#------------------------------------------------------------------------------
#$Date: 2016-03-23 03:56:46 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179270 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/90/4319007.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4319007
loop_
_publ_author_name
'Vincent J. Catalano'
'Mark A. Malwitz'
'Bruce C. Noll'
_publ_contact_author_address
;
Department of Chemistry
University of Nevada
Reno, NV  89557
;
_publ_contact_author_email       vjc@unr.edu
_publ_contact_author_name        'Professor Vincent J. Catalano'
_publ_contact_author_phone       '775 784 1329'
_publ_section_title
;
 Pd(0) and Pt(0) Metallocryptands Encapsulating a Spinning Mercurous Dimer
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6553
_journal_page_last               6559
_journal_paper_doi               10.1021/ic020439n
_journal_volume                  41
_journal_year                    2002
_chemical_formula_sum            'C119 H90 Cl2 F12 Hg2 N6 P8 Pt2'
_chemical_formula_weight         2941.99
_chemical_name_common            1
_chemical_name_systematic
; 
? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.329(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.995(4)
_cell_length_b                   27.707(6)
_cell_length_c                   23.561(5)
_cell_measurement_reflns_used    9125
_cell_measurement_temperature    135(2)
_cell_measurement_theta_max      31.271
_cell_measurement_theta_min      2.403
_cell_volume                     10948(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      135(2)
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.068
_diffrn_reflns_av_sigmaI/netI    0.0627
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       36
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            99964
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.77
_exptl_absorpt_coefficient_mu    5.583
_exptl_absorpt_correction_T_max  0.47
_exptl_absorpt_correction_T_min  0.28
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Blessing, Acta Cryst. (1995) A51, 33-38'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.785
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             5696
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.34
_refine_diff_density_max         2.336
_refine_diff_density_min         -4.486
_refine_diff_density_rms         0.225
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1432
_refine_ls_number_reflns         24741
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0701
_refine_ls_R_factor_gt           0.0510
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0930P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1374
_refine_ls_wR_factor_ref         0.1466
_reflns_number_gt                19273
_reflns_number_total             24741
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic020439n_2.cif
_cod_data_source_block           bc407
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to the built-in table from CIF Core dictionary named
'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multiscan'
changed to 'multi-scan' according to the built-in table from CIF Core
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_database_code               4319007
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.797333(14) 0.324539(9) 0.776442(10) 0.01881(7) Uani 1 1 d . . .
Pt2 Pt 0.556023(15) 0.226668(9) 0.737784(10) 0.01936(7) Uani 1 1 d . . .
Hg2 Hg 0.643826(15) 0.300147(9) 0.798778(10) 0.02238(7) Uani 1 1 d . . .
Hg1 Hg 0.691833(15) 0.267964(9) 0.700048(10) 0.02274(7) Uani 1 1 d . . .
N1 N 0.7325(3) 0.3167(2) 0.6220(2) 0.0222(12) Uani 1 1 d . . .
N2 N 0.6508(3) 0.2328(2) 0.6070(2) 0.0236(12) Uani 1 1 d . . .
N3 N 0.6555(3) 0.3631(2) 0.8696(2) 0.0217(11) Uani 1 1 d . . .
N4 N 0.5128(3) 0.3395(2) 0.8040(2) 0.0237(12) Uani 1 1 d . . .
N5 N 0.8397(3) 0.2046(2) 0.8279(2) 0.0241(12) Uani 1 1 d . . .
N6 N 0.6977(3) 0.1757(2) 0.8560(2) 0.0243(12) Uani 1 1 d . . .
C1 C 0.7705(4) 0.3585(3) 0.6314(3) 0.0262(15) Uani 1 1 d . . .
C2 C 0.8051(5) 0.3810(3) 0.5881(3) 0.0317(16) Uani 1 1 d . . .
H2A H 0.8340 0.4103 0.5957 0.038 Uiso 1 1 calc R . .
C3 C 0.7968(5) 0.3599(3) 0.5336(3) 0.0355(17) Uani 1 1 d . . .
H3A H 0.8198 0.3748 0.5039 0.043 Uiso 1 1 calc R . .
C4 C 0.7546(5) 0.3170(3) 0.5231(3) 0.0311(16) Uani 1 1 d . . .
C5 C 0.7234(4) 0.2964(3) 0.5688(3) 0.0248(14) Uani 1 1 d . . .
C6 C 0.6788(4) 0.2524(2) 0.5614(3) 0.0240(14) Uani 1 1 d . . .
C7 C 0.6615(5) 0.2310(3) 0.5056(3) 0.0315(17) Uani 1 1 d . . .
C8 C 0.6137(5) 0.1895(3) 0.4994(3) 0.0304(16) Uani 1 1 d . . .
H8A H 0.6023 0.1736 0.4633 0.037 Uiso 1 1 calc R . .
C9 C 0.5836(4) 0.1721(3) 0.5459(3) 0.0273(15) Uani 1 1 d . . .
H9A H 0.5486 0.1452 0.5413 0.033 Uiso 1 1 calc R . .
C10 C 0.6039(4) 0.1939(3) 0.6008(3) 0.0237(14) Uani 1 1 d . . .
C11 C 0.7389(6) 0.2941(3) 0.4678(3) 0.043(2) Uani 1 1 d . . .
H11A H 0.7600 0.3077 0.4364 0.052 Uiso 1 1 calc R . .
C12 C 0.6947(5) 0.2534(3) 0.4597(3) 0.041(2) Uani 1 1 d . . .
H12A H 0.6852 0.2392 0.4226 0.049 Uiso 1 1 calc R . .
C13 C 0.7276(4) 0.3760(2) 0.8976(3) 0.0224(13) Uani 1 1 d . . .
C14 C 0.7340(4) 0.4110(3) 0.9405(3) 0.0307(16) Uani 1 1 d . . .
H14A H 0.7850 0.4194 0.9611 0.037 Uiso 1 1 calc R . .
C15 C 0.6671(4) 0.4334(3) 0.9530(3) 0.0336(17) Uani 1 1 d . . .
H15A H 0.6718 0.4573 0.9822 0.040 Uiso 1 1 calc R . .
C16 C 0.5914(4) 0.4212(3) 0.9228(3) 0.0277(15) Uani 1 1 d . . .
C17 C 0.5886(4) 0.3857(3) 0.8802(3) 0.0252(14) Uani 1 1 d . . .
C18 C 0.5126(4) 0.3732(2) 0.8458(3) 0.0226(13) Uani 1 1 d . . .
C19 C 0.4437(4) 0.3966(3) 0.8551(3) 0.0282(15) Uani 1 1 d . . .
C20 C 0.3729(4) 0.3825(3) 0.8205(3) 0.0331(17) Uani 1 1 d . . .
H20A H 0.3240 0.3968 0.8261 0.040 Uiso 1 1 calc R . .
C21 C 0.3728(4) 0.3482(3) 0.7784(3) 0.0282(15) Uani 1 1 d . . .
H21A H 0.3243 0.3384 0.7555 0.034 Uiso 1 1 calc R . .
C22 C 0.4461(4) 0.3279(2) 0.7699(3) 0.0237(14) Uani 1 1 d . . .
C23 C 0.5173(5) 0.4447(3) 0.9312(3) 0.0351(17) Uani 1 1 d . . .
H23A H 0.5187 0.4693 0.9595 0.042 Uiso 1 1 calc R . .
C24 C 0.4481(4) 0.4325(3) 0.9000(4) 0.0355(18) Uani 1 1 d . . .
H24A H 0.4005 0.4475 0.9073 0.043 Uiso 1 1 calc R . .
C25 C 0.9084(4) 0.2186(3) 0.8129(3) 0.0261(14) Uani 1 1 d . . .
C26 C 0.9817(5) 0.1947(3) 0.8321(3) 0.0357(18) Uani 1 1 d . . .
H26A H 1.0295 0.2051 0.8199 0.043 Uiso 1 1 calc R . .
C27 C 0.9819(5) 0.1557(3) 0.8688(3) 0.0359(18) Uani 1 1 d . . .
H27A H 1.0303 0.1395 0.8831 0.043 Uiso 1 1 calc R . .
C28 C 0.9094(4) 0.1404(3) 0.8850(3) 0.0292(15) Uani 1 1 d . . .
C29 C 0.8404(4) 0.1661(2) 0.8635(3) 0.0227(14) Uani 1 1 d . . .
C30 C 0.7638(4) 0.1502(3) 0.8789(3) 0.0278(15) Uani 1 1 d . . .
C31 C 0.7615(5) 0.1097(3) 0.9140(3) 0.0320(16) Uani 1 1 d . . .
C32 C 0.6876(5) 0.0938(3) 0.9232(4) 0.044(2) Uani 1 1 d . . .
H32A H 0.6837 0.0666 0.9472 0.053 Uiso 1 1 calc R . .
C33 C 0.6198(5) 0.1172(3) 0.8980(3) 0.0375(18) Uani 1 1 d . . .
H33A H 0.5685 0.1055 0.9021 0.045 Uiso 1 1 calc R . .
C34 C 0.6283(4) 0.1590(3) 0.8657(3) 0.0259(15) Uani 1 1 d . . .
C35 C 0.9055(5) 0.0992(3) 0.9220(3) 0.0345(17) Uani 1 1 d . . .
H35A H 0.9528 0.0820 0.9365 0.041 Uiso 1 1 calc R . .
C36 C 0.8362(5) 0.0850(3) 0.9358(3) 0.0404(19) Uani 1 1 d . . .
H36A H 0.8353 0.0581 0.9606 0.048 Uiso 1 1 calc R . .
C37 C 0.6855(4) 0.4206(3) 0.6964(3) 0.0272(15) Uani 1 1 d . . .
C38 C 0.6450(4) 0.4264(3) 0.7425(3) 0.0296(16) Uani 1 1 d . . .
H38A H 0.6606 0.4081 0.7765 0.036 Uiso 1 1 calc R . .
C39 C 0.5820(5) 0.4588(3) 0.7397(4) 0.0367(18) Uani 1 1 d . . .
H39A H 0.5549 0.4622 0.7717 0.044 Uiso 1 1 calc R . .
C40 C 0.5586(5) 0.4860(3) 0.6908(4) 0.044(2) Uani 1 1 d . . .
H40A H 0.5167 0.5088 0.6893 0.053 Uiso 1 1 calc R . .
C41 C 0.5972(5) 0.4795(3) 0.6436(4) 0.043(2) Uani 1 1 d . . .
H41A H 0.5798 0.4971 0.6093 0.052 Uiso 1 1 calc R . .
C42 C 0.6614(5) 0.4473(3) 0.6460(3) 0.0374(18) Uani 1 1 d . . .
H42A H 0.6883 0.4438 0.6139 0.045 Uiso 1 1 calc R . .
C43 C 0.8546(4) 0.4264(3) 0.7070(3) 0.0247(14) Uani 1 1 d . . .
C44 C 0.8433(5) 0.4760(3) 0.7092(3) 0.0309(16) Uani 1 1 d . . .
H44A H 0.7911 0.4885 0.7081 0.037 Uiso 1 1 calc R . .
C45 C 0.9084(5) 0.5077(3) 0.7128(4) 0.043(2) Uani 1 1 d . . .
H45A H 0.8999 0.5415 0.7144 0.051 Uiso 1 1 calc R . .
C46 C 0.9845(5) 0.4900(4) 0.7142(4) 0.051(2) Uani 1 1 d . . .
H46A H 1.0289 0.5113 0.7175 0.062 Uiso 1 1 calc R . .
C47 C 0.9950(5) 0.4398(4) 0.7104(4) 0.049(2) Uani 1 1 d . . .
H47A H 1.0466 0.4268 0.7099 0.059 Uiso 1 1 calc R . .
C48 C 0.9310(4) 0.4097(3) 0.7075(3) 0.0335(17) Uani 1 1 d . . .
H48A H 0.9395 0.3759 0.7058 0.040 Uiso 1 1 calc R . .
C49 C 0.4798(4) 0.1408(2) 0.6362(3) 0.0224(13) Uani 1 1 d . . .
C50 C 0.4675(4) 0.0919(3) 0.6452(3) 0.0299(16) Uani 1 1 d . . .
H50A H 0.5091 0.0730 0.6661 0.036 Uiso 1 1 calc R . .
C51 C 0.3934(5) 0.0703(3) 0.6236(3) 0.0353(18) Uani 1 1 d . . .
H51A H 0.3848 0.0369 0.6298 0.042 Uiso 1 1 calc R . .
C52 C 0.3331(5) 0.0986(3) 0.5930(3) 0.0379(19) Uani 1 1 d . . .
H52A H 0.2829 0.0846 0.5784 0.046 Uiso 1 1 calc R . .
C53 C 0.3461(4) 0.1469(3) 0.5839(3) 0.0364(18) Uani 1 1 d . . .
H53A H 0.3050 0.1658 0.5625 0.044 Uiso 1 1 calc R . .
C54 C 0.4180(4) 0.1681(3) 0.6056(3) 0.0291(15) Uani 1 1 d . . .
H54A H 0.4257 0.2015 0.5997 0.035 Uiso 1 1 calc R . .
C55 C 0.6461(4) 0.1225(2) 0.6823(3) 0.0230(14) Uani 1 1 d . . .
C56 C 0.6978(4) 0.1233(3) 0.7338(3) 0.0265(15) Uani 1 1 d . . .
H56A H 0.6925 0.1478 0.7611 0.032 Uiso 1 1 calc R . .
C57 C 0.7574(4) 0.0891(3) 0.7465(3) 0.0314(16) Uani 1 1 d . . .
H57A H 0.7927 0.0903 0.7821 0.038 Uiso 1 1 calc R . .
C58 C 0.7653(5) 0.0529(3) 0.7066(3) 0.0347(17) Uani 1 1 d . . .
H58A H 0.8059 0.0292 0.7151 0.042 Uiso 1 1 calc R . .
C59 C 0.7135(4) 0.0515(3) 0.6543(3) 0.0321(16) Uani 1 1 d . . .
H59A H 0.7186 0.0268 0.6271 0.039 Uiso 1 1 calc R . .
C60 C 0.6554(4) 0.0857(3) 0.6423(3) 0.0279(15) Uani 1 1 d . . .
H60A H 0.6206 0.0848 0.6064 0.033 Uiso 1 1 calc R . .
C61 C 0.8885(4) 0.3931(2) 0.8950(3) 0.0230(13) Uani 1 1 d . . .
C62 C 0.9322(4) 0.3944(3) 0.9508(3) 0.0293(16) Uani 1 1 d . . .
H62A H 0.9251 0.3698 0.9776 0.035 Uiso 1 1 calc R . .
C63 C 0.9859(5) 0.4315(3) 0.9671(3) 0.0346(18) Uani 1 1 d . . .
H63A H 1.0151 0.4324 1.0051 0.041 Uiso 1 1 calc R . .
C64 C 0.9971(5) 0.4677(3) 0.9278(3) 0.0348(17) Uani 1 1 d . . .
H64A H 1.0350 0.4926 0.9384 0.042 Uiso 1 1 calc R . .
C65 C 0.9521(5) 0.4667(3) 0.8733(3) 0.0340(17) Uani 1 1 d . . .
H65A H 0.9578 0.4919 0.8469 0.041 Uiso 1 1 calc R . .
C66 C 0.8989(4) 0.4295(3) 0.8567(3) 0.0298(16) Uani 1 1 d . . .
H66A H 0.8693 0.4290 0.8188 0.036 Uiso 1 1 calc R . .
C67 C 0.8374(4) 0.2991(2) 0.9254(3) 0.0250(14) Uani 1 1 d . . .
C68 C 0.9136(4) 0.2779(3) 0.9348(3) 0.0287(15) Uani 1 1 d . . .
H68A H 0.9540 0.2903 0.9154 0.034 Uiso 1 1 calc R . .
C69 C 0.9307(5) 0.2388(3) 0.9724(3) 0.0347(17) Uani 1 1 d . . .
H69A H 0.9829 0.2254 0.9792 0.042 Uiso 1 1 calc R . .
C70 C 0.8718(5) 0.2200(3) 0.9994(3) 0.0359(18) Uani 1 1 d . . .
H70A H 0.8831 0.1931 1.0245 0.043 Uiso 1 1 calc R . .
C71 C 0.7963(5) 0.2397(3) 0.9904(3) 0.0365(18) Uani 1 1 d . . .
H71A H 0.7560 0.2264 1.0092 0.044 Uiso 1 1 calc R . .
C72 C 0.7790(5) 0.2791(3) 0.9539(3) 0.0324(17) Uani 1 1 d . . .
H72A H 0.7270 0.2925 0.9482 0.039 Uiso 1 1 calc R . .
C73 C 0.3584(4) 0.2612(3) 0.6908(3) 0.0287(16) Uani 1 1 d . . .
C74 C 0.3364(4) 0.2216(3) 0.7208(4) 0.0340(17) Uani 1 1 d . . .
H74A H 0.3728 0.2089 0.7521 0.041 Uiso 1 1 calc R . .
C75 C 0.2612(5) 0.1999(3) 0.7056(4) 0.045(2) Uani 1 1 d . . .
H75A H 0.2473 0.1727 0.7263 0.054 Uiso 1 1 calc R . .
C76 C 0.2079(5) 0.2181(4) 0.6609(4) 0.054(3) Uani 1 1 d . . .
H76A H 0.1572 0.2033 0.6502 0.065 Uiso 1 1 calc R . .
C77 C 0.2284(5) 0.2582(4) 0.6314(4) 0.056(3) Uani 1 1 d . . .
H77A H 0.1909 0.2714 0.6011 0.068 Uiso 1 1 calc R . .
C78 C 0.3036(5) 0.2794(4) 0.6457(4) 0.046(2) Uani 1 1 d . . .
H78A H 0.3174 0.3064 0.6245 0.056 Uiso 1 1 calc R . .
C79 C 0.4688(4) 0.3294(2) 0.6557(3) 0.0251(14) Uani 1 1 d . . .
C80 C 0.4273(5) 0.3729(3) 0.6501(4) 0.043(2) Uani 1 1 d . . .
H80A H 0.3920 0.3802 0.6763 0.051 Uiso 1 1 calc R . .
C81 C 0.4361(6) 0.4057(3) 0.6074(4) 0.048(2) Uani 1 1 d . . .
H81A H 0.4070 0.4351 0.6046 0.057 Uiso 1 1 calc R . .
C82 C 0.4876(5) 0.3958(3) 0.5684(4) 0.0406(19) Uani 1 1 d . . .
H82A H 0.4941 0.4183 0.5391 0.049 Uiso 1 1 calc R . .
C83 C 0.5284(5) 0.3532(3) 0.5732(3) 0.0341(17) Uani 1 1 d . . .
H83A H 0.5638 0.3461 0.5470 0.041 Uiso 1 1 calc R . .
C84 C 0.5186(4) 0.3199(3) 0.6162(3) 0.0265(15) Uani 1 1 d . . .
H84A H 0.5468 0.2902 0.6183 0.032 Uiso 1 1 calc R . .
C85 C 0.9999(4) 0.2945(3) 0.7763(3) 0.0255(14) Uani 1 1 d . . .
C86 C 1.0651(5) 0.2744(3) 0.7541(4) 0.0385(19) Uani 1 1 d . . .
H86A H 1.0558 0.2483 0.7277 0.046 Uiso 1 1 calc R . .
C87 C 1.1399(5) 0.2911(4) 0.7694(5) 0.051(2) Uani 1 1 d . . .
H87A H 1.1822 0.2774 0.7529 0.061 Uiso 1 1 calc R . .
C88 C 1.1558(5) 0.3288(3) 0.8094(4) 0.044(2) Uani 1 1 d . . .
H88A H 1.2090 0.3394 0.8216 0.053 Uiso 1 1 calc R . .
C89 C 1.0929(4) 0.3507(3) 0.8314(4) 0.0358(18) Uani 1 1 d . . .
H89A H 1.1025 0.3771 0.8574 0.043 Uiso 1 1 calc R . .
C90 C 1.0151(4) 0.3329(3) 0.8144(3) 0.0292(15) Uani 1 1 d . . .
H90A H 0.9721 0.3474 0.8293 0.035 Uiso 1 1 calc R . .
C91 C 0.8877(4) 0.2411(3) 0.6934(3) 0.0295(15) Uani 1 1 d . . .
C92 C 0.8460(4) 0.1974(3) 0.6848(4) 0.0322(16) Uani 1 1 d . . .
H92A H 0.8277 0.1822 0.7163 0.039 Uiso 1 1 calc R . .
C93 C 0.8306(5) 0.1756(3) 0.6295(4) 0.0369(18) Uani 1 1 d . . .
H93A H 0.8020 0.1461 0.6241 0.044 Uiso 1 1 calc R . .
C94 C 0.8572(5) 0.1975(3) 0.5840(3) 0.0363(18) Uani 1 1 d . . .
H94A H 0.8466 0.1832 0.5468 0.044 Uiso 1 1 calc R . .
C95 C 0.9002(5) 0.2407(3) 0.5923(3) 0.041(2) Uani 1 1 d . . .
H95A H 0.9187 0.2557 0.5606 0.050 Uiso 1 1 calc R . .
C96 C 0.9161(5) 0.2619(3) 0.6468(3) 0.0353(18) Uani 1 1 d . . .
H96A H 0.9466 0.2907 0.6522 0.042 Uiso 1 1 calc R . .
C97 C 0.4602(4) 0.1510(3) 0.8267(3) 0.0288(15) Uani 1 1 d . . .
C98 C 0.4214(5) 0.1442(3) 0.8747(3) 0.0380(19) Uani 1 1 d . . .
H98A H 0.4385 0.1615 0.9093 0.046 Uiso 1 1 calc R . .
C99 C 0.3584(5) 0.1123(3) 0.8714(4) 0.041(2) Uani 1 1 d . . .
H99A H 0.3320 0.1082 0.9037 0.049 Uiso 1 1 calc R . .
C100 C 0.3334(5) 0.0864(3) 0.8225(4) 0.043(2) Uani 1 1 d . . .
H10A H 0.2894 0.0650 0.8207 0.052 Uiso 1 1 calc R . .
C101 C 0.3721(5) 0.0912(3) 0.7754(3) 0.0368(18) Uani 1 1 d . . .
H10B H 0.3562 0.0725 0.7418 0.044 Uiso 1 1 calc R . .
C102 C 0.4343(5) 0.1239(3) 0.7781(3) 0.0318(16) Uani 1 1 d . . .
H10C H 0.4599 0.1278 0.7455 0.038 Uiso 1 1 calc R . .
C103 C 0.5220(4) 0.2357(3) 0.8833(3) 0.0253(14) Uani 1 1 d . . .
C104 C 0.4461(5) 0.2569(3) 0.8801(3) 0.0366(18) Uani 1 1 d . . .
H10D H 0.4054 0.2488 0.8490 0.044 Uiso 1 1 calc R . .
C105 C 0.4294(6) 0.2895(3) 0.9215(4) 0.045(2) Uani 1 1 d . . .
H10E H 0.3775 0.3028 0.9192 0.055 Uiso 1 1 calc R . .
C106 C 0.4891(6) 0.3023(3) 0.9657(4) 0.048(2) Uani 1 1 d . . .
H10F H 0.4786 0.3251 0.9936 0.057 Uiso 1 1 calc R . .
C107 C 0.5643(6) 0.2820(4) 0.9698(4) 0.047(2) Uani 1 1 d . . .
H10G H 0.6052 0.2911 1.0003 0.056 Uiso 1 1 calc R . .
C108 C 0.5801(5) 0.2482(3) 0.9291(3) 0.0378(19) Uani 1 1 d . . .
H10H H 0.6313 0.2337 0.9329 0.045 Uiso 1 1 calc R . .
C8S C 0.4700(9) 0.0128(5) 0.9442(6) 0.079(4) Uani 1 1 d . . .
H8SA H 0.4492 0.0220 0.9059 0.095 Uiso 1 1 calc R . .
C9S C 0.4210(8) 0.0163(5) 0.9860(6) 0.079(4) Uani 1 1 d . . .
H9SA H 0.3676 0.0271 0.9757 0.095 Uiso 1 1 calc R . .
C7S C 0.5503(8) -0.0039(4) 0.9570(6) 0.071(3) Uani 1 1 d . . .
H7SA H 0.5829 -0.0065 0.9280 0.085 Uiso 1 1 calc R . .
C1S C 0.2811(6) 0.9458(4) 0.7704(5) 0.065(3) Uani 1 1 d . . .
H1SA H 0.3178 0.9217 0.7866 0.078 Uiso 1 1 calc R . .
C2S C 0.2233(6) 0.9601(4) 0.7995(4) 0.060(3) Uani 1 1 d . . .
H2SA H 0.2202 0.9466 0.8361 0.072 Uiso 1 1 calc R . .
C3S C 0.1695(7) 0.9938(5) 0.7764(5) 0.073(4) Uani 1 1 d . . .
H3SA H 0.1285 1.0038 0.7968 0.088 Uiso 1 1 calc R . .
C4S C 0.1747(8) 1.0134(5) 0.7235(6) 0.081(4) Uani 1 1 d . . .
H4SA H 0.1376 1.0372 0.7069 0.097 Uiso 1 1 calc R . .
C5S C 0.2359(7) 0.9974(5) 0.6946(5) 0.069(3) Uani 1 1 d . . .
H5SA H 0.2399 1.0100 0.6577 0.082 Uiso 1 1 calc R . .
C6S C 0.2883(6) 0.9649(4) 0.7185(5) 0.061(3) Uani 1 1 d . . .
H6SA H 0.3307 0.9550 0.6994 0.074 Uiso 1 1 calc R . .
C10S C 0.5471(17) 0.1202(9) 0.0614(15) 0.104(11) Uani 0.50 1 d P . .
H10I H 0.5116 0.1178 0.0907 0.125 Uiso 0.50 1 calc PR . .
H10J H 0.5275 0.0963 0.0312 0.125 Uiso 0.50 1 calc PR . .
C11S C 0.6168(17) 0.1053(10) 0.0859(14) 0.124(15) Uani 0.50 1 d P . .
H11B H 0.6136 0.0696 0.0848 0.149 Uiso 0.50 1 calc PR . .
H11C H 0.6204 0.1144 0.1269 0.149 Uiso 0.50 1 calc PR . .
C12S C 0.4911(8) 0.4058(7) 0.0929(6) 0.037(4) Uani 0.50 1 d P . .
H12B H 0.4541 0.3930 0.0619 0.044 Uiso 0.50 1 calc PR . .
C13S C 0.4646(10) 0.4252(6) 0.1427(8) 0.043(4) Uani 0.50 1 d P . .
H13A H 0.4287 0.4517 0.1397 0.052 Uiso 0.50 1 calc PR . .
Cl1 Cl 0.5316(3) 0.17368(16) 0.0316(2) 0.0483(11) Uani 0.50 1 d P . .
Cl2 Cl 0.7086(3) 0.11889(18) 0.0687(2) 0.0569(13) Uani 0.50 1 d P . .
Cl3 Cl 0.5892(3) 0.4062(2) 0.0905(2) 0.0600(14) Uani 0.50 1 d P . .
Cl4 Cl 0.4996(4) 0.3990(3) 0.2087(2) 0.080(2) Uani 0.50 1 d P . .
F1 F 0.0918(3) 0.0480(2) 0.8955(2) 0.0626(16) Uani 1 1 d . . .
F2 F 0.2150(3) 0.0367(2) 1.0128(2) 0.0586(15) Uani 1 1 d . . .
F3 F 0.2190(4) 0.0726(3) 0.9287(3) 0.0715(19) Uani 1 1 d . . .
F4 F 0.0893(4) 0.0112(2) 0.9808(3) 0.0688(17) Uani 1 1 d . . .
F5 F 0.1894(3) -0.0064(2) 0.9320(3) 0.0705(18) Uani 1 1 d . . .
F6 F 0.1189(4) 0.0904(2) 0.9778(3) 0.0596(15) Uani 1 1 d . . .
F7 F 0.2800(19) 0.4762(8) 0.9416(10) 0.140(13) Uani 0.50 1 d P . .
F7A F 0.3033(13) 0.4758(6) 0.9571(10) 0.099(10) Uani 0.50 1 d P . .
F8 F 0.2438(17) 0.3945(7) 1.0297(7) 0.130(9) Uani 0.50 1 d P . .
F8A F 0.1855(12) 0.4038(6) 0.9987(9) 0.093(6) Uani 0.50 1 d P . .
F9 F 0.2011(4) 0.4790(3) 1.0059(3) 0.081(2) Uani 1 1 d . . .
F10 F 0.3074(17) 0.3947(11) 0.9598(16) 0.090(10) Uani 0.50 1 d P . .
F10A F 0.2777(16) 0.4006(12) 0.9389(15) 0.084(10) Uani 0.50 1 d P . .
F11 F 0.3137(7) 0.4428(4) 1.0316(5) 0.163(5) Uani 1 1 d . . .
F12 F 0.1790(9) 0.4476(8) 0.9168(6) 0.084(5) Uani 0.50 1 d P . .
F12A F 0.1761(13) 0.4154(8) 0.9454(12) 0.131(10) Uani 0.50 1 d P . .
P1 P 0.77404(10) 0.38222(6) 0.70540(7) 0.0221(3) Uani 1 1 d . . .
P2 P 0.57260(10) 0.17132(6) 0.66748(7) 0.0204(3) Uani 1 1 d . . .
P3 P 0.81326(10) 0.34672(6) 0.87165(7) 0.0199(3) Uani 1 1 d . . .
P4 P 0.45950(10) 0.28519(6) 0.71171(7) 0.0217(3) Uani 1 1 d . . .
P5 P 0.89755(11) 0.27034(6) 0.76400(8) 0.0233(4) Uani 1 1 d . . .
P6 P 0.54275(11) 0.19372(7) 0.82690(7) 0.0237(4) Uani 1 1 d . . .
P7 P 0.15370(12) 0.04217(8) 0.95439(9) 0.0334(4) Uani 1 1 d . . .
P8 P 0.24722(16) 0.43751(10) 0.97812(11) 0.0510(6) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Hg Hg -2.3894 9.2266 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P3 Pt1 P1 120.20(6) . . ?
P3 Pt1 P5 108.84(6) . . ?
P1 Pt1 P5 113.58(6) . . ?
P3 Pt1 Hg1 137.52(4) . . ?
P1 Pt1 Hg1 84.53(5) . . ?
P5 Pt1 Hg1 87.89(5) . . ?
P3 Pt1 Hg2 81.29(4) . . ?
P1 Pt1 Hg2 104.26(5) . . ?
P5 Pt1 Hg2 125.90(5) . . ?
Hg1 Pt1 Hg2 58.152(13) . . ?
P3 Pt1 Pt2 107.05(4) . . ?
P1 Pt1 Pt2 102.12(4) . . ?
P5 Pt1 Pt2 103.20(5) . . ?
Hg1 Pt1 Pt2 30.537(8) . . ?
Hg2 Pt1 Pt2 29.321(9) . . ?
P2 Pt2 P4 115.98(6) . . ?
P2 Pt2 P6 115.26(6) . . ?
P4 Pt2 P6 110.17(6) . . ?
P2 Pt2 Hg2 137.67(5) . . ?
P4 Pt2 Hg2 85.54(5) . . ?
P6 Pt2 Hg2 86.76(5) . . ?
P2 Pt2 Hg1 80.98(4) . . ?
P4 Pt2 Hg1 102.18(5) . . ?
P6 Pt2 Hg1 129.80(5) . . ?
Hg2 Pt2 Hg1 58.178(13) . . ?
P2 Pt2 Pt1 107.86(4) . . ?
P4 Pt2 Pt1 101.42(5) . . ?
P6 Pt2 Pt1 104.50(4) . . ?
Hg2 Pt2 Pt1 29.824(7) . . ?
Hg1 Pt2 Pt1 30.060(10) . . ?
N3 Hg2 N4 67.82(18) . . ?
N3 Hg2 Hg1 145.63(14) . . ?
N4 Hg2 Hg1 125.08(13) . . ?
N3 Hg2 Pt2 150.23(13) . . ?
N4 Hg2 Pt2 86.41(13) . . ?
Hg1 Hg2 Pt2 62.052(13) . . ?
N3 Hg2 Pt1 88.90(13) . . ?
N4 Hg2 Pt1 139.56(13) . . ?
Hg1 Hg2 Pt1 60.534(10) . . ?
Pt2 Hg2 Pt1 120.855(13) . . ?
N2 Hg1 N1 67.44(19) . . ?
N2 Hg1 Hg2 145.82(14) . . ?
N1 Hg1 Hg2 127.82(13) . . ?
N2 Hg1 Pt1 151.06(14) . . ?
N1 Hg1 Pt1 86.86(13) . . ?
Hg2 Hg1 Pt1 61.313(15) . . ?
N2 Hg1 Pt2 89.52(14) . . ?
N1 Hg1 Pt2 142.39(13) . . ?
Hg2 Hg1 Pt2 59.770(11) . . ?
Pt1 Hg1 Pt2 119.403(16) . . ?
C1 N1 C5 119.6(6) . . ?
C1 N1 Hg1 122.7(4) . . ?
C5 N1 Hg1 117.2(4) . . ?
C10 N2 C6 121.2(6) . . ?
C10 N2 Hg1 120.5(4) . . ?
C6 N2 Hg1 118.2(4) . . ?
C13 N3 C17 120.8(6) . . ?
C13 N3 Hg2 120.1(4) . . ?
C17 N3 Hg2 119.1(4) . . ?
C22 N4 C18 120.4(6) . . ?
C22 N4 Hg2 123.2(4) . . ?
C18 N4 Hg2 116.3(4) . . ?
C25 N5 C29 118.2(6) . . ?
C34 N6 C30 116.9(6) . . ?
N1 C1 C2 121.0(7) . . ?
N1 C1 P1 114.0(5) . . ?
C2 C1 P1 125.0(6) . . ?
C3 C2 C1 119.4(7) . . ?
C4 C3 C2 119.7(7) . . ?
C3 C4 C5 117.4(7) . . ?
C3 C4 C11 123.7(7) . . ?
C5 C4 C11 118.8(7) . . ?
N1 C5 C4 122.8(7) . . ?
N1 C5 C6 116.3(6) . . ?
C4 C5 C6 120.8(6) . . ?
N2 C6 C7 121.1(6) . . ?
N2 C6 C5 119.5(6) . . ?
C7 C6 C5 119.4(6) . . ?
C8 C7 C6 117.6(6) . . ?
C8 C7 C12 124.6(7) . . ?
C6 C7 C12 117.8(7) . . ?
C9 C8 C7 119.4(7) . . ?
C8 C9 C10 120.9(7) . . ?
N2 C10 C9 119.7(6) . . ?
N2 C10 P2 115.5(5) . . ?
C9 C10 P2 124.8(6) . . ?
C12 C11 C4 121.0(7) . . ?
C11 C12 C7 122.1(7) . . ?
N3 C13 C14 120.0(6) . . ?
N3 C13 P3 115.1(5) . . ?
C14 C13 P3 124.8(5) . . ?
C15 C14 C13 120.1(7) . . ?
C14 C15 C16 120.4(7) . . ?
C17 C16 C15 117.0(6) . . ?
C17 C16 C23 118.7(6) . . ?
C15 C16 C23 124.3(7) . . ?
N3 C17 C16 121.6(6) . . ?
N3 C17 C18 118.9(6) . . ?
C16 C17 C18 119.5(6) . . ?
N4 C18 C19 122.6(6) . . ?
N4 C18 C17 117.6(6) . . ?
C19 C18 C17 119.8(6) . . ?
C18 C19 C20 116.4(7) . . ?
C18 C19 C24 119.6(6) . . ?
C20 C19 C24 123.9(7) . . ?
C21 C20 C19 121.1(7) . . ?
C20 C21 C22 118.8(6) . . ?
N4 C22 C21 120.5(6) . . ?
N4 C22 P4 114.2(5) . . ?
C21 C22 P4 125.3(5) . . ?
C24 C23 C16 121.2(7) . . ?
C23 C24 C19 121.2(7) . . ?
N5 C25 C26 122.9(7) . . ?
N5 C25 P5 113.0(5) . . ?
C26 C25 P5 124.0(6) . . ?
C27 C26 C25 118.4(7) . . ?
C26 C27 C28 119.3(7) . . ?
C29 C28 C27 117.9(7) . . ?
C29 C28 C35 120.3(7) . . ?
C27 C28 C35 121.8(7) . . ?
N5 C29 C28 123.2(7) . . ?
N5 C29 C30 117.9(6) . . ?
C28 C29 C30 118.9(6) . . ?
N6 C30 C31 123.4(7) . . ?
N6 C30 C29 116.9(6) . . ?
C31 C30 C29 119.7(6) . . ?
C32 C31 C30 117.6(7) . . ?
C32 C31 C36 123.8(7) . . ?
C30 C31 C36 118.5(7) . . ?
C33 C32 C31 120.1(7) . . ?
C32 C33 C34 118.2(7) . . ?
N6 C34 C33 123.7(7) . . ?
N6 C34 P6 112.5(5) . . ?
C33 C34 P6 123.6(6) . . ?
C36 C35 C28 120.6(7) . . ?
C35 C36 C31 122.0(7) . . ?
C38 C37 C42 119.1(7) . . ?
C38 C37 P1 118.8(5) . . ?
C42 C37 P1 121.8(6) . . ?
C37 C38 C39 121.0(7) . . ?
C40 C39 C38 120.5(8) . . ?
C39 C40 C41 119.1(8) . . ?
C40 C41 C42 121.0(8) . . ?
C41 C42 C37 119.2(8) . . ?
C48 C43 C44 117.9(7) . . ?
C48 C43 P1 118.4(6) . . ?
C44 C43 P1 123.7(6) . . ?
C43 C44 C45 120.6(8) . . ?
C46 C45 C44 120.4(8) . . ?
C45 C46 C47 118.5(8) . . ?
C48 C47 C46 120.0(8) . . ?
C47 C48 C43 122.6(8) . . ?
C50 C49 C54 119.1(6) . . ?
C50 C49 P2 121.8(5) . . ?
C54 C49 P2 118.9(5) . . ?
C49 C50 C51 120.4(7) . . ?
C52 C51 C50 119.0(7) . . ?
C53 C52 C51 120.2(7) . . ?
C54 C53 C52 120.7(7) . . ?
C53 C54 C49 120.6(7) . . ?
C56 C55 C60 118.4(6) . . ?
C56 C55 P2 118.2(5) . . ?
C60 C55 P2 123.4(5) . . ?
C55 C56 C57 121.2(7) . . ?
C56 C57 C58 119.6(7) . . ?
C59 C58 C57 119.9(7) . . ?
C60 C59 C58 119.7(7) . . ?
C59 C60 C55 121.2(7) . . ?
C66 C61 C62 119.2(6) . . ?
C66 C61 P3 118.2(5) . . ?
C62 C61 P3 122.6(5) . . ?
C63 C62 C61 120.3(7) . . ?
C62 C63 C64 120.2(7) . . ?
C65 C64 C63 119.0(7) . . ?
C66 C65 C64 120.9(7) . . ?
C65 C66 C61 120.3(7) . . ?
C72 C67 C68 117.8(7) . . ?
C72 C67 P3 121.4(6) . . ?
C68 C67 P3 120.5(6) . . ?
C69 C68 C67 121.0(7) . . ?
C70 C69 C68 119.6(8) . . ?
C69 C70 C71 120.5(7) . . ?
C70 C71 C72 120.3(8) . . ?
C71 C72 C67 120.8(7) . . ?
C74 C73 C78 118.3(7) . . ?
C74 C73 P4 117.9(6) . . ?
C78 C73 P4 123.7(7) . . ?
C73 C74 C75 121.1(8) . . ?
C76 C75 C74 120.0(9) . . ?
C75 C76 C77 119.5(8) . . ?
C76 C77 C78 120.7(9) . . ?
C73 C78 C77 120.3(9) . . ?
C84 C79 C80 117.3(7) . . ?
C84 C79 P4 119.6(5) . . ?
C80 C79 P4 123.2(6) . . ?
C81 C80 C79 121.7(8) . . ?
C80 C81 C82 120.3(8) . . ?
C83 C82 C81 118.7(8) . . ?
C82 C83 C84 120.7(7) . . ?
C79 C84 C83 121.3(7) . . ?
C90 C85 C86 117.8(7) . . ?
C90 C85 P5 116.9(5) . . ?
C86 C85 P5 125.1(6) . . ?
C87 C86 C85 121.8(8) . . ?
C86 C87 C88 120.5(8) . . ?
C89 C88 C87 119.7(8) . . ?
C88 C89 C90 118.8(8) . . ?
C85 C90 C89 121.4(7) . . ?
C96 C91 C92 118.5(7) . . ?
C96 C91 P5 122.6(6) . . ?
C92 C91 P5 118.8(6) . . ?
C91 C92 C93 120.8(7) . . ?
C94 C93 C92 119.7(7) . . ?
C93 C94 C95 120.0(7) . . ?
C96 C95 C94 120.4(7) . . ?
C91 C96 C95 120.6(8) . . ?
C102 C97 C98 117.6(7) . . ?
C102 C97 P6 119.6(6) . . ?
C98 C97 P6 122.8(6) . . ?
C99 C98 C97 119.9(7) . . ?
C100 C99 C98 121.1(8) . . ?
C99 C100 C101 120.1(8) . . ?
C100 C101 C102 119.0(8) . . ?
C97 C102 C101 122.1(7) . . ?
C108 C103 C104 118.0(7) . . ?
C108 C103 P6 121.6(6) . . ?
C104 C103 P6 120.4(6) . . ?
C105 C104 C103 121.5(8) . . ?
C106 C105 C104 119.1(9) . . ?
C105 C106 C107 120.5(8) . . ?
C106 C107 C108 120.2(8) . . ?
C103 C108 C107 120.6(8) . . ?
C9S C8S C7S 122.3(12) . . ?
C8S C9S C7S 120.5(12) . 3_657 ?
C9S C7S C8S 117.2(11) 3_657 . ?
C2S C1S C6S 121.6(11) . . ?
C1S C2S C3S 119.9(11) . . ?
C2S C3S C4S 119.8(11) . . ?
C3S C4S C5S 118.4(12) . . ?
C6S C5S C4S 120.5(11) . . ?
C5S C6S C1S 119.8(11) . . ?
C11S C10S Cl1 123(2) . . ?
C10S C11S Cl2 129(2) . . ?
C13S C12S Cl3 118.2(11) . . ?
C12S C13S Cl4 118.2(14) . . ?
F8A F8 P8 61.5(9) . . ?
F8 F8A F12A 129(2) . . ?
F8 F8A P8 77.1(14) . . ?
F12A F8A P8 61.5(11) . . ?
F10A F10 P8 66(5) . . ?
F10 F10A P8 90(5) . . ?
F12A F12 P8 57.2(11) . . ?
F12 F12A F8A 141(2) . . ?
F12 F12A P8 82.5(18) . . ?
F8A F12A P8 68.1(9) . . ?
C37 P1 C43 102.2(3) . . ?
C37 P1 C1 101.4(3) . . ?
C43 P1 C1 99.6(3) . . ?
C37 P1 Pt1 122.0(2) . . ?
C43 P1 Pt1 114.2(2) . . ?
C1 P1 Pt1 114.4(2) . . ?
C37 P1 P2 95.6(2) . . ?
C43 P1 P2 160.3(2) . . ?
C1 P1 P2 68.4(2) . . ?
Pt1 P1 P2 61.28(4) . . ?
C49 P2 C55 104.5(3) . . ?
C49 P2 C10 99.3(3) . . ?
C55 P2 C10 97.5(3) . . ?
C49 P2 Pt2 113.4(2) . . ?
C55 P2 Pt2 120.8(2) . . ?
C10 P2 Pt2 118.1(2) . . ?
C49 P2 P1 146.6(2) . . ?
C55 P2 P1 107.3(2) . . ?
C10 P2 P1 67.1(2) . . ?
Pt2 P2 P1 56.55(4) . . ?
C67 P3 C61 103.3(3) . . ?
C67 P3 C13 100.8(3) . . ?
C61 P3 C13 98.1(3) . . ?
C67 P3 Pt1 117.4(2) . . ?
C61 P3 Pt1 116.5(2) . . ?
C13 P3 Pt1 117.7(2) . . ?
C67 P3 P4 106.4(2) . . ?
C61 P3 P4 148.9(2) . . ?
C13 P3 P4 67.7(2) . . ?
Pt1 P3 P4 55.71(4) . . ?
C79 P4 C73 103.7(3) . . ?
C79 P4 C22 98.2(3) . . ?
C73 P4 C22 102.0(3) . . ?
C79 P4 Pt2 121.3(2) . . ?
C73 P4 Pt2 114.1(3) . . ?
C22 P4 Pt2 114.6(2) . . ?
C79 P4 P3 93.4(2) . . ?
C73 P4 P3 161.6(2) . . ?
C22 P4 P3 68.4(2) . . ?
Pt2 P4 P3 60.16(4) . . ?
C25 P5 C91 102.1(3) . . ?
C25 P5 C85 100.9(3) . . ?
C91 P5 C85 104.4(3) . . ?
C25 P5 Pt1 115.3(2) . . ?
C91 P5 Pt1 116.1(3) . . ?
C85 P5 Pt1 116.0(2) . . ?
C25 P5 P6 67.6(2) . . ?
C91 P5 P6 96.1(2) . . ?
C85 P5 P6 158.4(2) . . ?
Pt1 P5 P6 58.60(4) . . ?
C97 P6 C103 100.0(3) . . ?
C97 P6 C34 101.8(3) . . ?
C103 P6 C34 101.4(3) . . ?
C97 P6 Pt2 115.8(2) . . ?
C103 P6 Pt2 117.3(2) . . ?
C34 P6 Pt2 117.7(2) . . ?
C97 P6 P5 155.3(2) . . ?
C103 P6 P5 103.9(2) . . ?
C34 P6 P5 67.5(2) . . ?
Pt2 P6 P5 57.43(4) . . ?
F3 P7 F2 88.9(3) . . ?
F3 P7 F4 179.1(4) . . ?
F2 P7 F4 90.3(3) . . ?
F3 P7 F6 90.5(4) . . ?
F2 P7 F6 90.4(3) . . ?
F4 P7 F6 89.9(3) . . ?
F3 P7 F5 89.7(4) . . ?
F2 P7 F5 88.6(3) . . ?
F4 P7 F5 89.8(4) . . ?
F6 P7 F5 179.0(4) . . ?
F3 P7 F1 91.0(3) . . ?
F2 P7 F1 179.7(4) . . ?
F4 P7 F1 89.8(3) . . ?
F6 P7 F1 89.3(3) . . ?
F5 P7 F1 91.7(3) . . ?
F12A P8 F10A 74.4(14) . . ?
F12A P8 F7 110.0(17) . . ?
F10A P8 F7 86.5(18) . . ?
F12A P8 F8A 50.5(12) . . ?
F10A P8 F8A 95.7(15) . . ?
F7 P8 F8A 158.1(15) . . ?
F12A P8 F11 153.8(14) . . ?
F10A P8 F11 106.3(11) . . ?
F7 P8 F11 96.1(13) . . ?
F8A P8 F11 104.1(11) . . ?
F12A P8 F7A 127.9(16) . . ?
F10A P8 F7A 88.8(15) . . ?
F7 P8 F7A 18.3(17) . . ?
F8A P8 F7A 174.2(11) . . ?
F11 P8 F7A 78.0(11) . . ?
F12A P8 F9 95.7(9) . . ?
F10A P8 F9 166.6(12) . . ?
F7 P8 F9 88.5(10) . . ?
F8A P8 F9 84.4(7) . . ?
F11 P8 F9 86.6(5) . . ?
F7A P8 F9 90.4(6) . . ?
F12A P8 F10 93.2(13) . . ?
F10A P8 F10 23.6(18) . . ?
F7 P8 F10 93.3(16) . . ?
F8A P8 F10 97.3(14) . . ?
F11 P8 F10 83.2(12) . . ?
F7A P8 F10 88.3(14) . . ?
F9 P8 F10 169.7(12) . . ?
F12A P8 F8 87.8(14) . . ?
F10A P8 F8 91.0(16) . . ?
F7 P8 F8 160.5(15) . . ?
F8A P8 F8 41.4(10) . . ?
F11 P8 F8 66.0(9) . . ?
F7A P8 F8 142.4(14) . . ?
F9 P8 F8 97.8(8) . . ?
F10 P8 F8 77.4(15) . . ?
F12A P8 F12 40.3(11) . . ?
F10A P8 F12 81.3(12) . . ?
F7 P8 F12 70.9(13) . . ?
F8A P8 F12 87.8(11) . . ?
F11 P8 F12 164.9(9) . . ?
F7A P8 F12 89.2(11) . . ?
F9 P8 F12 85.3(7) . . ?
F10 P8 F12 104.8(13) . . ?
F8 P8 F12 127.8(11) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 P3 2.2990(17) . ?
Pt1 P1 2.3017(17) . ?
Pt1 P5 2.3246(18) . ?
Pt1 Hg1 2.8045(5) . ?
Pt1 Hg2 2.8258(6) . ?
Pt1 Pt2 4.8776(8) . ?
Pt2 P2 2.3078(17) . ?
Pt2 P4 2.3175(17) . ?
Pt2 P6 2.3338(18) . ?
Pt2 Hg2 2.7823(5) . ?
Pt2 Hg1 2.8447(6) . ?
Hg2 N3 2.401(5) . ?
Hg2 N4 2.500(5) . ?
Hg2 Hg1 2.7362(6) . ?
Hg1 N2 2.398(5) . ?
Hg1 N1 2.468(5) . ?
N1 C1 1.329(9) . ?
N1 C5 1.358(8) . ?
N2 C10 1.334(9) . ?
N2 C6 1.357(9) . ?
N3 C13 1.342(8) . ?
N3 C17 1.357(8) . ?
N4 C22 1.319(8) . ?
N4 C18 1.357(9) . ?
N5 C25 1.330(9) . ?
N5 C29 1.358(9) . ?
N6 C34 1.321(9) . ?
N6 C30 1.362(9) . ?
C1 C2 1.404(10) . ?
C1 P1 1.854(7) . ?
C2 C3 1.396(10) . ?
C3 C4 1.390(11) . ?
C4 C5 1.397(10) . ?
C4 C11 1.434(11) . ?
C5 C6 1.432(10) . ?
C6 C7 1.430(9) . ?
C7 C8 1.403(10) . ?
C7 C12 1.437(10) . ?
C8 C9 1.368(10) . ?
C9 C10 1.419(9) . ?
C10 P2 1.847(7) . ?
C11 C12 1.351(12) . ?
C13 C14 1.391(9) . ?
C13 P3 1.856(7) . ?
C14 C15 1.370(10) . ?
C15 C16 1.406(10) . ?
C16 C17 1.400(9) . ?
C16 C23 1.459(10) . ?
C17 C18 1.451(9) . ?
C18 C19 1.387(9) . ?
C19 C20 1.396(10) . ?
C19 C24 1.443(10) . ?
C20 C21 1.372(10) . ?
C21 C22 1.411(9) . ?
C22 P4 1.853(7) . ?
C23 C24 1.327(11) . ?
C25 C26 1.420(10) . ?
C25 P5 1.830(7) . ?
C26 C27 1.383(11) . ?
C27 C28 1.413(11) . ?
C28 C29 1.395(9) . ?
C28 C35 1.445(10) . ?
C29 C30 1.473(10) . ?
C30 C31 1.399(10) . ?
C31 C32 1.380(11) . ?
C31 C36 1.460(11) . ?
C32 C33 1.371(11) . ?
C33 C34 1.406(10) . ?
C34 P6 1.855(7) . ?
C35 C36 1.331(12) . ?
C37 C38 1.386(10) . ?
C37 C42 1.404(10) . ?
C37 P1 1.826(7) . ?
C38 C39 1.389(10) . ?
C39 C40 1.381(11) . ?
C40 C41 1.390(13) . ?
C41 C42 1.404(11) . ?
C43 C48 1.377(10) . ?
C43 C44 1.388(10) . ?
C43 P1 1.833(7) . ?
C44 C45 1.404(10) . ?
C45 C46 1.379(13) . ?
C46 C47 1.409(14) . ?
C47 C48 1.362(11) . ?
C49 C50 1.392(10) . ?
C49 C54 1.395(10) . ?
C49 P2 1.836(7) . ?
C50 C51 1.413(10) . ?
C51 C52 1.395(12) . ?
C52 C53 1.379(12) . ?
C53 C54 1.377(10) . ?
C55 C56 1.378(9) . ?
C55 C60 1.414(9) . ?
C55 P2 1.837(7) . ?
C56 C57 1.384(9) . ?
C57 C58 1.395(11) . ?
C58 C59 1.395(10) . ?
C59 C60 1.364(10) . ?
C61 C66 1.385(9) . ?
C61 C62 1.402(9) . ?
C61 P3 1.833(7) . ?
C62 C63 1.386(10) . ?
C63 C64 1.399(11) . ?
C64 C65 1.385(10) . ?
C65 C66 1.385(10) . ?
C67 C72 1.398(10) . ?
C67 C68 1.406(10) . ?
C67 P3 1.830(7) . ?
C68 C69 1.398(10) . ?
C69 C70 1.374(12) . ?
C70 C71 1.379(11) . ?
C71 C72 1.391(10) . ?
C73 C74 1.389(11) . ?
C73 C78 1.390(11) . ?
C73 P4 1.834(7) . ?
C74 C75 1.404(11) . ?
C75 C76 1.369(13) . ?
C76 C77 1.384(15) . ?
C77 C78 1.399(12) . ?
C79 C84 1.380(10) . ?
C79 C80 1.393(10) . ?
C79 P4 1.827(7) . ?
C80 C81 1.381(12) . ?
C81 C82 1.394(12) . ?
C82 C83 1.364(11) . ?
C83 C84 1.401(10) . ?
C85 C90 1.388(10) . ?
C85 C86 1.414(10) . ?
C85 P5 1.842(7) . ?
C86 C87 1.347(11) . ?
C87 C88 1.403(13) . ?
C88 C89 1.400(11) . ?
C89 C90 1.407(10) . ?
C91 C96 1.392(10) . ?
C91 C92 1.400(10) . ?
C91 P5 1.835(7) . ?
C92 C93 1.421(11) . ?
C93 C94 1.370(11) . ?
C94 C95 1.400(12) . ?
C95 C96 1.400(11) . ?
C97 C102 1.381(10) . ?
C97 C98 1.412(10) . ?
C97 P6 1.834(8) . ?
C98 C99 1.381(10) . ?
C99 C100 1.366(12) . ?
C100 C101 1.384(11) . ?
C101 C102 1.386(10) . ?
C103 C108 1.382(10) . ?
C103 C104 1.408(11) . ?
C103 P6 1.844(7) . ?
C104 C105 1.391(12) . ?
C105 C106 1.377(13) . ?
C106 C107 1.385(13) . ?
C107 C108 1.397(12) . ?
C8S C9S 1.392(17) . ?
C8S C7S 1.427(17) . ?
C9S C7S 1.393(18) 3_657 ?
C7S C9S 1.393(18) 3_657 ?
C1S C2S 1.346(15) . ?
C1S C6S 1.354(15) . ?
C2S C3S 1.357(16) . ?
C3S C4S 1.376(17) . ?
C4S C5S 1.404(17) . ?
C5S C6S 1.327(16) . ?
C10S C11S 1.30(3) . ?
C10S Cl1 1.64(2) . ?
C11S Cl2 1.72(3) . ?
C12S C13S 1.43(2) . ?
C12S Cl3 1.678(15) . ?
C13S Cl4 1.733(19) . ?
F1 P7 1.607(5) . ?
F2 P7 1.593(6) . ?
F3 P7 1.589(6) . ?
F4 P7 1.594(6) . ?
F5 P7 1.599(6) . ?
F6 P7 1.597(6) . ?
F7 P8 1.534(19) . ?
F7A P8 1.560(13) . ?
F8 F8A 1.16(2) . ?
F8 P8 1.709(17) . ?
F8A F12A 1.28(3) . ?
F8A P8 1.540(11) . ?
F9 P8 1.592(7) . ?
F10 F10A 0.67(5) . ?
F10 P8 1.67(3) . ?
F10A P8 1.53(3) . ?
F11 P8 1.557(9) . ?
F12 F12A 1.12(3) . ?
F12 P8 1.721(15) . ?
F12A P8 1.458(16) . ?
P1 P2 6.758(3) . ?
P3 P4 6.776(3) . ?
P5 P6 6.779(3) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P3 Pt1 Pt2 P2 -148.90(6) . . . . ?
P1 Pt1 Pt2 P2 83.93(7) . . . . ?
P5 Pt1 Pt2 P2 -34.14(6) . . . . ?
Hg1 Pt1 Pt2 P2 27.70(5) . . . . ?
Hg2 Pt1 Pt2 P2 -178.47(5) . . . . ?
P3 Pt1 Pt2 P4 88.77(6) . . . . ?
P1 Pt1 Pt2 P4 -38.39(6) . . . . ?
P5 Pt1 Pt2 P4 -156.47(7) . . . . ?
Hg1 Pt1 Pt2 P4 -94.62(5) . . . . ?
Hg2 Pt1 Pt2 P4 59.21(5) . . . . ?
P3 Pt1 Pt2 P6 -25.79(7) . . . . ?
P1 Pt1 Pt2 P6 -152.95(7) . . . . ?
P5 Pt1 Pt2 P6 88.98(7) . . . . ?
Hg1 Pt1 Pt2 P6 150.82(5) . . . . ?
Hg2 Pt1 Pt2 P6 -55.35(5) . . . . ?
P3 Pt1 Pt2 Hg2 29.57(5) . . . . ?
P1 Pt1 Pt2 Hg2 -97.60(5) . . . . ?
P5 Pt1 Pt2 Hg2 144.33(5) . . . . ?
Hg1 Pt1 Pt2 Hg2 -153.83(2) . . . . ?
P3 Pt1 Pt2 Hg1 -176.61(5) . . . . ?
P1 Pt1 Pt2 Hg1 56.23(5) . . . . ?
P5 Pt1 Pt2 Hg1 -61.84(5) . . . . ?
Hg2 Pt1 Pt2 Hg1 153.83(2) . . . . ?
P2 Pt2 Hg2 N3 179.8(3) . . . . ?
P4 Pt2 Hg2 N3 55.3(3) . . . . ?
P6 Pt2 Hg2 N3 -55.2(3) . . . . ?
Hg1 Pt2 Hg2 N3 162.6(3) . . . . ?
Pt1 Pt2 Hg2 N3 177.7(3) . . . . ?
P2 Pt2 Hg2 N4 150.47(15) . . . . ?
P4 Pt2 Hg2 N4 25.93(14) . . . . ?
P6 Pt2 Hg2 N4 -84.60(14) . . . . ?
Hg1 Pt2 Hg2 N4 133.24(13) . . . . ?
Pt1 Pt2 Hg2 N4 148.31(13) . . . . ?
P2 Pt2 Hg2 Hg1 17.23(6) . . . . ?
P4 Pt2 Hg2 Hg1 -107.31(5) . . . . ?
P6 Pt2 Hg2 Hg1 142.16(5) . . . . ?
Pt1 Pt2 Hg2 Hg1 15.072(12) . . . . ?
P2 Pt2 Hg2 Pt1 2.16(7) . . . . ?
P4 Pt2 Hg2 Pt1 -122.38(5) . . . . ?
P6 Pt2 Hg2 Pt1 127.09(5) . . . . ?
Hg1 Pt2 Hg2 Pt1 -15.072(12) . . . . ?
P3 Pt1 Hg2 N3 29.65(14) . . . . ?
P1 Pt1 Hg2 N3 -89.43(14) . . . . ?
P5 Pt1 Hg2 N3 136.65(14) . . . . ?
Hg1 Pt1 Hg2 N3 -163.55(13) . . . . ?
Pt2 Pt1 Hg2 N3 -178.85(13) . . . . ?
P3 Pt1 Hg2 N4 82.4(2) . . . . ?
P1 Pt1 Hg2 N4 -36.7(2) . . . . ?
P5 Pt1 Hg2 N4 -170.6(2) . . . . ?
Hg1 Pt1 Hg2 N4 -110.8(2) . . . . ?
Pt2 Pt1 Hg2 N4 -126.1(2) . . . . ?
P3 Pt1 Hg2 Hg1 -166.79(4) . . . . ?
P1 Pt1 Hg2 Hg1 74.12(5) . . . . ?
P5 Pt1 Hg2 Hg1 -59.79(6) . . . . ?
Pt2 Pt1 Hg2 Hg1 -15.298(12) . . . . ?
P3 Pt1 Hg2 Pt2 -151.49(4) . . . . ?
P1 Pt1 Hg2 Pt2 89.42(5) . . . . ?
P5 Pt1 Hg2 Pt2 -44.50(6) . . . . ?
Hg1 Pt1 Hg2 Pt2 15.298(12) . . . . ?
N3 Hg2 Hg1 N2 -135.8(3) . . . . ?
N4 Hg2 Hg1 N2 -33.7(3) . . . . ?
Pt2 Hg2 Hg1 N2 28.9(2) . . . . ?
Pt1 Hg2 Hg1 N2 -165.9(2) . . . . ?
N3 Hg2 Hg1 N1 -29.7(3) . . . . ?
N4 Hg2 Hg1 N1 72.4(2) . . . . ?
Pt2 Hg2 Hg1 N1 135.10(16) . . . . ?
Pt1 Hg2 Hg1 N1 -59.75(16) . . . . ?
N3 Hg2 Hg1 Pt1 30.1(2) . . . . ?
N4 Hg2 Hg1 Pt1 132.18(16) . . . . ?
Pt2 Hg2 Hg1 Pt1 -165.144(12) . . . . ?
N3 Hg2 Hg1 Pt2 -164.8(2) . . . . ?
N4 Hg2 Hg1 Pt2 -62.67(16) . . . . ?
Pt1 Hg2 Hg1 Pt2 165.144(12) . . . . ?
P3 Pt1 Hg1 N2 -176.9(3) . . . . ?
P1 Pt1 Hg1 N2 53.1(3) . . . . ?
P5 Pt1 Hg1 N2 -60.9(3) . . . . ?
Hg2 Pt1 Hg1 N2 163.6(3) . . . . ?
Pt2 Pt1 Hg1 N2 178.3(3) . . . . ?
P3 Pt1 Hg1 N1 156.42(15) . . . . ?
P1 Pt1 Hg1 N1 26.35(14) . . . . ?
P5 Pt1 Hg1 N1 -87.58(14) . . . . ?
Hg2 Pt1 Hg1 N1 136.89(13) . . . . ?
Pt2 Pt1 Hg1 N1 151.62(13) . . . . ?
P3 Pt1 Hg1 Hg2 19.54(6) . . . . ?
P1 Pt1 Hg1 Hg2 -110.53(5) . . . . ?
P5 Pt1 Hg1 Hg2 135.53(5) . . . . ?
Pt2 Pt1 Hg1 Hg2 14.731(12) . . . . ?
P3 Pt1 Hg1 Pt2 4.81(7) . . . . ?
P1 Pt1 Hg1 Pt2 -125.27(5) . . . . ?
P5 Pt1 Hg1 Pt2 120.80(5) . . . . ?
Hg2 Pt1 Hg1 Pt2 -14.731(12) . . . . ?
P2 Pt2 Hg1 N2 27.43(14) . . . . ?
P4 Pt2 Hg1 N2 -87.38(14) . . . . ?
P6 Pt2 Hg1 N2 142.90(15) . . . . ?
Hg2 Pt2 Hg1 N2 -164.22(13) . . . . ?
Pt1 Pt2 Hg1 N2 -179.19(14) . . . . ?
P2 Pt2 Hg1 N1 77.7(2) . . . . ?
P4 Pt2 Hg1 N1 -37.1(2) . . . . ?
P6 Pt2 Hg1 N1 -166.9(2) . . . . ?
Hg2 Pt2 Hg1 N1 -114.0(2) . . . . ?
Pt1 Pt2 Hg1 N1 -128.9(2) . . . . ?
P2 Pt2 Hg1 Hg2 -168.34(4) . . . . ?
P4 Pt2 Hg1 Hg2 76.85(5) . . . . ?
P6 Pt2 Hg1 Hg2 -52.87(6) . . . . ?
Pt1 Pt2 Hg1 Hg2 -14.962(12) . . . . ?
P2 Pt2 Hg1 Pt1 -153.38(4) . . . . ?
P4 Pt2 Hg1 Pt1 91.81(5) . . . . ?
P6 Pt2 Hg1 Pt1 -37.91(6) . . . . ?
Hg2 Pt2 Hg1 Pt1 14.962(12) . . . . ?
N2 Hg1 N1 C1 177.8(6) . . . . ?
Hg2 Hg1 N1 C1 33.6(6) . . . . ?
Pt1 Hg1 N1 C1 -15.8(5) . . . . ?
Pt2 Hg1 N1 C1 121.5(5) . . . . ?
N2 Hg1 N1 C5 -10.0(5) . . . . ?
Hg2 Hg1 N1 C5 -154.3(4) . . . . ?
Pt1 Hg1 N1 C5 156.3(5) . . . . ?
Pt2 Hg1 N1 C5 -66.4(6) . . . . ?
N1 Hg1 N2 C10 -173.4(6) . . . . ?
Hg2 Hg1 N2 C10 -48.7(6) . . . . ?
Pt1 Hg1 N2 C10 157.5(4) . . . . ?
Pt2 Hg1 N2 C10 -24.0(5) . . . . ?
N1 Hg1 N2 C6 8.9(5) . . . . ?
Hg2 Hg1 N2 C6 133.7(4) . . . . ?
Pt1 Hg1 N2 C6 -20.1(7) . . . . ?
Pt2 Hg1 N2 C6 158.4(5) . . . . ?
N4 Hg2 N3 C13 -174.8(5) . . . . ?
Hg1 Hg2 N3 C13 -54.6(6) . . . . ?
Pt2 Hg2 N3 C13 153.3(4) . . . . ?
Pt1 Hg2 N3 C13 -28.7(5) . . . . ?
N4 Hg2 N3 C17 4.4(5) . . . . ?
Hg1 Hg2 N3 C17 124.6(4) . . . . ?
Pt2 Hg2 N3 C17 -27.5(7) . . . . ?
Pt1 Hg2 N3 C17 150.5(5) . . . . ?
N3 Hg2 N4 C22 177.6(6) . . . . ?
Hg1 Hg2 N4 C22 34.2(6) . . . . ?
Pt2 Hg2 N4 C22 -17.7(5) . . . . ?
Pt1 Hg2 N4 C22 118.3(5) . . . . ?
N3 Hg2 N4 C18 -4.6(4) . . . . ?
Hg1 Hg2 N4 C18 -148.0(4) . . . . ?
Pt2 Hg2 N4 C18 160.2(5) . . . . ?
Pt1 Hg2 N4 C18 -63.9(5) . . . . ?
C5 N1 C1 C2 -3.4(10) . . . . ?
Hg1 N1 C1 C2 168.6(5) . . . . ?
C5 N1 C1 P1 177.6(5) . . . . ?
Hg1 N1 C1 P1 -10.4(7) . . . . ?
N1 C1 C2 C3 2.5(11) . . . . ?
P1 C1 C2 C3 -178.6(6) . . . . ?
C1 C2 C3 C4 -0.1(12) . . . . ?
C2 C3 C4 C5 -1.2(12) . . . . ?
C2 C3 C4 C11 176.3(8) . . . . ?
C1 N1 C5 C4 2.0(10) . . . . ?
Hg1 N1 C5 C4 -170.3(6) . . . . ?
C1 N1 C5 C6 -177.4(6) . . . . ?
Hg1 N1 C5 C6 10.2(8) . . . . ?
C3 C4 C5 N1 0.3(11) . . . . ?
C11 C4 C5 N1 -177.3(7) . . . . ?
C3 C4 C5 C6 179.7(7) . . . . ?
C11 C4 C5 C6 2.1(11) . . . . ?
C10 N2 C6 C7 -2.4(10) . . . . ?
Hg1 N2 C6 C7 175.3(5) . . . . ?
C10 N2 C6 C5 174.8(6) . . . . ?
Hg1 N2 C6 C5 -7.6(8) . . . . ?
N1 C5 C6 N2 -2.0(10) . . . . ?
C4 C5 C6 N2 178.6(7) . . . . ?
N1 C5 C6 C7 175.2(6) . . . . ?
C4 C5 C6 C7 -4.2(11) . . . . ?
N2 C6 C7 C8 0.9(11) . . . . ?
C5 C6 C7 C8 -176.3(7) . . . . ?
N2 C6 C7 C12 -178.8(7) . . . . ?
C5 C6 C7 C12 4.0(11) . . . . ?
C6 C7 C8 C9 2.1(11) . . . . ?
C12 C7 C8 C9 -178.2(8) . . . . ?
C7 C8 C9 C10 -3.7(11) . . . . ?
C6 N2 C10 C9 0.8(10) . . . . ?
Hg1 N2 C10 C9 -176.8(5) . . . . ?
C6 N2 C10 P2 179.0(5) . . . . ?
Hg1 N2 C10 P2 1.4(7) . . . . ?
C8 C9 C10 N2 2.4(11) . . . . ?
C8 C9 C10 P2 -175.7(6) . . . . ?
C3 C4 C11 C12 -177.3(9) . . . . ?
C5 C4 C11 C12 0.2(13) . . . . ?
C4 C11 C12 C7 -0.2(15) . . . . ?
C8 C7 C12 C11 178.4(9) . . . . ?
C6 C7 C12 C11 -1.9(13) . . . . ?
C17 N3 C13 C14 3.6(10) . . . . ?
Hg2 N3 C13 C14 -177.2(5) . . . . ?
C17 N3 C13 P3 -172.9(5) . . . . ?
Hg2 N3 C13 P3 6.4(7) . . . . ?
N3 C13 C14 C15 -1.8(11) . . . . ?
P3 C13 C14 C15 174.3(6) . . . . ?
C13 C14 C15 C16 0.1(12) . . . . ?
C14 C15 C16 C17 -0.1(11) . . . . ?
C14 C15 C16 C23 -176.8(8) . . . . ?
C13 N3 C17 C16 -3.6(10) . . . . ?
Hg2 N3 C17 C16 177.1(5) . . . . ?
C13 N3 C17 C18 175.2(6) . . . . ?
Hg2 N3 C17 C18 -4.0(8) . . . . ?
C15 C16 C17 N3 1.8(11) . . . . ?
C23 C16 C17 N3 178.8(7) . . . . ?
C15 C16 C17 C18 -177.1(7) . . . . ?
C23 C16 C17 C18 -0.1(11) . . . . ?
C22 N4 C18 C19 0.5(10) . . . . ?
Hg2 N4 C18 C19 -177.4(5) . . . . ?
C22 N4 C18 C17 -177.6(6) . . . . ?
Hg2 N4 C18 C17 4.5(8) . . . . ?
N3 C17 C18 N4 -0.5(10) . . . . ?
C16 C17 C18 N4 178.4(6) . . . . ?
N3 C17 C18 C19 -178.7(6) . . . . ?
C16 C17 C18 C19 0.2(10) . . . . ?
N4 C18 C19 C20 2.2(11) . . . . ?
C17 C18 C19 C20 -179.7(7) . . . . ?
N4 C18 C19 C24 -179.4(7) . . . . ?
C17 C18 C19 C24 -1.3(11) . . . . ?
C18 C19 C20 C21 -1.8(11) . . . . ?
C24 C19 C20 C21 179.9(8) . . . . ?
C19 C20 C21 C22 -1.1(12) . . . . ?
C18 N4 C22 C21 -3.6(10) . . . . ?
Hg2 N4 C22 C21 174.1(5) . . . . ?
C18 N4 C22 P4 175.0(5) . . . . ?
Hg2 N4 C22 P4 -7.2(7) . . . . ?
C20 C21 C22 N4 3.9(11) . . . . ?
C20 C21 C22 P4 -174.5(6) . . . . ?
C17 C16 C23 C24 1.2(12) . . . . ?
C15 C16 C23 C24 177.9(8) . . . . ?
C16 C23 C24 C19 -2.3(13) . . . . ?
C18 C19 C24 C23 2.4(12) . . . . ?
C20 C19 C24 C23 -179.3(8) . . . . ?
C29 N5 C25 C26 0.8(11) . . . . ?
C29 N5 C25 P5 179.2(5) . . . . ?
N5 C25 C26 C27 -1.5(12) . . . . ?
P5 C25 C26 C27 -179.6(6) . . . . ?
C25 C26 C27 C28 1.5(12) . . . . ?
C26 C27 C28 C29 -1.0(11) . . . . ?
C26 C27 C28 C35 178.2(8) . . . . ?
C25 N5 C29 C28 -0.3(10) . . . . ?
C25 N5 C29 C30 -178.7(6) . . . . ?
C27 C28 C29 N5 0.4(10) . . . . ?
C35 C28 C29 N5 -178.8(6) . . . . ?
C27 C28 C29 C30 178.8(7) . . . . ?
C35 C28 C29 C30 -0.4(10) . . . . ?
C34 N6 C30 C31 -3.5(10) . . . . ?
C34 N6 C30 C29 174.4(6) . . . . ?
N5 C29 C30 N6 -0.1(9) . . . . ?
C28 C29 C30 N6 -178.7(6) . . . . ?
N5 C29 C30 C31 177.8(6) . . . . ?
C28 C29 C30 C31 -0.7(10) . . . . ?
N6 C30 C31 C32 3.1(12) . . . . ?
C29 C30 C31 C32 -174.7(7) . . . . ?
N6 C30 C31 C36 179.7(7) . . . . ?
C29 C30 C31 C36 1.8(11) . . . . ?
C30 C31 C32 C33 0.8(13) . . . . ?
C36 C31 C32 C33 -175.6(8) . . . . ?
C31 C32 C33 C34 -3.9(13) . . . . ?
C30 N6 C34 C33 0.1(10) . . . . ?
C30 N6 C34 P6 -174.8(5) . . . . ?
C32 C33 C34 N6 3.6(12) . . . . ?
C32 C33 C34 P6 177.9(7) . . . . ?
C29 C28 C35 C36 0.2(12) . . . . ?
C27 C28 C35 C36 -178.9(8) . . . . ?
C28 C35 C36 C31 1.0(13) . . . . ?
C32 C31 C36 C35 174.3(9) . . . . ?
C30 C31 C36 C35 -2.0(12) . . . . ?
C42 C37 C38 C39 -0.9(11) . . . . ?
P1 C37 C38 C39 173.8(6) . . . . ?
C37 C38 C39 C40 -0.3(12) . . . . ?
C38 C39 C40 C41 2.1(13) . . . . ?
C39 C40 C41 C42 -2.7(13) . . . . ?
C40 C41 C42 C37 1.6(13) . . . . ?
C38 C37 C42 C41 0.2(11) . . . . ?
P1 C37 C42 C41 -174.3(6) . . . . ?
C48 C43 C44 C45 -1.2(11) . . . . ?
P1 C43 C44 C45 177.2(6) . . . . ?
C43 C44 C45 C46 0.2(12) . . . . ?
C44 C45 C46 C47 1.4(14) . . . . ?
C45 C46 C47 C48 -2.2(14) . . . . ?
C46 C47 C48 C43 1.3(14) . . . . ?
C44 C43 C48 C47 0.4(12) . . . . ?
P1 C43 C48 C47 -178.0(7) . . . . ?
C54 C49 C50 C51 0.1(10) . . . . ?
P2 C49 C50 C51 175.9(5) . . . . ?
C49 C50 C51 C52 0.1(11) . . . . ?
C50 C51 C52 C53 0.4(12) . . . . ?
C51 C52 C53 C54 -1.1(12) . . . . ?
C52 C53 C54 C49 1.4(12) . . . . ?
C50 C49 C54 C53 -0.9(11) . . . . ?
P2 C49 C54 C53 -176.8(6) . . . . ?
C60 C55 C56 C57 -0.2(10) . . . . ?
P2 C55 C56 C57 -176.5(6) . . . . ?
C55 C56 C57 C58 -0.3(11) . . . . ?
C56 C57 C58 C59 0.2(11) . . . . ?
C57 C58 C59 C60 0.2(12) . . . . ?
C58 C59 C60 C55 -0.7(11) . . . . ?
C56 C55 C60 C59 0.7(11) . . . . ?
P2 C55 C60 C59 176.8(6) . . . . ?
C66 C61 C62 C63 -0.8(11) . . . . ?
P3 C61 C62 C63 -177.1(6) . . . . ?
C61 C62 C63 C64 -0.4(12) . . . . ?
C62 C63 C64 C65 2.1(12) . . . . ?
C63 C64 C65 C66 -2.6(13) . . . . ?
C64 C65 C66 C61 1.4(12) . . . . ?
C62 C61 C66 C65 0.3(11) . . . . ?
P3 C61 C66 C65 176.7(6) . . . . ?
C72 C67 C68 C69 -1.4(11) . . . . ?
P3 C67 C68 C69 -174.8(5) . . . . ?
C67 C68 C69 C70 1.8(11) . . . . ?
C68 C69 C70 C71 -1.0(12) . . . . ?
C69 C70 C71 C72 -0.1(13) . . . . ?
C70 C71 C72 C67 0.4(12) . . . . ?
C68 C67 C72 C71 0.3(11) . . . . ?
P3 C67 C72 C71 173.6(6) . . . . ?
C78 C73 C74 C75 0.9(12) . . . . ?
P4 C73 C74 C75 -177.2(7) . . . . ?
C73 C74 C75 C76 -0.6(14) . . . . ?
C74 C75 C76 C77 -0.8(15) . . . . ?
C75 C76 C77 C78 1.9(16) . . . . ?
C74 C73 C78 C77 0.1(13) . . . . ?
P4 C73 C78 C77 178.2(7) . . . . ?
C76 C77 C78 C73 -1.5(15) . . . . ?
C84 C79 C80 C81 -0.9(13) . . . . ?
P4 C79 C80 C81 179.6(7) . . . . ?
C79 C80 C81 C82 0.0(15) . . . . ?
C80 C81 C82 C83 0.3(14) . . . . ?
C81 C82 C83 C84 0.3(12) . . . . ?
C80 C79 C84 C83 1.5(11) . . . . ?
P4 C79 C84 C83 -179.0(5) . . . . ?
C82 C83 C84 C79 -1.3(12) . . . . ?
C90 C85 C86 C87 0.7(13) . . . . ?
P5 C85 C86 C87 -173.4(7) . . . . ?
C85 C86 C87 C88 1.6(15) . . . . ?
C86 C87 C88 C89 -3.2(15) . . . . ?
C87 C88 C89 C90 2.6(13) . . . . ?
C86 C85 C90 C89 -1.3(11) . . . . ?
P5 C85 C90 C89 173.3(6) . . . . ?
C88 C89 C90 C85 -0.3(12) . . . . ?
C96 C91 C92 C93 -2.0(12) . . . . ?
P5 C91 C92 C93 174.3(6) . . . . ?
C91 C92 C93 C94 0.3(12) . . . . ?
C92 C93 C94 C95 0.8(12) . . . . ?
C93 C94 C95 C96 -0.1(13) . . . . ?
C92 C91 C96 C95 2.8(12) . . . . ?
P5 C91 C96 C95 -173.4(6) . . . . ?
C94 C95 C96 C91 -1.8(13) . . . . ?
C102 C97 C98 C99 -1.7(12) . . . . ?
P6 C97 C98 C99 178.5(7) . . . . ?
C97 C98 C99 C100 1.0(14) . . . . ?
C98 C99 C100 C101 1.1(14) . . . . ?
C99 C100 C101 C102 -2.3(13) . . . . ?
C98 C97 C102 C101 0.5(12) . . . . ?
P6 C97 C102 C101 -179.8(6) . . . . ?
C100 C101 C102 C97 1.5(13) . . . . ?
C108 C103 C104 C105 0.0(12) . . . . ?
P6 C103 C104 C105 -178.6(6) . . . . ?
C103 C104 C105 C106 1.7(13) . . . . ?
C104 C105 C106 C107 -1.5(13) . . . . ?
C105 C106 C107 C108 -0.3(14) . . . . ?
C104 C103 C108 C107 -1.9(12) . . . . ?
P6 C103 C108 C107 176.7(6) . . . . ?
C106 C107 C108 C103 2.1(13) . . . . ?
C7S C8S C9S C7S 1(2) . . . 3_657 ?
C9S C8S C7S C9S -1(2) . . . 3_657 ?
C6S C1S C2S C3S 1.3(17) . . . . ?
C1S C2S C3S C4S -0.4(18) . . . . ?
C2S C3S C4S C5S 0.4(19) . . . . ?
C3S C4S C5S C6S -1.3(19) . . . . ?
C4S C5S C6S C1S 2.1(18) . . . . ?
C2S C1S C6S C5S -2.1(17) . . . . ?
Cl1 C10S C11S Cl2 -32(6) . . . . ?
Cl3 C12S C13S Cl4 -60.0(18) . . . . ?
P8 F8 F8A F12A 35(2) . . . . ?
P8 F12 F12A F8A 41(3) . . . . ?
F8 F8A F12A F12 -84(5) . . . . ?
P8 F8A F12A F12 -44(4) . . . . ?
F8 F8A F12A P8 -40(2) . . . . ?
C38 C37 P1 C43 -108.2(6) . . . . ?
C42 C37 P1 C43 66.3(7) . . . . ?
C38 C37 P1 C1 149.3(6) . . . . ?
C42 C37 P1 C1 -36.2(7) . . . . ?
C38 C37 P1 Pt1 20.8(7) . . . . ?
C42 C37 P1 Pt1 -164.7(5) . . . . ?
C38 C37 P1 P2 80.3(6) . . . . ?
C42 C37 P1 P2 -105.2(6) . . . . ?
C48 C43 P1 C37 -173.5(6) . . . . ?
C44 C43 P1 C37 8.2(7) . . . . ?
C48 C43 P1 C1 -69.5(6) . . . . ?
C44 C43 P1 C1 112.1(6) . . . . ?
C48 C43 P1 Pt1 52.8(6) . . . . ?
C44 C43 P1 Pt1 -125.6(5) . . . . ?
C48 C43 P1 P2 -19.2(11) . . . . ?
C44 C43 P1 P2 162.5(4) . . . . ?
N1 C1 P1 C37 -92.5(6) . . . . ?
C2 C1 P1 C37 88.5(7) . . . . ?
N1 C1 P1 C43 162.8(5) . . . . ?
C2 C1 P1 C43 -16.1(7) . . . . ?
N1 C1 P1 Pt1 40.7(6) . . . . ?
C2 C1 P1 Pt1 -138.3(6) . . . . ?
N1 C1 P1 P2 -0.9(4) . . . . ?
C2 C1 P1 P2 -179.9(7) . . . . ?
P3 Pt1 P1 C37 -62.0(3) . . . . ?
P5 Pt1 P1 C37 166.6(3) . . . . ?
Hg1 Pt1 P1 C37 81.3(3) . . . . ?
Hg2 Pt1 P1 C37 26.1(3) . . . . ?
Pt2 Pt1 P1 C37 56.2(3) . . . . ?
P3 Pt1 P1 C43 61.7(3) . . . . ?
P5 Pt1 P1 C43 -69.8(3) . . . . ?
Hg1 Pt1 P1 C43 -155.0(3) . . . . ?
Hg2 Pt1 P1 C43 149.8(3) . . . . ?
Pt2 Pt1 P1 C43 179.8(3) . . . . ?
P3 Pt1 P1 C1 175.5(2) . . . . ?
P5 Pt1 P1 C1 44.0(3) . . . . ?
Hg1 Pt1 P1 C1 -41.3(2) . . . . ?
Hg2 Pt1 P1 C1 -96.4(3) . . . . ?
Pt2 Pt1 P1 C1 -66.4(3) . . . . ?
P3 Pt1 P1 P2 -139.79(6) . . . . ?
P5 Pt1 P1 P2 88.77(6) . . . . ?
Hg1 Pt1 P1 P2 3.48(2) . . . . ?
Hg2 Pt1 P1 P2 -51.68(2) . . . . ?
Pt2 Pt1 P1 P2 -21.626(17) . . . . ?
C50 C49 P2 C55 21.8(7) . . . . ?
C54 C49 P2 C55 -162.4(5) . . . . ?
C50 C49 P2 C10 122.1(6) . . . . ?
C54 C49 P2 C10 -62.1(6) . . . . ?
C50 C49 P2 Pt2 -111.7(6) . . . . ?
C54 C49 P2 Pt2 64.1(6) . . . . ?
C50 C49 P2 P1 -175.9(4) . . . . ?
C54 C49 P2 P1 -0.1(8) . . . . ?
C56 C55 P2 C49 -137.3(5) . . . . ?
C60 C55 P2 C49 46.6(6) . . . . ?
C56 C55 P2 C10 121.1(6) . . . . ?
C60 C55 P2 C10 -55.1(6) . . . . ?
C56 C55 P2 Pt2 -8.1(6) . . . . ?
C60 C55 P2 Pt2 175.8(5) . . . . ?
C56 C55 P2 P1 52.8(6) . . . . ?
C60 C55 P2 P1 -123.3(5) . . . . ?
N2 C10 P2 C49 154.7(5) . . . . ?
C9 C10 P2 C49 -27.2(7) . . . . ?
N2 C10 P2 C55 -99.2(5) . . . . ?
C9 C10 P2 C55 79.0(6) . . . . ?
N2 C10 P2 Pt2 31.7(6) . . . . ?
C9 C10 P2 Pt2 -150.1(5) . . . . ?
N2 C10 P2 P1 6.5(4) . . . . ?
C9 C10 P2 P1 -175.4(7) . . . . ?
P4 Pt2 P2 C49 -54.1(3) . . . . ?
P6 Pt2 P2 C49 76.7(3) . . . . ?
Hg2 Pt2 P2 C49 -168.1(2) . . . . ?
Hg1 Pt2 P2 C49 -153.3(2) . . . . ?
Pt1 Pt2 P2 C49 -167.0(2) . . . . ?
P4 Pt2 P2 C55 -179.3(2) . . . . ?
P6 Pt2 P2 C55 -48.4(3) . . . . ?
Hg2 Pt2 P2 C55 66.7(3) . . . . ?
Hg1 Pt2 P2 C55 81.5(2) . . . . ?
Pt1 Pt2 P2 C55 67.9(3) . . . . ?
P4 Pt2 P2 C10 61.4(3) . . . . ?
P6 Pt2 P2 C10 -167.7(2) . . . . ?
Hg2 Pt2 P2 C10 -52.6(3) . . . . ?
Hg1 Pt2 P2 C10 -37.8(2) . . . . ?
Pt1 Pt2 P2 C10 -51.5(3) . . . . ?
P4 Pt2 P2 P1 89.48(6) . . . . ?
P6 Pt2 P2 P1 -139.67(6) . . . . ?
Hg2 Pt2 P2 P1 -24.51(4) . . . . ?
Hg1 Pt2 P2 P1 -9.75(2) . . . . ?
Pt1 Pt2 P2 P1 -23.383(19) . . . . ?
C37 P1 P2 C49 24.4(5) . . . . ?
C43 P1 P2 C49 -130.4(7) . . . . ?
C1 P1 P2 C49 -75.6(5) . . . . ?
Pt1 P1 P2 C49 148.0(4) . . . . ?
C37 P1 P2 C55 -173.5(3) . . . . ?
C43 P1 P2 C55 31.7(7) . . . . ?
C1 P1 P2 C55 86.4(3) . . . . ?
Pt1 P1 P2 C55 -50.0(2) . . . . ?
C37 P1 P2 C10 95.5(3) . . . . ?
C43 P1 P2 C10 -59.3(7) . . . . ?
C1 P1 P2 C10 -4.5(3) . . . . ?
Pt1 P1 P2 C10 -140.9(2) . . . . ?
C37 P1 P2 Pt2 -57.7(2) . . . . ?
C43 P1 P2 Pt2 147.5(6) . . . . ?
C1 P1 P2 Pt2 -157.7(2) . . . . ?
Pt1 P1 P2 Pt2 65.90(6) . . . . ?
C72 C67 P3 C61 129.5(6) . . . . ?
C68 C67 P3 C61 -57.4(6) . . . . ?
C72 C67 P3 C13 28.4(7) . . . . ?
C68 C67 P3 C13 -158.5(6) . . . . ?
C72 C67 P3 Pt1 -100.8(6) . . . . ?
C68 C67 P3 Pt1 72.4(6) . . . . ?
C72 C67 P3 P4 -41.3(6) . . . . ?
C68 C67 P3 P4 131.8(5) . . . . ?
C66 C61 P3 C67 165.5(6) . . . . ?
C62 C61 P3 C67 -18.1(7) . . . . ?
C66 C61 P3 C13 -91.3(6) . . . . ?
C62 C61 P3 C13 85.0(6) . . . . ?
C66 C61 P3 Pt1 35.2(6) . . . . ?
C62 C61 P3 Pt1 -148.4(5) . . . . ?
C66 C61 P3 P4 -31.7(8) . . . . ?
C62 C61 P3 P4 144.7(5) . . . . ?
N3 C13 P3 C67 -100.0(5) . . . . ?
C14 C13 P3 C67 83.7(7) . . . . ?
N3 C13 P3 C61 154.7(5) . . . . ?
C14 C13 P3 C61 -21.6(7) . . . . ?
N3 C13 P3 Pt1 29.0(6) . . . . ?
C14 C13 P3 Pt1 -147.3(6) . . . . ?
N3 C13 P3 P4 3.5(4) . . . . ?
C14 C13 P3 P4 -172.8(7) . . . . ?
P1 Pt1 P3 C67 -176.5(3) . . . . ?
P5 Pt1 P3 C67 -43.0(3) . . . . ?
Hg1 Pt1 P3 C67 65.3(3) . . . . ?
Hg2 Pt1 P3 C67 82.0(3) . . . . ?
Pt2 Pt1 P3 C67 67.9(3) . . . . ?
P1 Pt1 P3 C61 -53.2(3) . . . . ?
P5 Pt1 P3 C61 80.3(3) . . . . ?
Hg1 Pt1 P3 C61 -171.4(2) . . . . ?
Hg2 Pt1 P3 C61 -154.7(2) . . . . ?
Pt2 Pt1 P3 C61 -168.8(2) . . . . ?
P1 Pt1 P3 C13 62.9(3) . . . . ?
P5 Pt1 P3 C13 -163.7(2) . . . . ?
Hg1 Pt1 P3 C13 -55.3(3) . . . . ?
Hg2 Pt1 P3 C13 -38.6(2) . . . . ?
Pt2 Pt1 P3 C13 -52.8(3) . . . . ?
P1 Pt1 P3 P4 91.70(6) . . . . ?
P5 Pt1 P3 P4 -134.85(6) . . . . ?
Hg1 Pt1 P3 P4 -26.49(4) . . . . ?
Hg2 Pt1 P3 P4 -9.79(3) . . . . ?
Pt2 Pt1 P3 P4 -23.94(2) . . . . ?
C84 C79 P4 C73 -109.6(6) . . . . ?
C80 C79 P4 C73 69.9(7) . . . . ?
C84 C79 P4 C22 145.9(6) . . . . ?
C80 C79 P4 C22 -34.7(7) . . . . ?
C84 C79 P4 Pt2 20.4(6) . . . . ?
C80 C79 P4 Pt2 -160.2(6) . . . . ?
C84 C79 P4 P3 77.2(5) . . . . ?
C80 C79 P4 P3 -103.3(7) . . . . ?
C74 C73 P4 C79 171.4(6) . . . . ?
C78 C73 P4 C79 -6.7(8) . . . . ?
C74 C73 P4 C22 -87.0(6) . . . . ?
C78 C73 P4 C22 95.0(7) . . . . ?
C74 C73 P4 Pt2 37.3(7) . . . . ?
C78 C73 P4 Pt2 -140.8(7) . . . . ?
C74 C73 P4 P3 -30.4(12) . . . . ?
C78 C73 P4 P3 151.5(6) . . . . ?
N4 C22 P4 C79 -93.2(6) . . . . ?
C21 C22 P4 C79 85.4(7) . . . . ?
N4 C22 P4 C73 160.8(5) . . . . ?
C21 C22 P4 C73 -20.6(7) . . . . ?
N4 C22 P4 Pt2 36.9(6) . . . . ?
C21 C22 P4 Pt2 -144.5(6) . . . . ?
N4 C22 P4 P3 -2.7(4) . . . . ?
C21 C22 P4 P3 175.8(7) . . . . ?
P2 Pt2 P4 C79 -64.0(3) . . . . ?
P6 Pt2 P4 C79 162.7(3) . . . . ?
Hg2 Pt2 P4 C79 77.9(3) . . . . ?
Hg1 Pt2 P4 C79 21.8(3) . . . . ?
Pt1 Pt2 P4 C79 52.5(3) . . . . ?
P2 Pt2 P4 C73 61.2(3) . . . . ?
P6 Pt2 P4 C73 -72.0(3) . . . . ?
Hg2 Pt2 P4 C73 -156.9(3) . . . . ?
Hg1 Pt2 P4 C73 147.0(3) . . . . ?
Pt1 Pt2 P4 C73 177.7(3) . . . . ?
P2 Pt2 P4 C22 178.4(3) . . . . ?
P6 Pt2 P4 C22 45.2(3) . . . . ?
Hg2 Pt2 P4 C22 -39.7(3) . . . . ?
Hg1 Pt2 P4 C22 -95.8(3) . . . . ?
Pt1 Pt2 P4 C22 -65.1(3) . . . . ?
P2 Pt2 P4 P3 -138.48(6) . . . . ?
P6 Pt2 P4 P3 88.31(5) . . . . ?
Hg2 Pt2 P4 P3 3.42(2) . . . . ?
Hg1 Pt2 P4 P3 -52.67(2) . . . . ?
Pt1 Pt2 P4 P3 -21.955(18) . . . . ?
C67 P3 P4 C79 -166.6(3) . . . . ?
C61 P3 P4 C79 30.9(5) . . . . ?
C13 P3 P4 C79 98.3(3) . . . . ?
Pt1 P3 P4 C79 -54.2(2) . . . . ?
C67 P3 P4 C73 34.6(8) . . . . ?
C61 P3 P4 C73 -127.9(9) . . . . ?
C13 P3 P4 C73 -60.5(8) . . . . ?
Pt1 P3 P4 C73 146.9(8) . . . . ?
C67 P3 P4 C22 96.0(3) . . . . ?
C61 P3 P4 C22 -66.6(5) . . . . ?
C13 P3 P4 C22 0.8(3) . . . . ?
Pt1 P3 P4 C22 -151.7(2) . . . . ?
C67 P3 P4 Pt2 -42.1(2) . . . . ?
C61 P3 P4 Pt2 155.4(4) . . . . ?
C13 P3 P4 Pt2 -137.2(2) . . . . ?
Pt1 P3 P4 Pt2 70.24(6) . . . . ?
N5 C25 P5 C91 -94.7(6) . . . . ?
C26 C25 P5 C91 83.6(7) . . . . ?
N5 C25 P5 C85 157.8(5) . . . . ?
C26 C25 P5 C85 -23.9(7) . . . . ?
N5 C25 P5 Pt1 32.0(6) . . . . ?
C26 C25 P5 Pt1 -149.6(6) . . . . ?
N5 C25 P5 P6 -3.1(4) . . . . ?
C26 C25 P5 P6 175.3(7) . . . . ?
C96 C91 P5 C25 -147.5(7) . . . . ?
C92 C91 P5 C25 36.3(7) . . . . ?
C96 C91 P5 C85 -42.7(8) . . . . ?
C92 C91 P5 C85 141.1(6) . . . . ?
C96 C91 P5 Pt1 86.2(7) . . . . ?
C92 C91 P5 Pt1 -90.0(6) . . . . ?
C96 C91 P5 P6 144.1(7) . . . . ?
C92 C91 P5 P6 -32.1(6) . . . . ?
C90 C85 P5 C25 -97.8(6) . . . . ?
C86 C85 P5 C25 76.4(7) . . . . ?
C90 C85 P5 C91 156.5(6) . . . . ?
C86 C85 P5 C91 -29.3(8) . . . . ?
C90 C85 P5 Pt1 27.6(6) . . . . ?
C86 C85 P5 Pt1 -158.3(6) . . . . ?
C90 C85 P5 P6 -42.3(10) . . . . ?
C86 C85 P5 P6 131.9(7) . . . . ?
P3 Pt1 P5 C25 52.0(3) . . . . ?
P1 Pt1 P5 C25 -171.2(3) . . . . ?
Hg1 Pt1 P5 C25 -88.1(3) . . . . ?
Hg2 Pt1 P5 C25 -40.9(3) . . . . ?
Pt2 Pt1 P5 C25 -61.5(3) . . . . ?
P3 Pt1 P5 C91 171.3(3) . . . . ?
P1 Pt1 P5 C91 -51.9(3) . . . . ?
Hg1 Pt1 P5 C91 31.2(3) . . . . ?
Hg2 Pt1 P5 C91 78.5(3) . . . . ?
Pt2 Pt1 P5 C91 57.8(3) . . . . ?
P3 Pt1 P5 C85 -65.6(3) . . . . ?
P1 Pt1 P5 C85 71.2(3) . . . . ?
Hg1 Pt1 P5 C85 154.3(3) . . . . ?
Hg2 Pt1 P5 C85 -158.5(3) . . . . ?
Pt2 Pt1 P5 C85 -179.1(3) . . . . ?
P3 Pt1 P5 P6 90.49(5) . . . . ?
P1 Pt1 P5 P6 -132.71(6) . . . . ?
Hg1 Pt1 P5 P6 -49.61(2) . . . . ?
Hg2 Pt1 P5 P6 -2.34(3) . . . . ?
Pt2 Pt1 P5 P6 -22.980(18) . . . . ?
C102 C97 P6 C103 156.2(6) . . . . ?
C98 C97 P6 C103 -24.1(7) . . . . ?
C102 C97 P6 C34 -99.8(6) . . . . ?
C98 C97 P6 C34 79.9(7) . . . . ?
C102 C97 P6 Pt2 29.1(7) . . . . ?
C98 C97 P6 Pt2 -151.2(6) . . . . ?
C102 C97 P6 P5 -38.7(10) . . . . ?
C98 C97 P6 P5 141.0(6) . . . . ?
C108 C103 P6 C97 128.5(6) . . . . ?
C104 C103 P6 C97 -53.0(6) . . . . ?
C108 C103 P6 C34 24.1(7) . . . . ?
C104 C103 P6 C34 -157.3(6) . . . . ?
C108 C103 P6 Pt2 -105.5(6) . . . . ?
C104 C103 P6 Pt2 73.1(6) . . . . ?
C108 C103 P6 P5 -45.2(6) . . . . ?
C104 C103 P6 P5 133.4(6) . . . . ?
N6 C34 P6 C97 160.2(5) . . . . ?
C33 C34 P6 C97 -14.7(7) . . . . ?
N6 C34 P6 C103 -96.9(5) . . . . ?
C33 C34 P6 C103 88.2(7) . . . . ?
N6 C34 P6 Pt2 32.5(6) . . . . ?
C33 C34 P6 Pt2 -142.4(6) . . . . ?
N6 C34 P6 P5 3.6(4) . . . . ?
C33 C34 P6 P5 -171.3(7) . . . . ?
P2 Pt2 P6 C97 -57.8(3) . . . . ?
P4 Pt2 P6 C97 75.8(3) . . . . ?
Hg2 Pt2 P6 C97 159.8(3) . . . . ?
Hg1 Pt2 P6 C97 -157.5(3) . . . . ?
Pt1 Pt2 P6 C97 -176.0(3) . . . . ?
P2 Pt2 P6 C103 -175.6(3) . . . . ?
P4 Pt2 P6 C103 -42.1(3) . . . . ?
Hg2 Pt2 P6 C103 42.0(3) . . . . ?
Hg1 Pt2 P6 C103 84.7(3) . . . . ?
Pt1 Pt2 P6 C103 66.2(3) . . . . ?
P2 Pt2 P6 C34 62.9(3) . . . . ?
P4 Pt2 P6 C34 -163.5(3) . . . . ?
Hg2 Pt2 P6 C34 -79.5(3) . . . . ?
Hg1 Pt2 P6 C34 -36.8(3) . . . . ?
Pt1 Pt2 P6 C34 -55.3(3) . . . . ?
P2 Pt2 P6 P5 94.85(6) . . . . ?
P4 Pt2 P6 P5 -131.57(6) . . . . ?
Hg2 Pt2 P6 P5 -47.52(2) . . . . ?
Hg1 Pt2 P6 P5 -4.80(3) . . . . ?
Pt1 Pt2 P6 P5 -23.332(19) . . . . ?
C25 P5 P6 C97 -65.7(6) . . . . ?
C91 P5 P6 C97 34.9(6) . . . . ?
C85 P5 P6 C97 -126.7(8) . . . . ?
Pt1 P5 P6 C97 151.8(6) . . . . ?
C25 P5 P6 C103 99.2(3) . . . . ?
C91 P5 P6 C103 -160.2(3) . . . . ?
C85 P5 P6 C103 38.2(7) . . . . ?
Pt1 P5 P6 C103 -43.3(2) . . . . ?
C25 P5 P6 C34 2.5(4) . . . . ?
C91 P5 P6 C34 103.1(3) . . . . ?
C85 P5 P6 C34 -58.5(7) . . . . ?
Pt1 P5 P6 C34 -140.0(3) . . . . ?
C25 P5 P6 Pt2 -147.0(3) . . . . ?
C91 P5 P6 Pt2 -46.4(3) . . . . ?
C85 P5 P6 Pt2 152.0(6) . . . . ?
Pt1 P5 P6 Pt2 70.50(6) . . . . ?
F12 F12A P8 F10A -95(2) . . . . ?
F8A F12A P8 F10A 111.3(19) . . . . ?
F12 F12A P8 F7 -15(2) . . . . ?
F8A F12A P8 F7 -168.4(14) . . . . ?
F12 F12A P8 F8A 154(2) . . . . ?
F12 F12A P8 F11 169.7(15) . . . . ?
F8A F12A P8 F11 16(3) . . . . ?
F12 F12A P8 F7A -19(2) . . . . ?
F8A F12A P8 F7A -172.8(12) . . . . ?
F12 F12A P8 F9 75.8(18) . . . . ?
F8A F12A P8 F9 -77.9(12) . . . . ?
F12 F12A P8 F10 -109(2) . . . . ?
F8A F12A P8 F10 96.9(18) . . . . ?
F12 F12A P8 F8 173.4(19) . . . . ?
F8A F12A P8 F8 19.7(14) . . . . ?
F8A F12A P8 F12 -154(2) . . . . ?
F10 F10A P8 F12A -141(7) . . . . ?
F10 F10A P8 F7 107(6) . . . . ?
F10 F10A P8 F8A -95(6) . . . . ?
F10 F10A P8 F11 11(6) . . . . ?
F10 F10A P8 F7A 88(6) . . . . ?
F10 F10A P8 F9 174.9(19) . . . . ?
F10 F10A P8 F8 -54(6) . . . . ?
F10 F10A P8 F12 178(6) . . . . ?
F8 F8A P8 F12A 149(2) . . . . ?
F8 F8A P8 F10A 85.0(17) . . . . ?
F12A F8A P8 F10A -64.4(17) . . . . ?
F8 F8A P8 F7 180(3) . . . . ?
F12A F8A P8 F7 30(3) . . . . ?
F8 F8A P8 F11 -23.4(15) . . . . ?
F12A F8A P8 F11 -172.8(13) . . . . ?
F8 F8A P8 F7A -134(11) . . . . ?
F12A F8A P8 F7A 76(11) . . . . ?
F8 F8A P8 F9 -108.4(14) . . . . ?
F12A F8A P8 F9 102.2(13) . . . . ?
F8 F8A P8 F10 61.4(18) . . . . ?
F12A F8A P8 F10 -88.0(17) . . . . ?
F12A F8A P8 F8 -149(2) . . . . ?
F8 F8A P8 F12 166.1(15) . . . . ?
F12A F8A P8 F12 16.6(15) . . . . ?
F10A F10 P8 F12A 37(6) . . . . ?
F10A F10 P8 F7 -73(6) . . . . ?
F10A F10 P8 F8A 87(6) . . . . ?
F10A F10 P8 F11 -169(6) . . . . ?
F10A F10 P8 F7A -91(6) . . . . ?
F10A F10 P8 F9 -173(3) . . . . ?
F10A F10 P8 F8 124(6) . . . . ?
F10A F10 P8 F12 -2(6) . . . . ?
F8A F8 P8 F12A -23.1(16) . . . . ?
F8A F8 P8 F10A -97.5(16) . . . . ?
F8A F8 P8 F7 -180(100) . . . . ?
F8A F8 P8 F11 155.1(16) . . . . ?
F8A F8 P8 F7A 173.2(12) . . . . ?
F8A F8 P8 F9 72.4(13) . . . . ?
F8A F8 P8 F10 -116.8(17) . . . . ?
F8A F8 P8 F12 -17.7(19) . . . . ?
F12A F12 P8 F10A 76(2) . . . . ?
F12A F12 P8 F7 165(2) . . . . ?
F12A F12 P8 F8A -20(2) . . . . ?
F12A F12 P8 F11 -162(3) . . . . ?
F12A F12 P8 F7A 165(2) . . . . ?
F12A F12 P8 F9 -104.5(19) . . . . ?
F12A F12 P8 F10 77(2) . . . . ?
F12A F12 P8 F8 -8(2) . . . . ?
