 65.8(3) . . ?
C8 B4 H4 128(3) . . ?
B3 B4 H4 116(3) . . ?
B1 B4 H4 116(3) . . ?
B5 B4 H4 120(3) . . ?
Rh9 B4 H4 115(3) . . ?
B6 B5 B1 59.5(5) . . ?
B6 B5 B10 60.4(4) . . ?
B1 B5 B10 110.1(6) . . ?
B6 B5 B4 104.6(5) . . ?
B1 B5 B4 58.9(4) . . ?
B10 B5 B4 108.5(5) . . ?
B6 B5 Rh9 115.1(5) . . ?
B1 B5 Rh9 116.6(5) . . ?
B10 B5 Rh9 64.2(3) . . ?
B4 B5 Rh9 64.2(3) . . ?
B6 B5 H5 123(3) . . ?
B1 B5 H5 116(3) . . ?
B10 B5 H5 125(3) . . ?
B4 B5 H5 120(3) . . ?
Rh9 B5 H5 115(3) . . ?
B2 B6 B1 60.1(5) . . ?
B2 B6 B5 109.3(6) . . ?
B1 B6 B5 60.5(4) . . ?
B2 B6 B10 113.1(6) . . ?
B1 B6 B10 111.2(5) . . ?
B5 B6 B10 60.7(4) . . ?
B2 B6 B11 61.2(5) . . ?
B1 B6 B11 108.0(5) . . ?
B5 B6 B11 107.5(5) . . ?
B10 B6 B11 61.5(4) . . ?
B2 B6 H6 121(4) . . ?
B1 B6 H6 127(4) . . ?
B5 B6 H6 124(4) . . ?
B10 B6 H6 114(4) . . ?
B11 B6 H6 117(4) . . ?
B6 B10 B5 58.9(4) . . ?
B6 B10 B11 60.0(4) . . ?
B5 B10 B11 105.0(5) . . ?
B6 B10 Rh9 115.8(4) . . ?
B5 B10 Rh9 66.6(3) . . ?
B11 B10 Rh9 109.0(4) . . ?
B6 B10 H10 117(3) . . ?
B5 B10 H10 122(3) . . ?
B11 B10 H10 122(3) . . ?
Rh9 B10 H10 120(3) . . ?
B6 B10 H13 104(3) . . ?
B5 B10 H13 124(3) . . ?
B11 B10 H13 46(2) . . ?
Rh9 B10 H13 80(2) . . ?
H10 B10 H13 113(4) . . ?
C7 B11 B2 57.7(4) . . ?
C7 B11 B6 102.1(5) . . ?
B2 B11 B6 57.2(4) . . ?
C7 B11 B10 109.7(5) . . ?
B2 B11 B10 107.2(6) . . ?
B6 B11 B10 58.6(4) . . ?
C7 B11 H11 119(3) . . ?
B2 B11 H11 115(3) . . ?
B6 B11 H11 124(3) . . ?
B10 B11 H11 127(3) . . ?
C7 B11 H13 90(3) . . ?
B2 B11 H13 131(3) . . ?
B6 B11 H13 103(3) . . ?
B10 B11 H13 46(3) . . ?
H11 B11 H13 112(4) . . ?
P1 B' Rh9 112.3(3) . . ?
P1 B' H12B 107(3) . . ?
Rh9 B' H12B 49(3) . . ?
P1 B' H12C 115(3) . . ?
Rh9 B' H12C 133(3) . . ?
H12B B' H12C 113(4) . . ?
P1 B' H12D 108(3) . . ?
Rh9 B' H12D 63(3) . . ?
H12B B' H12D 112(4) . . ?
H12C B' H12D 102(4) . . ?
B6' B1' B5' 61.3(4) . . ?
B6' B1' B3' 108.5(6) . . ?
B5' B1' B3' 112.0(5) . . ?
B6' B1' B2' 59.3(5) . . ?
B5' B1' B2' 108.9(5) . . ?
B3' B1' B2' 58.9(5) . . ?
B6' B1' B4' 108.6(5) . . ?
B5' B1' B4' 61.8(4) . . ?
B3' B1' B4' 60.5(4) . . ?
B2' B1' B4' 105.9(5) . . ?
B6' B1' H1' 116(3) . . ?
B5' B1' H1' 120(3) . . ?
B3' B1' H1' 123(3) . . ?
B2' B1' H1' 119(3) . . ?
B4' B1' H1' 128(3) . . ?
C7' B2' B3' 59.3(5) . . ?
C7' B2' B6' 105.0(5) . . ?
B3' B2' B6' 110.3(6) . . ?
C7' B2' B1' 103.3(6) . . ?
B3' B2' B1' 60.4(5) . . ?
B6' B2' B1' 59.9(4) . . ?
C7' B2' B11' 58.2(4) . . ?
B3' B2' B11' 109.7(5) . . ?
B6' B2' B11' 61.0(4) . . ?
B1' B2' B11' 107.8(5) . . ?
C7' B2' H2' 122(3) . . ?
B3' B2' H2' 122(3) . . ?
B6' B2' H2' 122(3) . . ?
B1' B2' H2' 129(3) . . ?
B11' B2' H2' 116(3) . . ?
C8' B3' C7' 53.7(4) . . ?
C8' B3' B2' 102.0(5) . . ?
C7' B3' B2' 57.8(5) . . ?
C8' B3' B1' 102.9(5) . . ?
C7' B3' B1' 102.5(5) . . ?
B2' B3' B1' 60.8(5) . . ?
C8' B3' B4' 56.5(4) . . ?
C7' B3' B4' 99.2(5) . . ?
B2' B3' B4' 107.1(5) . . ?
B1' B3' B4' 60.2(4) . . ?
C8' B3' H3' 120(3) . . ?
C7' B3' H3' 121(3) . . ?
B2' B3' H3' 124(3) . . ?
B1' B3' H3' 131(3) . . ?
B4' B3' H3' 126(3) . . ?
C8' B4' B1' 103.3(6) . . ?
C8' B4' B3' 58.0(4) . . ?
B1' B4' B3' 59.3(4) . . ?
C8' B4' B5' 107.8(5) . . ?
B1' B4' B5' 58.6(4) . . ?
B3' B4' B5' 108.3(5) . . ?
C8' B4' Rh9' 67.6(3) . . ?
B1' B4' Rh9' 116.7(4) . . ?
B3' B4' Rh9' 120.1(5) . . ?
B5' B4' Rh9' 65.4(3) . . ?
C8' B4' H4' 123(3) . . ?
B1' B4' H4' 123(3) . . ?
B3' B4' H4' 118(3) . . ?
B5' B4' H4' 124(3) . . ?
Rh9' B4' H4' 111(3) . . ?
B1' B5' B10' 110.0(5) . . ?
B1' B5' B6' 59.2(4) . . ?
B10' B5' B6' 59.6(4) . . ?
B1' B5' B4' 59.6(4) . . ?
B10' B5' B4' 110.4(5) . . ?
B6' B5' B4' 105.2(5) . . ?
B1' B5' Rh9' 116.9(4) . . ?
B10' B5' Rh9' 64.8(3) . . ?
B6' B5' Rh9' 114.2(4) . . ?
B4' B5' Rh9' 64.7(3) . . ?
B1' B5' H5' 119(3) . . ?
B10' B5' H5' 118(3) . . ?
B6' B5' H5' 118(3) . . ?
B4' B5' H5' 126(3) . . ?
Rh9' B5' H5' 117(3) . . ?
B2' B6' B1' 60.8(5) . . ?
B2' B6' B10' 113.8(5) . . ?
B1' B6' B10' 110.4(5) . . ?
B2' B6' B11' 60.2(4) . . ?
B1' B6' B11' 107.8(5) . . ?
B10' B6' B11' 63.5(4) . . ?
B2' B6' B5' 108.7(5) . . ?
B1' B6' B5' 59.5(4) . . ?
B10' B6' B5' 59.7(4) . . ?
B11' B6' B5' 107.4(5) . . ?
B2' B6' H6' 120(3) . . ?
B1' B6' H6' 122(3) . . ?
B10' B6' H6' 117(3) . . ?
B11' B6' H6' 121(3) . . ?
B5' B6' H6' 123(3) . . ?
B6' B10' B5' 60.7(4) . . ?
B6' B10' B11' 58.5(4) . . ?
B5' B10' B11' 104.5(5) . . ?
B6' B10' Rh9' 116.4(4) . . ?
B5' B10' Rh9' 66.4(3) . . ?
B11' B10' Rh9' 107.4(4) . . ?
B6' B10' H13' 97(3) . . ?
B5' B10' H13' 131(3) . . ?
B11' B10' H13' 38(3) . . ?
Rh9' B10' H13' 92(3) . . ?
B6' B10' H10' 120(3) . . ?
B5' B10' H10' 123(3) . . ?
B11' B10' H10' 124(3) . . ?
Rh9' B10' H10' 118(3) . . ?
H13' B10' H10' 106(4) . . ?
C7' B11' B2' 57.3(4) . . ?
C7' B11' B6' 102.5(6) . . ?
B2' B11' B6' 58.8(4) . . ?
C7' B11' B10' 109.2(5) . . ?
B2' B11' B10' 108.0(6) . . ?
B6' B11' B10' 58.0(4) . . ?
C7' B11' H13' 103(3) . . ?
B2' B11' H13' 141(3) . . ?
B6' B11' H13' 100(3) . . ?
B10' B11' H13' 42(3) . . ?
C7' B11' H11' 118(3) . . ?
B2' B11' H11' 113(3) . . ?
B6' B11' H11' 125(3) . . ?
B10' B11' H11' 129(3) . . ?
H13' B11' H11' 106(5) . . ?
P1' B'' Rh9' 111.3(3) . . ?
P1' B'' H12E 111(3) . . ?
Rh9' B'' H12E 137(3) . . ?
P1' B'' H12F 99(2) . . ?
Rh9' B'' H12F 41(2) . . ?
H12E B'' H12F 131(4) . . ?
P1' B'' H12G 107(3) . . ?
Rh9' B'' H12G 58(3) . . ?
H12E B'' H12G 107(4) . . ?
H12F B'' H12G 99(4) . . ?
P1 C1 P2 110.8(3) . . ?
P1 C1 H1A 109.5 . . ?
P2 C1 H1A 109.5 . . ?
P1 C1 H1B 109.5 . . ?
P2 C1 H1B 109.5 . . ?
H1A C1 H1B 108.1 . . ?
C8 C7 B11 113.6(5) . . ?
C8 C7 B2 111.8(6) . . ?
B11 C7 B2 65.5(5) . . ?
C8 C7 B3 62.0(4) . . ?
B11 C7 B3 117.6(5) . . ?
B2 C7 B3 61.9(5) . . ?
C8 C7 H7 115(3) . . ?
B11 C7 H7 122(3) . . ?
B2 C7 H7 120(3) . . ?
B3 C7 H7 112(3) . . ?
C7 C8 B4 113.4(5) . . ?
C7 C8 B3 63.8(4) . . ?
B4 C8 B3 64.3(4) . . ?
C7 C8 Rh9 118.3(4) . . ?
B4 C8 Rh9 67.5(3) . . ?
B3 C8 Rh9 125.7(4) . . ?
C7 C8 H8 116(3) . . ?
B4 C8 H8 118(3) . . ?
B3 C8 H8 110(3) . . ?
Rh9 C8 H8 114(3) . . ?
P1' C1' P2' 109.4(3) . . ?
P1' C1' H1'1 109.8 . . ?
P2' C1' H1'1 109.8 . . ?
P1' C1' H1'2 109.8 . . ?
P2' C1' H1'2 109.8 . . ?
H1'1 C1' H1'2 108.2 . . ?
C8' C7' B2' 113.4(6) . . ?
C8' C7' B11' 114.8(5) . . ?
B2' C7' B11' 64.5(5) . . ?
C8' C7' B3' 62.7(5) . . ?
B2' C7' B3' 62.9(5) . . ?
B11' C7' B3' 118.0(6) . . ?
C8' C7' H7' 124(4) . . ?
B2' C7' H7' 116(4) . . ?
B11' C7' H7' 109(4) . . ?
B3' C7' H7' 121(4) . . ?
C7' C8' B4' 113.9(5) . . ?
C7' C8' B3' 63.5(5) . . ?
B4' C8' B3' 65.5(4) . . ?
C7' C8' Rh9' 117.4(4) . . ?
B4' C8' Rh9' 67.6(3) . . ?
B3' C8' Rh9' 126.6(4) . . ?
C7' C8' H8' 114(4) . . ?
B4' C8' H8' 121(4) . . ?
B3' C8' H8' 111(4) . . ?
Rh9' C8' H8' 114(4) . . ?
C2A C1A C6A 119.3(6) . . ?
C2A C1A P1 121.0(5) . . ?
C6A C1A P1 119.7(5) . . ?
C3A C2A C1A 120.8(6) . . ?
C3A C2A H2A 119.6 . . ?
C1A C2A H2A 119.6 . . ?
C4A C3A C2A 119.4(6) . . ?
C4A C3A H3A 120.3 . . ?
C2A C3A H3A 120.3 . . ?
C5A C4A C3A 120.6(6) . . ?
C5A C4A H4A 119.7 . . ?
C3A C4A H4A 119.7 . . ?
C4A C5A C6A 120.6(6) . . ?
C4A C5A H5A 119.7 . . ?
C6A C5A H5A 119.7 . . ?
C5A C6A C1A 119.3(6) . . ?
C5A C6A H6A 120.3 . . ?
C1A C6A H6A 120.3 . . ?
C12A C7A C8A 120.0(6) . . ?
C12A C7A P1 118.4(5) . . ?
C8A C7A P1 121.6(5) . . ?
C7A C8A C9A 120.1(6) . . ?
C7A C8A H8A 119.9 . . ?
C9A C8A H8A 119.9 . . ?
C10A C9A C8A 119.7(7) . . ?
C10A C9A H9A 120.1 . . ?
C8A C9A H9A 120.1 . . ?
C9A C10A C11A 120.5(8) . . ?
C9A C10A H10A 119.7 . . ?
C11A C10A H10A 119.7 . . ?
C10A C11A C12A 120.1(8) . . ?
C10A C11A H11A 119.9 . . ?
C12A C11A H11A 119.9 . . ?
C7A C12A C11A 119.4(8) . . ?
C7A C12A H12A 120.3 . . ?
C11A C12A H12A 120.3 . . ?
C14A C13A C18A 118.8(6) . . ?
C14A C13A P2 122.6(5) . . ?
C18A C13A P2 118.6(5) . . ?
C13A C14A C15A 119.3(7) . . ?
C13A C14A H14A 120.3 . . ?
C15A C14A H14A 120.3 . . ?
C16A C15A C14A 121.2(7) . . ?
C16A C15A H15A 119.4 . . ?
C14A C15A H15A 119.4 . . ?
C17A C16A C15A 119.3(7) . . ?
C17A C16A H16A 120.3 . . ?
C15A C16A H16A 120.3 . . ?
C16A C17A C18A 121.2(6) . . ?
C16A C17A H17A 119.4 . . ?
C18A C17A H17A 119.4 . . ?
C17A C18A C13A 120.1(6) . . ?
C17A C18A H18A 119.9 . . ?
C13A C18A H18A 119.9 . . ?
C20A C19A C24A 118.7(6) . . ?
C20A C19A P2 120.6(5) . . ?
C24A C19A P2 120.7(5) . . ?
C21A C20A C19A 121.0(6) . . ?
C21A C20A H20A 119.5 . . ?
C19A C20A H20A 119.5 . . ?
C22A C21A C20A 119.5(6) . . ?
C22A C21A H21A 120.2 . . ?
C20A C21A H21A 120.2 . . ?
C23A C22A C21A 120.6(6) . . ?
C23A C22A H22A 119.7 . . ?
C21A C22A H22A 119.7 . . ?
C22A C23A C24A 120.7(6) . . ?
C22A C23A H23A 119.6 . . ?
C24A C23A H23A 119.6 . . ?
C23A C24A C19A 119.4(6) . . ?
C23A C24A H24A 120.3 . . ?
C19A C24A H24A 120.3 . . ?
C2B C1B C6B 120.4(6) . . ?
C2B C1B P1' 123.3(5) . . ?
C6B C1B P1' 116.2(5) . . ?
C1B C2B C3B 120.4(7) . . ?
C1B C2B H2B 119.8 . . ?
C3B C2B H2B 119.8 . . ?
C4B C3B C2B 119.6(7) . . ?
C4B C3B H3B 120.2 . . ?
C2B C3B H3B 120.2 . . ?
C3B C4B C5B 120.9(7) . . ?
C3B C4B H4B 119.6 . . ?
C5B C4B H4B 119.6 . . ?
C6B C5B C4B 119.4(7) . . ?
C6B C5B H5B 120.3 . . ?
C4B C5B H5B 120.3 . . ?
C5B C6B C1B 119.2(7) . . ?
C5B C6B H6B 120.4 . . ?
C1B C6B H6B 120.4 . . ?
C8B C7B C12B 119.8(6) . . ?
C8B C7B P1' 118.9(5) . . ?
C12B C7B P1' 121.2(4) . . ?
C7B C8B C9B 119.7(6) . . ?
C7B C8B H8B 120.2 . . ?
C9B C8B H8B 120.2 . . ?
C10B C9B C8B 120.4(6) . . ?
C10B C9B H9B 119.8 . . ?
C8B C9B H9B 119.8 . . ?
C9B C10B C11B 120.5(6) . . ?
C9B C10B H10B 119.7 . . ?
C11B C10B H10B 119.7 . . ?
C10B C11B C12B 120.0(7) . . ?
C10B C11B H11B 120.0 . . ?
C12B C11B H11B 120.0 . . ?
C11B C12B C7B 119.6(6) . . ?
C11B C12B H12B 120.2 . . ?
C7B C12B H12B 120.2 . . ?
C14B C13B C18B 119.3(6) . . ?
C14B C13B P2' 120.6(5) . . ?
C18B C13B P2' 120.0(4) . . ?
C15B C14B C13B 119.8(6) . . ?
C15B C14B H14B 120.1 . . ?
C13B C14B H14B 120.1 . . ?
C14B C15B C16B 120.7(6) . . ?
C14B C15B H15B 119.6 . . ?
C16B C15B H15B 119.6 . . ?
C17B C16B C15B 119.7(6) . . ?
C17B C16B H16B 120.2 . . ?
C15B C16B H16B 120.2 . . ?
C16B C17B C18B 120.1(6) . . ?
C16B C17B H17B 119.9 . . ?
C18B C17B H17B 119.9 . . ?
C17B C18B C13B 120.2(6) . . ?
C17B C18B H18B 119.9 . . ?
C13B C18B H18B 119.9 . . ?
C24B C19B C20B 118.5(5) . . ?
C24B C19B P2' 122.8(4) . . ?
C20B C19B P2' 118.5(4) . . ?
C21B C20B C19B 119.1(6) . . ?
C21B C20B H20B 120.4 . . ?
C19B C20B H20B 120.4 . . ?
C22B C21B C20B 121.4(6) . . ?
C22B C21B H21B 119.3 . . ?
C20B C21B H21B 119.3 . . ?
C21B C22B C23B 120.0(6) . . ?
C21B C22B H22B 120.0 . . ?
C23B C22B H22B 120.0 . . ?
C24B C23B C22B 119.7(6) . . ?
C24B C23B H23B 120.1 . . ?
C22B C23B H23B 120.1 . . ?
C23B C24B C19B 121.1(6) . . ?
C23B C24B H24B 119.4 . . ?
C19B C24B H24B 119.4 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh9 B10 2.144(7) . ?
Rh9 B4 2.156(7) . ?
Rh9 C8 2.162(6) . ?
Rh9 B5 2.185(7) . ?
Rh9 P2 2.2857(15) . ?
Rh9 B' 2.323(7) . ?
Rh9 H12B 1.81(5) . ?
Rh9 H12D 2.08(6) . ?
Rh9' B10' 2.146(7) . ?
Rh9' C8' 2.161(6) . ?
Rh9' B4' 2.161(7) . ?
Rh9' B5' 2.173(7) . ?
Rh9' P2' 2.2715(15) . ?
Rh9' B'' 2.298(7) . ?
Rh9' H12F 1.57(5) . ?
Rh9' H12G 1.95(6) . ?
P1 C1A 1.801(6) . ?
P1 C1 1.820(6) . ?
P1 C7A 1.825(6) . ?
P1 B' 1.918(7) . ?
P2 C19A 1.813(6) . ?
P2 C13A 1.821(6) . ?
P2 C1 1.844(6) . ?
P1' C1B 1.801(6) . ?
P1' C7B 1.802(6) . ?
P1' C1' 1.807(5) . ?
P1' B'' 1.935(7) . ?
P2' C19B 1.807(5) . ?
P2' C13B 1.828(6) . ?
P2' C1' 1.853(5) . ?
B1 B2 1.751(13) . ?
B1 B6 1.757(12) . ?
B1 B3 1.761(11) . ?
B1 B5 1.774(10) . ?
B1 B4 1.776(11) . ?
B1 H1 1.03(7) . ?
B2 C7 1.686(10) . ?
B2 B3 1.737(11) . ?
B2 B6 1.740(11) . ?
B2 B11 1.815(12) . ?
B2 H2 1.20(7) . ?
B3 C8 1.665(9) . ?
B3 C7 1.692(9) . ?
B3 B4 1.759(10) . ?
B3 H3 1.01(6) . ?
B4 C8 1.640(10) . ?
B4 B5 1.835(10) . ?
B4 H4 1.24(6) . ?
B5 B6 1.767(11) . ?
B5 B10 1.799(10) . ?
B5 H5 1.22(6) . ?
B6 B10 1.795(10) . ?
B6 B11 1.821(12) . ?
B6 H6 1.13(7) . ?
B10 B11 1.849(11) . ?
B10 H10 1.03(6) . ?
B10 H13 1.34(6) . ?
B11 C7 1.668(10) . ?
B11 H11 1.18(5) . ?
B11 H13 1.33(6) . ?
B' H12B 1.10(5) . ?
B' H12C 1.01(6) . ?
B' H12D 1.25(7) . ?
B1' B6' 1.766(11) . ?
B1' B5' 1.772(10) . ?
B1' B3' 1.773(11) . ?
B1' B2' 1.780(13) . ?
B1' B4' 1.789(10) . ?
B1' H1' 1.10(6) . ?
B2' C7' 1.660(10) . ?
B2' B3' 1.746(12) . ?
B2' B6' 1.754(11) . ?
B2' B11' 1.780(11) . ?
B2' H2' 1.15(6) . ?
B3' C8' 1.674(10) . ?
B3' C7' 1.686(11) . ?
B3' B4' 1.796(11) . ?
B3' H3' 1.11(6) . ?
B4' C8' 1.645(10) . ?
B4' B5' 1.829(10) . ?
B4' H4' 1.11(6) . ?
B5' B10' 1.785(11) . ?
B5' B6' 1.803(11) . ?
B5' H5' 1.09(5) . ?
B6' B10' 1.783(10) . ?
B6' B11' 1.794(11) . ?
B6' H6' 1.10(6) . ?
B10' B11' 1.882(11) . ?
B10' H13' 1.27(7) . ?
B10' H10' 1.15(6) . ?
B11' C7' 1.677(11) . ?
B11' H13' 1.18(7) . ?
B11' H11' 1.10(7) . ?
B'' H12E 1.15(6) . ?
B'' H12F 1.29(5) . ?
B'' H12G 1.25(6) . ?
C1 H1A 0.9900 . ?
C1 H1B 0.9900 . ?
C7 C8 1.530(8) . ?
C7 H7 0.98(5) . ?
C8 H8 1.06(5) . ?
C1' H1'1 0.9900 . ?
C1' H1'2 0.9900 . ?
C7' C8' 1.518(9) . ?
C7' H7' 0.97(8) . ?
C8' H8' 1.11(9) . ?
C1A C2A 1.379(8) . ?
C1A C6A 1.397(8) . ?
C2A C3A 1.379(9) . ?
C2A H2A 0.9500 . ?
C3A C4A 1.373(10) . ?
C3A H3A 0.9500 . ?
C4A C5A 1.369(10) . ?
C4A H4A 0.9500 . ?
C5A C6A 1.379(9) . ?
C5A H5A 0.9500 . ?
C6A H6A 0.9500 . ?
C7A C12A 1.369(9) . ?
C7A C8A 1.380(8) . ?
C8A C9A 1.391(9) . ?
C8A H8A 0.9500 . ?
C9A C10A 1.352(11) . ?
C9A H9A 0.9500 . ?
C10A C11A 1.379(13) . ?
C10A H10A 0.9500 . ?
C11A C12A 1.390(12) . ?
C11A H11A 0.9500 . ?
C12A H12A 0.9500 . ?
C13A C14A 1.376(9) . ?
C13A C18A 1.384(8) . ?
C14A C15A 1.386(10) . ?
C14A H14A 0.9500 . ?
C15A C16A 1.368(11) . ?
C15A H15A 0.9500 . ?
C16A C17A 1.336(10) . ?
C16A H16A 0.9500 . ?
C17A C18A 1.381(9) . ?
C17A H17A 0.9500 . ?
C18A H18A 0.9500 . ?
C19A C20A 1.390(8) . ?
C19A C24A 1.397(8) . ?
C20A C21A 1.381(9) . ?
C20A H20A 0.9500 . ?
C21A C22A 1.373(10) . ?
C21A H21A 0.9500 . ?
C22A C23A 1.362(10) . ?
C22A H22A 0.9500 . ?
C23A C24A 1.391(9) . ?
C23A H23A 0.9500 . ?
C24A H24A 0.9500 . ?
C1B C2B 1.370(9) . ?
C1B C6B 1.401(9) . ?
C2B C3B 1.393(10) . ?
C2B H2B 0.9500 . ?
C3B C4B 1.360(11) . ?
C3B H3B 0.9500 . ?
C4B C5B 1.405(11) . ?
C4B H4B 0.9500 . ?
C5B C6B 1.385(9) . ?
C5B H5B 0.9500 . ?
C6B H6B 0.9500 . ?
C7B C8B 1.382(8) . ?
C7B C12B 1.389(8) . ?
C8B C9B 1.388(9) . ?
C8B H8B 0.9500 . ?
C9B C10B 1.360(10) . ?
C9B H9B 0.9500 . ?
C10B C11B 1.374(10) . ?
C10B H10B 0.9500 . ?
C11B C12B 1.388(9) . ?
C11B H11B 0.9500 . ?
C12B H12B 0.9500 . ?
C13B C14B 1.380(8) . ?
C13B C18B 1.397(8) . ?
C14B C15B 1.377(9) . ?
C14B H14B 0.9500 . ?
C15B C16B 1.388(10) . ?
C15B H15B 0.9500 . ?
C16B C17B 1.369(9) . ?
C16B H16B 0.9500 . ?
C17B C18B 1.380(9) . ?
C17B H17B 0.9500 . ?
C18B H18B 0.9500 . ?
C19B C24B 1.385(8) . ?
C19B C20B 1.401(8) . ?
C20B C21B 1.388(8) . ?
C20B H20B 0.9500 . ?
C21B C22B 1.355(9) . ?
C21B H21B 0.9500 . ?
C22B C23B 1.378(9) . ?
C22B H22B 0.9500 . ?
C23B C24B 1.378(8) . ?
C23B H23B 0.9500 . ?
C24B H24B 0.9500 . ?
